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Aggregate Segregation 3
Aggregate Segregation 3
Abstract: In this study, properties of warm mix asphalt (WMA) compacted with various levels of gradation segregation were evaluated in the
laboratory. Six segregated gradations were designed to compare with the control gradation and test sections were paved with the control
gradation. Then pavement quality indicator (PQI) and field coring were used to evaluate the uniformity of the WMA test sections with the
statistical method. In addition, sieve analysis of the cores was conducted to evaluate the level of segregation. The test results show that
gradation segregation has a remarkable effect on water stability, high-temperature stability, low-temperature cracking, and tensile strength
of WMA mixtures. Statistical analysis results show that the levels of segregation in localized areas are quite typical because the air void
contents follow a normal distribution and the mixtures along the central line are denser than other areas. Sieve analyses of the cores show that
most places of the typical segregated localized areas in the test sections have no segregation or low-level segregation, so the construction
quality is good. It also shows that the air void content increases as the gradation gets coarser, which is consistent with laboratory test results.
DOI: 10.1061/(ASCE)MT.1943-5533.0002208. © 2018 American Society of Civil Engineers.
Author keywords: Warm mix asphalt; Gradation segregation; Property; Pavement quality indicator.
Sasobit, a product of Sasol Wax (Free State, South Africa), is white S¼ ðPij − Paj Þ2 ð1Þ
i¼1
granules that have longer chemical chains. The longer chains, keep-
ing the wax in solution, decrease the viscosity of the asphalt and
compaction temperature of the WMA mixture. The melting temper- where n = different sieve size levels; and Pij and Paj = passing
ature of Sasobit used in this study is 115°C. In view of past studies, percentages of the segregated gradation and the control, respec-
the optimum additive content was 3% of the binder mass (Li et al. tively. The level of segregation can be divided into four levels:
2016). The basic properties of Sasobit are shown in Table 1. no segregation, and low-level, medium-level, and high-level segre-
gation. The corresponding limits of S values were less than 10%,
10–20%, 20–35%, and greater than 35% (Li and Ma 2007), respec-
Asphalt
tively. Seven different segregated gradations, as shown in Fig. 1,
The base styrene-butadiene-styrene (SBS)–modified asphalt that was were designed in this study: high-level segregation of coarse aggre-
used was provided by a company in Guangxi Guochuang Road gate (HC), medium-level segregation of coarse aggregate (MC),
Material limited company (Nanning, Guangxi Province, China). low-level segregation of coarse aggregate (LC), control, high-level
The needle penetration test, ductility test, softening point test, and segregation of fine aggregate (HF), medium-level segregation of
other tests were conducted to detect the basic performance of the fine aggregate (MF), and low-level segregation of fine aggregate
asphalt in accordance with the standard test methods used in China (LF). The related S values are 43.5, 28.3, 15.0, 0, 39.0, 23.3,
[JTG E20-2011 (Ministry of Transport of China 2011)]. Related test and 10.3%, respectively.
results are shown in Table 2. They are all in the range of the speci-
fication limits, which means that the asphalt is acceptable. Optimum Asphalt Content
The optimum asphalt binder content of the mixture was 4.2%,
which was selected based on the results of the air void content,
Aggregates
density, stability, and flow of Marshall samples using the Marshall
Coarse aggregates, fine aggregates, and filler used in this study mix design methodology in accordance with JTG F40-2004
were all limestone from Jingxi Aggregate Limited Company (Ministry of Transport of China 2004). The physical indexes of
(Jingxi, China). The water absorption and different densities of ag- control AC-20 are presented in Table 4. The asphalt content of
gregates are shown in Table 3. other segregated AC-20 mixtures was calculated by the principle
90 HC
MC
80 LC
Control
40
30
20
10
0
0
0. 5
15
18
36
75
.2
16
19
.5
0.
0.
9.
07
13
26
1.
2.
4.
0.
Table 4. Physical Indexes of Design Asphalt Mixture AC-20 Gradation Segregation in the Field
Index Value Specification limits Test sections were paved in a tunnel of the Jingxi-Napo segment on
Asphalt content (%) 4.2 — one of the Guangxi expressways in South China. Twenty-nine typ-
Theoretical maximum specific 2.542 — ical segregated localized areas in the field were evaluated with PQI
gravity (g=cm3 ) and field coring by the statistical method. Sieve analyses of the
Bulk specific gravity (g=cm3 ) 2.454 — burned core samples were also carried out.
Air void content (%) 3.5 3–6
Voids filled with asphalt (VFA) (%) 72.0 65–75
Voids in mineral aggregate (VMA) (%) 12.52 ≥12.5
Results
Stability (kN) 16.13 ≥8.0
Flow (mm) 3.6 1.5–4
Water Stability
Moisture susceptibility is one of the major forms of premature
of equal thickness of the asphalt membrane; the results are shown failure in asphalt pavements. Therefore, the tensile strength ratio
in Table 5. (TSR) using the freeze-thaw split tensile test was measured. The
volumetric properties and the TSR of samples are presented in
Table 6.
Effect of Gradation Segregation on Mix Properties In Table 6, the mixes with upper (finer) gradation display better
Six segregated gradations, AC-20, were designed to compare to the water stability than the lower (coarser) gradation. The TSRs of HC
control gradation. Water stability, high-temperature stability, low- and MC are 65.5 and 71.6%, respectively, while the specification
temperature cracking, and indirect tensile strength (ITS) of these limit is 75%. As a result, they are both out of the range of JTG
seven gradations were tested in this study according to the standard F40-2004 (Ministry of Transport of China 2004). However, TSRs
test methods of asphalt mixtures used in China [JTG E20-2011 increase as the gradation gets finer: the TSRs of LF, MF, and HF are
(Code of China 2011)]. 93.4, 95.1, and 95.9%, respectively. It also can be seen from
Tables 5 and 6 that the air void content increases but asphalt content
decreases as the gradation gets coarser. The adhesive bond strength
between the aggregate and asphalt decreases at the same time.
Table 5. Specific Surface Areas and Optimum Asphalt Content of Various
Therefore, coarser aggregate segregation is prone to moisture dam-
Asphalt Mixtures
age due to a high air void content and low asphalt content.
Gradation Specific surface area (g=cm3 ) Asphalt content (%)
HC 1.57 1.6
High-Temperature Stability
MC 2.44 2.5
LC 3.21 3.3 The rutting tests at 60°C were performed to detect the high-
Control 4.03 4.2 temperature stability, or rutting resistance, of the mixtures; the re-
LF 4.58 4.8 sults of dynamic stability are shown in Fig. 2.
MF 5.39 5.7 As can be observed from Fig. 3, the differences between HF and
HF 6.28 6.7
HC are very obvious. The gradation segregation has a significant
6000
5223.4 MC 4.01 1,980 2,025
5000 LC 7.94 3,210 2,474
4321.5
Control 9.88 3,767 2,622
4000 LF 11.79 4,632 2,545
MF 12.84 5,320 2,414
3000
2404.6 HF 12.53 6,120 2,047
2000
1000 778.7
778.7
2.5
0
HC MC LC Control LF MF HF 2.02
2
Fig. 2. Dynamic stability of various gradations 1.81
1.66 1.66
1.5 1.35
ITS (MPa)
1.14
1 0.86
0.5
0
HC MC LC Control LF MF HF
Low-Temperature Cracking
Fig. 3. Gradation segregation: (a) HF; (b) HC Low-temperature cracking is a common problem in asphalt pave-
ment both in cold and hot areas. This kind of cracking can be ini-
tiated by low temperatures alone or by multiple cycles of warming
and cooling. The low-temperature cracking performance of the
effect on the dynamic stability, especially for finer aggregate mixtures were evaluated by the low-temperature bending tests;
segregation, as shown in Fig. 2. The dynamic stabilities of fine- the results are shown in Table 7. The effect of gradation segregation
aggregate segregation are lower than that of the control. The dy- on the low-temperature cracking is obvious. Flexural strength or
namic stability decreases as the gradation gets finer. The dynamic strain of finer gradation is higher than that of coarser gradation,
stability of HF is 778.7 cycles=mm, which is far less than the as shown in Table 7. This indicates that mixes with finer gradation
specification limits. This means fine-aggregate segregation is ad- perform better in terms of low-temperature cracking resistance than
versely affected by the high-temperature stability and is more sus- the coarser gradation.
ceptible to rutting. However, the dynamic stabilities of MC and LC
are both greater than that of the control because the stone-skeleton
structures of MC and LC are enhanced significantly with coarser Indirect Tensile Strength
aggregates. But the dynamic stability of HC decreases suddenly Splitting tests were performed according to standards for ITS. The
because the asphalt content decreases with the increase in ITS values of mixtures are shown in Fig. 4. From Fig. 4, ITS values
coarse-aggregate content, which would result in a decrease in change obviously with the gradation. That is, low-temperature
the adhesive bond strength. The mixture would be very difficult cracking is affected significantly by gradation segregation. The
to compact. maximum ITS value is the ITS value of the control gradation.
void content and low asphalt content. The wheel tracking tests The Q-Q plot is a graphical technique used to assess if a set of
present that fine-aggregate segregation is adversely affected by data plausibly came from a normal or exponential distribution
the high-temperature stability and is more susceptible to rutting. As- (Peng 2004). In this study, the PQI_AV, shown in Table 8, was an-
phalt content with coarse-aggregate segregation is decreased, result- alyzed by a Q-Q plot, as presented in Fig. 5.
ing in a decrease of the adhesive bond strength, causing the coarser From Fig. 5, it can be seen that PQI_AV is almost on the diago-
mixture to be very difficult to compact. The mixes with finer nal, indicating that PQI_AV follows a normal distribution. Addi-
gradation show better resistance to low-temperature cracking than
tionally, these segregated localized areas are obviously observed
the coarser gradation. However, the indirect tensile strength tests in-
to be different. Air void contents at 14 locations are 3–6%, which
dicate that asphalt pavement with control gradation is the best.
is in the range of the Chinese specification [JTG F40-2004 (Code of
Therefore, the test sections were paved with the control gradation.
China 2004)]. Air void contents at three locations are less than 3%.
Air void contents at 12 locations are more than 6%. As a result, the
Field Test levels of segregation in these localized areas are quite typical.
20
15
S (%)
10
5
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0
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29
Core ID
Fig. 5. Q-Q plot of PQI_AV
Fig. 7. Segregation level of field cores (data from Xiong 2015)
80
70
i Percentage
60
t
L3, Location R3, Location L2, Location R2, and Location L1. CTL Core1 Core4 Core10 Core23 Core27
Therefore, PQI_AV becomes smaller as the detection location gets
Fig. 9. Sieve analysis of the high air void content samples
closer to the central line. This means the mixtures along the central
line are denser than the other places.
• The rutting tests indicate that fine-aggregate segregation is ad- Cross, S. A., and Brown, E. (1993). “Effect of segregation on performance
versely affected by the high-temperature stability and is more of hot-mix asphalt.” Transp. Res. Rec., 1417, 117–126.
susceptible to rutting. Asphalt content with coarse-aggregate de León Izeppi, E. (2006). “Non-contact methods for detecting hot-mix
asphalt nonuniformity.” Ph.D. dissertation, Virginia Polytechnic
segregation is decreased, which would result in a decrease in
Institute and State Univ., Blacksburg, VA.
the adhesive bond strength. Li, L., and Ma, X. (2007). “Influence research of gradation segregation on
• The mixes with finer gradation show better resistance in low- performance of asphalt mixture.” J. Tongji Univ., 35(12), 1622–1626.
temperature cracking than the coarser gradation. However, Li, X., Zhou, Z., and You, Z. (2016). “Compaction temperatures of Sasobit
the indirect tensile strength tests indicate that asphalt pavement produced warm mix asphalt mixtures modified with SBS.” Constr.
with control gradation is the best. Build. Mater., 123, 357–364.
• Statistical analyses show that the level of segregation in loca- Lu, Q., Kohler, E., Harvey, J., and Ongel, A. (2009). “Investigation of noise
lized field detection areas is quite typical because the air void and durability performance trends for asphaltic pavement surface types:
content follows a normal distribution. The mixtures along the Three-year results.” Research Rep. UCPRC-RR-2009-01, Univ. of
central line are denser than the other places. California, Davis, CA.
Ministry of Transport of China. (2004). “Technical specification for con-
• Sieve analyses show that most places of the 29 typical
struction of highway asphalt pavements.” JTG F40-2004, Beijing (in
segregated localized areas in the test sections have no segrega- Chinese).
tion or low-level segregation, so the construction quality is Ministry of Transport of China. (2011). “Standard test methods of bitumen
good. and bituminous mixtures for highway engineering.” JTG E20-2011,
• Sieve analysis results of the cores are consistent with laboratory Beijing (in Chinese).
test results. That is, the cores with a low air void content have a Peng, G. (2004). “Testing normality of data using SAS.” Paper PO04,
greater passing percentage of aggregates compared with control Eli Lilly and Company, Indianapolis.
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tion, and vice versa. ating asphalt mixture homogeneity.” J. Test. Eval., 39(3), 327–334.
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Acknowledgments Sun, Z., Cheng, H., Zhu, G., and Ma, J. (2017). “Low temperature perfor-
mance prediction model of GAC-20 modified asphalt mixture.” Proc.,
This work was supported by the National Natural Science IOP Conf. Series: Materials Science and Engineering, IOP Publishing,
Foundation of China (Grant No. 51308075), Department of Bristol, U.K.
Transport of Hainan Province (Number JT20160898009), Foun- Tang, X., Wang, S.-L., and Dai, J.-L. (2010). “Evaluated model and stan-
dation of Hunan Educational Committee (Number 15C0044), dard of segregation for asphalt mixture.” Jiaotong Yunshu Gongcheng
and Open Fund of State Engineering Laboratory of High- Xuebao, 10(2), 1–5.
Williams, R., Duncan, G., Jr., and White, T. (1996). “Hot-mix asphalt seg-
way Maintenance Technology (Changsha University of Science
regation: Measurement and effects.” Transp. Res. Rec., 1543, 97–105.
and Technology) (Grant Nos. kfj160101 and kfj140104). The Xiong, K. (2015). “The long tunnel warm mix flame-retardant warm mix
financial support to Siyu Chen from the China Scholarship asphalt pavement construction variability analysis and quality control.”
Council and Michigan Technological University is also gratefully Master’s dissertation, Changsha Univ. of Science and Technology,
appreciated. Changsha, China (in Chinese).