CHM096 Class: E07 Lab Group: Group 1 Group members:

EXPERIMENT 8
Acid Base Titration
 Class:E07 Lab Group:Group 1 Group
CHM096 members:

EXPERIMENT 8
Evaluation of techniques used
Acid Base Titration Mark √ for correct technique or X for wrong technique and
justify the wrong technique(s).
Record
SET 1 Titration Data the data. Determination of acid molarity Techniques √ or X Justification
Calculate the molarity of HCl solution.
Acid used: __HCL__ Base used: __NaOH___ To clean the burette, we must add some
average pH = 1.27 + 1.23 + 1.19 deionised water into the burette. Then, hold
Trial 3 the burette horizontally to allow water to flow
0 X through all the surface of the burette. Then
Burette reading = 1..23
(mL) I II III rotate the burette and drain the deionised
pH = - log ( Molarity) water out.
Initial 0.00 13.20 26.80 1.23 = - log ( Molarity )
Molarity = 10^-1.23 Tap gently to remove the air bubble while the
Molarity = 0.059 M 1 X solution is flowing in burette.
Final 13.20 26.80 38.00
Volume NaOH Eyes should be perpendicular to the reading
used (mL)
13.20 13.60 11.20 2 X scale of burette to avoid parallax error.
Calibration of pH meter
• State the calibrated pH values. 3 √
pH value I II III 4.01 and 7.01
A pH electrode is fragile and should
Initial 1.27 1.23 1.19 aaaa
4 X not be use it as a stirring glass rod
Final 7.29 8.17 7.10 • Briefly explain the purpose of calibration and the when titration occur.
effect of temperature on pH measurements (as the
Color changes colourless to pale pink ‘temp’ knob has been adjusted to 25 °C). 5 √

-To maintain accuracy, standardization and

Indicator used: Phenolphtalein
repeatability in measurements, assuring reliable 6 √
benchmarks and results.
State the importance of repetition in titration.
-pH decrease with rise in temperature.
A titration is repeated at least 3 times in order to
provide a statistically valid result of the titration.
Plot a titration curve
Next page
for SET 2 titration between CH3COOH and NaOH.
 Class: E07 Lab Group: Group 1 Group
CHM096 members:

EXPERIMENT 8 Group members

Acid Base Titration Student’s Name Student’s ID

SET 2 Titration Data Titration curve S1 ADAM ALHAJJ BIN MOHD AMRAN 2021206498

Plot a titration curve for SET 2; Titration between CH3COOH and S2 AISYAH BINTI KHAIRUL SHAHRIN 2021821468
Acid used: CH3COOH Base used: NaOH NaOH. Label the buffer region and pH at equivalence point.
Indicator used: phenolphthalein S3 HASZRYN NATASHA BINTI HISHAMUDDIN 2021857352

S4 IFHAM FATHI BIN SAYUTI 2021484812

Burette reading (mL) pH value
MOHAMAD HISYAMMUDIN BIN MOHD
S5 LUKMAN
2021463256
0.00 2.92
MUHAMAD NASRUL FIRDAUS BIN
1.00 3.46 S6 SHAMSUDIN
2021894866

3.00 3.99
5.00 4.26 Discussion & Conclusion
7.00 4.47
9.00 4.65 SET 1
-In conclusion, the higher volume of NaOH used, the pH value
11.00 4.83 increase.
13.00 5.01 -When a strong acid react with a strong base, it will produce a
neutral salt.
15.00 5.22
17.00 5.49 SET 2
-When a weak acid react with a strong base, it will produce a basic
19.00 6.02 salt solution.
21.00 11.34 - At equivalence point, pH > 7
- We have plotted the equivalence point equals to 8.60
23.00 11.79 - The buffer region is between pH=2.92 and pH=6.02
25.00 11.99
27.00 12.12