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Petroleum Research xxx (xxxx) xxx

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Petroleum Research
journal homepage: http://www.keaipublishing.com/en/journals/
petroleum-research/

Full Length Article

The effect of type waves on vibroseismic implementation of changes


properties of rock, oil viscosity, oil compound composition, and
enhanced oil recovery
Stevy Canny Louhenapessy*, Tutuka Ariadji
Petroleum Engineering, Faculty of Mining and Petroleum Engineering, Bandung Institue of Technology, Indonesia

a r t i c l e i n f o a b s t r a c t

Article history: Based on the results of laboratory studies, the frequency of 35 Hz in longitudinal waves and 20 Hz in
Received 21 February 2020 circular waves is the optimum frequency that can increase the maximum oil recovery. Coreflooding test
Received in revised form results before the vibration effect can increase oil production by 51.96% and reduce the residual oil
15 May 2020
saturation by 59.03%. The surprising results when the vibration effect was applied to the coreflooding
Accepted 18 May 2020
Available online xxx
test method with P wave types continuously succeeded in increasing oil production by 60.54%, inter-
mittent P waves by 63.53% and circular waves by 64.76%, while also reducing Sor by 48.49% in continuous
P waves, intermittent P waves at 44.81% and C waves at 43.3%. The P wave type vibrational method has
Keywords:
Vibroseismic
an increase in oil gain by 16%, intermittently by 22%, Sor reduction by 18% and 24%, in circular wave oil
Longitudinal wave (P) gain increases by 25%, and Sor decreases by 27% from before the vibration effect given. Besides vibration
Circular wave (C) can change the physical properties of rocks, among others; permeability has increased by 7% using P
Enhanced oil recovery waves continuously, intermittently by 31% and C waves by 4%; porosity of 5.88% with P waves contin-
Coreflooding uously, intermittently of 6.46% and circular waves of 4.63%; grain size before vibration of 45.16 mm after
Residual oil saturation (sor) vibration using continuous P waves of 42.01 mm, intermittently of 47.98 mm, and circular of 50.46 mm;
Frequency changes in oil composition to contain more alkanes, and lack of aromatic compounds; oil viscosity
Chemical composition
increased by 3% with continuous P waves, intermittent of 5%, and circular 61%. The new point from this
Viscosity
paper is analyzing the vibroseismic effect by using SEM images in terms of the watershed segmentation
of the Rabbani algorithm compared to lab results, which have an error rate of under 2%, and a review of
oil composition by the GC-MS method.
© 2020 Chinese Petroleum Society. Publishing Services by Elsevier B.V. on behalf of KeAi. This is an open
access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

1. Introduction has been summarized and explained by Barabanov and Pavlov


(2009). The increase in oil carried out by vibration can be done
Viberoseismic is a technology that can be applied to increase oil on the surface or below the surface, with various technologies that
recovery, and some papers say that this vibroseismic research has have developed and combined with the EOR method in general.
long been carried out in laboratory studies and applied to the field. Experimental and theoretical studies of seismic stimulation
Moreover, the success rate obtained by the researchers also from oil reservoirs have begun at the Earth Physics Institute, RAS, in
differed, which reached an increase of 60% (Kouznetsov et al., 1998), the early 1980s. A standard seismic vibrator with a power of up to
and some also reached an increase of 27%e47.6% (Zhu et al., 2005). 20 t and an operating frequency range of 10e40 Hz used as a
The idea of using elastic waves has introduced since the late 1950s seismic oscillation source. Even the first field experiments on oil
(adapted from Paper Cidoncha, 2007), with time the development reservoirs of various types (350e1100 m deep) have brought about
of vibroseismic was increasingly growing, which at the beginning of the positive effect of this stimulation action. The water cut from the
his journey began and observed in the effect of earthquakes, this well decreases with a total indicating an increase in oil recovery.
Other investigators obtained the same results. Despite the first
success, it still has questions about the mechanism of action of
seismic oscillations in the multiphase flow in the oil reservoir.
* Corresponding author. The application of elastic waves from the research stage in the
E-mail addresses: stevycannyl@hotmail.com, stevycannyl@students.itb.ac.id
(S.C. Louhenapessy).
laboratory to the application stage to the field could provide

https://doi.org/10.1016/j.ptlrs.2020.05.001
2096-2495/© 2020 Chinese Petroleum Society. Publishing Services by Elsevier B.V. on behalf of KeAi. This is an open access article under the CC BY-NC-ND license (http://
creativecommons.org/licenses/by-nc-nd/4.0/).

Please cite this article as: Louhenapessy, S.C., Ariadji, T., The effect of type waves on vibroseismic implementation of changes properties of rock,
oil viscosity, oil compound composition, and enhanced oil recovery, Petroleum Research, https://doi.org/10.1016/j.ptlrs.2020.05.001
2 S.C. Louhenapessy, T. Ariadji / Petroleum Research xxx (xxxx) xxx

surprising results with the addition of oil by 40%e50% (Barabanov Stimulation (ISS), Perfection Tool System, Pressure Pulse Technol-
and Pavlov, 2009). ogy (PPT), and The Power Wave Technology. The benefits of
The application of vibration could increase oil recovery by 60% acoustic wave technology can selectively clean wells and increase
(Kouznetsov et al., 1998). This increase obtained when after oil recovery.
waterflooding, which was only able to increase the oil spread by Cidoncha (2007) describes the application of acoustic waves as
32%. Observation of the application of vibration was carried out for reservoir simulation. It can be seen from two aspects, namely lab
51 h with a frequency of 100e200 Hz, on sandstone rocks. Ac- review, and application in the field. In his research, it concluded
cording to Kouznetsov, that seismic waves can be emitted 1e2 Km that so far, the application of vibroacoustic could only be applied to
without significant attenuation. the onshore area, and based on vibrational tests in the field, it
Ridaliani et al. (2003) predict changes in the physical properties recorded frequencies ranging from 20 to 200 Hz. In the Jirnovskiy
of reservoir rocks by laboratory studies of vibration stimulation of field, a vibration with low water saturation carried out against the
field rock samples at various overburden pressures. Where the statement of Bresnev et al. which claims to be applied more than
frequency sets tested were 5 Hz, 10 Hz, 15 Hz, and 25 Hz, with 90% water saturation. After the vibrations, the water cut has
variations in the effects of overburden pressure used 100psig, decreased.
125psig, 150psig, 175psig, and 200psig. In this study, two conditions The increase in oil acquisition that can be applied with one of
tested vertically or horizontally. Ridaliani explained that there was them by in-situ seismic stimulation developed by Applied Seismic
an increase in porosity, permeability, and decreased Sor. Research Corporation (ASR) (Kostrov and Wooden, 2008). This tool
Acoustic waves is successfully used in cleaning well beds of cake is called the ASR Hydro-Impact Tool. This tool produces hydrody-
filters (Van Der Bas et al., 2004). The frequency used in this study is namic shock waves between 2 and 10 million watts. Age in using
20 KHz, with the amplitude maintained at 10e20 mm, which uses this tool is 8e10 months.
equipment that can be derived using wireline or coiled tubing. The Using ultrasonic waves with waterflooding can improve oil re-
researcher also explained that it is instrumental if the acoustic covery (Mohammadian et al., 2011). This research was conducted in
wave treatment done in a burst rather than a continuous manner. a laboratory using sandstone rocks, using two types of ultrasonic
Zhu et al. (2005) describe the downhole harmonic vibration, generators, dynamically used an ultrasonic crest generator
where this tool can increase oil production and also minimize water (reducer) with a frequency of 40 KHz out of 100e500 power, while
cut. This tool is called the downhole harmonic vibration oil - the ultrasonic cleaner used a 40 KHz frequency with 110 W of po-
displacement (DHVOS) developed by CNPC (China National Petro- wer. From the results of this study, when tested using only water-
leum Company), this tool provides waves that produce pressure flooding, the increase in oil reached 64% after the ultrasonic wave
differences along the pore throat thereby reducing the capillary radiation experienced an increase in oil gain by 16%.
effect on rock pore cavities. The frequency used is 88 spm (shocks The effects of ultrasonic waves on controlled and uncontrolled
per minute; each shock has 5 tons of strength). The average cu- temperatures (Hamidi et al., 2013). This experiment uses an ultra-
mulative increase in oil for the field in this study was between 27% sonic generator with a maximum power of 600 W. All three sam-
and 47.6%, and the water cut decreased between 8% and 75%. ples (Paraffin, Synthetic Oil, and Kerosene) will be irradiated with a
Hamida and Babadagli (2005) explain the effect of high fre- wave frequency of 25 kHz and 68 kHz. From the experiments found
quency and intensity of ultrasonic wave radiation on capillary to experience a significant viscosity depreciation. Ultrasonic waves
imbibition. Using an ultrasonic bath with a frequency of 40 KHz and are more effective in light liquid than heavy liquid. It caused by the
an intensity of 2 kW to produce a homogeneous ultrasonic. Almost viscous fluid of ultrasonic wave cavitation, which is difficult to
all experiments experienced an increase in oil recovery when ul- occur due to the presence of a large force. Therefore, viscous liquid
trasonic waves were applied. Except in experiments using water- requires greater amplitude and intensity of the wave.
water and mineral oil - surfactant 14%. In the case of mineral oil - The experiment in improving oil recovery is conducted by using
surfactants, there is no increase in recovery, which means it could ultrasonic waves during waterflooding (Alhomadhi et al., 2014).
be due to very different rheology. Ultrasonic does not affect This experiment observed at high frequencies with a value of
wettability. At low IFT, ultrasonic does not affect the transport 50 KHz power-dense of 300 W. From this study, it found an increase
mechanisms on porous media. Conversely, at high IFT, ultrasonic of 5% from OOIP for horizontal coreflood and 8.1% vertical coreflood,
can reduce IFT as well as capillary pressure. Oil recovery can be while the Sor for both cores increased between 5 and 10%. In this
influenced by wave energy intensity. study, Alhamidi stated that stimulation waves not recommended
Ariadji (2005) explains the changes that occur in the physical for unconsolidated formations with compressive strength below
properties of rocks and fluids when vibroseismic. In the experi- 150 Psi. Whereas for vertically cased hole wells and perforations,
mental study used a variety of frequency variations to see in- seismic waves highly recommended when the permeability de-
dicators of change. From the results of the research, the optimum creases and the depth of the wells increases.
frequency results are 10 Hz and 15 Hz. With this optimum fre- The use of elastic waves applied in the field utilizing in situ
quency, it can reduce the remaining saturation of oil, increase rock combustions can effectively increase oil extraction and reduce
porosity, increase permeability, decrease oil viscosity, and change water cut (Marfin et al., 2015). This method is applied in the
capillary pressure. Research carried out on sandstone rocks. Mardovo-Karmalskoye field, using a downhole oscillator with a
The remaining oil trapped in rock pores as ganglia can overcome frequency variation of 1000 Hze2800 Hz, and the amplitude used
by providing vibrational disturbance Barabanov and Pavlov, 2009. varies between one well with another well with 0.12 MPa, 0.17Mpa,
With a low frequency and with a high amplitude will make the and 0.18Mpa.
mobilization oil develop. In this study, the frequencies tested were Ultrasonic waves combined with surfactant-flooding and
10, 30, and 60 Hz, with wave variations of 0.5, 1.75, 3.5, and 7.5 m/s. waterflooding increase oil recovery (Agi et al., 2019). Using a fre-
Anchliya (2006) explains and reviews the use of acoustic waves quency of 40 kHz with intensities of 150 W, 300 W, and 500 W.
to stimulate wells due to damage to formations around drill holes Using brine with 50,000 ppm NaCl using anionic surfactant Sodium
where this damage usually occurs due to drilling, completion, Dodecyl Sulfate (SDS) with 96% purity and molecular weight
production activities, in general, there is plugging of solid particles. 288.38 g/mol. Experiments use two different concentrations: 1).
A. Anchliya discusses acoustic waves, especially about the equip- 0.1 wt% (under CMC); 2). 1 wt% (above CMC). Waterflooding,
ment used in seismic stimulation. Among them are In-Situ Seismic combined with ultrasonic radiation, gets an increase of 11% OOIP.

Please cite this article as: Louhenapessy, S.C., Ariadji, T., The effect of type waves on vibroseismic implementation of changes properties of rock,
oil viscosity, oil compound composition, and enhanced oil recovery, Petroleum Research, https://doi.org/10.1016/j.ptlrs.2020.05.001
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Surfactant-flooding. The combination of ultrasonic and surfactant- carries out with a frequency variation of 35e50 Hz for longitudinal
flood gets a recovery increase of 12%. Recovery increases higher as waves and 10e25 Hz for circular waves, and the third scenario
wave intensity and concentration added. optimizes the results of increasing oil with time variations on the
The purpose of this laboratory study is to determine the appli- longitudinal waves.
cation and implementation of efforts to optimally increase oil
production using longitudinal and circular wave types by changing 2.4. Core and fluid sample testing
parameters of rock physical properties, fluid viscosity, oil compo-
sition, decreasing oil saturation, and increasing oil recovery. Core and fluid sample testing is carried out before and after the
pressing testing process. It is done to determine the process of
2. Method change that occurs in the core and oil samples. The parameters
measured in the core sample are: dry weight, wet weight, porosity,
This study conducted to find the optimum frequency of vibro- permeability, oil viscosity, and oil composition. Core cleaning using
seismic with longitudinal and circular wave types. Longitudinal the distillation method uses soxhlet extraction equipment; the
wave frequency ranges between 35 and 50 Hz and circular waves solvent used as a core cleaner is toluene. The toluene can clean up
between 10 and 25 Hz, which can increase the value of porosity, the remaining oil and brine in the core sample. This cleaning is
absolute permeability, and residual oil saturation (Sor) to the carried out at a temperature of 65  C. After cleaning the core
maximum. Also, this study wants to see changes in the physical samples, proceed to the drying stage using an oven, is proceeded at
properties of fluids between other viscosities, and the effect of vi- a temperature of 60  C for 48 h. Measurement of permeability,
brations on the results of components seen from the results of gas porosity using PORG-200, and PERG-200 equipment are made by
chromatography. corelab, for SEM analysis using, tools with the Jeol brand with type
JSM IT-300LA are used.Whereas for fluid samples, the viscosity and
2.1. Research data oil composition are measured. Oil viscosity is measured using
Brookfield viscosimeter equipment at a temperature of 60  C, with
This study is conducted using crude oil samples from the field a measurement speed of 40e90 rpm. The oil composition is
and using berea cores, where the cores used in vibroseismic testing measured Gas Chromatography (GC) using GC-MS QP-2010 Ultra,
are focused only on the permeability of 200e265mD, and porosity using Rtx-5MS type column gas, with a column length of 30 m,
between 20-23%. Cleveland Quarries, sandstone cores are used. The thickness of 0.25 mm, and column diameter of 0.25 mm. The testing
fluid tested has a density of 450API. The brine used was 9,993 ppm, of oil composition is carried out at an injection temperature of
with viscosity and of 0.51cp and density of 1,098g/cc. 270  C, oven temperature of 80  C column, with the pressure of
87.2 kPa. The gas used in testing uses Helium gas. Whereas Mass
2.2. Research flow Spectrometry (MS) temperature measurements is carried out using
ion temperatures of 230  C, interface temperatures of 280  C.
Research on vibroseismic to enhanced oil recovery has been
widely carried out by previous researchers, and in general, seismic
2.5. Core sample analysis
waves used by researchers, which have two wave effects namely
longitudinal waves (P) and transverse waves (S) or even both waves
This study uses two methods in analyzing core samples. The first
P and SV waves, are called Rayleigh waves. Based on previous
method uses laboratory equipment, and the second method uses
research, this study is to compare the use of longitudinal waves and
SEM results. The parameters compared by the two methods are
circular waves (Rayleigh) utilizing vibration. In addition to using
porosity and permeability. Measurement of porosity and perme-
variations of the two waves, frequency variations are also carried
ability values from SEM results are done using a watershed seg-
out to obtain optimum results in changing rock structure, changing
mentation algorithm which the algorithm is developed by Arash
fluid viscosity, and affecting the composition of petroleum in terms
Rabani (Rabbani et al., 2014; Rabbani and Ayatollahi, 2015; Rabbani
of gas chromatography results. Besides that, an increase in oil
and Salehi, 2017). The algorithm developed by Rabani is only able to
production is maximized by using intermittent longitudinal waves.
produce porosity values and grain size, whereas to find out the
permeability value calculated using the Carman & Kozeny equation,
2.3. Coreflooding
it can see in Equation (1a) and Equation (1b) Al-bazzaz (2007).

Coreflooding test uses a modified Hassler Permeameter with a


d2 : 43
vibration unit by the scheme designed in Fig. 1a and Fig. 1b as a k ¼ 3:631: 109 : (1a)
support for the needs of vibroseismic testing with longitudinal and ð1  4Þ2
circular wave types utilizing vibration. Berea sandstone core sam-
Where: k ¼ permeability,mD; d ¼ grain size, inch; 4 ¼ porosity,
ples are inserted into the core holders that are met by the oil phase
fraction
using the vacuum method and given an overburden pressure of
100psig. The brine used as an oil pressing process, the brine from a
field sample. During the coreflooding process vibration, effects are
d2 : 43
k ¼ 5:6281 : (1b)
given simultaneously with the frequency variations that have ð1  4Þ2
determined in this study, and fluid will be produced to the point
where only the brine produces. It is assumed that the cores filled Where: k ¼ permeability,mD; d ¼ grain size, mm; 4 ¼ porosity,
with oil are fulfilled by brines. The oil that does not come out again fraction.
due to pressure by brine can be said to be residual oil saturation,
while the amount of oil volume found due to vibrations while doing 2.6. Analysis of fluid samples
coreflooding can be said to be RF (recovery factor). In this study,
three scenarios are conducted. The first scenario carries out core- This study analyzes the oil viscosity that occurs due to the ef-
flooding testing without vibroseismic influence, the second sce- fects of longitudinal and circular waves with the implementation of
nario coreflooding testing given a vibration effect simultaneously, vibrations. The value of viscosity observed in this study is carried

Please cite this article as: Louhenapessy, S.C., Ariadji, T., The effect of type waves on vibroseismic implementation of changes properties of rock,
oil viscosity, oil compound composition, and enhanced oil recovery, Petroleum Research, https://doi.org/10.1016/j.ptlrs.2020.05.001
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Fig. 1a. Vibroseismic testing tool scheme in the laboratory for longitudinal waves.

Fig. 1b. Vibroseismic testing tool scheme in the laboratory for circular waves.

out for changes in frequency and compared the changes with the 3. Result & discussion
two types of waves tested. In addition to viscosity, observations
made of changes in the chemical composition of the crude oil are The yield of oil before vibration is 51.96%, Sor is 48.04%. The re-
tested through the results of gas chromatography. The results of gas sults of the oil treatment after vibration with the longitudinal wave
chromatography analysis are based on changes due to vibrational continue by 60.54% and decrease Sor by 39.46 Fig. 2a and b, while in
effects on groups of compounds found in hydrocarbons. The the intermittent longitudinal wave, the results of the oil acquisition
analyzed compounds include alkanes, cycloalkanes, aromatics, and is 63.53% and Sor 36.47% Fig. 3. Oil acquisition by the effects of
polar compounds. circular wave-type vibrations at frequencies is increased by 64.76%

Please cite this article as: Louhenapessy, S.C., Ariadji, T., The effect of type waves on vibroseismic implementation of changes properties of rock,
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Fig. 2a. Comparison of the results of enhanced oil recovery on the effects of frequency on longitudinal and circular waves.

Fig. 2b. Comparison of the results of the reduction in residual oil saturation on the effects of frequency on longitudinal waves and circular waves.

and decreases Sor by 35.34% Fig. 2a and b. The optimum frequency turned on varies from 2, 4, 6, 8, and 10 min. The sweeps effect is
that can increase oil recovery is 20 Hz for circular waves and 35 Hz suitable if applied when the vibration position is turned on for 8 min
for longitudinal waves. The vibrational effect on the core can in- and extinguished for 5 min. Fig. 4 shows the comparison of the results
crease the acquisition of oil that was previously still attached to the of the increase in oil gain and Sor decrease with the three scenarios.
rock, and this justifies the opinion of Nikolaevskiy et al. (1996), The vibration effect with longitudinal wave continue can in-
which states the vibrational effect gives rise to droplets of oil which crease porosity by 6% and permeability by 7%, while intermittent
fuse and flow as liquid fines, which simultaneously pressed by longitudinal waves increase porosity by 6% and permeability by
brine to produce. 31%. Circular waves can increase porosity by 5% and permeability by
An intermittent longitudinal wave is an effort to increase oil 41%. SEM results can be seen in Fig. 5a, Fig. 5b, and Fig. 5c. A
acquisition with time variation. The time variation is assumed based comparison of SEM and lab digitization results can be seen in
on the effect of the sweep of the seismic truck. The intended sweep Table 1.
effect is an intermittent vibration process with a specified time in- The oil viscosity increased after the vibration results for circular
terval. Usually, when the vibration is turned on for only a few seconds, wave vibrations of 2.04cp, the longitudinal continue, and inter-
while the vibration when it stops depends on the desired time. Based mittent waves of 1.46cp and 1.47cp Fig. 6.
on the sweep effect process, a sufficient time search is conducted in Circular waves are still better at increasing oil recovery and
the process of increasing oil recovery. The assumed time when the decreasing saturation of residual oil than longitudinal waves; this is
engine turns off for 5 min, and the period of the vibration engine evidenced by the results of the acquisition of tests and observations

Please cite this article as: Louhenapessy, S.C., Ariadji, T., The effect of type waves on vibroseismic implementation of changes properties of rock,
oil viscosity, oil compound composition, and enhanced oil recovery, Petroleum Research, https://doi.org/10.1016/j.ptlrs.2020.05.001
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Fig. 3. comparison of residual oil saturation results and enhanced oil recovery in continue longitudinal waves and intermittent longitudinal waves (time variation).

Fig. 4. comparison of enhanced oil recovery and decreased residual oil saturation after vibration.

made in the study. Besides this research, it can also be linked to flow moves turbulently in mobilizing oil droplets in the porous
literature review on waves as is described (Novotny, 1999) in his walls of rocks. It is what makes pressing oil with the help of circular
book about the understanding of longitudinal waves that propagate wave-type vibrations more effective in increasing oil gain and
parallel to the direction of propagation or opposite direction in the decreasing oil saturation.
direction of its propagation. Rayleigh is a wave that occurs due to The results of gas chromatography tests on longitudinal waves
the influence of 2 waves, namely the P wave and SV wave. The SV have a little more alkane than between circular waves and before
wave itself is part of a transverse wave or better known as a shear vibrations. The difference in alkane compounds after vibration and
wave whose direction of propagation moves perpendicularly but in before vibration has a difference of 12%, while the circular waves
a vertical plane. have a smaller yield of 10%. Whereas for cycloalkanes or called
The statement (Barabanov and Pavlov, 2009), describes the cir- naphthene compounds have a difference that is not too far between
cular wave radiation that can form vortex flow, in which the vortex before and after vibration, the longitudinal waves have a difference

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oil viscosity, oil compound composition, and enhanced oil recovery, Petroleum Research, https://doi.org/10.1016/j.ptlrs.2020.05.001
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Fig. 5a. SEM results a). Base case scenario; b). Scenarios after P wave vibrations; c). Scenarios after intermittent P wave vibrations; and d). The scenario after the vibrations of the C
wave. (this image was zoom 2000X).

Fig. 5b. Porosity analysis results a). Base case scenario; b). Scenarios after P wave vibrations; c). Scenarios after intermittent P wave vibrations; and d). The scenario after the
vibrations of the C wave. (this image was zoom 2000X).

of 3%. This result decreases compared to the results before vibra- Observation of the distribution of n-alkane carbon compounds,
tion, while the circular waves by 4%. Aromatic compounds have which compares between before and after vibrations. The distri-
decreased, the ratio of the results of the decrease experienced after bution of the n-alkanes carbon atom value is similar for the three
vibrations by using circular wave types by 5%, and for longitudinal test results before and after the vibration by both types of waves. It
wave types by 7%. Moreover, the last polar compound also sees using the same oil sample Fig. 8. The difference can be seen
decreased by 2% from before and after vibration with the type of when viewed from the carbon atom values of C6 to C16 where the
longitudinal wave, while 1% by using circular waves. The main results of prior vibrations of the oil with the composition of the C6-
difference that occurs during the process before and after the vi- C16 atoms are 22%, whereas after vibrations the results obtained
bration made is that the oil after vibration increases oil recovery increase by 7%e29% for circular wave types and longitudinal waves
and changes to the composition of the oil by having a little more increased by 5%e27%. The results show from C6 to C16 are different
composition of alkane compounds and less composition of aro- from before vibrations where changes in the composition of oil are
matic compounds Fig. 7. not much, but this is reversed when viewed from the solid phase

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Fig. 5c. Grain size analysis results a). Base case scenario; b). Scenarios after P wave vibrations; c). Scenarios after intermittent P wave vibrations; and D). The scenario after the
vibrations of the C wave. (this image was zoom 2000X).

Table 1
Results of SEM analysis validation of the laboratory results.

Test Item Laboratorium Result SEM Result Error (%)

f, % k, mD f, % Grain Size, mm k, mD f k

Base Case 20.74 164 20.84 45.1623 166 0.46 0.99


Continue Longitudinal Wave 21.96 176 22.14 42.011 178 0.80 0.93
Intermittent Longitudinal Wave 22.08 215 21.78 47.9801 219 1.34 1.83
Circular Wave 21.70 232 21.63 50.4505 236 0.32 1.74

Fig. 6. The results of viscosity to the research scenario (comparison of the results of the viscosity of circular waves, continuous longitudinal waves, intermittent longitudinal waves,
and coreflooding without vibrational effects).

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Fig. 7. comparison of the results of changes in the composition of compounds after vibration.

Fig. 8. Distribution of carbon number #C atoms before and after the vibro effect.

with carbon atom chains between C18-C36, which shows the in- results of gas chromatographic tests prove the existence of changes in
crease in solid due to the effect of vibrational effects. The increase chemical composition due to the effect of vibration. Changes can be
occurs in C18-C36 by 18% in circular waves and 22% by using lon- seen in an increase in the composition of alkane compounds and a
gitudinal waves. These results are compared with the results before decrease in the composition of aromatic compounds.
the vibration, which only produced a value of 13%. The distribution In which alkane compounds have a lighter density compared to
of #C atoms can be seen in Table 2. aromatic and polar groups of compounds. Polar compounds also
The results of gas chromatography testing, if associated with vis- decrease with the effect of vibration. Polar compounds themselves
cosity, are complicated; the possibility is to determine and declare this consist of a resin or asphaltene fraction, or both (Schobert, 2013).
oil classified as viscous or not. However, according to Schobert, 2013, However, for this study, the polar compound contained in this oil
the number of carbon values or long chains of carbon or the incor- sample is resin. This reason is that the asphalt in compound forms
poration of nitrogen or oxygen atoms can increase the density of oil when the molecular weight contained is between 500 and 2000gr/
relative to hydrocarbons of the same molecular weight. Overall the mol (adapted from Aske, 2002).

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Table 2
Results of comparison of the distribution of #C atoms before and after vibration.

Compound n-Alkanes #C Area% Atmosphere


Condition
Before Vibration After Vibration

Circular Wave Longitudinal Wave

n-Hexane 6 2.07 0.30 0.57 liquid


n-Octane 8 1.40 0 0 liquid
n-Decane 10 3.25 2.38 2.19 liquid
n-Undecane 11 2.51 2.92 2.54 liquid
n-Dodecane 12 3.04 3.34 3.26 liquid
n-Tetradecane 14 5.15 7.62 7.99 liquid
n-Pentadecane 15 0 3.80 0.00 liquid
n-Hexadecane 16 4.56 8.97 10.61 liquid
n-Octadecane 18 0.62 0.76 0.68 Solid
n-Nonadecane 19 0.35 2.51 0.51 Solid
n-Eicosane 20 3.55 2.26 8.01 Solid
n-Pentacosane 25 1.47 9.51 1.99 Solid
n-Hexacosane 26 2.50 0.95 6.99 Solid
n-Dotriacontane 32 4.34 1.80 4.04 Solid
n-Hexatriacontane 36 0.22 0.23 0 Solid

Visible with the effect of fluid vibrations experiencing viscous, Acknowledgments


this happens because there is a possibility of a turbulent flow effect
when the fluid flows when testing coreflooding while mechanical We want to thank the researchers who provided input and di-
vibration effects are given, in which the vibration factor itself ex- rection related to the research and writing of this thesis; Barabanov
periences kinetic energy during the vibration process. Kinetic en- as a Russian vibroseismic researcher, Arash Rabbani University of
ergy can make the oil viscosity lighter, but it is also able to make the Manchester researcher, Huang Zeng BP Chemist, Diana Chirkova
oil viscous because of the turbulence effect or known in Barabanov University of Manitoba researcher, Prof. Yana Maolana Syah, M.S.,
research with the term vortex flow. This turbulence effect causes Ph.D. as ITB chemistry lecturer, and LPDP scholarships.
pressure to decrease so that gas trapped in the oil out. It is proven
by the formation of a solid fraction in gas chromatography testing, References
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oil viscosity, oil compound composition, and enhanced oil recovery, Petroleum Research, https://doi.org/10.1016/j.ptlrs.2020.05.001

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