UDC 622.348: 543.

71

M 8109

Garnierite Nickel

Method of deciding sampling, sample

preparation, and moisture

JIS M 8 1 09-1996
(2005 confirmations)

Revision on May 1, 1996

Japan Industrial
1
(Japanese Standards Association issue)
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by the Copyright Law.
M 8109-1996

5 and main 'Tsutomu large: Trade industry Minister enactment: 1965. 9 and 1 revision: 1996. 1
Notice through official gazettes: 1996. 5.1
Original bill making cooperator: Japan Mining Industry Association
Discussion departmental meeting: Japan Industrial Standards Committee resource energy departmental meeting(departmental
meeting Chouuehara former Hajime)
The opinion or the question on this standard is reported to the Agency of Industrial Science and Technology standard material fee
standard section (-100-Tokyo Chiyoda Ward remark is 1 chome 3-I in the barrier).
Please do.
Japan Industrial Standards Japanese industry and the standard will be investigated by providing for Article 15 of the industrial
standardization method by the day that passes at least five years.
It is fixed to the discussion on the meeting, and it reams, the crab, it confirms, it revises or it is abolished.

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 Japan Industrial Standards JIS

M 8109-1996

Garnierite nickel ores-Methods for sampling, sample

preparation and determination of moisture content

1.The coverage standard is flat of the element and moisture of the lot of the Garnierite nickel ores (Hereafter, it is called
ore).

It provides for the following method to decide Narane (Hereafter, it is said the average fineness).
(1)Method of gathering sample
(2)Method of making moisture examination sample and element examination sample
(3)Method of measuring moisture
(4)Method of deciding moisture and dry measure

Remarks 1. As a rule, this standard conforms to JIS M 8100.

2. Next, the normative reference for this standard is shown.

General rules of method of JIS M 8100 Cocatamari compound-sampling
Method of measuring nickel in JIS M 8126 ore
How to round JIS Z 8401 numerical value
It is old for the JIS Z 8801 examination.

2.Next, the definition of the main term that the term defines and likes and uses by the standard depends.
(1)Ore of mass decided among persons concerned to decide lot average fineness. It is Rotsu as for the
mass of ore that composes one lot.
It is said the size of To.
(2)The sublot lot is divided and the ore of the mass. The mass of ore that composes the sublot with the
size of the sublot
It says.
(3)The ore of the amount of the unit gathered as a rule by one operation from the increment lot or the
sublot according to the sample collection machine.
Bow
Moreover, it is ore of the amount of the unit gathered from the sample in the method of subdividing the
increment.
The mass of one increment is called the size of the increment.
(4)Sample that collected increments several partial samples. After increment is individually made, if
necessary
There is a partial sample collected samples of several, too.
(5)From fall Ro on the belt conveyer when the belt sampling lot is carried by the belt conveyer etc.
Method of gathering increment.
(6)Incrime from track or wagon when track sampling lot is track or is handed over by goods
Method of gathering Nt.
(7)When Grot is handed over with Fnets in the hold San pudding, it is an increment in the loading from
among the hold or the loading tools.
Method of gathering.
(8)Generic name of sample gathered for sample element analysis for element. The sample for the element
is made, and the one supplied to the analysis is element examination Tame.
It is called Ryou.

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M 8109-1996

(9)Generic name of sample gathered for sample moisture measurement for moisture. The sample for
moisture is made, and the one supplied to the measurement of moisture content is moisture Tame.
It is called an effect sample.
(10)Divide the sample of using combinedly of the sample, use one side for the water determination, and use
the other side for the componential analysis on the element examination sample.
(11)Use the whole quantity or a part of the sample used to measure the moisture of promoting an important
position of the sample for the componential analysis on the element examination sample.
(12)Minimum spirited is ox-eyed, that the maximum grain degree sample old and residual rate become less
than 5%.
As a rule, spirited in this standard depends on regulations of JIS Z 8801.

3.Next, the sign used for the sign standard depends.

y:Size of lot
Number of increments gathered from μ:1 lot
Cy: The one that accuracy was shown by standard deviation
Ton:The one that the difference between layers was shown by standard deviation
:The one that the difference between increments in layer was shown by standard deviation
..drinking..:The one that accuracy of the sampling was shown by standard deviation
..summons..:The one that making accuracy was shown by standard deviation
-: ..(.. the one that accuracy including making, analysis or measurement was shown by signpost
preparation difference
g: The one that accuracy (integrated accuracy) including sampling, making, analysis or
measurement was shown by standard deviation

4. General matter
4.1The outline of sampling the outline of sampling and the sample preparation and the sample preparation is
Figure 1 joining ..(.. Ltd. that depends next.
(I)The lot is decided. The number of sublots is decided in proportion to the size of the lot.
(2)It sizes about the increment and of the collection method and the increment according to the maximum
grain degree of the lot and the fineness change of the characteristic.
Sodous is decided.
(3)The increment is gathered, this is collected, and it makes it to a partial sample.
(4)This is crushed, subdivided, and the moisture examination sample and the element examination sample
are made.
Outline of Figure 1 sampling and sample preparation(one example)
Hiki
1111

Increment Partial Sample for Moisture Day Ev

One en
Increment sample moisture examination
&

One in
Lot Sublot ― One sample Day g
･･
One
11

Sample for
element
..goin

Partial Sample for Moisture Data

Increment sample examination

Sublot ………… Two times of ditto work work

……………………………………… sweat
Sampling Sample Analytical
preparatio determinat

The sample is not lost, and not changed in quality through the period of the handling sampling of the t2
sample, the sample preparation, and the measurement.
Of ..pull.. attention.
Moreover, the apparatus used so that the foreign body should not mix with the sample is cleaned enough.
(1)Next, the sample container sample container depends.
(a)Various samples are transported, and the container used for the purpose such as keeping enters the
whole quantity of the sample, and caps clean durable and Mino.

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8109-1996
The one that it is possible to seal it.
(b)Especially, the container of the sample for moisture is the one that it makes from the material without the
moisture absorption because of airtight, and rust etc. are not generated internally.
(2)The aluminum foil and the polyethylene, etc. of wrapping and the display element examination sample of
the element examination sample that paint the resin internally.
It puts in the bag on the inside, it seals up, this is enclosed with the paper bag in addition, it sends, it
distributes or it keeps it.
As a rule, the following item is displayed in wrapping the element examination sample.
(a)Name of articles(brand of ore)
(b)Lot name (ship name) and size
(e)Sublot number
(d)Date of sampling and sample preparation
(e)Office name of sampling and sample preparation
(f)Sample preparation (responsibility) person's name
(g)Additionally, necessary matter
(3)Next, keeping the keeping element examination sample of the element examination sample depends.
(a)(2)As a rule, a part of the element examination sample that wraps is kept for six months.
(b)When keeping it, the inventory location is noted so that there is no influence by the temperature,
humidity, and direct sunshine, etc.
(4)As a rule, samples other than the sending element examination sample of the sample are not sent.
However, that when unavoidably sending it.
It depends on the conference between the receiving contact persons concerned about the law.
Each sublot is analyzed by providing for JiS M 8126 about the decision nickel of the average of t3 fineness,
and each Sabrotsu.
Iing thirdly below the decimal point calculates ..standing.. the mean value of which it weights the mass of To
with weight. This is rounded to 2nd place after the decimal point, and the lot.
It drinks and it is assumed the decision value of Hira Hitoshi fineness.
Moreover, it is 7 as for moisture . The numerical value obtained by the method of regulations to the method
of measuring moisture is assumed to be a decision value of the lot.
How to round the numerical value of how to round it of the t4 numerical value depends on regulations of JIS
Z 84ol.
Next, other t5 matter and other matters depend.
(1)The necessary matter not provided for by this standard is decided by the conference between the
receiving contact persons concerned.
(2)By methods other than providing to this standard by the conference between receiving contact persons
concerned when a part of this standard cannot be applied
The fault can be done.
(3)The check experiment of the sampling method is attached book 5 on JIS M 8IOO (experiment method of
checking the accuracy of sampling).
Attached book 6 (experiment method of checking bias of sampling) and ..(of attached book 7.. the truth that
checks bias and accuracy of subdivision machine
It does by the method of the effect), and whether the provided accuracy is achieved is investigated.

5.Sampling method
5.1As a rule, the lot and the size of the size lot of Sabrotst are assumed to be an amount of ore of
one ship.
Moreover, the size of the sublot is 5 or less It is assumed 000t.
5.2Characteristic and accuracy
The characteristic that provides for 5.2.1 characteristic accuracy is assumed to be a nickel and
moisture.
The value of 5.2.2 synthesis accuracy synthesis accuracy is indicated in Table 1 with respondent to
the size of the lot.

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M 8109-1996

Table I synthesis accuracy (a of two)

Size of lot t

Characteristic
30 From 000 or
20 000 or more is 10 000 or more is
more to fulling
30 Less than 000. 20 Less than 000. 10 Less than
block 000 or less
000
It 0.025 0.030 0.0 0,050
is ..nickel.. %.
Moisture % 0.5 0.6 0.8 1.0

The value of 5.2.3 accuracy of the sampling accuracy of the sampling is indicated in Table 2 according to the size of the lot.
Table 2 accuracy of the sampling(2)

Size of lot t

Characteristic
30 000 or more 20 000 or more 10 000 or more
is 45 000 or is 30 Less than is 20 Less than
less. 000. 000.
10 Less than 000
It 0.020 0.024 0.032 0.0
is ..nickel.. %.
Moisture % 0.48 0.58 O｡76 0.94

5.3 As for Table 3 and moisture, when it attaches to the nickel, the division of the size of the fineness change of the division
ore of the size of the fineness change is Tables 4.
.
Division of size of Table 3 fineness change (for for nickel)
Unit %

Division of size of Change in

Layer..change.
fineness change layer(mind)
Largeness 0.25 or more 0.15 or more

From 0.15 to less than From 0.05 to less than

Inside 0.25 0.15

Smallness Less than 0.15 Less than 0.05

Division of size of Table 4 fineness change

(moisture)
Unit %
Division of size of Change in
fineness change
Layer..change.
layer..(.. ..peel..)
Largeness Five or more Three or more
Three or more Less One or more Less
Inside
than 5. than 3.
Smallness Less than three Less than one

The first ..Remarks I. change in layer.. ..sampling unit.. ..(.. glove ..for instance.. ..track..
The bucket) It is good, and ..standard deviation between increments.. layer.
The change means the standard deviation between the sampling units the first among.
2.The size of the fineness change is a San ..(of attached book 3.. pudding of JIS M 8100
according to the layer.
The examination method of the fineness change in G and the system sampling) Or, Ts.
Belonging book 4 (examination method of fineness change in forked sampling)
Is requested.

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5-8109-1996

3.When the size of the fineness change of the object is an uncertainty, it is principle until turning out.
Do..fineness..change..size..division..handle.
5.4It depends on the following either of the collection time of the execution time of sampling increment.
(I)It does while moving the lot at the receiving contact time of the lot.
(2)It does as much as possible before and behind that the measurement of the mass of the lot at near time.
5.5The kind of kind sampling of sampling depends on the following method according to the loading or the
mode of transportation.
Two methods can be used together.
(1)Belt sampling
(2)Track sampling
(3)Hold sampling
5.6Increment
The size of the size increment of 5.6.1 increments is Sco of the capacity shown in Table 5 according to the
maximum grain degree of the lot.
It is assumed more than the mass that can be gathered with Pp.
To become constant almost in each increment, the size of the remarks increment is gathered. What is
constancy almost?
It is said that the difference of the size of the increment is less than 20% as the coefficient of variation.
Next, the collection tools of the collection tools increment of 5.6.2 increments depend.
(1)As a rule, the shovel for the shovel increment collection for the increment collection : according to the
maximum grain degree of the lot.
The one more than the shovel number in Table 5 is used.

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M 8109-1996
Shovel for Table 5 increment collection and for subdivision

Size mm
Big
Shovel Capacity
degree No.
number Thi m1
mm
￡Z み C j g / ckn
g ess
About 35
150 ].50 450 190 450 380 170 3 0.4,2
000

About
125 125 380 160 380 320 150 3 0.42
21000
About 11
100 100 300 130 300 260 120 3 0.43
000

Leopard
70 71 200 100 200 !70 80 2 O｡50
3 700
About 1
50 50 150 75 150 130 65 2 0.50
600
O｡ About
40 40 110 65 ].!0 95 50 2
59 730
Pr O｡ About
30 31.5 90 50 90 80 40 Pro 2
op 56 380
per
erl O｡ About
20 22.4 80 45 80 70 35 ly 2
56 270
y
About
15 16 70 40 70 60 30 2 0.57
180

10 10 60 35 60 50 25 1 0.58 Some.

5 5 50 30 50 匍 20 1 0.60 About 70

3 2.8 40 25 40 30 15 0.5 0.62 About 35

1 1 30 20 30 25 12 0.5 0.67 About 16

0.25 D 0.25 15 10 15 12 0 0.3 0.67 2.

Remarks 1. The one that doesn't exist for child Ncriment subdivision at time with these shovels
(g=O)D is put on the right of the number of it is and the shovel for.
2.Shovel number O. 25 D is used only for the increment subdivision.

(α=c)

(2)Next, the machine sampling device machine sampling installation depends.

(a)The installation sample collection device of the device is set up at the position over which the whole
quantity passes when the lot is moved.
It sets it up in remarks etc. , for instance, , main conveyer fall Ro. There are cutter type Sampra etc. as a
device.
(b)The size of open Ro of the sample collection machine sample collection machine is principle ..size (.. that
can easily gather the particle of the maximum grain degree of the lot.
It is assumed three times or more maximum grain degree).
Moreover, the one structural that doesn't overflow from the collection machine the sample, and is not blocked
in the shot.
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(e)It is preferable at collection intervals of the collection interval changed.
(d)The safety machine sampling doctrine is designed, and when setting it up, enough consideration is paid
about worker's safety.
(e)Maintenance and the watch machine sampling device are maintained through all systems such as the
sample collection machine, the conveyer, hoppers, and disintegrators.
However, it is preferable that it is a structure cleaned easily easily, and a material that doesn't corrode.
Running moreover, it is preferable that it is a structure to observe the function of each part easily.
(f)There must not be bias in the sample gathered with this device in the check machine sampling of bias after
setting up the device.
It confirms it by check experiment.
The remarks check experiment method depends on attached book 6 on JIS M 8100.
(g)The check machine sampling device of accuracy becomes a structure that the check experiment of the
accuracy of the sampling can be facilitated.
It is preferable.
The remarks check experiment method depends on attached book 5 on JIS M 8100.
(3)Next, the collection tools of the collection tools of other increments and other increments depend.
(a)(two household f)Bias must be the one according to the experiment of ..drinking.. check that doesn't enter.
(b)It is respondent to the maximum grain degree of the lot, and ink more than the mass that the size of open
Ro is more than α in Table 5, and provides for by 5.6.1.
The one that Riment can be gathered.
A minimum, necessary number of increments gathered from the number of lots of 5.6.3 increments : according
to the kind of sampling.
It depends on, 5.9.2, 5.10.2 or 5.11.2.
Next, the method of gathering the increment of the method of gathering 5.6.4 increments depends.
(1)One work of the increment for the size of the increment to steady almost with a collection tools that provide to
5.6.2.
It gathers it by operation at random. However, one place specified at random when it is difficult to gather it by
one work operation.
It twines, it gathers by Su operation, this is annexed, and it is good as one increment.
(2)The increment is gathered while moving the lot in the Nits inside and the load wholesale, etc. as a rule.
(3)Do not change the collection interval during the sampling work of one Sabrot.
(4)When the loading of the sublot is continuously done, the collection is stricken even if it finishes catching a
prescribed number of increments.
It keeps catching the increment without cutting it at prescribed intervals.
5.7The increment is brought together at each mass (About 100-500 t) when Sabrot of how to bring it together of
the increment was subdivided further.
Partial sample is made, and moisture and the element examination sample are made from these.
5, using eight samples combinedly, and the sample of promoting an important position are used combinedly or
can be promoted an important position for moisture and for the element. However, for moisture and for the
element
The sample that satisfies the characteristic in one with a lot of minimum, necessary numbers of increments is
used when fineness change division is different.
Moreover, when the sample is promoted an important position, it is necessary to satisfy the following various
conditions.
(1)When crushing and subdividing, equipment that prevents the minute powder ore from dispersing : because
the minute powder ore disperses easily to a dry sample after moisture is measured.
Arrange.
(2)It must be confirmed that there are no bias in moisture and the nickel by the check experiment.
5.9Belt sampling
Is when moving, collection place lot of 5.9.1 increments the fall mouth on the belt according to the belt
conveyer?
Increment is gathered.
Table 6 shows a minimum, necessary number of increments gathered from the number of one lot of 5.9.2
increments.

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M 8109-1996 Minimum, necessary number of Table 6 increments

Change in layer()
Size of lot t Sm
Largenes Insi
alln
s de
ess
10 Less than 000 225 100 40

10 000 or more is 20 Less

than 000. 360 160 65

20000 or more is 30 Less

than 000.
670 300 115

30 000 or more is 45 000

or less.
900 400 160

Next, the method of gathering the increment of the method of gathering 5.9.3 increments depends.
(1)The system by a random start is sampled. In this case, the collection interval of the increment is a size of the
lot.
(y)..showing.. is divided, and increment ..collection number (.. is decided. In this case, the fraction is rounded
down.
(2)The amount at the position of the belt when the belt conveyer is stopped and it gathers it more than the size of
a regulated increment.
Is gathered. In this case, have the length three times or more the Nageootsb degree of the lot in the traveling
direction of the belt, and to all fluencies of the belt
It extends and the whole quantity is gathered as one increment.
When ore moves by the belt conveyer, remarks whole content is a direction of the movement or a fall mouth of
the conveyer and a fall.
It has the length that is, in that direction against, and the cutting part of right-angled ..carving.. is said.
(3)A regulated increment in the fall Ro on the belt when gathering it from the belt conveyer while driving.
The amount more than the size is gathered over all fluencies.
In the fall Ro on the belt after confirming there is no bias when fluent all remarks cannot be gathered
The collection position in all fluencies is chosen at random, and the increment is To according to regulated
increment collection tools.
And. taking
5.10 track sampling
The increment is gathered from the track or the wagon in collection place loading of 5.10.1 increments.
Tracks of a minimum, necessary number are extracted from one lot by Table 7 as the first minimum, necessary
track number step 5.10.2 extractions.
The second step, the increment of ..hardness.. of two I is gathered from the extracted individual track.
Number of minimum, necessary tracks to extract Table 7

Middle of the forehead change)

Largeness Inside Smallness

Horiuchi Change in
Change in
Size of lot t change..(.. ..p layer..(.. ..peel..
layer(mind)
eel..) )
Lar Lar Lar
Sm Sm Sm
ge Insi ge Insi ge Insi
alln alln alln
ne de ess ne de ne de
ess ess
ss ss ss
Je
10 Less than 000 215 150 120 HO 75 alo 115 55 25
usy
10 000 or more is 20 Less than
000.
340 240 195 220 120 75 185 85 35

Next, the method of gathering the increment of the method of gathering 5.10.3 increments depends.
(1)The track where the increment should be caught is chosen as the first step of the two-stage sampling. The how to choose
is a system San pudding.
It depends on G.

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M 8109-1996

(2)The size of the lot is divided in the number of extraction tracks and the extraction interval of the track where the
increment should be caught is decided. この
When happening, the fraction is rounded down.
(3)The collection position is decided at random to gather the increment in the track, and new of the freight that
appears in the loading.
The increment is gathered from ..saying.. Men.
There is no bias by the check experiment when it gathers it from the surface part of the freight while piled up in the
track
It confirms it.
5.11 hold sampling
Collection place lot of 5.11.1 increments is in the loading tools the loading according to the loading tools in the glove
bucket etc.
Or, the increment is gathered from the position immediately after the loading in the hold. With this loading tools in
place of the collection from among the loading tools
After transferring the ore grabbed at to a flat place, you may gather it. However, bias according to the check
experiment.
It confirms it.
Table 6 shows a minimum, necessary number of increments gathered from the number of one lot of 5.11.2
increments. However, one G.
When the gathered number of increments is two, it is putting in the number of glove buckets from the love bucket as
for the number of tracks of 5.10.2.
It gets, the necessary glove bucket is extracted, and two increments are gathered from the extracted glove bucket.
Next, the method of gathering the increment of the method of gathering 5.11.3 increments depends.
(1)The system by a random start is sampled. In this case, the collection interval of the increment is a size of the lot.
(Ⅳ)It rules, is divided, and increment ..collection number (.. is decided. In this case, the fraction is rounded down.
(2)The collection position is decided at random when gathering it from the position immediately after the loading in
the hold and the increment is gathered.

6.Method of making sample

6.1Next, making the making sample of the sample depends.
(1)The sample is crushed, subdivided, and the element examination sample and the moisture examination
sample are made.
(2)The sample for the element dries if it is necessary on the way for crushing and the cotton crepe.
(3)The increment is subdivided by each partial sample, and the sample for moisture is made.
(4)About the sample after moisture is measured, when the sample for the sample and the element ..for
moisture.. is promoted an important position, it subdivides and the ..the whole quantity.. part.
Sublot each is amalgamated, and the element examination sample is made.
(5)It subdivides according to the subdivision standard of six referring 6 by an appropriate subdivision method.
(6)It is noted enough that a part of the sample doesn't disperse in the sample preparation, and neither
surrounding powder Shin nor other foreign bodies mix.
6.2The value of the making accuracy making accuracy is indicated in Table 8 according to the size of the lot.
Table 8 making accuracy(2･)

Size of lot t

Characteristic
30000 or more 20 000 or more
From 000 10 to
is 45 000 or is 30 Less than
less than 20000 10 Less than
less. 000.
000

It is ..nickel.. %. 0.011 0.013 0.017 0.021

Moisture % o｡11 O｡16 0.22 0.32

The remarks moisture is shown by the twice accuracy ((7-) including making and the measurement.
6.3Natural Cawa when it is difficult to be extreme to be moist of preliminary, of sample for element dry
sample, to sift out, to crush, and to subdivide
100 according to or the drying equipment, etc. It ..all right level.. dries the use of the installation by the
temperature of ℃ or less ..the disintegrator and the cotton crepe...

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M 8109-1996

6.4Crushing the crushing sample of the sample crushes the whole quantity of the sample to the grain degree of a
prescribed sample whole quantity street with an appropriate disintegrator.
(1)Hardness, strong Shin character, specific gravity, and ..physical description (.. moisture of sample grain degree
after it crushes of grain degree of sample by which disintegrator does selection crushing and sample
Cohesiveness..ream..model..ability..have..disintegrator..select.
(2)The cleaning disintegrator cleans the inside before supplying the sample.
(3)Wash..last time..crush..sample..differ..brand..sample..crush..beforehand..the..lot..another..gather.
It is preferable to clean it through the ore of this amount of ..departure.. Cana.
(4)It is noted that there is no sample to stay in the taking out disintegrator of the sample.
(5)It is noted that the sample doesn't change in quality by generation of heat such as models of the changing in
quality prevention disintegrator and continuous driving for a long time.
6.5..cotton crepe of the sample..
Next, ..6.5.1 cotton crepe.. method ....method.. subdivision it.. depends.
(1)The sample is subdivided using the method whether what one method or seed it together among the following
methods.
(a)It is ..increment cotton crepe.. method.
(b)Method with riffle sampler
(c)It is a method of the cone for four minutes.
(d)Method by subdivision machine
Because the method of (b), (c), and (d) causes the emanation loss of moisture easily in making the sample for the
remarks moisture, ..use...
.
(2)It ..cotton crepe.. does with the sample of the grain degree 22.4mm or less of the sample whole quantity street
as a rule.
(3)The standard of subdivision is shown in 6 and 5 and 6.
(4)The equipment used to subdivide is cleaned enough before it uses it. When you subdivide the sample
subdivided last time and the sample of a different brand
It is preferable beforehand to clean it through the ore of the suitable amount separately gathered from the lot.
(5)It doesn't note it. While subdividing ..mixing dispersion, changing in quality, and the foreign body of the sample
etc...
Next, ..referring.. method of six of subdividing the increment of the method of subdividing 2 increments depends.
(1)The sample is expanded to the square, and the sample is subdivided with a shovel for the increment subdivision.
Shovel for increment subdivision
It drinks and the thickness of Dai , and the expanded sample is shown in Table 9 with respondent to the grain
degree of the sample.
The pipe etc. can be used instead of the shovel for the remarks increment subdivision. However, the inside
diameter of the pipe :.
It is assumed more than α in Table 5 according to the maximum grain degree of the lot. The pipe reaches the
bottom, and the gathered sample the sample
It expands it to thickness switching off ..no dropout.. ..the ream...

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M 8109-1996

Grain degree of Table 9 sample and shovel for increment subdivision

Thickness of size and expanded sample

Grain degree of
Shovel Thickness of
sample whole
number expanded sample
quantity street
22.4mm or less 20D 35～45

16.0mm or less 15D 30～40

10.0mm or less 10D 25～35

5.00mm or less 5D 20～30

2.80mm or less 3D 15～25

1.00mm or less 1D 10～20

250μ ﾟ or less o｡25D 5～10

Table 5 shows the size of the remarks shovel and capacity.

(2)The number of increments is assumed to be 100 pieces or more per sublot. However, the grain degree of
the sample whole quantity street : by 10mm or less.
When it is dried enough by the level that can be mixed, it is assumed 20 pieces or more per sublot.
(3)Applying ..(.. Figure 1 by the following procedure when ..increment cotton crepe.. situation of partial
sample by manual operation , for instance, division into 20
Joining Ltd..
(procedure 1)The sample is uniformly expanded to the rectangle by the thickness of Table 9 on monotony.
(procedure 2)Five capitation of this in side by four capitation in length.
(procedure 3)It is a shovel for the increment subdivision, and a meter from each division by 1 piece (The
place is chosen at random in each division).
20 pieces are collected, and it makes it to the sample after this is subdivided. The sample ..insertion up to
the bottom of the sample layer... the shovel at this time
Is gathered.
Remarks 1. Ink when mass of sample after it subdivides is demanded from mass of sample gathered by the
above-mentioned method voluminously
The size of Riment is enlarged or the number of increments is increased.
The number of division is increased when the number of increments is increased or it is Incri gathered from
division into one.
The number of Ment is increased. In this case, the collection number from each division should be constant.
2.When the increment cotton crepe is done, the application board is applied and Na ..the collection of the
increment.. ..preferable...
Next, the method with the container depends for the method with the container for two minutes for 6.5.32
minutes.
(1)The riffle samplers of the number of titles shown in table IO as a rule are selected according to the grain
degree of the sample.

13

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 12

M 8109-1996

Times of ten Table and kinds of riffle sampler

Grain degree of
sample whole quantity
Kind of riffle Width mm of
street
sampler ditch
Excess As follows

16.0 22.4 No.50 50 soils 1

10.0 16.0 No.30 30 people 1

5.00 10.0 No.20 20 soils 1

2.80 5.00 No.10 Ten people O. 5

2.80 No.6 Six soils 0.5

(2)Next, two separate volumes depend.

(a)Applying Figure 2 shows shape, the size, and the structure of the riffle sampler.
(b)Corner (θ) scissors of both slopes and under is assumed to be 60 degrees or less.
(e)The number of ditches is assumed the even number piece, and, as a rule, assumed to be 16 or more.
However, No.50 and 30 titles are assumed to be 12 or more.
(d)The sample receiving container is assumed to be a structure that a minute powder doesn't disperse from
the machine exit for two minutes.
(e)The inside of the riffle sampler uses the one that is smooth, and doesn't include rust etc.
(3)It puts in sample ore container, it drops to the main body of the riffle sampler uniformly, and the sample is
divided into two. The either of them to random
It chooses, and it makes it to the sample after it subdivides.
When the container ..remarks.. is used for two minutes, ..blocking.. of Hi of eyes of ..crowding.. attention of the
ditch.
(4)The standard of subdivision is shown in 6.5.6.
The method depends on six referring 4 of JIS M 8100 (It is a method of the cone for four minutes) for four
minutes for 6.54 cone four minutes as for the method cone.
The method subdivision machine by 6.5.5 subdivision machine confirms there is accuracy enough neither or
bias.
Moreover, the standard of subdivision is shown in 6.5 and 6.
The equipment used for the remarks subdivision is cleaned enough before it uses it. It is ..cotton crepe.. as for
the sample of a brand ..last cotton crepe.. different from the sample.
The situation is ..washing.. ..hope.. and : beforehand separately from the lot through the ore of the gathered
suitable amount.

..sa
ying
As a rule, the relation to the mass of the sample the grain degree of 6.5.6 subdivision standard sample
whole quantity street and after it subdivides is done by table II. However, the Inn.
It depends on 6.5.2 at the Criment subdivision.

14

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 13
It is times of 11 Table and ..cotton crepe.. standards.
M 8109-1996

Grain degree of
Mass of sample after
sample whole
cotton crepe Kg
quantity street
22.4 Mm or less 140 or more

16.0 Mm or less 70 or more

10.0 Mm or less 35 or more

5.00mm or less Eight or more

2.80mm or less Two or more

1.00mm or less 0.5 or more

420μlll or less 0.1 or more

250 eggs 1 or less O and 05 or more

Remarks 1. The mass of the sample in this table is an umbrella of the sample.
The density indicates the case of one.
2.It is a cotton crepe below the mass of the sample shown in this table.
..understanding..
6.6Next, making the making element examination sample of the element examination sample depends.
(1)The sample for the made element of each sublot is minute crushed to 150μm or less, and it often mixes it.
Increment cotton crepe in the future
The sample of each 1oo g or more is prescribed number made with ..cotton crepe.. machine of ..method of the
amount.. appropriateness it.
(2)This sample is incased, sealed up, it seals, and it makes it to the element examination sample.
(3)The element examination sample is assumed to be 4 pieces or more for the seller, for the purchaser, and for
the umpire and for keeping as a rule.
6.7Next, making the making moisture examination sample of the moisture examination sample depends.
(I)It subdivides after it crushes to 22.4mm or less with a disintegrator appropriate in each partial sample that
subdivides the sublot further and 1.
As a rule, one sample of -5kg is made.
(2)As a rule, it depends on ..increment cotton crepe.. method the cotton crepe. The number of increments in this
case applies 6.5.2 correspondingly, and is I.
The shovel for the Ncriment subdivision : one stage small dice one from the standard in Table 5 as long as a
prescribed amount of the moisture examination sample is satisfied.
You may use it.
The moisture examination sample made from the standard in remarks table 5 with one stage small dice shovel is
a Japanese oak when promoting to the sample for the element.
It is not.

7.Method of measuring moisture

7.1It dries until becoming a constant mass a temperature to which the summary moisture examination sample is
provided. Request individual moisture from losses on drying, and to 7.6
The moisture of the lot is decided.
7.2L that uses moisture examination sample made with sample 6.7
7.3Next, the device device depends.
(1)A dry plate is the one with the bottom product that the thickness of the sample becomes 30mm or less in the
one of anti-corrosion heatproof.
(2)The limit deviation tolerance of the maintenance temperature of the constant temperature dryness machine is
assumed to be the soil 5℃.
(3)In the measurement, the minimum scale value is the one below the merit of Tamemurehoshi.
7 and four operation operation are done by the following procedure.

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14

M 8109-1996

(I)1-5 made by 6.7 So that the moisture examination sample of kg may be moved to a dry plate of mass
already-known, and the thickness of the sample may steady almost
It makes to flat, and the amount of Shi ..left.. is measured.
(2)Person dries 5 and 105 soil C beforehand ..the adjusted constant temperature dryness machine...
(3)The mass whenever it takes out after it dries during the fixed time, mass is measured, and it dries for two
hours afterwards is measured, and the heat losses on drying are counted.
..putting out...
(4)The heat losses on drying rate keeps drying with 0.1% or less every two hours until becoming it.
The time required when it experiments on each remarks brand, and the time required to reaching to the constant
mass can be requested
You may consider that it reached the constant mass.
(5)Mass is measured while it is the remainder.
7.5The calculation moisture is calculated and even 3rd place below the decimal point is calculated by the
following expression.
Correction s= { k3 { Do ×100
It is here: Moisture. (%)
..glare..:Mass of dry plate(g)
Positive:Moisture examination sample and ..remainder.. amount of Shiti of dry plate(g)
Horse:Yoshitsryou when dryness ends(g)
7.6Next, the decision value decision value depends.
(1)The moisture of the sublot is Cama as for mass or a partial sample of the first each Sampri y G that each
measurements of the moisture requested by 7.5 represents.
The sublot of the value in which it does and the number of increments is rounded to 2nd place for the mean
value with weight after the decimal point as weight.
It is assumed moisture.
(2)The smallness of the moisture of the lot for the mean value with weight of which it weights the mass of the
sublot of the moisture of the sublot requested by (1).
It rounds to 2nd place below the scatter point and it is assumed the decision value.

8.Next, the decision of the amount of Cawa of the method of deciding dried-up Haca depends.
(1)The dry measure of the sublot is calculated by the following expression.
j

ぐ _凰ﾚ
1

Calm j= skin. 100,

×
t こに Dry measure of wind entrance Sabrot(t)
Mass of wind entrance Sabrot(t)
Moisture of sublot requested by y 7 and 6(%)

(2)The dry measure of the sublot is added, and this is assumed to be a decision value of the dry measure of
the lot.

16

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 15

The method is illustrated applying Figure 1 increment line. (one example of division into 20) M 8109-1996

Thickness that provides for crushed

partial sample to Table 9
It expands it to the rectangle.

20 capitation of this.
For instance, four capitation in length and
five capitation in side.

It is an Inn from each division 20 capitation in

random.
Crimentoscopp is put in the bottom.
One increment is caught, and this.
It .... collects and it makes it to ..cotton crepe..
sample.

Points chart where increment is gathered by using application board

17

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16

M 8109-1996

Form and size of ..applying

Figure.. container for 22 minutes

C
A a
p
e 1
う - 1

S
u
m
m
o
n
s

Unit mm
Number of riffle 50 30 20 10 6
sampler
Number of ditches 12 12 16 16 16

j
sum
mo
ns 30 people
20 people Ten soils Six soils
①It is a main C 50 soils 1 1 380
1 346 0.5 171 0.5 112
￡) 630 250 170 340
body of the 500 300 200 30
105 210 55 110 40 80
machine for ￡F 50340200 elbows
135 75 20 60 20
G .. 30210 110 45 80 30
two minutes. 640220 01403902
853601 184 65 120 55
ran 20
ging
.. y
tile
￡
②Sample cor
rect 22034025 22034017 14021010 65110 55 55804015
receiving ion 0 75340 0 55340 5 35210 20110 80
container y?
Q

③Sample Gin ￡S 63040026 38030020 34620013 171120 112 80 45

7 5200 0150 5105 70 50 35
container

18

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 17
Garnierite nickel ores-Methods for sampling, sample preparation and
determination of moisture content
JIS M 8 1 09-1996

Sampling
Explanation
Method of deciding sample preparation and moisture
This explanation is the one to explain the matter that provides to the main body and the matter related
to this, and no part of the standard.

I.The details standard of the revision is Sei in 1965 as the method of deciding the sampling method and
moisture concerning the Kei worried soil nickel ore.
Sadamu. Afterwards, it was revised diversifying of the dealings brand, enlarging of the amount of the delivery,
and decreasing in the nickel fineness in 1974.
As the main revision point
(1)The size of the sublot assumed one lot a ship, and was large so far, and was 5 or less It assumed it until
000t.
(2)Lot..ore..amount..nickel..synthesis..accuracy..level..coefficient of variation..do..lot..large.
It matched and the accuracy of the sampling and the sample making accuracy were reviewed.
(3)Integrated accuracy of moisture (100-moisture) was provided for for (%) to become it more than the equal to
integrated accuracy for the nickel.
(4)The classification of the size of the fineness change of moisture was revised, and a necessary number of
increments was reviewed according to this.
(5)The accuracy of the method and the subdivision ..increment cotton crepe.. method with the riffle sampler was
reexamined, and provided for to satisfy necessary accuracy.
It is.
About 20 years passed after the revision in 1974, and, meanwhile, the revision over two degrees was done as
for related standard JIS M 8100.
Then, the fact of further enlargement of the amount of the delivery etc. revise a related part of a related
standard in this revision (1996)
The revision of the part where is not suitable is also executed, and the name of the standard is sampling,
sample preparation, and Kei worried soil nickel ore-moisture ..".. Kima.
It was renewed as Sadacatahou "
The main point considered in the original bill making is as follows.
(1)Therefore, the adjustment of the term was aimed at in accordance with JIS M 8100-1992 (general rules of
the method of sampling the Cocatamari compound one).
(2)The maximum grain degree matches to the sizes of eyes that JIS Z 8801 (It is old for the examination) is old,
and, therefore, is Incrimentosco.
The size of Pp and the kind and the subdivision standard of the riffle sampler were revised.
(3)20 in consideration of the fact of the ship type enlargement though one lot of the size of the lot is an amount
of ore of one ship It is 30 by 000t or more Less than 000t.
And, 30 The division of 000t or more was newly installed.
It is 45 for the convenience of the calculation like integrated accuracy etc. as for the thought current state
maximum amount of one ship It is assumed 000t, and the division is 30 It is 45 by 000t or more 000t.
It made it to the under.
(4)Therefore, Incri. revise integrated accuracy, the accuracy of the sampling, and the making accuracy
according to the revision of the size of the lot
A necessary number of Ment was revised.
It is.
H.The explanation of the content of a part of the revision, the main part where the explanation regulations of a
content and a regulated item content was revised, and a regulated item is as follows.
..going out.. .
2."Meaning of the term" and "Sign" are separated from general rules of a definition old standard of the term
(1974), and in the form of which "General matter" who another.
One was done.
Moreover, the term changed and added the name in accordance with JIS M 8100.

Solution
1
19

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 18
M 8109-1996 explanation

3.The name was changed and added in accordance with sign JIS M 8100.
The outline of t general matter sampling and the sample story was made figure and the addition example was
recorded.
Method of sampling &
5.1The amount of ore of one ship is assumed to be one lot as a size principle of the lot and the sublot, and the size of
the sublot is 5 or less 000t.
It provided.
Moreover, the number of sublots was assumed to be set within this regulated range.
5.2Characteristic and accuracy
Ten of the lots in the size about 5.2.2 synthesis accuracy nickel The lot based on level CV1% of accuracy at 000t.
To drink, in inverse proportion to the square root of Dai, and to increase and decrease, it calculated. Accuracy
(100-moisture door %) of moisture is ,that is, Cawa.
Ten of the lots of the amounts (%) in the size It is an anti-ratio in the square root of the size of the lot based on level
CV1% of accuracy at 000t.
It calculated assuming that example increased and decreased.
The division division of the size of the lot in table I into three was assumed to be division into four in consideration of
the fact of the ship type enlargement.
Moreover, thought current state maximum amount 45 of one ship After 000t had been divided, accuracy was
calculated as a limit.
In 5.2.3 accuracy of the sampling table 2, it was 20 It was 30 by 000t or more 000 less than t and 30 It is 45 by 000t
or more The division of 000t or less was installed.
5.3In the calculation from which the collection number of division increments of the size of the fineness change is
requested, the Horiuchi change () and the middle of the forehead change () are Ni.
Kkel and moisture were calculated by the numerical value in explanation table I and each explanation table 2.
The making a joint experiment result of the size of the fineness change is explanation table 3.
Value of respondent and seagull that used it for explanation table I calculation(For the nickel. )
Unit %

Fineness Change in Development

change layer(shame) change()

Oonacaco 0.300.200.125 0,200』.00.025

The value of the seagull when Niing and using it. (moisture)
Explanation table 2 calculation C.

Unit %

Middle of the
Change in
Fineness forehead
layer..(.. ..peel
change change ..swim
..)
..)

Oonacaco 6､04.02.5 4.02.00.5

Solutio
n2
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 19
M 8109-1996 explanation

One example (manual

Unit %

Ni+CO Moisture
Kind of sampling Brand
Respo
Sake
Mind 嗚 ndent
Tio 0.14 -

Poya O｡13 1.47

Tomo 0.19 1.75

Tontsuta 0.13 1.27

Belt sampling hatch

Carambe 0.10 2.35
sampling
Mondor 0.09 1.91

Paita 0.12 2.75

Pomara A 0.08 1.51

Pomara B 0.05 1､87

Uine 0.15 0.09 2.25 O｡00

Tontsuta 0.11 O｡12 1.H 0.90

Burai 0.20 0.10 - One

Nepi 0.18 0.11 1.44 1.14

Track sampling hatch

Teudie 0,07 0.15 1.11 1.46
sampling
Canara 0.04 0.09 L23 1.10

Pomara A O､05 0.03 0.87 0.76

Pomara B 0.10 0.10 - One

Pomara C 0.05 0.01 1.56 1.37

Making a joint experiment data of remarks JIS M 8109-1974.

5.5Kind term of sampling changed the name in accordance with JIS M 8100.
It matches to the sizes of old eyes for the examination provided for by size JIS Z 8801 of 5.6.1 increments, and JIS.
The size of the shovel was changed in accordance with M 8100.
It matches to the sizes of old eyes for the examination provided for with collection tools JIS Z 8801 of 5.6.2 increments,
and S.
Semi-revisions of the size of the glass to regulations of JIS M 8100.
Moreover, the shovel for the increment collection when it is difficult to gather it with the shovel for a prescribed increment
collection.
Suitable tools such as hoes (hoe) ..placing of the size of length, side, and height this in the collection part with tools that
this level is almost ..others.. suitable...
Is removed and it is possible to gather it. One example of the collection tools of the increment is shown in times 1 of the
explanation.

Solutio
n3
21

The reproduction and the reprint, etc. without permission are

 20

M 8109-1996 explanation

Example of explanation chart 1 increment

collection tools
Unit mm

J∂
-

To the following each expression with respondent to the method of each sampling when you decide the number of the
number of increments of 5.6.3 increments
Was calculated.
(1)It requested it by the expression of the following systematic sampling at the time of the belt and the hold sampling.

2(y=2
Ten Rin Tei(20 ..peel..
minds 2)
_..peel.. Gen____
μ~ ぐ
y

な 2 1
- - (mind 62)
2 ￡

However,

My 2+1 Do of seven = (y
It is 4 here: The number of increments.
￡:Number of sublots
:Making accuracy
..drinking.. .:Reproduction accuracy of the analysis between different analysis places
analyzing it twice in the same analysis place
(yg1: Repetition accuracy of analysis in the same analysis place
･Seven: Reproduction semi-accuracy of the analysis between different analysis places

(2)It is requested by the expression of the following two-stage sampling at the time of the track
sampling.
j

ぐ Correction It is 10j neck N for ten

Two =2 - Eternal
One minutes. (.20 minds 2)
Imitation 2+ Rin
Ten Tamacamome 21
~ hands(.20.22)
y

ぐ 2(y
One
2

1 And: In the two-stage sampling, it is numerical of the first unit of sampling (track) extracted to the first role.
Mi
: Inn gathered as the second step from the first unit of sampling (track) in two-stage sampling
Average and 1 of numbers of Criment
However: The number at the time of the first each sampling that composes one lot. (number of all tracks)

Moreover, it was assumed =2 in this standard at the time of the track sampling though the state as it is was requested in
general based on the next expression.
=

〃 And tile: Cost in which the first one sampling unit is sampled.
Tile: Cost in which one sampling secondunit (increment) is gathered.

Solutio
n4 22

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 21

M 8109-1996 explanation

Moreover, because it is usually 1≦0.1, The number of rack extractions was

To. requested by using the next expression.
One guess
N ..doing j...
揖 O ぐ 2(y

j
-
(e20 mind 2)
2

When the sample after moisture of promoting an important position is measured of using combinedly of 5 and eight samples is promoted
to the sample for the element, the minute powder ore : a dry sample after moisture is measured.
The minute powder ore disperses easily, and the crushing size in general is to be nickeled small or disperse when crushing and
subdividing because it is high.
It notes it for ten minutes. Explanation table 4 shows the result of the survey for the nickel according to the grain degree distribution and
each grain degree at each stage for crushing and the cotton crepe.
Fineness according to time distribution of four explanation tables and grain degrees
Unit %

Mass ratio according to grain

Each grain degree Ni10CO
Crushing degree
Ore
subdivision ~"of
kind stage 149μII54 To ~44μ“1
~149 To
~44 Fk“|
1°10 FIII1
11
159μm 159μll1

-10 Mm- 33.544).478.

A ore 3mm~149 Do III
56.446.2- 10.113.421.7
3
2.142.08 - 2.242.161.84 2.822.762.52

-10 Mm-
32.536.881.
B ore 3mm~149 F 57.549.2 - 10.014.018.3
7
2.252.21 - 2.452.411.78 2.752.752.58
Futoshi lll

Making a joint experiment data of remarks JIS M 8109-1974.

5.9Belt sampling
In the number of tables 6 of 5.9.2 increments, it was 20 It was 30 by 000t or more 000 less than t and 30 It is 45 by 000t or more The division of 000t or
less was installed.
Belt when 5, 9, and Cocatamari compound like nickel of method of gathering three increments ore are carried by belt conveyer
It depends up and down, and ..distribution of the grain degree.. ..difference.. .... Oo according to the separation of Cocatamari on the fall eyes etc. right and
left of ore on the belt
..saying.. .Fear to cause bias in sample when sample is gathered only from one side or the upper part of flow for instance when sampling it
. Therefore, it is necessary to take a prescribed amount over all fluencies of the flow of ore on the belt to avoid this bias.
This is similar when gathering it with fall Ro of the belt.
5.10 track sampling
In 5, 10, and minimum, necessary track number table 7 two extractions, it is 20 It is 30 by 000t or more 000 less than t and 30 It is 45 by 000t or more It is
as for divide about 000t or less.
Digit.
Method of gathering 5.10.3 increments
(1)When the increment is gathered in the track, the track is divided into eight beforehand for instance (Refer to the explanation chart 2).
If it puts, and each division of each track where the increment is gathered is gathered one by one, the random sampling is the truth.
It is easy to give it. The collection of the increment from each division is , for instance, Kima ..the collection from the center part of each division...
Manipulatory is easy.
(2)Because ore that unloads the load from the hatch is usually received from the hopper, and extracted from the hopper to the track, Toratsu.
Bias might be caused so that transportation is ..length.. Hana situation though respect where the flow of ore is random appears on the surface of C.
It notes it enough.

Solutio
n5
23

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 22

M 8109-1996 explanation

Increment collection position in explanation chart 2 track

レ
/ 3 5 7

2 4 6 8

5.11 hold sampling

Method of gathering 5.11.3 increments
(I)When the increment is gathered in the glove, the number is divided beforehand for instance in the glove and it ..(.. joins explanation
chart 3.
Sunshiny) It is preferable to gather the increment from prescribed , Ihada etc. of √ each division , for instance, the center part.
(2)As for god's ore, is after it moves it to a flat place in the deck or the quay, etc. , it one Koyama of the ore of the loading tools such as
gloves?
Increment..gather..lower side..some..place..explanation..chart..reference..random..choose..gather.このと
The ratio of Cocatamari is not caught accurately when it comes, and it gathers it from the top part or the lower side of the mountain, and
because bias might be caused in the sample
It notes it enough.
Increment collection position in explanation chart 3 glove

Increment collection position in explanation chart 4 quay

6.Method of making sample

6.2In making accuracy table 8, it was 20 It was 30 by 000t or more 000 less than t and 30 It is 45 by 000t or more The division of 000t
or less was installed.
6.5To check accuracy and the truth degree, -20 the increment ..sample.. cotton crepe of the first subdivision of the sample The mm and
-10.
About 100 before grain degree of mm is dried each sample Between division when it divides into and 4×5=20 and increment is
gathered k
Explanation table 5 and each explanation table 6 shows the result from which the difference () in the difference () and division is
requested. However, Incri.
The shovel for the Ment cotton crepe is 20 in the grain degree -20mm 10D was used for D and -10 the mm.

Solutio
n6 24

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 23

M 8109-1996 explanation

Seagull and S when explanation table 5 increment is

subdivided(Ni10Co)
Unit %

Grain degree -20mm Tsbryouiti 10mm

Brand
φ, J
ら (y

Uine o｡000 0.060 0.000 0.059

Tio O｡000 0.184 O｡004 O｡099

Burai 0.026 0.054 0.000 0.040

Pomara o｡000 0.039 O｡000 o｡040

Carambe 0.081 0.0 0.051 0.069

Tontsuta 0.021 0.054 0.000 0.040

Teudie 0.052 0.047 0.062 0.035

Making a joint experiment data of remarks JIS M

8109-1974.
Charm and when explanation table 6 increment is
subdivided(moisture)
Unit %
Grain degree Grain degree
-20mm -10mm
Brand
Imitatio ..(..
n Ton ら
Uine 0.42 0.58 0.53 1.63

Tio 0.29 0.97 O､00 O｡96

Burai 0.00 ].41 O､00 0.91

Pomara 0,22 O｡50 O､17 0.37

Carambe o｡34 o｡46 O and 0.41

Tontsuta o｡12 0.42 0.16 0.26

Teudie 0.57 O､57 0.25 0.75

Making a joint experiment data of remarks JIS M 8109-1974.

6.5.2(1) Table 9 was revised in accordance with JIS M 8100.
Regulations of the pipe for the increment cotton crepe were newly added to remarks.
6.5.3(1) Table IO was revised in accordance with JIS M 8IOO.
6 and 5.6 subdivision standard table 11 were revised in accordance with JIS M 8100.
7.Method of measuring moisture
It is 100- nO °C and 1-5 as for the sample of 7 and the moisture four operation 25% or more Usual for about ten hours
when kg(size 20mm or less) is dried.
Dryness doesn't end if Cansou is not continued.
Moreover, it is a surely line song that installs the time of two hours or more as for dryness. of the amount of the leopard
of the leopard once (scale) it as for the sample after the amount next
It might break off dryness when and this time of are shortened with moisture remained.
Still constant opinions are the profits though the necessity of the moisture correction in the hatch by the rain wetting was
examined during 7 and six decision value rainfall.
It was assumed that it saw off this time because it was not.
Solution 7

25

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 24.

M 8109-1996 explanation

JIS M 8109 Original bill making committee composition

Name table
Belonging
(chairma Int Valley M Nihon University
n) eri loyalty al Agency of Natural Resources and Energy
or Taki e Mining Industry Division
M This Agency of Industrial Science and
Hi
Yuz Technology standard material fee standard
a Wealth section

Iron
Otocotacashi
Uma Tscasadotstom
H Field
ei The Ministry of Finance Mint Bureau Tokyo
Tomb
gh Book branch
t Furukawa Electric Co., Ltd.
Ki Nippon Yakin Kogyo Co., Ltd.
B Hyuga smelting place Ltd.
un Pacific Metals Ltd.
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Japan Energy Corporation analysis center
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Mitsui Mining and Smelting Co., Ltd.

Japan Mining Industry Association
Mitsubishi Materials Corporation
Mitsui Mining and Smelting Co., Ltd.
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Solution
8. 26

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When the correction vote of JIS standard vote is issued, I will guide it according to the following.
(1)I will publish the content of positive and the mistake in monthly periodical "Standardization journal"
of this society issue.
(2)Advertising column of JIS issue of "Nikkei Industrial News" and "Nikkan Kogyo Shimbun" on the
third Tuesday every month
I will inform of JIS standard number and the standard name from which and the correction vote are
issued.
If he or she can contact the following of √ (business), the person who wants the issued correction
vote will send it.
For those who reserve it JIS about this society, the correction vote issued in the reserved section : to
an automatic target.
It is sent.

One Kei worried soil nickel ore sampling Fixed price 927
Japan yen
Industrial Method of deciding sample preparation and (main body 900
moisture

The first Shaccou on May 31, 1996

Vo Int -
lu eri P Fukuhara On
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m or er
Issue
place
This standard association money of
foundation H
Minato Ward Akasaka 4-1-24 of 107 bit
Tele
phon Time of Bo 100D
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FAX
H)
Seal genius second
Tele base (t
Transfer account 00160-2-195146

In this life pill 3 chome in City Chuo Ward north Article 3 in 060 Sapporo west one
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Transfer: 02760-7-4351
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Japanese high com Ltd. print and Printed in

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27

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 JAPANESE INDUSTRIAL STANDARD

Gornierite nickel OreS

Methods for sampling, sample
prepclrotion and determincltion
of moisture content

JS M 8109-1996

Revised 1996-05-01

lnvestigated by

Japanese lndustrial Standards Committee

Published by
｣｡P｡nese StondQrds AssociQtion

1-24,AkasQko 4-chome,Minoto-ku
Toky0,107JAPAN 28
Prin↑ed in Japon
Fixed price 927 yen(main

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