JIS JAPANESE INDUSTRIAL STANDARD Translated and Published by Japanese Standards Association JIS K 6256-1: (IRMA/JSA) Rubber, vulcanized or thermoplastic — Determination of adhesion test— Part 1: Adhesion to textile fabric ICS 59,080.40; 83.060 Reference number : JIS K 6256-1 : 2006 (E) PROTECTED BY COPYRIGHT 78 awe | a) Gay ? ss a 1 poste coc era Te ota Po aoa K 6256-1: 2006 Foreword This translation has been made based on the original Japanese Industrial Standard established by the Minister of Economy, Trade and Industry through deliberations at the Japanese Industrial Standards Committee according to the proposal of establishing a Japanese Industrial Standard from The Japan Rubber Manufacturers Association (JRMA)/Japanese Standards Association (JSA) with a draft being attached, based on the provision of Article 12 Clause 1 of the Industrial Standardization Law. JIS K 6256, which was prepared based on three relevant International Standards, have been reestablished at this time as three separate parts in order to be in accordance with the International Standard, Consequently, JIS K 6256: 1999 is withdrawn and replaced with JIS K 6256-1, JIS K 6256-2 and JIS K 6256-3, This Standard has been prepared based on ISO 36:2005 Rubber, vulcanized or thermoplastic—Determination of adhesion to textile fabrics for the purposes of making it easier to compare this Standard with International Standard; to prepare Japanese Industrial Standard conforming with International Standard; and to propose a draft of an International Standard which is based on Japanese Industrial Standard. Attention is drawn to the possibility that some parts of this Standard may confliet with a patent right, application for a patent after opening to the public, utili right or application for registration of utility model after opening to the pub! have technieal properties. The relevant Minister and the Japanese Industrial Standards Committee are not responsible for identifying the patent right, application for a patent after opening to the public, utility model right or application for registration of utility model after opening to the publie which have the said technical properties. SIS K 6256 consists of the following 3 parts under the general time “Rubber, vulcanized or thermoplastie—Determination of adhesion test” Part 1: Adhesion to textile fabric Part 2 :Adhesion to a rigid substrate—90° peel method Part 3: Adhesion to metal—Two-plate method Date of Establishment: 2006-12-20 Date of Public Notice in Official Gazette: 2006-12-20 Investigated by: Japanese Industrial Standards Committee Standards Board Technical Committee on Chemical Products JIS K 6256-1:2006, First English edition published in 2007-07 ‘Translated and published by: Japanese Standards Association 4-1-24, Akasaka, Minato-ku, Tokyo, 107-8440 JAPAN In the event of any doubts arising as to the contents, the original JIS is to be the final authority © JSa 2007 Al rights reserved. Unless otherwise spe 1d, no part of this publication may be eproduced or Utilized in any form oF by any means, electronic or mechanical, including photocopying and rnierofilm, without permission in writing from the publisher. Printed in Japan NHIAT PROTECTED BY COPYRIGHT ea — a > 1 porte al rere Panay K 6256-1 2006 Contents Page Introduction .... 1 1 Scope 1 2 Normative references... 2 3 Terms and definitions 2 4 Principle... 2 8) *owbsamacttfise sscnesssnseneanetstntoteantinttsnntntsetien 6 Test piece... 3 6.1 Test piece shape and dimensions .. 3 6.2 Test piece sampling and preparation 3 7 Number of test pieces . 4 8 Test method 4 8.1 Test conditions 4 82 Procedure 4 9 Caleulation cision . 4 10 Expression of test results... 5 10.1 Adhesion strength .... . . 5 10.2 Expression of type of separation or failure .. 5 A, TasSR eG ara arecrear sarecemeescira ranean cee ea RaRrara 5 Annex (informative) Comparison table between JIS and corresponding International Standard . 6 @ PROTECTED BY COPYRIGHT JAPANESE INDUSTRIAL STANDARD JIS K 6256-1: 2006 L Rubber, vulcanized or thermoplastic— Determination of adhesion test— Part 1: Adhesion to textile fabric introduction This Japanese Industrial Standard has been prepared based on the fourth edition of ISO 86 Rubber, vulcanized or thermoplastic—Determination of ad- hesion to textile fabrics published in 2005 with some modification of the technical c ontents, ‘The portions underlined with dots are the matters in which the contents of the original International Standard have been modified. A list of modifications with ex- planations is given in Annex. WARNING: Persons using this Standard should be familiar with normal labora- tory practice. This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user to establish appropriate safety and health practices and to ensure compliance with any national regulatory conditions. 1 Seope This part of JIS K 6256 specifies a method of test for measuring the force required to separate, by stripping, two plies of fabric bonded with rubber, or a rubber layer and a fabric ply bonded together. u ‘The method is applicable when the ply surfaces are approximately plane or when hey are in the form of a cylinder having an internal diameter greater than approxi- mately 50 mm. The method is not applicable when the ply surfaces contain sharp bends, angles or other gross irregularities which cannot be excluded when cutting out test pieces. This part of JIS K 6256 does not apply to coated fabrics, which are tested in accordance with ISO 2411:2000 Rubber-or plastics-coated fabries—Determination of ef ‘oating adhesion, or textile conveyor belts, which are tested in accordance with ISO 252-1: 1999 Textile conveyor belts—Adhesive strength between constitutive elements— Part 1: Methods of test. NOTE: The International Standard corresponding to this Standard is as fol- lows. In addition, the symbols which denote the degree of correspondence in the contents between JIS and the relevant International Standard are IDT (identical), MOD (modified) and NEQ (not equivalent) accord- ing to ISOMTEC Guide 21. ISO 36:2005 Rubber, vulcanized or thermoplastic—Determination of adhesion to textile fabrics (MOD) Information : For adhesion test for hose products, JIS K 6330-6 (Testing methods for rubber and plastics hoses—Part 6: Determination of adhesion between components) should be referred to. PROTECTED BY COPYRIGHT are ‘esi pote ae pac 2 K 6256-1: 2006 2 Normative references The following standards contain provisions which, through reference in this text, constitute provisions of this Standard. The most recent edi- tions of the standards (including amendments) indicated below shall be applied. JIS K 6200 Rubber—Vocabulary JIS K 6250 Rubber—General procedures for preparing and conditioning test pieces for physical test methods NOTE: ISO 28529: 2004 Rubber—General procedures for preparing and con- ditioning test pieces for physical test methods is equivalent to the said standard ISO 28529: 2004, in its establishment, has integrated ISO 471: 1995, 180 3883: 1985, 150 4648: 1991 and ISO 4661-1: 1993. JIS K 6272 Rubber—Tensile, flexural and compression test equipment (constant rate of traverse)—Specification NOTE: ISO 5893:2002 Rubber and plastics test equipment—Tensile, flexural and compression types (constant rate of traverse)—Specification is equivalent to the said standard, Informatio! JIS K 6274 Rubber and plastics—Analysis of multi-peak traces obtained in de- terminations of tear strength and adhesion strength NOTE: ISO 6133:1998 Rubber and plastics—Analysis of multi-peak traces obtained in determinations of tear strength and adhesion strength is identical to the said standard. JIS Z 8401. Guide to the rounding of numbers 3 Terms and definitions For the purposes of this document, the terms and defi- nitions given in JIS K 6200 and the following apply a) adhesion strength force per unit width required to cause a separation at the interface between the assembled components(") Note (!) Any separation occurring at any other point, for example inside either component under test, is a failure of the component material, and does not indicate an adhesion strength. In such cases, the adhesion strength is greater than the strength of the weakest component involved. There fore, it is important in this test that the condition of fracture of the separated surface is observed together with the determination of the adhesion strength, and the evaluation is carried out taking into con- sideration the separation and fracture types as shown in 10.2 4 Principle The stripping force required to separate two plies of fabric bonded with rubber, or a rubber layer and a fabric ply bonded together, is measured under speci- fied conditions using test pieces of standard dimensions in the form of a flat strip. 5 Test machine The test machine, specified in JIS K 6272, power-driven and equipped with a suitable dynamometer, shall be capable of maintaining a substan- tially constant rate of traverse of the moving head during the test. PROTECTED BY COPYRIGHT 3 K 6256-1: 2006 The machine shall be fitted with grips capable of holding the test piece and the ply to be separated without slipping during the test. a) Dynamometer An inertialess dynamometer (of the electronie or optical type, for example) should preferably be used. It shall be capable of measuring force with an accuracy at least Class 2 as defined in clause 4 of JIS K 6272. b) Autographie recorder, with a scale sufficiently large to permit easy interpre- tation of the trace, or computer with graphic capabilities and software enabling it to comply with the procedure for data processing described in JIS K 6274. 6 Test piece 6.1 Test piece shape and dimensions The test piece shall have a width of 25.0 mm £0.5 mm and shall be of sufficient length to permit ply separation during measure- ment over a length of at least 100 mm (at least 150 mm is required if the length of the grip part, which is approximately 50 mm, is considered). ‘The minimum thickness of the constituent components, or of one of them, shail be such that the weakest com- ponent can transmit the force necessary for separation without breaking. 6.2. Test piece sampling and preparation The sampling and preparation of test piece shall be as follows. a) The test piece shall be cut in the specified dimensions, the longitudinal direction of the cut surface being parallel to warp and transverse direction, to weft, When a part of yarn gets scraped off by the cutting due to the irregularity of yarn di- rection even if the cut is precisely in parallel to the weft or to the warp, the test, Piece shall have a little greater width, except for the ply to be separated which shall have the specified width of 25 mm. b) The thickness shall be suitably reduced as specified in 8.2 of JIS K 6250, if necessary, in order to ensure that the line of separation of the plies during the test: lies as close as possible to the plane (180°) of the strips of test piece held in the grips (see figure 1, Cdeal)). For tests intended to be comparable, the test pieces shall have the same dimensions. ==> Tension axis < Line of separation Line of separation Figure 1 Position of line of separation of plies c) Whenever possible, the standard test piece shall be cut from the article and prepared in accordance with the relevant product standard, if one exists, PROTECTED BY COPYRIGHT FI? = IA a oss oa POPP ey 4 K 6256-1 : 2006 7 Number of test pieces Unless otherwise specified, three test pieces shall be tested 8 Test method 8.1 Test conditions The test conditions shall be as follows. a) The standard temperature in the laboratory shall be as specified in 6.1 of JIS K 6250. If the standard humidity in the laboratory needs to be controlled, 6.2 of JIS K 6250 shall be referred to. b) The storage of specimen and test pieces shall be as specified in clause 7 of JIS K 6250. ©) The conditioning of test piece shall be as specified in clause 9 of JIS K 6250. If the separation of test pieces requires buffing, the interval between buffing and testing shall be not less than 16 h and not greater than 72h, d) The standard laboratory temperature shall be as specified in 11.2.1 of JIS K 6250. For the test at temperature other than above, select it from the specifi- cation in 11.2.2 of JIS K 6250. 8.2 Procedure ‘Take the test piece as described in 6.2 and separate a ply of fabric or a rubber layer by hand for a distance of approximately 50 mm. The use of a scal- pel or similar implement may be necessary to initiate the separation. Fix the sepa- rated ends of the test piece in the grips of the test machine (clause 5), and adjust so that the tension is distributed uniformly and so that no twisting of the test piece will oceur during the test. Place the body of the test piece in the non-driven grip and the ply to be separated in the power-driven grip so that the angle of separation is approxi- mately 180° as shown in figure 1, It is important to ensure that the strips of test piece held in the grips lie in the same plane. ‘The rate of travel of the power-driven grip shall be 50.0 mm/min+5.0 mm/min. Over a length separation of at least 100 mm, the wavy curve of adhesion strength shall be recorded. ‘The adhesion strength shall be ob- tained from this wavy curve in accordance with the specification of JIS K 6274. Information: When it is not the interface separation at the adhesion part but tears are produced in vuleanized rubber layer or thermoplastic rub- ber layer during the test, a cul is given in order to obtain the adhesion strength of interface at the adhesion part and the test should be continued again after it recovers to the interface sepa- ration at the adhesion part. In such a case, the recorded values of tears of vulcanized rubber layer or thermoplastie rubber layer shall be excluded. 9 Calculation The calculation shall be as follows. a) For the adhesion strength of the test piece, calculate the peak value of the medi- ans of the wave form (in the case of method A, B or C) or the average (in the case of method D or E) in accordance with the method A, B, C, D or E in JIS K 6274. b) The adhesion strength shall be calculated according to the following equation. PROTECTED BY COPYRIGHT 5 K 6256-1; 2006 where, Tr: adhesion strength (N/mm) Fr: resistance to separation (N) 5: width of test piece (mm) 10 Expression of test results 10.1 Adhesion strength The adhesion strength shall be the median of the val- ues obtained by the individual test pieces. The median shall be expressed with the rounding width of 0.1 as specified in JIS Z 8401. 10.2. Expression of type of separation or failure Describe the type of separa- tion or failure using the following terminology: a) failure in the rubber layer (symbol: R); b) separation between the rubber layer and the adhesive (symbol: RA); ©) separation between the adhesive and the fabric (symbol: AT); 4) failure in the rubber bond between two fabric plies (symbol: RB); e) failure in the fabric (symbol: T); ) separation between the rubber and the textile when no adhesive is present (symbol: RT). 11 Test report ‘The test report shall include the following particulars: a) a reference to this part of JIS K 6256; b) all details necessary for the identification of the sample; ©) the type of test piece used, and the test piece dimensions; d) the rate of ply separation; e) the temperature and relative humidity of the test; f) the nature of the interface between the assembled components and calculated adhesion strength; g) method of analysis of wave form used to calculate the adhesion strength; h) the adhesion strength; i) the type of failure or separation; i) the date of testing; k) other matters to be noted. 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