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  • Revised Manufacturing Process

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    Sanjeev Singh
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    The document outlines a 3-step manufacturing process for producing 2,4-Dichlorophenol acetic acid sodium salt that takes approximately 6 hours total. Step 1 involves reacting 2,4-Dichlorophenol with sodium hydroxide to form a sodium salt intermediate. Step 2 then reacts this intermediate with monochloroacetic acid in the presence of sodium hydroxide to form the mono hydrate product. Step 3 washes the mono hydrate to yield the pure 2,4-Dichlorophenol acetic acid sodium salt end product.

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    revised manufacturing process

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    The document outlines a 3-step manufacturing process for producing 2,4-Dichlorophenol acetic acid sodium salt that takes approximately 6 hours total. Step 1 involves reacting 2,4-Dichlorophenol with sodium hydroxide to form a sodium salt intermediate. Step 2 then reacts this intermediate with monochloroacetic acid in the presence of sodium hydroxide to form the mono hydrate product. Step 3 washes the mono hydrate to yield the pure 2,4-Dichlorophenol acetic acid sodium salt end product.

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    © All Rights Reserved
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    3 views2 pages

    Revised Manufacturing Process

    Uploaded by

    Sanjeev Singh
    The document outlines a 3-step manufacturing process for producing 2,4-Dichlorophenol acetic acid sodium salt that takes approximately 6 hours total. Step 1 involves reacting 2,4-Dichlorophenol with sodium hydroxide to form a sodium salt intermediate. Step 2 then reacts this intermediate with monochloroacetic acid in the presence of sodium hydroxide to form the mono hydrate product. Step 3 washes the mono hydrate to yield the pure 2,4-Dichlorophenol acetic acid sodium salt end product.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
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    of 2

    MANUFACTURING PROCESS

    STEP WISE MANUFACTURING PROCESS

    The product of 2,4-Dichlorophenol acetic acid sodium salt is manufactured as per below
    steps. Total time taken in whole process is about 6 hours.

    Step 1: Formation of 2,4-Dichlorophenol Sodium salt:

    2,4-Dichloro Phenol react with Sodium Hydroxide and form 2,4-Dichloro phenol sodium salt.
    This step takes about 2 hours to complete.

    ONa
    OH

    Cl Cl
    + H 2O
    + NaOH

    Cl
    Cl

    2,4-Dichloro phenol sodium salt


    2,4-dichlorophenol
    Step 2: Formation of 2,4-Dichlorophenol acetic acid sodium salt mono hydrate:

    2,4-Dichloro phenol sodium salt react with monochloro acetic acid in presence of sodium
    hydroxide formed 2,4-Dichlorophenol acetic acid sodium salt mono hydrate. This step takes
    about 3 hours

    OCH 2COONa
    ONa
    Cl
    Cl
    + ClCH 2COOH + NaOH + NaCl + H 2O

    Monochloro acetic acid


    Cl
    Cl 2,4-Dichlorophenol acetic acid
    sodium salt mono hydrate

    Step 3: Formation of 2,4-Dichlorophenol acetic acid sodium salt:

    2,4-Dichlorophenol acetic acid sodium salt mono hydrate is washed and pure 2,4-
    Dichlorophenol acetic acid sodium salt received. This step takes about 1 hour.

    Total Time requirement: 6 Hours

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