CHEMICAL

Distilled water

PROCEDURE
A. Calibration of volumetric flask
1. A 25 ml volumetric flask was cleaned and weighed accurately using analytical balance.
The mass of empty volumetric flask is recorded.
2. The calibration mark was added with distilled water (used a dropper to add the last few
drops of distilled water) and the balance was weight again (used the same balance). The
mass of distilled water and volumetric flask is recorded.
3. The temperature of distilled water was recorded.
4. From the table 1, the actual volume of the volumetric flask was determined.

B. Calibration of Pipette
1. A 50 mL beaker was cleaned and weighed accurately using analytical balance. The mass
of empty beaker is recorded.
2. clean a pipette (20 or 25 mL) and rinse with distilled water.
3. The pipette filled with distilled water used the procedures that had been discussed in
the introduction part.
4. The distilled water was drained into the beaker and weight again. The mass of distilled
water and beaker is recorded.
5. Step 1-4 repeated one more time and the temperature of distilled water and beaker is
recorded.
6. From the table 1, the actual volume of the pipette was determined.

C. Calibration of Burette
1. A 50 mL beaker was cleaned and weight accurately using analytical balance. The mass of
empty beaker is recorded.
2. The burette clean and rinse used distilled water and used distilled water to fill in the
burette until the zero mark (make sure there are no bubbles in the tip of the burette).
3. 5 mL of the water drained from the burette into the beaker and has weight as soon as
possible. The mass is recorded.
4. Step 3 by drained water from the burette until the following burette reading become 10
mL, 15 mL and 20 mL was repeated. (From the burette has been added 5 mL distilled
water each time). The mass (distilled water + beaker) is recorded every time after add 5
mL of water.
5. The temperature of distilled water is recorded.
6. From the table 1, the actual volume for every addition of 5 mL of distilled water has
determined.