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This is to attest that

ANALYTICAL LABORATORY E.I.R.L


AV. GUARDIA CHALACA NO 1877 BELLAVISTA - PROV. CONSTITUCIONAL DEL CALLAO
LIMA, 07001, REPUBLIC OF PERU

Testing Laboratory TL-833

has met the requirements of AC89, IAS Accreditation Criteria for Testing Laboratories, and has demonstrated compliance
with ISO/IEC Standard 17025:2017, General requirements for the competence of testing and calibration laboratories. This
organization is accredited to provide the services specified in the scope of accreditation.

Effective Date November 4, 2022

President

IAS is an ILAC MRA Signatory


ANALYTICAL LABORATORY E.I.R.L
www.alab.com.pe

Contact Name Lucio Capcha Contact Phone + +51-949998382


Accredited to ISO/IEC 17025:2017 Effective Date November 4, 2022

FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD


TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils, Sediment and Total Metals EPA METHOD 3050B, Rev.
CHEMISTRY - Sludge Ag, Al, Ba, Be, Ca, Cd, Co, 2,1996 / EPA METHOD 200.7,
INORGANIC Cr, Cu, Fe, K, Mg, Mn, Mo, Rev. 4.4,1994
(Field collection + Lab Na, Ni, Pb, Sb, Tl, V, Zn, B, Acid Digestion of Sediments,
Testing) Si and SiO2 (by Sludges, and Solis
calculation) Determination of Metals and
Trace Elements in Water and
Wastes by Inductively Coupled
Plasma-Atomic Emission
Spectrometry

Total Metals EPA METHOD 3050B, Rev.


Validated: As, Bi, Ce, Li, P, 2,1996 / EPA METHOD 200.7,
Se, Sn, Sr, Ti, U Rev. 4.4,1994.
VALIDATED (Applied out of
reach), 2018
Metals: EPA METHOD 6020B, Rev.2,
Ag, Al, As, Ba, Be, Cd, Cr, 2014 / EPA METHOD 3050B
Co, Cu, Mn, Ni, Pb, Sb, Se, Rev. 2, 1996.
Tl, V, Zn, Hg. Inductively coupled plasma—
mass spectrometry / Acid
Digestion of Sediments,
Sludges, and Soils

Metals: EPA METHOD 6020B, Rev.2,


Validated: B, Ca, Ce, Fe, K, 2014 / EPA METHOD 3050B
Li, Mg, Mo, Na, P, Si, Sn, Rev. 2, 1996.
Sr, Ti, Bi, U, Th VALIDATED (Applied out of
reach), 2020.
n-Hexane Extractable EPA Method 9071B, Rev.2,
Material 1998.
n-Hexane extractable material
(HEM) for sludge, sediment and
solid samples

Effective Date November 4, 2022


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ANALYTICAL LABORATORY Page 2 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils, Sediment and True Total Barium Alberta Environment 2009
CHEMISTRY - Sludge (ISBN No. 978-0-7785-7691-4)
INORGANIC (cont’d.) / EPA Method 200.7 Rev.4.4 -
(Field collection + Lab 1994 (VALIDATED)
Testing)
(cont’d.) Soil Remediation Guidelines for
Barite: Environmental Health
and Human Health. Section
2.2.1. Soil (Fusion Methods),
9.1.3 True Total Barium
EPA Method 200.7 Rev.4.4 -
1994 Determination of Metals
and Trace Elements in Water
and Wastes by Inductively
Coupled Plasma-Atomic
Emission Spectrometry
Extractable Barium Alberta Environment 2009
(ISBN No. 978-0-7785-7691-4)
/ EPA Method 200.7 Rev.4.4 -
1994 (VALIDATED)

Soil Remediation Guidelines for


Barite: Environmental Health
and Human Health. Section
6.2.2 Analytical Method for
Extractable Barium
EPA Method 200.7 Rev.4.4 -
1994 Determination of Metals
and Trace Elements in Water
and Wastes by Inductively
Coupled Plasma-Atomic
Emission Spectrometry
Total Cyanide EPA 9013 A, Rev 2 - July 2014
/SMEWW-APHA-AWWA-WEF
Part 4500-CN¯ C, F, 23rd Ed.

Cyanide Extraction Procedure


for Solids and Oils. Total
Cyanide after Distillation.
Cyanide-Selective Electrode
Method 2017
Sulfides or Total Sulfides EPA Method 9031, Rev. 0 1992

Extractable Sulfides in soils


Sulfates and Total SMEWW-APHA-AWWA-WEF P
Sulfates 4500-SO42- E, 23rd Ed. 2017.
Sulfates in soil - Turbidimetric
Method.

Effective Date November 4, 2022


TL-833
ANALYTICAL LABORATORY Page 3 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils, Sediment and Granulometric analysis NTP 339.128: 1999 (revised
CHEMISTRY - Sludge 2019) (Validated - Applied out
INORGANIC (cont’d.) of reach)
(Field collection + Lab Soil: Test Method for
Testing) Granulometric Analysis
(cont’d.)
Soils, Metals: EPA Method 3051A /
Sludge, Al, Sb, As, Ba, Be, B, Cd, EPA Method 6010D
Sediments and Ca, Cr, Co, Cu, Fe, Pb, (Validated Applied out of
Oils Mg, Mn, Hg, Mo, Ni, K, reach)
Se, Ag, Na, Sr, Tl, V, Zn
Microwave Assisted Acid
Digestion of Sediments,
Validated:
Sludged, Soils, and Oils /
Li, P, SiO2, Sn, Ti, Bi, U,
Inductively Coupled Plasma -
Ce, Si
Optical Emission Spectrometry
Soils and Changeable Acidity Official Mexican Standard,
Sediments NOM-021-RECNAT-2000, AS-
33 (Validated - Applied out of
reach)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Determination of Changeable
Acidity
Changeable Aluminum Official Mexican Standard,
NOM-021-RECNAT-2000, AS-
33 (Validated - Applied out of
reach)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Changeable Aluminum
Changeable Hydrogen Official Mexican Standard,
NOM-021-RECNAT-2000, AS-
33 (Validated - Applied out of
reach)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Determination of
Exchangeable Hydrogen
Bicarbonates in EPS Official Mexican Standard,
(Saturated Pasta Extract)

Effective Date November 4, 2022


TL-833
ANALYTICAL LABORATORY Page 4 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils and NOM-021-RECNAT-2000, AS-
CHEMISTRY - Sediments 16/AS-17/AS-20 (Validated -
INORGANIC (cont’d.) Applied out of reach)
(Field collection + Lab Which establishes the
Testing) specifications of fertility, salinity
(cont’d.) and classification of soils.
Studies, sampling and analysis
- Bicarbonates in EPS
Carbonates Official Mexican Standard,
NOM-021-RECNAT-2000, AS-
29 (Validated - Applied out of
reach)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Determination of Carbonates
Carbonates in EPS Official Mexican Standard,
(Saturated Pasta Extract) NOM-021-RECNAT-2000, AS-
16/AS-17/AS-20 (Validated -
Applied out of reach)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Carbonates in EPS
Wad Cyanide EPA Method 9013A-Rev.2 /
SMEWW-APHA-AWWA-WEF
Part 4500-CN¯ I, F, 23rd Ed.
2017 (Validated - Modified)
Cyanide extraction procedure
for solids and oils /Weak Acid
Dissociable Cyanide. Cyanide-
Selective Electrode Method
Textural Class Official Mexican Standard,
NOM-021-RECNAT-2000, AS-
09 (Validated - Modified)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Determination of Textural
Class
B, Ca, Cu, Mg, Official Mexican Standard,
Mn, K, Na, Zn, P, Fe NOM-021-RECNAT-2000, AS-
16/AS-17/AS-20 (Validated -
Modified)

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ANALYTICAL LABORATORY Page 5 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils and Which establishes the
CHEMISTRY - Sediments specifications of fertility, salinity
INORGANIC (cont’d.) and classification of soils.
(Field collection + Lab Studies, sampling and analysis
Testing) - Determination of Soluble
(cont’d.) Metals in EPS
Changeable Bases: Official Mexican Standard,
Changeable Calcium NOM-021-RECNAT-2000, AS-
Changeable Potassium 12 (Validated - Modified)
Changeable Magnesium Which establishes the
Changeable Sodium specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Determination of
Exchangeable Bases
Bases Available: Official Mexican Standard,
Available Calcium NOM-021-RECNAT-2000, AS-
Available Potassium 12 (Validated - Modified)
Available Magnesium Which establishes the
Available Sodium specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Determination of Available
Bases
Cation Exchange Official Mexican Standard,
Capacity (C.I.C) NOM-021-RECNAT-2000, AS-
12 (Validated - Modified)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Determination of Cation
Exchange Capacity
Chloride Official Mexican Standard,
Nitrate NOM-021-RECNAT-2000, AS-
Sulfate 16/AS-17/AS-20 / EPA 300.0
Phosphate Rev. 2.1, 1993 (Validated -
Modified)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Determination of Soluble
Anions in EPS / Determination
of Inorganic Anions by Ion
Chromatography
Olsen Available Official Mexican Standard,

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ANALYTICAL LABORATORY Page 6 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils and Phosphorus NOM-021-RECNAT-2000, AS-
CHEMISTRY - Sediments 10 (Validated - Applied out of
INORGANIC (cont’d.) reach)
(Field collection + Lab Which establishes the
Testing) specifications of fertility, salinity
(cont’d.) and classification of soils.
Studies, sampling and analysis
- Determination of Available
Phosphorus Olsen
Micronutrients Official Mexican Standard,
Cu (DTPA), NOM-021-RECNAT-2000, AS-
Fe (DTPA) 14 (Validated - Modified)
Mn (DTPA)
Which establishes the
Zn (DTPA)
specifications of fertility,
salinity and classification of
soils. Studies, sampling and
analysis - Determination of
Micronutrients
Soils, Fizz Rating MEND Report 1.20.1, Chapter
Sediment, (Degree of 13, Item 13.3.2, December
Rock Effervescence) 2009
Mining tailings Prediction Manual for Drainage
Mining waste Chemistry from Sulphidic
Mineral sample Geologic Materials
pH in Paste MEND Report 1.20.1, Chapter
13, Item 13.3.2, December
2009
Prediction Manual for Drainage
Chemistry from Sulphidic
Geologic Materials
Maximum Acidity MEND Report 1.20.1, Chapter
Potential (MPA) 13, Item 13.3.2, December
2009
Prediction Manual for Drainage
Chemistry from Sulphidic
Geologic Materials
Lawrence Neutralization MEND Report 1.20.1, Chapter
Potential 13, Item 13.3.3, December
2009
Prediction Manual for Drainage
Chemistry from Sulphidic
Geologic Materials
Sobek Neutralization MEND Report 1.20.1, Chapter
Potential 13, Item 13.3.2, December
2009

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TL-833
ANALYTICAL LABORATORY Page 7 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils, Prediction Manual for Drainage
CHEMISTRY - Sediment, Chemistry from Sulphidic
INORGANIC Rock Geologic Materials
(Field collection + Lab Mining tailings Net Neutralization MEND Report 1.20.1, Chapter
Testing) Mining waste Potential (NNP) 13, Item 13.3.2, December
(cont’d.) Mineral sample 2009
(cont’d.)
Prediction Manual for Drainage
Chemistry from Sulphidic
Geologic Materials
Ratio (NNP/MPA) MEND Report 1.20.1, Chapter
13, Item 13.3.2, December
2009
Prediction Manual for Drainage
Chemistry from Sulphidic
Geologic Materials
4 Acids MVAL-GEO-002
Digestion 4 Acids, Metals in
(Ag, Al, As, Ba, Be, Bi, Solid Samples
Ca, Cd, Co, Cr, Cu, Fe,
K, Li, Mg, Mn, Mo, Na,
Ni, P, Pb, S, Sb, Sn, Sr,
Ti, V, W, Zn)
Sulfur Sulfate ASTM E 1915-20
Standard Test Methods for
Analysis of Metal Bearing Ores
and Related Materials for
Carbon, Sulfur and acid-Base
Characteristics
Total Sulfur ASTM E 1915-20
Standard Test Methods for
Analysis of Metal Bearing Ores
and Related Materials for
Carbon, Sulfur and acid-Base
Characteristics
Dold Sequential Journal of Geochemical
Extraction Exploration 80 (2003) 55–68
(Ag, Al, As, Ba, Be, Bi, (Validated - Modified)
Ca, Cd, Co, Cr, Cu, Fe, Speciation of the most soluble
K, Li, Mg, Mn, Mo, Na, phases in a sequential
Ni, P, Pb, S, Sb, Se, Sn, extraction procedure adapted
Sr, Tl, Ti. V, Zn) for geochemical studies of
copper sulfide mine waste
Sequential Tessier Analytical Chemistry vol.51,
Extraction 1979
Sequential extraction
Ag, Al, As, Ba, Be, Bi, Procedure for the speciation of
Ca, Cd, Co, Cr, Cu, Fe, particulate trace metals

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TL-833
ANALYTICAL LABORATORY Page 8 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils, K, Li, Mg, Mn, Mo, Ni, P,
CHEMISTRY - Sediment, Pb, S, Sb, Se, Sn, Sr, Ti,
INORGANIC Rock Tl, V, Zn
(Field collection + Lab Mining tailings Leaching Test (Metals) EPA 1312, 1994 (Validated -
Testing) Mining waste SPLP Modified)
(cont’d.) Mineral sample
Synthetic precipitation leaching
(cont’d.) Ag, Al, As, B, Ba, Be, Bi, procedure - SPLP
Ca, Cd, Co, Cr, Cu, Fe,
K, Li, Mg, Mn, Mo, Na,
Ni, P, Pb, S, Sb, Se, Si,
Sn, Sr, Tl,Ti, U, V, Zn
Shake Flask Test, MEND Report 1.20.1, Chapter
Solubility 11, Item 11.5 December 2009
/ EPA 200.7 (Validated -
Testing (SFT) (Ag, Al, As, Applied out of reach)
B, Ba, Be, Bi, Ca, Cd, Prediction Manual for Drainage
Co, Cr, Cu, Fe, K, Li, Mg, Chemistry from Sulphidic
Mn, Mo, Na, Ni, P, Pb, S, Geologic Materials /
Sb, Se, Si, Sn, Sr, Ti, U, Determination of Metals and
V, Zn) Trace Elements in Water and
Wastes by Inductively Coupled
Plasma-Atomic Emission
Spectrometry
Shake Flask Test, MEND Report 1.20.1, Chapter
Solubility Testing (SFT) 11, Item 11.5 December 2009/
Chlorides, EPA 300.0 Rev. 2.1, 1993
Nitrates, Prediction Manual for Drainage
Nitrites, Chemistry from Sulphidic
Phosphates, Geologic Materials /
Fluorides, Determination of Inorganic
Sulfate Anions by Ion Chromatography
Total Sulfide ASTM E 1915-20
Standard Test Methods for
Analysis of Metal Bearing Ores
and Related Materials for
Carbon, Sulfur and acid-Base
Characteristics
Limestone Pyritic Sulfur ASTM E 1915-20 (Validated -
Quicklime Modified)
Hydrated lime Standard Test Methods for
Analysis of Metal Bearing Ores
and Related Materials by
Combustion Infrared-
Absorption Spectrometry
Soils – Agronomy pH (1: 1; 1: 2.5; 1:10; MVAL-AGR-01:2020
EPS) Determination of pH
Conductivity (1: 1; 1: 2.5; MVAL-AGR-02:2020

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IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Soils – Agronomy 1:10; EPS) Determination of Conductivity.
CHEMISTRY - (cont’d.)
Limestone Active MVAL-AGR-03:2020
INORGANIC
Determination of Active
(Field collection + Lab
Limestone. Active
Testing)
(cont’d.) Organic Matter Official Mexican NORMA
NOM-021-RECNAT-2000,
which establishes the
specifications of fertility,
salinity, and soil classification,
Studies, sampling and analysis.
AS-07; item 7.1.7
Organic Matter Content by the
Walkley and Black Method.
Soils Total Nitrogen ISO 16634-2: 2016 (Validated
Sediment - Modified)
Vegetal material Determination of Total Nitrogen
Organic Fertilizer Content by Combustion
Inorganic Fertilizer according to the Dumas
Principle
Natural Water, Dissolved Metals: EPA METHOD 200.7 Rev.4.4.,
Water for human Ag, Al, As, B, Ba, Be, Ca, 1994
use and Cd, Ce, Co, Cr, Cu, Fe, K, Determination of Metals and
consumption, Saline Li, Mg, Mn, Mo, Na, Ni, P, Trace Elements in Water and
Water, Process Pb, Sb, Se, SiO2, Sn, Sr, Wastes by Inductively Coupled
Water and Waste Tl, Ti, V, Zn, Hg Plasma-Atomic Emission
Water Spectrometry
Dissolved Metals: EPA Method 200.7, Rev. 4.4.,
Validated: U, Bi 1994. VALIDATED (Applied
out of reach), 2018
Total Metals: EPA METHOD 200.7 Rev.4.4.,
Ag, Al, As, B, Ba, Be, Ca, 1994
Cd, Ce, Co, Cr, Cu, Fe, K, Determination of Metals and
Li, Mg, Mn, Mo, Na, Ni, P, Trace Elements in Water and
Pb, Sb, Se, SiO2, Sn, Sr, Wastes by Inductively Coupled
Tl, Ti, V, Zn, Hg, U, Bi. Plasma-Atomic Emission
Spectrometry.

Total Metals: EPA Method 200.7, Rev. 4.4.,


Validated: U, Bi 1994. VALIDATED (Applied
out of reach), 2018
Un-ionized Hydrogen SMEWW-APHA-AWWA-WEF
Sulfide Part 4500-S2- D, H, 23rd Ed.,
2017

Sulfide. Methylene Blue


Method. Calculation of Un-
ionized Hydrogen Sulfide

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ANALYTICAL LABORATORY Page 10 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Natural Water, Total Nitrogen SMEWW-APHA-AWWA-WEF
CHEMISTRY - Water for human Part 4500-N C, 23rd Ed., 2017.
INORGANIC use and
(Field collection + Lab consumption, Saline Nitrogen. Persulfate Method
Testing) Water, Process Acidity SMEWW-APHA-AWWA-WEF
(cont’d.) Water and Waste Part 2310 B, 23rd Ed., 2017.
Water
(cont’d.) Acidity: Titration Method
Total Hardness SMEWW-APHA-AWWA-WEF P
2340-C, 23rd Ed.
EDTA Titrimetric Method. 2017
Hexavalent chromium - SMEWW-APHA-AWWA-WEF
dissolved Part 3500-Cr-B, 23rd Ed.
2017.

Chromium. Colorimetric Method


Natural Water, Anions EPA 300.0 Rev. 2.1, 1993,
Water for human Chloride, VALIDATED (Applied out of
use and Fluoride, reach), 2019
consumption, Nitrite,
Process Water and N-Nitrite, Determination of inorganic
Waste Water Nitrate, anions by ion chromatography
N-Nitrate,
N-Nitrate + N-Nitrite,
Sulfate,
Phosphate-P,
Bromide,
Bromate,
Fluor,
Chlorite,
Chlorate,
Monochloroacetate,
Dichloroacetate
Natural Water, Silica (SiO2) SMEWW-APHA-AWWA-WEF
Water for human Part 4500-SiO2 C.
use and 23rd Ed.
consumption, Saline Silica. Molybdosilicate Method
Water and Waste Silicates (Si-SiO3; SiO2- SMEWW-APHA-AWWA-
Water SiO3) WEF Part 4500-SiO2 C-4a,
23rd Ed., 2017.
VALIDATED (Applied out of
reach), 2019

Silica. Molybdosilicate Method


Biochemical Soluble SMEWW-APHA-AWWA-
Oxygen Demand WEF Part 5210 B, 23 rd Ed.
(Validated - Modified)

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ANALYTICAL LABORATORY Page 11 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Natural Water, Biochemical Oxygen Demand
CHEMISTRY - Water for human (BOD). 5-Day BOD Test
INORGANIC use and Organic Nitrogen SMEWW-APHA-AWWA-
(Field collection + Lab consumption, Saline WEF Part 4500-Norg B
Testing) Water, and Waste (Validated - Modified)
(cont’d.) Water (cont’d.) Macro-Kjeldahl Method
Natural Water, Soluble Chemical Oxygen SMEWW-APHA-AWWA-
Water for human Demand WEF
use and Part 5220 D, 23 rd Ed.
consumption, and (Validated - Modified)
Waste Water Chemical Oxygen Demand,
Closed Reflux, Colorimetric
Method
Water for human Total metals and Dissolved EPA Method 200.8, Revision
use and Metals 5.4, 1994.
consumption, Determination of Trace
Natural Water, Ag, Al, As, Ba, Be, Cd, Co, Elements in Waters and
Wastewater Cr, Cu, Mn, Mo, Ni, Pb, Sb, Wastes by Inductively Coupled
Se, Tl, V, Zn, Hg, U, Th Plasma –Mass Spectrometry

Total metals and Dissolved


EPA Method 200.8, Revision
Metals
5.4, 1994.
Validated: Bi, B, Ca, Ce,
VALIDATED (Applied out of
Cs, Fe, Ga, Ge, Hf, K, La,
reach), 2020
Li, Lu, Mg, Na, Nb, P, Rb,
Determination of Trace
Si, Sn, Sr, Ta, Te, Ti, W,
Elements in Waters and
Yb, Zr, In, Er, Y, Sm, Re,
Wastes by Inductively Coupled
Nd, Eu, Gd, Ho, Pr
Plasma –Mass Spectrometry
Saline Water Surfactants SMEWW-APHA-AWWA-WEF
Part 5540 C, 23rd Ed. 2017.

Surfactants. Anionic
Surfactants as MBAS
Nitrites / N-Nitrites (N-NO2) SMEWW-APHA-AWWA-WEF
Part 4500-NO2- B, 23rd Ed.
2017.

Nitrogen (Nitrite). Colorimetric


Method
Anions EPA 300.0 Rev. 2.1, 1993,
(VALIDATED - Applied out of
Chloride, reach, 2020).
Sulfate Determination of inorganic
anions by ion chromatography

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IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Saline Water Anions EPA 300.0 Rev. 2.1, 1993,
CHEMISTRY - (cont’d.) (VALIDATED - Applied out of
INORGANIC Bromide reach, 2022).
(Field collection + Lab Determination of inorganic
Testing) anions by ion chromatography
(cont’d.) Fluoride SMEWW-APHA-AWWA-WEF
Part 4500-F¯ C, 23rd Ed. 2017
Fluoride. lon-Selective
Electrode Method
Total Dissolved Solids SMEWW-APHA-AWWA-WEF
Part 2540 C, 23rd Ed. 2017.
Solids. Total Dissolved Solids
Dried at 180°C
Settleable Solids SMEWW-APHA-AWWA-WEF
Part 2540 F, 23rd Ed. 2017.
Solids. Settleable Solids
Total Alkalinity, SMEWW-APHA-AWWA-WEF
Carbonate Alkalinity and Part 2320 B, 23rd Ed. 2017
Bicarbonate Alkalinity
Alkalinity. Titration Method
Color SMEWW-APHA-AWWA-WEF
Part 2120 C, 23rd Ed. 2017
Color. Spectrophotometric -
Single - Wavelength Method
Total Solids SMEWW-APHA-AWWA-WEF
Part 2540 B, 23rd Ed. 2017.
Solids. Total Solids Dried at
103-105°C
Electric conductivity SMEWW-APHA-AWWA-WEF
Part 2510 B. 23rd Ed
Conductivity. Laboratory
Method
Total metals and Dissolved EPA Method 200.8, Revision
Metals 5.4, 1994. (VALIDATED)

Validated: Ag, Al, As, Ba, Determination of Trace


Be, Cd, Co, Cr, Cu, Mn, Elements in Waters and
Mo, Ni, Pb, Sb, Se, Tl, V, Wastes by Inductively Coupled
Zn, Hg, U, Th, Bi, B, Ca, Plasma –Mass Spectrometry
Ce, Cs, Fe, Ga, Ge, Hf, K,
La, Li, Lu, Mg, Nb, P, Rb,
Sn, Sr, Ta, Te, Ti, W, Yb,
Zr, In, Er, Y, Sm, Re, Na,
Eu, Gd, Ho, Pr
COD in Saline water SMEWW-APHA-AWWA-WEF
Part 5220 A,2; D, 23 rd Ed.
2017

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ANALYTICAL LABORATORY Page 13 of 63
IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Chemical Oxygen Demand,
CHEMISTRY - Closed Reflux, Colorimetric
INORGANIC Method. Modified (validated)
(Field collection + Lab Process Water Total metals and Dissolved EPA Method 200.8, Revision
Testing) Metals 5.4, 1994. (VALIDATED)
(cont’d.) Determination of Trace
Validated: Ag, Al, As, Ba, Elements in Waters and
Be, Cd, Co, Cr, Cu, Mn, Wastes by Inductively Coupled
Mo, Ni, Pb, Sb, Se, Tl, V, Plasma –Mass Spectrometry
Zn, Hg, U, Th, Bi, B, Ca,
Ce, Cs, Fe, Ga, Ge, Hf, K,
La, Li, Lu, Mg, Na, Nb, P,
Rb, Si, Sn, Sr, Ta, Te, Ti,
W, Yb, Zr, In, Er, Y, Sm,
Re, Nd, Eu, Gd, Ho, Pr
Drinking Water Determination of total alpha EPA 900.0
Drinking Water radioactivity concentration Gross alpha and gross beta
in Drinking water radioactivity in drinking water
Determination of total beta EPA 900.0
radioactivity concentration Gross alpha and gross beta
in Drinking water radioactivity in drinking water
Natural water Chloride SMEWW-APHA-AWWA-WEF
Part 4500-Cl-B, 23rd Ed. 2017
Chloride. Argentometric
Method
Ice Metal Determination EPA 200.8
Determination of trace
Al, Sb, As, Ba, Be, B, Cd, elements in waters and wastes
Ca, Cr, Co, Cu, Fe, Pb, Mg, by Inductively Coupled Plasma
Mn, Hg, Mo, Ni, K, Se, Ag, - Mass Spectrometry
Na, Sr, Tl, V, Zn
Air High Volume Metals (PTS, EPA COMPENDIUM
PM10, PM2.5): Al, As, B, METHOD IO-3.4, June 1999.
Ba, Be, Ca, Cd, Ce, Co, Cr,
Cu, Fe, K, Li, Mg, Mn, Mo, Determination of Metals in
Ni, P, Pb, Sb, Se, Sn, Sr, Ambient Particulate Matter
Tl, Ti, V, Zn, Hg using Inductively Coupled
Plasma (ICP) Spectroscopy

High Volume Metals (PTS, EPA COMPENDIUM


PM10, PM2.5): METHOD IO-3.4, June 1999.
Validated: SiO2 VALIDATED (Applied out of
reach), 2018
Low Volume Elements EPA COMPENDIUM
(PM10, PM2.5): METHOD IO-3.4, June 1999.
Al, As, B, Ba, Be, Ca, Cd, VALIDATED (Applied out of
Ce, Co, Cr, Cu, Fe, K, Li, reach), 2018

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Air Mg, Mn, Mo, Ni, P, Pb, Sb,
CHEMISTRY - (cont’d.) Se, Sn, Sr, Tl, Ti, V, Zn, Determination of Metals in
INORGANIC Hg, SiO2. Ambient Particulate Matter
(Field collection + Lab using Inductively Coupled
Testing) Plasma (ICP) Spectroscopy
(cont’d.) Determination of weight in NTP 900.030.2018
PM10 high volume filters in Reference method for
Air - Validated determining respirable
particulate matter such as
PM10 in the atmosphere. 2nd
Edition
Determination of weight in NTP 900.069.2017
PM 2.5 low volume filters in Reference method for the
Air - Validated determination of fine particulate
matter such as PM2.5 in the
atmosphere. 1st Edition
PM10 (Particulate matter NTP 900.030:2018
less than or equal to 10 Reference method for
µm) low and high vol determining respirable
particulate matter such as
PM10 in the atmosphere. 2nd
Edition.
PM2.5 (Particulate matter NTP 900.069:2017
less than or equal to 2.5 Reference method for the
µm) low vol determination of fine particulate
matter such as PM2.5 in the
atmosphere. 1st Edition
NO2 (Nitrogen dioxide) NTP ISO 7996:2019
Determination of the mass
concentration of nitrogen
oxides. Chemiluminescence
method. (Automatic method)
NO (Nitric oxide / Nitrogen NTP ISO 7996:2019
monoxide) Determination of the mass
concentration of nitrogen
oxides. Chemiluminescence
method. (Automatic method)
NOX (Nitrogen oxides) NTP ISO 7996:2019
Determination of the mass
concentration of nitrogen
oxides. Chemiluminescence
method. (Automatic method)
O3 (Ozone) NTP-ISO 13964: 2020
Determination of ozone in
ambient air - Ultraviolet
photometric method

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TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Air Hg (Total Gaseous NTP 900.068:2016/COR1:2017
CHEMISTRY - (cont’d.) Mercury) ENVIRONMENTAL QUALITY
INORGANIC MONITORING. Air quality
(Field collection + Lab Standard method for the
Testing) determination of total gaseous
(cont’d.) mercury. CORRIGENDA 1. 1st
Edition
Nitrogen Dioxide (NO2) ASTM D1607 – 91 (2018)e1
Standard Test Method for
Nitrogen Dioxide Content of the
Atmosphere (Griess-Saltzman
Reaction)
Ozone (O3) "Methods of Air Sampling
and Analysis"; 411:
Determination of Oxidizing
Substances in the Atmosphere.
Intersociety Committee, James
P. Lodge (Editor) Third edition
Hydrogen Sulfide (H2S) "Methods of Air Sampling
and Analysis" 701:
Determination of Hydrogen
Sulfide Content of the
Atmosphere. Intersociety
Committee, James P. Lodge
(Editor) Third edition
Total suspended particulate EPA CFR 40 Part 50
matter (PTS) Appendix B, 2018

Reference Method for the


Determination of Suspended
Particulate Matter in the
Atmosphere (High-Volume
Method)
PTS Filters (High Volume) EPA CFR 40 Part 50
Appendix B, 2018.
(Validated - Modified)
Determination of Suspended
Particulate Matter in the
Atmosphere (High-Volume
Method) Determination of
Weight.
Total Gaseous Mercury NIOSH Method 6009, Issue 2,
1994,
VALIDATED (Applied out of
reach), 2019

Mercury

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Emission / Nitrogen Oxides (NOX as EPA METHOD 7 / 2019
CHEMISTRY - Stationary Sources NO2)
INORGANIC Determination of Nitrogen
(Field collection + Lab Oxide Emissions from
Testing) Stationary Sources.
(cont’d.) Nitrogen Oxides (NOX as NTP 900.007, 2002(Revisada
NO2) el 2018).

ENVIRONMENTAL
MANAGEMENT: Atmospheric
emissions. Determination of
nitrogen oxide emissions from
stationary sources.
Sulfur Oxides (SOx) EPA METHOD 8, Rev. 2019.
(including mists of H2SO4 VALIDATED (Applied out of
and SO3) reach), 2019.

Determination of Sulfuric Acid


and Sulfur Dioxide Emission
from Stationary Sources
PM (Particulate Matter) NTP 900.005:2001
Determination of emissions of
particulate matter from
stationary sources
SO2 (Sulfur Dioxide) NTP 900.006:2002
Determination of sulfur dioxide
emissions from stationary
sources.
Metals in Atmospheric EPA METHOD 29, 2017
Emissions:
Ag, As, Ba, Be, Cd, Co, Cr, Determination of Metals
Cu, Mn, Ni, P, Pb, Sb, Se, Emissions from Stationery
Tl, Zn, Hg Sources
Metals
Emission Ammonia EPA METODO 207.1, 1994 /
EPA CTM-027, 1997
Determination of ammonia
emissions from stationary
sources /
Procedure for Collection and
Analysis of Ammonia in
Stationary Sources
Hydrogen Chloride (HCl), EPA CFR Title 40, Appendix
Hydrogen Fluoride (HF), A-8 to Part 60, Method 26 /
Br2, EPA CFR Title 40, Appendix
HBr, A-8 to Part 60, Method 26A
Cl2 Determination of Hydrogen
Halide and Halogen

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Emission Emissions From Stationary
CHEMISTRY - (cont’d.) Sources Non-Isokinetic
INORGANIC Method / Determination of
Hydrogen Halide and
(Field collection + Lab Halogen Emissions from
Testing) Stationary Sources
(cont’d.) Isokinetic Method
Total Organic Carbon EPA CFR Title 40, Appendix
(TOC), VOC A-7 to Part 60, Method 25A.
(calculated as Total Determination of total
Carbon) gaseous organic
concentration using a flame
ionization analyzer
CARBON DISULFIDE EPA CFR Title 40 Appendix A-
5 to Part 60, METHOD 15
Carbon disulfide (CS2) Determination of hydrogen
Carbonyl sulfide (COS) sulfide, carbonyl sulfide, and
Hydrogen sulfide (H2S) carbon disulfide emissions
from stationary sources
Flux EPA CFR Title 40, Appendix
A-1 to Part 60. Method 2C
Determination of gas
Velocity and Volumetric Flow
Rate in Small Stacks or
Ducts (Standard Pitot Tube).
Formaldehyde (CH2O) EPA CFR Title 40, Appendix A
to Part 63, Method 323 /
EPA CFR Title 40, Appendix A
to Part 63, Method 316
Measurement of
Formaldehyde Emissions
From Natural Gas-Fired
Stationary Sources - Acetyl
Acetone Derivatization
Method / Sampling and
analysis for formaldehyde
emissions from stationary
sources in the mineral wool
and wool fiberglass
industries.
HNO3, HClO4 EPA CFR Title 40 Appendix A-
6 to Part, 60 Method 18 /
NIOSH 7907
Measurement of Gaseus
Organic Compound Emissions
by Gas Chromatography /
VOLATILE ACIDS by Ion
Chromatography
(Hydrogen Chloride,
Hydrogen Bromide, Nitric
Acid)

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Emission Humidity EPA CFR Title 40, Appendix
CHEMISTRY - (cont’d.) A-3 to Part 60. Method 4
INORGANIC Determination of Moisture
(Field collection + Lab Content in Stack Gases.
Testing) Carbon Monoxide (CO) EPA CFR Title 40, Appendix
(cont’d.) A-4 to Part 60, Method 10.
Determination of Carbon
Monoxide Emissions from
Stationary Sources
(Instrumental Analyzer
Procedure)
Carbon Monoxide (CO) NTP 900.010:2021
ATMOSPHERIC
EMISSIONS MONITORING.
Determination of Carbon
Monoxide Emissions from
Stationary Sources
(Instrumental Analyzer
Procedure)
Nitrogen Oxide (NOX) EPA CFR 40, Appendix A-4 to
Part 60, Method 7E.
Determination of nitrogen
oxides emissions from
stationary sources
(instrumental analyzer
procedure)
Sulfur Oxides (SOx) EPA CFR Title 40, Appendix
A-4 to Part 60, Method 8.
Determination of Sulfuric
Acid and Sulfur Dioxide from
stationary sources
Oxygen (O2) / NTP 900.003:2021
Carbon Dioxide (CO2) MONITORING OF
ATMOSPHERIC
EMISSIONS. Gas analysis
for the determination of
molecular weight on a dry
basis. 2nd Edition
Hydrogen sulfide (H2S) CTM-022 /CTM-030
(Validated-out of scope)
Determination of Nitric
Oxide, Nitrogen Dioxide and
NOx Emissions from
Stationary Combustion
Sources by Electrochemical
Analyzer 1995 /
Determination of Nitrogen
Oxides, Carbon Monoxide,
and Oxygen Emissions from
Natural Gas-Fired Engines,
Boilers and Process Heaters

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TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Emission using Portable Analyzers,
CHEMISTRY - (cont’d.) 1997
INORGANIC Metal Determination EPA CFR Title 40, Appendix
(Field collection + Lab Sn, Ti, V, Fe A-8 to Part 60. Method 29,
Testing) 2021 (Validated-out of scope)
(cont’d.)
Determination of Metals
Emissions from Stationery
Sources Metals
Air Ambient Metals in PM 10 high EPA IO [Inorganic]
volume Filters: Compendium Method IO-
3.5:
Al, Sb, As, B, Ba, Be, Cd,
Determination of Metals in
Ca, Co, Cu, Cr, Sn, Sr, P,
Ambient Particulate Matter
Fe, Li, Mg, Mn, Hg, Mo, Ni,
using Inductively Coupled
Ag, Pb, K, Se, Si, Na, Tl,
Plasma/Mass Spectrometry
Ti, V, Zn
(ICP-MS)
Metals in PM 2.5 low EPA IO [Inorganic]
volume Filters: Compendium Method IO-
3.5:
Al, Sb, As, B, Ba, Be, Cd,
Determination of Metals in
Ca, Co, Cu, Cr, Sn, Sr, P,
Ambient Particulate Matter
Fe, Li, Mg, Mn, Hg, Mo, Ni,
using Inductively Coupled
Ag, Pb, K, Se, Si, Na, Tl,
Plasma/Mass Spectrometry
Ti, V, Zn
(ICP-MS)
Sedimentable ASTM D1739 − 98 Sedimentable Particulate
Particulate Matter (Reapproved 2017) Matter
Standard Test Method for
Collection and
Measurement of Dustfall
(Settleable Particulate
Matter)
Settleable Powders ASTM D1739 − 98 Settleable Powders
(Reapproved 2017)
Standard Test Method for
Collection and
Measurement of Dustfall
(Settleable Particulate
Matter)

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL High Volume Metals EPA IO [Inorganic] High Volume Metals (PM2.5)
CHEMISTRY - (PM2.5) Compendium Method
INORGANIC IO3.5: Validated Al, Sb, As, Ba, Be, Bi, Cd, Cr,
(Field collection + Lab Al, Sb, As, Ba, Be, Determination Of Metals In Co, Cu, Pb, Mg, Mn, Mo, Ni,
Testing) Bi, Cd, Cr, Co, Cu, Ambient Particulate Matter Se, Ag, Tl, Th, U, V, Zn, B, Ca,
(cont’d.) Pb, Mg, Mn, Mo, Ni, Using Inductively Coupled Fe, K, Li, Na, Si, Sn, Hg, P, Sr,
Se, Ag, Tl, Th, U, V, Plasma (ICP) Spectroscopy Ti
Zn, B, Ca, Fe, K, Li,
Na, Si, Sn, Hg, P,
Sr, Ti
Low Volume Metals EPA IO [Inorganic] Low Volume Metals (PM10)
(PM10) Compendium Method
IO3.5: Al, Sb, As, Ba, Be, Bi, Cd, Cr,
Al, Sb, As, Ba, Be, Validated Co, Cu, Pb, Mg, Mn, Mo, Ni,
Bi, Cd, Cr, Co, Cu, Determination Of Metals In Se, Ag, Tl, Th, U, V, Zn, B, Ca,
Pb, Mg, Mn, Mo, Ni, Ambient Particulate Matter Fe, K, Li, Na, Si, Sn, Hg, P, Sr,
Se, Ag, Tl, Th, U, V, Using Inductively Coupled Ti
Zn, B, Ca, Fe, K, Li, Plasma (ICP) Spectroscopy
Na, Si, Sn, Hg, P,
Sr, Ti
Air Determination of Metals for NIOSH 7303, Issue 1, 2003.
(Chemistry – SSO (metals fumes):
Occupational Health Elements by ICP (Hot
& Safety) Metals: Block/HCl/HNO3
Al, As, B, Be, Ca, Cd, Digestion).
Co, Cr, Cu, Fe, Mg, Mn,
Mo, Ni, P, Se, Sr, Tl, Ti,
V, Zn

Metals: NIOSH 7303, Issue 1, 2003.


Validated: Ba, Pb, VALIDATED (Applied out of
Sb, Sn reach), 2018.
Volatile Acids: NIOSH 7907, Issue 1, 2014.
Hydrogen Chloride, VOLATILE ACIDS by Ion
Hydrogen Bromide, Nitric Chromatography (Hydrogen
Acid Chloride, Hydrogen Bromide,
(HCl, HBr, HNO3) Nitric Acid)
Non-Volatile Acids NIOSH 7908 / Rev.1 2014
Ácido Sulfúrico, Ácido Non-Volatile Acids (Sulfuric
Fosfórico Acid and Phosphoric Acid)
(H2SO4, HPO4)
Asbestos and Other NIOSH 7400, Issue 3, 2019.
Fibers Asbestos and Other Fibers by
PCM
Biological Tissues - Metals: EPA Method 200.3, Rev. 1,
Animals, Ag, Al, As, Ba, Be, Ca, Cd, 1991 / EPA Method 200.7,
Vegetables, Tissues Co, Cr, Cu, Fe, K, Li, Mg, Rev. 4.4, 1994

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Biological Tissues - Mn, Mo, Na, Ni, P, Pb, Sb,
CHEMISTRY - Animals, Se, Sr, Tl, Th, U, V, Zn, Hg Sample Preparation Procedure
INORGANIC Vegetables, Tissues for Spectrochemical
(Field collection + Lab (cont’d.) Determination of Total
Testing) Recoverable Elements in
(cont’d.) Biological Tissues /
Determination of Metals and
Trace Elements in Water and
Wastes by Inductively Coupled
Plasma-Atomic Emission
Spectrometry
ENVIRONMENTAL Natural Water, Floatable Materials NMX-AA-006-SCFI-2010-
CHEMISTRY - Water for human Water analysis
INORGANIC use and Determination of floating matter
(Field Measurement) consumption, Saline in wastewater and treated
Water, Process wastewater, Test method
Water and Waste Flow UNE-EN ISO 748:2009
Water Measurement of liquid flow in
open channels using current-
meters or floats Flow
Natural Water, Turbidity SMEWW-APHA-AWWA-WEF
Water for human Part 2130 B. 23rd Ed, 2017.
use and
consumption, Saline Turbidity. Nephelometric
Water and Waste Method
Water Total Nitrogen Kjeldahl SMEWW-APHA-AWWA-WEF
Part 4500-Norg B / Part 4500-
NH3 D, 23rd Ed. 2017
(Validated - Modified)
Macro-Kjeldahl Method /
Ammonia Selective Electrode
Method
Cyanogen Chloride SMEWW-APHA-AWWA-WEF
Part 4500-CN-J,F 23rd Ed.
2017
(Validated - Modified)
Cyanogen Chloride. Cyanide-
Selective Electrode Method
Formaldehyde ASTM D6303-98
(Validated - Modified)
Standard Test Method for
Formaldehyde in Water
Sedimentable Solids SMEWW-APHA-AWWA-WEF
Part 2540 F, 23rd Ed.
Solids. Settleable Solids

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Emission / NOx, NO, NO2, CO, O2 CTM-034 / 1999
CHEMISTRY - Stationary Sources ICAC Test Method for Periodic
INORGANIC Monitoring. Test Method -
(Field Measurement) Determination of Oxygen,
(cont’d.) Carbon Monoxide and Oxides
of Nitrogen from Stationary
Sources For Periodic
Monitoring (Portable
Electrochemical Analyzer
Procedure)
CO USEPA METHOD 10
Determination of Carbon
Monoxide Emissions from
Stationary Sources
(Instrumental Analyzer
Procedure)
ENVIRONMENTAL Toys, Toys parts Metals: UNE-EN 71-3:2013+A3, 2018
CHEMISTRY - and Desktop tools Toy safety. Part 3: Migration of
INORGANIC based on: Al, As, Ba, B, Cd, Co, Cu, certain elements
(Lab Testing) Mn, Ni, Pb, Sb, Se, Sn, Sr,
-Glue Bar, Crystal, Hg, Zn
Ceramic, Metal
Materials
-Polymer Material
and similar,
Including Rolled or
Reinforced Textiles
or Not,
-Compressed Paint
Pad Materials,
Materials intended
to Leave a trace or
Similar in Solid
Form,
-Flexible modeling
materials, including
modeling clays and
plaster,
-Other colored
materials or not in
the mass,
-Paper and
Cardboard
-Liquid Paints
including finger
paints, Varnishes,
Lacquers, Liquid Ink
and Liquid
materials,

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL -Paint coatings, Metals: UNE-EN 71-3:2013+A3, 2018
CHEMISTRY - Varnishes, Toy safety. Part 3: Migration of
INORGANIC Lacquers, Printing Al, As, Ba, B, Cd, Co, Cu, certain elements
(Lab Testing) inks, Mn, Ni, Pb, Sb, Se, Sn, Sr,
(cont’d.) -Polymers and Hg, Zn
similar coatings, (cont’d.)
-Natural or Synthetic
textiles
Emissions - Determination of Metals EPA METHOD 29, 2017
Environmental Emissions from Stationery VALIDATED (Modified), 2019.
Filters Sources:
Ag, As, Ba, Be, Cd, Co, Cr,
Determination of Metals
Cu, Mn, Ni, P, Pb, Sb, Se,
Emissions from Stationery
Tl, Zn, Fe, V.
Sources
Air – Environmental PTS, PM10 and PM2.5 EPA COMPENDIUM
Filters High Volume filter metals: METHOD IO-3.4, June 1999.
Ag, Al, As, B, Ba, Be, Ca, VALIDATED (Modified), 2018.
Cd, Ce, Co, Cr, Cu, Fe, K,
Li, Mg, Mn, Mo, Na. Ni, P, Determination of Metals in
Pb, Sb, Se, Si, Sn, Sr, Tl, Ambient Particulate Matter
Ti, V, Zn, Hg, SiO2. using Inductively Coupled
Plasma (ICP) Spectroscopy
PM10 and PM2.5 Low EPA COMPENDIUM
Volume filter metals: METHOD IO-3.4, June 1999.
Ag, Al, As, B, Ba, Be, Ca, VALIDATED (Modified), 2018.
Cd, Ce, Co, Cr, Cu, Fe, K,
Li, Mg, Mn, Mo, Na. Ni, P, Determination of Metals in
Pb, Sb, Se, Si, Sn, Sr, Tl, Ambient Particulate Matter
Ti, V, Zn, Hg, SiO2 using Inductively Coupled
Plasma (ICP) Spectroscopy
Anions in PM10 and PM2.5 EPA Method Compendium
High volume: Method IO-3.1, June
1999/NIOSH 7908, Issue 1,
Chloride (Cl-) 2014/EPA 300.0 Rev. 2.1,
Nitrite (NO2-) 1993. (VALIDATED –
Nitrate (NO3-) Modified), 2020
Sulfate (SO42-)
Phosphate (PO43-) EPA Method Compendium
Bromide (Br-) Method IO-3.1. Selection,
Preparation and Extraction of
Filter Material / Non-Volatile
Acids (Sulfuric Acid and
Phosphoric Acid) /
Determination of inorganic
anions by ion chromatography
Anions in PM10 and PM2.5 EPA Method Compendium
Low volume: Method IO-3.1, June
1999/NIOSH 7908, Issue 1,

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Air – Environmental Chloride (Cl-) 2014/EPA 300.0 Rev. 2.1,
CHEMISTRY - Filters Nitrite (NO2-) 1993. (VALIDATED –
INORGANIC (cont’d.) Nitrate (NO3-) Modified), 2020
(Lab Testing) Sulfate (SO42-)
(cont’d.) Phosphate (PO43-)
Bromide (Br-) EPA Method Compendium
Method IO-3.1. Selection,
Preparation and Extraction of
Filter Material / Non-Volatile
Acids (Sulfuric Acid and
Phosphoric Acid) /
Determination of inorganic
anions by ion chromatography
Cations in PM10 and EPA Method Compendium
PM2.5 High volume: Method IO-3.1, June
1999/NIOSH 7908, Issue 1,
Lithium (Li+) 2014/EPA 300.0 Rev. 2.1,
Sodium (Na+) 1993. (VALIDATED –
Potassium (K+) Modified), 2020
Calcium (Ca2+)
Magnesium (Mg2+)
Ammonium (NH4+) EPA Method Compendium
Method IO-3.1. Selection,
Preparation and Extraction of
Filter Material / Non-Volatile
Acids (Sulfuric Acid and
Phosphoric Acid) /
Determination of inorganic
anions by ion chromatography
Cations in PM10 and EPA Method Compendium
PM2.5 Low volume: Method IO-3.1, June
1999/NIOSH 7908, Issue 1,
Lithium (Li+) 2014/EPA 300.0 Rev. 2.1,
Sodium (Na+) 1993. (VALIDATED –
Potassium (K+) Modified), 2020
Calcium (Ca2+)
Magnesium (Mg2+)
Ammonium (NH4+) EPA Method Compendium
Method IO-3.1. Selection,
Preparation and Extraction of
Filter Material / Non-Volatile
Acids (Sulfuric Acid and
Phosphoric Acid) /
Determination of inorganic
anions by ion chromatography

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Determination of EPA Method 3050B/ Determination of Metals in
CHEMISTRY - Metals in Settleable EPA Method 200.7 Settleable Powder:
INORGANIC Powder: (Validated - Applied Out
(Lab Testing) of Scope) Validated Applied out of scope:
(cont’d.) Validated Applied Acid Digestion of Al, Sb, Ba, Be, Cd, Ca, Cr, Co,
out of scope: Sediments, Sludges, and Cu, Fe, Pb, Mg, Mn, Ni, Mo, K,
Al, Sb, Ba, Be, Cd, Solis / Ag, Tl, V, As, Bi, B, Ce, Sn, Sr,
Ca, Cr, Co, Cu, Fe, Determination of P, Li, Se, Si(por calculo), Na,
Pb, Mg, Mn, Ni, Mo, Metals and Trace SiO2, Ti, U, Zn
K, Ag, Tl, V, As, Bi, Elements in Water
B, Ce, Sn, Sr, P, Li, and Wastes by
Se, Si(por calculo), Inductively Coupled
Na, SiO2, Ti, U, Zn Plasma-Atomic
Emission
Spectrometry.
Metals in Low EPA IO [Inorganic] Metals in Low Volume -Filter
Volume -Filter Compendium Method (PM10, PM2.5)
(PM10, PM2.5) IO3.5:
(Validated - Applied Out Validated Applied out of scope:
Validated Applied of Scope) Al, Sb, As, Ba, Be, Bi, Cd, Cr,
out of scope: Determination Of Co, Cu, Pb, Mg, Mn, Mo, Ni,
Al, Sb, As, Ba, Be, Metals In Ambient Se, Ag, Tl, Th, U, V, Zn, B, Ca,
Bi, Cd, Cr, Co, Cu, Particulate Matter Fe, K, Li, Na, Si, Sn, Hg, P, Sr,
Pb, Mg, Mn, Mo, Ni, Using Inductively Ti
Se, Ag, Tl, Th, U, V, Coupled Plasma (ICP)
Zn, B, Ca, Fe, K, Li, Spectroscopy
Na, Si, Sn, Hg, P,
Sr, Ti
Metals in High EPA IO [Inorganic] Metals in High Volume Filter
Volume Filter Compendium Method (PM10, PM2.5)
(PM10, PM2.5) IO3.5:
(Validated - Applied Out Validated Applied out of scope:
Validated Applied of Scope) Al, Sb, As, Ba, Be, Bi, Cd, Cr,
out of scope: Determination Of Co, Cu, Pb, Mg, Mn, Mo, Ni,
Al, Sb, As, Ba, Be, Metals In Ambient Se, Ag, Tl, Th, U, V, Zn, B, Ca,
Bi, Cd, Cr, Co, Cu, Particulate Matter Fe, K, Li, Na, Si, Sn, Hg, P, Sr,
Pb, Mg, Mn, Mo, Ni, Using Inductively Ti
Se, Ag, Tl, Th, U, V, Coupled Plasma (ICP)
Zn, B, Ca, Fe, K, Li, Spectroscopy
Na, Si, Sn, Hg, P,
Sr, Ti

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Cellulose Filter Determination of NIOSH 7303, Issue 1, 2003.
CHEMISTRY - Membrane Metals for SSO VALIDATED (Modified), 2018.
INORGANIC (metals fumes - In
(Lab Testing) (Chemistry - Cellulose Filter Elements by ICP (Hot
(cont’d.) Occupational Health Membrane): Block/HCl/HNO3 Digestion).
& Safety)
Al, As, B, Ba, Be, Ca, Cd,
Co, Cr, Cu, Fe, Mg, Mn,
Mo, Ni, P, Pb, Sb, Se, Sn,
Sr, Tl, Ti, V, Zn
ENVIRONMENTAL Atmosphere Meteorological Parameters: ASTM D5741-96 (2017)
CLIMATOLOGY Environmental Standard Practice for
(Field Measurement) Temperature, Relative Characterizing Surface Wind
Humidity, Environmental Using a Wind Vane and
Pressure, Wind Speed, Rotating Anemometer
Wind Direction (Wind
Rose)
ENVIRONMENTAL Natural Water, Total Coliform (NMP)
SMEWW-APHA-AWWA-WEF
MICROBIOLOGY Water for human
Part 9221 B, 23rd Ed. 2017.
(Field collection + Lab use and
Testing) consumption, Saline
Water and Waste Multiple-Tube Fermentation
Water Technique for Members of the
Coliform Group. Standard Total
Coliform Fermentation
Technique
Fecal Coliform
SMEWW-APHA-AWWA-WEF
(Thermotolerant) (NMP)
Part 9221 F.2, 23rd Ed. 2017.
Multiple-Tube Fermentation
Technique for Members of the
Coliform Group. Escherichia coli
Procedure Using Fluorogenic
Substrate. Simultaneous
Determination of Termotolerant
Coliforms and E. Coli
Escherichia Coli (NMP)
SMEWW-APHA-AWWA-WEF
Part 9221 F.2, 23rd Ed. 2017

Multiple-Tube Fermentation
Technique for Members of the
Coliform Group. Escherichia
coli Procedure Using
Fluorogenic Substrate.
Simultaneous Determination of
Termotolerant Coliforms and
E.coli.

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Natural Water, Heterotrophic (UFC/mL)
SMEWW-APHA-AWWA-WEF
MICROBIOLOGY Water for human
Part 9215 B, 23rd Ed. 017
(Field collection + Lab use and
Heterotrophic Plate Count.
Testing) consumption, Saline
Pour Plate Count Method
(cont’d.) Water and Waste
Water Virus (Somatic Coliphages)
SMEWW-APHA-AWWA-WEF
(cont’d.) Part 9224 B, 23rd Ed. 2017
Detection of Coliphages.
Somatic Coliphages Assay
Fecal Enterococcus or
SMEWW-APHA-AWWA-WEF
Intestinal Enterococcus
Part 9230 B, 23rd Ed. 2017
(NMP)

Fecal
Enterococcus/Streptococcus
Groups. Multiple-Tube
Technique.
Vibrio cholerae (Detection)
SMEWW-APHA-AWWA-WEF
Part 9260 H, Item 1, 2, 3.d.1
(exception test toxin and
serogroup O139), 6a, 23rd Ed.
2017
Detection of Pathogenic
Bacteria. Vibrio
Salmonella spp (Detection) ISO 19250, 1st Ed 2010
Water Quality. Detection of
Salmonella spp.
Natural Water, Total Coliform
SMEWW-APHA-AWWA-WEF
Water for human (UFC/100mL)
Part 9222 B, 23rd Ed. 2017.
use and
consumption
Membrane Filter Technique for
Members of the Coliform
Group. Standard Total Coliform
Membrane Filter Procedure
using Endo Media
Fecal (Thermotolerant)
SMEWW-APHA-AWWA-WEF
Coliform (UFC/100mL)
Part 9222 D, 23rd Ed. 2017.

Membrane Filter Technique for


Members of the Coliform
Group. Thermotolerant (Fecal)
Coliform Membrane Filter
Procedure

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TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Escherichia Coli SMEWW-APHA-AWWA-WEF
MICROBIOLOGY (UFC/100mL) Part 9222 H, 23rd Ed. 2017
(Field collection + Lab
Testing) Membrane Filter Technique for
(cont’d.) Members of the Coliform
Group. Partitioning E. coli from
MF Total Coliform using EC-
MUG Broth
Natural Water, Helminth eggs MVAL-LAB-24, VALIDATED,
Water for human 2018
use and Quantification and Identification
consumption, and of Helminth Eggs in Water
Waste Water Pathogenic Protozoal MVAL-LAB-31, VALIDATED,
2019
Cysts / Oocysts
Quantification and Identification
of Cysts and Oocysts of
Pathogenic Protozoa in Water
Larvae (Nematodes) MVAL-LAB-32, VALIDATED,
2019
Quantification and Identification
of Helminth Larvae
(Nematodes) in Water.
Giardia sp / MVAL-LAB-33, VALIDATED,
Cryptosporidium sp 2019
Identification of Giardia sp and
Cryptosporidium sp in Water.
Parasitic Forms MVAL-LAB-34, VALIDATED,
2019
Quantification and Identification
of Parasitic Forms in Water.
Saline Water / Macrophytes in water SMEWW Part 10400 D. 2 a, 3 e
Natural Water 23 rd Ed 2017, Macrophytes
Saline water Helminth Eggs in water MVAL-LAB-48, 2021
(VALIDATED) Quantification
and Identification of helminth
eggs in saline water
Ice Fecal Coliforms SMEWW-APHA-AWWA-WEF
(Thermotolerant) (NMP) Part 9221 F.2, 23rd Ed.
Multiple-Tube Fermentation
Technique for Members of the
Coliform Group. Escherichia coli
Procedure Using Fluorogenic
Substrate. Simultaneous
Determination of Termotolerant
Coliforms and E.coli.
Fecal Enterococci SMEWW-APHA-AWWA-WEF

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Ice Part 9230 B, 23rd Ed.
MICROBIOLOGY (cont’d.) Fecal Enterococcus /
(Field collection + Lab Streptococcus Groups. Multiple-
Testing) Tube Technique
(cont’d.) Escherichia Coli (NMP) SMEWW-APHA-AWWA-WEF
Part 9221 F.2, 23rd Ed. 2017
Multiple-Tube Fermentation
Technique for Members of the
Coliform Group. Escherichia coli
Procedure Using Fluorogenic
Substrate. Simultaneous
Determination of Termotolerant
Coliforms and E.coli.
Heterotrophics (UFC) SMEWW-APHA-AWWA-WEF
Part 9215 B. 23rd Ed.
Heterotrophic Plate Count. Pour
Plate Count Method
Air – Atmosphere/ Aerobic mesophilic APHA. Ch 3, Part 3.101. 5th
Environment Ed. 2015 / ICMSF Method 1, p.
117-124, 2nd Ed. Reprint 2000.

Microbiological monitoring of
the food processing
environment. Air sampling
methods. Sedimentation
methods / Enumeration of
mesophilic aerobic
microorganisms. Plate counting
methods. Method 1 (Standard
plate count, whole medium
seeding plate count or slice
count) of aerobic
microorganisms.
Yeast APHA. Ch 3, Part 3.101. 5th
Ed. 2015 / ICMSF. p. 165-167,
2nd Ed. Reprint 2000
Microbiological monitoring of
the food processing
environment. Air sampling
methods. Sedimentation
methods / Mold and yeast
counts. Method of counting
molds and yeasts by slatting in
plate throughout the medium
Mold APHA. Ch 3, Part 3.101. 5th
Ed. 2015 / ICMSF. p. 165-167,
2nd Ed. Reprint 2000

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Air – Atmosphere/ Microbiological monitoring of
MICROBIOLOGY Environment the food processing
(Field collection + Lab (cont’d.) environment. Air sampling
Testing) methods. Sedimentation
(cont’d.) methods / Mold and yeast
counts. Method of counting
molds and yeasts by slatting in
plate throughout the medium
Live Surfaces Salmonella detection ISO 6579-1:2017/ Amd.1:2020
Inert surfaces (except 9.3.3, 9.4.3 and annex
D) // RM No 461-2007-MINSA.
Microbiology of the food chain --
Horizontal method for the
detection, enumeration and
serotyping of Salmonella -- Part
1: Detection of Salmonella spp.
Coliform Count ISO 4832 / RM No. 461-2007-
MINSA.
Microbiology of food and animal
feeding stuffs - Horizontal
method for the enumeration of
coliforms - Colony-count
technique // Technical Guide for
the Microbiological Analysis of
Surfaces in contact with Food
and Beverages.
Yeast Count ICMSF Food Microorganisms.
Their meaning and
enumeration methods. Pages
165-166. 2nd Ed. Reprint 2000
// RM No. 461-2007- MINSA
Yeast and mold counts. Method
of enumeration of molds and
yeasts by plating on the entire
medium
Count of mesophilic ICMSF Food Microorganisms.
aerobic microorganisms. Their meaning and
enumeration methods.
Method 1, Pages 117-123 2nd
Ed. Reprint 2000 // RM No.
461-2007-MINSA
Enumeration of aerobic
mesophilic microorganisms:
Method 1 (Standard plate count,
plate count by seeding in the
whole medium or plate count of
Live Surfaces
aerobic microorganisms

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TESTING MATRIX ANALYTE(S) REFERENCE
Inert surfaces Mold count ICMSF Food Microorganisms.
ENVIRONMENTAL (cont’d.) Their meaning and
MICROBIOLOGY enumeration methods. Pages
(Field collection + Lab 165-166. 2nd Ed. Reprint 2000
Testing) // RM No 461-2007-MINSA
(cont’d.) Yeast and mold counts. Method
of enumeration of molds and
yeasts by plating on the entire
medium
Staphylococcus Aureus ISO 6888-1:12021, except 9.4.3
Cogalusae Count Positive / RM No 461-2007-MINSA
(Point 8.4).
Microbiology of food and animal
feeding stuffs -- Horizontal
method for the enumeration of
coagulase-positive
staphylococci (Staphylococcus
aureus and other species) --
Part 1: Technique using Baird-
Parker agar medium.
Amendment 1: Inclusion of
precision data. Amendment 2:
Inclusion of an alternative
confirmation test using RPFA
stab method. // Technical Guide
for the Microbiological Analysis
of Surfaces in Contact with Food
and Beverages.
Soils, Fecal Coliforms SMEWW-APHA-AWWA-WEF
Sediment and (Thermotolerant) Part 9221 F.2, 23rd Ed. 2017.
Sludge Multiple-Tube Fermentation
Technique for Members of the
Coliform Group. Escherichia col
Procedure Using Fluorogenic
Substrate.
Simultaneous Determination of
Termotolerant Coliforms and
E.coli.
Total coliforms SMEWW-APHA-AWWA-WEF
Part 9221 B, 23rd Ed. 2017.
Multiple-Tube Fermentation
Technique for Members of the
Coliform Group. Standard Total
Coliform Fermentation
Technique.
Escherichia coli SMEWW-APHA-AWWA-WEF
Soils, Escherichia coli Part 9221 F.2, 23rd Ed. 2017.
(cont’d.) Multiple-Tube Fermentation

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TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Sediment and Technique for Members of the
MICROBIOLOGY Sludge Coliform Group. Escherichia coli
(Field collection + Lab (cont’d.) Procedure Using Fluorogenic
Testing) Substrate. Simultaneous
(cont’d.) Determination of Termotolerant
Coliforms and E.coli.
ENVIRONMENTAL Biological Tissue Boron and Tin EPA Method 200.3
BIOLOGY “Sample Preparation
(Field collection + Lab Procedure for Spectrochemical
Testing) Determination of Total
Recoverable Elements in
Biological Tissues (VALIDATED-
Applied Out of Scope)

EPA Method 200.7


“Determination of Metals and
Trace Elements in Water and
Wastes by Inductively Coupled
Plasma-Atomic Emission
Spectrometry”
Biological Tissues Total Cyanide EPA Method 9013A-Rev.2 /
(Animals and SMEWW-APHA-AWWA-WEF
Plants) Part 4500-CN¯ F, 23rd Ed
Macroinvertebrates 2017 (Validated - Modified)
Cyanide extraction procedure
for solids and oils / Cyanide -
Selective Electrode Method
Wastewater Quantitative Phytoplankton SMEWW-APHA-AWWA-WEF
Part 10200 Fitems: F.2.a,
F.2.c.1, 23rd Ed. 2017.
Plankton. Phytoplankton
Counting Techniques
Quantitative Zooplankton SMEWW-APHA-AWWA-WEF
Part 10200 G, 23rd Ed. 2017.
Plankton. Zooplankton
Counting Techniques
Free living organisms SMEWW-APHA-AWWA-WEF
(Algae, protozoa, Part 10200 B. 2. a, C.1, F. 2. a,
copepods, rotifers and c, 23rd Edition / SMEWW-
nematodes) APHA-AWWA-WEF Part
10200 B. 2. b, C.1, G. 23rd
Edition 2017
Plankton. Sample collection.
Concentration Techniques.
Wastewater Phytoplankton Counting
ENVIRONMENTAL
(cont’d.) Techniques / Plankton. Sample
BIOLOGY
collection. Concentration

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
(Field collection + Lab Techniques. Zooplankton
Testing) Counting Techniques
(cont’d.) Saline water Quantitative phytoplankton UNE-EN 15204 / SMEWW-
APHA-AWWA-WEF Part 10200
B. 2. a, C. 1, F. 2. a, c. 23rd Ed
Water quality. Guide for
counting phytoplankton by
inverted microscopy (Utermöhl
technique) / Plankton. Sample
collection. Concentration
Techniques. Phytoplankton
Counting Techniques.
Qualitative phytoplankton EPA Method 670/4-73-001
Biological field and laboratory
methods for measuring the
quality of surface waters and
effluents. PLANKTON. 2.2
Phytoplankton and 4.1.1
Qualitative Analysis of
phytoplankton.
Quantitative zooplankton SMEWW-APHA-AWWA-WEF.
Part 10200 B. 2. b. C. 1, G.
23rd Ed.
Plankton. Sample collection.
Concentration Techniques.
Zooplankton Counting
Techniques.
Qualitative zooplankton EPA Method 670/4-73-001
Biological field and laboratory
methods for measuring the
quality of surface waters and
effluents. PLANKTON. 2.3
Zooplankton. 4.2.1 Qualitative
Analysis of Zooplankton.
Natural water and Nekton SMEWW-APHA-AWWA-WEF
Saline water Part 10600 B.3, C y D. 23rd
Ed. 2017.
Fishes, collection and
observation Method, sample
preservation and Analysis of
collections
ENVIRONMENTAL Water for human Odor ISO 4121:2003
SENSORY use and Sensory analysis - Guidelines
(Field collection + Lab consumption for the use of quantitative
Testing) response scales
ENVIRONMENTAL Water for human Flavor SMEWW-APHA-AWWA-WEF
SENSORY use and Part 2160 C, 23rd Ed. 2017.
consumption

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
(Field collection + Lab (cont’d.) Flavor Rating Assessment
Testing) (FRA)
(cont’d.) Soils, Color Official Mexican Standard,
Sediment and NOM-021-RECNAT-2000, AS-
Sludge 09 (Validated - Out of Scope)
Which establishes the
specifications of fertility, salinity
and classification of soils.
Studies, sampling and analysis
- Color Determination
Odor MVAL-AGR-015 (Validated -
Modified)
FAO Manual (Soil
Classification)
ENVIRONMENTAL Sediments, Sludges Polychlorinated Biphenyls EPA Method 8082 A, Rev.01,
CHEMISTRY - and Soils PCBs (As congeners) 2007
ORGANICS Polychlorinated Biphenyls
(Field collection + Lab PCB 28 (PCBs) by Gas
Testing) PCB 52 Chromatography
PCB 101
PCB 118
PCB 138
PCB 153
PCB 180

Reference in ECA Soil


(DS Nº011-2017-MINAM):
Bifenilos Policlorados –
PCB (Sum of seven
PCBs indicators: PCB 28,
PCB 52, PCB 101,
PCB 118, PCB 138,
PCB 153, PCB 180)
PolycyclicAromatic EPA Method 8270 E, Rev.06,
Hydrocarbons (PAHs): 2018

Acenaphthene Semivolatile Organic


Acenaphthylene Compounds by Gas
Benz(a)anthracene Cromatogrphy/ Mass
Benzo(b)fluoranthene Spectrometry
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Phenanthrene
Sediments, Sludges Fluorene
and Soils Indeno(1,2,3-cd)pyrene

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TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL (cont’d.) Naphthalene
CHEMISTRY - Pyrene
ORGANICS Anthracene
(Field collection + Lab Benzo(a)pyrene
Testing) Fluoranthene
(cont’d.) Organochlorine EPA Method 8270 E, Rev. 06,
Pesticides 2018

Aldrin Semivolatile Organic


4,4´-DDT Compounds by Gas
Endrin Chromatography/ Mass
Heptachlor Spectrometry
Volatile Organic EPA Method 8260 D, Rev.04,
Compounds (VOCs) 2017
Volatile Organic Compounds by
Trichloroethene Gas Chromatography/Mass
Tetrachloroethene Spectrometry (GC/MS)
Benzene
Ethylbenzene
m,p-Xylene
o-Xylene
Toluene
Naphthalene
Total Petroleum EPA Method 8015 C, Rev. 3,
Hydrocarbons (C5-C10) 2007/EPA 5021 A, Rev. 2,
2014.
VALIDATED (Applied out of
reach), 2020.

Nonhalogenated Organics by
Gas Chromatography
Total Petroleum EPA Method 8015C, Rev.3,
Hydrocarbons 2007.
(C6-C40)
Nonhalogenated Organics by
Gas Chromatography
Pristane EPA Method 8015 C, Rev. 3
Nonhalogenated Organics by
Gas Chromatography
(Validated-applied out of scope)
Phytane EPA Method 8015 C, Rev. 3
Nonhalogenated Organics by
Gas Chromatography
Sediments, (Validated-applied out of scope)
Sludges and Organochlorine and EPA METHOD 8270E (SW-
ENVIRONMENTAL Soils Organophosphate 846) Rev. 06
CHEMISTRY - (cont’d.) Pesticides Semivolatile Organic
ORGANICS Compounds By Gas

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
(Field collection + Lab Isodrin, Chromatography/ Mass
Testing) Malation and Spectrometry (GC/MS)
(cont’d.) Palation
Emission / Volatile Organic EPA Method 18, 2019
Stationary Sources Compounds (VOCs)
Ethylbenzene, Measurement of Gaseous
Styrene, Organic Compound Emissions
Cis-1,3-Dichloropopene, by Gas Chromatography
Trans-1,3-Dichloropropene,
(m + p) Xylene,
1,2-Dichloroethane,
Vinyl Acetate,
Toluene,
Chlorobenzene,
Chlorodibromomethane,
Tetrachloroethane,
Cis-1,2-Dichloroethane,
Benzene,
Trans-1,2-Dichloroethane,
Carbon tetrachloride,
Acetone,
Chloroform,
1,1,1-Trichloroethane,
Toluene,
Bromochloromethane,
Vinyl Chloride,
Carbon Disulfide,
Bromoform,
Bromodichloromethane,
1,1-Dichloroethane,
1,1,2 Trichlorotrifluoethane,
1,2-Dichloropropane,
1,1,2-Trichloroethane,
Trichloroethane,
1,1,2,2-Tetrachloroethane,
o-Xylene,
Trimethylamine,
Acrylonitrile,
Methyl isobutyl ketone
(MIBK), Methyl butyl ketone
(2-Hexanone),
Methyl ethyl ketone (2-
Butanone),
Total Xylenes
ENVIRONMENTAL Ambient air Benzene (C6H6) NTP 712.107:2020
CHEMISTRY - Ambient air Environmental Quality
ORGANICS (cont’d.) Monitoring.
Benzene concentration
measurement method in

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
(Field collection + Lab ambient air. Part 2: Aspiration
Testing) sampling followed by solvent
(cont’d.) desorption and gas
chromatography
Benzene (C6H6) NTP 712.107:2020
(VALIDATED - modified)
Environmental Quality
Monitoring.
Benzene concentration
measurement method in
ambient air. Part 2: Aspiration
sampling followed by solvent
desorption and gas
chromatography
Air Benzene UNE-EN 13528-1:2003 / UNE-
EN 13528-2:2003 / UNE-EN
13528-3:2004
Ambient air quality - Diffusive
sensors for the determination of
gas and vapor concentrations -
Part 1: General requirements -
Part 2: Specific requirements
and test methods - Part 3:
Guide to selection, use and
maintenance
Emission Non-Methane EPA CFR Title 40, Appendix
Hydrocarbons (NMHC) A-7 to Part 60, METHOD 25
Determination of total gaseous
nonmethane organic emissions
as carbon
Total Hydrocarbons / Total CTM-022 /CTM-030
Organic Hydrocarbons (Validated)
Determination of Nitric Oxide,
Nitrogen Dioxide and NOx
Emissions from Stationary
Combustion Sources by
Electrochemical Analyzer 1995
/ Determination of Nitrogen
Oxides, Carbon Monoxide, and
Oxygen Emissions from Natural
Gas-Fired Engines, Boilers and
Process Heaters using Portable
Analyzers, 1997
ENVIRONMENTAL Natural Water, Polychlorinated Biphenyls EPA Method 8082 A, Rev.01,
CHEMISTRY - Water for human PCBs (As Aroclor) 2007
ORGANICS use and Polychlorinated Biphenyls
consumption, Saline Aroclor 1016 (PCBs) by Gas
Aroclor 1221 Chromatography

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TESTING MATRIX ANALYTE(S) REFERENCE
(Field collection + Lab Water and Waste Aroclor 1232
Testing) Water Aroclor 1242
(cont’d.) Aroclor 1248
Aroclor 1254
Aroclor 1260
Aldicarb EPA Method 8270 E, Rev.6
2018.
VALIDATED (Applied out of
reach), 2018.

Semivolatile Organic
Compounds by Gas
Cromatography/ Mass
Spectrometry
Organochlorine Pesticides EPA Method 8081B, Rev. 02,
2007
α-BHC (alpha BHC)
β-BHC (beta BHC) Organochlorine Pesticides by
δ-BHC (delta BHC) Gas Chromatography
γ-BHC (Lindane)
cis-Chlordane
trans- Chlordane
Endosulfan I
Endosulfan II
Endosulfan Sulfate
4,4’-DDT
4,4’-DDD
4,4’-DDE
Endrin
Endrin aldehyde
Endrin ketone
Methoxychlor
Heptachlor
Heptachlor epoxide
Aldrin
Dieldrin

DS N° 004-2017-MINAM,
DDT (Sum) = 4,4’-DDD +
4,4’-DDE;
Aldrin + Dieldrin;
Heptachlor + Heptachlor
epoxide;
Natural Water, Chlordane (Sum)= cis-
ENVIRONMENTAL Water for human Chlordane+ trans-
CHEMISTRY - use and Chlordane
ORGANICS consumption, Saline Volatile Organic EPA Method 8260D, Rev.04,
Compounds (VOCs) 2017

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
(Field collection + Lab Water and Waste 1,1,1,2-Tetrachloroethane Volatile Organic Compounds by
Testing) Water 1,1,1-Trichloroethane Gas Chromatography/Mass
(cont’d.) (cont’d.) 1,1,2,2-Tetrachloroethane Spectrometry (GC/MS)
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethylene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-
Chloropropane
1,2-Dibromoethane
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane (1,2-
DCP)
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Carbon Tetrachloride
Chlorobenzene
cis-1,2-Dichloroethene
Dibromomethane
Ethylbenzene
Hexachlorobutadiene
m,p-Xylene
n-Butylbenzene
n-Propylbenzene
Naphthalene
o-Xylene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
ENVIRONMENTAL trans-1,2-Dichloroethylene EPA Method 8260D, Rev.04,
CHEMISTRY - Natural Water, Trichloroethene 2017
ORGANICS Water for human 1,1,2-Trichloroethene Volatile Organic Compounds by
(Field collection + Lab use and p-Isopropyltoluene Gas Chromatography/Mass
Testing) consumption, Saline Bromodichloromethane Spectrometry (GC/MS)
(cont’d.) Bromoform

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Water and Waste Dibromochloromethane
Water Chloroform
(cont’d.) Cumene
(Isopropylbenzene)
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Dichloromethane
Vinyl chloride

Trihalomethane:
Reference in ECA Water
(DS N°004-2017-MINAM)
y DS N° 031-2010-SA:
Total Trihalomethane:
Bromodichloromethane,
Bromoform,
Dibromochloromethane,
Chloroform and Total
Xylene.
Polycyclic Aromatic EPA Method 8270E, Rev. 06,
Hydrocarbons (PAHs): 2018

1-Methylnaphthalene Semi-volatile Organic


2-Methylnaphthalene Compounds by Gas
Acenaphthene Chromatography/Mass
Acenaphthylene Spectrometry (GC/MS)
Benz(a)anthracene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Chrysene
Dibenz(a,h)anthracene
Phenanthrene
Fluorene
Indeno(1,2,3-cd)pyrene
Naphthalene
Pyrene
Anthracene
Benzo(a)pyrene
Fluoranthene

Reference in ECA Water


ENVIRONMENTAL (DS Nº004-2017-MINAM):
CHEMISTRY - Total Oil Hydrocarbons
ORGANICS Natural Water, (Fraction Aromatic)
(Field collection + Lab Water for human
Testing) use and Organophosphorus and EPA 8270E, Rev 06,2018
(cont’d.) consumption, Saline Organochlorine Pesticides I Semivolatile Organic
Compounds by Gas

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Water and Waste • ALPHA-BCH Chromatography/ Mass
Water (alpha-HCH) Spectrometry (GC/MS)
(cont’d.) • Beta-BHC (beta-
HCH)
• Gamma-BHC
(Lindane)
• Delta-BHC (delta-
HCH)
• Heptachlor
• Aldrin
• Heptachlor epoxide
(isomer B)
• Trans-Chlordane
• Cis-Chlordane
• Endosulfan I
• 4,4'-DDE
• Dieldrin
• Endrin
• 4,4'-DDD
• Endosulfan II
• Endrin aldehyde
• 4,4'-DDT
• Endosulfan sulfate
• Methoxychlor
• Endrin ketone
• Malathion
• DDT (Sum) = (4,4´
DDD + 4,4´-DDE)
• Aldrin + Dieldrin
• Heptachlor +
Heptachlor
• Epoxide
Chlordane (Sum) )= cis-
Chlordane+ trans-
Chlordane
Organophosphorus EPA Method 8270E, Rev. 06,
ENVIRONMENTAL Pesticides 2018
CHEMISTRY - Semi-volatile Organic
ORGANICS Malathion Compounds by Gas
(Field collection + Lab Parathion Chromatography/Mass
Testing) Spectrometry (GC/MS)
(cont’d.)
Natural Water, Organophosphorus and EPA 8270E Rev.6, 2018.
Water for human Organochlorine VALIDATED (Applied out of
use and Pesticides II reach), 2019.
consumption

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Hexachlorobenzene, Semivolatile Organic
Trifluralin, Compounds by Gas
Chloropyrifos Chromatography/Mass
Spectrometry
Microcystin LR ISO 20179:2005
Determination of microcystins –
Method using solid phase
extraction (SPE) and high
performance liquid
chromatography (HPLC) with
ultraviolet (UV) detection
Water for human Total Petroleum EPA Method 8015 C, Rev. 3,
use and Hydrocarbons (C10-C40) 2007
consumption, Diesel DRO Range (C10- Nonhalogenated Organics by
Natural water, C28) Gas Chromatography
Waste water, Saline
water, Process Referenced in DS N ° 031-
water 2010-SA: Dissolved or
emulsioned hydrocarbon;
mineral oil
Total Petroleum EPA Method 8015C / Rev.3
Hydrocarbons (TPH) 2007

Ranges: (C8-C40), (C8- Nonhalogenated Organics by


C28), (C28-C40), (C6-C40) Gas Chromatography
BTEX: EPA Method 8015C Rev. 3,
2007 / EPA Method 5021 A
• Benzene Rev. 2, 2014
• Toluene Nonhalogenated Organics by
• Ethylbenzene Gas Chromatography / Volatile
• m,p- Xylene Organic Compounds in Various
Sample Matrices using
• o-Xylene
Equilibrium Headspace
• Total Xylenes Analysis.
ENVIRONMENTAL Water for human
CHEMISTRY - use and Gasoline EPA Method 8260D, Rev.4
ORGANICS consumption, 2018
(Field collection + Lab Natural water, Benzene,
Testing) Waste water, Saline Isooctane, Volatile Organic Compounds by
(cont’d.) water, Process Heptane, Gas Chromatography/Mass
water Toluene, Spectrometry
(cont’d.) Ethylbenzene,
m-Xylene,
p-Xylene,
o-Xylene,
1,2,4-trimethylbenzene
Steres Ftalatos EPA Method 8270E / Rev.6
2018
Dimethyl Phthalate,

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Diethyl Phthalate, Semivolatile Organic
Di-n-Butyl Phthalate, Compounds by Gas
Butyl Benzyl Phthalate, Chromatography /Mass
Di (2-Ethylhexyl) phthalate, Spectrometry
Di-n-Octyl Phthalate
Phenolics EPA Method 8270E / Rev.6
2018
2,3,4,6-Tetrachloro Phenol;
2,4,5-Trichlorophenol; Semivolatile Organic
2,4,6-Trichlorophenol; Compounds by Gas
2,4-Dichlorophenol; Chromatography/Mass
2,4-Dimethylphenol; Spectrometry
2,6-Dichlorophenol;
2-Chlorophenol;
2-Methylphenol (o-cresol);
2-Nitrophenol;
4-Chloro-3-Methylphenol;
4-Methylphenol;
Benzoic acid;
4 Nitrophenol;
Pentachlorophenol (PCP);
Phenol.
Water for human Volatile Organic Pollutants EPA Method 8260D / Rev.4
use and 2018
consumption, Vinyl Chloride, Volatile Organic Compounds by
natural water, Epichlorohydrin Gas Chromatography/Mass
process water Spectrometry
Fishes Total Petroleum EPA Method 8015 C, Rev. 3,
Hydrocarbons (C10-C40) 2007. (VALIDATED –
Biological Tissues Modified), 2020
ENVIRONMENTAL
CHEMISTRY - Nonhalogenated Organics by
ORGANICS Gas Chromatography
(Field collection + Lab Fishes Polycyclic Aromatic EPA Method 8270 E, 2018.
Testing) Hydrocarbons (PAHs): (VALIDATED – Modified),
(cont’d.) Biological Tissues Acenaphthene 2020
(cont’d.) Acenaphthylene Semivolatile Organic
Benzo (a) anthracene Compounds by Gas
Benzo(a)pyrene Chromatography/ Mass
Benzo(b)fluoranthene Spectrometry (GC/MS)
Benzo(k)fluoranthene
Anthracene
Chrysene
Phenanthrene
Fluoranthene
Fluorene
Pyrene

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
ENVIRONMENTAL Sediments, Sludges Recoverable Petroleum EPA METHOD 9074, Rev.0,
CHEMISTRY - and Soils Hydrocarbon 2007.
ORGANICS
Turbidimetric Screening
(Field Testing) Method for Total Recoverable
Petroleum Hydrocarbons in
Soil. (PetroFLAG analyzer)
Emissions Dioxins and Furans EPA CFR Title 40, Appendix
A-7 to Part 60, Method 23
Determination of
polychlorinated dibenzo-p-
dioxins and polychlorinated
dibenzofurans from stationary
sources
ACOUSTICS Environmental Noise
NTP-ISO 1996-1, 2007 /NTP-
(Field Measurement) Noise
ISO 1996-2, 2008

ACOUSTICS. Description.
measurement and assessment
of environmental noise.
Part1: Basic quantities and
assessment procedures /
ACOUSTICS. Description,
measurement and assessment
of environmental noise.
Part 2: Determination of
environmental noise levels.
NTP ISO 1996-2:2021 / NTP
ISO 1996-1:2020
ACOUSTICS. Description,
measurement and assessment
of environmental noise.
Part 2: Determination of
environmental noise levels
ACOUSTICS Environmental Noise ACOUSTICS. Description.
(Field Measurement) Noise (cont’d.) measurement and assessment
(cont’d.) (cont’d.) of environmental noise.
Part1: Basic quantities and
assessment procedures
OCCUPATOINAL Occupational Noise Occupational noise - DS 024-2016-EM modified as
HEALTH & SAFETY – Dosimetry per D.S. N° 023-2017-EM
ACOUSTICS Occupational noise - DS 024-2016-EM modified as
(Field Measurement) Sonometry per D.S. N° 023-2017-EM
Occupational health Occupational Vibration NTP – ISO 2631-
1:2011(revisada el 2016) /
NTP-ISO 2631-2:2012

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
(revisada el 2017)
Mechanical vibration and
shock -Evaluation of human
exposure to whole-body
vibration - Part 1: General
requirement. / Part 2: Vibration
in buildings (1 Hz to 80 Hz).
Thermal Stress UNE-EN ISO 7243:2017 /
UNE-EN ISO 11079:2009
Ergonomics of the thermal
environment. Heat stress
assessment using the WBGT
index (wet bulb and globe
temperature) (ISO 7243:2017)
(Ratified by the Spanish
Association for Standardization
in November 2017.) /
Ergonomics of the thermal
environment. Determination
and interpretation of cold
stress using required clothing
insulation (IREQ) and the
effects of local cooling. (ISO
11079:2007)
Sulfide K-600 Miltirae (Validated -
Sulfate Modified)
K-600M with built in pump
ENVIRONMENTAL – Non-ionizing Magnetic flux density R.M. Nº 613-2004-MTC-03
ELECTROMAGNETIC radiation Electrical field strength
RADIATION – AIR Fixed site radiation Magnetic field strength
(Field Measurement) power density
ENVIRONMENTAL – Air Non-Ionizing IEEE STD. 644.2019
ELECTROMAGNETIC Indoor Air Electromagnetic Radiation IEEE Standard for
RADIATION – AIR Measurement of Power
(Field Measurement) Frequency Electric and
(cont’d.) Magnetic Fields from AC Power
Lines.
Air Environmental Vibration UNE – EN ISO 5349-2 (2002).
Mechanical vibration -
Measurement and evaluation
of human exposure to hand-
transmitted vibration - Part 2:
Practical guidance for
measurement at the workplace.
AGRONOMY Foliar (Vegetation) Moisture content Official Mexican Standard
CHEMISTRY - NOM-021-RECNAT-2000,
INORGANIC which establishes the
specifications of fertility,

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
(Field collection + Lab salinity, and soil classification,
Testing) Studies, sampling and analysis.
AS-05; item 7.1.5
Moisture content by gravimetry
Dry Matter Official Mexican Standard
NOM-021-RECNAT-2000,
which establishes the
specifications of fertility,
salinity, and soil classification,
Studies, sampling and analysis.
AS-05; item 7.1.5 (Validated -
Out of Scope)
Moisture Content by
Gravimetry.
Total Metals: B, Ca, Cu, MVAL-AGR-04
Fe, K, Mg, Mn, Na, P, S,
Foliar Metals by ICP-OES
Zn.
Spectrophotometry.
Chlorides MVAL-AGR-05
Chlorides in Foliar by
Volumetry.
Organic Fertilizer Total Organic Carbon Official Mexican Standard
Fertilizer, NOM-021-RECNAT-2000, AS-
Substrate, 07 (Validated - Out of Scope)
Peat,
Compost Which establishes the
specifications of fertility, salinity
and soil classification. Studies,
sampling and analysis -
AGRONOMY Organic Fertilizer Determination of Organic
CHEMISTRY - Fertilizer, Carbon
INORGANIC Substrate,
(Field collection + Lab Conductivity (1:10) MVAL-AGR-002
Peat, Determination of conductivity
Testing) Compost
(cont’d.) (1:1; 1:2.5; 1:10; EPS)
(cont’d.)
Organic material Official Mexican Standard
NOM-021-RECNAT-2000, AS-
07 (Validated - Out of Scope)

Which establishes the


specifications of fertility, salinity
and soil classification. Studies,
sampling and analysis -
determination of organic matter
pH (1:10) MVAL-AGR-001
pH Determination
(1:1; 1:2.5; 1:10; EPS)

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
C/N ratio (Carbon and MVAL-AGR-022
Nitrogen) Calculated by ratio between
TOC: NOM-021-RECNAT-
2000, AS-07 (Validated Out of
Scope) and Nitrogen: ISO
16634-2: 2016 (Validated -
Modified)
Organic Fertilizer Ag, Al, As, B, Ba, Be, Ca, EPA Method 3050 B rev.2,
Inorganic Fertilizer Cd, Co, Cr, Cu, Fe, K, Li, 1996 / EPA METHOD 200.7,
Mg, Mn, Mo, Na, Ni, P, Pb, Rev. 4, (Validated - Modified)
Sb, Se, Sn, Tl, Ti, V, Zn, S Acid Digestion of Sediments,
Sludges, and Solis /
Determination of Metals and
Trace Elements in Water and
Wastes by Inductively Coupled
Plasma-Atomic Emission
Spectrometry.
As, Cd, Cr, Ni, Hg, Pb EPA Method 3050 B rev.2,
1996 / EPA METHOD 6020B,
Rev. 2, 2014 (Validated -
Modified)

Acid Digestion of Sediments,


Sludges, and Solis /
Determination of Metals and
Trace Elements in Inductively
Coupled Plasma - Mass
Spectrometry, part of Test
Methods for Evaluating Solid
Waste, Physical/Chemical
AGRONOMY Methods.
CHEMISTRY - Organic Fertilizer B, Ca, Cu, Mg, Mn, K, Na, EPA Method 3050 B rev.2,
INORGANIC Zn, P, Fe 1996 / EPA METHOD 200.7,
(Field collection + Lab Rev. 4, (Validated - Modified)
Testing) Acid Digestion of Sediments,
(cont’d.) Sludges, and Solis /
Determination of Metals and
Trace Elements in Water and
Wastes by Inductively Coupled
Plasma-Atomic Emission
Spectrometry.
Inorganic Fertilizer B, K2O, P2O5, CaO; MgO, EPA 200.7 (Validated -
Na, S, Fe, Mn, Zn Modified)
Determination of Metals and
Trace Elements in Water and
Wastes by Inductively Coupled
Plasma-Atomic Emission
Spectrometry

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
FOODS - INORGANIC Alcoholic drinks, As, Cd, Hg, Pb AOAC 2015.01 21st Edition
(Lab Testing) Canned fish Heavy Metals in Food.
Fruits Inductively Couples Plasma-
Fruit Juice (Nectars) Mass Spectrometry
Milk powder
Confectionery
products
(Chocolate)
Oils and fats
Protein Concentrate
Alcoholic drinks B, Na, Mg, Al, P, K, Ca, Cr, AOAC 2015.01 21st Edition
Canned Fish, Fruits Mn, Fe, Co, Ni, Cu, Zn, As, (VALIDATED-Out of scope)
Fruit Juice (Nectars) Se, Mo, Cd, Sn, Sb, Ba, Heavy Metals in Food.
Milk powder Hg, Pb Inductively Couples Plasma-
Confectionery Mass Spectrometry
products
(Chocolate)
Oils and fats
Protein Concentrate
Processed Fish
pota flour
Fish flour
Processed
Cephalopods.
Meat and Meat Pb, Cd, Zn, Cu, Fe AOAC 999.10-2005 21st
Producer Edition
Confectionery
Spices condiments Lead, Cadmiun, Zinc, Copper
and sauces, and Iron in foods Atomic
dried fruits Absorption Spectrophotometry
vegetables, cereal after Microwave Digestion
FOODS - INORGANIC grains, legumes
(Lab Testing) fresh and processed Pb, Cd, Zn, Cu, Fe
(cont’d.) mollusk (cont’d.)
fresh and processed
fish
Bakery, pastry and
biscuit products.
Canned fish Sn AOAC Official Method
Preserves in tin 2013.06-2013 21st Edition
containers (VALIDATED-Out of scope)
Fresh fish
refrigerated fish Arsenic, Cadmiun, Mercury and
Frozen fish Lead in foods. Pressure
bivalve molluscs digestion and inductively
mollusks coupled plasma mass
Crustaceans spectrometry
semi-preserves
Frozen products

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Fresh fish As, Cd, Hg, Pb AOAC 2013.06-2013 21st
Frozen fish Edition
bivalve molluscs (VALIDATED-Out of scope)
mollusks Arsenic, Cadmiun, Mercury and
Crustaceans Lead in foods. Pressure
semi-preserves digestion and inductively
Fish flour coupled plasma mass
squid flour spectrometry
Cr AOAC 2013.06-2013 21st
Edition
(VALIDATED-Out of scope)
Arsenic, Cadmiun, Mercury and
Lead in foods. Pressure
Digestion and Inductively
Coupled Plasma Mass
Spectrometry
Crude fish oil As, Cd, Hg, Pb AOAC 2013.06-2013 21st
Refined fish oil Edition
Semi-refined fish oil (VALIDATED-Out of scope)
Arsenic, Cadmiun, Mercury and
Lead in foods. Pressure
digestion and inductively
coupled plasma mass
spectrometry
Fish flour Cu y Zn AOAC 2011.14-2011
(VALIDATED-Out of scope)
Calcium, Copper, Iron,
Magnesium, Manganese,
Potassium, Phosphorus,
Sodium, and Zinc in Fortified
Food Products. Microwave
Digestion and ICP-OES
FOODS - Processed foods Count of Mesophilic ICMSF Food Microorganisms.
MICROBIOLOGY Foods for Special Aerobic Microorganisms. Their meaning and
(Lab Testing) Diets enumeration methods.
Sugars, Honeys and Method 1, Pages 117-123 2nd
Similar Ed. Reprint 2000
Beverages
Meat and meat Enumeration of aerobic
products mesophilic microorganisms:
Cereal Grains, Method 1 (Standard plate
Legumes, count, plate count by seeding in
Quenopodiaceas the whole medium or plate
and derivatives count of aerobic
(Flour and others) microorganisms
Spices, Condiments
and Sauces

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TESTING MATRIX ANALYTE(S) REFERENCE
Fruits, Vegetables,
Nuts and Other
Vegetables
Milk and Dairy
Products
Dehydrated
products:
Lyophilized or
concentrated and
mixtures
Frozen
hydrobiological
products
Refrigerated
Hydrobiological
Products
Pre-cooked and
cooked
hydrobiological
products
Crustaceans and
Molluscs raw;
Molluscs and
crustaceans pre-
cooked and cooked;
Frozen Raw
Breaded
Hydrobiological
Products;
Precooked and
frozen cooked
breaded
FOODS - hydrobiological
MICROBIOLOGY products
(Lab Testing) Processed foods Coliform Count ICMSF Food Microorganisms.
(cont’d.) Foods for Special Their meaning and
Diets enumeration methods.
Sugars, Honeys and Method 1, Pages 132-134.
Similar 2nd Ed. Reprint 2000
Beverages
Meat and meat COLIFORM BACTERIA.
products Coliform count: technique of
Cereal Grains, Most Probable Number (MPN).
Legumes, Method 1 (North American)
Quenopodiaceas
and derivatives
(Flour and others)
Spices, Condiments
and Sauces

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TESTING MATRIX ANALYTE(S) REFERENCE
Ice Cream and Ice
Cream Mixes
Milk and Dairy
Products
Dehydrated
products:
Lyophilized or
concentrated and
mixtures
Processed foods Escherichia Coli Count ISO 16649-3 2015
Meat and Meat Microbiology of food chain -
Products Horizontal method for the
Cereal Grains, enumeration of beta-
Legumes, glucuronidase-positive
Chenopodiaceae Escherichia coli -- Part 3:
and derivatives Detection and Most probable
(Flour and others) number technique using 5-
Spices, Condiments bromo-4-chloro-3-indolyl-beta-
and Sauces D-glucuronide
Fruits, Vegetables,
Nuts and Other
Vegetables
Bakery, Pastry and
Biscuit Products
Confectionery
products
Milk and Dairy
Products: Unripe
cheeses
Dehydrated
products:
Lyophilized or
FOODS - concentrated and Escherichia coli ISO 16649-3 2015
MICROBIOLOGY mixtures (cont’d.) (cont’d.)
(Lab Testing) Frozen
(cont’d.) hydrobiological
products
Refrigerated
hydrobiological
products
Pre-cooked and
cooked
hydrobiological
products
Crustaceans and
Molluscs raw;
*Molluscs and
crustaceans pre-
cooked and cooked;

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Frozen Raw
Breaded
Hydrobiological
Products;
Precooked and
frozen cooked
breaded
hydrobiological
products
Foods for Special Mold ICMSF Food Microorganisms.
Regimes Their meaning and
Sugars, Honeys and enumeration methods. Pages
Similar 165-166. 2nd Ed. Reprint 2000
Beverages: Non-
carbonated Yeast and mold counts. Method
beverages of enumeration of molds and
Stimulants and yeasts by plating on the entire
Fruits medium
Spices, Condiments
and Sauces
Fruits, Vegetables,
Nuts and Other
vegetables
Milk and Dairy
Products
Bakery, Pastry and
Biscuit Products
Confectionery
Products
Dehydrated
products:
Lyophilized or
FOODS - concentrated and
MICROBIOLOGY mixtures
(Lab Testing)
(cont’d.) Foods for Special Yeast ICMSF Food Microorganisms.
Regimes, Sugars, Their meaning and
Honeys and Similar enumeration methods. Pages
Beverages: Non- 165-166. 2nd Ed. Reprint 2000
carbonated
beverages Yeast and mold counts. Method
Stimulants and of enumeration of molds and
Fruits yeasts by plating on the entire
Spices, Condiments medium
and Sauces
Fruits, Vegetables,
Nuts and Other
vegetables
Milk and Dairy
Products

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E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Bakery, Pastry and
Biscuit Products
Confectionery
Products
Dehydrated
products:
Lyophilized or
concentrated and
mixtures
Processed Foods: Salmonella ISO 6579-1:2017/ ISO 6579-
Foods for Special 1:2017/Amd 1:2020 (except
Regimes 9.3.3, 9.4.3 and Annex D)
Meat and Meat
Products Microbiology of the food chain -
Cereal grains, Horizontal method for the
Legumes, detection, enumeration and
Chenopodiaceae serotyping of Salmonella.
and derivatives Part 1: Detection of Salmonella
(Flour and others) spp /
Spices, Microbiology of the food chain -
Condiments and Horizontal method for the
Sauces, detection, enumeration and
Sugars Honeys and serotyping of Salmonella.
Similar Part 1: Detection of Salmonella
Fruits, Vegetables, spp. - Amendment 1: Broader
Nuts and other range of incubation
vegetables, temperatures, amendment to
Ice Cream and the status of Annex D, and
Ice Cream Mixes correction of the composition of
Bakery, Pastry and MSRV and SC
Biscuit Products
FOODS - Confectionery
MICROBIOLOGY Products Salmonella ISO 6579-1:2017/ ISO 6579-
(Lab Testing) Dehydrated (cont’d.) 1:2017/Amd 1:2020 (except
(cont’d.) Products: 9.3.3, 9.4.3 and Annex D)
Lyophilized or
concentrated and Microbiology of the food chain -
mixtures Horizontal method for the
Milk and Dairy detection, enumeration and
Products serotyping of Salmonella.
Frozen Part 1: Detection of Salmonella
hydrobiological spp /
products Microbiology of the food chain -
Refrigerated Horizontal method for the
hydrobiological detection, enumeration and
products serotyping of Salmonella.
Pre-cooked and Part 1: Detection of Salmonella
cooked spp. - Amendment 1: Broader
range of incubation

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IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Hydrobiological temperatures, amendment to
Products; the status of Annex D, and
Raw Molluscs and correction of the composition of
Crustaceans MSRV and SC
Molluscs and
crustaceans pre-
cooked and cooked
Frozen Raw
Breaded
Hydrobiological
Products;
Precooked and
frozen cooked
breaded
hydrobiological
products
Processed Foods: Staphylococcus Aureus ICMSF Food Microorganisms.
Foods for Special Enumeration Their meaning and
Regimes enumeration methods. Pages
Meat and Meat 235-238. 2nd Ed. Reprint 2000
Products Staphylococcus aureus.
Cereal grains, Method 5 (NMP technique with
Legumes, mannitol glycine tellurite broth).
Chenopodiaceae Coagulase test.
and Derivatives
(Flour and others)
Ice Cream and Ice
Cream Mixes
Milk and Dairy
Products
Spices, Condiments
FOODS - and Sauces:
MICROBIOLOGY Mayonnaise and Staphylococcus Aureus ICMSF Food Microorganisms.
(Lab Testing) other egg-based Enumeration Their meaning and
(cont’d.) sauces (cont’d.) enumeration methods. Pages
Bakery, Pastry and 235-238. 2nd Ed. Reprint 2000
Biscuit Products Staphylococcus aureus.
Dehydrated Method 5 (NMP technique with
Products: mannitol glycine tellurite broth).
Lyophilized or Coagulase test.
concentrated and
mixtures
Foods for Special Bacillus Cereus Count. ISO 7932:2004
Regimes Microbiology of food and animal
Cereal grains, feeding stuffs - Horizontal
Legumes, method for the enumeration of
Chenopodiaceae presumptive Bacillus cereus -
and Derivatives Colony-count technique at 30
(Flour and others) degrees C / Microbiology of

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IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Stimulants and food and animal feeding stuffs -
Fruits Horizontal method for the
Dehydrated enumeration of presumptive
products: Bacillus cereus - Colony-count
Lyophilized or technique at 30 degrees C -
concentrated and Amendment 1: Inclusion of
mixtures optional tests
Bakery, Pastry and
Biscuit Products
Meat and Meat Clostridium Perfringens ICMSF Food Microorganisms.
Products Their meaning and
Cereal grains, enumeration methods.
Legumes, Method 2, Pages 281-283, I, II
Chenopodiaceae and III. 2nd Ed. Reprint 2000
and Derivatives
(Flour and others): Clostridium perfringens. North
Containing meat American Method 2
Bakery, Pastry and
Biscuit Products:
With meat filling
Dehydrated
products:
Lyophilized or
concentrated and
mixtures: Containing
meat
Processed foods: Coliform Count ISO 4832:2006
(with and without Microbiology of food and animal
heat treatment) feeding stuffs -- Horizontal
Spices, Condiments method for the enumeration of
FOODS - and Sauces coliforms -- Colony-count
MICROBIOLOGY Ice Cream and Ice technique
(Lab Testing) Cream Mixes Coliform Count ISO 4832:2006
(cont’d.) Milk and dairy (cont’d.) Microbiology of food and animal
products feeding stuffs -- Horizontal
Meat and Meat method for the enumeration of
Products coliforms -- Colony-count
Hydrobiological technique
Products:
Raw hydrobiological
products;
Pre-cooked and
cooked
Hydrobiological
Products;
Raw Molluscs and
Crustaceans;

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IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Molluscs and
crustaceans pre-
cooked and cooked;
Frozen Raw
Breaded
Hydrobiological
Products;
Precooked and
frozen cooked
breaded
hydrobiological
products
Ice Cream and Ice Listeria Monocytogenes ISO 11290-2:2017
Cream Mixes count Microbiology of the food chain
Frozen — Horizontal method for the
hydrobiological detection and enumeration of
products Listeria monocytogenes and of
Refrigerated Listeria spp. — Part 2:
hydrobiological Enumeration method
products
Pre-cooked and
cooked
Hydrobiological
Products;
Raw Molluscs and
Crustaceans;
Molluscs and
crustaceans pre-
cooked and cooked;
Frozen Raw
Breaded
Hydrobiological
Products;
FOODS - Precooked and Listeria Monocytogenes
MICROBIOLOGY frozen cooked count
(Lab Testing) breaded (cont’d.)
(cont’d.) hydrobiological
products
Meat and Meat Detection of Listeria ISO 11290-1:2017
Products: Sausages Monocytogenes Microbiology of the food chain -
with heat treatment Horizontal method for the
Fruits, Vegetables, detection and enumeration of
Nuts and other Listeria monocytogenes and of
vegetables Listeria spp. Part 1: Detection
Milk and Dairy method
Products,
Ice Cream and Ice
Cream Mixes

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E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Frozen
Hydrobiological
Products
Refrigerated
hydrobiological
products
Pre-cooked and
cooked
Hydrobiological
Products;
Raw Molluscs and
Crustaceans;
Molluscs and
crustaceans pre-
cooked and cooked;
Frozen Raw
Breaded
Hydrobiological
Products;
Precooked and
frozen cooked
breaded
hydrobiological
products
Processed Foods: Positive Cogalus ISO 6888-1:12021, except
Foods for Special Staphylococcus Aureus 9.4.3
Regimes Count Microbiology of food chain -
Meat and Meat Horizontal method for the
Products enumeration of coagulase-
Cereal grains, positive staphylococci
Legumes, (Staphylococcus aureus and
Chenopodiaceae other species) -- Part 1:
and Derivatives Technique using Baird-Parker
(Flour and others) agar medium.
Ice Cream and Ice Positive Cogalus ISO 6888-1:12021, except
FOODS - Cream Mixes Staphylococcus Aureus 9.4.3
MICROBIOLOGY Milk and Dairy Count Microbiology of food chain -
(Lab Testing) Products (cont’d.) Horizontal method for the
(cont’d.) Spices, Condiments enumeration of coagulase-
and Sauces: positive staphylococci
Frozen (Staphylococcus aureus and
hydrobiological other species) -- Part 1:
products Technique using Baird-Parker
Refrigerated agar medium.
hydrobiological
products
Pre-cooked and
cooked

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IAS/TL/101-1
E.I.R.L
IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Hydrobiological
Products;
Crustaceans and
Molluscs raw;
Molluscs and
crustaceans pre-
cooked and cooked;
Frozen Raw
Breaded
Hydrobiological
Products
Precooked and
frozen cooked
breaded
hydrobiological
products
FOODS - Canned Fish Histamine NCh 2637. Of 2001
(Lab Testing) Fish Flour (Does not include (VALIDATED - modified)
Frozen Fish sampling) Hydrobiological products -
Fresh Fish Determination of Histamine and
Semi-Canned Fish other Biogenic Amines - HPLC
method with UV detector
Prepared Foods Vitamin A AOAC 2001.13-2001 21st
Beverages, Edition
Excluding Dairy
Products Vitamin A (Retinol) in Foods.
Meat And Meat Liquid Chromatography
Products, Including
Poultry and Game
Cereals And Cereal-
Based Products,
Derived from Cereal
Grains, Roots and
Tubers, Vegetables,
Legumes and Soft
FOODS - Palm Marrow or Vitamin A AOAC 2001.13-2001 21st
(Lab Testing) Heart. Excluding (cont’d.) Edition
(cont’d.) Bakery Products of
Food Category 07.0 Vitamin A (Retinol) in Foods.
Confectionery Liquid Chromatography
Sweeteners,
Including Honey
Fats And Oils, And
Fat Emulsions
Eggs And Egg-
Based Products
Food Products for
Special Nutritional
Uses

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IAS is an ILAC MRA Signatory
FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Bakery Products
Dairy Products and
Analogue Products
Oils and Fats Vitamin E AACC International Methods
Nuts and Seeds 86-06.01. 11th Edition
Eggs and (Validated - Modified)
Derivatives Analysis of Vitamins A and E by
Milk and Dairy High-Performance Liquid
Products ChromatographY
Raw Milk Acidity NTP 202.116:2008 (revised
Pasteurized Milk 2018), 3rd Edition
Uht Milk
MILK AND DAIRY
PRODUCTS. raw milk
Determination of acidity of milk.
Volumetric method.
Cereal Flakes NTP 205.039:1975 (Revised
2016)
(Validated - Applied out of
scope)

FLOURS. Determination of
titratable acidity
Bakery Products NTP 206.008:1976 (Revised
2021)

BAKERY PRODUCTS.
Determination of the
percentage of titratable acidity
Biscuits NTP 206.013:1981 (Revised
Noodles 2021)
Biscuits
Panettons CAKES, BISCUITS, PASTA
Pasta AND NOODLES. Determination
FOODS -
of acidity
(Lab Testing)
(cont’d.) Flour (S) Ash AOAC 923.03, 21st Edition

Ash of Flour. Direct Method


Biscuits AOAC 935.39 (B) / AOAC
Biscuits 923.03 21st Edition
Bread(S)
Bakery Products Baked Products. Ash
Balanced Food AOAC 942.05, 21st Edition

Ash of Animal Feed


Cereals NTP 205.004:2022, 3rd
Cereal Flakes Edition

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
Menestras
CEREALS AND LEGUMES.
Determination of ashes.
Cereals and Cereal- Raw Fiber AOCS - Ba 6 - 84. 7ma Edition
Based Products
Bakery products Crude Fiber in Oilseed By-
bread Products
Fat AOAC 935.39 (D) / AOAC
922.06 21st Edition

Baked Products. Fat


Cereals NTP 205.006:2017, 2nd
Cereal Flakes Edition /
Menestras NTP 205.006:2017/CT 1:2018

CEREALS AND MENESTRAS.


Determination of fat /
CEREALS AND MENESTRAS.
Fat determination. TECHNICAL
CORRIGENDA 1
Biscuits NTP 206.017:1981 (revised
2021)
BISCUITS. Fat percentage
determination
Flour (S) Humidity AOAC 925.10, 21st Edition
Solids (Total) and Loss on
Drying (Moisture) in Flour. Air
Oven Method
Cereals NTP 205.002:2021, 2nd
Cereal Flakes Edition
Menestras
Humidity CEREALS AND LEGUMES.
(cont’d.) Determination of moisture
FOODS -
(Lab Testing) content. routine method
(cont’d.) Biscuits NTP 206.011:2018, 2nd
Noodles Edition
Biscuits
Pasta CAKES, BISCUITS AND
PASTAS OR NOODLES.
Moisture determination
Bread NTP 206.011:2018, 2nd
Edition
(Validated - Applied out of
scope)

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
CAKES, BISCUITS AND
PASTAS OR NOODLES.
Moisture determination
Biscuits Peroxide Index NTP 206.016:1981 (Revised
2011)

BISCUITS. Determination of
peroxides
Oils and Fats Iodine Value AOAC 920.158, 21st Edition

Iodine Absorption Number of


Oils and Fats. Hanus Method.
Meat and Meat Ammonia Nitrogen NTP 201.032:1982 (revised
Products, Including 2015)
Poultry and Game,
Fish and Fishery MEAT AND MEAT PRODUCTS
Products, Including Determination of ammoniacal
Molluscs, nitrogen content
Crustaceans and
Echinoderms
Meat and Meat pH AOAC 981.12, 21st Edition
Products, Including
Poultry and Game pH of Acidified Foods
Fruits and
Vegetables
Dairy Products and
Analogue Products
Balanced Food Protein AOAC 984.13, 21st Edition

Protein (Crude) in Animal Feed


and Pet Food. Copper Catalyst
Kjeldahl Method
Biscuit AOAC 984.13, 21st Edition
Biscuits Protein (Validated - Applied out of
Bread (cont’d.) scope)
FOODS -
(Lab Testing)
(cont’d.) Protein (Crude) in Animal Feed
and Pet Food. Copper Catalyst
Kjeldahl Method
Meat and Meat NTP 201.021:2002 (Revised
Products, including 2015)
poultry and game
MEAT AND MEAT
PRODUCTS. Determination of
protein content
Cereals NTP 205.005:2018
cereal flakes

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FIELDS OF MATERIAL/ DETERMINANT(S)/ METHOD
TESTING MATRIX ANALYTE(S) REFERENCE
stews CEREALS AND MENESTRAS.
Cereals. Determination of total
proteins (Kjeldahl method)

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