!

t 1!iPOB Tesl irethod k2,4:2004

Crude fib.e in PKC

UETHODS OF TEST FOR PALM KERNELPRODUCTS:

DETERMINATION OF CRUDE FIBRE IN PALM XEI{NEL CAXE

Relerenc€d docuftonts

do nol 3pD y However pa'1r05 to ag

d 10 nvorsala th6 possDr't or a

s.nprn9 orparm k6he cake

MPOB Ts( Merhod kl 2: 2004

For Ih6 purpos6 offir MPOBTesl Melhod

Thd oss ii mass undeGona bylhe piddudon ashiis ar 5o0.c or550

, and erp.essed a3. perceiiase by mass

succ$5v6ry wrh boiig sourons o, surphudc acJ and polass um

hyd,orde or specirc corce ration The r$due s sepa6l6d by rxsl
* qhed Anorashi9 lh6 ossofwe

A rcasenG srial be or rccolnsen aialyiicaisrade The walar used .

@rer or ar ban equ va e^l qlariy

SuiDhu c lcld iH,SOt),0123 M i6.96 mL of H,Sor diluled ro 1Ll

Pota*rumhydrcxrdglKoH) 12s9orxoHdrssorvedinl Loldisr edwar6..

 I
lvPoB Tosi r 6lhod k2.4:2004
Crude fibre in PKC

UiuaL aboralory aPPa€lus a^d, io P

61 Frb.n6c iy.r.m cois5li9 ofa HolEnEdon unl

crucibre wilh porc. ry40 !m {o 50 lh

Erdcric ovon, capabre ofma nrain ns a rempe,alurc o1130'c r 2'C

D*lccaroriconraiirisaieifconrdesic€ilsuchasphosphorusMordo, cager

'samp ns ii nol pa ol rhe melhod speien i 1h5 MPoB

8 Preparalio.oltestsamPra
P'oparcihosampe naccodan.e{rhlhemerhodqvei nMPOBT6sM6lrodkl2:2004

w6rshahomoseious $mpe(.boul 1s) iloceairlercrucrbes (61) pa.esiia

unr {61). rx .rd'be hod* r

'he

Adc a rsdrcp3or i"er3^o 15 3)ro

hoal 5nd bo ,oj30mi

^dj$l

I
I
{.,
Ur: ir l:sl Method ft2,4: 2004
Ctud. flbl€ I. PKC

9.7 Wash rhrc6lim$ with hol deionLz.d walerlrcm tho spEy deviod slidlno oi tho bar
abovelhe bo nglubes (J36 abour30 mL ol walar eaoh lim6 and suck e dryas possib 6

on (52) pchealLn ii u6

0.9 Addaaewdropsor,-octanoraid bo asaboveloranorhff F..do,30mn

9,lo
tucbes r.om the Hol Enracroi un lolhecold

w.Eh th'eelmaseith acelone (54) (.b0u125 mL eachlne) and srckdry.

Removerh6 crucbesand tansrsrt

orylhe.rucb aE n an ovei (6 s) a( 130oC lor2 h.

coorhe cru. bas n adesiocato, (6 6) andw0qh (w,

oo'c (6 3) Io, al eall3 h o,550'c ro,2 h

coo rhecrucib6s srowy 1o room t€mp.Glu€ aidvrg!i a3a i (w,)

Ri^se rho cruc b es by b@fg rhe ash dul wlh comprs*od a I or I ihe orucibleg ar.
didy washwlh chrcmicacd

10

11

(a) the meihod ii acoodance wilh which samp iqvescatriedod ifk rown

(b) thsmelhodused

98
 I
MPOB Tesl Method k2-4: 200.1
Crude fib.6 in PKC

the re51 resut(s) obla n€di.nd

ir''" rcDcaraoiq ra3 o6er .hedPo

t'h, r50 neiron arropohliis d€Lih iol spedficd ti rhG MpoB Tes
w$ d.rairE of aiy incidonG whlch m.y hav6 nflu.icad
oprlo^al, rd{olher th€ test rcsu (a).
Tl,o let .epon s5a iic ude ar nfomaroi nec.ssary lor ihe cdmpete deilflcation of the

99