OBJECTIVE OF EXPERIMENT:

1. To learn the qualitative and quantitative aspects of common laboratory equipment.

2. To expose student to the factors that affect the accuracy of an experiment.

CHEMICALS AND APPARATUS:

Distilled water

Analytical balance
Burette
Pipette (20 mL or 25 mL)
Volumetric flask (25mL)
Beaker (50mL)
Thermometer
Pipette filler or suction bulb
Retord stand
Burette clamp
Dropper
PROCEDURE:

A. Calibration of Volumetric Flask

d 2.Distilled water is added

to the calibration mark
(using a dropper to add the
last few drops
of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
and volumetric flasks are
recorded
1. A 25 mL volumetric is cleaned and dried then weighed accurately using
blanced analysis. The mass of empty volumetric flask is recorded.
2. Distilled water is added to the calibration mark (using a dropper to add
last few drops of distilled water) and weighed again. Masses of distilled
water and volumetric flask is recorded.
3. Temperature of the distilled water is recorded.
4. Determine the volume of the actual volumetric flask from Table 1.
B. Calibration of Pipette

Distilled water is added to the

calibration mark (using a
dropper to add the last few
drops
of distilled water) and weighed
again (using the same
balance). Masses of distilled
water
and volumetric flasks are
recorded.
Distilled water is added to
5.

the calibration mark (using

a dropper to add the last
few drops
of distilled water) and
6.

weighed again (using the

 same balance). Masses of
distilled water
7. and volumetric flasks are
recorded.
8. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
9. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
10. and volumetric flasks are
recorded.
11. Distilled water is added to
the calibration mark (using
 a dropper to add the last
few drops
12. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
13. and volumetric flasks are
recorded.
14. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
15. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
16. and volumetric flasks are
recorded.
17. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
18. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
19. and volumetric flasks are
recorded.
20. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
21. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
22. and volumetric flasks are
recorded.
23. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
24. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
25. and volumetric flasks are
recorded.
26. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
27. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
28. and volumetric flasks are
recorded.
29. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
30. of distilled water) and
weighed again (using the
 same balance). Masses of
distilled water
31. and volumetric flasks are
recorded.
32. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
33. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
34. and volumetric flasks are
recorded.
35. Distilled water is added to
the calibration mark (using
 a dropper to add the last
few drops
36. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
37. and volumetric flasks are
recorded.
38. 2.Distilled water is added
to the calibration mark
(using a dropper to add the
last few drops
39. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
40. and volumetric flasks are
recorde3
41. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
42. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
43. and volumetric flasks are
recorded.
44. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
 45. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
46. and volumetric flasks are
recorded.
47. Distilled water is added to
the calibration mark (using
a dropper to add the last
few drops
48. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
49. and volumetric flasks are
recorded.
1. A 50 mL beaker is cleaned and dried then weighed accurately using
balance analysis. The mass of empty beaker is recorded.
 2. A pipette (20 or 25 mL) is cleaned and rinsed with distilled water.
3. A pipette is filled with distilled water using the procedure discussed in
the introduction.
4. Distilled water is poured into the beaker and weighed again. Masses of
distilled water and beakers are recorded.
5. Step 1-4 are repeated again and the temperature of the distilled water is
recorded.
6. Determine the actualvolume of the pipette from Table 1.

C. Calibration of Burette
1. A 50 mL beaker is cleaned and dried and weighed accurately using
balance analysis. The mass of the empty beaker is recorded.
2. A burette is cleaned and rinsed using distilled water and the burette is
filled with distilled water to zero marks. (Make sure there are no
bubbles.)
3. 5 mL of water is poured from the burette into the beaker and weighed
as soon as possible. Mass recorded.
4. Step 3 is repeated by running water from the burette unitl the following
burette readings become 10 mL, 15 mL and 20 mL. (Each time 5 ml of
distilled water has been added from the burette). Mass (distilled water +
beaker) each time after adding 5 mL of water is recorded.
5. The temperature of the distilled water is recorded
6. Determine the actual volume for each addition of 5 mL of distilled
water from Table 1.

7. Distilled water is added to

the calibration mark (using
a dropper to add the last few
drops
8. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
9. and volumetric flasks are
recorded
10. Distilled water is added to
the calibration mark (using
a dropper to add the last few
drops
11. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
12. and volumetric flasks are
recorded
13. Distilled water is added to
the calibration mark (using
a dropper to add the last few
drops
14. of distilled water) and
weighed again (using the
same balance). Masses of
distilled water
15. and volumetric flasks are
recorded
16. Distilled water is added to
the calibration mark (using
a dropper to add the last few
drops
17. of distilled water) and
weighed again (using the
 same balance). Masses of
distilled water
and volumetric flasks are
18.

recorded
 FACULTY OF APPLIED SCIENCES
UiTM CAWANGAN PERLIS

CHM 127 FUNDAMENTAL OF CHEMISTRY

LAB REPORT
EXPERIMENT TITLE :

NAME :

STUDENT ID :

GROUP :

LECTURER :

DATE OF SUBMISSION :

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I/We declare that the lab report submitted is not plagiarised and is entirely my/our own work,
and that no part of it has been copied from any work produced by other person(s)/ source(s)
or provided by any other student(s).

I/We understand that issuing a false declaration can result in severe penalties and I/we
am/are willing to be penalized if any form of copying found valid.
 ___________________________
(STUDENT’S NAME)(STUDENT ID)