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Article history: Several researches have highlighted the influence of external environmental conditions (e.g. moisture
Received 15 October 2021 and temperature) on the concrete response at different strain rates, however, limited data are available
Revised 6 July 2022 considering such factors. This paper experimentally assesses the compressive strain rate effects of con-
Accepted 1 September 2022
crete at different saturation levels. The experimental assessment is conducted on sixty-six specimens
Available online xxxx
tested using the Split-Hopkinson Pressure Bar. The results of the experimental program were compared
against the Comite Euro-International du Beton (CEB) equations and calibration factors to account for the
Keywords:
degree of saturation were introduced. Furthermore, the proposed calibrated equation was tested against
Strain rate
Saturation
a large database collected from the literature which showed more reliable predictions than the current
Dynamic increase factor CEB equation. The presented work aims to enrich the concrete database subjected to high strain rates
Split-Hopkinson and to facilitate reliable material predictions to be used in further numerical assessments.
Ó 2022 THE AUTHORS. Published by Elsevier BV on behalf of Faculty of Engineering, Ain Shams Uni-
versity. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/
by-nc-nd/4.0/).
https://doi.org/10.1016/j.asej.2022.101976
2090-4479/Ó 2022 THE AUTHORS. Published by Elsevier BV on behalf of Faculty of Engineering, Ain Shams University.
This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).
Please cite this article as: S. Salem, E. Eissa, E. Zarif et al., Influence of moisture content on the concrete response under dynamic loading, Ain Shams Engi-
neering Journal, https://doi.org/10.1016/j.asej.2022.101976
S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
design practice and research consider either constant DIF [22–24] diameter and a 300 mm length and were cured according to the
or using the available DIF equations (based on Split-Hopkinson ASTM C39 [37]. Moreover, sixty-six specimens were cast to be
results) [7,8,25–27]. Several pieces of research have been pub- tested under high strain rates using the SHPB machine. The
lished aiming to quantify such absolute strain rate effects dynamic specimens were cylinders of a 75 mm diameter and a
[15,28–30]. 37.5 mm length (L/D = 0.5). The dynamic specimens were cast in
Concrete structures may be exposed to various environmental PVC molds. It is worth mentioning that the dynamic specimens
conditions as a wide range of temperature and moisture content had an extra surface adjustment to ensure parallelism of the spec-
[31]. The effect of moisture content on the concrete response under imens’ surface and to avoid any irregularities that may cause stress
dynamic loads has been the interest of several researchers, how- concentration during the dynamic testing. The surface adjustment
ever, limited data is available [31]. Multiple published articles have was achieved through a grinding machine, clean-cut marble saw,
reported higher DIF for concrete with a higher degree of saturation and finally a flat sander. Eighteen samples out of the sixty-six were
(Sr) which was attributed to the water in the capillary cavities of dried in the oven at 125 °C for 24 h, while twenty-four samples
the concrete [32,33]. Moreover, Rossi and Toutlemonde concluded were submerged in a water container till testing. It is worth men-
experimentally and analytically that at small strain rates, the tioning that the water on the surface of the submerged specimens
Stéfan effect takes place for the propagation of microcracks was removed using wet cotton (just before testing). Finally, the last
[34,35]. However, at higher strain rates, the inertia effect domi- twenty-four samples were left at room temperature. The moisture
nates the behavior of concrete response leading to the higher content of the room temperature specimens was measured for
DIF. Moreover, Cadoni et al. concluded that the free water in the three samples and the average moisture content was found to be
concrete voids may limit the concrete internal cracking and subse- 30% [38].
quently reduce its damage [36]. Although the mentioned investiga-
tions address the influence of moisture content on the DIF, no 2.2. Dynamic specimens sizing
unified constitutive model accounts for such parameters. As such
this paper experimentally evaluates the influence of moisture con- The dimensions of the specimens considered for high strain
tent on the compressive DIF through testing sixty-six concrete testing were selected based on strict criteria to minimize the influ-
specimens subjected to high strain loading. The high strain loading ence of the axial and radial inertia on the test results. The axial
is conducted using a Split-Hopkinson Pressure Bar apparatus that inertia may cause a non-uniform deformation of the specimen in
is manufactured and installed in the Centre for Advanced Materials the axial direction [39]. The presence of high axial inertia may lead
lab in the British University in Egypt. The concrete specimens were to undesirable failure due to the dynamic in-equilibrium at low
tested with the same concrete mix but with different degrees of loading rates. The in-equilibrium failure leads to the specimen’s
saturation (i.e. oven-dry, normal, and fully saturated). Further- premature failure which leads to an underestimating result [40].
more, a statical analysis for the observed results was conducted As such, the specimen thickness was minimized to eliminate the
and calibration factors for the CEB equations are proposed to con- effect of the axial inertia, however, a minimum thickness should
sider the influence of moisture content on the DIF. The calibrated be considered based on the used nominal aggregate size to reliably
model was compared against the current CEB model and backed represent the tested material. Based on the literature, a minimum
by a large experimental database. The proposed equation showed of three particles of the largest aggregate used should be consid-
better predictions for the DIF while considering the concrete mois- ered within the specimen thickness to allow reliable representa-
ture content. tion for the tested material [41]. Subsequently, the specimen
thickness was chosen to be 37.5 mm as the nominal aggregate size
was 10 mm.
2. Experimental work
Moreover, the radial inertia magnifies the friction between the
specimen and the end of the testing bar. This friction may lead to
In this experimental program, the compressive behavior of con-
stress concentration at the edge which in some cases may reach
crete considering different saturation levels (saturated, normal,
270% of the stress at the specimen’s center [42]. This stress concen-
and dry) were investigated at various strain rates. The loading var-
tration is not desirable in experimental testing especially for brittle
ied from quasi-static to high-speed impact loading with strain
material as concrete does not yield and may fracture before record-
rates up to 230 s1. The quasi-static test was performed using a
ing the actual stress capacity. Consequently, the diameter of the
hydraulic machine, while the high strain rate loading was applied
specimens should be minimized to reduce such errors. The speci-
through a Split-Hopkinson Pressure Bar (SHPB) machine. The
men’s dimensions are expressed in the form of length-to-
quasi-static test was performed as a reference datum for the con-
diameter ls/us. The ls/us ratio has upper and lower boundaries to
crete compressive strength. On the other side, smaller cylinders
limit the specimen’s buckling and the effect of radial inertia,
were cast and tested using the SHPB machine considering the min-
respectively [43]. In the quasi-static tests, the specimen ls/us ratio
imum dimensions to eliminate sizing errors as discussed later in
equals 2 to reduce the friction at the ends, while in the dynamic
the paper. The following subsections demonstrate the details of
testing, no well-defined ratio has been suggested [44]. Based on
the experimental program including the specimen’s preparation
the literature, the ls/us ratio has been proposed to vary from 0.5
as well as the test setup and instrumentation. The following sub-
to 1 to minimize the radial inertia, friction effect, and reduce the
sections include the specimen and test setup design procedure
probability of buckling of the specimen [43]. Moreover, a range
and precautions.
varied from 0.3 to 1 was proposed considering the material Pois-
son’s ratio [45]. As such, in this study, the ls/us was taken as 0.5
2.1. Test matrix resulting in a specimen diameter of 75 mm (3 in.) and length of
37.5 mm (1.5 in.).
The concrete tested in this study was designed to achieve a
30 MPa with a slump range of 80–130 mm considering 2.5% 2.3. Test setup and instrumentation
defects. The mixing proportions of the tested concrete are summa-
rized in Table 1. Two specimen configurations were cast in this This section briefly describes the design precautions of manu-
study, namely, the quasi-static and the dynamic specimens. Three facturing the Split-Hopkinson Pressure Bar (SHPB). Generally, the
standard quasi-static concrete cylinders were cast with a 150 mm SHPB consists of a pressure chamber, launching tube, striker, inci-
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S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
Table 1
The mixing proportions of the tested concrete.
dent, and transmitter bars. The SHPB shown in Fig. 1 works As for the launching system, Equation (1) can be used to deter-
through pressurizing air in the pressure chamber, which is released mine the length of the launching tube with corresponding pressure
suddenly to accelerate the striker inside the launching tube. The [46].
striker is responsible to hit the incident bar which transmits the
impact wave to the specimen then finally to the transmitted bar.
e0s 2 L2s mst
The launching tube is used to guide the striker till it hits the inci- P¼ ð1Þ
2 A Lc
dent bar.
The main idea of the SHPB apparatus is to propagate a pressure Where:
wave in the incident bar using a striker that can move with an P is the applied pressure on the striker;
adjustable velocity to strike the incident bar. The created pulse in e0 s is the expected strain rate in the specimen;
the incident bar propagates till hits the specimen and is subse- Ls is the length of the testing specimen;
quently divided into two waves. The first wave is reflected into mst is the mass of the striker;
the incident bar and carries the strain rate response of the speci- A is the striker cross-section area;
men, while the second wave travels through the specimen to the Lc is the striker travel distance inside the launching tube.
transmitted bar and carries the stress response of the specimen. To determine the lengths of the incident and transmitted bars
Subsequently, the stress–strain relation of the specimen under a the wave propagation mechanism should be investigated. At
high strain rate can be obtained using one-dimensional wave anal- (t = 0), when the striker bar hits the incident bar, two compression
ysis. The following section demonstrates the restrictions while waves are generated. One of them is in the incident bar while the
designing the SHPB apparatus. other wave is reflected in the striker bar. The wave in the striker
The transmitted and incident bar diameters are considered as will later propagate towards the incident bar in the form of a ten-
influencing parameters in the design of the SHPB apparatus. First, sile wave that acts as an unloading wave. Both waves define the
the diameter of transmitted and incident bars should be equal to incident pulse that is responsible for loading the testing specimen.
the tested specimen to avoid stress concentration in the specimen Furthermore, a portion of the wave propagates to the transmitted
[42]. Secondly, the designer should avoid any non-linearity for bar, while the other portion reflects into the incident bar as shown
either the transmitted or the incident bar to facilitate the repeata- in the distance-time diagram in Fig. 2. Both waves, in the transmit-
bility of the test. The non-linearity restriction may be controlled ted and incident bars, are responsible for loading the specimen and
through the materials used, using a material with relatively high are used to infer the stress, strain, strain rate. Subsequently, the
yield strength, or by the bars cross-section area, either solid or hol- incident and transmitted bars must be long enough to accommo-
low section. Regarding the non-linearity restrictions, previous date the pulses and avoid the interference of the waves.
studies have recommended not exceeding 30% of the bars yielding To do so, the length of each bar must be greater than or double
stress while testing [44]. This limit is considered as the minimum the length of the striker bar. As such, the strain pulses in the mid-
design limit for selecting the bar’s cross-section area. On the other dle of the incident and transmitted bars are measured, incident (ei),
side, the maximum design limit of the transmitted and incident reflected (er), and transmitted (et) strains. The strains are usually
bars cross-section area is to ensure a measurable strain in the measured using strain gauges, however, it is worth mentioning
transmitted bar. As such Clark (2016), proposed a hollow transmit- that laser extensometer [47], digital image correlations [48], and
ted bar to increase its stress and strain, while testing, which conse- optical measurements [49] have been reported [28]. Subsequently,
quently facilitates the measurement of the strain [40]. the specimen’s stress (rs ), strain (es ), and strain rate (e_s ) can be cal-
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S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
Fig. 2. Time-Distance diagram for the wave propagation in the SHPB apparatus.
culated using Equations (2–4) [50]. Equation (2–4) considers the loaded with a rate of 0.25 ± 0.05 MPa/s following the ASTM C39
two fundamental assumptions of the SHPB apparatus which are [37] representing quasi-static testing [28]. The average concrete
the one-dimensional wave propagation and the instantaneous compressive strength (fc’) was 22.3 MPa with a 0.04 MPa coeffi-
equilibrium of forces on two surfaces of the loaded specimen cient of variation.
[51–53].
3.2. SHPB results
Ab Eb
rs ð t Þ ¼ e t ðt Þ ð2Þ
As
Although most of the samples subjected to high strain rate load-
Z ing had similar failure modes (i.e. concrete crushing). Fig. 3 depicts
2C o t
es ðtÞ ¼ er ðtÞdt ð3Þ the typical failure of the tested specimens using the SHPB. The inci-
L 0
dent, transmitted, and reflected signals were collected using a PC-
2C 0 Based oscilloscope ‘‘DSO-2150 USB” device. Fig. 4a, shows the typ-
e_s ðtÞ ¼ er ðtÞ ð4Þ ical signal processing (i.e. incident and transmitted). The recorded
L
signals were processed using an in-house developed MATLAB code
Where, Ab and Eb are the cross-section area and young’s modu- based on Equations (2–4) to compute the stress, strain, and strain
lus of the transmitted bar respectively, while As and L are the cross- rate [54]. Fig. 5shows the stress–strain curves for the tested spec-
section area and the thickness of the specimen respectively, and imens subjected to high strain rates under different saturation con-
finally Co is the wave velocity. ditions and strain rates ranging from 86 s1 to 230 s1. The analysis
As for the developed SHPB apparatus, a 73/61 mm hollow tube of the observed results will be discussed and analyzed in the fol-
is selected for the transmitted bar (to magnify the transmitted
wave as recommended by Clark (2016) [40]). Whereas an endplate
has been attached to the tube to fit the specimen dimension
(75 mm). The transmitted bar is 1500 mm long satisfying both con-
ditions, twice the striker length, and greater than or equals to 20
times the specimen diameter (75 mm). Similarly, the incident bar
(solid bar) had the same length as the transmitted bar to satisfy
the same conditions for the transmitted bar. Table 2 summarizes
the dimensions of the developed SHPB apparatus.
Table 2
The developed SHPB apparatus dimensions.
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S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
DIF ¼ Ae_ c
B
ð8Þ
Where A, and B are the introduced calibration coefficients. Fur-
thermore, the Sr was introduced into the calibration factors to con-
sider their effect on the calculated DIF. Based in the observed data,
‘‘A” was in a linear relationship with Sr, while ‘‘B” was following an
exponential format as shown in Equation (9). It worth nothing to
mention that the proposed equation is bounded by 1 to overcome
Fig. 4b. Graphical demonstration for typical wave validation. any boundary errors.
5
S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
Fig. 5. Stress–strain curves for the tested specimens (a) Sr = 100%; (b) Sr = 30%;(c) Sr = 0%.
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S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
Table 3
DIF of the tested specimens.
0:275Sr
e_ 0:47e mental results are summarized in Table 4. It is worth nothing to
DIF ¼ ð0:1986 Sr þ 0:1945Þcs c
1 ð9Þ mention that the Sr of the oven-dry samples were introduced in
e_ 1=3
co the proposed equation as negligible value (0.01%) to avoid numer-
The proposed DIF equation showed an average deviation of 3.1, ical errors in the equation.
4.5, and 3.7% for the dry, normal (Sr = 30%), and saturated speci-
mens. Whereas Fig. 8 demonstrates the measured DIF as well as 3.6. Model validation
their corresponding predictions using the CEB/FIP and the pro-
posed equations (i.e., after introducing the Sr as an input variable). As a sort of validation, both DIF prediction equations discussed
Moreover, the mean and standard deviation of the prediction error in this paper (the CEB and the proposed equation) were compared
for both CEB/FIP and the proposed equations against the experi- against experimental database collected from literature. Both
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S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
Fig. 7. Relation between the DIF and strain rate of the tested samples.
Fig. 8. DIF of the tested specimens versus the predicted (using the CEB and the proposed equations).
8
S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
Fig. 9. Error histogram for the proposed and CEB/FIP predictive equations.
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S. Salem, E. Eissa, E. Zarif et al. Ain Shams Engineering Journal xxx (xxxx) xxx
[61] Xiong B, Demartino C, Xu J, Simi A, Marano GC, Xiao Y. High-strain rate [67] Ang A, Tang W. Probability concepts in engineering: emphasis on applications
compressive behavior of concrete made with substituted coarse aggregates: to civil and environmental engineering. 2nd editio. John Wiley & Sons; 2007.
Recycled crushed concrete and clay bricks. Constr Build Mater 2021;301:. doi:
https://doi.org/10.1016/j.conbuildmat.2021.123875123875.
[62] Xiong B, Demartino C, Xiao Y. High-strain rate compressive behavior of CFRP
confined concrete: Large diameter SHPB tests. Constr Build Mater Shady Salem: is a member of the ASCE Risk and Resi-
2019;201:484–501. doi: https://doi.org/10.1016/j.conbuildmat.2018.12.144. lience Measurements committee, the Social Science,
[63] Sparks PR, Menzies JB. The effect of rate of loading upon the static and fatigue Policy, Economics and Education Decision committee,
strengths of plain concrete in compression. Mag Concr Res 1973;25:73–80. and the research committee for The Masonry Society
doi: https://doi.org/10.1680/macr.1973.25.83.73. (TMS). He is also a member SEI blast protection of
[64] Chen X, Wu S, Zhou J. Experimental and modeling study of dynamic buildings standards committee. Dr. Salem has received
mechanical properties of cement paste, mortar and concrete. Constr Build Engineering Mechanics Institute Objective Resilience
Mater 2013;47:419–30. doi: https://doi.org/10.1016/ Award as well as the Outstanding Doctoral Dissertation
j.conbuildmat.2013.05.063. Award. His research interests include community resi-
[65] Guo YB, Gao GF, Jing L, Shim VPW. Response of high-strength concrete to lience, blast design, design of reinforced concrete and
dynamic compressive loading. Int J Impact Eng 2017;108:114–35. doi: https:// masonry structures.
doi.org/10.1016/j.ijimpeng.2017.04.015.
[66] Gary G, Bailly P. Behaviour of quasi-brittle material at high strain rate
experiment and modelling. Eur J Mech 1998;17:403–20.
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