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Comparative study between wear of uncoated and TiAlN-coated carbide tools


in milling of Ti6Al4V

Article  in  Advances in Manufacturing · December 2017


DOI: 10.1007/s40436-016-0166-1

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Adv. Manuf. (2017) 5:83–91
DOI 10.1007/s40436-016-0166-1

Comparative study between wear of uncoated and TiAlN-coated


carbide tools in milling of Ti6Al4V
M. S. Uddin1 • Binh Pham1 • Ahmed Sarhan2 • Animesh Basak3 • Alokesh Pramanik4

Received: 20 July 2016 / Accepted: 19 December 2016 / Published online: 18 February 2017
Ó Shanghai University and Springer-Verlag Berlin Heidelberg 2017

Abstract As is recognized widely, tool wear is a major researchers, and further imply that coated tools with
problem in the machining of difficult-to-cut titanium appropriate combinations of cutting parameters would be
alloys. Therefore, it is of significant interest and impor- able to increase the tool life in cutting of titanium alloys.
tance to understand and determine quantitatively and
qualitatively tool wear evolution and the underlying wear Keywords Tool wear  Titanium alloy  Tungsten carbide
mechanisms. The main aim of this paper is to investigate tool  Wear mechanism  High speed machining
and analyse wear, wear mechanisms and surface and chip
generation of uncoated and TiAlN-coated carbide tools in a
dry milling of Ti6Al4V alloys. The quantitative flank wear 1 Introduction
and roughness were measured and recorded. Optical and
scanning electron microscopy (SEM) observations of the Due to their excellent strength to weight ratio, toughness at
tool cutting edge, machined surface and chips were con- high temperature, and corrosion resistance, titanium alloys
ducted. The results show that the TiAlN-coated tool exhi- (e.g., Ti6Al4V) have attracted tremendous attention and
bits an approximately 44% longer tool life than the been extensively applied as structural components in
uncoated tool at a cutting distance of 16 m. A more regular aerospace and biomedical industries [1, 2]. Machining as a
progressive abrasion between the flank face of the tool and mechanical processing technique has been one of fast and
the workpiece is found to be the underlying wear mecha- effective operations in manufacturing to provide the final
nism. The TiAlN-coated tool generates a smooth machined shape of such components with required geometric accu-
surface with 31% lower roughness than the uncoated tool. racy and finish. However, the key challenge is the difficulty
As is expected, both tools generate serrated chips. How- to cut or shape titanium alloy materials due to their very
ever, the burnt chips with blue color are noticed for the low thermal conductivity [3]. As a result, a high tempera-
uncoated tool as the cutting continues further. The results ture is generated at the cutting zone, which affects the
are shown to be consistent with observation of other cutting tool life (i.e., wear performance) and surface
integrity of the final product. In the past, different types of
cutting tool materials along with combinations of various
& M. S. Uddin cutting parameters and environments have been investi-
Mohammad.Uddin@unisa.edu.au
gated in cutting of titanium alloys. The cutting tools
1
School of Engineering, University of South Australia, studied are made of carbide, high-speed steel (HSS), dia-
Mawson Lakes, SA 5095, Australia mond, while cutting speed and feed rate have been the
2
Department of Mechanical Engineering, University of dominating parameters influencing the machinability of
Malaya, Kuala Lumpur, Malaysia titanium alloys [4, 5]. A common consensus in evaluating
3
Adelaide Microscopy Unit, University of Adelaide, Adelaide, the machinability is that the cutting tool wear is the major
SA 5005, Australia factor, affecting the manufacturing productivity as a result
4
Department of Mechanical Engineering, Curtin University of of the underlying interaction and mechanics between the
Technology, Bently, WA 6845, Australia tool and the workpiece. Among many tools, tungsten

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84 M. S. Uddin et al.

carbide has been a good choice and widely used cutting tool This understanding also allows one to design and develop
in the machining industries due to its high strength and wear better cutting tool materials. The importance of the effect
resistance [6]. The carbide tools are made of tungsten carbide of tool wear on the machinability is stressed by a wider
(WC) with cobalt (Co) binders via compacting and sintering, community of machining researchers [4, 18].
making the material hard and resilient to heat and wear [7]. Keeping this spirit in mind, this paper focuses on further
The composition of WC-Co is often varied to produce the investigation and analysis of the wear and wear mecha-
tool with required mechanical and tribological properties. nisms of uncoated and TiAlN-coated tungsten carbide tools
While diamond tools (e.g., polycrystalline diamond (PCD)) in cutting of Ti6Al4V alloys in dry conditions. To follow
offer relatively improved machining performance in terms of up and measure consistent wear development, a series of
tool life, they are quite expensive and may not be affordable side milling operations with the same cutting parameters
for mass manufacturing [8, 9]. As a result, tungsten carbide were performed. Cutting edge wear, surface roughness and
has shown tremendous potential in high speed cutting of chips were observed and measured at a certain interval of
titanium alloys. Over the years, carbide tools have been cutting distance (often noted as cutting time). The results
studied in cutting of titanium alloys with a focus on under- are discussed and analyzed with respect to the findings
standing of wear and the associated wear mechanisms available in the literature.
[10, 11]. In the cutting of non-ferrous metals, abrasion,
adhesion, attrition and diffusion are shown to be typical wear
mechanisms, of which adhesion and diffusion are often cited 2 Experimental details
as the dominating effects, particularly, when machining of
titanium. Ghani et al. [12] studied the effects of various high 2.1 Workpieces
cutting speeds (120–135 m/min) on carbide tool wear in the
cutting of titanium and reported that higher speed caused The machining was conducted on the workpieces made of
brittle fracture and cracking of the tool edge due to high Ti6Al4V alloys. The chemical compositions and mechan-
temperature induced stress concentration and intermittent ical properties of the material are presented in Tables 1 and
fast thermal loading. They recommended suitable conserva- 2. The as-received material block was cut into a size of 100
tive cutting parameters to minimize tool wear effects. Har- mm 9 100 mm 9 80 mm (L 9 W 9 H). The top and
tung et al. [13] showed that crater wear due to adhesive layers bottom surfaces of the specimen were further rough
on the rake face was more dominant at lower cutting speeds machined with a very shallow cut to clean and even out the
(61–122 m/min), while the tool failed due to plastic defor- surfaces. This process used a 60 mm diameter solid carbide
mation at high cutting speeds (122–610 m/min). Adhesive indexed cutter running with a feed rate of 500 mm/min and
layers are formed due to the chemical reaction between a spindle speed of 1 200 r/min.
titanium and carbide particles via diffusion, which essen-
tially decreases the toughness of the tool edge. Generally, 2.2 Cutting tools
different tool materials behave differently according to dif-
ferent wear mechanisms. In this regard, hard and wear As cutters, two types of tungsten carbide end mills are
resistant coatings, e.g., TiN, TiCN, are applied to the tool used. One is uncoated (Hanita D014 supplied by Wahida
edge to improve the performance. Surprisingly, Ezugwu and Inc., Japan) and the other is coated with TiAlN via physical
Wang [14] found that the uncoated tool outperformed the vapor deposition (PVD) method (KCPM 15 is supplied by
coated tool in cutting of titanium. This finding was contra- Kennametal Inc., USA). The geometric dimension of both
dictory to the findings of other researchers [15]. Wear due to cutters is as follows: diameter D1 = 12 mm, number of
the elemental diffusion-dissolution through the tool-chip of flutes = 4, total length L = 83 mm, working length l = 26
carbide tools at high cutting speeds was further emphasized mm, helix angle = 30°, axial rake angle = 6° and secondary
in Ref. [16]. In a dry cutting of titanium alloy, Gerez et al. clearance angle = 15°. Figure 1 shows photographs of both
[17] observed that an adhesive layer or built up edge gen- the coated and uncoated carbide cutters used. The physical
erated at low cutting speeds often acted as a lubricant, min- and mechanical properties of the tungsten carbide and
imizing abrasion. However, the layers were momentarily TiAlN-coated tools are summarized in Tables 3 and 4.
removed at high cutting speeds, hence accelerating abrasion Before actual cutting tests, the edges of the cutters are
at the tool-rake interface. observed to be sharp and clean without any dirt.
Therefore, it is clear that insightful understanding of the
wear development and mechanisms is becoming more 2.3 Experimental
important to determine the limit of the tool capability,
enabling one to predict the onset of generation of degraded Using a CNC 4-axis vertical milling machine (Bridgeport’s
surface due to a worn-out/failed cutting edge of the tool. VMC 480PS, USA), a series of side milling operations

123
Comparative study between wear of uncoated and TiAlN-coated carbide tools in milling of Ti6Al4V 85

Table 1 Chemical composition of Ti6Al4V alloy


Element w(Ti)/% w(Al)/% w(V)/% w(Fe)/% w(C)/% w(N)/% w(H)/% w(O)/%

Value Balance 6.15 4.40 0.09 0.05 0.01 0.005 –

Table 2 Mechanical properties of Ti6Al4V alloy at room temperature of 25 °C


Hardness (HRC) Elastic modulus/GPa Yield strength/MPa Tensile strength/MPa Density/(kgm-3)

36 114 830 993 4 540

were performed on the workpiece. Figure 2 depicts to machine, higher cutting speed and feed rate are con-
experimental setup and illustration of cutting paths con- sidered. The cutting parameters used are as follows: cutting
sidered during tests. As titanium alloy is hard and difficult speed v = 80 m/min, feed rate f = 0.2 mm/r, width of cut d =
1 mm. During machining, the cutter was engaged with the
workpiece at 10 mm depth along the tool axis direction,
i.e., axial depth was 10 mm (see Fig. 2). The cutting con-
ditions were kept constant for machining with both types of
cutters. In order to understand the tool wear performance,
the cutter was observed at a certain interval of the cutting
length. To do this, the cutter was taken out of the spindle
head and the tool holder, and examined under microscopes.
A cutting length interval of 1 m was considered for the
uncoated cutter while a cutting length of 2 m was used for
the coated cutter. As it is expected that the coated one will
experience less wear as the cutting progresses. The flank
wear and wear mechanism were observed, measured and
recorded by an optical microscope equipped with high
resolution camera (Wild Heedbrugg’s Wild M20, V =
1.4X, Switzerland). Cutting chips were collected to
understand and observe the effect of tool wear on the
change of temperature in cutting zone. The topology of the
tool, machined surface and chips were further observed by
scanning electron microscopy (SEM) (FEI’s Quanta 450
equipped with EDX capability, Netherlands). The process
was repeated until the cutters reached closer to failure (i.e.,
average VB = 0.3 mm) according to the failure criterion
[19]. Note that the notation VB was generally defined as the
Fig. 1 Tungsten carbide end mills used in the tests height of the flank wear region of the cutting tool. All the

Table 3 Physical and mechanical properties of tungsten carbide end mill


Hardness (HV10) at 25 °C Density/(gm-3) Elastic modulus/GPa Thermal expansion rate/K-1 Particle size/lm

1 470 14.5 580 GPa 5.5 9 10-6 0.8

Table 4 Physical properties of the TiAlN coating


Type Material Thickness/lm Melting point/°C Hardness (HV10) at 25 °C

PVD TiAlN 4 3 070 2 300

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86 M. S. Uddin et al.

Fig. 2 Experimental setup and cutting paths used in milling tests

machining was performed in dry environment without using flank wear progression with respect to the cutting length for
any external coolant or lubricant. In addition to wear, the the uncoated and coated tools. It can be seen from Fig. 3
arithmetic average roughness (Ra) of the machined surface that, as the cutting length increases, TiAlN-coated carbide
was measured by a roughness tester (Mitutoyo’s Surftest SJ- tool exhibits a lower wear than the uncoated tool. For
210, cut-off length 2.5 mm, contact mode, stylus tip radius 5 instance, after a cutting of 10 m, the coated tool reaches a
lm, JIS-B0601 standard, Japan). The roughness values on wear value of 0.143 6 mm, which is about 32% smaller
five locations of the surface were measured and their than that of the uncoated tool wear (0.21 mm). The coated
average was considered. The same experimental procedure tool can cut up to 22 m in length with wear progression of
was followed for the cutting tests with both uncoated and about 0.23 mm, while the uncoated tool reaches wear of
TiAlN-coated tungsten carbide cutters. about 0.321 mm (i.e., failure criterion) at a shorter cutting
distance of 16 m. Overall, the coated tool, generally after a
cutting of 16 m, shows an enhancement of tool life by
3 Results and discussions about 44% over that of its counterpart. Further, a cutting
tool generally follows a three region wear characteristics:
3.1 Tool wear initial wear zone with relatively high wear, steady state
wear region and accelerated wear region leading to failure
The main focus is to investigate the tool wear and wear [20]. As shown in Fig. 3, both the uncoated and coated
mechanism associated with machining titanium alloy. In tools show approximately three wear zones as indicated by
general, the cutting tests continue until the tool reaches a the A-B-C and A0 -B0 -C0 areas, respectively. The initial wear
standard failure criterion, i.e., average flank wear is 0.3 mm rate of the uncoated tool is larger than that of the coated
for carbide tool. Figure 3 depicts a comparison of the tool tool as the slope of the curve in A zone is shown to be
relatively high. Further, the steady state wear region for the
uncoated tool starts after about a cutting distance of 3.5 m,
while for the coated tool it starts after cutting of 2 m. The
stability of the region is longer than that of the uncoated
one. This comparison indicates that the TiAlN-coated tool
exhibits a better tool life or wear resistance and can be
safely used for a greater cutting length in machining of
titanium alloys. Moreover, the findings are consistent with
those of other researchers [21, 22].

3.2 Wear mechanisms

In order to evaluate the machining performance of the


Fig. 3 Comparison of the uncoated and TiAlN-coated tool wear
cutting tools, an understanding of the underlying wear
progress as a function of cutting length mechanisms is essential. The wear and wear mechanism

123
Comparative study between wear of uncoated and TiAlN-coated carbide tools in milling of Ti6Al4V 87

Fig. 4 Wear in uncoated carbide tool at a cutting length of 16 m a abrasion on flank land b chipping/plastic deformation on cutting edge c BUEs

vary with the combination and interaction of the cutting minor wear marks on the flank land, as shown in Fig. 5a.
tool and the workpiece, in addition to the cutting envi- The observed gradual flank wear can be due to the
ronment. As titanium is hard material, the wear mecha- increased wear resistance of the TiAlN coating during
nisms that influence the failure of carbide tools may be continuous abrasion of the tool with the workpiece.
different from those when machining other materials. As a Similar progressive wear on the flank region for the
representative example, Fig. 4a shows SEM images of the coated tool in cutting of titanium was reported by Dhar
flank wear land of the uncoated tool after a cutting of 16 m. et al. [21]. No significant chipping and fracture on the
A large abrasive wear region along the cutting edge is cutting edge were observed. But, similar to uncoated one,
observed on the uncoated tool. As the wear increases, the sticky BUEs are noticed on the cutting edge. However, it
onset of tool failure is initiated by small edge chipping and/ is notable that the coating on the cutting edge appears to
or plastic deformation as seen in Fig. 4b. This chipping is come off due to the continuous abrasion between the
due to the increased friction because of wear causing workpiece (including BUE) and the tool (see Fig. 5b). As
thermal stress at the edge. Built up edges (BUEs) due to reported by König et al. [23], accelerated adhesion took
adhesion between the tool and the workpiece materials are place after the coating had been removed due to pro-
noticed on the cutting edge and flank region (see Fig. 4c), longed cutting. In such a case, the adhered material was
which are expected to potentially further accelerate abra- hit and squashed by the tool in the event of re-entry into
sion and friction between the tool and workpiece, and the workpiece, resulting in chipping and eventually
result in increased wear. leading to the breakage of carbide at the cutting edge. The
For the same cutting distance, the cutting edge of the adhering metal was often noticed on the flank face rather
coated tool appears to be very smooth with very small or than on the rake face. This finding clearly supports our

123
88 M. S. Uddin et al.

Fig. 5 Wear in TiAlN coated carbide tool at a cutting length of 16 m a flank wear with BUEs b removal of coating due to abrasion

observation and analysis on the wear and wear mecha- Similar wear mechanisms with an extensive EDX analysis
nism of the uncoated and coated carbide tools. of chemical compositions and their diffusions of BUE
In this study, we employed a single set of relatively materials in the cutting of titanium alloys were reported in
conservative-medium cutting conditions (speed of 80 Ref. [26]. Note that, in this study, the crater wear region is
m/min, feed rate of 0.1 mm/r), and no severity of the tool not of interest as at low cutting speed, flank wear is often
damage or failure was noticed for the coated tool even after regarded as the dominant indicator of tool wear perfor-
a cutting of 22 m. However, at a cutting speed of more than mance [10].
100 m/min, cutting edge cracking and brittle fracture due to In a dry cutting, reduction of cutting induced tempera-
high stress concentration because of high temperature are ture is essential to sustain tool life. While the use of cutting
often regarded as the major reasons for tool failure [15]. lubricants and coolants is found for certain extent, the
This phenomenon has been reiterated and observed by design of heat and wear resistant tool material with low
many researchers [10, 11, 24]. In particular, Ghani et al. friction needs to be developed to minimize the cutting
[12] recently reported that cutting titanium at a speed of temperature. In addition, proper choice of cutting param-
120–135 m/min was likely to induce high temperature at eters including cutting speed and feed rate, which are
the cutting edge, which weakened the micro-bonding shown to be the most dominating factors in influencing the
between the carbide particles and their binders, thus tool failure, needs to be sought in order to improve the
resulting in early brittle fracture at the nose of the tool. machinability of titanium alloys.
As seen in Fig. 5b, the TiAlN coating is expected to be
diffused and removed from the cutting edge. Thus, the part 3.3 Surface roughness and cutting chips
of the tool which is engaged with the workpiece becomes
uncoated causing the tungsten carbide to be exposed at the The surface roughness and cutting chips were investigated
cutting zone. This suggestion can be further supported by as a measure of the tool performance. Figure 7 illustrates
the presence of fairly large amount of Ti on the tool edge roughness average of machined surface for uncoated and
detected by EDX and illustrated in Fig. 6. Diffusion of the coated tools with respect to the cutting length. It can be
coating materials into the workpiece/chips resulting in tool seen that at a cutting distance of up to 2 m, the uncoated
failure has been reported by researchers. In an extensive and coated tools exhibit almost the same roughness (Ra =
study by Odelros [25], EDX analysis revealed a high 1.88 lm). After this, the uncoated tool shows a drastic
content of Ti in the particles that adhered to the cutting increase in roughness as compared to the coated tool as the
tool, indicating that the detected Ti content was due to the cutting length increases. For instance, at a cutting length of
underlying chemical reaction between the coating material 16 m, the roughness for the coated tool is about 31% lower
and titanium alloy. It is notable that these adhered layers of than that for the uncoated tool. It is to be pointed that the
materials (often termed as BUE) cause furthur abrasion larger roughness with the uncoated tool is due to severe
between the tool and cutting chips/workpiece, hence flank wear on the cutting edge, as observed in Fig. 4. Wear
resulting in accelerated wear on the flank face of the tool. further causes large cutting forces, hence accelerating

123
Comparative study between wear of uncoated and TiAlN-coated carbide tools in milling of Ti6Al4V 89

Fig. 6 EDX analysis of the elements on the coated tool surface

surface topology for the uncoated and coated tools at a


cutting distance of 16 m. The uncoated tool reveals some
unexpected dents and dirt on the surface, causing a larger
roughness (Ra = 2.89 lm). On the other hand, the surface
machined and the coated tool appears to be relatively
smooth with fine cutting marks with a roughness of Ra =
2.21 lm. The results clearly indicate that, in addition to
prolonged tool life, the TiAlN-coated tool is able to gen-
erate improved surface quality.
Further, cutting chips or swarf generated at the cutting
zone were collected and observed by optical microscopy.
Figure 9 shows the chips generated by uncoated and
Fig. 7 Comparison of surface roughness between uncoated and TiAlN-coated tools at a cutting distance of 16 m. More
TiAlN-coated tools discontinuous and fracture chips are noticed for the
uncoated tool (see Fig. 9a). Further, burnt chips with blue
development of micro fracture and chipping at the cutting color are observed, which could be due to the heat gener-
edge, and as a result of this, an uneven machined surface is ated at the cutting zone of the blunted tool due to wear. On
generated [27]. Figure 8 shows SEM images of machined the other hand, the coated tool generates fairly continuous

Fig. 8 SEM photos of machined surface topology at a cutting distance of 16 m for a uncoated tool and b TiAlN coated tool

123
90 M. S. Uddin et al.

Fig. 9 Optical microscopic photos of chips formed by a uncoated tool, b TiAlN coated tool at a cutting length of 16 m and c magnified SEM
photo of the chips

and unbroken chips (see Fig. 9b). Interestingly, chips 4 Conclusions


generated by both tools appear to be of the saw tooth or
serrated type, as shown in Fig. 9c. Mechanisms and This paper has focused on an investigation and comparison
modelling of serrated chips generated during cutting of of the wear progression and wear mechanism of uncoated
titanium alloys were widely reported and confirmed by and TiAlN coated tungsten carbide tools in high speed
many research works in Refs. [28–31]. It is shown that cutting of Ti6Al4V alloy. The followings are the key
the small initial chip thickness and large rake angle affect conclusions drawn from this study.
the generation and geometry of regular serrated chips
(i) The TiAlN coated tool exhibits improved tool life
[32]. While the initial thickness is related to the feed rate
with approximately 44% lower flank wear than the
to be chosen, the actual chip thickness during the cutting
uncoated tool at a cutting distance of 16 m.
can be affected by the cutting edge of the associated tool.
(ii) A more regular progressive abrasion between the
Therefore, it is possible that the severe tool wear at the
flank face of the tool and workpiece is found. The
cutting edge may influence the geometry of the serrated
underlying wear mechanism and small edge
chips. Hence, in order to minimize the serrated chipping,
chipping and/or plastic deformation for prolonged
the tool wear must be regulated to an acceptable level
cutting are noticed for the uncoated tool.
without sacrificing machining productivity. With this aim,
(iii) Diffusion as a form of BUEs due to the chemical
one possible solution is to develop a predictive model of
reaction between the coating and the workpiece
the energy efficient machining of titanium alloys by
materials at high cutting temperature is shown to
controlling inherent cutting temperature and vibration
cause the removal of coating from the tool, and
generated [33], which will allow the optimum machining
weakez the cutting edge, which may result in
conditions including cutting parameters to be chosen to
further acceleration of potential failures.
enhance the tool life.

123
Comparative study between wear of uncoated and TiAlN-coated carbide tools in milling of Ti6Al4V 91

(iv) The TiAlN coated tool generates smooth 16. Deng JX, Li YS, Song WL (2008) Diffusion wear in dry cutting
machined surface with 31% lower roughness over of Ti-6Al-4V with WC/Co carbide tools. Wear 265(11–12):
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