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GC-2010 Pro
GC-2010 Pro
Shimadzu Gas Chromatograph
The GC-2010 Pro represents a new generation in Routine GC. Fast oven heating and cooling reduces the
analysis time and allow high sample throughput. Based on GC-2010 Plus™ technology, it combines easy
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Achieving excellent reproducibility
All units including the column oven, flow controller and sample
injection unit are comprehensively optimized at the design stage
to achieve world-class repeatability of peak area and peak height.
The large vaporization capacity ensures excellent repeatability,
even when using solvents that are highly volatile upon injection,
such as acetone. Long-term stability of retention time is realized by
the new room compensation technology built into the advanced
flow controller (AFC).
High-speed analysis
High-speed analysis with narrow bore capillary columns reduces analysis time and improves sample throughput. GC-2010 Pro has
excellent flow and pressure control system, which can meet the requirements of rapid analysis with conventional configuration and
effectively improve the analysis efficiency.
DB-WAX
0.25mm×60m, 0.25µm
( He 25cm/s )
6 12
Rtx-WAX
0.1mm×20m, 0.1µm
( He 25cm/s )
20 minutes
Analysis time reduced by GC-2010 Pro
3 5
GC-2010 Pro
Capillary Gas Chromatograph 5
Rapid oven heating / cooling
GC-2010 Pro incorporates a double-jet cooling system, which enables the reduction of cooling time from 450℃ to 50℃
in 3.4min, realizing more efficient and rapid cooling. In addition, with the ability of rapid heating, GC-2010 Pro can
significantly reduce the analysis time.
Column oven temperature (℃)
450
Large fan rapidly
discharges hot air 400
GC-2010
350
Pro
GC-2010 Pro
300
250
Small fan added to Significant reduction
enhance efficiency of 200 of cooling time
cooling air intake 150
100
3.4 min
50
0
0 1 2 3 4 5 6
Time (minutes)
Approx.
3 min
12.5 min 2.7min
Cooling Equilibrium To next analysis
time time
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Constant linear velocity mode quickly determines separation conditions
The constant linear velocity mode related to the separation performance is recommended for the carrier gas control and
can obtain the optimum separation conditions in the shortest time compared with the previous control method by setting
the column inlet pressure and flow.
Constant column inlet pressure
[Conditions of Analysis]
1.Pencycuron Column: SH-Rtx column 30m X 0.32mm i.d.df=0.25 μm
2.Benfluralin Column temperature: 60℃(1 min)-7℃/min-230℃
3.Propyzamide Injection port temperature: 240℃
4.Diazinon Detector temperature: 270℃ (FID)
Carrier gas: He
5.Fenitrothion(MEP)
Carrier gas linear velocity: 40cm/sec, column inlet pressure 44.0kPa
6.Chlorpyrifos Injection volume: 1 μL (splitless analysis)
1.Pencycuron
2.Benfluralin
3.Propyzamide
4.Diazinon
5.Fenitrothion(MEP)
6.Chlorpyrifos
Comparison of chromatograms with constant linear velocity and constant column inlet pressure
(Pesticides analysis)
200
Helium consumption [mL]
2000
Carrier gas saver function example Analysis time: 30min split ratio: 100
Carrier gas saver function: split ratio 10 one minute later
Column temperature: 170℃
In this example, the split flow is set to 200mL/min only upon injection and in the remaining time, Chromatographic column: inner diameter 0.25mm
the split ratio is reduced to 20mL/min to save carrier gas consumption. The carrier gas saving length 30m film thickness 0.25μm
mode is maintained after the end of batch processing analysis until the beginning of the next
Comparison of helium consumption for one analysis
batch processing analysis. using and not using carrier gas saver function
GC-2010 Pro
Capillary Gas Chromatograph 7
Industry Leading Detector Sensitivity
Responding to the ever increasing demands for trace level analysis, all detectors
of GC-2010 Pro realize high sensitivity in miniaturization design. The new flame
photometric detector (FPD) and flame ionization detector (FID) show significantly
increased sensitivity.
High-sensitivity has been achieved by thorough cleaning of detector gas lines and the latest noise-reduction technology.
·FID ( without noise reduction technology) ·FID ( with noise reduction technology)
C12 C12
C14
C14
C16
C16
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Flame photometric detector FPD
It achieves compact design and improves the flame stability by improving the nozzle form. In addition, the
"dual-focus system" achieves excellent ultra high sensitivity. The dual-focus system adds a lens to the inter-
ference filter for efficient light collection at the photomultiplier light receptor.
Lens
Photomultiplier
Nozzle
Dual-focus system
Benzene
CS2
Benzene
Thiophene
Thiophene
GC-2010 Pro
Capillary Gas Chromatograph 9
Options enhancing scalability
For detector
*Only two analytical lines could be running simultaneously. 7 3
6 2
5 1
In order to obtain good data, it is necessary to select an appropriate injection method according to the analysis purpose and sample.
GC-2010 Pro can select the most suitable injection method from three injection units.
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Small and high-sensitivity detector series
The full range of high-sensitivity detectors supports a wide variety of application analyses.
Each detector is equipped with an advanced pressure controller (APC) that digitally sets the gas parameters of each
detector. To ensure secure use of hydrogen the connector joints have reverse threads to prevent incorrect pipe connec-
tions (FID, FPD, FTD).
23
10
8
3:Hexachlorobenzene
6
5
11
12
9
14
1
13
3 4:γ-BHC
15
5:Heptachlor
6:Dichloropropionic acid
2.5 5.0 7.5 10.0 12.5 min
7.0 8.0 9.0 10.0 11.0 12.0 13.0 14.0 min 7:Heptachlor-exo-epoxide
Analysis of aqueous solution of medicine residual solvent Analysis of 10ppb of organochlorine pesticides 8:Heptachlor epoxide A+
USP467 Class1 ProcedureA oxychlordane isomer
9:Chlordane-cis
10:Chlordane-trans
For analysis of 11:Dieldrin
Thermal conductivity detector inorganic gases and
12:Endrin
13:o, p'-DDT
concentrated organic 14:p, p'-DDT
TCD compounds 15:Dicofol
GC-2010 Pro
Capillary Gas Chromatograph 11
Advanced flow technology
Advanced flow technology is a capillary analysis system implementing chromatographic techniques like backflush, heart
cut, and detector switching.
It can achieve high efficiency and high separation by improving the efficiency of analysis and accurately separating the
target component from the complex original samples.
Special software for each system can be downloaded free of charge from the homepage of Shimadzu official website.
The backflush system reverses the carrier gas flow after the target compounds have eluted, to discharge residual late eluting com-
pounds in the column through the injection port split vent, thus shortening the analysis time and improving productivity. In addition,
high-boiling point components are discharged efficiently to reduce the bakeout time and thus prevent column deterioration, contamina-
tion and retention time shifts.
Target component Unnecessary (high-boiling point) component
Injector Detector
Chromatographic Damper
column tube
8 min
Backflush
analysis time shortened from about 22min to device
Low boiling point
High boiling point component
Backflush analysis component
2.5 5.0 7.5 10.0 12.5 15.0 17.5 20.0 22.5 min Schematic diagram of backflush system
Analysis of ethanol in solution
(comparison between conventional analysis and backflush analysis)
The heart cutting system uses two chromatographic columns Injector 1st column 2nd detector
Switching unit
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Advanced flow technology - detector splitting system
Detector
Chromatographic
column
Simultaneous analysis of grape seed oil with detector splitting system (FID, FTD, FPD)
Detector
The detector switching system controls sample introduction Injector 1st detector 2nd detector
GC-2010 Pro
Capillary Gas Chromatograph 13
Efficient workstation LabSolutions
meeting customer needs
The LabSolutions series is the next-generation workstation software that integrates GC control, LC control, and other
improvements in functionality, while maintaining compatibility with GC solution products. LabSolutions offers sophisticat-
ed functionality and easy operation.
・LabSolutions CS
User-friendly interface
Fast batch function simplifies the tedious process of creating sample injection sequence (batch file)
The fast batch function in LabSolutions makes it easy to
create batch files. The fast batch window displays the sample
bottle racks graphically in the system. The operator can
directly confirm the location of the sample bottle through the
window, so as to create the batch file faster and more
accurately.
Fast batch window of LabSolutions The figure corresponds to the position of the actual sample disk
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LabSolutions CS: free access to the analysis network
*2 *3
Client PC Laboratory or office iPad LabSolutions server
*1
Collection
control PC
GCMS AA TOC Grain size analysis ICP Thermal analysis EDX CBM-201m Non-Shimadzu
LC/GC unit
Multi-data registration license is used to realize instrument and data integration management.
*1 The collection control PC is used to control the analysis device. Like the client PC, it can also execute analytical instructions and data reanalysis.
*2 LabSolutions software is not required on the client PC when using terminal services.
*3 If an iPad is used, then XenApp from Citrix must be installed.
GC-2010 Pro
Capillary Gas Chromatograph 15
Customized analysis systems
based on different analysis requirements
All kinds of accessories are available for GC analysis
Analysis applications
Measurement of residual solvents in pharmaceuticals
Measurement of flavor components in foods
System configuration
GC-2010 Pro + HS-10
Analysis applications
Analysis of residual solvents
Blood alcohol
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Liquid injection/headspace/SPME analysis system Dual tower injection system
Liquid, large volume, headspace and SPME injection in one The AOC-20 series includes a dual tower auto injector option
single instrument. Used to analyze the volatile components in which doubles the productivity of a single dual injector, dual
solid or liquid samples. detector gas chromatograph.
System configuration The hignest productivity is then assured for applications
GC-2010 Pro + AOC-6000
such as simple hign sample throughput on identical GC
analysis channels or for dual column confirmation. In either
Analysis applications case, the AOC-20 dual tower configration is a powerful tool
Measurement of residual solvents in pharmaceuticals
for laboratory productivity.
Measurement of flavor components in foods
System configuration
* Appended software package
GC-2010 Pro + Dual tower AOC-20i
Decomposes samples at high temperatures and analyzes the Measure the boiling point distribution of petroleum fractions
pyrolytic decomposition products. using the relationship between retention time and boiling
System configuration point. Print formatted reports after analysis of distillation
GC-2010 Pro + EGA/PY-3030D
characteristics.
autosampler and cryotrap accessories available System configuration
GC-2010 Pro +WBI or OCI + LabSolutions + simulated distillation software
Analysis applications
Characterization of high molecular weight compounds Analysis applications
Measurement of outgassing from inorganic samples, such as ceramics Petroleum fractions
* Some ASTM standards are not supported when using LabSolutions LE
GC-2010 Pro
Capillary Gas Chromatograph 17
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GC-2010 Pro
Capillary Gas Chromatograph 19
GC-2010 Pro
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