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IS 17943 : 2022
Indian Standard
E20 Reference Fuel — Admixture of
Anhydrous Ethanol and Motor
Gasoline — Specification
BIS 2022
Petroleum and Their Related Products of Synthesis or Biological Origin Sectional Committee, PCD 3
FOREWORD
This Indian Standard was adopted by the Bureau of Indian Standards, after the draft finalized by the Petroleum,
Lubricants and their Related Products of Synthesis or Biological Origin Sectional Committee had been approved
by the Petroleum, Coal and Related Products Division Council.
Ethanol is considered an alternative fuel source that possesses environment friendly characteristics associated with
its use. IS 15464 ‘Anhydrous Ethanol for use in Automotive Fuel’ specifies the requirement of denatured ethyl
alcohol only which need to be used as admixture with motor gasoline to make E5, E10 and E20 blends which can
be used in suitably designed positive ignition engines. The requirements of E20 fuel is specified in IS 17021 :
2018 ‘E20 Fuel — Admixture of Anhydrous Ethanol and Gasoline — As Fuel for Spark Ignited Engine Powered
Vehicles — Specification’. This standard describes the specification of E20 fuel for regular usage by consumer
and to be dispensed for use in suitably compatible vehicles.
However, as per the CMVR requirement (rule No. 115), for new vehicles type approval and conformity of
production tests, test agencies and OEMs shall use reference fuel. The reference fuel specification parameters
have closer tolerance limits, essential for the above-mentioned regulatory tests consistency and has additional
parameters which are not part of the IS 17021 : 2018.
Hence, this new standard is derived based on available global references of reference fuel, by expert committee
comprising OEMs and test agencies.
The usage of this standard is limited to the above-mentioned purpose, application and not to be referred as an
alternate for commercial manufacturing of E20 fuel for consumer usage and dispensing in the retail outlets.
Title of the ISO standards or other standards referred in table are given in Annex C. The composition of the
Committee responsible for the formulation of this standard is given in Annex D.
For the purpose of deciding whether a particular requirement of this standard is complied with, the final value,
observed or calculated, expressing the result of a test or analysis, shall be rounded off in accordance with IS 2 :
2022 ‘Rule for rounding off numerical values (second revision)’. The number of significant places retained in the
rounded off value should be the same as that of the specified value in this standard.
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IS 17943 : 2022
Indian Standard
E20 REFERENCE FUEL — ADMIXTURE OF ANHYDROUS ETHANOL
AND MOTOR GASOLINE — SPECIFICATION
1 SCOPE
IS No. Title
1.1 This standard prescribes requirements, methods
of sampling and test methods for E20 reference fuel, (Part 26) : Determination of knock
an admixture of anhydrous ethanol at 20 percent by 2018/ISO 5163 characteristics of motor and
volume and ethanol free motor gasoline at 80 : 2014 aviation fuels — Motor
percent volume, for use in Positive-Ignition Engines method (second revision)
Type Approval (TA) and Conformity of Production
(COP) tests by authorized test agencies and OEMs. (Part 27) : Determination of knock
2018/ISO 5164 characteristics of motor fuels
1.2 This standard does not purport to address all of : 2014 — Research method (second
the safety problems associated with its use. It is the revision)
responsibility of the user of this specification to
establish appropriate safety and health practices and (Part 28) : Petroleum products —
determine the applicability of regulatory limitations 2008/ISO 7536 Determination of oxidation
prior to use. : 1994 stability of gasoline —
Induction period method
2 REFERENCES (fourth revision)
The following standards contain provisions, which (Part 29) : Petroleum Products — Gum
through reference in this text constitute the 2021/ISO 6246 content of fuels — Jet
provisions of the standards. At the time of : 2017 evaporation method (fourth
publication, the editions indicated were valid. All revision)
standards are subject to revision and parties to
agreements based on this standard are encouraged to (Part 39) : Determination of vapour
investigate the possibility of applying the most 2012/ISO 3007 pressure — Reid method
recent editions of the standard indicated below: : 1999 (second revision)
1
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IS 17943 : 2022
3.2 Ethyl Alcohol (Absolute Alcohol) 4.3 Stabilizing Agents and Additives
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4.4.1 Permitted Components 5.2.2 Each container shall also be marked with the
following information:
The following components may be used either
individually or as mixtures as blending components a) Name and grade of the material;
or as stabilizing agents to prevent phase separation b) Indication of the source of manufacture,
of the E20 reference fuel: initials or trade-mark, if any;
c) Volume of the contents, in litres;
Ethers — Methyl tertiary butyl ether (MTBE), d) Year of manufacture or packing; and
tertiary amyl methyl ether (methoxy-2-methyl e) Any other statutory requirements.
butane) TAME, ethyl tertiary butyl ether (2-ethoxy-
2-methyl propane) ETBE and other ethers (R-O-R) 5.3.1 BIS Certification Marking
with final boiling point not exceeding 210oC and
The container may also be marked with the
with molecules containing five or more carbon
Standard Mark.
atoms.
5.3.1.1 The use of the Standard Mark is governed by
4.4.2 Content
the provisions of Bureau of Indian Standard Act,
When tested, the content of the individual 2016 and the Rules and Regulations made
components listed in Table 1 shall comply with the thereunder. The details of conditions under which
limiting requirements as given against the respective the license for the use of the Standard Mark may be
components in col 3, for the E20 reference fuel. granted to manufacturers or producers may be
obtained from the Bureau of Indian Standards.
In E20 reference fuel, the individual components
defined in 4.4.1 or their mixtures are permitted but 6 SAMPLING AND TEST METHODS
the total oxygen content shall not exceed the
6.1 Representative samples of the material shall be
requirements mentioned in Table 1, Sl No. (xvii).
drawn as prescribed in IS 1447 (Part 1).
4.4.3 Subject to the effect of the added denaturant,
anhydrous ethanol shall comply with the 6.2 Tests shall be conducted by the test method(s) as
prescribed in col 4 of Table 1.
3
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IS 17943 : 2022
Table 1 Requirement for E20 reference fuel for use in positive ignition engines TA and COP Tests
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NOTES
1 All the test methods referred in this standard include a precision statement. The Interpretation of results shall be based on test method
and precision data of test method whenever applicable. In case of dispute the procedure described in ISO 4259 shall be used.
2 The dry vapour test method and water tolerance test method given in Annex A and B shall be respectively followed.
3 In case of disputes, this method shall be the referee method.
4 MTBE, ETBE or TAME if added, need to be reported.
5 No addition of detergents, dispersants, silicon, chlorine containing additives, materials and metallic additives are allowed in the
reference fuel.
6
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ANNEX A
[Table 1, Sl No. (viii)]
TEST METHOD FOR VAPOUR PRESSURE OF GASOLINE-ALCOHOL BLEND
(DRY METHOD)
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A-7.1.1 Discard the sample if its volume is less than connection is inserted into a plastic bag to keep it
70 percent of the container capacity. completely dry during cooling.
A-7.1.2 If the container is more than 80 percent full, A-7.4 Preparation of Air Chamber
pour out enough sample to bring the container
contents within the 70 to 80 percent range. Under no Observe the apparatus preparation procedure of A-
circumstances, may any sample poured out, be 8.5. Connect the gauge to the air chamber and close
returned to the container. the lower opening securely with a dry No. 6 rubber
stopper. Make sure the stopper is inserted far enough
A-7.2 Air Saturation of Sample in Sample to securely close the vent hole in the air chamber
Container connection. Immerse the air chamber to at least 25
A-7.2.1 With the sample again at a temperature of 0 mm above its top in the water bath until the fuel
to 1oC take the container from the cooling bath, wipe chamber has been filled with the sample as
it dry with an absorbent material, unseal it described in A-8.1.
momentarily, taking care to prevent water entry,
reseal it, and shake it vigorously. Return it to the A-8 PROCEDURE
bath for a minimum of 2 min.
A-8.1 Sample Transfer
A-7.2.2 Repeat A-7.2.1 twice more. Return the
sample to the bath and keep it there until the With everything in readings, remove the chilled
beginning of the procedure (A-8). sample container from the bath, dry it with absorbent
material, uncap it, and dry and insert the chilled
A-7.3 Preparation of Fuel Chamber transfer apparatus (see Fig. 1). Quickly place the
Observe the apparatus preparation procedure of A- chilled fuel chamber, in an inverted position, over
8.5, then store the stoppered fuel chamber and the the sample delivery tube of the transfer apparatus.
sample transfer connection in a refrigerator or ice- Invert the entire system rapidly so that the fuel
water bath for a sufficient time to allow the chamber chamber is upright, with the end of the delivery tube
and the connection to reach a temperature of 0 to touching the bottom of the fuel chamber. Fill the fuel
1oC. If an ice-water bath is used, keep the chamber chamber to the overflowing. Withdraw the delivery
upright and not immersed over the top of the tube from the fuel chamber while allowing the
coupling threads. The transfer connection is inserted sample to continue flowing up to the moment of
over the top of the coupling threads. The transfer complete withdrawal.
FIG. 1 SIMPLIFIED SKETCHES OUTLINING METHOD OF TRANSFERRING SAMPLES TO GASOLINE CHAMBER FROM
OPEN-TYPE CONTAINERS
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upward at an angle of 45o with the coupling of the for and avoid condensation on the transfer
gauge pointing in the same direction. Swing the connection and interior walls of the apparatus.
arms downward through an arc of about 135o so that
the centrifugal force aids gravity in removing the A-10 REPORT
trapped liquid. Repeat this operation three times to
expel all liquid. Purge the pressure gauge by A-10.1 Reporting Results
directing a small jet of air into its Bourdon tube for
atleast 5 min. Rinse both chambers and the sample Report to the nearest 0.25 kPa or 0.5 kPa the gauge
transfer connection several times with petroleum result observed in A-8.4, after correcting for any
naphtha, then several times with acetone, then blow difference between the gauge and manometer, as the
dry using dried air. Stopper the fuel chamber and vapour pressure in kilopascals without reference to
place it in the refrigerator or ice-water bath for the temperature.
next test.
A-11 PRECISION AND BIAS
NOTE — If the purging of the air chamber is done in a
bath, be sure to avoid small and unnoticeable films of A-11.1 Precision
floating sample by keeping the bottom and top opening of
the chamber closed as they pass through the water surface. The following criteria should be used for judging the
acceptability of results (95 percent confidence).
A-9 PRECAUTIONS
A-11.1.1 Repeatability
A-9.1 Gross errors can be obtained in vapour
pressure measurements, if the prescribed procedure The difference between successive test results
is not followed carefully. The following list obtained by the same operator with the same
emphasizes the importance of strict adherence to the apparatus under constant operating conditions on
precautions given in the procedure. identical test material would, in the long run, in the
normal and correct operation of the test method,
A-9.1.1 Checking the Pressure Gauge exceed the following value only in one case in
twenty.
Check all gauges against a manometer after each test
in order to ensure high precision of results (see A-
8.4). Read all gauges while the gauges are in a Component Gauge Repeatability
vertical position and after tapping them lightly.
(Range) kPa
A-9.1.2 Shake the container vigorously to ensure
equilibrium of the sample with the air in the 0 to 100 kPa 4.90
container (see A-7.2).
11
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IS 17943 : 2022
ANNEX B
[Table 1 Sl No. (xii)]
TEST METHOD FOR WATER TOLERANCE (PHASE SEPARATION) OF GASOLINE-ALCOHOL
BLEND
This test method determines the ability of gasoline- B-4.1 Test Container — Any glass container of
oxygenate blends to retain water in solution or in a about 100 ml capacity may be used. This container
stable suspension at the lowest temperature to which may be marked at the level of 40 ml.
they are likely to be exposed in use.
B-4.2 Thermometers — A thermometer must be
B-2 SUMMARY OF TEST METHOD provided for each container, mounted to pass
through the stopper, with the requirements as
The sample of fuel is cooled at a controlled rate to follows:
its expected use temperature and is periodically
observed for both haze and phase separation. The a) Range – 80 to + 20°C,
apparatus as given in 4 of IS 1448 (Part 10/Sec 1) or b) Graduations 1°C, and
a dry ice-isopropyl alcohol bath may be used. A c) Immersion 76 mm.
maximum cooling rate of 2oC/mm is specified
because phase separation in gasoline-oxygenate B-4.3 Viton Rubber Stopper — To fit sample
blends has a relatively long but unpredictable container bored centrally for the test thermometer.
induction period.
B-4.4 Cooling Bath — May be of similar
B-3 SIGNIFICANCE AND USE dimensions to those specified in 4 of IS 1448 (Part
10/Sec 1) and provided with a jacket disk and gasket
B-3.1 Some oxygenate-containing fuels, and (as specified in the apparatus section) filled with an
gasoline-alcohol blends in particular have a very equal-volume mixture of water and ‘Permanent’
limited ability to retain water in solution or in stable antifreeze and provided with refrigeration coils
suspension, and if the amount of water in the blend capable of reducing its temperature to – 40°C.
exceeds this limit, the fuel will separate into a lower Alternatively, a dry ice-isopropyl alcohol bath may
oxygenate-rich aqueous phase and an upper be used.
oxygenate-lean hydrocarbon phase. The most
important factor governing the ability of a specific B-5 SAMPLING AND HANDLING
fuel to retain water without such separation is its
B-5.1 Draw samples in accordance with IS 1447
temperature. This method is intended to determine
(Part 1), except water displacement shall not be
the maximum temperature at which the fuel will
separate. The temperatures represent the maximum used.
temperatures above which the fuel must not separate
B-5.2 Draw the samples in steel cans that have been
into two distinct phases.
solvent washed.
B-3.2 Note that in this test, actual separation of the
B-5.3 Store the samples in refrigerator (2 to 7°C)
sample into two distinct phases is the criterion for
whenever not actually transferring sample.
failure. The following are indications of phase
separation. B-5.4 Because gasoline-alcohol blends are
hygroscopic as well as volatile, minimize contact
B-3.2.1 The formation of droplets large enough to
with the atmosphere by keeping sample containers
be detected by the unaided eye. They may be either
tightly closed except when transferring sample.
clinging to sides of the container or collect on the
bottom. B-6 PROCEDURE
B-3.2.2 The formation of two layers separated by B-6.1 Warm the sample to 15°C and shake, to re-
either a common boundary, or a layer of emulsion. dissolve any water that may have settled out at the
Formation of haze without one of these indications refrigerator temperature.
of separation is not cause for rejection.
B-6.2 Cool the test container to 10 to 15°C. Carry
out steps B-6.3 through B-6.5 as promptly as
possible to minimize vaporization losses and
absorption of water from the atmosphere.
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IS 17943 : 2022
B-6.3 Rinse out the cooled test container with some sample for no more than 5 s against a light coloured
of the sample to be tested. Drain. illuminated background.
B-6.4 Pour about 40 ml of the sample into the test B-6.8 It is likely that the sample will get hazy prior
container. The precise amount is not critical, but it to actual phase separation as defined in B-3.2.
must be enough to submerge the thermometer bulb Record the sample temperature at the first indication
adequately, without being so much as to require an of haze (when cooling); and the temperature when
excessive amount of cooling time. If the sample has the haze disappears (warming).
separated, as defined in B-3.2, terminate the test.
B-6.9 Record the temperature of phase separation
B-6.5 Seal the test container with the rubber stopper. (see B-3.2). Then allow the sample to warm at
Locate the thermometer bulb approximately at the ambient temperature. Shake the sample vigorously
centre of the fuel sample. after a temperature rise of 2°C, and observe. Record
a ‘warming’ phase recombination temperature, and
B-6.6 Cool the sample by intermittent immersion in the haze disappearance temperature. Average these
or circulation of the coolant. The sample is not to be ‘cooling’ and ‘warming’ temperatures to determine
swirled or shaken while in the cooling bath. Starting the actual phase separation and haze point
at a cooling bath temperature not higher than 10°C temperatures. Repeat this process for improved
or 16°C above the test temperature, cool the sample accuracy.
at a maximum rate of 2°C/min until phase separation
occurs, or the test temperature is reached. B-7 REPORT
B-6.7 At 2°C intervals, remove the test container B-7.1 Report the following information.
from the cooling bath and shake vigorously for 5 to
10 s. Wipe the exterior of the sample container with B-7.1.1 Report the averaged haze point and phase
a towel moistened with isopropyl alcohol to remove separation temperatures found in B-6.9.
any condensation, and observe the condition of the
13
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ANNEX C
BIBLIOGRAPHICAL REFERENCES
ISO 2160 : 1998 Petroleum products — Corrosiveness to copper — Copper strip test
ISO 3405 : 2019 Petroleum and related products from natural or synthetic sources — Determination
of distillation characteristics at atmospheric pressure
ISO 5163 : 2014 Petroleum products — Determination of knock characteristics of motor and aviation
fuels — Motor method
ISO 5164 : 2014 Petroleum products — Determination of knock characteristics of motor fuels —
Research method
ISO 6246 : 2017 Petroleum products — Gum content of fuels — Jet evaporation method
ISO 7536 : 1994 Petroleum products — Determination of oxidation stability of gasoline — Induction
period method
ISO 12185 : 1996 Crude petroleum and petroleum products — Determination of density — Oscillating
U-tube method
ISO 12937 : 2000 Petroleum products — Determination of water — Coulometric Karl Fischer titration
method
ISO 20846 : 2019 Petroleum products — Determination of sulfur content of automotive fuels —
Ultraviolet fluorescence method
ISO 22854 : 2016 Liquid petroleum products — Determination of hydrocarbon types and oxygenates
in automotive-motor gasoline and in ethanol (E85) automotive fuel —
Multidimensional gas chromatography method
ASTM D240-19 Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by
Bomb Calorimeter
ASTM D5291-21 Standard Test Methods for Instrumental Determination of Carbon, Hydrogen, and
Nitrogen in Petroleum Products and Lubricants
EN 228 : 2017 Automotive fuels — Unleaded petrol — Requirements and test methods
EN 237 : 2004 Liquid petroleum products — Petrol — Determination of low lead concentrations by
atomic absorption spectrometry
EN 238 : 1996 Methods of test for petroleum and its products. Liquid petroleum products. Petrol.
Determination of the benzene content by infrared spectrometry
EN 12177 : 1998 Liquid petroleum products — Unleaded petrol — Determination of benzene content
by gas chromatography
EN 13016-1 : 2018 Liquid petroleum products — Vapour pressure — Part 1: Determination of air
saturated vapour pressure (ASVP) and calculated dry vapour pressure equivalent
(DVPE)
EN 15376 : 2014 Automotive fuels — Ethanol as a blending component for petrol — Requirements
and test methods
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ANNEX D
(Foreword)
COMMITTEE COMPOSITION
Petroleum and their Related Products of Synthesis or Biological Origin Sectional Committee, PCD 03
Organization Representative(s)
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Organization Representative(s)
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Organization Representative(s)
Member Secretary
SHRI ARIDAMAN
Scientist ‘B’
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Organization Representative(s)
Centre for Science and Environment, New Delhi MISS ANUMITA ROY CHOWDHURY
SHRI VIVEK CHATOPADYAY (Alternate)
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Organization Representative(s)
Gulf Oil Lubricants India Limited, Mumbai SHRI JENCEN MATHAI ARIVANNOOR
SHRI SANJAY KUMAR (Alternate)
Kaleesuwari Refinery and Industry Private Ltd, SHRI SHYAM SUNDAR SAI NUDURUPATI
Kakinada
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Organization Representative(s)
Ministry of Petroleum and Natural Gas, New Delhi SHRI MANISH SARDA
SHRI RAJESH MANOCHA (Alternate)
Oil and Natural Gas Corporation Limited, New Delhi SHRI AJAY KUMAR JAIN
SHRIMATI LEENA JOHN (Alternate I)
SHRI DINESH S. R. REDDY KAKUTURI (Alternate
II)
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Organization Representative(s)
Organization Representative(s)
Automotive Research Association of India (ARAI), Pune DR THIPSE S. S.
Bureau of Indian Standards, New Delhi SHRI ARIDAMAN
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BIS is a statutory institution established under the Bureau of Indian Standards Act, 2016 to promote harmonious
development of the activities of standardization, marking and quality certification of goods and attending to
connected matters in the country.
Copyright
BIS has the copyright of all its publications. No part of these publications may be reproduced in any form without
the prior permission in writing of BIS. This does not preclude the free use, in the course of implementing the
standard, of necessary details, such as symbols and sizes, type or grade designations. Enquiries relating to
copyright be addressed to the Head (Publication & Sales), BIS.
Amendments are issued to standards as the need arises on the basis of comments. Standards are also reviewed
periodically; a standard along with amendments is reaffirmed when such review indicates that no changes are
needed; if the review indicates that changes are needed, it is taken up for revision. Users of Indian Standards
should ascertain that they are in possession of the latest amendments or edition by referring to the website-
www.bis.gov.in or www.standardsbis.in.
This Indian Standard has been developed from Doc No.: PCD 03 (19448).