Professional Documents
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Company name: Chongqing TOP Oil Purifier Co., Ltd Web: www.topoilpurifier.com; www.toptester.cn
Address: No 1 Jianlong North Rd., Jiulongpo District, Chongqing China Zip:400039
Tel: 0086-23-88901306 Fax: 0086-23-88901306 Email: sales@topoilpurifier.com
CATALOG
FOREWORD.................................
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1.1OVERVIEW...............................
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1.2PERFORMANCE CHARACTERISTICS..
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1.3CONDITIONS OF USE AND USER-SUPPLIED MATERIALS.............
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1.4TECHNICAL PARAMETERS.........................
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1.5WORKING ENVIRONMENT.........................
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STRUCTURE AND WORKING PRINCIPLE.
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2.1OVERALL STRUCTURE DIAGRAM......................
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2.2Component description.........................
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2.2.1Detection principle........................
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2.2.2work process..........................
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2.2.3Analyzer measurement process..................
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2.2.4Instrument installation......................
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2.2.5Computer installation......................
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2.2.6Printer installation........................
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2.2.7Installation of data communication................
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2.2.8Instrument startup (shutdown) debugging.............
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2.2.9Weigh rod adjustment......................
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Software Installation.............................
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Function Description............................
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4.1setting menu.............................
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4.2Start test menu............................
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4.3Function menu.............................
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4.4Data management menu........................
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Operating instructions...........................
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5.1Preparation for operation.......................
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5.1.1Crucible preparation.......................
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5.1.2Gas preparation.........................
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5.1.3Sample spoon..........................
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Foreword
1.1、Overview:
Thank you for purchasing our company's automatic industrial analyzer. In order to ensure that you
operate and maintain the instrument correctly, please read this manual carefully. If you have any questions,
Fully automatic industrial analyzer is a new generation of full-automatic industrial analyzer based on the
new industrial design of coal. The instrument has a variety of test methods for users to choose from. The
entire test process fully meets the national standard requirements. It can also perform fast test, customize
the heating temperature and constant temperature time, and shorten the total test time.
1.2、Performance characteristics
●Wireless transmission and sharing function, users can wirelessly transmit experimental results over long
distances. Production can be guided at any time without the need to manually copy experimental results.
●The instrument's electronic control design uses DSP technology, and the control is more real-time and
reliable. The user can easily control the sample weight and set the weighing range to make the instrument
test more accurate.
●The experiment is suspended in the middle of the experiment, and the experiment process can be
continued the next day.
●The electric push rod automatically opens the cover and lifts automatically, and adopts stepper motor
imported from South Korea to make the instrument more stable.●Automation: After putting in the sample,
you only need to give out a few mouse clicks to automatically complete the test print results and
automatically wirelessly transfer the data. The operation is simple.
●The user can set whether to use oxygen or nitrogen at any time.
●The addition of a new generation of weighing mechanism, sample delivery mechanism and heat insulation
mechanism has greatly improved the thermal stability of this product.
●New users can set whether to use open oxygen or nitrogen at any time.
●Newly added users can set the dryness check, and the user can set the check error range to improve the
instrument's higher test accuracy.
●Accurate test: After testing more than 20 standard coal samples, the results are accurate; the test
accuracy compared with the national standard method meets the requirements.
●High efficiency: rapid method: moisture, ash and volatile matter of 19 samples for 150min.
●The three indexes of moisture, ash and volatile matter can be measured arbitrarily or separately.
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●The printing function can be queried at any time during the test. Allows users to easily and statistically
analyze data during the test.
1、Ambient temperature:5℃--40℃。
2、Relative temperature:≤85%。
3、There is no strong vibration, dust, strong electromagnetic interference and corrosive gas around.
4、The user should have a suitable work surface (preferably a flat cement work surface because the
instrument cannot be shaken during the experiment) in order to place the instrument. The work
surface needs (width) 700 mm × (length) 2500 mm.
5 、 Self-prepared coal samples: air-dried coal samples with a particle size of less than 0.2 mm.
Standard coal sample.
7、power supply:220V±10%,50A。
1.4、Technical Parameters
1.4.1)Power requirements
Analyzer:220V±22V、50Hz±1Hz 、25A(maximum)、9.0kW(maximum)
monitor:220V±22V、50Hz±1Hz、 200W(maximum)
1.4.2)Gas requirements
Oxygen: 99.5% purity, pressure 0.1MPa after decompression (using self-contained air pump
1.4.3)Crucible number
1.4.4)test method
The water ash part can test 19 samples at the same time;
1.4.5)Sample quality
0.5000g~1.0000g(User-defined)
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1.4.6)Furnace temperature range
100℃~1000℃
1.4.7)Analysis accuracy
1.4.8)Dimensions
Ⅰpart605mm(L)×605mm(W)×630mm(H)
1.4.9)Weight
Analyzer:90 kg;
1.5working environment
106kPa.
1.5.2) The protective ground terminal of the power socket must be connected to the earth to ensure
1.5.3)Prepare a sturdy work surface (preferably a cement table, because the instrument cannot be
shaken during the experiment) to place the instrument. The area is about 700mm (width) x 2000 mm
(length).
1.5.4)The instrument should be placed in a laboratory without strong vibration, strong electromagnetic
1.5.5 ) User-supplied: 1 oxygen cylinder (not required if using the built-in compressor); 1 nitrogen
cylinder
The instrument is mainly composed of three parts: tester host, computer system, and
printer. (See Figure 2-1)
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monitor
High temperature furnace MCU
Balance transmiss
(Figure2-1)
2.2Component description
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6. Windshield: Used to reduce the influence of the balance sensor on airflow.
7. Bracket: Used to install and fix the electronic balance.
8. Bolts: Used to adjust the overall level of the instrument.
9. Chimney: It is used to exhaust the smoke generated during the test to the outside (external exhaust
pipe is required).
10.Heating device: used for heating in a constant temperature furnace.
11. Weighing mechanism: used to place the crucible on the weighing rod
12. Circuit breaker: used for heating circuit overcurrent protection (user-supplied).
13. Host power: used to provide power to the internal circuit board of the instrument.
14. Electric furnace power supply: used to provide heating power for high temperature furnace and
constant temperature furnace of the instrument.
balance for weighing, and weighs the sample during heating under specific atmospheric conditions,
specified temperature, and specified time. Based on this, industrial analysis indexes such as moisture, ash
The analyzer, which is tested separately, greatly improves the test efficiency on the premise of ensuring
full compliance with national standards. The PC can simultaneously control the automatic analyzer to
Enter the test program test menu, enter the relevant sample information and the instrument
automatically weighs the empty crucible.After the empty crucible is weighed, the system prompts to place
the sample, and then the system weighs the sample and starts heating the high temperature furnace(The
system will open the nitrogen valve and pass nitrogen into the high temperature furnace, and the gas flow
rate is controlled at 4 ~ 5L / min ) First heat the high temperature furnace to 107 ℃ for 45 minutes.
(According to the custom method, the temperature and constant temperature time can be customized)
Then start to weigh the crucible and perform optional inspection drying. When the crucible quality does not
exceed the system set value (recommended crucible error value is 0.0005), the moisture analysis ends.
The system reports the results of moisture measurement and closes the nitrogen valve at the same time.
The high-temperature furnace continues to increase the experimental temperature to a constant
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temperature and then heats to 900 ° C for 7 minutes. After that, the system automatically opens the lid and
cools down to the set time and temperature. After weighing the volatile matter, the system reports the
volatility measurement result and print.
In order to protect the instrument from impact, vibration, dust and corrosive gases during transportation
and storage, the instrument has been packed in accordance with relevant regulations before leaving the
factory. After the instrument arrives at the user, it must be unboxed and installed in accordance with the
following conditions:
1. Please unpack the instrument carefully, and check whether the parts are complete and damaged
according to the enclosed shipping list.
2. The instrument must not be exposed to direct sunlight.
3. The instrument must be kept at a sufficient distance from the heat source.
4. The distance between the back of the instrument and the wall must not be less than 25cm.
5. Do not place other debris on top of the instrument.
6. Connected to the power supply can withstand 20A single-phase hot wire, the ground wire needs to
be connected reliably.
7. The plane on which the instrument is installed must be level.
8. Keep away from strong air convection openings (such as windows, doorways, air conditioners).
9. The installation site must provide the power required for the instrument to work.
10.Install the balance as described in the instructions supplied with the balance.
1. After unpacking the main unit, move the main unit of the instrument to the workbench of a standard
studio with a power supply and gas supply. The workbench must be cement or ceramic, and the height
2. Open the accessory package box, remove the accessory, and place the accessory in a standard
studio (check whether all parts of the instrument (including the circuit board) are installed in the correct
position, whether the plug of the electrical control part is connected, and whether the wiring is intact,
3. Check whether all the key parts of the instrument (weighing mechanism, sample delivery mechanism,
light trough, motor, etc.) are loose. Connect the RS232 serial communication cable and power cable of
the instrument and the control computer. Before connecting, please make sure that the power of the
instrument and computer is turned off and the power cable is installed.
5. Install the test software and enter [Settings], [General Settings], [Basic Settings] to set the device port
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7. Install the sample delivery rod, the installation and position adjustment of the sample delivery rod.
8. Install the electronic balance, install and debug the electronic balance, and be careful not to damage
Install the electronic balance weighing rod. Install the weighing rod. Be careful not to damage the
The computer system in the standard configuration includes computers, monitors, and
printers. These devices can be purchased from our company or purchased by yourselves.
The computer must have an idle RS232 communication port.
3. Connect the data signal cable of the monitor and the computer.
6. Connect the keyboard cable to the keyboard connector on the back of the computer, and place the
7. Connect the mouse cable to the mouse connector on the back of the computer and place the mouse
9. Connect the power cables of the printer and the computer separately.
3. Connect the printer and computer according to the printer installation instructions.
4. 4. Install the printer on the work platform according to the printer installation instructions, and connect
all necessary cables and parts Install the printer driver according to the printer installation instructions.
This step must be performed after the printer and computer are powered on. At this time, it is not
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5. After successfully installing the printer and completing the test, power off the printer and computer.
1. Connect the communication cable between the computer and the main body of the automatic industrial
analyzer;
2. Connect the communication cable between the computer and the printer;
3. Connect the signal cable between the computer and the monitor; connect the power cord between the
4. Connect the control power of the host computer and the power of the computer and printer to the power
5. Connect the main unit heating power to the heating power socket. The heating power supply and the PC
power supply cannot be connected to the same phase of the hot wire. The host needs to use a
dedicated heating power socket separately. The socket can allow a current of not less than 20A, but
the 220V AC power socket is not connected to the heating power socket.
1.First confirm whether the instrument host, computer, monitor, and printer are connected.
2.Then power on the instrument, power on the computer and printer again, and let the built-in electronic
3.Power off the analyzer and PC before inserting the serial cable or balance signal cable! Otherwise it will
damage the analyzer, balance and PC! Before powering on the instrument, make sure that the power
cord and signal cable connectors of the balance do not touch the conductors such as the circuit board
4.The power supply must be well grounded, otherwise it will affect the normal operation of the instrument!
5.Wear clean, dry work gloves when placing samples.
6.When the analyzer is heating test, pay attention to work around the high temperature furnace! If you
touch a high-temperature furnace or crucible, you may be seriously burned. Wear work clothes, gloves,
7.When moving the analyzer, first remove the balance from the analyzer.
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2.2.9 Weigh rod adjustment
Observe whether the weighing rod is in the center of the high-temperature furnace weighing rod jack
(that is, whether it touched the high-temperature furnace body), and adjust the balance floor bolts according
to the deviation so that the weighing rod is located at the center of the high-temperature furnace weighing
rod jack and cannot touch the high-temperature furnace body.Then, run the test program in the PC and
open [System Test] under [Test]. After the turntable is reset (that is, the hole at position 0 is a positive
symmetrical rod, if it is not correct, you need to adjust the position of the turntable). Put the crucible in the
hole at position 0 of the turntable. Then click [Drop on the turntable] to observe whether the crucible is fully
lifted (that is, the outer wall of the crucible does not touch the turntable) and the balance reading is stable.
Otherwise, please adjust the height and center position of the weighing rod.The height of the weighing rod
can be adjusted by adjusting the height of the balance or the depth of the weighing rod inserted into the
weighing rod seat. When the weighing rod is not vertical, you can also adjust the center position of the
Software Installation
●Hardware requirements:
P4 2GMHz CPU、512M memory, 2 free serial ports, 40G hard disk.
●Software requirements:
Windows 2000/XP installation Excel2000。
Display method:
Can support 800 * 600, 1024 * 768, 1280 * 1024 and other resolutions. The recommended
resolution is 1024 * 768.
System installation:
Put the disk or CD into the drive, enter the "program installation disk", double-click the file "Fully
Automatic Industrial Analyzer", and then click the [Next] button in turn to complete the installation.
Click [Finish]. Restart and the computer will restart.
Function Description
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The program interface adopts the common style of Windows XP, and the main interface is divided
into a title area. These operating instructions are introduced in the order of the main menu of the
system.
(4-1)
This menu contains the following 5 sub-menus,
【General settings】
【change Password】
【System correction】
【Printing settings】
【Exit system】
set the parameters used in the system test.After you modify the settings, click the [OK] button, the program
will save the settings you just modified and exit the system settings, so that your modified settings will take
effect in the experiment.If you don't want to save the settings you just modified, just click the [Exit without
saving] button, and the program will exit without saving the settings.
1. General settings
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Set port, printing method, weighing range, detection unit, laboratory technician, auditor
There are two methods for setting water experiments: classical method and custom method."Classic
method" (applicable to arbitration): When the coal sample is moisture-tested at a constant temperature of
107 ° C for 45 minutes (the default constant-temperature time is 45 minutes; the user can customize the
constant-temperature time), weigh to the crucible constant weight,Moisture is obtained after crucible
dynamic correction."Custom" (only applicable for guidance production): When the coal sample is directly
heated to 135 ° C during moisture test, the temperature is constant for 10 minutes (the default constant
temperature time is 10 minutes; the user can customize the constant temperature time), when weighing to
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There are two methods for setting ash experiment: classical method and fast method. "Fast method" (for
arbitration) After 815 ℃, after 30 minutes of constant temperature (the default constant temperature time is
30 minutes; the user can customize the constant temperature time), When weighing to the constant weight
of the crucible, the ash content is obtained after the crucible is dynamically corrected."Custom" (only
applicable to guide production): After the coal sample is directly heated to 815 ° C during the ash test, the
temperature is constant for 30 minutes (the default constant temperature time is 30 minutes; users can
customize the constant temperature time).When weighing to the constant weight of the crucible, the ash is
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4-8
a.“Setting accuracy”
Set the difference between several consecutive weighings during the determination of moisture and ash. If
it is less than this value, it is considered to be constant weight, otherwise it will be automatically weighed
again.
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Enter standard value and measured value system to automatically correct test results
图 4-2
4.1.3 [Print Preview] menu
Preview the currently viewed data.
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4.2 [Start test] menu
1. Click [Start Experiment] to reset the system. Weigh the empty crucible. After capping, click to determine
the cap weight. The shift input is as shown in Figure (4-3). Enter “Sample Number”, “Sample Name”, Click
4-3
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(4-4)
It mainly controls the lifting of the turntable. After clicking the [Reset] button, the No. 0 position on the
turntable will be turned directly above the weighing rod, and the crucible will not fall on the weighing
rod.Click the [Dial Up] button, and the dial will move up. Click the [Dial Down] button, and the dial will move
downward. If the turntable is not in the correct position, the turntable cannot be raised and lowered.
1,Click the [Sample One by One] button, and the turntables will rotate one by one.
It is mainly to check whether the oxygen and nitrogen valves of the analyzer can be opened and closed
normally, and whether the nitrogen valves of the analyzer can be opened and closed normally.After clicking
[Oxygen valve open], the oxygen valve is opened, and the float on the panel of the water-ash measurement
part indicates the current oxygen flow rate. At the same time, the [oxygen valve open] button will turn
gray.After clicking [Oxygen Valve Off], the oxygen valve will be closed and the [Oxygen Valve On] button will
light up. The operation of the nitrogen valve is the same as that of the oxygen valve.
It is mainly to check whether hole 0 on the turntable can be reset normally.After clicking [Reset], the
turntable starts to rotate. When the 0 position on the turntable is turned directly above the weighing rod, the
turntable stops rotating, which is the default reset position of the system.
5. After debugging, click [OK] or [Cancel] to exit the hardware debugging program.
tar on the crucible wall must be ignited by burning. It can also be burned in a muffle furnace. Such as
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Set a save to appear during the experiment to save temporary data
Set to open the saved data during the experiment during the next experiment【Data upload port】
4-5
1. In the [Data Management] menu, there are [Data Preview], [Data Backup], [Data Recovery], [Export
Excel], [Coal Quality Calculator], which mainly query the test results in the current system database.[Hot
hydrogen calculation] Mainly based on the industrial analysis test results in the current system database,
and then enter the coke slag number and coal type to automatically calculate the calorific value and
hydrogen content.It is mainly to query the test results in the backup database of your choice.[Result Query]
is the same interface as [Query Backup], but [Result Query] does not need to select a database. The
current system database is the default, and [Query Backup] requires a backup database.[Data backup] is to
back up the test results of the specified date range, and delete all backed up records from the system
database at the same time.Whether it is [Result Query] or [Query Backup], the purpose is to view the
2.[Print] button
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Printing is to print all the results currently displayed (this version adds the function of printing
Operating instructions
The crucible must be clean and dry. It is recommended to wash the crucible with water and dry it in
an oven at 107 ° C for 2 hours, then put it in a desiccator to cool it. Take out the crucible and put it in
According to the requirements of 1.3, a bottle of oxygen and a bottle of nitrogen can be prepared, and
the air pipe is connected to the gas connector on the back of the analyzer (note that the oxygen and
nitrogen can not be reversed according to the label on the instrument). Adjust the pressure reducer so
that the display pressure of the low pressure gauge of the pressure reducer is 0.1 MPa.There is a flow
meter on the front panel of the analyzer to indicate the gas flow rate. The gas flow rate is 4-5 liters /
minute during the test of the instrument. There is a gas flow regulator inside the analyzer.Adjustable
gas flow (adjusted when the instrument leaves the factory),If you need to adjust the flow rate, you can
enter the “hardware debugging” menu. Open the oxygen valve and nitrogen valve respectively, and
watch the flow meter on the front panel of the analyzer. Adjust the gas flow regulator inside the
analyzer to adjust the gas flow.
This instrument is equipped with a special sample spoon. The sample spoon should be dry before use, and must
be cleaned after each use before use.
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Automatic industrial analyzer packing list
No name unit qty mark
4 Communication line pc 1
7 tweezers pc 1
8 Crucible forceps pc 1
9 Sample spoon pc 1
10 brush pc 1
11 Chimney tube pc 1
14 user's manual pc 1
15 Product certification pc 1
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