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December 2020
ABSTRACT
2
THEORY
1. Introduction
2. Theory
� = 𝑋𝐻
𝑀 � (2)
3
X is the magnetic susceptibility. Relating (1) and (2) gives the magnetic
field [1]
𝐵� = (1 + 𝑋)𝜇0 𝐻
� (3)
1 𝑎
� 2 = 𝑔𝜌𝑆 𝑧 �1 + �
𝜇0 (𝑋𝑆 − 𝑋0 )𝐻 (4)
2 𝐴
2𝑔𝜌
= 𝐻 2 − 𝐻02 (5)
(𝜇0 𝑋)(𝑍 − 𝑍0 )
Where H0 is the residual magnetic field strength when the power supply
is off, and Z0 is the height of the liquid column when the magnetic field is
at H0. If H0 is a constant, Equation (5) can be re-written as [1]
2𝑔𝜌
= 𝐻2 (6)
(𝜇0 𝑋)(𝑍 − 𝑍0 )
The value of X can be calculated from the gradient of the graph of (Z – Z0)
versus H2. [1]
4
Volume susceptibility and mass susceptibility of FeCl3 can be calculated
if density of solution and density of FeCl3 are known. The density of
FeCl3 salt is 2.80 kg/l. The volume susceptibility of FeCl3, XF is given by
[1]
(𝜌𝐹 − 𝜌𝑊 ) (𝜌𝐹 − 𝜌𝑆 )
𝑋𝐹 = 𝑋𝑆 − 𝑋𝑊 (7)
(𝜌𝑆 − 𝜌𝑊 ) (𝜌𝑆 − 𝜌𝑊 )
Note that the volume susceptibility is defined as for unit volume. Mass
susceptibility for a unit mass is defined as [1]
𝑋𝐹
𝐾𝐹 = (8)
𝜌𝐹
5
EXPERIMENTAL METHODOLOGY
Part 1
The power supply is switched on and the current is first set at 0.0 A. The
magnetic flux between the electromagnets’ poles is determined using a
fluxmeter and a search coil. The readings of the magnetic flux is
repeated with increasing current values. Then, the readings of the
magnetic flux is again repeated but with decreasing currents values. The
values of the magnetic flux are recorded and tabulated. [1]
The power supply is switched off. The circuit is reconnected for parallel
connections as shown in Figure 2. [1]
6
Figure 2. Parallel connection.
The readings of the magnetic flux are repeated with increasing current
values and the results are tabulated. Then, the readings of the magnetic
flux are repeated with decreasing current values and the results are also
tabulated. [1]
The calibration graphs (magnetic flux versus current) are plotted, two for
series connection, the other two for parallel connection. [1]
Part 2
The FeCl3 solution is prepared from the provided materials and the mass
of the solution is determined. [1]
One of the calibration graphs of the first part is selected to be used for
the second part. The circuit layout is determined by the choice of the
calibration graph. [1]
The U-tube is filled with FeCl3 solution and the narrow limb of the U-tube
is placed between the electromagnets. The meniscus of the solution is
made sure to be at the centre of the flat pole pieces of the
electromagnets. [1]
7
The change in the liquid column is measured as a function of current.
The experiment is repeated with water. [1]
The experimental values obtained for FeCl3 and distilled water are
tabulated. [1]
8
EXPERIMENTAL DATA
Part 1
Series Circuit
9
Parallel Circuit
10
Part 2
FeCl3
Water
11
DATA ANALYSIS & DISCUSSION
Part 1
Series Circuit
12
For the series circuit, we may find the standard error of the measurement
and thus find the best value for the magnetic flux, conveniently, at
current I = 0 A. It is given that the best value of a quantity is as such [4]
𝑥 = 𝑥̅ ± 𝑆𝑚 (𝑥 ) (9)
𝑆 (𝑥 )
𝑆𝑚 (𝑥 ) = (10)
√𝑁
𝑁
1
𝑆 (𝑥 ) = � �[(𝑥𝑖 − 𝑥̅ )2 ] (11)
𝑁−1
𝑖=1
Deviation, di = Φi
Measurement Value, Φi � di2
-Φ
Series – forward 1.45 -0.085 7.225 x 10-3
Series - reverse 1.62 0.085 7.225 x 10-3
� = 1.535
Φ ∑ 𝑑𝑖2 = 0.01445
It follows that,
� 1 (0.01445)
2−1
𝑆𝑚 (Φ0 ) = = 0.01022
√2
Therefore, the best value for the magnetic flux at I = 0 A, Φ0 for the
series circuit is given as
13
It is observed that the standard error of the magnetic flux in series
connection is substantially minute. One possible reason is it may be due
to the electromagnets receiving equal value of current at any instant of
time for that the current in a series connection is given by I = I1 = I2.
Parallel Circuit
14
For the parallel circuit, we may find the standard error of the
measurement and thus find the best value for the magnetic flux,
conveniently, at current I = 0 A. Likewise, the calculation uses Equation
(9), (10) and (11). [4]
Deviation, di = Φi
Measurement Value, Φi � di2
-Φ
Parallel –
1.59 -0.015 2.25 x 10-4
forward
Parallel -
1.62 0.015 2.25 x 10-4
reverse
� = 1.605
Φ ∑ 𝑑𝑖2 = 4.5 x 10-4
It follows that,
� 1 (4.5 × 10−4 )
2−1
𝑆𝑚 (Φ0 ) = = 3.182 × 10−4
√2
Therefore, the best value for the magnetic flux at I = 0 A, Φ0 for the
parallel circuit is given as
15
Part 2
Figure 7 and Figure 8 shows the graph of (Z – Z0) against H2 for FeCl3
and water, respectively. Both graphs are of forward-current series
connection.
FeCl3
0.006
0.004
0.002
0
-0.05 0 0.05 0.1 0.15 0.2 0.25 0.3
-0.002
X = 0.04
Now, we may find the best value for the magnetic susceptibility, X for
FeCl3. Since X is a derived quantity as of Equation (6), then it suggests
16
that the determination of the error involves the method of error
propagation.
As given, X is a function of (Z – Z0) and H2. It follows that, for FeCl3, the
standard error for (Z – Z0) is given by (0.247 ± 0.05) cm. The 0.247 cm is
obtained from Table 5. The assumption made is as such, all quantities
are taken at I = 0.4 A for the particular current being the median of the
measurement. Whereas, as for the ±0.05 cm, the standard error is
assumed to be of random error measured by a measuring instrument.
Consequently, from Reference [4], it is stated that the corresponding
standard error for a random error is 1/2 of the smallest range of scale of
the measuring instrument used. [4]
Φ
𝐻= (12)
𝑁𝐴𝜇0
Where it is given that N = 100 turns, A = 6.26 x 10-4 m2, and µ0 = 4π x 10-
7
T m A-1. [1] Then, it suggests that the determination of the standard
error for H involves the method of error propagation.
2( )
𝜕𝐻 2 2 1 2 2
𝑆𝑚 𝐻 = � � 𝑆𝑚 (Φ) = � � 𝑆𝑚 (Φ)
𝜕Φ 𝑁𝐴𝜇0
17
2 2
𝑆𝑚 (𝐻 ) 𝑆𝑚 (Φ)
� � =� �
𝐻 Φ
It follows that,
Φ
𝐻= = 267.972 𝑚𝑇
𝑁𝐴𝜇0
Then,
𝑆𝑚 (Φ)
= 4.744 × 10−4
Φ
So,
2
𝑆𝑚 (𝐻 ) 𝑆𝑚 (Φ)
= �� � = �(4.744 × 10−4 )2
𝐻 Φ
Therefore, it is obtained that the best value for the magnetic field
intensity is
H = (267.97 ± 0.13) mT
2
2( )
𝜕𝑋 2 [(
𝜕𝑋 2 2
𝑆𝑚 𝑋 =� � 𝑆𝑚 𝑍 − 𝑍0 )] + � � 𝑆𝑚 (𝐻 )
𝜕(𝑍 − 𝑍0 ) 𝜕𝐻
2
2( )
1 2 2 −2(𝑍 − 𝑍0 ) 2( )
𝑆𝑚 𝑋 = � 2 � 𝑆𝑚 [(𝑍 − 𝑍0 )] + � � 𝑆𝑚 𝐻
𝐻 𝐻3
18
2 2
𝑆𝑚 (𝑋) 1 2 [(
−2 2 2
� � =� � 𝑆 𝑍 − 𝑍0 )] + � � 𝑆𝑚 (𝐻 )
𝑋 (𝑍 − 𝑍0 ) 𝑚 𝐻
As given, (Z – Z0) = (0.247 ± 0.05) cm, H = (267.97 ± 0.13) mT. From the
function X, [1]
(𝑍 − 𝑍0 )
𝑋= (13)
𝐻2
𝑋 = 0.0344
Then,
𝑆𝑚 (𝑍 − 𝑍0 )
= 0.2024
(𝑍 − 𝑍0 )
𝑆𝑚 (𝐻 )
= 4.8513 × 10−4
𝐻
So,
2 2
𝑆𝑚 (𝑋) 𝑆𝑚 (𝑍 − 𝑍0 ) 𝑆𝑚 (𝐻 )
= �� � + �−2 �
𝑋 𝑍 − 𝑍0 𝐻
𝑆𝑚 (𝑋)
= �(0.2024)2 + [(−2)(4.8513 × 10−4 )]2
𝑋
Therefore, it is obtained that the best value for the magnetic susceptibility
of FeCl3 is
19
experiment being conducted and the calculation is close to ideal and
consistent, respectively.
Water
0
-0.05 0 0.05 0.1 0.15 0.2 0.25 0.3
-0.0001
-0.0002
-0.0003
-0.0004
-0.0005
y = -0.0019x - 0.0002
-0.0006
-0.0007
X = -0.0019
Now, we may find the best value for the magnetic susceptibility, X for
water. Since X is a derived quantity as of Equation (6), then it suggests
that the determination of the error involves the method of error
propagation.
20
As given, X is a function of (Z – Z0) and H2. It follows that, for water, the
standard error for (Z – Z0) is given by (-0.036 ± 0.05) cm. The -0.036 cm
is obtained from Table 6. The assumption made is as such, all quantities
are taken at I = 0.4 A for the particular current being the median of the
measurement. Whereas, as for the ±0.05 cm, the standard error is
assumed to be of random error measured by a measuring instrument.
Consequently, from Reference [4], it is stated that the corresponding
standard error for a random error is 1/2 of the smallest range of scale of
the measuring instrument used. [4]
2
2( )
𝜕𝑋 2 [(
𝜕𝑋 2 2
𝑆𝑚 𝑋 =� � 𝑆𝑚 𝑍 − 𝑍0 )] + � � 𝑆𝑚 (𝐻 )
𝜕(𝑍 − 𝑍0 ) 𝜕𝐻
2
2( )
1 2 2 −2(𝑍 − 𝑍0 ) 2( )
𝑆𝑚 𝑋 = � 2 � 𝑆𝑚 [(𝑍 − 𝑍0 )] + � 3
� 𝑆𝑚 𝐻
𝐻 𝐻
2 2
𝑆𝑚 (𝑋) 1 2 [(
−2 2 2
� � =� � 𝑆 𝑍 − 𝑍0 )] + � � 𝑆𝑚 (𝐻 )
𝑋 (𝑍 − 𝑍0 ) 𝑚 𝐻
(𝑍 − 𝑍0 )
𝑋= 2
= −5.0134 × 10−3
𝐻
Then,
𝑆𝑚 (𝑍 − 𝑍0 )
= −1.3889
(𝑍 − 𝑍0 )
21
𝑆𝑚 (𝐻 )
= 4.8513 × 10−4
𝐻
So,
2 2
𝑆𝑚 (𝑋) 𝑆𝑚 (𝑍 − 𝑍0 ) 𝑆𝑚 (𝐻 )
= �� � + �−2 �
𝑋 𝑍 − 𝑍0 𝐻
𝑆𝑚 (𝑋)
= �(−1.3889)2 + [(−2)(4.8513 × 10−4 )]2
𝑋
Therefore, it is obtained that the best value for the magnetic susceptibility
of water is
22
Volume and Mass Susceptibilities
(𝜌𝐹 − 𝜌𝑊 ) (𝜌𝐹 − 𝜌𝑆 )
𝑋𝐹 = 𝑋𝑆 − 𝑋𝑊
(𝜌𝑆 − 𝜌𝑊 ) (𝜌𝑆 − 𝜌𝑊 )
1
𝑋𝐹 = ([𝑋𝑠 (𝜌𝐹 − 𝜌𝑊 )] + 𝑋𝑊 𝜌𝑆 − 𝑋𝑊 𝜌𝐹 )
𝜌𝑠 − 𝜌𝑊
1 133
𝑋𝐹 = �1800𝑋𝑆 − 0.0019𝜌𝑆 + �
𝜌𝑠 − 1000 25
It follows that, from Equation (8), the mass susceptibility of FeCl3 is given
by
𝑋𝐹
𝐾𝐹 =
𝜌𝐹
1 133
𝐾𝐹 = �1800𝑋𝑆 − 0.0019𝜌𝑆 + �
[2800𝜌𝑆 − (2.80 × 106 )] 25
It is for certain that both the volume and mass susceptibilities of FeCl3
can be determined provided XS and ρS are known.
23
CONCLUSION
For part 1, all the calibration graphs of magnetic flux against current are
plotted and the relationships are sufficed to say linear. The best value for
magnetic flux is obtained at I = 0 A. For series connection, Φ0 = (1.54 ±
0.01) x 10-6 mWb. For parallel connection, Φ0 = [(1.61 x 10-6) ± (3.18 x
10-4)] mWb. The standard error for series connection is minute and is
probably due to the electromagnets receiving equal value of current, for I
= I1 = I2. The standard error for parallel connection is relatively large and
is speculated for the electromagnets receiving different values of current,
for I = V (1/R1 + 1/R2) and also for the heat generated further differ the
resistance.
For part 2, the series connection with forward current is chose. The
graph of (Z – Z0) against H2 is plotted for FeCl3 and water. It is obtained
that FeCl3 is paramagnetic and water is diamagnetic. In particular, for
FeCl3, X = 0.04 ± (6.76 x 10-6). Whereas, for water, X = - (1.9 ± 7.0) x 10-
3
. The standard error for magnetic susceptibility of FeCl3 is minute and it
may suggest that both the experiment conducted and the method of
calculation are consistent. The standard error for magnetic susceptibility
of water is substantially large and it may be due to the suspected
mathematical error arose from the point at H2 = 0 for which the
corresponding (Z – Z0) value is too far off from the best-fit line.
24
REFERENCES
25
ATTACHMENT
26
Exported excel sheet for the graph of Figure 3.
Current Flux
(A) (10^-6) Flux
0 1.45 0.00000145
0.1 5.95 0.00000595
0.2 11.04 0.00001104
0.3 16.2 0.0000162
0.4 21.08 0.00002108
0.5 25.63 0.00002563
0.6 29.87 0.00002987
0.7 33.75 0.00003375
0.8 36.87 0.00003687
Current Flux
(A) (10^-6) Flux
0.8 36.77 0.00003677
0.7 34.09 0.00003409
0.6 30.69 0.00003069
0.5 26.72 0.00002672
0.4 22.33 0.00002233
0.3 17.65 0.00001765
0.2 12.57 0.00001257
0.1 7.09 0.00000709
0 1.62 0.00000162
Current Flux
(A) (10^-6) Flux
0 1.59 0.00000159
0.1 3.74 0.00000374
0.2 6.01 0.00000601
0.3 8.49 0.00000849
0.4 11.11 0.00001111
0.5 13.64 0.00001364
0.6 16.08 0.00001608
0.7 18.52 0.00001852
0.8 20.91 0.00002091
27
Exported excel sheet for the graph of Figure 6.
Current Flux
(A) (10^-6) Flux
0.8 20.8 0.0000208
0.7 18.91 1.891E-05
0.6 16.8 0.0000168
0.5 14.59 1.459E-05
0.4 12.13 1.213E-05
0.3 9.61 9.61E-06
0.2 6.87 6.87E-06
0.1 4.21 4.21E-06
0 1.62 1.62E-06
Flux (for
Current Z (cm) Z (m) Z-Z_0 ser) H (mT) H (T) H^2
1.45E-
0 3.05 0.0305 0 06 18.43259 0.018433 0.00034
5.95E-
0.1 3.085 0.03085 0.00035 06 75.6372 0.075637 0.005721
0.2 3.159 0.03159 0.00109 1.1E-05 140.342 0.140342 0.019696
1.62E-
0.3 3.249 0.03249 0.00199 05 205.9366 0.205937 0.04241
2.11E-
0.4 3.297 0.03297 0.00247 05 267.9718 0.267972 0.071809
2.56E-
0.5 3.551 0.03551 0.00501 05 325.812 0.325812 0.106153
2.99E-
0.6 3.704 0.03704 0.00654 05 379.7114 0.379711 0.144181
3.38E-
0.7 3.839 0.03839 0.00789 05 429.0345 0.429035 0.184071
3.69E-
0.8 3.873 0.03873 0.00823 05 468.6964 0.468696 0.219676
28
Exported excel sheet for the graph of Figure 8.
Flux (for
Current Z (cm) Z (m) Z-Z_0 ser) H (mT) H (T) H^2
1.45E-
0 3.323 0.03323 0 06 18.43259 0.018433 0.00034
- 5.95E-
0.1 3.3 0.033 0.00023 06 75.6372 0.075637 0.005721
-
0.2 3.299 0.03299 0.00024 1.1E-05 140.342 0.140342 0.019696
- 1.62E-
0.3 3.295 0.03295 0.00028 05 205.9366 0.205937 0.04241
- 2.11E-
0.4 3.287 0.03287 0.00036 05 267.9718 0.267972 0.071809
- 2.56E-
0.5 3.282 0.03282 0.00041 05 325.812 0.325812 0.106153
- 2.99E-
0.6 3.279 0.03279 0.00044 05 379.7114 0.379711 0.144181
- 3.38E-
0.7 3.274 0.03274 0.00049 05 429.0345 0.429035 0.184071
- 3.69E-
0.8 3.269 0.03269 0.00054 05 468.6964 0.468696 0.219676
29