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International Journal of Mechanical Sciences 131–132 (2017) 75–80

Contents lists available at ScienceDirect

International Journal of Mechanical Sciences


journal homepage: www.elsevier.com/locate/ijmecsci

A study on fiber metal laminates by using a new damage model for


composite layer
M. Kashfi a,∗, G.H. Majzoobi a, N. Bonora b, G. Iannitti b, A. Ruggiero b, E. Khademi c
a
Department of Mechanical Engineering, Bu-Ali Sina University, Hamedan, Iran
b
Department of Civil and Mechanical Engineering, University of Cassino and Southern Lazio, Cassino, Italy
c
Department of Robotics, Hamedan University of Technology, Hamedan, Iran

a r t i c l e i n f o a b s t r a c t

Keywords: Fiber metal laminates (FMLs) are new hybrid materials which are widely used in aircraft industry due to their
Fiber metal laminates higher mechanical properties compared to monolithic metal and epoxy based composites. In this work, mechani-
Glare cal behavior of the FML is investigated by experiment and simulation. The FML used in this study is made of two
Nonlinear damage model
layers of aluminum 2024 and a layer of glass-fiber reinforced epoxy (GFRE). The experiments showed nonlinear
Finite element method
elastic behavior for GFRE layer. This behavior is due to damage evolution and material degradation. Therefore,
a simple nonlinear damage is presented to improve the results of the proposed material model. Mechanical prop-
erties of the layers are measured by uniaxial tensile test. Numerical simulations are performed by implementing
the material model into the user subroutine of MSC MARC FE code. The results of the proposed model showed
a reasonable agreement with the experiments. The agreement confirms the nonlinear damage behavior of the
FMLs observed in the experiments.
© 2017 Elsevier Ltd. All rights reserved.

1. Introduction based material model can be used to analysis different grades of GLARE
laminates in structural applications. The effect of fiber orientation on
During the last few decades the composite materials have attracted the tensile behavior of glass-Kevlar fiber/aluminum laminates under
the attention of many researchers across the world. During the process static in-plane loading conditions was reported by Moussavi-Torshizi
of time, the innovations in the composite area led to significant weight et al. [5]. They used a numerical simulation method based on finite
reduction in structural design. Composites offer many advantages when element method to predict the stress–strain response of FMLs. Lee et
compared to metallic alloys, especially when high strength and stiffness al. [8] evaluated the tensile behavior of the self-reinforced polypropy-
to weight ratio is required. Moreover, they provide excellent fatigue lene and aluminum alloy laminates under static in-plane tensile load-
properties and corrosion resistance in applications [1,2]. ing by simulation and classical lamination theory. They found that for
Fiber metal laminates (FMLs) are hybrid laminates fabricated from plastic deformation of the FMLs, the results obtained from the classical
thin aluminum alloy sheets bonded into laminates by intermediate thin lamination theory were more realistic than those predicted by the vol-
fiber-epoxy layers. The FMLs bring together the best features of the ume fraction approach. Khalili et al. [9] presented a FML composites
composing metal and fiber-reinforced composites. They exhibit more based on Steel/aluminum/glass-reinforced plastic laminate. Esfandiar
advantages over the conventional monolithic aluminum alloys or fiber- et al. [10] investigated the nonlinear tensile behavior of GLARE fiber
reinforced composite materials [3,4]. The FMLs with glass fibers (with metal laminates under in-plane loading conditions. They used two ana-
trade name GLARE, Glass Laminate Aluminum Reinforced Epoxy) were lytical approaches, orthotropic plasticity and modified laminated plate
used as the upper fuselage materials in Airbus 380 and lower wing pan- theories to predict the stress-strain curve and deformation behavior of
els of the Fokker 27 [5]. The ultimate tensile strength of GLARE has GLARE laminates. The results showed that the GLARE behavior was al-
been found to be 33–140% higher than aluminum in the direction of most bilinear under tensile loading condition and the tensile strength
the reinforcement [6]. of unidirectional GLARE laminates was considerably higher than alu-
Soltani et al. [7] used a finite element modeling approach to predict minum alloys in the longitudinal direction.
the stress–strain response and deformation behavior of GLARE under In addition, due to superior electrical, mechanical and thermo-
uniaxial loading conditions. They showed that their proposed macro- mechanical properties of the nanostructures, they are widely used in
nano-electro-mechanical systems (NEMS) and FMLs [11–14]. The size-


Corresponding author.
E-mail addresses: m.kashfi@basu.ac.ir, mohamad1367@gmail.com (M. Kashfi).

http://dx.doi.org/10.1016/j.ijmecsci.2017.06.045
Received 11 April 2017; Received in revised form 6 June 2017; Accepted 25 June 2017
Available online 27 June 2017
0020-7403/© 2017 Elsevier Ltd. All rights reserved.
M. Kashfi et al. International Journal of Mechanical Sciences 131–132 (2017) 75–80

Table 1
Chemical composition of aluminum 2024 alloy.

Element Si Fe Cu Mn Mg Cr Zn Ti Impurities total Aluminum

Quantity (%) 0.1 0.26 3.8 0.5 1.3 0.01 0.08 0.02 0.08 Base

ducted for two different quantities of Metal Volume Fraction (MVF).


Samples with four and six sub-layers of glass fiber are called FML-4 and
FML-6, respectively. Obviously, the MVF of FML-4 is higher than FML-
6. The tensile FML specimens were fabricated with the dimensions of
250 × (25 ± 0.99) × (2.44 ± 0.15) mm as suggested by ASTM D3039. FML
specimen which includes tabs, painted area for Digital Image Correla-
tion (DIC) and gauge length are presented in Fig. 2. As the figure shows,
one layer of GFRE is sandwiched between two layers of aluminum 2024.

2.1. Aluminum 2024

Fig. 1. Woven form of E-glass fiber. All specimens were tested under uniaxial stress condition. The ten-
sile tests were conducted on an Instron 5582 testing machine at the
cross head velocity of 1.52 mm/min that corresponds to a strain rate of
dependent continuum theories, e.g., classical couple stress theory [15], 2.5 × 10−4 s−1 . Four specimens were tested and the mean value of the
modified couple stress theory [16], nonlocal elasticity theory [17], measurements was used as the specimen property. Experimental engi-
and strain gradient theory [18] have been employed to analyze the neering stress-strain curve of aluminum 2024 is shown in Fig. 3.
nanostructures. For example, a nonlocal continuum plate model has Voce constitutive equation is considered to describe the relation be-
been developed for the transverse vibration of double-piezoelectric- tween true stress and plastic strain in plastic region as follows [26]:
[ ( )] [ ( )]
nanoplate systems (DPNPS), piezoelectric nanofilms (PNFs) and double- −𝜀𝑝 −𝜀𝑝
piezoelectric-nanofilm (DPNF) systems were studied by Asemi et al. 𝜎 = 𝑎 + 𝑏1 1 − 𝑒𝑥𝑝 + 𝑏2 1 − 𝑒𝑥𝑝 (1)
𝑐1 𝑐2
[19,20]. Farajpour et al. [21] developed a higher-order nonlocal strain
Where 𝜎 is the true stress, 𝜀p is plastic strain and a, b1 , b2 , c1 and c2
gradient plate theory for the buckling of orthotropic nanoplates under
are the material constants which are determined by optimization. In the
biaxial compression in thermal environment. Mohammadi et al. [22] in-
optimization procedure the difference between the load-displacement
vestigated the vibration behavior of annular and circular graphene sheet
curves predicted by simulation and measured by experiment is consid-
coupled with temperature change and under in-plane pre-stressed. They
ered as the objective function. Genetic algorithm is used as the opti-
reported obtained results could be used for the design of the next gen-
mization algorithm and 128 simulations are performed to minimize the
eration of nanodevices.
error. The optimized coefficients of aluminum 2024 and its mechanical
Although many attempts have been made to explore the FMLs be-
properties are listed in Table 2.
havior, assuming linear elastic behavior for GFRE layer and nonrealistic
plastic model for metallic layers has resulted in insufficient accuracy.
2.2. GFRE layer
Experimental results indicate that damage evolve gradually in the fiber
layer which cause nonlinearity in its behavior. Therefore, in the present
In order to obtain the orthotropic behavior of GFRE layer, tensile
work a simple nonlinear damage model is introduced to improve the
tests were carried out in three directions. Five 100 mm × 10 mm speci-
numerical results.
mens (as suggested by ASTM D3039) in warp, weft and 45° directions
were cut out of a rectangular GFRE plates as shown in Fig. 4.
2. Materials and experiments The stress-strain curves of GFRE layer were obtained in warp and
weft directions by uniaxial tensile test. The results are illustrated in Fig.
The materials used to fabricate the FML specimens were aluminum 5. Table 2 shows the summery of orthotropic properties of the GFRE
2024 sheets with 0.84 mm thickness (chemical composition is given in layer calculated by ASTM D3039 suggestion where subscripts 1 and 2
Table 1), woven glass fiber (E-glass, 200 g/cm2 ) and epoxy resin (made indicate warp and weft directions, respectively. The difference between
by Huntsman Company). The woven form of E-glass fiber is illustrated the elasticity modulus along the warp and the weft directions is about
in Fig. 1. Araldite LY 5052 and Aradur 5052 were used as the resin 26% that is related to the volume of fibers in each direction. This is the
epoxy and the hardener, respectively. This type of epoxy resin is used in case in most of composites with woven fibers and been reported in the
aerospace and industrial composites, tooling and aircraft repair [23]. In literature [27–30].
order to obtain a proper bonding between aluminum and GFRE layers, As Fig. 5 suggests, the GFRE layer exhibits a brittle elastic behavior
the specimens were pretreated according to the ASTM D2651 [12,24] in- due to its very small failure strain. Also, behavior of the warp and weft
structions. directions is nonlinear. However, as it is presented in Fig. 6, loading-
FML specimens were fabricated by hand lay-up method. The glass- unloading in uniaxial tensile test shows a decreasing trend in the mod-
fiber layer was impregnated with epoxy resin. Fabricated specimens ulus of elasticity with the increase in the strain. Therefore, the GFRE
were placed in a mold designed to press the layers together under a behavior can be assumed elastic combined with nonlinear damage. Ac-
controlled pressure. The specimens were then moved to a curing cham- cording to the thermodynamics of continuum damage mechanics and
ber for heat treatment. The curing temperature and the time were definition of a dissipation potential from which the laws of evolution of
80 °C and 8 h, respectively as suggested by the epoxy manufacturer. the state variables associated with the dissipative mechanisms are de-
The pressure level plays important role to decrease the voids and to rived, the nonlinear behavior of GFRE layer in warp and weft directions
remove the redundant resin. It has been shown that plain specimens can be explained by damage evolution during a tensile test [31].
are more appropriate for conducting the tensile tests on fiber/metal During tensile tests some irreversible damages occur in the compos-
hybrid laminates [25]. The tensile tests on FML specimens were con- ite layer. The damage includes delamination between each layer of com-

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M. Kashfi et al. International Journal of Mechanical Sciences 131–132 (2017) 75–80

Fig. 2. Schematic view of FML specimen.

Table 2
Mechanical properties of aluminum 2024 and GFRE layers.

Aluminum 2024

E (GPa) 𝜈 𝜎 ult (MPa) Elongation (%) a (MPa) b1 (MPa) b2 (MPa) c1 c2


74.08 0.34 194.80 9.88 84.00 93.80 31.80 0.024 0.166
GFRE

E11 (GPa) E22 (GPa) 𝜈 12 G12 (GPa)

13.47 10.69 0.1017 1.83

Fig. 3. Experimental engineering stress-strain curve of aluminum 2024.

Fig. 5. Stress versus longitudinal and transverse strain in warp and weft directions for
GFRE.

2.3. FML tensile test

Uniaxial tensile test was performed on FML samples. The gripped


FML specimen and its geometry are shown in Fig. 8. Steel tabs were
glued to both ends of the specimens using glue to increase the thickness
of specimen in grip section. The cross head velocity and strain rate were
1.52 mm/min and 2.5 × 10−4 s−1 , respectively. Strain was measured us-
ing extensometer and DIC method simultaneously. Tensile tests were
continued until the complete breakage of all three layers of FML. In
Fig. 4. Warp, weft and 45° specimens were cut out from GFRE plate. all samples, failure initiated from the GFRE layer and extended to alu-
minum layers, as it can be seen in Fig. 8
posite, matrix failure and matrix and fiber debonding. The most dam-
ages in the GFRE layer can be observed in micro-scale; thus, optical mi- 3. Damage model for GFRE layer
croscope was employed to observe the delamination and other defects
in GFRE layer. Typical delamination of sub layer of GFRE layer during As stated in the previous section, GFRE layer has nonlinear elas-
tensile test is illustrated in Fig. 7. tic behavior and the loading-unloading test demonstrated that damage

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M. Kashfi et al. International Journal of Mechanical Sciences 131–132 (2017) 75–80

Table 3
Damage parameters for warp, weft and av-
erage.

Warp Weft Average

𝜀th 0.000 0.002 0.001


𝜀f 0.0265 0.0238 0.02515
Dcr 0.31 0.268 0.289
𝛽 0.78 0.64 0.71

Fig. 6. The loading-unloading stages for GFRE layer.

Fig. 9. Damage evolution in warp and weft directions comparing with average curve.

Where Dcr is the critical damage, 𝜀th is the threshold strain, 𝜀f is


Fig. 7. Delamination of each sub layer during tensile test. the failure strain and 𝛽 is the damage exponent and can be obtained by
simple tensile test.

4. Finite element modeling

4.1. Damage constants determination

The numerical simulations were performed using the commercial fi-


nite element code, MSC MARC. Because of the symmetry condition, only
1/8 of the model was simulated. By assuming the power law model de-
fined by Eq. (3) for damage evolution and using an optimization tech-
nique to find the damage constants, two sets of damage parameters were
obtained for warp and weft directions. For optimization, the average of
five experimental force-displacement curves was used as the target value
and RMS (Root Mean Square) of the difference between the experimen-
tal and finite element model was adopted as the error. Genetic algorithm
Fig. 8. FML specimen instrumented and gripped to the test machine. was used to minimize the error and the material constants were com-
puted. The presented damage model for GFRE layer was incorporated
in a user subroutine called unlcdm. The subroutine was used to predict
evolved as the strain increased. Most of the damage models have been the stiffness variation during loading for simulation [33,34].
proposed only for 2D composite laminates. However, the few investi- In warp direction yarns have wavy shape as they cross the top and
gations of the damage evolution behavior in the 3D fiber reinforced the beneath surfaces of the weft alternatively. Another important point
composites, are accompanied by some limitations. Typical limitations is that the fiber fractions in the two directions of weft and warp are
are, (1) most of the adopted classical criteria were unable to accurately different. The optimized damage constants obtained for each direction
and effectively predict the initial damage; (2) the damage and failure and their averages are listed in Table 3.
modes were usually not described adequately [32]. The material stiff- The damage evolutions in warp and weft directions are compared
ness degradation is defined as follows: with average value in Fig. 9. As the figure indicates, the difference be-
tween damage evolution in warp and weft directions and the average
𝐸 = (1 − 𝐷 )𝐸 0 (2) curve is negligible. Therefore, the average of damage constants can be
Where E0 , D and E are initial elasticity modulus, damage parame- used in numerical simulations to reduce number of material constants.
ter and the current elasticity modulus of the composite, respectively. A The Fig. 10 illustrates the experimental and numerical engineering
damage evolution is proposed in this work as follows: stress-strain curves of GFRE layer in warp and weft directions by con-
sidering the mean of the damage constants. As the figure suggests, the
( )𝛽
𝜀 − 𝜀𝑡ℎ stress-strain curve predicted by the proposed damage model coincides
𝐷 = 𝐷𝑐𝑟 (3) exactly with the experimental curve. It can also be observed that the
𝜀𝑓 − 𝜀𝑡ℎ

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M. Kashfi et al. International Journal of Mechanical Sciences 131–132 (2017) 75–80

Fig. 12. Engineering stress-strain curve for FML-4.


Fig. 10. Comparison between FE and experimental results in warp and weft directions.

Fig. 13. Engineering stress-strain curve for FML-6.


Fig. 11. The damage evolution in FML-4 manifested by removal of damaged elements (a)
Equivalent Von-Misses stress in MPa and (b) experimental failure pattern.

stress-strain curve consists of two distinct regions. In the first region,


difference between the numerical predictions with and without consid- the stress increases in a non-linear fashion to a maximum and drops
ering damage is significant and cannot be ignored. sharply due to failure initiation of the GFRE layer while the aluminum
layers still keep being strain hardened. In the second region, the GFRE
4.2. FML simulation layer loses its load carrying capacity altogether due to complete failure
of the composite fibers indicating that the aluminum layers have lonely
Similar to the previous section, the FML simulations were performed carry the load and the stress begins to rise again due to work hardening
using MSC MARC and 1/8 of the model was simulated. Glue contact was until the failure of the aluminum layers. The difference between the
used to simulate the contact between aluminum and GFRE layer [35]. experimental and the FE results after the GFRE failure in the second
The Von-Misses stress contour of FML-4 is illustrated in Fig. 11. The region can be due to the influence of damage model in FE result that is
figure shows the progressive failure of GFRE layer of the FML-4. As the significant after the threshold strain. It is evident that by ignoring the
figure indicates, when the damage parameter attains its critical level damage effect, the stress will be overestimated by FE simulation.
and failure occurs, the Von-Misses equivalent stress in the element is set FE simulation was also carried out for the FML with lower MVF,
to zero and the failed element is removed from the computations. FML-6. The results are shown in Fig. 13 where the stress-strain curve
of FML-6 is compared with experiment. As it can be seen, the numeri-
5. Results and discussions cal prediction agrees well with the experiment in the first region. After
GFRE failure in the second region, the experimental curve is initially
In this work, a new damage model for GFRE layer in fiber metal lam- considerably higher than the FE prediction but converges to the numer-
inate is proposed to increase the accuracy of FE model for simulating the ical prediction for higher strains. As a matter of fact, some fibers still
mechanical behavior of FML. The stress-strain curves predicted by nu- resist against tensile loading after the failure of the GFRE layer and after
merical simulation considering and ignoring the damage model, defined full tearing of the fibers the numerical prediction converges to the exper-
by Eq. (3), for the GFRE layer are compared with the experimental stress imental stress-strain curve. The difference between FML-4 and FML-6 in
strain curves for FML-4 in Fig. 12. the second region of Figs. 12 and 13 can be explained by the fact that for
As the figure suggests, the numerical model could accurately predict the increased number of sub-layer in the GFRE, some fibers may carry
the behavior of FML and in particular before the GFRE failure. Also, the part of the load while other fibers have completely lost their resistance.

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M. Kashfi et al. International Journal of Mechanical Sciences 131–132 (2017) 75–80

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