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University of Santo Tomas
Faculty of Pharmacy
Department of Pharmacy
PHA6113 (Physical Pharmacy) Laboratory
. L'f-fH
Section: _ _ __
Group No.:_$_ Date: Oc--\ ' I 'lo'L'L
Leader: lM. ~1o,c~.11 \ Y1I 024r:
Members: o-.,u.w,.n K.ulat"
J«.r- (141{\ i«fa)o
ACTIVITY 3
Viscosity Determination

Presentation of Data

Barometric Pressure

Room Temperature

Prlnclple/s Involved:

A. Ostwald Viscometer
1

i\- iuorkc "' i~ -1\\(. f ei1t.u,\\<, S \o"" w\,tf(,n i'kc.\~v.,c>.', RowtctW. i£°"'tMW0 of~(.Gf.\H. (Aj~~ ...
-t-0-\N. \I\SCOu.C ..U\C'()na..1\.(11,.s~ttuHc."u. vc,r,u
oH\.1.~.
t~,o.
"''~ '""-'vi1co&\h-\ c,f,t'r(. ear-<,\ +1-.~ l ~

8. Brookelleld Viscometer
Tht 4pfCcfQ-fue v-lt\Czt( "'°'t.f''"'"Pl<. <>f-ro½4t'10r<.1\ v\(to.u~ ~\\l&i rnu..su'°" -tt\t forte.of ~\.\(
~t1n, &t\-t1-< tp,rJ\4 1.\- is rett Mette. o~ Ct>~a"t u~u\c.w- ~t\oc.."-\, ,,-o,CQ\'ii
#)(\/UC9l<ilj -tl\l \<.'fA icl

I. Ostwald Viscometer

Trial Efflux lime

Water Ethyl Alcohol

1 a~s l',6s
2 J)l$ i~,
M /
3

Average Time
"'"'
1112. .t,n / / ~.~
Temp (°C) ~•c L_ /U·~
I
#~
/ /
/i
/ II. Brookefleld OV-ll+Pro Viscometer

Sample:

Trial Spindle No. Speed (RPM) Viscosity (cp) % Torque Temp (0 C)

11,.0
2

Average

Addfflonal Data

Density of Water at its temperature o.4\q.•7' t.:,l~t..


Density of Ethyl Alcohol at its temperature \-\50 ~(\,\I\L

Viscosity of Water at its temperature 0 0461\ Cf


Theoretical Viscosity of Ethyl Alcohol at its temperature
, . r Goc.r

Computations

a. Absolute Viscosity of Ethyl Alcohol


p,l \
1\,::1 P1: o.'t~~ rJ.~L n,. th :.t() ,:J<l~~ ~,!\1JS.<.~(o.,, \\tr)
\>t.tz. -t:>
r, o.405'(~ t 2 :: 21l. C'fJ
-tc ::'.:,r, .,=t .r n,-:. ~, ni_. (o.q1.:ic~) ic.(11;i..C-"i,'1

b.
ht,~ 0 •'i,u t.f
Relative Viscosity of Ethyl Alcohol
A.t1,.
t O. ~<i't c.~
{l(.l r,: - (),'&~?fl Cf : -~-.-q1-s-~--,\
0.1 (,l\q>

C. C. % Error for Ethyl Alcohol


-,, \W'(Clr-:
-r'(
-Lloo1, --o-:: ·\·\so "'<.l.ict\'\ Y--O>o ·1, -::.
\. ,so
\:t •'ll'!'/tl
Post-laboratory Questions

1. Define the following terms: absolute viscosity, relative viscosity, kinematic viscosity, efflux time.
A\,So\~t.1,\wU~- Ottt.rmnq bJu f\v.itl<r.w-t nsu+ w\o-tn\Y\ ,~~c..c.tioh w~Q" ~Wfrv.\ t'llrtt,
~\c.c~~vlS,c,o!.1~· Th<. -c'4hO of tt-.<. V\lt.o\ln..\ of-'°' 1W-i-\u1t.c\ -11, 0\ ,Ut..N.Aci~ h"c.tl.4\c( ttl wol<r.
Mtmorti(. V\\wS~ - ""-' r4'\-i o c,E- c.b,a. "'°'I.( "uuo "~'1 -to o<ns \~ c,t vw.tt~t;l
£ffl1.1J+j - 0<.ti'flli ~lo"1 -\N F~f(J (Oh., ~-\of .\"4 Jl1tf1m
~dd\\\ol"I() \ Oo~o Co~t,O'\S De.Y\tt½ of -M~\ ~ \ o\- \-\',1 ~v,tre.-\1\'f-t
• Otyl!.\~ o~ V"~ttr ct\- \\-~ ~°'r'rc,h,\N
')(,: 'lslc. --(,:: o. ~'\2 3l""L
"'{.7.: 1i·l Yi
'f. \ -
- lt)' t y,::0,0.q~tf"'L
"-i : ~·<. Yt = ?
'l-1: J.~' C. 11 : (). =!g4't 3(\'-L
aIW\L Yt -1!
-Y1-Y1
i.) : "iO't 'f 1 -: t> A\}a
i-7.-7,.l :
i,-'I.,

'2.-1.() :. Yt -o -7'l>cri
ir-io o. ~l\'t • D. =lt'l2.
-7.. .-

-: 1-i. -oAct1 l
' a, -
-o. ~'f~
C, - 1 .'14C.
- () . 00 0V - ""fl.
J.c .- () .oo<. '!> .'f"H y :.~1.
-0.01',),. 20'f z - \~-'I~½ s
14 A\?lf -o.o 12.. :. "!_6 j1. Yi :0.1%1S ~{Jhl..
J-0
[E, 0 ·'"l't'li ff ,My
V,O(),l~ of uotc, Q+- t~'s +!~\)(.rr.'\utt
Y,,: '1.f:l•c 'le :. l. OOlOc...p
Y.z: ll."'"C. y-'1
L • •
'A'.1 '!t.:l6 c., y, : 6 .=,,-:,s,r
)(1. • )(.\

~3-1'1 ---
- 'fz
·t1-Y1
I ?Ci -'f... \
...,...,, --,.\
= 'f-t.-Yt
'{1-~ I
J.,.,l- io :: fi - \,f:P'lb
J.l~ -- Yi-FIDO
'\o •lo O ·-1<tlJS-l· OOW
11-tu
-:. 'lt-l•OOU) l · O,c.i - 1-~00
LO - 0 . 'Lo '1f'
-o-~()q_ :toyi- lO.o't
l0-01. -o . 4D't = lO 'f 2
-o .lS1: Sy '2 -, .ooo
't.,i.l\ -:.~
to , .ol.Q -o. 2.&..L -;.
jY i~o.tHI\ r
4. What are· the classes of non-Newtonian
. ma tena
· Is. Give examples of each.
.
O..• Y.1.~L ~dl (1.\,.\\ Ill - I ~1"4"' l'dk I '-'11--0Wtl l\,,,.(c/. ' """' f"'"ltr- , N<......, "' l!<f-/MI ,.._ Ow,./,lkj
Vlllo,

\,.~'"" ""-"t Go. VUCO( I~1\.,\ ovtrtt>N SW. 4' 1


f'<l"'f lul1,r Y"'f"i c,n(l<fl''f'l<dt.l~
~\1-v... "ff '-" VIS<c1sm:, itt.tlt'O(all(,!, «.,di,·~'™" SUch"' Oo\,lcd,. ..J.uf C...n twolno>A.u«<r,
1 1
C,. ~ \ ( 6<

cl-~s~ 0,,9-" ff,,,.,.""f llll ~l'fdd ....._ ,~I l'dlS,,.. 1-t n'l>41o &era.« Vll<b\.., GJ,-&n.., ii "R)lctd.

· . 'red for acetone to flow between 2 marks of the


5. Using Ostwald Viscometer, the time r~, for water or standard the time was 300 seconds at
capiltar; viscometer was 245 ~onds an >and that of water is 0.997 g/cm'. The viscosity of
2soc. The
water ~ensity
at this of acet~n0e891s
temperature 1s . 040.786
cp temperature. Calculate the viscosity of acetone.
Gtvtf\·.
n, =? - pt't\
f,:. 0. Y}i ('li;L
t I: '2. '\£J
t\1 :.ftlttlt
ht: o.1'1ol\,f
pL ': 0• '\Ca °l 'f (C. Y\-\ l {' t t1.

~,_;'\ct)~
\-h: (\) .=t~~(,~1),,.(tLt51) i'( () .Cf>'Jt>'t,p)
W~U't\f\".
(o. 11? 8(tl\l) 'I- (juO .s)
1 -; C,(.(-flf'\ '{
l ; fA. ft..,. h , '.--Q. Si 1<f
k "-ftnt!S :
"u·m~t.Y-, ~- (lo~l. WM.It i$ Abso\u\t Vu~.JJsi-\"') ?. Al\~ StiChC<.
~&: If 1uww. '4l\\'ticlc.lcf\~ •O~ / 1,1"""'-is-A1o1o\~ -V(i.o &\~ •httvl

Notl -1-l<u.J\0Na---. ftu.{il..s. (iow). Sc.1<net \..t'"11'\\~ \n.\b, http&: ltw1,1,,1w, SC.tet"t< lel.tm, Ol'C). f\Z./
rl~rct.s I lsei~- °"" ~"ICI" -ft~ dr

('~ l M- 0010). ~(()\~~ • S\vlc.~. h~s ill~'-"· s\ulc..snc,rc. nt~ H.\c.ih(w~ P ~ I


rhw\~"' · '}U Cf>C\ 70"\S

Unl'ict\ L ~- ~ ~ ) . NO"•Nt~\tAY'\ 'fl\,\0., B'1~"''s: l:,cCafVI {hf'· nl+f>S =ll ~A\A3 tl'CAMrcr -~ \
nu,v f\w,.\t>n\o"! - flMttls-·,

lf i StoO\<.-\tv- (e,Roo~~1. (io \tt). Labortt\-1),rt ·t,t ay,itm. MtfS ! (l m~-pt"'. \At\W A'tn. fr)
Rhto"'dtr - !>\Wt\"-f\~l\>-Nt , MTV\\

w~ ,, tfrltA1,. ?, (n-~.). Trtnt:hl<.CC\~io.' h\ipt :l( WIAIICI •-frtN.ht.(U~(t4 ,(O(n /dtnt.,~C)l\r


)..' l. i' {tff \tA+ #

Wo•~~ P,1nu~( oE v\~~, Cn.A.). %,.diCMS G"'1' nt"-t\)S: {( Si'wAiAAS (.o~ \

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