Saved Recs

FN Clarivate Analytics Web of Science
VR 1.0
PT J
AU Moskalyk, RR
Alfantazi, AM
AF Moskalyk, RR
Alfantazi, AM
TI Processing of vanadium: a review
SO MINERALS ENGINEERING
LA English
DT Review
DE extractive metallurgy; hydrometallurgy; non-ferrous metallic ores;
minerals economicas
AB Vanadium is an important by-product that is used almost exclusively in ferrous
and non-ferrous alloys due to its physical properties such as high tensile
strength, hardness, and fatique resistance. Vanadium consumption in the iron and
steel industry represents about 85% of the vanadium-bearing products produced
worldwide. The ubiquitous vanadium is employed in a wide range of alloys in
combination with iron, titanium, nickel, aluminum, chromium, and other metals for a
diverse range of commercial applications extending from train rails, tool steels,
catalysts, to aerospace. The global supply of vanadium originates from primary
sources such as ore feedstock, concentrates, metallurgical slags, and petroleum
residues. Vanadium-bearing host minerals consist of carnotite, mottramite,
patronite, roscoelite, and vanadinite. Deposits of titaniferous magnetite,
uraniferous sandstone, bauxite, phosphate rock, crude oils, oil shale and tar sands
host vanadium. Apart from titanomagnetite and ilmenite ore deposits containing
vanadium, slags from the ferrous industry are a major source of supply. At present,
known world reserves are expected to supply the next century's needs. Vanadium-
bearing materials are treated by means of several processes such as calcium
reduction, roast/leach, solvent extraction and ion exchange to recover vanadium
either as metal, ferrovanadium, vanadium pentoxide, or in the form of various
chemicals. The recovery of aluminum and magnesium metal from smelters and
refineries generates vanadium and associated compounds. Countries such as China,
South Africa, and Russia are the largest world producers of ferrovanadium and its
toxic oxides while about 40 other countries contribute smaller quantities in
different forms for global consumption. Australia is poised to become a major
player for this essential substance during the next decade. The supply and demand
of vanadium products during the past 20 years has been relatively stable and
subject to a gradual decline in delivered price. The paper describes established
industrial processes for recovery of vanadium from sources such as raw ore and
process reverts. The comprehensive condensation of pertinent facts is intended to
provide a single reference source rather than the reader perusing many articles.
(C) 2003 Elsevier Ltd. All rights reserved.
C1 Univ British Columbia, Dept Met & Mat Engn, Vancouver, BC V6T 1Z4, Canada.
Nord Met Consultants Inc, Sudbury, ON P3E 5Y7, Canada.
C3 University of British Columbia
RP Alfantazi, AM (corresponding author), Univ British Columbia, Dept Met & Mat
Engn, 309-6350 Stores Rd, Vancouver, BC V6T 1Z4, Canada.
OI alfantazi, akram/0000-0002-4039-5110
CR *ACTED CONS, 2003, VAN PENT FERR
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NR 45
TC 688
Z9 789
U1 6
U2 388
PU PERGAMON-ELSEVIER SCIENCE LTD
PI OXFORD
PA THE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, ENGLAND
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD SEP
PY 2003
VL 16
IS 9
BP 793
EP 805
DI 10.1016/S0892-6875(03)00213-9
PG 13
WC Engineering, Chemical; Mineralogy; Mining & Mineral Processing
WE Science Citation Index Expanded (SCI-EXPANDED)
SC Engineering; Mineralogy; Mining & Mineral Processing
GA 711QF
UT WOS:000184752000002
DA 2023-12-05
ER
PT J
AU Ben Haha, M
Le Saout, G
Winnefeld, F
Lothenbach, B
AF Ben Haha, M.
Le Saout, G.
Winnefeld, F.
Lothenbach, B.
TI Influence of activator type on hydration kinetics, hydrate assemblage
and microstructural development of alkali activated blast-furnace slags
SO CEMENT AND CONCRETE RESEARCH
LA English
DT Article
DE Alkali Activated Cement; Microstructure; Calcium-Silicate-Hydrate
(C-S-H); Image Analysis; Mechanical Properties
ID CALCIUM SILICATE HYDRATE; C-S-H; PORTLAND-CEMENT; MECHANICAL-PROPERTIES;
STRENGTH BEHAVIOR; PORE SOLUTION; PASTES; PRODUCTS; GEL; QUANTIFICATION
AB The hydration of two slags with different Al(2)O(3) contents activated with
sodium hydroxide and hydrous sodium metasilicate (commonly named water glass) is
studied using a multi-method approach. In all systems, C-S-H incorporating
aluminium and a hydrotalcite-like phase with Mg/Al ratio similar to 2 are the main
hydration products. The C-S-H gels present in NaOH activated pastes are more
crystalline and contain less water; a calcium silicate hydrate (C-S-H) and a sodium
rich C-N-S-H with a similar Ca content are observed at longer hydration times. The
activation using NaOH results in high early strength, but strength at 7 days and
longer is lower than for the sodium metasilicate systems. The drastic difference in
C-S-H structure leads to a coarser capillary porosity and to lower compressive
strength for the NaOH activated than for the sodium metasilicate activated slags at
the same degree of slag reaction. (C) 2010 Elsevier Ltd. All rights reserved.
C1 [Ben Haha, M.; Le Saout, G.; Winnefeld, F.; Lothenbach, B.] Empa, Swiss Fed Labs
Mat Sci & Technol, Lab Concrete & Construct Chem, CH-8600 Dubendorf, Switzerland.
C3 Swiss Federal Institutes of Technology Domain; Swiss Federal
Laboratories for Materials Science & Technology (EMPA)
RP Ben Haha, M (corresponding author), Empa, Swiss Fed Labs Mat Sci & Technol, Lab
Concrete & Construct Chem, Ueberlandstr 129, CH-8600 Dubendorf, Switzerland.
EM mohsen.ben-haha@empa.ch
RI Le Saout, Gwenn/H-9886-2019; Ben Haha, Mohsen/AAC-4859-2020; Winnefeld,
Frank/B-5335-2009; Lothenbach, Barbara/C-6275-2013
OI Le Saout, Gwenn/0000-0002-2761-0584; Ben Haha,
Mohsen/0000-0001-7570-326X; Winnefeld, Frank/0000-0002-6864-6196;
Lothenbach, Barbara/0000-0002-9020-6488
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NR 46
TC 618
Z9 657
U1 19
U2 249
PI OXFORD
SN 0008-8846
J9 CEMENT CONCRETE RES
JI Cem. Concr. Res.
PD MAR
PY 2011
VL 41
IS 3
BP 301
EP 310
DI 10.1016/j.cemconres.2010.11.016
PG 10
WC Construction & Building Technology; Materials Science, Multidisciplinary
SC Construction & Building Technology; Materials Science
GA 742FI
UT WOS:000288926300011
DA 2023-12-05
ER
PT J
AU Winnefeld, F
Lothenbach, B
AF Winnefeld, Frank
Lothenbach, Barbara
TI Hydration of calcium sulfoaluminate cements - Experimental findings and
thermodynamic modelling
LA English
DT Article
DE Calcium sulfoaluminate cement; Hydration products; Pore solution;
Thermodynamic modeling
ID BELITE CEMENT; PORTLAND-CEMENT; BEHAVIOR; SYSTEM; PASTES; PHASE; SLAG;
ASH
AB Calcium sulfoaluminate cements (CSA) are a promising low-CO2 alternative to
ordinary Portland cements and are as well of interest concerning their use as
binder for waste encapsulation. In this study, the hydration of two CSA cements has
been investigated experimentally and by thermodynamic modelling between 1 h and 28
days at w/c ratios of 0.72 and 0.80, respectively.
The main hydration product of CSA is ettringite, which precipitates together
with amorphous Al(OH)(3) until the calcium sulfate is consumed after around 1-2
days of hydration. Afterwards, monosulfate is formed. In the presence of belite,
stratlingite occurs as an additional hydration product. The pore solution analysis
reveals that stratlingite can bind a part of the potassium ions, which are released
by the clinker minerals. The microstructure of both cements is quite dense even
after 16 h of hydration, with not much pore space available at a sample age of 28
days.
The pore solution of both cements is dominated during the first hours of
hydration by potassium, sodium, calcium, aluminium and sulfate; the pH is around
10-11. When the calcium sulfate is depleted, the sulfate concentration drops by a
factor of 10. This increases pH to around 12.5-12.8.
Based on the experimental data, a thermodynamic hydration model for CSA cements
based on cement composition, hydration kinetics of clinker phases and calculations
of thermodynamic equilibria by geochemical speciation has been established. The
modelled phase development with ongoing hydration agrees well with the experimental
findings. (C) 2009 Elsevier Ltd. All rights reserved.
C1 [Winnefeld, Frank; Lothenbach, Barbara] Empa, Swiss Fed Labs Mat Testing & Res,
Lab Concrete & Construct Chem, Dubendorf, Switzerland.
RP Winnefeld, F (corresponding author), Empa, Swiss Fed Labs Mat Testing & Res, Lab
Concrete & Construct Chem, Dubendorf, Switzerland.
EM Frank.Winnefeld@empa.ch
RI Lothenbach, Barbara/C-6275-2013; Winnefeld, Frank/B-5335-2009
OI Lothenbach, Barbara/0000-0002-9020-6488; Winnefeld,
Frank/0000-0002-6864-6196
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NR 43
TC 531
Z9 569
U1 13
U2 242
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD AUG
PY 2010
VL 40
IS 8
BP 1239
EP 1247
DI 10.1016/j.cemconres.2009.08.014
PG 9
GA 632XP
UT WOS:000280463200010
DA 2023-12-05
ER
PT J
AU Puertas, F
Palacios, M
Manzano, H
Dolado, JS
Rico, A
Rodríguez, J
AF Puertas, F.
Palacios, M.
Manzano, H.
Dolado, J. S.
Rico, A.
Rodriguez, J.
TI A model for the C-A-S-H gel formed in alkali-activated slag cements
SO JOURNAL OF THE EUROPEAN CERAMIC SOCIETY
LA English
DT Article
DE Microstructure-final; Spectroscopy; Mechanical properties; Atomistic
modelling; Cements
ID ALUMINUM INCORPORATION; ELASTIC PROPERTIES; MAS NMR; CALCIUM; AL-27;
SIMULATION; RESISTANCE; CONCRETE; MORTARS; CARBONATION
AB For first time, an experimental and computational study has been conducted to
define a structural model for the C-A-S-H gel forming in alkali-activated slag
(AAS) pastes that would account for the mechanical properties of these materials.
The study involved a comparison with the C-S-H gel forming in a Portland cement
paste.
The structure of the C-A-S-H gels in AAS pastes depends on the nature of the
alkali activator. When the activator is a NaOH, the structure of the C-S-H gel
falls in between tobermorite 1.4 nm with a mean chain length of five, and
tobermorite 1.1 nm with a mean length of 14. When waterglass is the activator the
structure of the C-A-S-H gel is indicative of the co-existence of tobermorite 1.4
nm with a chain length of 11 and tobermorite 1.1 nm with a chain length of 14. This
very densely packed structure gives rise to excellent mechanical properties. (C)
2011 Elsevier Ltd. All rights reserved.
C1 [Puertas, F.] Inst Ciencias Construcc Eduardo Torroja IETcc CSI, Madrid, Spain.
[Palacios, M.] Inst Bldg Mat ETH Zurich, Zurich, Switzerland.
[Manzano, H.; Dolado, J. S.] Labein Tecnalia, Bilbao, Spain.
[Manzano, H.] MIT, Cambridge, MA 02139 USA.
[Rico, A.; Rodriguez, J.] Univ Rey Juan Carlos, Madrid, Spain.
C3 Consejo Superior de Investigaciones Cientificas (CSIC); CSIC - Instituto
de Ciencias de la Construccion Eduardo Torroja (IETCC); Massachusetts
Institute of Technology (MIT); Universidad Rey Juan Carlos
RP Puertas, F (corresponding author), Inst Ciencias Construcc Eduardo Torroja IETcc
CSI, Madrid, Spain.
EM puertasf@ietcc.csic.es
RI Manzano, Hegoi/A-2984-2010; Dolado, Jorge S/Q-1815-2016; Dolado, Jorge
Sanchez/ABF-9005-2020; Puertas, Francisca/F-5366-2016; Palacios,
Marta/K-3699-2016; Pérez, Jesús Rodríguez/F-2402-2012
OI Manzano, Hegoi/0000-0001-7992-2718; Dolado, Jorge S/0000-0003-3686-1438;
Dolado, Jorge Sanchez/0000-0003-3686-1438; Puertas,
Francisca/0000-0002-4215-0184; Palacios, Marta/0000-0001-5004-128X;
Pérez, Jesús Rodríguez/0000-0002-0269-1189; Rico,
Alvaro/0000-0002-0015-5761
FU European Union [NMP3-SL-2008-214030]; Spanish Ministry of Science and
Innovation [BIA2007-61380]; Spanish National Research Council; Basque
Government through Education, University and Research Department
FX This research was funded by the European Union under contract
NMP3-SL-2008-214030 and the Spanish Ministry of Science and Innovation
under project BIA2007-61380. M. Palacios participated under a
postdoctoral contract awarded by the Spanish National Research Council.
H. Manzano acknowledges the grant received from the Basque Government
through the "Improvement of Research Staff" program of the Education,
University and Research Department.
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NR 48
TC 508
Z9 541
U1 15
U2 213
PU ELSEVIER SCI LTD
PI OXFORD
PA THE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD OX5 1GB, OXON, ENGLAND
SN 0955-2219
EI 1873-619X
J9 J EUR CERAM SOC
JI J. Eur. Ceram. Soc.
PD OCT 15
PY 2011
VL 31
IS 12
BP 2043
EP 2056
DI 10.1016/j.jeurceramsoc.2011.04.036
PG 14
WC Materials Science, Ceramics
SC Materials Science
GA 791LS
UT WOS:000292667300003
DA 2023-12-05
ER
PT J
AU Bernal, SA
Provis, JL
Walkley, B
Nicolas, RS
Gehman, JD
Brice, DG
Kilcullen, AR
Duxson, P
van Deventer, JSJ
AF Bernal, Susan A.
Provis, John L.
Walkley, Brant
Nicolas, Rackel San
Gehman, John D.
Brice, David G.
Kilcullen, Adam R.
Duxson, Peter
van Deventer, Jannie S. J.
TI Gel nanostructure in alkali-activated binders based on slag and fly ash,
and effects of accelerated carbonation
LA English
DT Article
DE Alkali activated cements (D); Granulated blast-furnace slag (D); Fly ash
(D); Carbonation (C); NMR spectroscopy
ID C-S-H; BLAST-FURNACE SLAG; AL-27 MAS-NMR; HYDRATED PORTLAND CEMENTS;
THERMAL-DECOMPOSITION; SODIUM-CARBONATE; ALUMINUM INCORPORATION; PART I;
SI-29; CONCRETE
AB Binders formed through alkali-activation of slags and fly ashes, including 'fly
ash geopolymers', provide appealing properties as binders for low-emissions
concrete production. However, the changes in pH and pore solution chemistry induced
during accelerated carbonation testing provide unrealistically low predictions of
in-service carbonation resistance. The aluminosilicate gel remaining in an alkali-
activated slag system after accelerated carbonation is highly polymerised,
consistent with a decalcification mechanism, while fly ash-based binders mainly
carbonate through precipitation of alkali salts (bicarbonates at elevated CO2
concentrations, or carbonates under natural exposure) from the pore solution, with
little change in the binder gel identifiable by nuclear magnetic resonance
spectroscopy. In activated fly ash/slag blends, two distinct gels (C-A-S-H and N-A-
S-H) are formed; under accelerated carbonation, the N-A-S-H gel behaves comparably
to fly ash-based systems, while the C-A-S-H gel is decalcified similarly to alkali-
activated slag. This provides new scope for durability optimisation, and for
developing appropriate testing methodologies. (C) 2013 Elsevier Ltd. All rights
reserved.
C1 [Bernal, Susan A.; Provis, John L.; Walkley, Brant; Nicolas, Rackel San; Brice,
David G.; Kilcullen, Adam R.; van Deventer, Jannie S. J.] Univ Melbourne, Dept Chem
& Biomol Engn, Melbourne, Vic 3010, Australia.
[Bernal, Susan A.; Provis, John L.] Univ Sheffield, Dept Mat Sci & Engn,
Sheffield S1 3JD, S Yorkshire, England.
[Gehman, John D.] Univ Melbourne, Sch Chem, Melbourne, Vic 3010, Australia.
[Gehman, John D.] Univ Melbourne, Inst Bio21, Melbourne, Vic 3010, Australia.
[Brice, David G.; Kilcullen, Adam R.; Duxson, Peter; van Deventer, Jannie S. J.]
Zeobond Pty Ltd, Docklands, Vic 8012, Australia.
C3 University of Melbourne; University of Sheffield; University of
Melbourne; University of Melbourne
RP Bernal, SA (corresponding author), Univ Sheffield, Dept Mat Sci & Engn,
EM s.bernal@sheffield.ac.uk; j.provis@sheffield.ac.uk
RI San Nicolas, Rackel RSN/F-2882-2015; Provis, John/AAR-3260-2020; Bernal,
Susan A/E-8938-2011; Provis, John L/A-7631-2008
OI San Nicolas, Rackel RSN/0000-0002-7866-630X; Provis,
John/0000-0003-3372-8922; Provis, John L/0000-0003-3372-8922; Bernal,
Susan A/0000-0002-9647-3106; Walkley, Brant/0000-0003-1069-1362; Gehman,
John D/0000-0002-2599-6292
FU Australian Research Council, through a Linkage Project co-sponsored by
Zeobond Pty Ltd; Particulate Fluids Processing Centre
FX This work has been funded by the Australian Research Council, through a
Linkage Project co-sponsored by Zeobond Pty Ltd, and also including
partial funding through the Particulate Fluids Processing Centre. We
also wish to acknowledge the Advanced Microscopy Facility at The
University of Melbourne for assistance with the electron microscopy
experiments conducted in this study, particularly Mr. Roger Curtain in
the use of the Micro-Analysis facilities.
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NR 78
TC 504
Z9 535
U1 47
U2 327
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD NOV
PY 2013
VL 53
BP 127
EP 144
DI 10.1016/j.cemconres.2013.06.007
PG 18
GA 288GJ
UT WOS:000329599700014
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Bernal, SA
Provis, JL
Rose, V
de Gutierrez, RM
AF Bernal, Susan A.
Provis, John L.
Rose, Volker
Mejia de Gutierrez, Ruby
TI Evolution of binder structure in sodium silicate-activated
slag-metakaolin blends
SO CEMENT & CONCRETE COMPOSITES
LA English
DT Article
DE Alkali-activated slag; Metakaolin; Silicate modulus; Structural
evolution; High-resolution X-ray diffraction
ID BLAST-FURNACE SLAG; C-S-H; ALKALINE ACTIVATION; HYDRATION PRODUCTS;
CALCIUM HYDROXIDE; CEMENT; GEL; MICROANALYSIS; TEMPERATURE; KAOLINITE
AB Structural evolution in pastes produced from alkali silicate-activated
granulated blast furnace slag (GBFS)/metakaolin (MK) blends is assessed. In the
initial period of the reaction, the addition of MK leads to an increase in the
total setting time, reduces the heat release, and affects the reaction mechanism by
introduction of a large quantity of additional Al. This effect is more significant
when an activating solution with a higher silicate modulus is used, and leads to a
slight reduction in the final mechanical strength of mortars but a significant
increase in setting time, which is valuable in the development of alkali-activated
slag binders as these are known to sometimes harden more rapidly than is desirable.
High-energy synchrotron X-ray diffractometry reveals that the main reaction
products in alkali-activated GBFS/MK blends are segregated and partially
crystalline calcium silicate hydrate and aluminosilicate phases, including a small
component with a zeolitic (gismondine) structure. No hydrotalcite-type phases are
observed in these samples, which are synthesized from a low-Mg slag. A secondary
reaction product (Na-substituted C-S-H) is also identified in pastes activated with
a modulus of solution of 2.0. Infrared spectroscopy carried out over a period of
180 days shows the development of the gel structure, with aluminum incorporation
leading to an increase in the extent of crosslinking, and higher alkalinity giving
a more depolymerized gel structure. (C) 2010 Elsevier Ltd. All rights reserved.
C1 [Bernal, Susan A.; Mejia de Gutierrez, Ruby] Univ Valle, CENM, Composite Mat
Croup, Dept Mat Engn, Cali, Colombia.
[Provis, John L.] Univ Melbourne, Dept Chem & Biomol Engn, Melbourne, Vic 3010,
Australia.
[Rose, Volker] Argonne Natl Lab, Adv Photon Source, Argonne, IL 60439 USA.
C3 Universidad del Valle; University of Melbourne; United States Department
of Energy (DOE); Argonne National Laboratory
RP Bernal, SA (corresponding author), Aarhus Univ, Dept Chem, Instrument Ctr Solid
State NMR Spect, Langelandsgade 140, DK-8000 Aarhus C, Denmark.
EM susana.bernal@gmail.com; jprovis@unimelb.edu.au
RI Rose, Volker/B-1103-2008; Bernal, Susan A/E-8938-2011; Provis,
John/AAR-3260-2020; Provis, John L/A-7631-2008
OI Rose, Volker/0000-0002-9027-1052; Provis, John/0000-0003-3372-8922;
Provis, John L/0000-0003-3372-8922; Bernal, Susan A/0000-0002-9647-3106;
MEJIA DE GUTIERREZ, RUBY/0000-0002-5404-2738
FU Universidad del Valle (Colombia); Instituto Colombian para el Desarrollo
de la Ciencia y Tecnologia "Francisco Jose de Caldas" (COLCIENCIAS);
Centre of Excellence of Novel Materials (CENM); US Department of Energy,
Office of Science, Office of Basic Energy Sciences [DE-AC02-06CH11357];
Australian Research Council (ARC) through the Particulate Fluids
Processing Centre
FX This study was sponsored by Universidad del Valle (Colombia), Instituto
Colombian para el Desarrollo de la Ciencia y Tecnologia "Francisco Jose
de Caldas" (COLCIENCIAS) and the Centre of Excellence of Novel Materials
(CENM). Use of the Advanced Photon Source at Argonne National Laboratory
was supported by the US Department of Energy, Office of Science, Office
of Basic Energy Sciences, under Contract No. DE-AC02-06CH11357. The
participation of JLP was funded by the Australian Research Council
(ARC), including partial funding through the Particulate Fluids
Processing Centre, a Special Research Centre of the ARC.
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NR 58
TC 448
Z9 480
U1 14
U2 153
PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
J9 CEMENT CONCRETE COMP
JI Cem. Concr. Compos.
PD JAN
PY 2011
VL 33
IS 1
BP 46
EP 54
DI 10.1016/j.cemconcomp.2010.09.004
PG 9
WC Construction & Building Technology; Materials Science, Composites
GA 693ML
UT WOS:000285228100006
DA 2023-12-05
ER
PT J
AU Yip, CK
Lukey, GC
Provis, JL
van Deventer, JSJ
AF Yip, Christina K.
Lukey, Grant C.
Provis, John L.
TI Effect of calcium silicate sources on geopolymerisation
LA English
DT Article
DE geopolymer; microstructure; characterisation; mechanical properties;
metakaolin
ID ASH-BASED GEOPOLYMERS; ALKALINE ACTIVATION; METAKAOLIN; HYDROXIDE;
CEMENTS; GEL; PERFORMANCE; MIXTURES; PRODUCTS; ALUMINUM
AB Seven different calcium silicate materials were used to investigate the role of
calcium in geopolymerisation. At low alkalinity, the compressive strength of
matrices prepared with predominantly amorphous calcium silicates (blast furnace
slag) or containing crystalline phases specifically manufactured for reactivity
(cement) is much higher than when the calcium is supplied as crystalline silicate
minerals. The compressive strength of matrices containing natural (crystalline)
calcium silicates improves with increasing alkalinity, however the opposite trend
is observed in matrices synthesised with processed calcium silicate sources. The
difference in compressive strength between matrices synthesised using different
calcium silicate sources is significantly reduced at high alkalinity. An
insufficient amount of calcium is dissolved from crystalline calcium silicates at
relatively low alkalinity to enable formation of calcium silicate hydrate in
coexistence with the aluminosilicate geopolymeric gel, and this leads to the poor
mechanical properties of such matrices. At high alkalinity, calcium plays a lesser
role in affecting the nature of the final binder, as it forms precipitates rather
than hydrated gels. Thus, the different calcium silicate sources will not have a
major impact on the mechanical properties of these matrices. The effects of
different calcium silicates on geopolymerisation are therefore seen to depend most
significantly on two factors: the crystallinity of the calcium silicate source, and
the alkalinity of the activating solution used. (C) 2007 Elsevier Ltd. All rights
reserved.
C1 [Yip, Christina K.; Lukey, Grant C.; Provis, John L.; van Deventer, Jannie S.
J.] Univ Melbourne, Dept Chem & Biomol Engn, Melbourne, Vic 3010, Australia.
C3 University of Melbourne
RP van Deventer, JSJ (corresponding author), Univ Melbourne, Dept Chem & Biomol
Engn, Melbourne, Vic 3010, Australia.
EM jannie@unimelb.edu.au
RI Provis, John/AAR-3260-2020; Provis, John L/A-7631-2008
OI Provis, John/0000-0003-3372-8922; Provis, John L/0000-0003-3372-8922
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10.1016/j.cemconres.2004.10.042
NR 33
TC 403
Z9 446
U1 11
U2 124
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD APR
PY 2008
VL 38
IS 4
BP 554
EP 564
DI 10.1016/j.cemconres.2007.11.001
PG 11
GA 286BF
UT WOS:000254819600014
DA 2023-12-05
ER
PT J
AU Sakadevan, K
Bavor, HJ
AF Sakadevan, K
Bavor, HJ
TI Phosphate adsorption characteristics of soils, slags and zeolite to be
used as substrates in constructed wetland systems
SO WATER RESEARCH
LA English
DT Article
DE wastewater; phosphorus; adsorption; Freundlich; Langmuir; slags; zeolite
ID PHOSPHORUS REMOVAL; SORPTION; CLAY; PH
AB Constructed wetlands are used to remove pollutants from wastewater. The
performance of such wetlands to remove pollutants from wastewater can be improved
by using suitable substrates. In this study the phosphorus (P) adsorption
capacities of soils, two industrial by-products and a clinoptilolite material
(zeolite) were examined for their potential use as substrates to remove P in
constructed wetlands. Both Freundlich and Langmuir adsorption isotherms were used
to describe the adsorption characteristics of these substrates. The Langmuir
adsorption isotherm was used to calculate the maximum P adsorption capacity of
these substrates. One of the industrial by-products, namely blast furnace slag,
showed the highest P adsorption capacity (44.2 g P kg(-1) slag) followed by soil
samples collected from an operating (Byron Bay) constructed wetland system in
Northern NSW (4.2 to 5.2 g P kg(-1) soil). The surface soils collected from two
regional constructed wetland systems were found to have the least P adsorption
capacity (1153 and 934 mg P kg(-1) soil, respectively for Richmond and Carcoar
wetlands). The clinoptilolite material (zeolite), which is used to remove ammonium
ion from wastewater, was found to have a P adsorption capacity of 2.15 g kg(-1).
The relationship between P adsorption and oxalate extractable iron (Fe) and
aluminium (Al) showed that P adsorption related more closely to extractable Al
(r(2) = 0.890) than Fe (r(2) = 0.736). Multiple regression analysis showed that P
adsorption is more closely related to a combination of both oxalate extractable Fe
and Al (r(2) = 0.901) than extractable Fe or Al alone. The P saturation capacity of
wetland systems incorporating these substrates is described. The results suggest
that selected industrial by-products and adsorptive materials may be used alone or
in combination with soils to improve the performance of constructed wetland systems
subject to other properties Such as pH, permeability and structural stability of
these materials. (C) 1998 Elsevier Science Ltd. All rights reserved.
C1 Univ Western Sydney Hawkesbury, Water Res Lab, Richmond, NSW 2753, Australia.
C3 Western Sydney University
RP Sakadevan, K (corresponding author), Univ Western Sydney Hawkesbury, Water Res
Lab, Richmond, NSW 2753, Australia.
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NR 37
TC 399
Z9 584
U1 3
U2 300
PI OXFORD
SN 0043-1354
EI 1879-2448
J9 WATER RES
JI Water Res.
PD FEB
PY 1998
VL 32
IS 2
BP 393
EP 399
DI 10.1016/S0043-1354(97)00271-6
PG 7
WC Engineering, Environmental; Environmental Sciences; Water Resources
SC Engineering; Environmental Sciences & Ecology; Water Resources
GA YR551
UT WOS:000071506600013
DA 2023-12-05
ER
PT J
AU Lecomte, I
Henrist, C
Liégeois, M
Maseri, F
Rulmont, A
Cloots, R
AF Lecomte, I.
Henrist, C.
Liegeois, M.
Maseri, F.
Rulmont, A.
Cloots, R.
TI (Micro)-structural comparison between geopolymers, alkali-activated slag
cement and Portland cement
LA English
DT Article
DE electron microscopy; microstructure-final; spectroscopy; X-ray methods;
cements; geopolymers
ID C-S-H; AL-27 NMR; SI-29; PASTES; ALUMINOSILICATE; SPECTROSCOPY;
ALUMINUM; PHASES; FTIR
AB Concurrently to research conducted on ordinary Portland cement (PC), new types
of binders were developed during the last decades. These are formed by alkali-
activation of metakaolin or ground-granulated blast furnace slag (GGBFS) and are
named, respectively, geopolymers (GP) or alkali-activated slag (AAS). Four
different cementitious materials were synthesised: PC, AAS, GP, and a mix GP-AAS
and fully compared about their compositions and (micro)-structures.
X-ray diffraction has revealed the presence of semi-crystalline C-S-H gel
binding phase in PC while AAS, GP and GP-AAS are nearly amorphous. Progressive
structural changes have been observed between the different samples by means of
infrared spectroscopy, Si-29 and At-27 magic-angle-spinning nuclear magnetic
resonance spectroscopy: there is a polymerisation extent of the (alumino)-silicate
framework from PC [SiQ(1) and SiQ(2) units] to AAS [SiQ(2) and SiQ(2)(1Al) units]
and finally to GP [SiQ(4)(2Al) and SiQ(4)(3Al) units]. Scanning electron microscopy
has shown that GP is a homogeneous matrix while the other materials are composites
containing GGBFS grains surrounded by a binding matrix. Energy dispersive X-ray EDX
analyses (line scans) have shown the absence of formation of any specific phase at
the matrix-grains interfaces. (c) 2006 Elsevier Ltd. All rights reserved.
C1 Univ Liege, Dept Chem, SUPRATECS, LCIS,Dept Chem,Chem Inst B6, B-4000 Cointe
Ougree, Belgium.
Arcelor Innovat, Construct Steel Design Ctr, B-4000 Cointe Ougree, Belgium.
C3 University of Liege; ArcelorMittal
RP Lecomte, I (corresponding author), Univ Liege, Dept Chem, SUPRATECS, LCIS,Dept
Chem,Chem Inst B6, B-4000 Cointe Ougree, Belgium.
EM I.Lecomte@ulg.ac.be
OI CLOOTS, Rudi/0000-0002-2648-0407
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6
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3
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0
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8846(01)00530-0
9
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NR 25
TC 357
Z9 382
U1 9
U2 99
PU ELSEVIER SCI LTD
PI OXFORD
SN 0955-2219
EI 1873-619X
J9 J EUR CERAM SOC
PY 2006
VL 26
IS 16
BP 3789
EP 3797
PG 9
GA 102VL
UT WOS:000241841300037
OA Green Published
DA 2023-12-05
ER
PT J
AU Myers, RJ
Bernal, SA
San Nicolas, R
Provis, JL
AF Myers, Rupert J.
Bernal, Susan A.
San Nicolas, Rackel
Provis, John L.
TI Generalized Structural Description of Calcium-Sodium Aluminosilicate
Hydrate Gels: The Cross-Linked Substituted Tobermorite Model
SO LANGMUIR
LA English
DT Article
ID C-S-H; BLAST-FURNACE SLAG; HIGH-RESOLUTION NMR; ACTIVATED SLAG; ALUMINUM
INCORPORATION; TRICALCIUM SILICATE; PORTLAND-CEMENT; REAL STRUCTURE; OD
CHARACTER; PART I
AB Structural models for the primary strength and durability-giving reaction
product in modern cements, a calcium (alumino)silicate hydrate gel, have previously
been based solely on non-cross-linked tobermorite structures. However, recent
experimental studies of laboratory-synthesized and alkali-activated slag (AAS)
binders have indicated that the calcium sodium aluminosilicate hydrate [C-(N)-A-S-
H] gel formed in these systems can be significantly cross-linked. Here, we propose
a model that describes the C-(N)-A-S-H gel as a mixture of cross-linked and non-
crosslinked tobermorite-based structures (the cross-linked substituted tobermorite
model, CSTM), which can more appropriately describe the spectroscopic and density
information available for this material Analysis of the phase assemblage and Al
coordination environments of AAS binders shows that it is not possible to fully
account for the chemistry of AAS by use of the assumption that all of the
tetrahedral Al is present in a tobermorite-type C-(N)-A-S-H gel, due to the
structural constraints of the gel. Application of the CSTM can for the first time
reconcile this information, indicating the presence of an additional activation
product that contains highly connected four-coordinated silicate and aluminate
species. The CSTM therefore provides a more advanced description of the chemistry
and structure of calcium sodium aluminosilicate gel structures than that previously
established in the literature.
C1 [Myers, Rupert J.; Bernal, Susan A.; Provis, John L.] Univ Sheffield, Dept Mat
Sci & Engn, Sheffield S1 3JD, S Yorkshire, England.
[Myers, Rupert J.; Bernal, Susan A.; San Nicolas, Rackel; Provis, John L.] Univ
Melbourne, Dept Chem & Biomol Engn, Melbourne, Vic 3010, Australia.
C3 University of Sheffield; University of Melbourne
RP Provis, JL (corresponding author), Univ Sheffield, Dept Mat Sci & Engn, Sir
Robert Hadfield Bldg,Mappin St, Sheffield S1 3JD, S Yorkshire, England.
EM jprovis@sheffield.ac.uk
RI Provis, John L/A-7631-2008; Provis, John/AAR-3260-2020; Bernal, Susan
A/E-8938-2011; Myers, Rupert Jacob/H-8449-2019; San Nicolas, Rackel
RSN/F-2882-2015
OI Provis, John L/0000-0003-3372-8922; Provis, John/0000-0003-3372-8922;
Myers, Rupert Jacob/0000-0001-6097-2088; San Nicolas, Rackel
RSN/0000-0002-7866-630X; Bernal, Susan A/0000-0002-9647-3106
FU Australian Research Council (ARC); Zeobond Pty Ltd.; University of
Sheffield; Particulate Fluids Processing Centre, a Special Research
Centre of the ARC
FX This work was funded in part by the Australian Research Council (ARC),
including support through a Linkage Project cofunded by Zeobond Pty Ltd.
and through the Particulate Fluids Processing Centre, a Special Research
Centre of the ARC. We thank Dr. John Gehman (Bio21 Institute/School of
Chemistry, University of Melbourne) for useful discussions and
assistance with NMR spectroscopy and data processing, and Mr. Roger
Curtain (Bio21 Institute, University of Melbourne) and the Electron
Microscopy Unit for assistance with the SEM work. Funding support
provided by the University of Sheffield is also gratefully acknowledged.
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8846(93)90143-W
8846(94)90002-7
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NR 58
TC 322
Z9 339
U1 13
U2 178
PU AMER CHEMICAL SOC
PI WASHINGTON
PA 1155 16TH ST, NW, WASHINGTON, DC 20036 USA
SN 0743-7463
J9 LANGMUIR
JI Langmuir
PD APR 30
PY 2013
VL 29
IS 17
BP 5294
EP 5306
DI 10.1021/la4000473
PG 13
WC Chemistry, Multidisciplinary; Chemistry, Physical; Materials Science,
Multidisciplinary
SC Chemistry; Materials Science
GA 136BC
UT WOS:000318333400024
PM 23534827
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Fernández-Jiménez, A
Puertas, F
Sobrados, I
Sanz, J
AF Fernández-Jiménez, A
Puertas, F
Sobrados, I
Sanz, J
TI Structure of calcium silicate hydrates formed in alkaline-activated
slag:: Influence of the type of alkaline activator
SO JOURNAL OF THE AMERICAN CERAMIC SOCIETY
LA English
DT Article
ID C-S-H; BLAST-FURNACE SLAG; TRICALCIUM SILICATE; AL-27 NMR; PASTES;
CEMENT; SI-29; PHASES; TEMPERATURE; GEL
AB The influence of the alkaline activator (NaOH, waterglass, or Na2CO3) on the
structure of the hydrated calcium silicate formed in alkali-activated slag (AAS)
cement pastes has been investigated by FTIR, Si-29 and Al-27 magic-angle scattering
nuclear magnetic resonance, and TEM/EDX techniques. In all cases, the main product
formed after 7 d of activation, with activators giving an Na2O concentration of 4%,
is a semicrystalline calcium silicate hydrate with a dreierkette-type anion. In
these structures, linear finite chains of silicate tetrahedra (Q(2) units) are
linked to central Ca-O layers, and tetrahedral aluminum occupies bridging positions
in the chains. The main chain length and the amount of aluminum incorporated in the
tetrahedral chains depend on the activator used. The detection of Q(3) silicon
entities in alkaline-activated slags is discussed in relation to the possible
formation of cross-linked structures that may be responsible for increased flexural
and compressive strengths in AAS mortars.
C1 CSIC, Inst Ciencias Construct Eduardo Torroja, Madrid 28033, Spain.
CSIC, Inst Ciencia Mat, E-28049 Madrid, Spain.
de Ciencias de la Construccion Eduardo Torroja (IETCC); Consejo Superior
de Investigaciones Cientificas (CSIC); CSIC - Instituto de Ciencias
Matematicas (ICMAT); Instituto de Ciencia de Materiales de Sevilla
(ICMS-CSIC); CSIC - Instituto de Ciencia de Materiales de Madrid (ICMM)
RP Fernández-Jiménez, A (corresponding author), CSIC, Inst Ciencias Construct
Eduardo Torroja, Madrid 28033, Spain.
RI de la Plaza, Maria Isabel Sobrados/B-2101-2010; Fernández, ANA
Maria/G-2597-2016; Puertas, Francisca/F-5366-2016
OI de la Plaza, Maria Isabel Sobrados/0000-0002-7865-4843; Fernández, ANA
Maria/0000-0002-5721-2923; Puertas, Francisca/0000-0002-4215-0184
CR Colomdet P., 1994, APPL NMR SPECTROSCOP
Engelhardth G., 1987, HIGH RESOLUTION SOLI
8846(99)00154-4
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MASSE S, 1993, CEMENT CONCRETE RES, V23, P1169, DOI 10.1016/0008-8846(93)90177-B
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9465(00)00022-6
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8846(94)90002-7
Richardson IG, 1997, J MATER SCI, V32, P4793, DOI 10.1023/A:1018639232570
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Wang SD, 2000, ADV CEM RES, V12, P163, DOI 10.1680/adcr.2000.12.4.163
NR 21
TC 306
Z9 325
U1 8
U2 106
PU AMER CERAMIC SOC
PI WESTERVILLE
PA 735 CERAMIC PLACE, PO BOX 6136, WESTERVILLE, OH 43086-6136 USA
SN 0002-7820
J9 J AM CERAM SOC
JI J. Am. Ceram. Soc.
PD AUG
PY 2003
VL 86
IS 8
BP 1389
EP 1394
DI 10.1111/j.1151-2916.2003.tb03481.x
PG 6
GA 713YN
UT WOS:000184885700024
DA 2023-12-05
ER
PT J
AU Nordstrom, DK
Blowes, DW
Ptacek, CJ
AF Nordstrom, D. Kirk
Blowes, David W.
Ptacek, Carol J.
TI Hydrogeochemistry and microbiology of mine drainage: An update
SO APPLIED GEOCHEMISTRY
LA English
DT Article
ID MULTICOMPONENT REACTIVE TRANSPORT; WASTE-ROCK; IRON MOUNTAIN; PYRITE
OXIDATION; RICH TAILINGS; PYRRHOTITE DISSOLUTION; ACID NEUTRALIZATION;
ARSENITE OXIDATION; SULFIDE TAILINGS; DISSOLVED-OXYGEN
AB The extraction of mineral resources requires access through underground
workings, or open pit operations, or through drillholes for solution mining.
Additionally, mineral processing can generate large quantities of waste, including
mill tailings, waste rock and refinery wastes, heap leach pads, and slag. Thus,
through mining and mineral processing activities, large surface areas of sulfide
minerals can be exposed to oxygen, water, and microbes, resulting in accelerated
oxidation of sulfide and other minerals and the potential for the generation of
low-quality drainage. The oxidation of sulfide minerals in mine wastes is
accelerated by microbial catalysis of the oxidation of aqueous ferrous iron and
sulfide. These reactions, particularly when combined with evaporation, can lead to
extremely acidic drainage and very high concentrations of dissolved constituents.
Although acid mine drainage is the most prevalent and damaging environmental
concern associated with mining activities, generation of saline, basic and neutral
drainage containing elevated concentrations of dissolved metals, non-metals, and
metalloids has recently been recognized as a potential environmental concern. Acid
neutralization reactions through the dissolution of carbonate, hydroxide, and
silicate minerals and formation of secondary aluminum and ferric hydroxide phases
can moderate the effects of acid generation and enhance the formation of secondary
hydrated iron and aluminum minerals which may lessen the concentration of dissolved
metals. Numerical models provide powerful tools for assessing impacts of these
reactions on water quality. Published by Elsevier Ltd.
C1 [Nordstrom, D. Kirk] US Geol Survey, Boulder, CO 80303 USA.
[Blowes, David W.; Ptacek, Carol J.] Univ Waterloo, Dept Earth & Environm Sci,
Waterloo, ON N2L 3G1, Canada.
C3 United States Department of the Interior; United States Geological
Survey; University of Waterloo
RP Nordstrom, DK (corresponding author), US Geol Survey, 3215 Marine St, Boulder,
CO 80303 USA.
EM dkn@usgs.gov
FU National Research Program of the USGS
FX We thank Kate Campbell, Jeff Bain, and Krista Paulson for assistance
with the preparation of this manuscript. One of the authors (DKN) is
grateful for the support of the National Research Program of the USGS.
Use of trade names is for identification purposes only and does not
constitute endorsement by the USGS.
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NR 147
TC 305
Z9 345
U1 18
U2 273
PI OXFORD
SN 0883-2927
J9 APPL GEOCHEM
JI Appl. Geochem.
PD JUN
PY 2015
VL 57
BP 3
EP 16
DI 10.1016/j.apgeochem.2015.02.008
PG 14
WC Geochemistry & Geophysics
SC Geochemistry & Geophysics
GA CH8JS
UT WOS:000354283200002
DA 2023-12-05
ER
PT J
AU Yan, LG
Xu, YY
Yu, HQ
Xin, XD
Wei, Q
Du, B
AF Yan, Liang-guo
Xu, Yuan-yuan
Yu, Hai-qin
Xin, Xiao-dong
Wei, Qin
Du, Bin
TI Adsorption of phosphate from aqueous solution by hydroxy-aluminum,
hydroxy-iron and hydroxy-iron-aluminum pillared bentonites
SO JOURNAL OF HAZARDOUS MATERIALS
LA English
DT Article
DE Pillared bentonite; Phosphate; Adsorption isotherm; Adsorption kinetics;
Thermodynamics
ID SIMULTANEOUS SORPTION; SIMULTANEOUS REMOVAL; FURNACE SLAG; FLY-ASH;
MONTMORILLONITE; WATER; MECHANISMS; PHOSPHORUS; AKAGANEITE; SURFACTANT
AB Phosphorus removal is important for the control of eutrophication, and
adsorption is an efficient treatment process. In this study, three modified
inorganic-bentonites: hydroxy-aluminum pillared bentonite (Al-Bent), hydroxy-iron
pillared bentonite (Fe-Bent), and mixed hydroxy-iron-aluminum pillared bentonite
(Fe-Al-Bent), were prepared and characterized, and their phosphate adsorption
capabilities were evaluated in batch experiments. The results showed a significant
increase of interlayer spacing. BET surface area and total pore volume which were
all beneficial to phosphate adsorption. Phosphate adsorption capacity followed the
order: Al-Bent > Fe-Bent > Fe-Al-Bent. The adsorption rate of phosphate on the
adsorbents fits pseudo-second-order kinetic models (R-2 = 1.00, 0.99, 1.00,
respectively). The Freundlich and Langmuir models both described the adsorption
isotherm data well. Thermodynamic studies illustrated that the adsorption process
was endothermic and spontaneous in nature. Finally, phosphate adsorption on the
inorganic pillared bentonites significantly raised the pH, indicating an anion/OH-
exchange reaction. (c) 2010 Elsevier B.V. All rights reserved.
C1 [Yan, Liang-guo; Xin, Xiao-dong; Du, Bin] Univ Jinan, Coll Resources & Environm
Sci, Jinan 250022, Peoples R China.
[Xu, Yuan-yuan; Yu, Hai-qin; Wei, Qin] Univ Jinan, Coll Chem & Chem Engn, Jinan
250022, Peoples R China.
[Yu, Hai-qin] Ocean Univ China, Coll Chem & Chem Engn, Qingdao 266100, Peoples R
China.
C3 University of Jinan; University of Jinan; Ocean University of China
RP Du, B (corresponding author), Univ Jinan, Coll Resources & Environm Sci, Jinan
EM yanyu-33@163.com; sdjndb@263.com
RI Wei, Qin/AAF-3325-2019; Yan, Liangguo/L-5084-2015; Yan,
Liangguo/AAJ-2399-2020; li, he/ISB-4278-2023; Zhang, Li/GWM-7501-2022
OI Yan, Liangguo/0000-0002-2721-0142; Yan, Liangguo/0000-0002-2721-0142;
FU Natural Science Foundation of China [20577016]; Department of Science &
Technology of Shandong Province [20088509008]; Project of Shandong
Province Higher Educational Science and Technology Program [J08LC06]
FX This study was supported by the Natural Science Foundation of China
(20577016), Department of Science & Technology of Shandong Province
(20088509008), and Project of Shandong Province Higher Educational
Science and Technology Program (J08LC06). Thanks to Chris P. Tostado at
Tsinghua University and Dr. Edward C. Mignot at Shandong University for
their suggestions and advice.
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NR 43
TC 287
Z9 336
U1 6
U2 322
PU ELSEVIER SCIENCE BV
PI AMSTERDAM
PA PO BOX 211, 1000 AE AMSTERDAM, NETHERLANDS
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
JI J. Hazard. Mater.
PD JUL 15
PY 2010
VL 179
IS 1-3
BP 244
EP 250
DI 10.1016/j.jhazmat.2010.02.086
PG 7
WC Engineering, Environmental; Environmental Sciences
SC Engineering; Environmental Sciences & Ecology
GA 609AI
UT WOS:000278626700035
PM 20334967
DA 2023-12-05
ER
PT J
AU Kumar, S
Kumar, R
Bandopadhyay, A
AF Kumar, Sanjay
Kumar, Rakesh
Bandopadhyay, Amitava
TI Innovative methodologies for the utilisation of wastes from
metallurgical and allied industries
SO RESOURCES CONSERVATION AND RECYCLING
LA English
DT Review
DE waste management; value added products; recycling; metal recovery;
utilisation of granulated blast furnace slag and fly ash; mechanical
activation
ID MECHANICAL ACTIVATION
AB This paper is an overview on the utilisation of solid wastes with focus on blast
furnace slag, red mud and fly ash generated in large quantities from iron and steel
industry; primary aluminium production and coal fired power plants, respectively.
Innovative methodologies, based on the recent research by the authors, are
highlighted and these include: (a) smelting reduction of red mud to produce pig
iron and titania rich slag, (b) mechanical activation of the slag and fly ash to
prepare improved blended cements in terms of higher usage of waste and enhanced
cement properties, (c) synergistic usage of fly ash, blast furnace slag and iron
ore tailings in the preparation of floor and wall tiles and (d) preparation of
synthetic granite from fly ash as a value added product. (c) 2006 Elsevier B.V. All
rights reserved.
C1 CSIR, Natl Met Lab, Jamshedpur 831007, Bihar, India.
C3 Council of Scientific & Industrial Research (CSIR) - India; CSIR -
National Metallurgical Laboratory (NML)
RP Kumar, S (corresponding author), CSIR, Natl Met Lab, Jamshedpur 831007, Bihar,
India.
EM sanjay_kumar_nml@yahoo.com
RI Kumar, Rakesh/J-4685-2012; Kumar, Rakesh/IAP-9601-2023
OI Kumar, Rakesh/0000-0002-8967-3855; Kumar, Rakesh/0000-0003-3698-0445;
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NR 43
TC 257
Z9 278
U1 10
U2 125
PU ELSEVIER
PI AMSTERDAM
PA RADARWEG 29, 1043 NX AMSTERDAM, NETHERLANDS
SN 0921-3449
EI 1879-0658
J9 RESOUR CONSERV RECY
JI Resour. Conserv. Recycl.
PD OCT
PY 2006
VL 48
IS 4
BP 301
EP 314
DI 10.1016/j.resconrec.2006.03.003
PG 14
GA 092YI
UT WOS:000241133200001
DA 2023-12-05
ER
PT J
AU RICHARDSON, IG
BROUGH, AR
BRYDSON, R
GROVES, GW
DOBSON, CM
AF RICHARDSON, IG
BROUGH, AR
BRYDSON, R
GROVES, GW
DOBSON, CM
TI LOCATION OF ALUMINUM IN SUBSTITUTED CALCIUM SILICATE HYDRATE (C-S-H)
GELS AS DETERMINED BY SI-29 AND AL-27 NMR AND EELS
LA English
DT Article
ID TRICALCIUM SILICATE; CATION-EXCHANGE; TOBERMORITES; SPECTROSCOPY;
MASNMR; AL
AB Solid-state Al-27 and Si-29 magic angle spinning NMR spectroscopy has been
combined with electron energy loss spectroscopy carried out in the transmission
electron microscope to determine the location of Al substituting in a
semicrystalline C-S-H gel present in a hydrated synthetic slag glass. The gel is
found to contain mainly pentameric silicate chains in which the central silicon is
substituted by aluminum.
C1 UNIV OXFORD, INORGAN CHEM LAB, OXFORD OX1 3QR, ENGLAND.
UNIV SURREY, DEPT MAT SCI & ENGN, GUILDFORD GU2 5XH, SURREY, ENGLAND.
C3 University of Oxford; University of Surrey
RP RICHARDSON, IG (corresponding author), UNIV OXFORD, DEPT MAT, OXFORD OX1 3PH,
ENGLAND.
RI Richardson, Ian G/P-5897-2016; Brydson, Rik/AAP-5531-2020
OI Richardson, Ian G/0000-0002-4340-7121; Drummond-Brydson,
Richard/0000-0003-2003-7612
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NR 18
TC 251
Z9 269
U1 0
U2 36
PU WILEY
PI HOBOKEN
PA 111 RIVER ST, HOBOKEN 07030-5774, NJ USA
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD SEP
PY 1993
VL 76
IS 9
BP 2285
EP 2288
DI 10.1111/j.1151-2916.1993.tb07765.x
PG 4
GA LZ616
UT WOS:A1993LZ61600017
DA 2023-12-05
ER
PT J
AU d'Espinose de la Caillerie, JB
Fretigny, C
Massiot, D
AF d'Espinose de la Caillerie, Jean-Baptiste
Fretigny, Christian
Massiot, Dorninique
TI MAS NMR spectra of quadrupolar nuclei in disordered solids: The Czjzek
model
SO JOURNAL OF MAGNETIC RESONANCE
LA English
DT Article
DE solid-state NMR; quadrupolar nuclei; amorphous materials; glass; gel;
aluminum-27; lineshape; electrical field gradient; disorder
ID SHORT-RANGE ORDER; ELECTRON-PARAMAGNETIC-RESONANCE; LOCAL-FIELD
DISTRIBUTION; HIGH-RESOLUTION NMR; ANGLE-SPINNING NMR; ALUMINOSILICATE
GLASSES; AL-27; ALUMINUM; SI-29; QUANTIFICATION
AB Structural disorder at the scale of two to three atomic positions around the
probe nucleus results in variations of the EFG and thus in a distribution of the
quadrupolar interaction. This distribution is at the origin of the lineshape
tailing toward high fields which is often observed in the MAS NMR spectra of
quadrupolar nuclei in disordered solids. The Czjzek model provides an analytical
expression for the joint distribution of the NMR quadrupolar parameters Do and 17
from which a lineshape can be predicted. This model is derived from the Central
Limit Theorem and the statistical isotropy inherent to disorder. It is thus
applicable to a wide range of materials as we have illustrated for Al-27 spectra on
selected examples of glasses (slag), spinels (alumina), and hydrates (cement
aluminum hydrates). In particular, when relevant, the use of the Czjzek model
allows a quantitative decomposition of the spectra and an accurate extraction of
the second moment of the quadrupolar product. In this respect, it is important to
realize that only rotational invariants such as the quadrupolar product can make
sense to describe the quadrupolar interaction in disordered solids. (c) 2008
Elsevier Inc. All rights reserved.
C1 [d'Espinose de la Caillerie, Jean-Baptiste; Fretigny, Christian] ESPCI
ParisTech, CNRS, UPMC, Phys Chim Polymeres & Milieux Disperses,UMR 7615, F-75005
Paris, France.
[Massiot, Dorninique] CNRS, UPR 4212, Ctr Rech Mat Hautes Temp, F-45071 Orleans
2, France.
C3 Universite PSL; Ecole Superieure de Physique et de Chimie Industrielles
de la Ville de Paris (ESPCI); Centre National de la Recherche
Scientifique (CNRS); CNRS - Institute of Chemistry (INC); Sorbonne
Universite; Centre National de la Recherche Scientifique (CNRS)
RP d'Espinose de la Caillerie, JB (corresponding author), ESPCI ParisTech, CNRS,
UPMC, Phys Chim Polymeres & Milieux Disperses,UMR 7615, 10 Rue Vauquelin, F-75005
Paris, France.
EM jean-Baptiste.dEspinose@espci.fr
RI Massiot, Dominique/C-1287-2008; de Lacaillerie, Jean Baptiste
d'Espinose/F-9387-2010
OI Massiot, Dominique/0000-0003-1207-7040; de Lacaillerie, Jean Baptiste
d'Espinose/0000-0002-2463-6877
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PU ACADEMIC PRESS INC ELSEVIER SCIENCE
PI SAN DIEGO
PA 525 B ST, STE 1900, SAN DIEGO, CA 92101-4495 USA
SN 1090-7807
EI 1096-0856
J9 J MAGN RESON
JI J. Magn. Reson.
PD JUN
PY 2008
VL 192
IS 2
BP 244
EP 251
DI 10.1016/j.jmr.2008.03.001
PG 8
WC Biochemical Research Methods; Physics, Atomic, Molecular & Chemical;
Spectroscopy
SC Biochemistry & Molecular Biology; Physics; Spectroscopy
GA 310OG
UT WOS:000256538300009
PM 18362082
DA 2023-12-05
ER
PT J
AU Taylor, R
Richardson, IG
Brydson, RMD
AF Taylor, R.
Richardson, I. G.
Brydson, R. M. D.
TI Composition and microstructure of 20-year-old ordinary Portland
cement-ground granulated blast-furnace slag blends containing 0 to 100%
slag
LA English
DT Article
DE Portland cement; Granulated blast-furnace slag; C-S-H; TEM; NMR
ID C-S-H; SI-29 MAS NMR; THERMAL-DECOMPOSITION; MG-AL; SILICATE; AL-27;
HYDROTALCITE; PASTES; ALUMINUM; MICROANALYSIS
AB The morphology of outer-product (Op) C-S-H in 20-year-old slag-cement pastes
appeared in most blends to be finer than at younger ages. The Ca/Si and Ca/(Si +
Al) ratios of the Op C-S-H decreased with increasing slag content, and the Al/Si
ratio increased. The Ca/Si ratio of C-S-H in the slag-containing pastes was lower
at 20 years than at 14 months and the amount of Ca(OH)(2) was reduced indicating
that additional slag must have reacted. The mean aluminosilicate chain length of
the C-S-H was very long in all the samples and would be expected to have increased
with age. The TEM-EDX and NMR data are consistent with nanostructural models for C-
S-H. The Mg/Al ratio of the Mg-Al layered double hydroxide phase (LDH) was lower at
20 years than at 14 months in all cases except for the neat slag paste; aluminium
hydroxide-based structure might be interstratified with those of the Mg-Al LDH. (C)
C1 [Taylor, R.; Richardson, I. G.] Univ Leeds, Sch Civil Engn, Leeds LS2 9JT, W
Yorkshire, England.
[Taylor, R.; Brydson, R. M. D.] Univ Leeds, Inst Mat Res, Leeds LS2 9JT, W
Yorkshire, England.
C3 University of Leeds; University of Leeds
RP Richardson, IG (corresponding author), Univ Leeds, Sch Civil Engn, Leeds LS2
9JT, W Yorkshire, England.
EM I.G.Richardson@leeds.ac.uk
RI Brydson, Rik/AAP-5531-2020; Richardson, Ian G/P-5897-2016
OI Richardson, Ian G/0000-0002-4340-7121; Drummond-Brydson,
Richard/0000-0003-2003-7612
FU Nuclear Decommissioning Authority [GR/545874/01]; Castle Cement and
Lafarge Cements; Engineering and Physical Sciences Research Council
[GR/S45874/01] Funding Source: researchfish
FX Thanks are due to the Nuclear Decommissioning Authority for financial
support, to the Engineering and Physical Sciences Research Council (for
funding under Grant No. GR/545874/01 and for a studentship (RT)), and to
Castle Cement and Lafarge Cements for additional technical and financial
support; thanks are also due to Dr D.C. Apperley at Durham University's
EPSRC-funded NMR service for collection of the 27Al NMR
spectra.
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PD JUL
PY 2010
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IS 7
BP 971
EP 983
DI 10.1016/j.cemconres.2010.02.012
PG 13
GA 614YM
UT WOS:000279095700001
DA 2023-12-05
ER
PT J
AU Lloyd, RR
Provis, JL
van Deventer, JSJ
AF Lloyd, Redmond R.
Provis, John L.
TI Pore solution composition and alkali diffusion in inorganic polymer
cement
LA English
DT Article
DE Inorganic polymer; Geopolymer; Aluminosilicate; Pore solution (B);
Durability (C); Alkali (D)
ID ACTIVATED FLY-ASH; CALCIUM SILICATE HYDRATE; BEARING SOLID-PHASES;
BLAST-FURNACE SLAG; C-S-H; PORTLAND-CEMENT; ALUMINUM INCORPORATION;
SOLUBILITY BEHAVIOR; MIGRATION TEST; AL-BEARING
AB Extraction of pore solutions from hardened inorganic polymer cement
("geopolymer") paste samples shows that the pore network of these materials is rich
in alkali cations and has pH>13, with a relatively low dissolved Si concentration.
However, there is little soluble Ca available in these materials to play a
buffering role similar to Ca(OH)2 or high-Ca C-S-H in hydrated Portland cements,
meaning that preventing alkali loss is essential in ensuring the protection of
reinforcing steel. It has been seen previously that calcium in an inorganic polymer
cement binder is important in the formation of a low-permeability pore system;
alkali diffusion measurements confirm these observations and highlight the role of
Ca in reducing effective alkali diffusion coefficients by up to an order of
magnitude. This is crucial for the durability of inorganic polymer concretes
containing steel reinforcement, as it appears that the use of calcium-containing
raw materials will be highly preferable. (C) 2010 Elsevier Ltd. All rights
reserved.
C1 [Lloyd, Redmond R.; Provis, John L.; van Deventer, Jannie S. J.] Univ Melbourne,
Dept Chem & Biomol Engn, Melbourne, Vic 3010, Australia.
RP Provis, JL (corresponding author), Univ Melbourne, Dept Chem & Biomol Engn,
Melbourne, Vic 3010, Australia.
EM jprovis@unimelb.edu.au
RI Provis, John/AAR-3260-2020; Provis, John L/A-7631-2008
OI Provis, John/0000-0003-3372-8922; Provis, John L/0000-0003-3372-8922
FU Australian Research Council (ARC)
FX This work was funded by the Australian Research Council (ARC), including
partial funding via the Particulate Fluids Processing Centre, a Special
Research Centre of the ARC. We also thank Dr. A. Fernandez-Jimenez for
providing a prepublication copy of reference 8.
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NR 40
TC 237
Z9 249
U1 7
U2 113
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD SEP
PY 2010
VL 40
IS 9
BP 1386
EP 1392
DI 10.1016/j.cemconres.2010.04.008
PG 7
GA 634ZR
UT WOS:000280625900006
DA 2023-12-05
ER
PT J
AU Gupta, VK
Sharma, S
AF Gupta, VK
Sharma, S
TI Removal of cadmium and zinc from aqueous solutions using red mud
SO ENVIRONMENTAL SCIENCE & TECHNOLOGY
LA English
DT Article
ID INDUSTRY WASTE MATERIAL; LOW-COST ADSORBENT; METAL-CATIONS; FLY-ASH;
WATER; SORPTION; LEAD; ADSORPTION; SLAG; IONS
AB Red mud, an aluminum industry waste, has been converted into an inexpensive and
efficient adsorbent. The product obtained has been characterized and utilized in
batch and column operations for the removal of cadmium and zinc from aqueous
solutions over a wide range of initial metal ion concentrations (1.78 x 10(-5) to
1.78 x 10(-3) M for Cd2+ and 3.06 x 10(-5) to 3.06 x 10(-3) M for Zn2+; contact
time, 24 h) adsorbent dose (5-20 g/L), and pH (1.0-6.0). The removal of Cd2+ and
Zn2+ was almost complete at low concentrations, while it was 60-65% at higher
concentrations at optimum pH's of 4.0 and 5.0, respectively, with 10 g/L of
adsorbent in an 8-10 h equilibration time. The adsorption decreased with increase
in temperature. Kinetic studies have been used to describe the mechanism of
adsorption. Chemical regeneration of the columns has been achieved with 1% HNO3.
C1 Indian Inst Technol, Dept Chem, Roorkee 247667, Uttar Pradesh, India.
C3 Indian Institute of Technology System (IIT System); Indian Institute of
Technology (IIT) - Roorkee
RP Gupta, VK (corresponding author), Indian Inst Technol, Dept Chem, Roorkee
247667, Uttar Pradesh, India.
EM vinodfcy@iitr.ernet.in
RI Sharma, Saurabh/E-1221-2011
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NR 35
TC 235
Z9 250
U1 3
U2 64
PI WASHINGTON
SN 0013-936X
EI 1520-5851
J9 ENVIRON SCI TECHNOL
JI Environ. Sci. Technol.
PD AUG 15
PY 2002
VL 36
IS 16
BP 3612
EP 3617
DI 10.1021/es020010v
PG 6
GA 584CA
UT WOS:000177448600022
PM 12214656
DA 2023-12-05
ER
PT J
AU Gruskovnjak, A
Lothenbach, B
Holzer, L
Figi, R
Winnefeld, F
AF Gruskovnjak, A.
Lothenbach, B.
Holzer, L.
Figi, R.
Winnefeld, F.
TI Hydration of alkali-activated slag: comparison with ordinary Portland
cement
SO ADVANCES IN CEMENT RESEARCH
LA English
DT Article
ID C-S-H; AQUEOUS SULFIDE; AL-27 NMR; PART I; PASTES; ALUMINUM; SI-29;
OXIDATION; STRENGTH; KINETICS
AB A multi-method approach was used for the investigation and comparison of alkali-
activated slag binders (AAS), pure slag and ordinary Portland cement (OPC). X-ray
fluorescence, X-ray powder diffraction, granulometry, calorimetry, thermo-
gravimetric analysis and environmental scanning electron microscope investigations
of the microstructure with energy dispersive X-ray analyses were used to
characterise the cements and their hydrate phases. In addition, the chemical
composition of the pore solution, including the different sulphur-containing ions,
was analysed. The precipitation mechanisms during binder hydration in the AAS and
OPC systems exhibit significant differences: in AAS the formation of the 'outer
product' C-S-H is much faster than in OPC. The high Si concentrations in the pore
solution during the early hydration of AAS are related to the fast dissolution of
Na-metasilicate. The fast reaction of Na is an important factor for the voluminous
precipitation of C-S-H within the interstitial space already during the first 24 h.
In addition to the Na-metasilicate component, the high fineness of the slag
represents a further important factor for the fast hydration of AAS. The small slag
particles (<2 mu m) are completely dissolved or hydrated within the first 24 h,
whereas hydration of the larger particles is much slower. The fast formation of a
gel-like matrix in AAS is the product of a fast 'through solution' precipitation,
which contrasts with the slower dissolution-precipitation mechanism of a
'topotactic' growth of C-S-H in OPC. The chemical and mineralogical
characterisation of solid and liquid phases and their changes with time are the
basis for thermodynamic modelling of the corresponding hydration process, which is
presented in a second paper.
C1 EMPA, Mat Sci & Technol, CH-8600 Dubendorf, Switzerland.
RP Gruskovnjak, A (corresponding author), EMPA, Mat Sci & Technol, Uberlandstr 129,
CH-8600 Dubendorf, Switzerland.
RI Winnefeld, Frank/B-5335-2009; holzer, lorenz/M-9072-2019; Lothenbach,
Barbara/C-6275-2013
OI Winnefeld, Frank/0000-0002-6864-6196; Lothenbach,
Barbara/0000-0002-9020-6488; Holzer, Lorenz/0000-0002-3532-5994
8846(00)00349-5
8846(81)90069-7
8846(02)00717-2
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8
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NR 34
TC 234
Z9 246
U1 4
U2 114
PU ICE PUBLISHING
PI WESTMINISTER
PA INST CIVIL ENGINEERS, 1 GREAT GEORGE ST, WESTMINISTER SW 1P 3AA, ENGLAND
SN 0951-7197
EI 1751-7605
J9 ADV CEM RES
JI Adv. Cem. Res.
PD JUL
PY 2006
VL 18
IS 3
BP 119
EP 128
DI 10.1680/adcr.2006.18.3.119
PG 10
GA 067UH
UT WOS:000239327600005
DA 2023-12-05
ER
PT J
AU Xue, YJ
Hou, HB
Zhu, SJ
AF Xue, Yongjie
Hou, Haobo
Zhu, Shujing
TI Characteristics and mechanisms of phosphate adsorption onto basic oxygen
furnace slag
LA English
DT Article
DE Adsorption mechanisms; Basic oxygen furnace slag; Ligand exchange;
Phosphate removal; Surface complex
ID AQUEOUS-SOLUTION; REMOVAL; WATER
AB The adsorption characteristics of phosphate adsorption on the basic oxygen
furnace (BOF) slag were identified as a function of pH and ion strengths in
solution. In addition, adsorption mechanisms were investigated by conducting batch
tests on both the hydrolysis and phosphate adsorption process of the BOF slag, and
making a comparative analysis to gain newer insights into understanding the
adsorption process. Results show that the adsorption capacity from 4.97 to 3.71 mg
P/g slag when the solution pH was increased from 2.0 to 13.0 and phosphate initial
concentration was 50 mg/L, indicating that adsorption capacity is largely dependent
upon the pH of the system. The results of the competitive adsorption between
phosphate and typical anions found in wastewater, such as NO3-, SO42- and Cl-, onto
BOF slag reveal that BOF slag can selectively adsorb phosphate ions. The
insignificant effect of NO3-, SO42- and Cl- on phosphate adsorption capacity
indicates that phosphate adsorption is through a kind of inner-sphere complex
reaction. During the adsorption process, the decrease of phosphate concentration in
solution accompanied with an increase in pH values and concentrations of NO3-,
SO42- and Cl- suggests that phosphate replaced the functional groups from the
surface of BOF slag which infers that ligand exchange is the dominating mechanism
for phosphate removal. At the same time, the simultaneous decreases in PO43- and
total calcium, magnesium and aluminum concentration in solution indicate that
chemical reaction and precipitation are other mechanisms of phosphate removal. (C)
2008 Elsevier B,V. All rights reserved.
C1 [Xue, Yongjie; Hou, Haobo; Zhu, Shujing] Wuhan Univ, Sch Resource & Environm
Sci, Wuhan 430072, Hubei, Peoples R China.
[Xue, Yongjie] Wuhan Kaidi Elect Power Environm Protect Co Ltd, Wuhan, Hubei,
Peoples R China.
C3 Wuhan University
RP Xue, YJ (corresponding author), Wuhan Univ, Sch Resource & Environm Sci, Wuhan
430072, Hubei, Peoples R China.
EM xueyj_whu@yahoo.com.cn
FU ZhongGu New Materials Co. Ltd; Wuhan University of Technology; Key
Laboratory for Silicate Materials Science and Engineering Ministry of
Education
FX Financial and technical supports from ZhongGu New Materials Co. Ltd. and
Wuhan University of Technology "Key Laboratory for Silicate Materials
Science and Engineering Ministry of Education" in China are gratefully
acknowledged.
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NR 17
TC 223
Z9 247
U1 3
U2 148
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD MAR 15
PY 2009
VL 162
IS 2-3
BP 973
EP 980
DI 10.1016/j.jhazmat.2008.05.131
PG 8
GA 407MY
UT WOS:000263370200051
PM 18614283
DA 2023-12-05
ER
PT J
AU Zhang, P
Zheng, YX
Wang, KJ
Zhang, JP
AF Zhang, Peng
Zheng, Yuanxun
Wang, Kejin
Zhang, Jinping
TI A review on properties of fresh and hardened geopolymer mortar
SO COMPOSITES PART B-ENGINEERING
LA English
DT Review
DE Geopolymer mortar; Physical properties; Fresh properties; Mechanical
properties; Durability; Microstructure
ID OIL FUEL ASH; BLAST-FURNACE SLAG; FLY-ASH; COMPRESSIVE STRENGTH;
MECHANICAL-PROPERTIES; PORTLAND-CEMENT; MICROSTRUCTURAL ANALYSIS;
THERMAL-BEHAVIOR; SETTING TIME; METAKAOLIN
AB Geopolymer mortar refers to the mortar manufactured with sand and geopolymer,
which is composed by the base materials containing affluent aluminium and silicon
that was activated by adopting alkaline solution to serve as a binder. The
investigation of the properties and application of the geopolymer mortar has
attracted more and more attention of the researchers and cement based industries
because of its sustainability advantages. This study reviews the properties of the
geopolymer mortars including fresh performance (workability, setting time, and
temperature of fresh mortar), physical properties, mechanical properties
(compressive strength, tensile strength, elastic properties, flexural performance,
bonding behavior, and fracture behavior), durability properties (acid resistance,
resistance to elevated temperature, frost resistance, water absorption, and
shrinkage properties) and microstructure analysis. This study also reviews the
properties of different types of geopolymer mortars prepared using various source
materials as base materials. The current study results indicate that the geopolymer
mortar has exhibited significant feasibility and application prospect to be used as
an environmental friendly building material, which may be an appropriate
replacement to the traditional cement mortar in the future.
C1 [Zhang, Peng; Zheng, Yuanxun; Zhang, Jinping] Zhengzhou Univ, Sch Water
Conservancy & Environm, Zhengzhou 450001, Henan, Peoples R China.
[Wang, Kejin] Iowa State Univ, Dept Civil Construct & Environm Engn, Ames, IA
50011 USA.
C3 Zhengzhou University; Iowa State University
RP Zheng, YX (corresponding author), Zhengzhou Univ, Sch Water Conservancy &
Environm, Zhengzhou 450001, Henan, Peoples R China.
EM yxzheng@zzu.edu.cn
RI Zhang, Peng/ABD-2212-2021; Zhang, Peng/Y-4108-2018
OI Zhang, Peng/0000-0001-9505-3858
FU Open Projects Funds of Dike Safety and Disaster Prevention Engineering
Technology Research Center of Chinese Ministry of Water Resources
[2018006]; National Natural Science Foundation of China [51678534];
State Key Laboratory of High Performance Civil Engineering Materials
[2016CEM010]; Program for Science & Technology Innovation Talents in
Universities of Henan Province [16HASTIT012]
FX The authors would like to acknowledge the financial support received
from Open Projects Funds of Dike Safety and Disaster Prevention
Engineering Technology Research Center of Chinese Ministry of Water
Resources (Grant no. 2018006), National Natural Science Foundation of
China (Grant No. 51678534), Foundation Supported by State Key Laboratory
of High Performance Civil Engineering Materials (No. 2016CEM010),
Foundation Sponsored by Program for Science & Technology Innovation
Talents in Universities of Henan Province (Grant No. 16HASTIT012).
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NR 117
TC 222
Z9 228
U1 12
U2 175
PU ELSEVIER SCI LTD
PI OXFORD
SN 1359-8368
EI 1879-1069
J9 COMPOS PART B-ENG
JI Compos. Pt. B-Eng.
PD NOV 1
PY 2018
VL 152
BP 79
EP 95
DI 10.1016/j.compositesb.2018.06.031
PG 17
WC Engineering, Multidisciplinary; Materials Science, Composites
SC Engineering; Materials Science
GA GX2RT
UT WOS:000447568500008
DA 2023-12-05
ER
PT J
AU Huseien, GF
Mirza, J
Ismail, M
Ghoshal, SK
Hussein, AA
AF Huseien, Ghasan Fahim
Mirza, Jahangir
Ismail, Mohammad
Ghoshal, S. K.
Hussein, Ahmed Abdulameer
TI Geopolymer mortars as sustainable repair material: A comprehensive
review
SO RENEWABLE & SUSTAINABLE ENERGY REVIEWS
LA English
DT Review
DE Sustainability; Alkaline solution; Binder; Waste materials; Fresh and
hardened state properties; Durability; Microstructure; Economic
feasibility
ID FLY-ASH GEOPOLYMER; BLAST-FURNACE SLAG; EARLY STRENGTH PROPERTIES;
LIFE-CYCLE ASSESSMENT; LOW-CALCIUM FLY; ACTIVATED SLAG; PORTLAND-CEMENT;
BOND STRENGTH; COMPRESSIVE STRENGTH; AMBIENT-TEMPERATURE
AB Environmentally sustainable repair materials with reduced carbon footprint have
been in great demand by the construction industry worldwide. Gradual deterioration
of concrete containing large quantities of Portland cement is inevitable, and
requires repair or replacement. Numerous repair materials including cementitious
mortars, polymer-modified cementitious mortars, resinous mortars, etc. have been
utilized to rectify the problem. Cement-free geopolymer mortars prepared from waste
materials with high content of silicate aluminum and alkaline activator solution
are emerging as prominent sustainable repair materials. Geopolymer binders are
preferred because they generate 70-80% less carbon dioxide with remarkably lesser
greenhouse gas emissions than ordinary Portland cement. These new binders are
highly sought-after due to their enhanced durability performance, sustainability,
and environmental affability. This paper provides a comprehensive overview of
state-of-the-art research on sustainable geopolymers for repairing deteriorated and
damaged concrete structures as well as restoring their integrity. Present
challenges and future prospects of various geopolymer mortars as repair materials
are emphasized.
C1 [Huseien, Ghasan Fahim; Mirza, Jahangir; Ismail, Mohammad; Hussein, Ahmed
Abdulameer] Univ Teknol Malaysia, Fac Civil Engn, Utm Johor Bahru 81310, Johor,
Malaysia.
[Mirza, Jahangir] Res Inst Hydroquebec, Dept Mat Sci, 1800 Mte Ste Julie,
Varennes, PQ J3X 1S1, Canada.
[Ghoshal, S. K.] Univ Teknol Malaysia, Dept Phys, AOMRG, Fac Sci, Utm Johor
Bahru 81310, Johor, Malaysia.
C3 Universiti Teknologi Malaysia; Universiti Teknologi Malaysia
RP Mirza, J (corresponding author), Univ Teknol Malaysia, Fac Civil Engn, Utm Johor
Bahru 81310, Johor, Malaysia.
EM mirza7861@gmail.com
RI Mirza, Jahangir/HOF-8557-2023; HUSSEIN, AHMED ABDULAMEER/N-7378-2018;
Ismail, Mohammad/F-9868-2011; Huseien, Ghasan Fahim/AEC-3508-2022
OI Mirza, Jahangir/0000-0002-3783-8048; HUSSEIN, AHMED
ABDULAMEER/0000-0003-4369-5108; Huseien, Ghasan
Fahim/0000-0002-2963-0335
FU Ministry of Education through GUP/RU [12H42, 13H50]
FX The authors are indebted to Universiti Teknologi Malaysia and the
Ministry of Education for financial support through GUP/RU Vote 12H42
and 13H50.
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PI OXFORD
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J9 RENEW SUST ENERG REV
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PY 2017
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BP 54
EP 74
DI 10.1016/j.rser.2017.05.076
PG 21
WC Green & Sustainable Science & Technology; Energy & Fuels
SC Science & Technology - Other Topics; Energy & Fuels
GA FJ5JK
UT WOS:000412787600005
DA 2023-12-05
ER
PT J
AU Teir, S
Eloneva, S
Fogelholm, CJ
Zevenhoven, R
AF Teir, Sebastian
Eloneva, Sanni
Fogelholm, Carl-Johan
Zevenhoven, Ron
TI Dissolution of steelmaking slags in acetic acid for precipitated calcium
carbonate production
SO ENERGY
LA English
DT Article; Proceedings Paper
CT 18th International Conference on Efficiency, Costs, Optimization,
Simulation, and Environmental Impact of Energy Systems
CY JUN 22-24, 2005
CL Trondheim, NORWAY
DE mineral carbonation; CO2 storage; CO2 utilization; steel slag; calcium
carbonate; calcium silicate
AB A promising option for long-term storage of CO2 is to fixate carbon dioxide as
magnesium- and calcium carbonates. Slags from iron and steel works are potential
raw materials for carbonation due to their high contents of calcium silicates.
Precipitated calcium carbonate (PCC) is used as filler and coating materials in
paper. If slag could be used instead of limestone for producing PCC, considerable
energy savings and carbon dioxide emissions reductions could be achieved. In this
paper, the leaching of calcium from iron and steel slags using acetic acid was
investigated. Thermodynamic equilibrium calculations at atmospheric gas pressures
showed that extraction of calcium is exothermic and feasible at temperatures lower
than 156 degrees C, while the precipitation of calcium carbonate is endothermic and
feasible at temperatures above 45 degrees C. The formation of calcium- and
magnesium acetate in the solution was found to be thermodynamically possible.
Laboratory-scale batch experiments showed that iron and steel slags rapidly
dissolve in acetic acid in a few minutes and the exothermic nature of the reaction
was verified. While silicon was successfully removed by filtration using solution
temperatures of 70-80 degrees C, further separation methods are required for
removing iron, aluminum and magnesium from the solution. (c) 2006 Elsevier Ltd. All
rights reserved.
C1 Aalto Univ, Lab Energy Engn & Environm Protect, Teknillinen Korkeakoulu, FIN-
02015 Helsinki, Finland.
Abo Akad Univ, Heat Engn Lab, FIN-20500 Turku, Turku, Finland.
C3 Aalto University; Abo Akademi University
RP Teir, S (corresponding author), Aalto Univ, Lab Energy Engn & Environm Protect,
Teknillinen Korkeakoulu, POB 4400, FIN-02015 Helsinki, Finland.
EM sebastian.teir@tkk.fi
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10.1146/annurev.energy.27.122001.083433
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10.1016/j.enconman.2004.05.009
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Teir S., 2005, P 18 INT C EFF COST
TEIR S, 2005, UNPUB J CLEAN PR OCT
*US GEOL SURV, 2003, MIN YB MET MIN, V1
YOGO K, 2004, 7 INT C GREENH GAS C
Zevenhoven R., 2004, INT J THERMODYN, V7, P23
NR 13
TC 217
Z9 250
U1 8
U2 98
PI OXFORD
SN 0360-5442
EI 1873-6785
J9 ENERGY
JI Energy
PD APR
PY 2007
VL 32
IS 4
SI SI
BP 528
EP 539
DI 10.1016/j.energy.2006.06.023
PG 12
WC Thermodynamics; Energy & Fuels
WE Science Citation Index Expanded (SCI-EXPANDED); Conference Proceedings Citation
Index - Science (CPCI-S)
SC Thermodynamics; Energy & Fuels
GA 129PP
UT WOS:000243741700035
DA 2023-12-05
ER
PT J
AU Walkley, B
San Nicolas, R
Sani, MA
Rees, GJ
Hanna, JV
van Deventer, JSJ
Provis, JL
AF Walkley, Brant
San Nicolas, Rackel
Sani, Marc-Antoine
Rees, Gregory J.
Hanna, John V.
Provis, John L.
TI Phase evolution of C-(N)-A-S-H/N-A-S-H gel blends investigated via
alkali-activation of synthetic calcium aluminosilicate precursors
LA English
DT Article
DE Alkali-activated cement (D); Aluminosilicate powder synthesis;
Calcium-silicate-hydrate (C-S-H) (B); Spectroscopy (B)
ID C-S-H; HYDRATED PORTLAND CEMENTS; BLAST-FURNACE SLAG; FLY-ASH; ALUMINUM
INCORPORATION; THERMODYNAMIC MODEL; PART I; NMR; SI-29; AL-27
AB Stoichiometrically-controlled alkali-activated pastes containing calcium-
(sodium) aluminosilicate hydrate (C-(N)-A-S-H) and sodium aluminosilicate hydrate
(N-A-S-H) gels are produced by alkali-activation of high-purity synthetic calcium
aluminosilicate powders. These powders are chemically comparable to the glass in
granulated blast furnace slag, but without interference from minor constituents.
The physiochemical characteristics of these gels depend on precursor chemical
composition. Increased Ca content of the precursor promotes formation of low-AI,
high-Ca C-(N)-A-S-H with lower mean chain length as determined by quantification of
solid state nuclear magnetic resonance spectra, and less formation of calcium
carboaluminate 'Alumino-ferrite mono' (AFm) phases. Increased Al content promotes
Al inclusion and reduced crosslinking within C-(N)-A-S-H, increased formation of
calcium carboaluminate AFm phases, and formation of an additional N-A-S-H gel.
Small changes in precursor composition can induce significant changes in phase
evolution, nanostructure and physical properties, providing a novel route to
understand microstructural development in alkali-activated binders and address key
related durability issues. (C) 2016 Elsevier Ltd. All rights reserved.
C1 [Walkley, Brant; van Deventer, Jannie S. J.] Univ Melbourne, Dept Chem & Biomol
Engn, Melbourne, Vic 3010, Australia.
[San Nicolas, Rackel] Univ Melbourne, Dept Infrastruct Engn, Melbourne, Vic
3010, Australia.
[Sani, Marc-Antoine] Univ Melbourne, Sch Chem, Melbourne, Vic 3010, Australia.
[Sani, Marc-Antoine] Univ Melbourne, Inst Bio21, Melbourne, Vic 3010, Australia.
[Rees, Gregory J.; Hanna, John V.] Univ Warwick, Dept Phys, Coventry CV4 7AL, W
Midlands, England.
[van Deventer, Jannie S. J.] Zeobond Pty Ltd, POB 23450, Docklands, Vic 8012,
Australia.
[Provis, John L.] Univ Sheffield, Dept Mat Sci & Engn, Sheffield S1 3JD, S
Yorkshire, England.
C3 University of Melbourne; University of Melbourne; University of
Melbourne; University of Melbourne; University of Warwick; University of
Sheffield
RP Provis, JL (corresponding author), Univ Sheffield, Dept Mat Sci & Engn,
EM j.provis@sheffield.ac.uk
RI Provis, John L/A-7631-2008; Provis, John/AAR-3260-2020; Rees,
Gregory/AAQ-8688-2021; Sani, Marc-Antoine/B-7707-2013
Rees, Gregory/0000-0002-7514-1516; Sani,
Marc-Antoine/0000-0003-3284-2176; Walkley, Brant/0000-0003-1069-1362
FU Australian Research Council (ARC); University of Melbourne; Particulate
Fluids Processing Centre, a Special Research Centre of the ARC
FX This work has been funded in part by the Australian Research Council
(ARC), including support through the Particulate Fluids Processing
Centre, a Special Research Centre of the ARC. The University of
Melbourne also provided support through an Overseas Research Experience
Scholarship to support an extended visit by the first author to the
University of Sheffield. We also wish to thank and acknowledge Mr. Roger
Curtain, Advanced Microscopy Facility, The University of Melbourne for
assistance with scanning electron microscopy experiments.
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NR 73
TC 216
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U1 13
U2 158
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD NOV
PY 2016
VL 89
BP 120
EP 135
DI 10.1016/j.cemconres.2016.08.010
PG 16
GA EC3VU
UT WOS:000388056000013
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Cyr, M
Coutand, M
Clastres, P
AF Cyr, Martin
Coutand, Marie
Clastres, Pierre
TI Technological and environmental behavior of sewage sludge ash (SSA) in
cement-based materials
LA English
DT Article
DE sewage sludge ash; characterization; mineral admixture; leaching; waste
ID HYDRATION CHARACTERISTICS; LIGHTWEIGHT AGGREGATE; COMPRESSIVE STRENGTH;
BRICK MANUFACTURE; GLASS-CERAMICS; WASTE-WATER; MORTARS; CLAY; SLAG;
ADMIXTURES
AB Sewage sludge ash (SSA) is a waste material obtained from the incineration of
wastewater sludge. The physical, chemical and mineralogical characteristics of SSA,
and the evaluation of its use in cement-based materials, are presented in this
paper. Results show that SSA is composed of irregular grains having a high specific
surface area and thus leading to a significantly high water demand. A fraction of
the ash is rapidly soluble (sulfates, aluminum and silica) and can create new-
formed products in presence of lime. SSA induces short delays of cement hydration,
probably due to both minor elements of the ash and dilution effect. Compressive
strengths of mortars containing 25% and 50% of SSA are always lower than those of
reference mortars but it is shown that SSA has a long-term positive effect which
might be related to a slight pozzolanic activity. The amount of elements leached
from SSA mortars is slightly higher than from the reference mortar without residue
but it remains of the same order of magnitude. An extensive literature review was
performed in order to compare the residue used in this study with others included
in the same category. This analysis highlighted the principal characteristics that
must be taken into account to use SSA correctly in cement-based materials. (c) 2007
Elsevier Ltd. All rights reserved.
C1 INSA UPS, Lab Mat & Durabil Construct, F-31077 Toulouse 04, France.
C3 Universite Federale Toulouse Midi-Pyrenees (ComUE); Universite de
Toulouse; Institut National des Sciences Appliquees de Toulouse
RP Cyr, M (corresponding author), INSA UPS, Lab Mat & Durabil Construct, 135 Ave
Rangueil, F-31077 Toulouse 04, France.
EM cyr@insa-toulouse.fr
RI CYR, Martin/A-8953-2013
OI CYR, Martin/0000-0002-5012-9131
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NR 88
TC 211
Z9 231
U1 5
U2 79
PI OXFORD
SN 0008-8846
JI Cem. Concr. Res.
PD AUG
PY 2007
VL 37
IS 8
BP 1278
EP 1289
DI 10.1016/j.cemconres.2007.04.003
PG 12
GA 207CO
UT WOS:000249229400016
DA 2023-12-05
ER
PT J
AU Gardner, LJ
Bernal, SA
Walling, SA
Corkhill, CL
Provis, JL
Hyatt, NC
AF Gardner, Laura J.
Bernal, Susan A.
Walling, Samuel A.
Corkhill, Claire L.
Provis, John L.
Hyatt, Neil C.
TI Characterisation of magnesium potassium phosphate cements blended with
fly ash and ground granulated blast furnace slag
LA English
DT Article
DE Microstructure; SEM; Fly ash; Granulated blast furnace slag; Chemically
Bonded Ceramics
ID MAS-NMR-SPECTROSCOPY; SOLID-STATE NMR; AL-27 NMR; AQUEOUS-SOLUTION;
RAPID REPAIR; SI-29; STRUVITE; REMOVAL; SURFACE; PHASES
AB Magnesium potassium phosphate cements (MKPCs), blended with 50 wt.% fly ash (FA)
or ground granulated blast furnace slag (GBFS) to reduce heat evolution, water
demand and cost, were assessed using compressive strength, X-ray diffraction (XRD),
scanning electron microscopy (SEM) and nuclear magnetic resonance (NMR)
spectroscopy on Mg-25, Al-27, Si-29, P-31 and K-39 nuclei. We present the first
definitive evidence that dissolution of the glassy aluminosilicate phases of both
FA and GBFS occurred under the pH conditions of MKPC. In addition to the main
binder phase, struvite-K, an amorphous orthophosphate phase was detected in FA/MKPC
and GBFS/MKPC systems. It was postulated that an aluminium phosphate phase was
formed, however, no significant Al-O-P interactions were identified. High-field NMR
analysis of the GBES/MKPC system indicated the potential formation of a potassium-
aluminosilicate phase. This study demonstrates the need for further research on
these binders, as both FA and GBFS are generally regarded as inert fillers within
MKPC (C) 2015 The Authors. Published by Elsevier Ltd. This is an open access
article under the CC BY license (http://creativecommons.org/licenses/by/4.0/).
C1 [Gardner, Laura J.; Bernal, Susan A.; Walling, Samuel A.; Corkhill, Claire L.;
Provis, John L.; Hyatt, Neil C.] Univ Sheffield, Dept Mat Sci & Engn, Immobilisat
Sci Lab, Sheffield S1 3JD, S Yorkshire, England.
C3 University of Sheffield
RP Hyatt, NC (corresponding author), Univ Sheffield, Dept Mat Sci & Engn,
Immobilisat Sci Lab, Sir Robert Hadfield Bldg,Portobello St, Sheffield S1 3JD, S
Yorkshire, England.
EM n.c.hyatt@sheffield.ac.uk
RI Bernal, Susan A/E-8938-2011; Corkhill, Claire L/E-3729-2016; Provis,
John/AAR-3260-2020; Provis, John L/A-7631-2008
OI Corkhill, Claire L/0000-0002-7488-3219; Provis,
John/0000-0003-3372-8922; Provis, John L/0000-0003-3372-8922; Bernal,
Susan A/0000-0002-9647-3106; Hyatt, Neil/0000-0002-2491-3897; Walling,
Sam/0000-0002-7592-1221; Gardner, Laura/0000-0003-3126-2583
FU Royal Academy of Engineering [R/124464-11-1]; Nuclear Decommissioning
Authority [R/124464-11-1]; EPSRC [EP/G037140/1]; University of
Sheffield; BBSRC; University of Warwick viaBirmingham Science City
Advanced Materials Projects 1 and 2; Advantage West Midlands (AWM);
European Regional Development Fund (ERDF); EPSRC [EP/F017901/1] Funding
Source: UKRI; Engineering and Physical Sciences Research Council
[974539, EP/F017901/1] Funding Source: researchfish
FX LJG is grateful to the Nuclear Decommissioning Authority for provision
of a PhD bursary and to Dr. Nick C. Collier for industrial supervision
(National Nuclear Laboratory). NCH wishes to acknowledge the Royal
Academy of Engineering and the Nuclear Decommissioning Authority for
funding (R/124464-11-1). NCH and SAW are grateful to EPSRC for provision
of a CDT PhD studentship under grant reference: EP/G037140/1. CLC is
grateful to the University of Sheffield for the award of a Vice
Chancellor's Fellowship. Solid-state NMR spectra (27Al,
29Si, 31P) were obtained at the EPSRC UK National
Solid-state NMR Service at Durham, and we thank Dr David Apperley for
his generous assistance in collection and interpretation of the results.
The UK 850 MHz Solid-State NMR Facility used in this research
(25Mg, 39K) was funded by EPSRC and BBSRC, as well
as the University of Warwick including via part funding through
Birmingham Science City Advanced Materials Projects 1 and 2 supported by
Advantage West Midlands (AWM) and the European Regional Development Fund
(ERDF). The input of Dr Dinu Iuga in conducting the experiments and the
assistance of Dr John V. Hanna in data interpretation at that facility
are also gratefully acknowledged.
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NR 59
TC 197
Z9 206
U1 10
U2 153
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD AUG
PY 2015
VL 74
BP 78
EP 87
DI 10.1016/j.cemconres.2015.01.015
PG 10
GA CK4LB
UT WOS:000356194200009
OA hybrid, Green Accepted, Green Published
DA 2023-12-05
ER
PT J
AU Sippel, TR
Son, SF
Groven, LJ
AF Sippel, Travis R.
Son, Steven F.
Groven, Lori J.
TI Aluminum agglomeration reduction in a composite propellant using
tailored Al/PTFE particles
SO COMBUSTION AND FLAME
LA English
DT Article
DE Aluminum; Agglomeration; Solid propellant; Combustion; Mechanical
activation; Polytetrafluoroethylene
ID SOLID-PROPELLANT; COMBUSTION PRODUCTS; BURN TIME; IGNITION;
NANOALUMINUM; REACTIVITY; TRANSITION; SIZE
AB In solid propellants, aluminum is widely used to improve performance, yet
theoretical specific impulse is still not achieved largely because of two-phase
flow losses. Losses could be reduced if aluminum particles quickly ignited, more
gaseous products were produced and if upon combustion, aluminum particle breakup
occurred. To explore this, tailored, fuel-rich, mechanically activated composite
particles (aluminum/polytetrafluoroethylene, Al/PTFE 90/10 and 70/30 wt.%) are
considered as replacements for reference aluminum powders (spherical, flake, or
nanoscale) in a composite solid propellant. The effects on burning rate, pressure
dependence, and aluminum ignition, combustion, and agglomeration are quantified.
Using microscopic imaging, it is observed that tailored particles promptly ignite
at the burning surface and appear to breakup into smaller particles, which can
increase the heat feedback to the burning surface. Replacement of spherical
aluminum with Al/PTFE 90/10 wt.% does not significantly affect propellant burning
rate. However, Al/PTFE 70/30 wt.% increases the pressure exponent from 0.36 to
0.58, which results in a 50% increase in propellant burning rate at 13.8 MPa. This
increased pressure sensitivity is consistent with more kinetically controlled
combustion that occurs from smaller burning metal particles near the surface.
Combustion products were quench collected using a new, liquid-free technique at 2.1
and 6.9 MPa and were measured. Both Al/PTFE 90/10 and 70/30 wt.% composite
particles reduce the coarse product fraction and diameter. The most significant
reduction occurs from 70/30 wt.% particle use, where average coarse product
diameter is 25 mu m, which is smaller than the original, average particle size and
is also smaller than the 76 mu m products collected from reference spherical
aluminized propellant. This is a 66% decrease in agglomerate diameter or a 96%
decrease in volume compared to agglomerates formed from reference spherical
aluminum. Smaller diameter condensed phase products and more gaseous products will
likely decrease two-phase flow loss and reduce slag accumulation. (C) 2013 The
Combustion Institute. Published by Elsevier Inc. All rights reserved.
C1 [Sippel, Travis R.; Son, Steven F.; Groven, Lori J.] Purdue Univ, Sch Mech Engn,
W Lafayette, IN 47907 USA.
C3 Purdue University System; Purdue University West Lafayette Campus;
Purdue University
RP Sippel, TR (corresponding author), Iowa State Univ, Dept Mech Engn, 2090 Black
Engn Bldg, Ames, IA 50010 USA.
EM travis.sippel@gmail.com
RI Sippel, Travis/AEW-0245-2022
OI Son, Steven/0000-0001-7498-2922
FU Air Force Office of Scientific Research MURI [FA9550-13-1-0004]
FX The authors would like to acknowledge the financial support of the Air
Force Office of Scientific Research MURI under the supervision of Dr.
Mitat Birkan (#FA9550-13-1-0004).
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NR 41
TC 193
Z9 249
U1 18
U2 169
PU ELSEVIER SCIENCE INC
PI NEW YORK
PA STE 800, 230 PARK AVE, NEW YORK, NY 10169 USA
SN 0010-2180
EI 1556-2921
J9 COMBUST FLAME
JI Combust. Flame
PD JAN
PY 2014
VL 161
IS 1
BP 311
EP 321
DI 10.1016/j.combustflame.2013.08.009
PG 11
WC Thermodynamics; Energy & Fuels; Engineering, Multidisciplinary;
Engineering, Chemical; Engineering, Mechanical
SC Thermodynamics; Energy & Fuels; Engineering
GA 257WU
UT WOS:000327419300029
DA 2023-12-05
ER
PT J
AU Zhou, JB
Yang, SL
Yu, JG
Shu, Z
AF Zhou, Jiabin
Yang, Siliang
Yu, Jiaguo
Shu, Zhan
TI Novel hollow microspheres of hierarchical zinc-aluminum layered double
hydroxides and their enhanced adsorption capacity for phosphate in water
LA English
DT Article
DE Zn-Al LDHs; Hierarchical porous structures; Hollow microspheres;
Phosphate; Adsorption isotherm; Kinetics
ID MACRO-/MESOPOROUS TITANIA; TEMPLATE-FREE FABRICATION; PHOSPHORUS
REMOVAL; PHOTOCATALYTIC ACTIVITY; AQUEOUS-SOLUTION; ACTIVATED CARBON;
FURNACE SLAG; WASTE-WATER; FLY-ASH; IRON
AB Hollow microspheres of hierarchical Zn-Al layered double hydroxides (LDHs) were
synthesized by a simple hydrothermal method using urea as precipitating agent. The
morphology and microstructure of the as-prepared samples were characterized by X-
ray diffraction (XRD), field-emission scanning electron microscopy (FE-SEM),
nitrogen adsorption-desorption isotherms and fourier transform infrared (FTIR)
spectroscopy. It was found that the morphology of hierarchical Zn-Al LDHs can be
tuned from irregular platelets to hollow microspheres by simply varying
concentrations of urea. The effects of initial phosphate concentration and contact
time on phosphate adsorption using various Zn-Al LDHs and their calcined products
(LDOs) were investigated from batch tests. Our results indicate that the
equilibrium adsorption data were best fitted by Langmuir isothermal model, with the
maximum adsorption capacity of 54.1-232 mg/g: adsorption kinetics follows the
pseudo-second-order kinetic equation and intra-particle diffusion model. In
addition, Zn-Al LDOs are shown to be effective adsorbents for removing phosphate
from aqueous solutions due to their hierarchical porous structures and high
specific surface areas. (C) 2011 Elsevier B.V. All rights reserved.
C1 [Zhou, Jiabin; Yu, Jiaguo; Shu, Zhan] Wuhan Univ Technol, State Key Lab Adv
Technol Mat Synth & Proc, Wuhan 430070, Hubei, Peoples R China.
[Zhou, Jiabin; Yang, Siliang] Wuhan Univ Technol, Sch Resources & Environm Engn,
Wuhan 430070, Hubei, Peoples R China.
C3 Wuhan University of Technology; Wuhan University of Technology
RP Yu, JG (corresponding author), Wuhan Univ Technol, State Key Lab Adv Technol Mat
Synth & Proc, 122 Luoshi Rd, Wuhan 430070, Hubei, Peoples R China.
EM jiaguoyu@yahoo.com
RI Zhou, Jiabin/IQV-0967-2023; Zhou, Jiabin/ABB-3033-2021; Zhou,
Jiabin/A-7769-2015; Yu, Jiaguo/G-4317-2010
OI Zhou, Jiabin/0000-0001-8965-7188; Zhou, Jiabin/0000-0001-8965-7188;
Zhou, Jiabin/0000-0001-8965-7188; Yu, Jiaguo/0000-0002-0612-8633
FU National Natural Science Foundation of China [20877061, 51072154];
Natural Science Foundation of Hubei Province [2010CDA078]; National
Basic Research Program of China [2007CB613302]; China Postdoctoral
Science Foundation [20090460998]
FX This work was partially supported by the National Natural Science
Foundation of China (20877061 and 51072154) and the Natural Science
Foundation of Hubei Province (2010CDA078), the National Basic Research
Program of China (2007CB613302), and the China Postdoctoral Science
Foundation project (20090460998).
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NR 55
TC 193
Z9 207
U1 7
U2 364
PI AMSTERDAM
SN 0304-3894
J9 J HAZARD MATER
PD SEP 15
PY 2011
VL 192
IS 3
BP 1114
EP 1121
DI 10.1016/j.jhazmat.2011.06.013
PG 8
GA 824XZ
UT WOS:000295236800025
PM 21719194
DA 2023-12-05
ER
PT J
AU Adu-Amankwah, S
Zajac, M
Stabler, C
Lothenbach, B
Black, L
AF Adu-Amankwah, Samuel
Zajac, Maciej
Stabler, Christopher
Lothenbach, Barbara
Black, Leon
TI Influence of limestone on the hydration of ternary slag cements
LA English
DT Article
DE Limestone; Hydration; PONKCS; Microstructure; Granulated blast-furnace
slag
ID MERCURY INTRUSION POROSIMETRY; BLAST-FURNACE SLAG; PORTLAND-CEMENT; PORE
STRUCTURE; FLY-ASH; SILICA FUME; BLENDS; PRODUCTS; PHASE; QUANTIFICATION
AB The hydration kinetics, microstructure and pore solution composition of ternary
slag-limestone cement have been investigated. Commercial CEM I 52.5 R was blended
with slag and limestone; maintaining a clinker to SCM ratio of 50:50 with up to 20%
slag replaced by limestone. The sulphate content was maintained at 3% in all
composite systems. Hydration was followed by a combination of isothermal
calorimetry, chemical shrinkage, scanning electron microscopy, and
thermogravimetric analysis. The hydration of slag was also followed by SEM image
analysis and the QXRD/PONKCS method. The accuracy of the calibrated PONKCS phase
was assessed on slag and corundum mixes of varying ratios, at different water/solid
ratios. Thus, the method was used to analyse hydrated cement without dehydrating
the specimens. The results show that the presence of limestone enhanced both
clinker and slag hydration. The pore volume and pore solution chemistry were
further examined to clarify the synergistic effects. The nucleation effects account
for enhanced clinker hydration while the space available for hydrate growth plus
the lowering of the aluminium concentration in the pore solution led to the
improved slag hydration.
C1 [Adu-Amankwah, Samuel; Black, Leon] Univ Leeds, Sch Civil Engn, Inst Resilient
Infrastruct, Woodhouse Lane, Leeds LS2 9JT, W Yorkshire, England.
[Zajac, Maciej; Stabler, Christopher] HeidelbergCement Technol Ctr GmbH,
Oberklamweg 2-4, D-69181 Leimen, Germany.
[Lothenbach, Barbara] Empa, Lab Concrete & Construct Chem, Uberlandstr 129, CH-
8600 Dubendorf, Switzerland.
C3 University of Leeds; Swiss Federal Institutes of Technology Domain;
Swiss Federal Laboratories for Materials Science & Technology (EMPA)
RP Adu-Amankwah, S (corresponding author), Univ Leeds, Sch Civil Engn, Inst
Resilient Infrastruct, Woodhouse Lane, Leeds LS2 9JT, W Yorkshire, England.
EM s.adu-amankwah@leeds.ac.uk
RI Lothenbach, Barbara/C-6275-2013; Zajac, Maciej/AAP-8225-2020; Black,
Leon/B-5840-2008
OI Lothenbach, Barbara/0000-0002-9020-6488; Black,
Leon/0000-0001-8531-4989; Adu-Amankwah, Samuel/0000-0002-0568-2093
FU University of Leeds; Heidelberg Technology Centre
FX This work was funded by the University of Leeds and additional funding
from Heidelberg Technology Centre. The authors wish to thank L. Brunetti
(Empa) for the pore solution measurements and Dr. Jan Skocek of
Heidelberg Technology Centre for fruitful discussions and support.
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10.1016/j.cemconcomp.2013.11.007
NR 54
TC 192
Z9 198
U1 4
U2 73
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD OCT
PY 2017
VL 100
BP 96
EP 109
DI 10.1016/j.cemconres.2017.05.013
PG 14
GA FH9QW
UT WOS:000411547800010
DA 2023-12-05
ER
PT J
AU Masi, G
Rickard, WDA
Vickers, L
Bignozzi, MC
Van Riessen, A
AF Masi, Giulia
Rickard, William D. A.
Vickers, Les
Bignozzi, Maria Chiara
Van Riessen, Arie
TI A comparison between different foaming methods for the synthesis of
light weight geopolymers
SO CERAMICS INTERNATIONAL
LA English
DT Article
DE Porosity; Foaming agent; Surfactant; Geopolymers
ID CEMENT-BASED MATERIALS; PORE STRUCTURE; FLY-ASH; MERCURY POROSIMETRY;
INORGANIC POLYMER; TEMPERATURE; INTRUSION; BEHAVIOR; PASTES; SLAG
AB Foaming to reduce the density of geopolymeric materials is increasingly being
reported in the literature as it has been shown to be effective in improving their
insulating properties. However, there is no consistency in foaming methods and as
such this study was performed to compare methods in order to better understand
their effect on the properties of geopolymers. A surfactant and two chemical
foaming agents (hydrogen peroxide and aluminium powder) were added to a fly ash
based geopolymer matrix. Surfactant was also combined with each of the chemical
foaming agents in order to stabilise the foam in the geopolymer matrix and to
reduce coarse pores. The physical, mechanical and microstructural properties of the
low density geopolymers are presented and the effects of the foaming agents'
characteristics on the hardened product is discussed, as well as the relative
merits of the different procedures to synthesise the foamed geopolymer. It was
found that homogeneous microstructures with small pores can be obtained by adding
surfactant and hydrogen peroxide. The combination of hydrogen peroxide (0.1 wt%)
and surfactant (1.0 wt%) produced geopolymer foams with density and compressive
strength values of 0.94 g/cm(3) and 4.6 MPa, respectively. (C) 2014 Elsevier Ltd
and Techna Group S.r.l. All rights reserved.
C1 [Masi, Giulia; Bignozzi, Maria Chiara] Univ Bologna, Dept Civil Chem Environm &
Mat Engn, I-40131 Bologna, Italy.
[Masi, Giulia; Rickard, William D. A.; Vickers, Les; Van Riessen, Arie] Curtin
Univ, Geopolymer Res Grp, Perth, WA 6845, Australia.
C3 University of Bologna; Curtin University
RP Masi, G (corresponding author), Univ Bologna, Dept Civil Chem Environm & Mat
Engn, Via Terracini 28, I-40131 Bologna, Italy.
EM giu.masi88@gmail.com
RI Rickard, William/E-9963-2013; Rickard, William David Athol/N-1509-2019;
Masi, Giulia/AAE-8078-2019
OI Rickard, William/0000-0002-8118-730X; Rickard, William David
Athol/0000-0002-8118-730X; Masi, Giulia/0000-0001-5204-2059; Bignozzi,
Maria/0000-0002-1939-5909
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10.1016/j.conbuildmat.2014.01.081
NR 33
TC 190
Z9 200
U1 4
U2 140
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD NOV
PY 2014
VL 40
IS 9
BP 13891
EP 13902
DI 10.1016/j.ceramint.2014.05.108
PN A
PG 12
GA AO6LL
UT WOS:000341463500017
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Lodeiro, IG
Fernández-Jimenez, A
Palomo, A
Macphee, DE
AF Garcia Lodeiro, I.
Fernandez-Jimenez, A.
Palomo, A.
Macphee, D. E.
TI Effect on fresh C-S-H gels of the simultaneous addition of alkali and
aluminium
LA English
DT Article
DE Calcium-Silicate-Hydrate (C-S-H); Spectroscopy; TEM; Stratlingite
ID CALCIUM-SILICATE-HYDRATE; NUCLEAR-MAGNETIC-RESONANCE; SUBSTITUTED
TOBERMORITES; PORTLAND CEMENTS; PHASE-RELATIONS; ACTIVATED SLAG; AL-27;
SI-29; METAKAOLIN; NMR
AB Reducing Portland cement content in cementitious binders offers a means to
address the adverse environmental impacts of Portland cement manufacture. This
paper investigates the impacts on hydration product chemistry of partially
replacing Portland cement with alkali-activated aluminosilicates. Here, short-term
effects of soluble alkali and aluminium, likely to be available in an alkali-
activated system, on the structure of synthetic C-S-H gels are assessed. C-S-H gels
(synthesized at pH values of over 13) were mixed with different concentrations of
aluminium nitrate and sodium hydroxide. The gels were characterized by FTIR,
TEM/EDX and XRD 72 h later. The results showed that both alkali and aluminium
increased the degree of silicate polymerisation in the C-S-H gels and precipitated
a crystalline calcium aluminosilicate phase. (C) 2009 Elsevier Ltd. All rights
reserved.
C1 [Garcia Lodeiro, I.; Fernandez-Jimenez, A.; Palomo, A.] CSIC, Eduardo Torroja
Inst, Madrid 28033, Spain.
[Macphee, D. E.] Univ Aberdeen, Dept Chem, Old Aberdeen AB24 3UE, Scotland.
de Ciencias de la Construccion Eduardo Torroja (IETCC); University of
Aberdeen
RP Lodeiro, IG (corresponding author), CSIC, Eduardo Torroja Inst, Serrano Galvache
4, Madrid 28033, Spain.
EM iglodeiro@ietcc.csic.es; d.e.macphee@abdn.ac.uk
RI Garcia-Lodeiro, Ines/ABG-8528-2020; Fernández, ANA Maria/G-2597-2016;
PALOMO, ANGEL/G-2584-2016; Garcia Lodeiro, Ines/V-5044-2017
OI Garcia-Lodeiro, Ines/0000-0003-1778-1651; Fernández, ANA
Maria/0000-0002-5721-2923; Garcia Lodeiro, Ines/0000-0003-1778-1651;
Macphee, Donald/0000-0002-0298-7713; PALOMO, ANGEL/0000-0002-6964-2269
FU Ministry of Education and Science [BIA2004-04835]; Spanish Council for
Scientific Research [I3P, 13P-PC2004L]
FX The present research was funded by the Ministry of Education and Science
through project BIA2004-04835 and by the Spanish Council for Scientific
Research in the form of the award of pre-doctoral grant I3P to Ines
Garcia Lodeiro and a post-doctoral contract (ref. 13P-PC2004L) to Dr Ana
Fernandez-Jimenez. The authors wish to thank E.E. Lachowski for his help
with the TEM/EDX analysis of the gels.
10.1016/j.cemconres.2005.04.010
8846(02)00717-2
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NR 35
TC 188
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U1 9
U2 102
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD JAN
PY 2010
VL 40
IS 1
BP 27
EP 32
DI 10.1016/j.cemconres.2009.08.004
PG 6
GA 538FC
UT WOS:000273168700004
DA 2023-12-05
ER
PT J
AU Ke, XY
Bernal, SA
Provis, JL
AF Ke, Xinyuan
Bernal, Susan A.
Provis, John L.
TI Controlling the reaction kinetics of sodium carbonate-activated slag
cements using calcined layered double hydroxides
LA English
DT Article
DE Calorimetry; Kinetics; Alkali activated cement; Granulated blast furnace
slag; MgO
ID BLAST-FURNACE SLAG; HYDROTALCITE-LIKE COMPOUNDS; AL-27 MAS NMR;
HYDRATION PRODUCTS; CHEMISTRY; PHASES; ALUMINUM; BEHAVIOR; CHLORIDE;
SYSTEM
AB In this study, Na2CO3-activated slag cements were produced from four different
blast furnace slags, each blended with a calcined layered double hydroxide (CLDH)
derived from thermally treated hydrotalcite. The aim was to expedite the reaction
kinetics of these cements, which would otherwise react and harden very slowly. The
inclusion of CLDH in these Na2CO3-activated cements accelerates the reaction, and
promotes hardening within 24 h. The MgO content of the slag also defines the
reaction kinetics, associated with the formation of hydrotalcite-type LDH as a
reaction product. The effectiveness of the CLDH is associated with removal of
dissolved CO32- from the fresh cement, yielding a significant rise in the pH, and
also potential seeding effects. The key factor controlling the reaction kinetics of
Na2CO3-activated slag cements is the activator functional group, and therefore
these cements can be designed to react more rapidly by controlling the slag
chemistry and/or including reactive additives. (C) 2015 The Authors. Published by
Elsevier Ltd.
C1 [Ke, Xinyuan; Bernal, Susan A.; Provis, John L.] Univ Sheffield, Dept Mat Sci &
Engn, Sheffield S1 3JD, S Yorkshire, England.
RP Bernal, SA; Provis, JL (corresponding author), Univ Sheffield, Dept Mat Sci &
EM s.bernal@sheffield.ac.uk; j.provis@sheffield.ac.uk
RI Provis, John L/A-7631-2008; Bernal, Susan A/E-8938-2011; Provis,
John/AAR-3260-2020
Bernal, Susan A/0000-0002-9647-3106; Ke, Xinyuan/0000-0002-1239-6861
FU European Research Council under the European Union's Seventh Framework
Programme (FP7) / ERC [335928]; China Scholarship Council (CSC)
FX This research was funded by the European Research Council under the
European Union's Seventh Framework Programme (FP7/2007-2013) / ERC Grant
Agreement #335928 (GeopolyConc). Solid-state NMR spectra were obtained
at the EPSRC UK National Solid-state NMR Service at Durham. XK thank the
China Scholarship Council (CSC) for sponsoring her PhD studies. The
technical support provided by Dr. Oday Hussein, and the donation of the
slags by ECOCEM (R) and Prof. Josee Duchesne (Universite Laval, Canada),
are also greatly acknowledged.
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10.1016/j.cemconres.2011.05.002
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NR 63
TC 182
Z9 188
U1 8
U2 91
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD MAR
PY 2016
VL 81
BP 24
EP 37
DI 10.1016/j.cemconres.2015.11.012
PG 14
GA DD7ES
UT WOS:000370087100003
OA Green Accepted, hybrid, Green Published
DA 2023-12-05
ER
PT J
AU Li, YC
Min, XB
Ke, Y
Liu, DG
Tang, CJ
AF Li, Yuancheng
Min, Xiaobo
Ke, Yong
Liu, Degang
Tang, Chongjian
TI Preparation of red mud-based geopolymer materials from MSWI fly ash and
red mud by mechanical activation
SO WASTE MANAGEMENT
LA English
DT Article
DE Mechanical activation; MSWIFA; Red mud; Red mud-based geopolymer
materials
ID WASTE INCINERATION; BOTTOM ASH; COMPRESSIVE STRENGTH; GYPSUM SLUDGE;
HEAVY-METALS; CO-TREATMENT; CEMENT; MICROSTRUCTURE; SLAG;
SOLIDIFICATION/STABILIZATION
AB A novel method to activate red mud was proposed in this study. Municipal solid
waste incineration fly ash (MSWIFA) and red mud were utilized to prepare red mud-
based geopolymer materials (RGM). The hydration characteristics of RGM were studied
by X-ray diffraction, scanning electronic microscopy, and Fourier transform
infrared spectroscopy. The long-term stability and physical properties of RGM were
tested by freeze-thaw cycle, European Community Bureau reference (BCR) and
unconfined compressive strength (UCS) tests. Results showed that mechanical
activation can not only effectively activate red mud, but also effectively improve
the reaction of MSWIFA and red mud. When 14% sodium silicate was added to the
binder, the UCS reached 12.75 MPa at 28 days. In the RGM, aluminosilicate was
effectively activated by mechanical activation and reacted with calcium ion to form
complex hydration products. The activator reacts adequately with activated aluminum
to form a high-strength geopolymer. The freeze-thaw cycles and BCR test results
also showed that the RGM had long-term stability and the characteristics satisfied
the requirements of MU10 fly ash bricks. This study demonstrated that RGM may be
utilized in cement composites. (C) 2018 Elsevier Ltd. All rights reserved.
C1 [Li, Yuancheng; Min, Xiaobo; Ke, Yong; Liu, Degang; Tang, Chongjian] Cent South
Univ, Sch Met & Environm, Changsha 410083, Hunan, Peoples R China.
[Min, Xiaobo; Ke, Yong; Tang, Chongjian] Chinese Natl Engn Res Ctr Control &
Treatment Hea, Changsha 410083, Hunan, Peoples R China.
[Ke, Yong] Guangdong Jiana Energy Technol Co Ltd, Qingyuan 513056, Peoples R
China.
C3 Central South University
RP Min, XB (corresponding author), Cent South Univ, Sch Met & Environm, Changsha
410083, Hunan, Peoples R China.
EM mxbcsu@163.com
RI Li, yuancheng/IUO-3866-2023
OI LI, Yuancheng/0000-0001-8458-4645
FU key project of National Natural Science Foundation of China [51634010];
Natural Science Foundation of China [51474247, 51474102]; China
Postdoctoral Science Foundation [2017M612583]; Key research and
development project of Hunan Province, China [2015SK2084]; Science and
Technology Project of Hunan, China [2017RS3010]
FX The authors gratefully acknowledge the key project of National Natural
Science Foundation of China (51634010), the Natural Science Foundation
of China (51474247 and 51474102), the China Postdoctoral Science
Foundation (2017M612583), Key research and development project of Hunan
Province, China (2015SK2084), and Science and Technology Project of
Hunan, China (2017RS3010).
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NR 49
TC 177
Z9 190
U1 60
U2 425
PI OXFORD
SN 0956-053X
EI 1879-2456
J9 WASTE MANAGE
JI Waste Manage.
PD JAN
PY 2019
VL 83
BP 202
EP 208
DI 10.1016/j.wasman.2018.11.019
PG 7
GA HF6TO
UT WOS:000454371400022
PM 30514467
OA hybrid
DA 2023-12-05
ER
PT J
AU Gan, FQ
Zhou, JM
Wang, HY
Du, CW
Chen, XQ
AF Gan, Fangqun
Zhou, Jianmin
Wang, Huoyan
Du, Changwen
Chen, Xiaoqin
TI Removal of phosphate from aqueous solution by thermally treated natural
palygorskite
SO WATER RESEARCH
LA English
DT Article
DE Thermally treated palygorskite; Structure changes; Physico-chemical
properties; Phosphate
ID FLY-ASH; ADSORPTION; IONS; EQUILIBRIUM; PHOSPHORUS; HYDROXIDES;
KINETICS; SLAG; DYE
AB The potential of activated palygorskite was assessed for sorption of phosphate
from aqueous solution. The natural palygorskite used was treated by thermal
activation over 100-1000 degrees C for 2 h. The thermal activation increased the
phosphate sorption capacity and the highest phosphate sorption capacity occurred at
700 degrees C. H700 (palygorskite heated at 700 degrees C) showed higher sorption
rate than natural palygorskite (NPAL), and the removal was favorable in acidic
media. The sorption data were described using Freundlich isotherm equation over the
concentration range (5-1000 mg/L) (25 degrees C). Calcium bound phosphorus was the
main fraction of the adsorbed phosphorus, about 98.0% in NPAL and 58.2% in H700,
but the extractive Ca-P species varied greatly, Ca-2-P was 87.7% in NPAL and 3.0%
in H700, Ca-8-P was 10.1% in NPAL and 54.5% in H700, and metal bound phosphorus was
less than 2% in NPAL but more than 41.4% in H700, respectively. The dependence of
the phosphate sorption capacity in the heating samples on thermal activation
appears to be related to major changes in the crystal structure of palygorskite,
and more calcium, iron and aluminum were released from the crystal matrix at 700
degrees C, which promoted phosphorus sorption. (C) 2009 Elsevier Ltd. All rights
reserved.
C1 [Gan, Fangqun; Zhou, Jianmin; Wang, Huoyan; Du, Changwen; Chen, Xiaoqin] Chinese
Acad Sci, Inst Soil Sci, State Key Lab Soil & Sustainable Agr, Nanjing 210008,
Peoples R China.
[Gan, Fangqun] Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China.
C3 Chinese Academy of Sciences; Institute of Soil Science, CAS; Chinese
Academy of Sciences; University of Chinese Academy of Sciences, CAS
RP Zhou, JM (corresponding author), Chinese Acad Sci, Inst Soil Sci, State Key Lab
Soil & Sustainable Agr, Nanjing 210008, Peoples R China.
EM jmzhou@issas.ac.cn
RI Gan, Fangqun/F-4175-2012; Changwen, Du/E-5239-2013
OI Changwen, Du/0000-0002-9064-3581
FU Chinese Academy of Sciences [ISSASIP0712]; National Natural Science
Foundation of China [NSFC40801085]; Cooperative Program of International
Plant Nutrition Institute (Nanjing-10)
FX This work was supported by the Knowledge Innovation Program of Chinese
Academy of Sciences (grants ISSASIP0712), the National Natural Science
Foundation of China (NSFC40801085) and the Cooperative Program of
International Plant Nutrition Institute (Nanjing-10). We are grateful to
Mr. Peiyou Shen and Dr. Yun Liu for the help with the experimental work.
We thank Dr. Hongting Zhao and Mr. Wenzhao Zhang for their kind
assistance in the manuscript revision. We also thank professors Yijie Ma
and Yuanhua Dong, as well as two anonymous reviewers whose comments and
suggestions greatly improved the quality of this manuscript.
8846(02)00888-8
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PM 19447464
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ER
PT J
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Lothenbach, B
Winnefeld, F
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Adler, M
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AF Gruskovnjak, A.
Lothenbach, B.
Winnefeld, F.
Figi, R.
Ko, S. -C.
Adler, M.
Maeder, U.
TI Hydration mechanisms of super sulphated slag cement
LA English
DT Article
DE granulated blast-furnace slag; compressive strength; acceleration;
hydration; hydration products
ID AQUEOUS SULFIDE; OXIDATION; KINETICS
AB The hydration and the strength evolution of supersulphated cements (SSC)
produced by the activation of two different ground granulated blast furnace slags
with anhydrite and small amounts of an alkaline activator have been investigated.
The main differences between the two mixtures are found to be the strength
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individual hydration products formed and the growth mechanisms of the ettringite.
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hydrates formed and thus on the volume of the hydrated slag. Advancement of the
amount of hydrates of a slag with low reactivity by adding aluminium sulphate and
calcium hydroxide did increase the amount of ettringite. Nevertheless, the early
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Switzerland.
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NR 24
TC 168
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U1 9
U2 111
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD JUL
PY 2008
VL 38
IS 7
BP 983
EP 992
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PG 10
GA 313II
UT WOS:000256733900012
DA 2023-12-05
ER
PT J
AU Aguilar, RA
Díaz, OB
García, JIE
AF Arellano Aguilar, R.
Burciaga Diaz, O.
Escalante Garcia, J. I.
TI Lightweight concretes of activated metakaolin-fly ash binders, with
blast furnace slag aggregates
SO CONSTRUCTION AND BUILDING MATERIALS
LA English
DT Article
DE Geopolymers; Strength; Metakaolin; Fly ash; Lightweight concrete;
Blastfurnace slag
ID COMPRESSIVE STRENGTH; GEOPOLYMER MATERIALS; BEHAVIOR; SODIUM; GEL
AB This work investigated geopolymeric lightweight concretes based on binders
composed of metakaolin with 0% and 25% fly ash, activated with 15.2% of Na2O using
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thermal conductivity diminished from 1.65 to 0.47 W/mK for densities from 1800 to
600 kg/m(3). The microstructures revealed dense cementitious matrices conformed of
reaction products and unreacted metakaolin and fly ash. Energy dispersive
spectroscopy and X-ray diffraction showed the formation of amorphous
silicoaluminate reaction products. (C) 2009 Published by Elsevier Ltd.
C1 [Arellano Aguilar, R.; Burciaga Diaz, O.; Escalante Garcia, J. I.] Ctr Res & Adv
Studies, Saltillo 25900, Coahuila, Mexico.
RP García, JIE (corresponding author), Ctr Res & Adv Studies, Saltillo 25900,
Coahuila, Mexico.
EM ivan.escalante@cinvestav.edu.mx
RI Escalante-Garcia, J Ivan/A-1038-2008; burciaga-diaz, oswaldo/F-2744-2013
OI Escalante-Garcia, J Ivan/0000-0001-8128-943X; burciaga-diaz,
Oswaldo/0000-0002-1766-3236
FU National Council of Science and Technology (CONACYT) [53563];
Arellano-Aguilar [203529]
FX The National Council of Science and Technology (CONACYT) is acknowledged
for the Research Project 53563 and Arellano-Aguilar scholarship 203529.
Thanks are due to R. Flores Farias from the laboratory of photothermal
techniques from Cinvestav Queretaro for the support provided for the
thermal conductivity tests.
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AERATED CONCRETE LIG
NR 46
TC 164
Z9 174
U1 3
U2 69
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
J9 CONSTR BUILD MATER
JI Constr. Build. Mater.
PD JUL
PY 2010
VL 24
IS 7
BP 1166
EP 1175
DI 10.1016/j.conbuildmat.2009.12.024
PG 10
WC Construction & Building Technology; Engineering, Civil; Materials
Science, Multidisciplinary
SC Construction & Building Technology; Engineering; Materials Science
GA 601DX
UT WOS:000278039400010
DA 2023-12-05
ER
PT J
AU Tan, HB
Zhang, X
He, XY
Guo, YL
Deng, XF
Su, Y
Yang, J
Wang, YB
AF Tan, Hongbo
Zhang, Xun
He, Xingyang
Guo, Yulin
Deng, Xiufeng
Su, Ying
Yang, Jin
Wang, Yingbin
TI Utilization of lithium slag by wet-grinding process to improve the early
strength of sulphoaluminate cement paste
SO JOURNAL OF CLEANER PRODUCTION
LA English
DT Article
DE Lithium slag; Wet grinding; Early strength; Hydration
ID LAYERED DOUBLE HYDROXIDES; BLAST-FURNACE SLAG; PORTLAND-CEMENT;
ETTRINGITE FORMATION; HYDRATION MECHANISM; CONCRETE; MICROSTRUCTURE;
EXPANSION; EMISSIONS; ASH
AB Lithium slag is a by-product of lithium carbonate industry: in the past decades,
due to ascending demand of lithium salts, emission of this kind of solid waste is
dramatically increased and results in serious environmental problem. Utilization of
lithium slag is of great importance to the sustainable development of lithium
carbonate industry. In this study, one new way to utilize lithium slag in
sulphoaluminate cement system was attempted. Lithium slag was processed with wet
grinding, in order to obtain fine particles and facilitate the ions dissolution.
Addition of wet-grinded lithium slag was expected to improve the early strength of
sulphoaluminate cement. The hydration mechanism was investigated in terms of
setting time, hydration process, hydrates, and pore structure. The results show
that lithium slag with D(0.5) of 3.04 mu m, which is extremely difficult to be
prepared in dry-grinding system, can be easily obtained with wet-grinding process:
the ions dissolution of lithium, aluminum, and silicon phase can also be
significantly facilitated in wet-grinding process. With the dosage less than 10%,
wet-grinded lithium slag can notably promote the early strength of the
sulphoaluminate cement paste, and the main reason for the promotion is not only
because of the filling effect of fine particles and nucleation seed induction of
nano particles formed in wet-grinding process, but also due to the fact that the
dissolved lithium can noticeably facilitate the precipitation of hydrates to induce
the cement hydration. The findings suggest that lithium slag has great potential to
be utilized in sulphoaluminate cement system, and also provide one new way to
utilize solid waste in cement-based materials. (C) 2018 Elsevier Ltd. All rights
reserved.
C1 [Tan, Hongbo; Zhang, Xun; Guo, Yulin; Deng, Xiufeng] Wuhan Univ Technol, State
Key Lab Silicate Mat Architectures, Wuhan 430070, Hubei, Peoples R China.
[He, Xingyang; Su, Ying; Yang, Jin; Wang, Yingbin] Hubei Univ Technol, Sch Civil
Engn Architecture & Environm, Wuhan 430070, Hubei, Peoples R China.
[He, Xingyang; Su, Ying; Yang, Jin; Wang, Yingbin] Hubei Univ Technol, Bldg
Waterproof Engn & Technol Res Ctr Hubei Prov, Wuhan 430070, Hubei, Peoples R China.
C3 Wuhan University of Technology; Hubei University of Technology; Hubei
University of Technology
RP He, XY (corresponding author), Hubei Univ Technol, Sch Civil Engn Architecture &
Environm, Wuhan 430070, Hubei, Peoples R China.
EM hexycn@163.com
RI Deng, Xiufeng/GWC-8986-2022; cheng, shu/IZE-4788-2023; Yang,
Jin/AAY-3338-2021; Tan, Hongbo/Q-5972-2018
OI Yang, Jin/0000-0002-5332-7862; Tan, Hongbo/0000-0003-1706-9939
FU Major Technical Innovation Project in Hubei Province of China
[2017ACA178, 2018AAA002]
FX Financial support from Major Technical Innovation Project in Hubei
Province of China (2017ACA178 and 2018AAA002) is gratefully
acknowledged.
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NR 43
TC 162
Z9 169
U1 29
U2 248
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD DEC 20
PY 2018
VL 205
BP 536
EP 551
DI 10.1016/j.jclepro.2018.09.027
PG 16
WC Green & Sustainable Science & Technology; Engineering, Environmental;
Environmental Sciences
SC Science & Technology - Other Topics; Engineering; Environmental Sciences
& Ecology
GA GZ1MX
UT WOS:000449133300042
DA 2023-12-05
ER
PT J
AU Bernal, SA
Provis, JL
Myers, RJ
San Nicolas, R
van Deventer, JSJ
AF Bernal, Susan A.
Provis, John L.
Myers, Rupert J.
San Nicolas, Rackel
TI Role of carbonates in the chemical evolution of sodium
carbonate-activated slag binders
SO MATERIALS AND STRUCTURES
LA English
DT Article
DE Alkali-activated slag; Sodium carbonate; X-ray diffraction; Nuclear
magnetic resonance; X-ray microtomography
ID BLAST-FURNACE SLAG; C-S-H; ACCELERATED CARBONATION; STRENGTH BEHAVIOR;
ALKALI; HYDRATION; NMR; CHEMISTRY; CEMENT; AL-27
AB Multi-technique characterisation of sodium carbonate-activated blast furnace
slag binders was conducted in order to determine the influence of the carbonate
groups on the structural and chemical evolution of these materials. At early age (<
4 days) there is a preferential reaction of Ca2+ with the CO3 (2-) from the
activator, forming calcium carbonates and gaylussite, while the aluminosilicate
component of the slag reacts separately with the sodium from the activator to form
zeolite NaA. These phases do not give the high degree of cohesion necessary for
development of high early mechanical strength, and the reaction is relatively
gradual due to the slow dissolution of the slag under the moderate pH conditions
introduced by the Na2CO3 as activator. Once the CO3 (2-) is exhausted, the
activation reaction proceeds in similar way to an NaOH-activated slag binder,
forming the typical binder phases calcium aluminium silicate hydrate and
hydrotalcite, along with Ca-heulandite as a further (Ca,Al)-rich product. This is
consistent with the significant gain in compressive strength and reduced porosity
observed after 3 days of curing. The high mechanical strength and reduced
permeability developed in these materials beyond 4 days of curing elucidate that
Na2CO3-activated slag can develop desirable properties for use as a building
material, although the slow early strength development is likely to be an issue in
some applications. These results suggest that the inclusion of additions which
could control the preferential consumption of Ca2+ by the CO3 (2-) might accelerate
the reaction kinetics of Na2CO3-activated slag at early times of curing, enhancing
the use of these materials in engineering applications.
C1 [Bernal, Susan A.; Provis, John L.; Myers, Rupert J.] Univ Sheffield, Dept Mat
[San Nicolas, Rackel; van Deventer, Jannie S. J.] Univ Melbourne, Dept Chem &
Biomol Engn, Parkville, Vic 3010, Australia.
[van Deventer, Jannie S. J.] Zeobond Pty Ltd, Docklands, Vic 8012, Australia.
C3 University of Sheffield; University of Melbourne
RI Provis, John/AAR-3260-2020; Myers, Rupert Jacob/H-8449-2019; Provis,
John L/A-7631-2008; Bernal, Susan A/E-8938-2011; San Nicolas, Rackel
RSN/F-2882-2015
OI Provis, John/0000-0003-3372-8922; Myers, Rupert
Jacob/0000-0001-6097-2088; Provis, John L/0000-0003-3372-8922; San
Nicolas, Rackel RSN/0000-0002-7866-630X
FU Australian Research Council; Zeobond Pty Ltd; Particulate Fluids
Processing Centre; U.S. Department of Energy, Office of Science, Office
of Basic Energy Sciences [DE-AC02-06CH11357]; European Research Council
under the European Union [335928]; University of Sheffield; European
Research Council (ERC) [335928] Funding Source: European Research
Council (ERC)
FX This work has been funded by the Australian Research Council, through a
Linkage Project cosponsored by Zeobond Pty Ltd, including partial
funding through the Particulate Fluids Processing Centre. We wish to
thank Adam Kilcullen and David Brice for preparation of pastes
specimens, John Gehman for his assistance in NMR data collection and
Volker Rose and Xianghui Xiao for assistance in the data collection and
processing on the 2BM instrument. Use of the Advanced Photon Source was
supported by the U.S. Department of Energy, Office of Science, Office of
Basic Energy Sciences, under Contract DE-AC02-06CH11357. The work of JLP
and SAB received funding from the European Research Council under the
European Union's Seventh Framework Programme (FP/2007-2013)/ERC Grant
Agreement #335928 (GeopolyConc), and from the University of Sheffield.
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Z9 172
U1 7
U2 101
PU SPRINGER
PI DORDRECHT
PA VAN GODEWIJCKSTRAAT 30, 3311 GZ DORDRECHT, NETHERLANDS
SN 1359-5997
EI 1871-6873
J9 MATER STRUCT
JI Mater. Struct.
PD MAR
PY 2015
VL 48
IS 3
SI SI
BP 517
EP 529
DI 10.1617/s11527-014-0412-6
PG 13
GA CB2FY
UT WOS:000349443600002
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Love, CA
Richardson, IG
Brough, AR
AF Love, C. A.
Richardson, I. G.
Brough, A. R.
TI Composition and structure of C-S-H in white Portland cement-20%
metakaolin pastes hydrated at 25 °C
LA English
DT Article
DE metakaolin; NMR; TEM; C-S-H
ID MAS NMR-SPECTROSCOPY; CEMENT PASTES; TRICALCIUM SILICATE; CALCIUM
HYDROXIDE; HARDENED PASTES; AL-27; ALUMINUM; BLENDS; PHASES; SLAG
AB The microstructure and composition of water- and alkali-activated hardened
pastes of white Portland cement-20% metakaolin blends have been studied using
solid-state NMR spectroscopy and analytical TEM. The results show that after
hydration for 1 day nearly half the cement had reacted in the water-activated paste
but very little, if any, of the metakaolin; by 28 days two-thirds of the cement had
reacted and most of the metakaolin. In contrast, whilst alkali-activation again led
to about half the cement reacting by I day, about a quarter of the metakaolin had
also reacted; and whilst most of the metakaolin had again reacted by 28 days, there
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the water-activated paste are consistent with both the tobermorite/jennite (T/J)
and tobermorite/calcium hydroxide (T/CH) models for the nanostructure of C-S-H -
although very little J- or CH-like structure is needed to account for the observed
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for on the T/CH viewpoint. (C) 2006 Elsevier Ltd. All rights reserved.
C1 Univ Leeds, Sch Civil Engn, Leeds LS2 9JT, W Yorkshire, England.
Univ Leeds, Inst Mat Res, Leeds LS2 9JT, W Yorkshire, England.
C3 University of Leeds; University of Leeds
EM I.G.Richardson@leeds.ac.uk
RI Richardson, Ian G/P-5897-2016
OI Richardson, Ian G/0000-0002-4340-7121
FU Engineering and Physical Sciences Research Council [GR/S45874/01]
Funding Source: researchfish
10.1016/j.cemconres.2005.04.010
[Anonymous], 2002, STRUCTURE PERFORMANC
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SN 0008-8846
JI Cem. Concr. Res.
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PT J
AU Schneider, J
Cincotto, MA
Panepucci, H
AF Schneider, J
Cincotto, MA
Panepucci, H
TI 29Si and 27Al high-resolution NMR characterization
of calcium silicate hydrate phases in activated blast-furnace slag
pastes
LA English
DT Article
DE granulated blast-furnace slag; calcium-silicate-hydrate (C-S-H); NMR
spectroscopy; thermal treatment
AB Within the framework of improving mechanical properties of activated blast-
furnace slag cements, a set of hardened pastes of 28 days age were analyzed by Si-
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and compositional differences among C-S-H phases obtained with different activation
and curing conditions were characterized by NMR. Activation of the slag was done
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the extent of the hydration reaction, the polymerization degree of the aluminum-
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resulting from activation with sodium silicate and gypsum/calcium hydroxide blend.
Steam curing and a higher alkali concentration enhanced the incorporation of Al in
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alkali addition. (C) 2001 Elsevier Science Ltd. All rights reserved.
C1 Univ Sao Paulo, Inst Fis Sao Carlos, BR-13560970 Sao Carlos, SP, Brazil.
Univ Sao Paulo, EPUSP, PCC, Dept Engn Construcao Civil, BR-05424970 Sao Paulo,
Brazil.
C3 Universidade de Sao Paulo; Universidade de Sao Paulo
RP Schneider, J (corresponding author), Univ Sao Paulo, Inst Fis Sao Carlos, Av
Carlos Botelho 1465,Caixa Postal 369, BR-13560970 Sao Carlos, SP, Brazil.
EM schnei@if.sc.usp.br
RI Schneider, José F/G-9534-2012; Cincotto, Maria Alba A/G-2560-2013
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NR 16
TC 161
Z9 177
U1 5
U2 49
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD JUL
PY 2001
VL 31
IS 7
BP 993
EP 1001
DI 10.1016/S0008-8846(01)00530-0
PG 9
GA 456NN
UT WOS:000170089100003
DA 2023-12-05
ER
PT J
AU Myers, RJ
Bernal, SA
Gehman, JD
van Deventer, JSJ
Provis, JL
AF Myers, Rupert J.
Bernal, Susan A.
Gehman, John D.
Provis, John L.
TI The Role of Al in Cross-Linking of Alkali-Activated Slag Cements
LA English
DT Article
ID C-S-H; BLAST-FURNACE SLAG; LAYERED DOUBLE HYDROXIDES; HIGH-RESOLUTION
NMR; MAS-NMR; ALUMINUM INCORPORATION; ALUMINOSILICATE GEOPOLYMER;
HYDRATION PRODUCTS; AL-27 NMR; PART I
AB The structural development of a calcium (sodium) aluminosilicate hydrate (C-
(N-)A-S-H) gel system, obtained through the reaction of sodium metasilicate and
ground granulated blast furnace slag, is assessed by high-resolution Si-29 and Al-
27 MAS NMR spectroscopy during the first 2yr after mixing. The cements formed
primarily consist of C-(N-)A-S-H gels, with hydrotalcite and disordered alkali
aluminosilicate gels also identified in the solid product assemblages.
Deconvolution of the Al-27 MAS NMR spectra enables the identification of three
distinct tetrahedral Al sites, consistent with the Si-29 MAS NMR data, where Q(3)
(1Al), Q(4)(3Al), and Q(4)(4Al) silicate sites are identified. These results
suggest significant levels of cross-linking in the C-(N-)A-S-H gel and the presence
of an additional highly polymerized aluminosilicate product. The mean chain length,
extent of cross-linking, and Al/Si ratio of the C-(N-)A-S-H gel decrease slightly
over time. The de-cross-linking effect is explained by the key role of Al in mixed
cross-linked/non-cross-linked C-(N-)A-S-H gels, because the cross-linked components
have much lower Al-binding capacities than the noncross-linked components. These
results show that the aluminosilicate chain lengths and chemical compositions of
the fundamental structural components in C-(N-)A-S-H gels vary in a way that is not
immediately evident from the overall bulk chemistry.
[Bernal, Susan A.; van Deventer, Jannie S. J.; Provis, John L.] Univ Melbourne,
Dept Chem & Biomol Engn, Melbourne, Vic 3010, Australia.
[Gehman, John D.] Univ Melbourne, Sch Chem, Melbourne, Vic 3010, Australia.
[Gehman, John D.] Univ Melbourne, Inst Bio21, Melbourne, Vic 3010, Australia.
[Gehman, John D.] GehmanLab, Woodend, Vic 3442, Australia.
[van Deventer, Jannie S. J.] Zeobond Pty Ltd, Docklands, Vic 8012, Australia.
C3 University of Sheffield; University of Melbourne; University of
RP Provis, JL (corresponding author), Univ Sheffield, Dept Mat Sci & Engn, Mappin
St, Sheffield S1 3JD, S Yorkshire, England.
RI Bernal, Susan A/E-8938-2011; Myers, Rupert Jacob/H-8449-2019; Provis,
John L/A-7631-2008; Provis, John/AAR-3260-2020
OI Myers, Rupert Jacob/0000-0001-6097-2088; Provis, John
L/0000-0003-3372-8922; Provis, John/0000-0003-3372-8922; Bernal, Susan
A/0000-0002-9647-3106; Gehman, John D/0000-0002-2599-6292
FU Australian Research Council (ARC); Zeobond Pty Ltd, and through the
Particulate Fluids Processing Centre, a Special Research Centre of the
ARC; University of Sheffield
FX This work was funded in part by the Australian Research Council (ARC),
including support through a Linkage Project co-funded by Zeobond Pty
Ltd, and through the Particulate Fluids Processing Centre, a Special
Research Centre of the ARC. Funding support provided by the University
of Sheffield is also gratefully acknowledged. We thank Sam A. Walling
(University of Sheffield) for sharing important results regarding the
NMR analysis of hydrotalcite.
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6
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10.1016/j.cemconres.2010.11.012
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Vyalikh A, 2009, SOLID STATE NUCL MAG, V36, P19, DOI 10.1016/j.ssnmr.2009.04.002
NR 59
TC 159
Z9 164
U1 2
U2 110
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD MAR
PY 2015
VL 98
IS 3
BP 996
EP 1004
DI 10.1111/jace.13360
PG 9
GA CD4KC
UT WOS:000351050300044
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Li, ZJ
Liu, SF
AF Li, Zongjin
Liu, Sifeng
TI Influence of slag as additive on compressive strength of fly ash-based
geopolymer
SO JOURNAL OF MATERIALS IN CIVIL ENGINEERING
LA English
DT Article
ID KAOLINITE; METAKAOLINITE; TEMPERATURE; ALUMINUM; METALS; NMR
AB Slag was utilized as an additive for fly ash-based geopolymers in this study. It
was found that the incorporation of slag could significantly increase the
compressive strength of the geopolymer. The compressive strength of geopolymer with
4.0% slag reached 50 and 70 MPa when cured for 14 days at 30 and 70 degrees C,
respectively. The mechanism of slag as additive on the enhancement of compressive
strength of geopolymer was investigated using X-ray diffractometer (XRD), 'Fourier
transform infrared (FTIR) spectroscopy, X-ray photoelectron spectroscopy (XPS), and
mercury intrusion porosimetry (MIP). The XRD and FTIR results showed that the
addition of slag could generate more amorphous products and accelerate the reaction
rate of raw materials. From XPS results, the decrease of binding energy and a
broadening of peaks were observed for Si 2p, A12p, and O 1s elements due to the
Ca2+ provided by slag. The decrease in binding energy was more favorable to zeolite
formation. The results of MIP suggested that the 4% slag addition significantly
influenced pore structure of geopolymer. A refinement of pore size was exhibited
after 4% slag addition, especially for specimens being cured at 70 degrees C. For
these reasons, the compressive strength of geopolymer made with 4% slag addition
was greatly improved.
C1 Hong Kong Univ Sci & Technol, Dept Civil Engn, Kowloon, Hong Kong, Peoples R
China.
Tongji Univ, Sch Mat Sci & Engn, Shanghai 200092, Peoples R China.
C3 Hong Kong University of Science & Technology; Tongji University
RP Li, ZJ (corresponding author), Hong Kong Univ Sci & Technol, Dept Civil Engn,
Clear Water Bay, Kowloon, Hong Kong, Peoples R China.
OI Li, Zongjin/0000-0002-8477-6863
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10.1016/j.cemconres.2004.06.031
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Zhang YS, 2003, THESIS SE U NANJING
NR 23
TC 159
Z9 176
U1 9
U2 103
PU ASCE-AMER SOC CIVIL ENGINEERS
PI RESTON
PA 1801 ALEXANDER BELL DR, RESTON, VA 20191-4400 USA
SN 0899-1561
J9 J MATER CIVIL ENG
JI J. Mater. Civ. Eng.
PD JUN
PY 2007
VL 19
IS 6
BP 470
EP 474
DI 10.1061/(ASCE)0899-1561(2007)19:6(470)
PG 5
GA 173MF
UT WOS:000246876500004
DA 2023-12-05
ER
PT J
AU Soutsos, M
Boyle, AP
Vinai, R
Hadjierakleous, A
Barnett, SJ
AF Soutsos, Marios
Boyle, Alan P.
Vinai, Raffaele
Hadjierakleous, Anastasis
Barnett, Stephanie J.
TI Factors influencing the compressive strength of fly ash based
geopolymers
LA English
DT Article
DE Geopolymer; Alkali activated material; Fly ash; Slag; Structural
characterisation; Mechanical properties; Alkali dosages optimisation
ID BLAST-FURNACE SLAG; CALCIUM SILICATE HYDRATE; C-S-H; MICROSTRUCTURAL
DEVELOPMENT; TECHNOLOGY; REACTIVITY; ACTIVATION
AB Several factors affecting the reactivity of fly ash (FA) as a precursor for
geopolymer concrete have been investigated. These include physical and chemical
properties of various FA sources, inclusion of ground granulated blast furnace slag
(ggbs), chemical activator dosages and curing temperature. Alkali activated FA was
found to require elevated curing temperatures and high alkali concentrations. A
mixture of sodium hydroxide and sodium silicate was used and this was shown to
result in high strengths, as high as 70 MPa at 28 days. The presence of silicates
in solution was found to be an important parameter affecting strength. Detailed
physical and chemical characterisation was carried out on thirteen FA sources from
the UK. The most important factor affecting the reactivity was found to be the
particle size of FA. The loss on ignition (LOI) and the amorphous content are also
important parameters that need to be considered for the selection of FA for use in
geopolymer concrete. The partial replacement of FA with ggbs was found to be
beneficial in not only avoiding the need for elevated curing temperatures but also
in improving compressive strengths. Microstructural characterisation with scanning
electron microscope (SEM) coupled with energy dispersive X-ray spectroscopy (EDS)
was performed on FAiggbs pastes. The reaction product of FA and ggbs in these
binary systems was calcium aluminium silicate hydrate gel (C-A-S-H) with inclusion
of Na in the structure. (C) 2015 Elsevier Ltd. All rights reserved.
C1 [Soutsos, Marios; Vinai, Raffaele] Queens Univ Belfast, Sch Planning
Architecture & Civil Engn, Belfast BT9 5AG, Antrim, North Ireland.
[Boyle, Alan P.; Hadjierakleous, Anastasis] Univ Liverpool, Sch Environm Sci,
Liverpool L69 3GP, Merseyside, England.
[Barnett, Stephanie J.] Univ Portsmouth, Sch Civil Engn & Surveying, Portsmouth
PO1 2UP, Hants, England.
C3 Queens University Belfast; University of Liverpool; University of
Portsmouth
RP Soutsos, M (corresponding author), Queens Univ Belfast, Sch Planning
Architecture & Civil Engn, Belfast BT9 5AG, Antrim, North Ireland.
EM m.soutsos@qub.ac.uk
RI Vinai, Raffaele/AAE-4894-2019; Boyle, Alan P/B-9649-2011
OI Vinai, Raffaele/0000-0001-9506-1591; Barnett,
Stephanie/0000-0001-8619-8318
FU University of Liverpool in the framework of the Carbon Trust Applied
Research Grant [0911-0252]; SUSCON project; European Union [285463]
FX This research was carried out at the University of Liverpool in the
framework of the Carbon Trust Applied Research Grant 0911-0252 "Ultra
High Performance Fibre Reinforced Cementless Precast Concrete Products".
The work was then continued at Queen's University of Belfast with the
financial support of the SUSCON project, which has received funding from
the European Union Seventh Framework Programme (FP7/2007-2013) under
Grant Agreement No. 285463 (Call FP7-2011-NMP ENV-ENERGY-ICT-EeB).
CR Andini S, 2008, WASTE MANAGE, V28, P416, DOI 10.1016/j.wasman.2007.02.001
[Anonymous], 2006, RES REP GC2
6
British Standards Institution, 1235052000 BS EN
British Standards Institution, 45012005A12007 BS EN
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10.1016/j.cemconres.2004.10.042
NR 37
TC 158
Z9 167
U1 11
U2 96
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD MAY 1
PY 2016
VL 110
BP 355
EP 368
DI 10.1016/j.conbuildmat.2015.11.045
PG 14
GA DI5LQ
UT WOS:000373541000041
OA Green Submitted, Green Accepted
DA 2023-12-05
ER
PT J
AU Myers, RJ
Bernal, SA
Provis, JL
AF Myers, Rupert J.
Bernal, Susan A.
Provis, John L.
TI A thermodynamic model for C-(N-)A-S-H gel: CNASH_ss. Derivation and
validation
LA English
DT Article
DE Calcium-silicate-hydrate (C-S-H); Thermodynamic calculations;
Alkali-activated cement; Blended cement; Modelling
ID C-S-H; CALCIUM-SILICATE-HYDRATE; ALKALI-ACTIVATED SLAG; BLAST-FURNACE
SLAG; AQUEOUS SOLUBILITY DIAGRAMS; WASTE STABILIZATION SYSTEMS; PARTIAL
MOLAL PROPERTIES; CEMENT PASTES; ALUMINUM INCORPORATION; TRICALCIUM
SILICATE
AB The main reaction product in Ca-rich alkali-activated cements and hybrid
Portland cement (PC)-based materials is a calcium (alkali) aluminosilicate hydrate
(C-(N-)A-S-H) gel. Thermodynamic models without explicit definitions of
structurally-incorporated Al species have been used in numerous past studies to
describe this gel, but offer limited ability to simulate the chemistry of blended
PC materials and alkali-activated cements. Here, a thermodynamic model for C-(N-)A-
S-H gel is derived and parameterised to describe solubility data for the CaO-
(Na2O,Al2O3)-SiO2-H2O systems and alkali-activated slag (AAS) cements, and chemical
composition data for C-A-S-H gels. Simulated C-(N-)A-S-H gel densities and molar
volumes are consistent with the corresponding values reported for MS cements,
meaning that the model can be used to describe chemical shrinkage in these
materials. Therefore, this model can provide insight into the chemistry of AAS
cements at advanced ages, which is important for understanding the long-term
durability of these materials. (C) 2014 Elsevier Ltd. All rights reserved.
RP Provis, JL (corresponding author), Univ Sheffield, Dept Mat Sci & Engn, Sir
Robert Hadfield Bldg,Mappin St, Sheffield S1 3JD, S Yorkshire, England.
RI Provis, John L/A-7631-2008; Myers, Rupert Jacob/H-8449-2019; Bernal,
Susan A/E-8938-2011; Provis, John/AAR-3260-2020
OI Provis, John L/0000-0003-3372-8922; Myers, Rupert
Jacob/0000-0001-6097-2088; Provis, John/0000-0003-3372-8922; Bernal,
Susan A/0000-0002-9647-3106
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NR 101
TC 157
Z9 167
U1 12
U2 118
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD DEC
PY 2014
VL 66
BP 27
EP 47
DI 10.1016/j.cemconres.2014.07.005
PG 21
GA AQ0MQ
UT WOS:000342477800004
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Gustafsson, JP
AF Gustafsson, Jon Petter
TI Vanadium geochemistry in the biogeosphere -speciation, solid-solution
interactions, and ecotoxicity
LA English
DT Review
DE Vanadate; Vanadyl; Water; Soil; Sediment; Bioavailability
ID X-RAY-ABSORPTION; SEQUENTIAL EXTRACTION PROCEDURE; K-EDGE XANES; STEEL
SLAG; TRACE-ELEMENTS; ION-BINDING; RED MUD; ISOTOPE COMPOSITION;
ORGANIC-MATTER; BLOOD-CELLS
AB Vanadium is a metal that receives increasing attention due to its possible
toxicity and its increased use in society, i.e. in high-grade steel and in vanadium
redox-flow batteries. Already today, the global biogeochemical cycle of vanadium is
heavily impacted by human activities, and these impacts will probably increase. The
total V concentration in the upper part of the Earth's crust, and in soils, is near
100 mg V kg(-1). Usually, the dissolved V concentration is low. In seawater the
mean dissolved V concentration is 1.8 mu g L-1, and in freshwaters the
concentration is commonly below 1 mu g L-1 although in areas with volcanic and
sedimentary rocks it may be much higher, i.e. at the slopes of Mt. Etna, Italy,
concentrations of up to 180 mu g V L-1 have been recorded.
Vanadium is a redox-sensitive element, which occurs in three oxidation states
(+III, +IV and +V) in the environment. Whereas vanadium(V) usually occurs as the
oxyanion vanadate(V) under most environmental conditions, vanadyl(IV) is an
oxocation that is stable at low pH and/or mildly reducing conditions, particularly
when the organic matter concentration is high. Vanadium(III), which is the least
studied form of vanadium, occurs under strongly reducing conditions. All vanadium
forms are strongly bound to environmental sorbents: vanadate(V) is bound as a
bidentate complex to iron, aluminium, and titanium (hydr)oxides, and with a
stronger affinity than that of orthophosphate (o-phosphate). Vanadyl(IV) is
strongly complexed to natural organic matter, while vanadium(III) may substitute
for other trivalent ions in mineral structures. Despite this, vanadium may be
mobilized to the aqueous phase, for example under high-pH conditions. Studies with
V K-edge XANES spectroscopy have shown that most oxic soils usually contain a
mixture of vanadium(IV) that is octahedrally coordinated in primary minerals, and
surface-bound vanadate(V) on iron and aluminium (hydr) oxides, although acid
organic soils are dominated by organically complexed vanadyl(IV). In reduced
environments, such as in sediments and black shales, available evidence suggests
that the V consists of a mixture of organically complexed vanadyl(IV) and unknown
vanadium(III) species. However, considerable uncertainty exists on the V speciation
under reducing conditions, and additional research is recommended.
Vanadium is essential for some species of cyanolichens and algae due to its
presence in vanadium nitrogenase, which can be important for N fixation in boreal
ecosystems, and in vanadium haloperoxidases, which mediate the oxidation of
halides, particularly iodine and bromine. In certain organisms vanadium is
accumulated for unknown reasons, e.g. in ascidians, where V accumulates as a
vanadium(III) complex with organic S, and in Amanita mushrooms, in which amavadin,
a stable vanadium(IV)-organic complex, is accumulated. However, at high
concentrations vanadium is toxic to many organisms. This is mostly due to its
interference with o-phosphate in a number of biomolecules. Available evidence shows
that toxic effects appear in the mg V L-1 range for most studied species. However,
some organisms, i.e. algae and possibly some soil bacteria, are more sensitive. In
soils, the toxic response is related to the soil solution V concentration, rather
than to the solid-phase concentration. The o-phosphate concentration has been
identified as a parameter that influences toxicity, but the relationship between
the P status and the environmental risk of V toxicity is not yet well determined -
as a result risk-based guidelines remain uncertain. There is urgent need for more
research on this topic.
Vanadium, being a redox-sensitive element, responds to sudden environmental
change such as flooding that leads to decreased redox potential. In most, but not
all, cases, an increased solubilisation of vanadium is observed after flooding,
which can be attributed to reductive dissolution of vanadate(V)-sorbing iron
(hydr)oxides and to vanadate(V) reduction to vanadyl(IV) that forms stable
complexes with dissolved organic matter. The vanadium redox conversions are carried
out by a large number of genera of bacteria. Bioremediation methods are being
developed that may reduce vanadate(V) to vanadyl(IV), which may reduce the
bioavailability of vanadium in many soils.
C1 [Gustafsson, Jon Petter] Swedish Univ Agr Sci, Dept Soil & Environm, Box 7014,
S-75007 Uppsala, Sweden.
[Gustafsson, Jon Petter] KTH Royal Inst Technol, Dept Sustainable Dev Environm
Sci & Engn, Teknikringen 10B, S-10044 Stockholm, Sweden.
C3 Swedish University of Agricultural Sciences; Royal Institute of
Technology
RP Gustafsson, JP (corresponding author), Swedish Univ Agr Sci, Dept Soil &
Environm, Box 7014, S-75007 Uppsala, Sweden.
EM jon-petter.gustafsson@slu.se
RI Gustafsson, Jon Petter/B-1655-2010
OI Gustafsson, Jon Petter/0000-0001-8771-7941
FU Swedish Research Council [I811]; Knut och Alice Wallenbergs Stiftelse
[I811]
FX First of all I thank Maja Larsson, our previous PhD student, who
authored six papers during her PhD studies, all of which are mentioned
in this review. I also thank my other "vanadium collaborators" from
previous research projects, Stijn Baken, Erik Smolders, Golshid
Hadialhejazi, Francesco Cubadda, Andrea Raggi, Marilena D'Amato, Ingrid
Oborn, Dan Berggren Kleja, Ingrid Oborn, Ingmar Persson, Carin Sjostedt,
and Lars Johnsson. Torbjorn Carlsson and Jeanette Stemne at Merox are
the ones who introduced us into the vanadium world and are hereby
thankfully acknowledged. Rolf Lindblom at LKAB is thanked for
stimulating discussions. The EXAFS results for vanadium sorbed on
amorphous Al hydroxide were collected at beamline I811, MAX-Lab
synchrotron radiation source, Lund University, Sweden. Funding for the
beamline I811 project was kindly provided by The Swedish Research
Council and The Knut och Alice Wallenbergs Stiftelse.
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NR 245
TC 152
Z9 159
U1 36
U2 275
PI OXFORD
SN 0883-2927
J9 APPL GEOCHEM
JI Appl. Geochem.
PD MAR
PY 2019
VL 102
BP 1
EP 25
DI 10.1016/j.apgeochem.2018.12.027
PG 25
GA HM9FT
UT WOS:000459789000001
OA hybrid
DA 2023-12-05
ER
PT J
AU Rezvani, M
Eftekhari-Yekta, B
Solati-Hashjin, M
Marghussian, VK
AF Rezvani, M
Eftekhari-Yekta, B
Solati-Hashjin, M
Marghussian, VK
TI Effect of Cr2O3, Fe2O3 and
TiO2 nucleants on the crystallization behaviour of
SiO2-Al2O3-CaO-MgO(R2O)
glass-ceramics
LA English
DT Article
DE glass-ceramics; diopside; nucleants; crystallization behaviour
ID OCCURRING CAO-MGO-AL2O3-SIO2 MATERIALS; ALUMINOSILICATE GLASS;
CRYSTAL-GROWTH; NUCLEATION; SLAG; KINETICS; SYSTEM
AB The effects of Cr2O3, Fe2O3 and TiO2 on the crystallization behaviour of glass
compositions in the SiO2-Al2O3-CaO-MgO(R2O) system were investigated by DTA, XRD
and SEM. It was shown that the simultaneous addition of Cr2O3, Fe2O3 and TiO2 was
more effective in inducing bulk crystallization in these glasses. The Avrami
constant, it, and activation energy for crystallization of the most promising glass
specimens were determined as 3.23 and 253.600/mol, respectively, suggesting a two-
dimensional bulk crystallization mechanism. In this work the best nucleation
temperature was determined to be 740degreesC. The main crystalline phase detected
in the most promising specimens after a two stage 3 It heat treatment at
740degreesC and at 885degreesC was an aluminium diopside. (C) 2004 Elsevier Ltd and
Techna S.H. All rights reserved.
C1 Mat & Energy Res Ctr, Tehran, Iran.
Iran Univ Sci & Technol, Dept Mat, Div Ceram, Tehran, Iran.
C3 Materials & Energy Research Center (MERC); Iran University Science &
Technology
RP Rezvani, M (corresponding author), Mat & Energy Res Ctr, POB 14155-4777, Tehran,
Iran.
EM m_rezvani@scientific.net
RI Solati-Hashjin, Mehran/X-8822-2019; Solati-Hashjin, Mehran/A-5535-2010;
yekta, Bijan Eftekhari/Y-8241-2018
OI Solati-Hashjin, Mehran/0000-0002-1187-1237; Solati-Hashjin,
Mehran/0000-0002-1187-1237;
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Z9 173
U1 2
U2 106
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
J9 CERAM INT
JI Ceram. Int.
PY 2005
VL 31
IS 1
BP 75
EP 80
DI 10.1016/j.ceramint.2004.03.037
PG 6
GA 881IL
UT WOS:000225856600012
DA 2023-12-05
ER
PT J
AU Tsakiridis, PE
AF Tsakiridis, P. E.
TI Aluminium salt slag characterization and utilization - A review
LA English
DT Review
DE Aluminium salt slag; Properties, Utilization; Waste processing
ID DROSS; WASTE; RECOVERY; CAKE; MANAGEMENT; PRODUCTS; METALS; REUSE
AB Aluminium salt slag (also known as aluminium salt cake), which is produced by
the secondary aluminium industry, is formed during aluminium scrap/dross melting
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C1 Natl Tech Univ Athens 9, Dept Mining & Met Engn, Athens 15780, Greece.
C3 National Technical University of Athens
RP Tsakiridis, PE (corresponding author), Natl Tech Univ Athens 9, Dept Mining &
Met Engn, Iroon Polytechniou St, Athens 15780, Greece.
EM ptsakiri@central.ntua.gr
RI Tsakiridis, Petros/AAH-6232-2019
OI Tsakiridis, Petros/0000-0002-2180-2454
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NR 67
TC 149
Z9 167
U1 11
U2 152
PI AMSTERDAM
SN 0304-3894
J9 J HAZARD MATER
PD MAY 30
PY 2012
VL 217
BP 1
EP 10
DI 10.1016/j.jhazmat.2012.03.052
PG 10
GA 941DJ
UT WOS:000303943600001
PM 22480708
DA 2023-12-05
ER
PT J
AU Richardson, IG
Groves, GW
AF Richardson, IG
Groves, GW
TI The structure of the calcium silicate hydrate phases present in hardened
pastes of white Portland cement blast-furnace slag blends
SO JOURNAL OF MATERIALS SCIENCE
LA English
DT Article
ID C-S-H; TRACE-ELEMENTS; GEL; SI-29; MICROSTRUCTURE; MICROANALYSIS;
MODELS; NMR
AB The C-S-H gels present in both water-and alkali-activated hardened pastes of
white Portland cement/blast-furnace slag blends have been studied by solid-state
Si-29 magic angle spinning nuclear magnetic resonance (NMR) spectroscopy and
analytical transmission electron microscopy (TEM). Structural data are obtained by
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aluminium substitutes for silicon at tetrahedral sites; (2) aluminium only
substitutes for silicon in the central tetrahedron of pentameric silicate chains;
(3) the results strengthen confidence in dreierkette-based models for the structure
of C-S-H. Compositional similarities suggest that these conclusions will be true
for OPC/slag blends, and possibly also for OPC/pulverized fuel ash blends
indicating that the same structural model applies to C-S-H gels in a wide range of
hardened cement pastes.
C1 UNIV OXFORD, DEPT MAT, OXFORD OX1 3PH, ENGLAND.
C3 University of Oxford
RP Richardson, IG (corresponding author), UNIV LEEDS, DEPT CIVIL ENGN, MAT UNIT,
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NR 29
TC 148
Z9 169
U1 0
U2 26
PU SPRINGER
PI NEW YORK
PA ONE NEW YORK PLAZA, SUITE 4600, NEW YORK, NY, UNITED STATES
SN 0022-2461
EI 1573-4803
J9 J MATER SCI
JI J. Mater. Sci.
PD SEP 15
PY 1997
VL 32
IS 18
BP 4793
EP 4802
DI 10.1023/A:1018639232570
PG 10
WC Materials Science, Multidisciplinary
GA XY095
UT WOS:A1997XY09500007
DA 2023-12-05
ER
PT J
AU Li, YJ
Su, MY
Xie, X
Wu, SM
Liu, CT
AF Li, Yingjie
Su, Mengying
Xie, Xin
Wu, Shuimu
Liu, Changtian
TI CO2 capture performance of synthetic sorbent prepared from
carbide slag and aluminum nitrate hydrate by combustion synthesis
SO APPLIED ENERGY
LA English
DT Article
DE Carbide slag; Aluminum nitrate hydrate; Synthetic CO2 sorbent;
Combustion synthesis; CO2 capture
ID CALCIUM-BASED SORBENT; THERMAL-ENERGY STORAGE; CARBON CAPTURE; CAO;
ENHANCEMENT; TEMPERATURE; CAPACITY; PELLETS; ASH
AB A new CO2 sorbent was prepared from carbide slag, aluminum nitrate hydrate and
glycerol water solution by combustion synthesis method. The effects of the sorbent
preparation conditions (glycerol addition, combustion synthesis temperature, ratio
of carbide slag to aluminum nitrate hydrate) and carbonation/calcination conditions
(temperature, atmosphere and time) on CO2 capture performance of the synthetic
sorbent were investigated in the calcium looping cycles. The addition of glycerol
during the sorbent preparation exhibits an improvement on the cyclic CO2 capture
capacity. It was also found that the optimal combustion synthesis temperature for
the synthetic sorbent was in the range of 750-800 degrees C. The synthetic sorbent
contained the mass ratio of CaO derived from carbide slag to Al2O3 derived from
aluminum nitrate hydrate = 90:10 exhibited higher CO2 capture capacity (038 g CO2/g
sorbent after 50 cycles). X-ray diffraction analysis showed that the main compounds
of the synthetic sorbent were CaO and Ca(3A)l(2)O(6) by X-ray diffraction analysis.
The synthetic sorbent showed higher CO2 capture capacity than the carbide slag
under severe calcination conditions (950 degrees C, CO2) and at short carbonation
time (<5 min). From the present investigation, it shows that a high active
synthetic CO2 sorbent could be obtained using the carbide slag in the calcium
looping technology. (C) 2015 Elsevier Ltd. All rights reserved.
C1 [Li, Yingjie; Xie, Xin; Wu, Shuimu; Liu, Changtian] Shandong Univ, Sch Energy &
Power Engn, Jinan 250061, Peoples R China.
[Su, Mengying] Univ Alabama, Dept Chem & Mat Engn, Huntsville, AL 35805 USA.
C3 Shandong University; University of Alabama System; University of Alabama
Huntsville
RP Li, YJ (corresponding author), Shandong Univ, Sch Energy & Power Engn, Jinan
EM liyj@sdu.edu.cn
FU National Natural Science Foundation of China [51376003]
FX Financial support from the National Natural Science Foundation of China
(51376003) is gratefully appreciated.
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NR 43
TC 146
Z9 155
U1 1
U2 129
PU ELSEVIER SCI LTD
PI OXFORD
SN 0306-2619
EI 1872-9118
J9 APPL ENERG
JI Appl. Energy
PD MAY 1
PY 2015
VL 145
BP 60
EP 68
DI 10.1016/j.apenergy.2015.01.061
PG 9
WC Energy & Fuels; Engineering, Chemical
SC Energy & Fuels; Engineering
GA CG0ZF
UT WOS:000353002100008
DA 2023-12-05
ER
PT J
AU Komljenovic, M
Bascarevic, Z
Marjanovic, N
Nikolic, V
AF Komljenovic, M.
Bascarevic, Z.
Marjanovic, N.
Nikolic, V.
TI External sulfate attack on alkali-activated slag
LA English
DT Article
DE External sulfate attack; Sodium sulfate; Alkali-activated slag;
Portland-slag cement
ID CONCRETE INCORPORATING GGBS; PORTLAND-CEMENT; BLENDED CEMENTS;
SODIUM-SULFATE; RESISTANCE; MORTARS; DURABILITY; PERFORMANCE; HYDRATION;
STRENGTH
AB This paper analyses the effects of external sulfate attack (5% Na2SO4 solution)
on mechanical and microstructural properties of alkali-activated slag (AAS).
Portland-slag cement (CEM II/A-S 42.5N) was used as a benchmark material.
External sulfate attack led to a decrease in strength of CEM II, but not of AAS.
Under the investigated experimental conditions, AAS showed significantly higher
resistance to sulfate attack with respect to the benchmark CEM II. A very
pronounced resistance of AAS to sulfate attack can be explained by the absence of
portlandite and unavailability of aluminum, present in C-S-H(I) and hydrotalcite
gels, for the reaction with sulfates. (C) 2013 Elsevier Ltd. All rights reserved.
C1 [Komljenovic, M.; Bascarevic, Z.; Marjanovic, N.; Nikolic, V.] Univ Belgrade,
Inst Multidisciplinary Res, Belgrade 11001, Serbia.
C3 University of Belgrade
RP Bascarevic, Z (corresponding author), Univ Belgrade, Inst Multidisciplinary Res,
Belgrade 11001, Serbia.
EM zvezdana@imsi.bg.ac.rs
RI Miroslav, Komljenovic/H-8557-2019
OI Miroslav, Komljenovic/0000-0001-5322-6984; Nikolic,
Violeta/0000-0003-0933-3197; Dzunuzovic, Natasa/0000-0001-9548-114X
FU Ministry of Education, Science and Technological Development of the
Republic of Serbia; [TR34026]
FX This work was carried out within the Project TR34026. The authors are
grateful to the Ministry of Education, Science and Technological
Development of the Republic of Serbia for financial support. We also
thank Dr. Aleksandra Rosic (Faculty of Mining and Geology, Belgrade
University) for XRD analysis.
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8846(03)00125-X
8846(01)00659-7
8846(01)00574-9
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10.1016/j.conbuildmat.2012.12.067
10.1016/j.cemconres.2010.11.016
10.1016/j.cemconres.2010.08.017
8846(02)00717-2
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8
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8846(96)00089-0
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8846(03)00222-9
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8846(02)00955-9
8846(02)00724-X
8846(01)00510-5
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9465(03)00160-4
9015-9
Van Tittelboom K., 2009, CONCRETE AGGRESSIVE, P298
Veiga KK, 2012, CONSTR BUILD MATER, V34, P494, DOI
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10.1016/j.cemconres.2010.02.001
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NR 60
TC 145
Z9 157
U1 12
U2 105
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD DEC
PY 2013
VL 49
BP 31
EP 39
DI 10.1016/j.conbuildmat.2013.08.013
PG 9
GA 281DT
UT WOS:000329080900005
DA 2023-12-05
ER
PT J
AU Zhou, Q
Milestone, NB
Hayes, M
AF Zhou, Q.
Milestone, N. B.
Hayes, M.
TI An alternative to Portland Cement for waste encapsulation - The calcium
sulfoaluminate cement system
LA English
CT 7th International Conference on Protection and Restoration of the
Environment
CY JUL, 2004
CL Mykonos Isl, GREECE
DE calcium sulfoaluminate cement; ettringite; waste encapsulation
ID ETTRINGITE; PERFORMANCE
AB Currently, Portland Cement (PC) is used extensively in the
solidification/stabilisation of a wide variety of wastes. In the nuclear industry,
low and intermediate level radioactive wastes are encapsulated or immobilised
within composite PC cement systems based on high replacement with blast furnace
slag or fly ash. However, the high alkalinity of these PC-based systems will
corrode reactive metals found in some wastes releasing hydrogen and forming
expansive corrosion products. Alternative cement systems could provide a different
hydration chemistry, which would allow wastes containing these metals to be
encapsulated with lower reactivity. Calcium sulfoaluminate (C (S) over barA) cement
is one such cement. It combines economy of cost and low emission of CO2 with rapid
strength gain and compatibility with other construction materials. Hydration
provides an internal pore solution where the pH is considerably lower than that of
PC. The main hydration product, ettringite, can incorporate a number of ions into
its crystal structure, making it an ideal candidate for waste immobilisation.
This paper details some results from a commercial C (S) over barA system that
examines aspects of mixing, hydration of different formulations and aluminium
corrosion behaviour. The fluidity of mixes can be adjusted by changing the
formulations. All designed mixes were set within 24 h with little bleeding and the
pH values were in the range of 10-11.5. In addition, a significant reduction in Al
corrosion was observed compared to a composite OPC system. Although these results
provide encouragement for the idea that C (S) over barA cement can provide a
possible alternative to PC in the immobilisation of difficult and reactive wastes,
further investigation is needed. (c) 2005 Elsevier B.V. All rights reserved.
C1 Univ Sheffield, Immobilisat Sci Lab, Dept Mat Engn, Sheffield S1 3JD, S
Yorkshire, England.
RP Zhou, Q (corresponding author), Univ Sheffield, Immobilisat Sci Lab, Dept Mat
Engn, Mappin St, Sheffield S1 3JD, S Yorkshire, England.
EM q.zhou@sheffield.ac.uk; n.b.milestone@sheffield.ac.uk;
martin.hayes@nexiasolutions.com
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NR 24
TC 143
Z9 154
U1 3
U2 58
PI AMSTERDAM
SN 0304-3894
J9 J HAZARD MATER
PD AUG 10
PY 2006
VL 136
IS 1
SI SI
BP 120
EP 129
DI 10.1016/j.jhazmat.2005.11.038
PG 10
WE Conference Proceedings Citation Index - Science (CPCI-S); Science Citation Index
Expanded (SCI-EXPANDED)
GA 062FW
UT WOS:000238931000014
PM 16406289
DA 2023-12-05
ER
PT J
AU Okuyama, G
Yamaguchi, K
Takeuchi, S
Sorimachi, K
AF Okuyama, G
Yamaguchi, K
Takeuchi, S
Sorimachi, K
TI Effect of slag composition on the kinetics of formation of
Al2O3-MgO inclusions in aluminum killed ferritic
stainless steel
SO ISIJ INTERNATIONAL
LA English
DT Article
DE secondary steelmaking; stainless steel; slag; inclusion
AB Kinetics of both slag/metal reactions and metal/inclusion reactions were
investigated experimentally using 20 kg vacuum induction furnace in order to
clarify the mechanism of the formation Of MgAl2O4 spinel inclusions in aluminum
killed ferritic stainless steel (SUS430). The results obtained are summarized as
follows :
1) By reducing CaO/SiO2 and CaO/Al2O3 ratio of top slag, MgO contents in Al2O3
based inclusions decreased.
2) The two film theory was employed to analyze the rate determining step of
slag/metal reaction (reduction of MgO in top slag). By this model, it was found
that the rate determining step of the reaction was the mass transfer of Mg through
the film in molten steel. The increase rate of Mg in molten steel is determined by
the activities of soluble oxygen and MgO at the slag/metal interface, and hence by
slag composition.
3) The unreacted core model was employed to analyze the rate determining step of
metal/inclusions reaction.
The analysis showed that the rate determining step of the reaction in the case
of 20 kg vacuum induction furnace was the diffusion of Mg in molten steel.
C1 Kawasaki Steel Corp, Tech Res Labs, Chuo Ku, Chiba 2600835, Japan.
C3 Kawasaki Heavy Industries
RP Okuyama, G (corresponding author), Kawasaki Steel Corp, Tech Res Labs, Chuo Ku,
Chiba 2600835, Japan.
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PU IRON STEEL INST JAPAN KEIDANREN KAIKAN
PI TOKYO
PA 9-4 OTEMACHI 1-CHOME CHIYODA-KU, TOKYO, 100, JAPAN
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VL 40
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BP 121
EP 128
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PG 8
WC Metallurgy & Metallurgical Engineering
SC Metallurgy & Metallurgical Engineering
GA 290EA
UT WOS:000085662200004
OA gold
DA 2023-12-05
ER
PT J
AU Mahinroosta, M
Allahverdi, A
AF Mahinroosta, Mostafa
Allahverdi, Ali
TI Hazardous aluminum dross characterization and recycling strategies: A
critical review
SO JOURNAL OF ENVIRONMENTAL MANAGEMENT
LA English
DT Review
DE Aluminum dross; Waste recycling; Waste treatment; Hazardous waste;
Recovery
ID ALN-POLYTYPOID CERAMICS; BLACK DROSS; RAW-MATERIAL; RED MUD; CEMENT
MORTARS; GAMMA-ALUMINA; SALT CAKES; WASTE; RECOVERY; SLAG
AB By finding appropriate recycling approaches, the volume of wastes, corresponding
disposal cost, and the pollution of environment could be diminished. Also, such
promising approaches can result in the conservation of natural sources and economic
benefits. Aluminum dross as a hazardous solid waste in aluminum production
industries has caused serious environmental and public health challenges. Various
methods have been introduced for management, utilization, and recycling of the
waste. The present review describes, firstly, different types of aluminum dross,
their environmental and health hazards, composition, and production process and
then focuses on the direct and indirect recycling approaches and recovery
strategies.
C1 [Mahinroosta, Mostafa; Allahverdi, Ali] Iran Univ Sci & Technol, Sch Chem Engn,
Res Lab Inorgan Chem Proc Technol, Tehran 1684613114, Iran.
[Allahverdi, Ali] Iran Univ Sci & Technol, Cement Res Ctr, Tehran 1684613114,
Iran.
C3 Iran University Science & Technology; Iran University Science &
Technology
RP Allahverdi, A (corresponding author), Iran Univ Sci & Technol, Sch Chem Engn,
Res Lab Inorgan Chem Proc Technol, Tehran 1684613114, Iran.
EM m_mahinroosta@chemeng.iust.ac.ir; ali.allahverdi@iust.ac.ir
RI Mahinroosta, Mostafa/J-5436-2016; Allahverdi, Ali/S-8924-2018
OI Mahinroosta, Mostafa/0000-0001-9709-2949; Allahverdi,
Ali/0000-0002-8988-9226
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NR 174
TC 139
Z9 143
U1 11
U2 199
PU ACADEMIC PRESS LTD- ELSEVIER SCIENCE LTD
PI LONDON
PA 24-28 OVAL RD, LONDON NW1 7DX, ENGLAND
SN 0301-4797
EI 1095-8630
J9 J ENVIRON MANAGE
JI J. Environ. Manage.
PD OCT 1
PY 2018
VL 223
BP 452
EP 468
DI 10.1016/j.jenvman.2018.06.068
PG 17
WC Environmental Sciences
SC Environmental Sciences & Ecology
GA GQ9AE
UT WOS:000442057500044
PM 29957419
DA 2023-12-05
ER
PT J
AU Chen, DS
Zhao, LS
Liu, YH
Qi, T
Wang, JC
Wang, LN
AF Chen, Desheng
Zhao, Longsheng
Liu, Yahui
Qi, Tao
Wang, Jianchong
Wang, Lina
TI A novel process for recovery of iron, titanium, and vanadium from
titanomagnetite concentrates: NaOH molten salt roasting and water
leaching processes
LA English
DT Article
DE Titanomagnetite concentrates; Rich titanium-vanadium slag; NaOH molten
salt roasting; Water leaching
ID DECOMPOSITION; SLAG
AB A novel process for recovering iron, titanium, and vanadium from titanomagnetite
concentrates has been developed. In the present paper, the treatment of rich
titanium-vanadium slag by NaOH molten salt roasting and water leaching processes is
investigated. In the NaOH molten salt roasting process, the metallic iron is
oxidized into ferriferous oxide, MgTi2O5 is converted to NaCl-type structure of
Na2TiO3, and M3O5 (M = Ti, Mg, Fe) is converted to alpha-NaFeO2-type structure of
NaMO2, respectively. Roasting temperature and NaOH-slag mass ratio played a
considerable role in the conversion of titanium in the rich titanium-vanadium slag
during the NaOH molten salt roasting process. Roasting at 500 degrees C for 60 min
and a 1:1 NaOH-slag mass ratio produces 96.3% titanium conversion. In the water
leaching process, the Na+ was exchanged with H+, Na2TiO3 is converted to undefined
structure of H2TiO3, and NaMO2 is converted to alpha-NaFeO2-type structure of HMO2.
Under the optimal conditions, 87.3% of the sodium, 42.3% of the silicon, 43.2% of
the aluminum, 22.8% of the manganese, and 96.6% of the vanadium are leached out.
Crown Copyright (c) 2012 Published by Elsevier B.V. All rights reserved.
C1 [Chen, Desheng; Zhao, Longsheng; Liu, Yahui; Qi, Tao; Wang, Jianchong; Wang,
Lina] Natl Engn Lab Hydromet Cleaner Prod Technol, Beijing 100190, Peoples R China.
[Chen, Desheng; Zhao, Longsheng; Liu, Yahui; Qi, Tao; Wang, Jianchong; Wang,
Lina] Chinese Acad Sci, Inst Proc Engn, Key Lab Green Proc & Engn, Beijing 100190,
Peoples R China.
C3 Chinese Academy of Sciences; Institute of Process Engineering, CAS;
Chinese Academy of Sciences
RP Wang, LN (corresponding author), Natl Engn Lab Hydromet Cleaner Prod Technol,
Beijing 100190, Peoples R China.
EM linawang@home.ipe.ac.cn
RI Wang, Li-Na/T-7047-2018
OI Wang, Li-Na/0000-0002-9194-3527
FU Major Program of the National Natural Science Foundation of China
[51090380]; National Science Foundation for Distinguished Young Scholars
of China [51125018]; National Natural Science Foundation of China
[51004091, 51104139, 21006115]
FX This work was financially supported by the Major Program of the National
Natural Science Foundation of China (Grant No. 51090380), the National
Science Foundation for Distinguished Young Scholars of China (Grant No.
51125018), and the National Natural Science Foundation of China (Grant
Nos. 51004091, 51104139 and 21006115).
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NR 32
TC 136
Z9 148
U1 12
U2 168
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
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PD JAN 15
PY 2013
VL 244
BP 588
EP 595
DI 10.1016/j.jhazmat.2012.10.052
PG 8
GA 090ST
UT WOS:000315001000069
PM 23177244
DA 2023-12-05
ER
PT J
AU Yi, YL
Gu, LY
Liu, SY
AF Yi, Yaolin
Gu, Liyang
Liu, Songyu
TI Microstructural and mechanical properties of marine soft clay stabilized
by lime-activated ground granulated blastfurnace slag
SO APPLIED CLAY SCIENCE
LA English
DT Article
DE Soft clay stabilization; Ground granulated blastfurnace slag; Lime;
Microstructure; Unconfined compressive strength
ID ENGINEERING PROPERTIES; PARTIAL SUBSTITUTION; GGBS; STRENGTH; SOILS
AB Although Portland cement (PC) is widely used for marine soft clay stabilization,
there are significant environmental impacts associated with its production. Hence,
the use of industrial by-products has been encouraged. In this paper, quicklime and
hydrated lime were used to activate ground granulated blastfurnace slag (GGBS), a
by-product of the steel industry, for stabilization of marine soft clay in
comparison to PC. X-ray diffraction (XRD), scanning electron microscopy (SEM),
mercury intrusion porosimetry (MIP), and unconfined compressive strength (UCS),were
used to investigate the microstructural and mechanical properties of stabilized
clays. The microstructural analysis results revealed that the main hydration
products in the two types of lime-GGBS stabilized clays were calcium silicate
hydrates (CSH), calcium aluminates (CAH), calcium aluminum silicate hydrates
(CASH), and alumino-ferrite monosulfate (AFm), and both types of lime-activated
GGBS stabilized clays could yield lower porosity than PC stabilized clay. The UCS
results demonstrated that hydrated lime-activated GGBS achieved slightly higher 90-
day UCS in stabilized clay than quicklime-activated GGBS, and the optimum 90-day
UCS, with a lime/GGBS ratio of 0.10, was 1.7 times that of PC stabilized clay. This
study indicated that both environmental and economical benefits could be expected
from replacing PC with lime-GGBS for soft clay stabilization. (C) 2014 Elsevier
B.V. All rights reserved.
C1 [Yi, Yaolin; Liu, Songyu] Southeast Univ, Inst Geotech Engn, Nanjing 210096,
Jiangsu, Peoples R China.
[Yi, Yaolin] Univ Alberta, Dept Civil & Environm Engn, Edmonton, AB T6G 2W2,
Canada.
[Gu, Liyang] Columbia Univ, Dept Civil Engn & Engn Mech, New York, NY 10027 USA.
C3 Southeast University - China; University of Alberta; Columbia University
RP Yi, YL (corresponding author), Southeast Univ, Sch Transportat, Inst Geotech
Engn, 2 Sipailou, Nanjing 210096, Jiangsu, Peoples R China.
EM yaolin@ualbertac.ca
RI Yi, Yaolin/X-5412-2019; Yi, Yaolin/L-1379-2016
OI Yi, Yaolin/0000-0002-1188-3799; Yi, Yaolin/0000-0002-1188-3799
FU National Science and Technology Pillar Program [2012BAJ01B02-01];
Natural Science Foundation of China [41330641]
FX The authors would like to thank Pengfei Guo, Zhao Wang, and Sheng Chang
at Southeast University, for their assistance in laboratory testing, and
Lauren Wozny at the University of Alberta, for the technical writing
check of the paper. The funding provided by the National Science and
Technology Pillar Program (2012BAJ01B02-01) and Natural Science
Foundation of China (41330641) is appreciated. The authors sincerely
appreciate the Editor's and Reviewers' comments, which have improved the
quality of the paper significantly.
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TC 135
Z9 140
U1 9
U2 76
PU ELSEVIER
PI AMSTERDAM
SN 0169-1317
EI 1872-9053
J9 APPL CLAY SCI
JI Appl. Clay Sci.
PD JAN
PY 2015
VL 103
BP 71
EP 76
DI 10.1016/j.clay.2014.11.005
PG 6
WC Chemistry, Physical; Materials Science, Multidisciplinary; Mineralogy
SC Chemistry; Materials Science; Mineralogy
GA AY5DL
UT WOS:000347593300011
DA 2023-12-05
ER
PT J
AU Ganesh, I
Bhattacharjee, S
Saha, BP
Johnson, R
Rajeshwari, K
Sengupta, R
Rao, MVR
Mahajan, YR
AF Ganesh, I
Bhattacharjee, S
Saha, BP
Johnson, R
Rajeshwari, K
Sengupta, R
Rao, MVR
Mahajan, YR
TI An efficient MgAl2O4 spinel additive for improved
slag erosion and penetration resistance of
high-Al2O3 and MgO-C refractories
LA English
DT Article
DE MgAl2O4; AlCl3; high Al2O3; MgO-C; slag erosion; slag penetration;
permanent linear change; EPMA
ID MAGNESIUM ALUMINATE SPINEL; BEHAVIOR
AB A stoichiometric dense MgAl2O4 spinel has been prepared according to a
conventional double stage firing process using AlCl3 as a sintering aid. A
stoichiometric mixture of aluminum trihydroxide and caustic MgO was calcined at
1300 degreesC for 1 h in order to achieve a desired degree of spinelization. AlCl3
in different amounts, i.e. 0.911, 1.822 and 2.733 wt.%, was coated on spinelized
powder using wet-impregnation technique and sintered at different temperatures
ranging from 1500 to 1600 degreesC for 1 h. Among the spinels sintered at 1550
degreesC for 1 h. spinel incorporated with 2.733 wt% AlCl3 has exhibited superior
properties in terms of bulk density, apparent porosity and water absorption.
Further, this sintered stoichiometric spinel incorporated with 2.733 wt.% AlCl3 was
characterized by means of scanning electron microscopy (SEM), energy dispersive
analysis with X-rays (EDAX) and electron probe microanalysis (EPMA). EDAX analysis
revealed that AlCl3 as a sintering aid helps in reducing the Na2O present in the
raw materials composition after sintering. EPMA studies revealed that spinel
prepared in this study is well comparable with the commercial spinel (Alcoa, AR-78,
USA). Finally, 20 wt.% of the stoichiometric spinel incorporated with 2.733 wt.%
AlCl3 prior to sintering was added to high-Al2O3 and MgO-C refractories to evaluate
its effect on slag erosion and penetration resistance as well as on repeated
permanent linear change (PLC) of these bricks. By the addition of stoichiometric
MgAl2O4 spinel, the slag erosion and penetration resistance of high Al2O3 and MgO-C
refractories was improved remarkably, and their PLCs exhibited more steady and
stable positive values after spinel addition. (C) 2002 Elsevier Science Ltd and
Techna S.r.l. All rights reserved.
C1 Int Adv Res Ctr Powder Met & New Mat, Ceram Mat Div, Hyderabad 500005, Andhra
Pradesh, India.
White Circle Oxides Ltd, Hyderabad 500020, Andhra Pradesh, India.
C3 Department of Science & Technology (India); International Advanced
Research Centre for Powder Metallurgy & New Materials (ARCI)
RP Mahajan, YR (corresponding author), Int Adv Res Ctr Powder Met & New Mat, Ceram
Mat Div, Balapur PO, Hyderabad 500005, Andhra Pradesh, India.
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NR 30
TC 135
Z9 150
U1 0
U2 33
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
J9 CERAM INT
JI Ceram. Int.
PY 2002
VL 28
IS 3
BP 245
EP 253
AR PII S0272-8842(01)00086-4
DI 10.1016/S0272-8842(01)00086-4
PG 9
GA 547BC
UT WOS:000175311600003
DA 2023-12-05
ER
PT J
AU Mozgawa, W
Deja, J
AF Mozgawa, W.
Deja, J.
TI Spectroscopic studies of alkaline activated slag geopolymers
SO JOURNAL OF MOLECULAR STRUCTURE
LA English
CT 29th European Congress on Molecular Spectroscopy
CY AUG 31-SEP 05, 2008
CL Opatija, CROATIA
DE Slag geopolymers; Alkaline activation; IR spectroscopy; NMR spectroscopy
ID INFRARED-SPECTROSCOPY; CEMENT; SI-29
AB In the work, results of structural studies of different geopolymers, obtained
using a granulated blast furnace slag, are presented. The slag Was Subjected to an
alkaline activation process. As activators, NaOH, Na2CO3 and liquid glass were
applied. IR and NMR spectroscopy were the main experimental methods used, the
results obtained were compared with XRD phase analysis and SEM observations. In the
IR spectra of raw slag as well as in the spectra of products of paste hydration,
the bands due to the characteristic vibrations of bonds observed in both types of
oxygen bridges: Si-O-Si and Si-O-Al, were assigned. These bridges constitute basic
structural units, forming tetrahedral geopolymer chains. It was found that the slag
composition, mainly SiO2/Al2O3 ratio and modification in oxides concentration,
influences the presence of the bands connected with the phases (mainly C-S-H)
formed during the hydration in the IR spectra. Additionally, significant effect of
amorphous phases share on the spectra shape was established. Si-29 and Al-27 MAS-
NMR spectra of initial slag geopolymers and pastes provided information concerning
coordination of both atoms in the structures. It was revealed that the kind of slag
geopolymers and the conditions of paste hydration influence connectedness of
silicooxygen tetrahedra and coordination number of aluminium atoms. Based on IR
spectra, it was also possible to determine the influence of the activator type,
activation time and hydration conditions on the products formed. Significant
changes were observed for the bands assigned to vibrations of carbonate and
hydroxide groups. The changes were also noticed in the case of bands due to
vibrations of silicate and aluminosilicate bonds. (C) 2008 Elsevier B.V. All rights
reserved.
C1 [Mozgawa, W.; Deja, J.] AGH Univ Sci & Technol, Fac Mat Sci & Ceram, PL-30059
Krakow, Poland.
C3 AGH University of Krakow
RP Mozgawa, W (corresponding author), AGH Univ Sci & Technol, Fac Mat Sci & Ceram,
Al Mickiewicza 30, PL-30059 Krakow, Poland.
EM mozgawa@agh.edu.pl
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NR 27
TC 134
Z9 140
U1 5
U2 50
PU ELSEVIER
PI AMSTERDAM
SN 0022-2860
EI 1872-8014
J9 J MOL STRUCT
JI J. Mol. Struct.
PD APR 30
PY 2009
VL 924
SI SI
BP 434
EP 441
DI 10.1016/j.molstruc.2008.12.026
PG 8
WC Chemistry, Physical
SC Chemistry
GA 452XJ
UT WOS:000266574200067
DA 2023-12-05
ER
PT J
AU Aubert, JE
Husson, B
Sarramone, N
AF Aubert, J. E.
Husson, B.
Sarramone, N.
TI Utilization of municipal solid waste incineration (MSWI) fly ash in
blended cement. Part 1: Processing and characterization of MSWI fly ash
LA English
DT Article
DE waste management; municipal solid waste incineration; fly ash;
stabilization process; characterization
ID HEAVY-METAL STABILIZATION; BOTTOM ASH; IMMOBILIZATION; RESIDUES;
BEHAVIOR
AB This paper is the first of a series of two articles dealing with the processes
applied to MSWI fly ash with a view to reusing it safely in cement-based materials.
Part 1 presents two stabilization processes and Part 2 deals with the use of the
two treated fly ashes (TFA) in mortars. Two types of binder were used: an Ordinary
Portland Cement (OPC) containing more than 95% clinker (CEM I 52.5R) and a binary
blend cement composed of 70% ground granulated blast furnace slag and 30% clinker
(CEM III-B 42.5N).
In this first part, two stabilization processes are presented: the conventional
process, called "A", based on the washing, phosphation and calcination of the ash,
and a modified process, called "B", intended to eliminate metallic aluminum and
sulfate contained in the ash. The physical, chemical and mineralogical
characteristics of the two TFA were comparable. The main differences observed were
those expected, i.e. TFA-B was free of metallic aluminum and sulfate. The
mineralogical characterization of the two TFAs highlighted the presence of large
amounts of a calcium aluminosilicate phase taking two forms, a crystalline form
(gehlenite) and an amorphous form. Hydration studies on pastes containing mixed TFA
and calcium hydroxide showed that this phase reacted with calcium hydroxide to form
calcium aluminate hydrates. This formation of hydrates was accompanied by a
hardening of the pastes. These results are very encouraging for the reuse of such
TFA in cement-based materials because they can be considered as pozzolanic
additions and could advantageously replace a part of the cement in cement-based
materials. Finally, leaching tests were carried out to evaluate the environmental
impact of the two TFAs. The elements which were less efficiently stabilized by
process A were zinc, cadmium and antimony but, when the results of the leaching
tests were compared with the thresholds of the European landfill directive, TFA-A
could nevertheless be accepted at landfills for non-hazardous waste. The
modifications of the process led to a significant reduction in the stabilization of
chromium, selenium and antimony. (c) 2006 Elsevier B.V. All rights reserved.
C1 UPS, INSA, LMDC, F-31077 Toulouse 4, France.
C3 Universite de Toulouse; Universite Toulouse III - Paul Sabatier;
Universite Federale Toulouse Midi-Pyrenees (ComUE); Institut National
des Sciences Appliquees de Toulouse
RP Aubert, JE (corresponding author), UPS, INSA, LMDC, 135 Ave Rangueil, F-31077
Toulouse 4, France.
EM aubert@insa-toulouse.fr
CR Aubert J. E., 2002, THESIS U P SABATIER
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NR 32
TC 134
Z9 148
U1 7
U2 101
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD AUG 25
PY 2006
VL 136
IS 3
BP 624
EP 631
DI 10.1016/j.jhazmat.2005.12.041
PG 8
GA 079WX
UT WOS:000240209700030
PM 16442718
DA 2023-12-05
ER
PT J
AU Li, C
Wan, JH
Sun, HH
Li, LT
AF Li, Chao
Wan, Jianhua
Sun, Henghu
Li, Longtu
TI Investigation on the activation of coal gangue by a new compound method
LA English
DT Article
DE Coal gangue; Compound mechanical-hydro-thermal activation (CMHTA);
Traditional mechanical-thermal activation (TMTA)
ID C-S-H; CEMENTITIOUS MATERIALS; POLYMERIZATION; SPECTROSCOPY;
COORDINATION; KAOLINITE; ALUMINUM; MULLITE; SI-29; SLAG
AB In order to comprehensively utilize coal gangue as the main raw material in
cementitious materials, improving its cementitious activity is a question of
fundamental importance. In this paper, we present a new compound mechanical-hydro-
thermal activation (CMHTA) technology to investigate the activation effect of coal
gangue, and the traditional mechanical-thermal activation (TMTA) technology was
used as reference. The purpose of this study is to give a detailed comparison
between these two methods with regard to the mineral composition, crystal structure
and microstructure, by XRD, IR, MAS NMR, XPS and mechanical property analysis. The
prepared coal gangue based blended cement, containing 52% of activated coal gangue
C (by CMHTA technology), has a better mechanical property than activated coal
gangue T (by TMTA technology) and raw coal gangue. The results show that both of
the TMTA and CMHTA technologies can improve the cementitious activity of raw gangue
greatly. Moreover, compared with TMTA, the mineral phases such as feldspar and
muscovite in raw coal gangue were partially decomposed, and the crystallinity of
quartz decreased, due to the effect of adding CaO and hydro-thermal process of
CMHTA technology. (C) 2010 Elsevier B.V. All rights reserved.
C1 [Li, Chao; Sun, Henghu; Li, Longtu] Tsinghua Univ, Dept Mat Sci & Engn, State
Key Lab New Ceram & Fine Proc, Beijing 100084, Peoples R China.
[Wan, Jianhua] China Univ Min & Technol, Sch Resource & Safety Engn, Beijing
[Sun, Henghu] Univ Pacific, Sch Engn & Comp Sci, Stockton, CA 95211 USA.
C3 Tsinghua University; China University of Mining & Technology; University
of the Pacific
RP Li, C (corresponding author), Tsinghua Univ, Dept Mat Sci & Engn, State Key Lab
New Ceram & Fine Proc, Room 2307,YIFU Sci & Technol Bldg, Beijing 100084, Peoples R
China.
EM chao-li07@mails.tsinghua.edu.cn
RI li, long/HOF-6990-2023
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10.1016/j.cemconres.2004.11.004
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5
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NR 24
TC 133
Z9 149
U1 7
U2 170
PI AMSTERDAM
SN 0304-3894
J9 J HAZARD MATER
PD JUL 15
PY 2010
VL 179
IS 1-3
BP 515
EP 520
DI 10.1016/j.jhazmat.2010.03.033
PG 6
GA 609AI
UT WOS:000278626700070
PM 20359819
DA 2023-12-05
ER
PT J
AU Schöler, A
Lothenbach, B
Winnefeld, F
Ben Haha, M
Zajac, M
Ludwig, HM
AF Schoeler, Axel
Lothenbach, Barbara
Winnefeld, Frank
Ben Haha, Mohsen
Zajac, Maciej
Ludwig, Horst-Michael
TI Early hydration of SCM-blended Portland cements: A pore solution and
isothermal calorimetry study
LA English
DT Article
DE Blended cements; Supplementary cementitious materials; Early hydration;
Pore solution chemistry; Kinetics
ID TRICALCIUM SILICATE; FLY-ASH; ALITE HYDRATION; SECONDARY COMPONENT;
POTASSIUM HYDROXIDE; HEAT-FLOW; FILLER; SODIUM; RATIO; OPC
AB In this study the hydration kinetics and the development of concentrations in
the pore solution of cement pastes containing different supplementary cementitious
materials (blast-furnace slag, Si-rich fly ash, limestone, quartz) at a cement
replacement of 50 wt.% were investigated during the first 6 h of hydration. The
results indicate that the degree of undersaturation with respect to alite is the
primary factor driving the early hydration kinetics. The accelerating effect of the
limestone is related to a higher undersaturation. The data reveal also that high
aluminium and sulfate concentrations, which depend on the type and chemical
composition of the used mineral addition, retard the reaction. High calcium
concentrations had no adverse effect on hydration kinetics. The investigations
underpin that the mechanisms controlling the early hydration are a complex
combination of the filler effect, the pore solution chemistry as well as intrinsic
reactivity of the mineral additions and their surface characteristics. (C) 2016
C1 [Schoeler, Axel; Lothenbach, Barbara; Winnefeld, Frank] Empa, Swiss Fed Labs Mat
Sci & Technol, Lab Concrete & Construct Chem, Uberlandstrasse 129, CH-8600
Dubendorf, Switzerland.
[Ben Haha, Mohsen; Zajac, Maciej] HeidelbergCement Technol Ctr GmbH, Rohrbacher
Str 95, D-69181 Leimen, Germany.
[Ludwig, Horst-Michael] Bauhaus Univ Weimar, Inst Bldg Mat Sci, Coudraystrasse
11, D-99423 Weimar, Germany.
Laboratories for Materials Science & Technology (EMPA);
Bauhaus-Universitat Weimar
RP Schöler, A (corresponding author), Empa, Swiss Fed Labs Mat Sci & Technol, Lab
Concrete & Construct Chem, Uberlandstrasse 129, CH-8600 Dubendorf, Switzerland.
EM axel.schoeler@freenet.de
RI Lothenbach, Barbara/C-6275-2013; Zajac, Maciej/AAP-8225-2020; Winnefeld,
Frank/B-5335-2009; Ben Haha, Mohsen/AAC-4859-2020
OI Lothenbach, Barbara/0000-0002-9020-6488; Winnefeld,
Frank/0000-0002-6864-6196; Ben Haha, Mohsen/0000-0001-7570-326X;
Scholer, Axel/0000-0002-2463-0926
FU HeidelbergCement, Leimen, Germany
FX This study was financially and analytically supported by
HeidelbergCement, Leimen, Germany. The authors wish to acknowledge F.
Bellmann (Bauhaus University Weimar) for helpful and inspiring
discussions.
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NR 47
TC 132
Z9 140
U1 8
U2 103
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD MAR
PY 2017
VL 93
BP 71
EP 82
DI 10.1016/j.cemconres.2016.11.013
PG 12
GA EP7JB
UT WOS:000397553000007
DA 2023-12-05
ER
PT J
AU Vasudevan, S
Lakshmi, J
Jayaraj, J
Sozhan, G
AF Vasudevan, Subramanyan
Lakshmi, Jothinathan
Jayaraj, Jeganathan
Sozhan, Ganapathy
TI Remediation of phosphate-contaminated water by electrocoagulation with
aluminium, aluminium alloy and mild steel anodes
LA English
DT Article
DE Electrocoagulation; Phosphate; Aluminium alloy anode; Kinetics; Isotherm
ID INDUSTRIAL SOLID-WASTE; BLAST-FURNACE SLAGS; AQUEOUS-SOLUTIONS;
PHOSPHORUS REMOVAL; ADSORPTION; SPECIATION; RAW
AB The present study provides an electrocoagulation process for the remediation of
phosphate-contaminated water using aluminium, aluminium alloy and mild steel as the
anodes and stainless steel as the cathode. The various parameters like effect of
anode materials, effect of pH, concentration of phosphate, current density,
temperature and co-existing ions, and so forth, and the adsorption capacity was
evaluated using both Freundlich and Langmuir isotherm models. The adsorption of
phosphate preferably fitting the Langmuir adsorption isotherm suggests monolayer
coverage of adsorbed molecules. The results showed that the maximum removal
efficiency of 99% was achieved with aluminium alloy anode at a current density of
0.2 A dm(-2), at a pH of 7.0. The adsorption process follows second-order kinetics.
(C) 2008 Elsevier B.V. All rights reserved.
C1 [Vasudevan, Subramanyan; Lakshmi, Jothinathan; Jayaraj, Jeganathan; Sozhan,
Ganapathy] Cent Electrochem Res Inst, Karaikkudi 630006, Tamil Nadu, India.
Central Electrochemical Research Institute (CECRI)
RP Vasudevan, S (corresponding author), Cent Electrochem Res Inst, Karaikkudi
630006, Tamil Nadu, India.
EM svdevan_2000@yahoo.com
RI VASUDEVAN, S./O-5124-2014
OI VASUDEVAN, S./0000-0003-4879-2847
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NR 41
TC 131
Z9 133
U1 1
U2 46
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD MAY 30
PY 2009
VL 164
IS 2-3
BP 1480
EP 1486
DI 10.1016/j.jhazmat.2008.09.076
PG 7
GA 435QM
UT WOS:000265358400152
PM 18977084
DA 2023-12-05
ER
PT J
AU Chung, Y
Cramb, AW
AF Chung, Y
Cramb, AW
TI Dynamic and equilibrium interfacial phenomena in liquid steel-slag
systems
SO METALLURGICAL AND MATERIALS TRANSACTIONS B-PROCESS METALLURGY AND
MATERIALS PROCESSING SCIENCE
LA English
CT Geoffrey Belton Memorial Symposium
CY JAN, 2000
CL SYDNEY, AUSTRALIA
ID ISOTOPE EXCHANGE-REACTION; SURFACE-TENSION; REACTION-KINETICS;
CARBON-DIOXIDE; IRON; ALLOYS; METAL; CO2; DECARBURIZATION; CONTACT
AB The equilibrium interfacial energy between a liquid iron alloy and a liquid slag
is a key physical parameter in the design of steel-refining processes as high
interfacial energies are desired to avoid emulsification of slag in steel and the
creation of casting defects. During a chemical reaction between a liquid iron alloy
droplet and a liquid slag, it is possible to observe by X-ray photography a number
of dynamic interfacial phenomena such as droplet flattening, interfacial
turbulence, and spontaneous emulsification that can potentially lead to serious
processing problems. These dynamic phenomena have been studied during reactions
between Fe-Al and Fe-Ti alloys and silica-containing slags, and the presence of
significant interfacial disturbance has been observed during the times of high
reaction rate between the slag and the metal. It is suggested that interfacial
chemical reactions induce Marangoni and natural convection at the slag-metal
interface. This interfacial flow gives rise to interfacial waves due to a Kelvin-
Helmholtz instability. The waves grow, become unstable, and lead to spontaneous
emulsification of slag in steel and steel in slag. Experiments using industrial
samples and controlled laboratory tests have indicated that this phenomenon may be
more common than once thought and could lead to some serious problems in the
processing of steel alloys containing high quantities of aluminum and/or titanium.
C1 Carnegie Mellon Univ, Dept Mat Sci & Engn, Pittsburgh, PA 15213 USA.
C3 Carnegie Mellon University
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NR 63
TC 131
Z9 138
U1 1
U2 43
PU SPRINGER
PI NEW YORK
PA 233 SPRING ST, NEW YORK, NY 10013 USA
SN 1073-5615
J9 METALL MATER TRANS B
JI Metall. Mater. Trans. B-Proc. Metall. Mater. Proc. Sci.
PD OCT
PY 2000
VL 31
IS 5
BP 957
EP 971
DI 10.1007/s11663-000-0072-5
PG 15
WC Materials Science, Multidisciplinary; Metallurgy & Metallurgical
Engineering
SC Materials Science; Metallurgy & Metallurgical Engineering
GA 365PV
UT WOS:000089960400010
DA 2023-12-05
ER
PT J
AU Cho, JW
Blazek, K
Frazee, M
Yin, HB
Park, JH
Moon, SW
AF Cho, Jung-Wook
Blazek, Kenneth
Frazee, Michael
Yin, Hongbin
Park, Jeong Hyouk
Moon, Sang-Woon
TI Assessment of CaO-Al2O3 Based Mold Flux System for
High Aluminum TRIP Casting
LA English
DT Article
DE mold flux; lime-alumina; alumina pickup; mold heat transfer; lubrication
ID CRYSTALLIZATION BEHAVIOR; HEAT-TRANSFER; VISCOSITY; STEEL; SLAB;
SOLIDIFICATION; RATIO; NA2O; AL; TI
AB Today, the demands for Advanced High Strength Steels (AHSS) have gradually
increased due to their ability to reduce vehicle weight as a means to save energy,
reduce the environmental impact while simultaneously improving passenger safety.
However, AHSS often require the addition of large amounts of alloying elements such
as aluminum and this can make it difficult to cast sound slabs without surface
defects. When casting high aluminum AHSS, due to the reaction between aluminum in
steel and silica in mold flux, the viscosity and crystallization characteristics of
the mold slag changes drastically, and deteriorates mold lubrication. Therefore, it
is critical to limit the reaction between Al in steel and mold slag and at the same
time to provide consistent and adequate mold slag in-use properties. This paper
describes the development of non-traditional lime-alumina based mold fluxes which
have the potential to reduce slag-steel interaction during casting of high aluminum
TRIP steel. Several trial casts of 1.45% Al TRIP steel have been conducted on a
pilot caster to examine the performance of mold fluxes developed. When the lime-
alumina based mold fluxes were applied successfully, alumina pickup was reduced to
less than 5% as compared to 15% alumina pickup for corollary trial casts using
conventional lime-silica mold fluxes. The developed lime-alumna mold fluxes showed
improved in-mold performance as indicated by enhanced lubrication and stable mold
heat transfer, again compared to lime-silica fluxes. Cast slabs from the trials
using these lime-alumina fluxes have periodic and sound oscillation marks and
minimized defects.
C1 [Cho, Jung-Wook] Pohang Univ Sci & Technol, GIFT, Pohang 790784, South Korea.
[Cho, Jung-Wook; Moon, Sang-Woon] POSCO, Steelmaking Res Grp, Tech Res Lab,
Pohang 790785, South Korea.
[Blazek, Kenneth; Yin, Hongbin] ArcelorMittal Global Res EC USA, E Chicago, IN
46312 USA.
[Frazee, Michael] Global Met Mkt S&B Ind Minerals SA, Niagara Falls, NY 14302
USA.
[Park, Jeong Hyouk] Stollberg & Samil CO LTD, Pohang 790240, South Korea.
C3 Pohang University of Science & Technology (POSTECH); POSCO;
ArcelorMittal
RP Cho, JW (corresponding author), Pohang Univ Sci & Technol, GIFT, Pohang 790784,
South Korea.
EM jungwook@postech.ac.kr
RI Cho, Jung-Wook/A-8142-2013; Yin, Hong/AAC-5784-2020
OI Cho, Jung-Wook/0000-0003-2364-1938;
CR Blazek K., 2011, ECCC METEC STEEL I V
Blazek K., 2011, AISTECH 2011 AIST WA
Cho J, 1998, ISIJ INT, V38, P440, DOI 10.2355/isijinternational.38.440
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Meng YA, 2003, METALL MATER TRANS B, V34, P685, DOI 10.1007/s11663-003-0040-y
Nakada H, 2008, ISIJ INT, V48, P446, DOI 10.2355/isijinternational.48.446
Park HS, 2011, METALL MATER TRANS B, V42, P324, DOI 10.1007/s11663-011-9474-9
Todoroki H, 2005, MAT SCI ENG A-STRUCT, V413, P121, DOI
10.1016/j.msea.2005.08.181
Tsukaguchi Y, 2011, TETSU TO HAGANE, V97, P433, DOI 10.2355/tetsutohagane.97.433
Wang H, 2011, IRONMAK STEELMAK, V38, P369, DOI 10.1179/1743281211Y.0000000011
Wang WL, 2008, METALL MATER TRANS B, V39, P66, DOI 10.1007/s11663-007-9110-x
Yin H., 2006, AISTECH 2006 AIST WA, P753
Zhang ZT, 2008, ISIJ INT, V48, P739, DOI 10.2355/isijinternational.48.739
NR 18
TC 130
Z9 132
U1 0
U2 26
PI TOKYO
PA NIIKURA BLDG 2F, 2 KANDA-TSUKASACHO 2-CHOME, TOKYO, CHIYODA-KU 101-0048,
JAPAN
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2013
VL 53
IS 1
BP 62
EP 70
PG 9
GA 102HC
UT WOS:000315834700009
OA gold, Green Submitted
DA 2023-12-05
ER
PT J
AU Zhang, LF
Gao, JW
Damoah, LNW
Robertson, DG
AF Zhang, Lifeng
Gao, Jianwei
Damoah, Lucas Nana Wiredu
Robertson, David G.
TI REMOVAL OF IRON FROM ALUMINUM: A REVIEW
SO MINERAL PROCESSING AND EXTRACTIVE METALLURGY REVIEW
LA English
DT Review
DE alloys; aluminum; iron removal; modification
ID ELECTROMAGNETIC EXPULSIVE FORCE; EXTRUDED AL-7SI-0.3MG ALLOY; 3-LAYER
ELECTROLYSIS CELL; FE-RICH INTERMETALLICS; CRYSTAL-STRUCTURE; CASTING
ALLOYS; NONMETALLIC INCLUSIONS; MECHANICAL-PROPERTIES; PURITY ALUMINUM;
MOLTEN ALUMINUM
AB In this paper, the Fe-rich phases in and their detrimental effect on aluminum
alloys are summarized. The existence of brittle platelet beta-Fe-rich phases lowers
the mechanical properties of aluminum alloys. The methods to neutralize the
detrimental effect of iron are discussed. The use of high cooling rate, solution
heat treatment, and addition of elements such as Mn, Cr, Be, Co, Mo, Ni, V, W, Cu,
Sr, or the rare earth elements Y, Nd, La, and Ce are reported to modify the
platelet Fe-rich phases in aluminum alloys. The mechanism of the modification is
briefly described. Technologies to remove iron from aluminum are reviewed
extensively. The precipitation and removal of Fe-rich phases (sludge) are
discussed. The dense phases can be removed by methods such as gravitational
separation, electromagnetic (EM) separation, and centrifuge. Other methods include
electrolysis, electro-slag refining, fractional solidification, and fluxing
refining. The expensive three-layer cell electrolysis process is the most
successful technique to remove iron from aluminum so far.
C1 [Zhang, Lifeng] Univ Sci & Technol Beijing, Sch Met & Ecol Engn, Beijing 100083,
Peoples R China.
[Zhang, Lifeng; Gao, Jianwei; Damoah, Lucas Nana Wiredu; Robertson, David G.]
Missouri Univ Sci & Technol, Dept Mat Sci & Engn, Rolla, MO USA.
[Gao, Jianwei] Shanghai Inst Qual Inspect & Tech Res, Shanghai, Peoples R China.
C3 University of Science & Technology Beijing; University of Missouri
System; Missouri University of Science & Technology
RP Zhang, LF (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol
Engn, Beijing 100083, Peoples R China.
EM zhanglifeng@ustb.edu.cn
RI Damoah, Lucas/P-2863-2018
OI Damoah, Lucas/0000-0002-1745-3722
FU Research Board Grant; Laboratory of Green Process Metallurgy and
Modeling (GPMM); Material Research Center (MRC); Intelligent Systems
Center (ISC) at Missouri University of Science and Technology (Missouri
ST)
FX This research is supported by the Research Board Grant, Laboratory of
Green Process Metallurgy and Modeling (GPMM), Material Research Center
(MRC), Intelligent Systems Center (ISC) at Missouri University of
Science and Technology (Missouri S&T).
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NR 185
TC 130
Z9 146
U1 21
U2 160
PU TAYLOR & FRANCIS INC
PI PHILADELPHIA
PA 530 WALNUT STREET, STE 850, PHILADELPHIA, PA 19106 USA
SN 0882-7508
EI 1547-7401
J9 MIN PROC EXT MET REV
JI Miner. Process Extr. Metall. Rev.
PY 2012
VL 33
IS 2
BP 99
EP 157
DI 10.1080/08827508.2010.542211
PG 59
WC Metallurgy & Metallurgical Engineering; Mining & Mineral Processing
SC Metallurgy & Metallurgical Engineering; Mining & Mineral Processing
GA 919EC
UT WOS:000302303600002
DA 2023-12-05
ER
PT J
AU Kikuchi, R
AF Kikuchi, R
TI Recycling of municipal solid waste for cement production: pilot-scale
test for transforming incineration ash of solid waste into cement
clinker
LA English
DT Article
DE recycling; municipal waste; incineration ash; sewage sludge; cement
AB Incineration ash of municipal solid waste accounts for a great portion of the
matter in landfills, and minimization of resource consumption and recycling of
waste are important factors for ensuring the future welfare of humankind. The study
presented in this paper reports a technology for producing cement from incineration
ash of municipal solid waste, incineration ash of sewage sludge and other wastes
such as aluminium dress acid copper slag. As incineration ash of municipal solid
waste contains chlorine, special attention should be paid to fixing the chlorine
within the cement. It was verified that proper treatment (formation of calcium-
chloroaluminate) is capable of fixing the chlorine. In order to confirm the
efficacy of this technology before it is used on an industrial scale, a pilot-scale
test (50 tons/day) was conducted. The quality of the resulting cement is sufficient
to enable the cement to be put to practical use. Furthermore, the tested process
does not cause secondary pollution. Consequently, 50% of raw materials for cement
production can be obtained from incineration ash of municipal solid waste. (C) 2001
Elsevier Science B.V. All rights reserved.
C1 Polytech Inst Coimbra, Escola Super Agr Coimbra, Dept Basic Sci & Environm, P-
3040316 Coimbra, Portugal.
RP Kikuchi, R (corresponding author), Polytech Inst Coimbra, Escola Super Agr
Coimbra, Dept Basic Sci & Environm, P-3040316 Coimbra, Portugal.
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*EUR ENV AG, 1999, WAST GEN MAN ENV EU, P212
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*MACH IND ASS JAP, 1999, 1998 REP ENV TRENDS, P9
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NR 10
TC 130
Z9 133
U1 0
U2 39
PI AMSTERDAM
SN 0921-3449
PD FEB
PY 2001
VL 31
IS 2
BP 137
EP 147
DI 10.1016/S0921-3449(00)00077-X
PG 11
GA 389PM
UT WOS:000166247000002
DA 2023-12-05
ER
PT J
AU Xie, RK
Seip, HM
Leinum, JR
Winje, T
Xiao, JS
AF Xie, RK
Seip, HM
Leinum, JR
Winje, T
Xiao, JS
TI Chemical characterization of individual particles (PM10) from
ambient air in Guiyang City, China
SO SCIENCE OF THE TOTAL ENVIRONMENT
LA English
DT Article
DE air pollution; individual particle analysis; hierarchical cluster
analysis; PM10; SEM-EDS
ID AEROSOL-PARTICLES; NORTH-SEA; MULTIVARIATE TECHNIQUES; CLUSTER-ANALYSIS;
CLASSIFICATION; POLLUTION; HEALTH; COMBUSTION; PHOENIX; PM2.5
AB PM10 samples were collected during 5 days in Guiyang, China in July 2003. A
total of about 2300 particles was analyzed by an automated Scanning Electron
Microscope with Energy-Dispersive Spectrometer (SEM-EDS). Hierarchical cluster
analysis (HCA) was used to identify different particle types that occurred in the
aerosol. Seventeen particle types wire identified and presented in the order of
decreasing number abundance as: silicomanganese slag, soil and fly ash, coal
burning, silicomanganese, quartz, syngenite, S-bearing iron, calcium rich, gypsum,
sphalerite, dolomite, iron, alloy, lead sulfate, zinc rich, sulfur-rich particles
and aluminum manufacturing dust. The majority of the particles in the studied size
range are of anthropogenic origin, especially from metallurgical industry. The
study illustrates the complexity of particle pollution in air of an industrial
Chinese city and the results should be useful in planning mitigation measures. (c)
2004 Elsevier B.V. All rights reserved.
C1 Univ Oslo, Dept Chem, Oslo, Norway.
Norwegian Univ Sci & Technol, Dept Mat Technol, N-7491 Trondheim, Norway.
Univ Oslo, Dept Geosci, Oslo, Norway.
Guizhou Inst Environm Sci, Guiyang 550002, Peoples R China.
C3 University of Oslo; Norwegian University of Science & Technology (NTNU);
University of Oslo
RP Xie, RK (corresponding author), Univ Oslo, Dept Chem, POB 1033, Oslo, Norway.
EM xieruik@yahoo.com
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NR 39
TC 129
Z9 144
U1 2
U2 53
PI AMSTERDAM
SN 0048-9697
EI 1879-1026
J9 SCI TOTAL ENVIRON
JI Sci. Total Environ.
PD MAY 1
PY 2005
VL 343
IS 1-3
BP 261
EP 272
DI 10.1016/j.scitotenv.2004.10.012
PG 12
GA 929JM
UT WOS:000229342400018
PM 15862850
DA 2023-12-05
ER
PT J
AU Agrawal, A
Sahu, KK
Pandey, BD
AF Agrawal, A
Sahu, KK
Pandey, BD
TI Solid waste management in non-ferrous industries in India
LA English
DT Article
DE pollution measures; non-ferrous metal; aluminium; copper; zinc; lead
AB This paper highlights the production capacity, type and quantity of solid wastes
generated, their chemical composition and treatment/disposal options for the Indian
aluminium, copper lead and zinc industries. Red mud, spent pot lining (SPL), fly
ash from aluminium industries; scrap, slag, dross, reverts, slime, flue dust, mill
scales, sludge etc. from copper industries; zinc tailing, slag, leach residue,
jarosite residue, beta-cake, etc. from zinc industries and BF slag, flue dust, ISF
slag etc. from lead industries are the major solid waste generated from the
process. Common practices of waste management in these industries are through
recycling and recovering the metal values and dumping. Owing to the presence of the
toxic elements in some of the solid wastes cause environmental degradation.
Stringent pollution control rules are being enacted and implemented as a result of
which all the metal producing industries in organised sector are now taking care of
the environment and waste management related problems, but pollution from
unorganized lead units are the major cause of concern. Permissible limits of toxic
constituents in zinc based secondaries and threshold zinc concentration for both
indigenous and imported raw material were worked out at National Metallurgical
Laboratory (NML) and based on these results a recommendation to MOEF, Government of
India was made to specify the permissible limits for the import of zinc
secondaries. An overview of the attempts made to recycle/recover metal values and
production of value added products, at NML are also mentioned in the text. (C) 2003
Published by Elsevier B.V.
C1 CSIR, Natl Met Lab, Nonferrous Proc Div, Jamshedpur 831007, Bihar, India.
National Metallurgical Laboratory (NML)
RP Agrawal, A (corresponding author), CSIR, Natl Met Lab, Nonferrous Proc Div,
Jamshedpur 831007, Bihar, India.
EM archana_nmI03@yahoo.comn
OI Pandey, Banshi Dhar/0000-0002-8453-9665
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1996, CSIR NEWS, V46
NR 40
TC 127
Z9 148
U1 2
U2 50
PI AMSTERDAM
SN 0921-3449
EI 1879-0658
PD SEP
PY 2004
VL 42
IS 2
BP 99
EP 120
DI 10.1016/j.resconrec.2003.10.004
PG 22
GA 840EC
UT WOS:000222838900001
DA 2023-12-05
ER
PT J
AU Deng, ZY
Zhu, MY
AF Deng, Zhiyin
Zhu, Miaoyong
TI Evolution Mechanism of Non-metallic Inclusions in Al-Killed Alloyed
Steel during Secondary Refining Process
LA English
DT Article
DE non-metallic inclusions; spinel; calcium aluminate; thermodynamic
calculation; evolution mechanism; secondary refining
ID DEOXIDATION EQUILIBRIUM; FREE-ENERGIES; THERMODYNAMICS; CALCIUM;
ALUMINUM
AB The evolution mechanism of inclusions in Al-killed alloyed steel during
secondary refining process was studied by industrial experiments and thermodynamic
calculations. It is found that during the tapping process, Al-O deoxidization
reaction is very close to equilibrium with the formation of many Al2O3 clusters.
With the slag/steel reaction, inclusions vary with the route as Al2O3 inclusions ->
MgO-Al2O3 system inclusions -> CaO-MgO-Al2O3 system inclusions, and finally change
into globular inclusions surrounded by CaO-Al2O3 outer layer, of which the melting
point is lower than liquid steel temperature. Since MgO is less stable than CaO and
it is easier to be reduced by Al, dissolved Mg is generated earlier and faster than
Ca before LF refining, thus the MgO-Al2O3 system inclusions form at first. The
mapping photos of inclusions show that the evolution mechanism of MgO-Al2O3 system
inclusions into CaO-MgO-Al2O3 system inclusions is Ca element substitution for Mg
element in MgO-Al2O3 inclusions. The line scanning shows that there is also the
reaction of Ca element substitution for Al element in the outer CaO-Al2O3 layer
without MgO.
C1 [Deng, Zhiyin; Zhu, Miaoyong] Northeastern Univ, Sch Met & Mat, Shenyang 110819,
Peoples R China.
C3 Northeastern University - China
RP Zhu, MY (corresponding author), Northeastern Univ, Sch Met & Mat, Shenyang
EM myzhu@mail.neu.edu.cn
RI Deng, Zhiyin/K-8739-2017
OI Deng, Zhiyin/0000-0002-0338-5896
FU National Natural Science Foundation of China [51134009]; Specialized
Research Fund for the Doctoral Program of Higher Education of China
[20110042110010]
FX The authors gratefully express their appreciation to National Natural
Science Foundation of China (Grant No. 51134009) and the Specialized
(Grant No. 20110042110010) for supporting this work. The authors also
wish to thank Mr. Baojun ZHONG and Mr. Yonggang DAI in Xingtai Steel of
China for their great help in this work.
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U1 3
U2 66
PI TOKYO
PA TEKKO KAIKAN-5F, 3-2-10, NIHONBASHI-KAYABACHO, TOKYO, CHUO-KU 103-0025,
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2013
VL 53
IS 3
BP 450
EP 458
PG 9
GA 114XO
UT WOS:000316776500010
OA Green Submitted, gold
DA 2023-12-05
ER
PT J
AU Balakrishnan, M
Batra, VS
Hargreaves, JSJ
Pulford, ID
AF Balakrishnan, M.
Batra, V. S.
Hargreaves, J. S. J.
Pulford, I. D.
TI Waste materials - catalytic opportunities: an overview of the
application of large scale waste materials as resources for catalytic
applications
SO GREEN CHEMISTRY
LA English
DT Review
ID SOLID BASE CATALYST; RED MUD; FLY-ASH; RICE HUSK; HETEROGENEOUS
CATALYST; CARBON NANOTUBES; LIGNITE TURKEY; SCYLLA-SERRATA; SHELL
CATALYST; COAL
AB In this overview, we present examples of the use of high volume waste materials
in catalysis or for catalyst synthesis. Waste materials derived from both
industrial and biological sources have attracted interest and this is briefly
summarized. The materials described include red mud, aluminium dross, fly ash,
blast furnace slag, rice husk and various kinds of shell.
C1 [Balakrishnan, M.; Batra, V. S.] TERI Univ, Ctr Energy & Environm, New Delhi
110003, India.
[Hargreaves, J. S. J.; Pulford, I. D.] Univ Glasgow, Sch Chem, WestCHEM, Glasgow
G12 8QQ, Lanark, Scotland.
C3 TERI University; University of Glasgow
RP Balakrishnan, M (corresponding author), TERI Univ, Ctr Energy & Environm,
Darbari Seth Block,Habitat Pl,Lodhi Rd, New Delhi 110003, India.
EM justinh@chem.gla.ac.uk
OI Balakrishnan, Malini/0000-0002-9892-7079
FU British Council [SA07/19]
FX The authors would like to express their appreciation to the British
Council for the generous award of a UKIERI project grant in the area of
the utilization of red mud (project SA07/19). The authors would also
like to thank Miss Caiomhe Moore and Mr Azlan Kamari for useful
discussions.
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TC 126
Z9 134
U1 11
U2 173
PU ROYAL SOC CHEMISTRY
PI CAMBRIDGE
PA THOMAS GRAHAM HOUSE, SCIENCE PARK, MILTON RD, CAMBRIDGE CB4 0WF, CAMBS,
ENGLAND
SN 1463-9262
EI 1463-9270
J9 GREEN CHEM
JI Green Chem.
PD JAN
PY 2011
VL 13
IS 1
BP 16
EP 24
DI 10.1039/c0gc00685h
PG 9
WC Chemistry, Multidisciplinary; Green & Sustainable Science & Technology
SC Chemistry; Science & Technology - Other Topics
GA 704ME
UT WOS:000286056300002
DA 2023-12-05
ER
PT J
AU Holappa, L
Hämäläinen, M
Liukkonen, M
Lind, M
AF Holappa, L
Hämäläinen, M
Liukkonen, M
Lind, M
TI Thermodynamic examination of inclusion modification and precipitation
from calcium treatment to solidified steel
SO IRONMAKING & STEELMAKING
LA English
CT 6th International Conference on Clean Steel
CY JUN 10-12, 2002
CL BALATONFURED, HUNGARY
AB Calcium treatment is a well established method to transform oxide and sulphide
inclusions in steel to less harmful inclusions which can have beneficial effects on
properties. Transformation of solid alumina clusters to liquid calcium aluminates
by calcium is a much used technique to avoid nozzle blocking in continuous casting
of aluminium deoxidised steels. Calcium treatment is also a key method to improve
machinability, which can be further improved by increased sulphur content.
Resulphurised steels, however, tend to have casting problems due to deficient
modification of oxides or formation of solid CaS inclusions which also have a
tendency to clog the nozzle. In this study, the formation and transformation of
liquid and solid inclusions containing oxidic and sulphiclic components were
examined by thermodynamic calculations. A quasichemical slag model was applied to
calculate equilibrium oxide and sulphide inclusions in steel. Calculations were
carried out over a wide temperature range to study the formation of species in the
melt corresponding to ladle treatment conditions as well as casting. To examine
inclusion behaviour during casting and solidification, the interdendritic
solidification model, IDS, was coupled with thermodynamic equilibrium calculations.
The results show the conditions in which liquid inclusions can be formed with
calcium treatment. The calculations were performed at different temperatures and
varying calcium, aluminium and sulphur contents. The effect of total oxygen content
was also studied. The main components in liquid calcium aluminates were CaO and
Al2O3 plus some SiO2 and CaS. The stability relations of different compounds alter
as a function of temperature. An abrupt change occurs during solidification when
the partition of the inclusion forming elements between the liquid and solid iron
phases are taken into account.
C1 Aalto Univ, FIN-02015 Espoo, Finland.
C3 Aalto University
RP Holappa, L (corresponding author), Aalto Univ, POB 6200, FIN-02015 Espoo,
Finland.
EM lauri.holappa@hut.fi
RI Lind, Minna/F-3370-2012
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NR 23
TC 125
Z9 142
U1 0
U2 45
PU TAYLOR & FRANCIS LTD
PI ABINGDON
PA 2-4 PARK SQUARE, MILTON PARK, ABINGDON OR14 4RN, OXON, ENGLAND
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
JI Ironmak. Steelmak.
PD APR
PY 2003
VL 30
IS 2
BP 111
EP 115
DI 10.1179/030192303225001748
PG 5
GA 680HT
UT WOS:000182970800005
DA 2023-12-05
ER
PT J
AU Kim, H
Sohn, I
AF Kim, Hyuk
Sohn, Il
TI Effect of CaF2 and Li2O Additives on the Viscosity
of CaO-SiO2 Na2O Slags
LA English
DT Article
DE mold flux; CaF2; Li2O; viscosity; XPS; slag structure
ID CAO-CAF2-SIO2; GLASSES; MELTS; MGO
AB High aluminum containing steels react vigorously with silica-based mold fluxes
to form alumina. The change in alumina content increases the viscosity and thus
silica-based mold fluxes are compensated with significant amounts of Na2O, CaF2,
and Li2O to ensure both lubrication and heat transfer control. Detailed viscosity
studies using the rotating spindle method showed that additions of CaF2 up to 8 wt%
in the CaO-SiO2-12wt%Na2O system at a constant CaO/SiO2 ratio of 0.8 decreases the
viscosity by breaking the network structure of molten fluxes, but is negligible
above 8 wt%. A similar modification of the network was observed for Li2O up to 2 wt
%. The viscosity data was correlated with the XPS analysis and verified CaF2 and
Li2O as effective in modifying complex silicate structures into simpler silicate
structures depending on the availability of complex silicates and thus was limited
to below certain concentrations.
C1 [Kim, Hyuk; Sohn, Il] Yonsei Univ, Dept Mat Sci & Engn, Seoul 120749, South
Korea.
C3 Yonsei University
RP Kim, H (corresponding author), Yonsei Univ, Dept Mat Sci & Engn, Seoul 120749,
South Korea.
EM ilsohn@yonsei.ac.kr
RI SOHN, IL/I-5815-2012
FU Division of the Humantronics Information Materials; Yonsei University;
National Research Foundation of Korea [2010-0007442] Funding Source:
Korea Institute of Science & Technology Information (KISTI), National
Science & Technology Information Service (NTIS)
FX This study was partially supported by the Brain Korea 21 (BK21) Project
the Division of the Humantronics Information Materials and the Yonsei
University Research Fund of 2009. The authors are also grateful for the
helpful comments from the reviewers.
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TC 123
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U2 35
PI TOKYO
JAPAN
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2011
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BP 1
EP 8
PG 8
GA 712RL
UT WOS:000286683800001
OA gold
DA 2023-12-05
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PT J
AU Bullerjahn, F
Schmitt, D
Ben Haha, M
AF Bullerjahn, Frank
Schmitt, Dirk
Ben Haha, Mohsen
TI Effect of raw mix design and of clinkering process on the formation and
mineralogical composition of (ternesite) belite calcium sulphoaluminate
ferrite clinker
LA English
DT Article
DE Ye'elimite (3CaO*3((Al2O3)(x); (Fe2O3)(1-x)) * CaSO4) polymorphs;
Ternesite (2Ca(2)SiO(4)* CaSO4); X-ray diffraction (B); Mixture
proportioning (A); Cement manufacture (E)
ID ALUMINATE SODALITE CA8<AL12O24>(WO4)2; BLAST-FURNACE SLAG; POWDER
DIFFRACTION; CRYSTAL-STRUCTURE; CHEMICAL GYPSUM; CEMENT; CHEMISTRY;
HYDRATION; BEHAVIOR; SULFATE
AB The effect of the clinkering process on mineral formation in calcium
sulphoaluminate clinker and its reactivity has been investigated using a multi-
method approach. Industrial by-products were used as main raw materials for clinker
production. Under the given conditions, clinker burning processes lead to variable
clinker reactivity and sometimes to an uncontrollable early hydration. The rapid
early age hydration seems to result from a simultaneous incorporation of iron in
ye'elimite, which stabilises its cubic polymorph at the expense of the orthorhombic
one. Ye'elimite has demonstrated as well a high capacity to substitute aluminium
with iron. This study proves the possibility to adjust the performance of calcium
sulphoaluminate ferrite based systems by applying specific clinkering and cooling
processes, and by optimizing the raw mix design accordingly. Additionally,
ternesite is formed. Ternesite, which is usually assumed to be inert, has shown
reactivity potential when it is a part of belite calcium sulphoaluminate ferrite
clinker. (C) 2014 Elsevier Ltd. All rights reserved.
C1 [Bullerjahn, Frank; Schmitt, Dirk; Ben Haha, Mohsen] HeidelbergCement AG,
HeidelbergCement Technol Ctr GmbH, D-69181 Leimen, Germany.
RP Bullerjahn, F (corresponding author), HeidelbergCement AG, HeidelbergCement
Technol Ctr GmbH, Rohrbacher Str 95, D-69181 Leimen, Germany.
EM Frank.bullerjahn@htc-gmbh.com; Mohsen.ben.haha@htc-gmbh.com
RI Ben Haha, Mohsen/AAC-4859-2020
OI Ben Haha, Mohsen/0000-0001-7570-326X; Bullerjahn,
Frank/0000-0002-7791-3807
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NR 59
TC 117
Z9 122
U1 6
U2 123
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD MAY
PY 2014
VL 59
BP 87
EP 95
DI 10.1016/j.cemconres.2014.02.004
PG 9
GA AH7XY
UT WOS:000336349900009
DA 2023-12-05
ER
PT J
AU Wongkeo, W
Thongsanitgarn, P
Pimraksa, K
Chaipanich, A
AF Wongkeo, Watcharapong
Thongsanitgarn, Pailyn
Pimraksa, Kedsarin
Chaipanich, Arnon
TI Compressive strength, flexural strength and thermal conductivity of
autoclaved concrete block made using bottom ash as cement replacement
materials
SO MATERIALS & DESIGN
LA English
DT Article
DE Concrete; Mechanical; Thermal
ID BLAST-FURNACE SLAG; LIGHTWEIGHT CONCRETE; MINERAL ADMIXTURES; AERATED
CONCRETE; FINE AGGREGATE; FLY-ASH; BEHAVIOR
AB The bottom ash (BA) from Mae Moh power plant, Lampang, Thailand was used as
Portland cement replacement to produce lightweight concrete (LWC) by autoclave
aerated concrete method. Portland cement type 1, river sand, bottom ash, aluminium
powder and calcium hydroxide (Ca(OH)(2)) were used in this study. BA was used to
replace Portland cement at 0%, 10%, 20% and 30% by weight and aluminium powder was
added at 0.2% by weight in order to produce the aerated concrete. Compressive
strength, flexural and thermal conductivity tests were then carried out after the
concrete were autoclaved for 6 h and left in air for 7 days. The results show that
the compressive strength, flexural strength and thermal conductivity increased with
increased BA content due to tobermorite formation. However, approximately, 20%
increase in both compressive (up to 11.61 MPa) and flexural strengths (up to 3.16
MPa) was found for mixes with 30% BA content in comparison to just around 6%
increase in the thermal conductivity. Thermogravimetry analysis shows C-S-H
formation and X-ray diffraction confirm tobermorite formation in bottom ash
lightweight concrete. The use of BA as a cement replacement, therefore, can be seen
to have the benefit in enhancing strength of the aerated concrete while achieving
comparatively low thermal conductivity when compared to the results of the control
Portland cement concrete. (C) 2011 Elsevier Ltd. All rights reserved.
C1 [Wongkeo, Watcharapong; Thongsanitgarn, Pailyn; Chaipanich, Arnon] Chiang Mai
Univ, Fac Sci, Adv Cement Based Mat Res Unit, Dept Phys & Mat Sci, Chiang Mai
50200, Thailand.
[Pimraksa, Kedsarin] Chiang Mai Univ, Fac Sci, Dept Ind Chem, Chiang Mai 50200,
Thailand.
[Chaipanich, Arnon] Chiang Mai Univ, Ctr Excellence Mat Sci & Technol, Chiang
Mai 50200, Thailand.
C3 Chiang Mai University; Chiang Mai University; Chiang Mai University
RP Chaipanich, A (corresponding author), Chiang Mai Univ, Fac Sci, Adv Cement Based
Mat Res Unit, Dept Phys & Mat Sci, Chiang Mai 50200, Thailand.
EM arnon@chiangmai.ac.th
RI Thongsanitgarn, Pailyn/GPK-5952-2022; Pimraksa, Kedsarin/AFL-0675-2022
OI Chaipanich, Arnon/0000-0001-8097-6609
FU National Research University, Commission of Higher Education (Thailand)
FX The authors are grateful for financial support funded by the National
Research University Project, Commission of Higher Education (Thailand).
The Graduate School, Chiang Mai University is also acknowledged.
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[Anonymous], 2003, CONCRETE
[Anonymous], C34897 ASTM
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NR 25
TC 117
Z9 121
U1 1
U2 70
PU ELSEVIER SCI LTD
PI OXFORD
SN 0261-3069
J9 MATER DESIGN
JI Mater. Des.
PD MAR
PY 2012
VL 35
BP 434
EP 439
DI 10.1016/j.matdes.2011.08.046
PG 6
GA 909QG
UT WOS:000301578700057
DA 2023-12-05
ER
PT J
AU Ma, M
Wang, DH
Wang, WG
Hu, XH
Jin, XB
Chen, GZ
AF Ma, Meng
Wang, Dihua
Wang, Wenguang
Hu, Xiaohong
Jin, Xianbo
Chen, George Z.
TI Extraction of titanium from different titania precursors by the FFC
Cambridge process
SO JOURNAL OF ALLOYS AND COMPOUNDS
LA English
DT Article
DE electrochemical reactions; solid state reactions; electrode materials;
metals and alloys; oxide materials
ID ELECTROCHEMICAL REDUCTION; MOLTEN-SALTS; DIOXIDE; OXYGEN
AB Cheap titania precursors including titania dust, metatitanic acid (solid) and
titanium-rich slag were tested as the feeding materials in the FFC Cambridge
process (laboratory scale). Porous pellets (similar to 20 mm in diameter, 2.0-3.0
mm in thickness) of the precursor were successfully reduced to titanium metal or
alloy by constant voltage electrolysis (2.9-3.1 V) in molten calcium chloride
(similar to 900 degrees C). The reduction was independent of the initial crystal
structure of the precursor. More importantly, some metallic impurities in the
titanium-rich slag, such as aluminium and manganese, were found to be partly or
completely removed after electrolysis. The current efficiency decreased with
electrolysis time, typically from 40% in the first 5 It to 20% in 12 h for the 2 mm
thick TiO2 pellets. The energy consumption of electrolysis was about 33 kWh/kg Ti
when the oxygen level in the produced metal was reduced to below 3000 ppm. Analyses
of the electrolysis data and of the phases and compositions in partially reduced
oxide pellets suggested strong dependence of the electro-reduction on mass (ion)
transfer in the pellet after metallisation of the pellet's surface. An earlier
proposed "double-melt electrolysis" was compared with the electrolysis data,
focusing on the origin and influence of background current. (c) 2005 Elsevier B.V.
All rights reserved.
C1 Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072, Peoples R China.
Univ Nottingham, Sch Chem Environm & Min Engn, Nottingham NG7 2RD, England.
C3 Wuhan University; University of Nottingham
RP Wang, DH (corresponding author), Wuhan Univ, Coll Chem & Mol Sci, Wuhan 430072,
Peoples R China.
EM wangdh@whu.edu.cn; george.chen@nottingham.ac.uk
RI Wang, Dihua/G-5728-2011; Jin, Xianbo/A-9109-2012; Chen, George
Zheng/A-4577-2009
OI Wang, Dihua/0000-0003-2364-8718; Jin, Xianbo/0000-0002-3095-8979; Chen,
George Zheng/0000-0002-5589-5767
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NR 26
TC 115
Z9 132
U1 1
U2 96
PU ELSEVIER SCIENCE SA
PI LAUSANNE
PA PO BOX 564, 1001 LAUSANNE, SWITZERLAND
SN 0925-8388
EI 1873-4669
J9 J ALLOY COMPD
JI J. Alloy. Compd.
PD AUG 31
PY 2006
VL 420
IS 1-2
BP 37
EP 45
DI 10.1016/j.jallcom.2005.10.048
PG 9
WC Chemistry, Physical; Materials Science, Multidisciplinary; Metallurgy &
Metallurgical Engineering
SC Chemistry; Materials Science; Metallurgy & Metallurgical Engineering
GA 067JY
UT WOS:000239299300009
DA 2023-12-05
ER
PT J
AU Whittaker, M
Zajac, M
Ben Haha, M
Bullerjahn, F
Black, L
AF Whittaker, Mark
Zajac, Maciej
Ben Haha, Mohsen
Bullerjahn, Frank
Black, Leon
TI The role of the alumina content of slag, plus the presence of additional
sulfate on the hydration and microstructure of Portland cement-slag
blends
LA English
DT Article
DE Granulated blast-furnace slag; Sulfate; Hydration; Microstructure;
Characterisation
ID BLAST-FURNACE SLAG; C-S-H; STRENGTH DEVELOPMENT; LIMESTONE; PASTES;
GYPSUM; QUANTIFICATION; TEMPERATURE; ACTIVATION; MECHANISMS
AB The effects on composite cements of the aluminium content of slag, plus that of
additional sulfate, have been investigated. Samples containing cement or composites
with 40% replacement by one of 2 different slags, differing in aluminium contents,
were prepared. A further blended sample was prepared with additional anhydrite
replacing 3% w/w of binder. Slag blended mortars showed comparable strengths to the
neat cement system at later ages. Adding slag changed the hydration kinetics of the
clinker phases. The addition of sulfate had no effect on slag reactivity but
increased that of alite. Slags richer in aluminium resulted in greater
incorporation of aluminium into C-S-H and encouraged the presence of
hemicarboaluminate over monocarboaluminate. The Ca/Si ratios of the C-S-H formed
were comparable between the two blends, being marginally lower than that of the
neat system. The addition of anhydrite resulted in the adsorption of sulfate onto
the C-S-H, plus stabilisation of ettringite. (C) 2014 Elsevier Ltd. All rights
reserved.
C1 [Whittaker, Mark; Black, Leon] Univ Leeds, Inst Resilient Infrastruct, Sch Civil
Engn, Leeds LS2 9JT, W Yorkshire, England.
[Zajac, Maciej; Ben Haha, Mohsen; Bullerjahn, Frank] Heidelberg Technol Ctr
GmbH, D-69181 Leimen, Germany.
C3 University of Leeds
RP Black, L (corresponding author), Univ Leeds, Inst Resilient Infrastruct, Sch
Civil Engn, Woodhouse Lane, Leeds LS2 9JT, W Yorkshire, England.
EM l.black@leeds.ac.uk
RI Zajac, Maciej/AAP-8225-2020; Ben Haha, Mohsen/AAC-4859-2020; Black,
Leon/B-5840-2008
OI Ben Haha, Mohsen/0000-0001-7570-326X; Black, Leon/0000-0001-8531-4989;
Bullerjahn, Frank/0000-0002-7791-3807
FU University Research Scholarship from the University of Leeds for MJW;
HeidelbergCement Technology Centre GmbH
FX This work was funded by a University Research Scholarship from the
University of Leeds for MJW, with additional funding and materials
provided by HeidelbergCement Technology Centre GmbH.
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NR 61
TC 113
Z9 123
U1 1
U2 74
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD DEC
PY 2014
VL 66
BP 91
EP 101
DI 10.1016/j.cemconres.2014.07.018
PG 11
GA AQ0MQ
UT WOS:000342477800008
OA Green Accepted
DA 2023-12-05
ER
PT J
AU BABU, SS
DAVID, SA
VITEK, JM
MUNDRA, K
DEBROY, T
AF BABU, SS
DAVID, SA
VITEK, JM
MUNDRA, K
DEBROY, T
TI DEVELOPMENT OF MACROSTRUCTURE AND MICROSTRUCTURE OF CARBON-MANGANESE
LOW-ALLOY STEEL WELDS - INCLUSION FORMATION
SO MATERIALS SCIENCE AND TECHNOLOGY
LA English
DT Article
ID SLAG-METAL REACTIONS; HSLA STEEL; MULTIPASS DEPOSITS; ACICULAR FERRITE;
SURFACE-TENSION; DEOXIDATION; TOUGHNESS; CHEMISTRY; STRENGTH; ALUMINUM
AB Ladle steel deoxidation reactions are reviewed and the principles are extended
to inclusion formation in steel weld metal. The dissolution of oxygen, the
stability of various oxides, and the nucleation and growth of inclusions are
discussed. Theoretical time-temperature transformation (TTT) diagrams are
calculated for various oxide inclusions based on an overall kinetics approach using
nucleation and growth rare expressions. These concepts are then extended to
understand the development of weld metal inclusion characteristics. A strong
correlation between the published inclusion composition and the stability of the
oxides was found. An analysis of the TTT diagrams indicates that, during weld
cooling, sequential oxidation of dissolved deoxidising elements takes place, which
agrees with the reported layered morphology of inclusions. The analysis indicates
that the inclusion characteristics are quite sensitive to the oxygen content, the
deoxidising element concent rations, the presence of performed inclusions, and the
reaction temperature. Inclusion coarsening and elimination of inclusions from welds
are discussed in relation to the final inclusion characteristics.
C1 PENN STATE UNIV, DEPT MAT SCI & ENGN, UNIVERSITY PK, PA 16802 USA.
C3 Pennsylvania Commonwealth System of Higher Education (PCSHE);
Pennsylvania State University; Pennsylvania State University -
University Park
RP BABU, SS (corresponding author), OAK RIDGE NATL LAB, DIV MET & CERAM, OAK RIDGE,
TN USA.
RI DebRoy, Tarasankar/A-2106-2010; Babu, Sudarsanam S/D-1694-2010
OI Babu, Sudarsanam S/0000-0002-3531-2579; DebRoy,
Tarasankar/0000-0003-1790-7066
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NR 69
TC 113
Z9 122
U1 1
U2 39
PU MANEY PUBLISHING
PI LEEDS
PA STE 1C, JOSEPHS WELL, HANOVER WALK, LEEDS LS3 1AB, W YORKS, ENGLAND
SN 0267-0836
EI 1743-2847
J9 MATER SCI TECH-LOND
JI Mater. Sci. Technol.
PD FEB
PY 1995
VL 11
IS 2
BP 186
EP 199
DI 10.1179/mst.1995.11.2.186
PG 14
Engineering
GA RE567
UT WOS:A1995RE56700016
DA 2023-12-05
ER
PT J
AU Wang, YS
Alrefaei, Y
Dai, JG
AF Wang, Yan-Shuai
Alrefaei, Yazan
Dai, Jian-Guo
TI Silico-Aluminophosphate and Alkali-Aluminosilicate Geopolymers: A
Comparative Review
SO FRONTIERS IN MATERIALS
LA English
DT Review
DE silico-aluminophosphate; alkali-aluminosilicate; geopolymerization
mechanism; environmental impacts; sustainable development
ID ACID-BASED GEOPOLYMERS; BONDED PHOSPHATE CERAMICS; ORDINARY
PORTLAND-CEMENT; ASH-BASED GEOPOLYMER; BLAST-FURNACE SLAG; S-H GELS;
FLY-ASH; PHOSPHORIC-ACID; CALCIUM-PHOSPHATE; ACTIVATED SLAG
AB Chemically activated materials (often termed as geopolymer) have received
attracting attentions in civil, material and environmental research fields as a
toolkit alternative to traditional Portland cement in specific applications. This
paper presents a comparative review on silico-aluminophosphate (SAP) geopolymers in
terms of definition, chemistries involved during geopolymerization, mechanical
performance, durability, environmental impacts, and their potentials in
applications relative to conventional alkali-aluminosilicate (AAS) geopolymers.
Recommendations for future applications are also highlighted. It is found that S-A-
P gels with six-coordinated aluminum environment dominate in SAP geopolymers, while
the aluminum in N-A-S-H gels formed in the AAS geopolymers is characterized by
four-coordinated features. Besides, the slow performance development of SAP
geopolymer matrix under ambient temperature curing can be compensated through
incorporating additional countermeasures (e.g., metal sources) which allow the
tailored design of such geopolymers for certain in-situ applications. Generally,
the calcium-bearing C-(A)-S-H gels co-existing with N-A-S-H gels are dominant in
AAS geopolymers, while the S-A-P gels enhanced by phosphate-containing
crystalline/amorphous phases are the main products in SAP geopolymers. The SAP
geopolymers show their environmental friendliness relative to the AAS geopolymers
due to the utilization of phosphate activators that require lower production energy
relative to silicate-containing activators. However, the higher cost of phosphate
activators may confine the applications of SAP geopolymers in some exquisite or
special fields.
C1 [Wang, Yan-Shuai; Alrefaei, Yazan; Dai, Jian-Guo] Hong Kong Polytech Univ, Dept
Civil & Environm Engn, Hong Kong, Peoples R China.
C3 Hong Kong Polytechnic University
RP Dai, JG (corresponding author), Hong Kong Polytech Univ, Dept Civil & Environm
Engn, Hong Kong, Peoples R China.
EM cejgdai@polyu.edu.hk
RI alrefaei, yazan/AFR-9469-2022; Dai, Jian-Guo/E-4503-2011
OI alrefaei, yazan/0000-0003-3665-6346; Dai, Jian-Guo/0000-0001-9904-7914
FU Hong Kong-Guangzhou Technology and Innovation Partnership Program
[201807010055]; National Science Foundation of China (NSFC) [51638008,
51478406]; HKSAR Innovation Technology Fund [ITS/009/17]; Hong Kong
Ph.D. Fellowship Scheme (HKPFS)
FX The authors would like to acknowledge the financial support received
from the Hong Kong-Guangzhou Technology and Innovation Partnership
Program (Project No. 201807010055), National Science Foundation of China
(NSFC) (Projects No. 51638008 and 51478406), HKSAR Innovation Technology
Fund (Project code: ITS/009/17) and the Hong Kong Ph.D. Fellowship
Scheme (HKPFS) awarded to the second author. The authors would also like
to thank Prof. John L. Provis for his advice toward the paper during the
study visit of the first author at the University of Sheffield.
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NR 159
TC 111
Z9 116
U1 24
U2 129
PU FRONTIERS MEDIA SA
PI LAUSANNE
PA AVENUE DU TRIBUNAL FEDERAL 34, LAUSANNE, CH-1015, SWITZERLAND
SN 2296-8016
J9 FRONT MATER
JI Front. Mater.
PD MAY 7
PY 2019
VL 6
AR 106
DI 10.3389/fmats.2019.00106
PG 17
GA HX3CO
UT WOS:000467269300001
OA gold
DA 2023-12-05
ER
PT J
AU Qaidi, SMAA
Tayeh, BAF
Isleem, HF
de Azevedo, ARG
Ahmed, HU
Emad, W
AF Qaidi, Shaker M. A.
Tayeh, Bassam A.
Isleem, Haytham F.
de Azevedo, Afonso R. G.
Ahmed, Hemn Unis
Emad, Wael
TI Sustainable utilization of red mud waste (bauxite residue) and slag for
the production of geopolymer composites: A review
SO CASE STUDIES IN CONSTRUCTION MATERIALS
LA English
DT Review
DE Red left-to-right markmud; Slag; Geopolymers, mechanical, durability,
and microstructure properties; Life cycle assessmentleft-to-right mark;
Radioactive; Economic and environmental impacts
ID FLY-ASH; BUILDING-MATERIALS; RADIOLOGICAL CHARACTERIZATION;
ENVIRONMENTAL-IMPACT; AQUEOUS-SOLUTIONS; CERAMIC MATERIALS;
PORTLAND-CEMENT; MIXTURE DESIGN; PAVING BLOCKS; HIGH-STRENGTH
AB The production of cement results in the emission of much carbon dioxide, which
contributes to (sic)undesirable environmental impacts such as climate change and
global warming. These (sic)phenomena (sic)have rekindled interest in utilizing a
variety of industrial waste products to (sic)produce geopolymer (sic)(GP)
composites and alkali-activated (AA) binders in order to reduce the (sic)usage of
ordinary (sic)Portland cement in building construction. Waste red mud (RM), also
known as bauxite residue, is one of these (sic)hazardous radioactive (sic)waste
materials that is formed as a by-product of Bayer's aluminum (sic)manufacturing
process. This (sic)paper conducts a systematic review of the literature on the use
of (sic)RM and slag in the production (sic)of red mud-slag geopolymer (RM-SGP). An
overview of the (sic)economic and environmental (sic)impacts, physical and chemical
properties, production, (sic)distribution, classification, and potential
applications (sic)of RM are presented. (sic)Besides, recent advancements in the
usage of RM and slag for geopolymer (sic)production are (sic)described in terms of
physical, mechanical, durability, and microstructure (sic) properties. Moreover,
this (sic)study attempts to chart a route toward a realistic valorization that
(sic)reflects both real and perceived (sic)concerns, such as radioactivity,
leaching, and the life cycle (sic)assessment of red mud geopolymer (RM-GP). The
potential (sic)use of RM-SGP production indicates the need for further studies into
(sic)the mixture proportion (sic)and combination of these two raw ingredients with
other cementitious materials (sic)leading to new (sic)energy-saving and affordable
building products and processes. Also, it is (sic)recommended that (sic)research
efforts be directed (sic)toward economic, life cycle, and environmental
(sic)assessments.
C1 [Qaidi, Shaker M. A.] Univ Duhok, Coll Engn, Dept Civil Engn, Duhok, Kurdistan
Regio, Iraq.
[Tayeh, Bassam A.] Islamic Univ Gaza, Fac Engn, Civil Engn Dept, POB 108, Gaza,
Gaza Strip, Palestine.
[Isleem, Haytham F.] Qujing Normal Univ, Dept Construction Management, Qujing
655011, Yunnan, Peoples R China.
[de Azevedo, Afonso R. G.] UENF State Univ Northern Rio Janeiro, LECIV Civil
Engn Lab, Ave Alberto Lamego 2000, BR-2000 Campos Dos Goytacazes, RJ, Brazil.
[Ahmed, Hemn Unis] Univ Sulaimani, Coll Engn, Civil Engn Dept, Sulaimaniyah,
Kurdistan Regio, Iraq.
[Emad, Wael] Komar Univ Sci & Technol, Dept Civil Engn, Sulaymaniyah, Kurdistan
Regio, Iraq.
C3 University of Duhok; Islamic University Gaza; University of Sulimanyah
RP Tayeh, BAF (corresponding author), Islamic Univ Gaza, Fac Engn, Civil Engn Dept,
POB 108, Gaza, Gaza Strip, Palestine.
EM btayeh@iugaza.edu.ps
RI Tayeh, Bassam/IYJ-5641-2023; Cuadrado, Glenda/HNJ-6380-2023; Isleem,
Haytham F./I-6476-2017; Qaidi, Shaker/AAM-8334-2020; Azevedo,
Afonso/K-4043-2016
OI Tayeh, Bassam/0009-0003-7522-333X; Isleem, Haytham
F./0000-0002-4826-7420; Qaidi, Shaker/0000-0001-8289-4877; Azevedo,
Afonso/0000-0002-4694-4459
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Zinoveev D, 2021, METALS-BASEL, V11, DOI 10.3390/met11030469
NR 196
TC 110
Z9 110
U1 59
U2 224
PU ELSEVIER
PI AMSTERDAM
SN 2214-5095
J9 CASE STUD CONSTR MAT
JI Case Stud. Constr. Mater.
PD JUN
PY 2022
VL 16
AR e00994
DI 10.1016/j.cscm.2022.e00994
EA MAR 2022
PG 28
GA 0J2AQ
UT WOS:000779908300003
OA gold
DA 2023-12-05
ER
PT J
AU Xiong, SJ
Burvall, J
Örberg, H
Kalen, G
Thyrel, M
Öhman, M
Boström, D
AF Xiong, Shaojun
Burvall, Jan
Orberg, Håkan
Kalen, Gunnar
Thyrel, Mikael
Ohman, Marcus
Bostrom, Dan
TI Slagging characteristics during combustion of corn stovers with and
without kaolin and calcite
SO ENERGY & FUELS
LA English
DT Article
ID REED CANARY GRASS; BIOMASS; BIOENERGY; QUALITY; HARVEST; CHINA; CROP
AB Ash-related problems have more than occasionally been observed in biomass-fired
boilers and also recently in biopellet burners. These problems can lead to reduced
reliability of the combustion systems as well as bad publicity for the market. When
agricultural residues are used as biofuel feedstock, slagging problems will be
worse. The objectives of the present work were, therefore, to examine the effects
of kaolin and calcite addition on the slagging tendency of corn stover fuel when
corn stover pellets are burned in a small-scale appliance and determine the slag
characteristics during combustion. Pellets with an additive/fuel ratio of 3% (dry
mass) were combusted in an underfed burner (50 kW) that is installed in a boiler
with 90 kW output. The choice of 3% additive/fuel ratio was based on analyses of
the ash melting behavior of seven fuel mixtures that combine either 0-3% kaolin or
0-3% calcite and corn stovers. The 3% kaolin and calcite addition increased the ash
melting temperature (IT) by about 100-200 degrees C. When the 3% kaolin or calcite
was added to the corn stover raw material, the severe slagging tendency of the fuel
was considerably reduced. The slag quantities from burning kaolin- and calcite-
added fuels were about half and one-third, respectively, of that from nonadditive
pellets. The slag deposits from the burner were characterized with scanning
electron microscopy (SEM) combined with energy dispersive X-ray analysis (EDS) and
X-ray diffraction (XRD). The XRD was also used to examine the chemical composition
of corresponding bottom ash in the boiler. The results indicated that the reduction
of slagging when using additives can be attributed to a change from relatively low
melting temperature silicates to higher melting temperature silicates. For the corn
stover without additives, the low melting fractions of the slag were assumed to
consist mainly of potassium calcium silicate, indirectly observed as a glass by the
XRD. When kaolin was added, a depletion of potassium was observed because of the
extensive formation of leucite (KAlSi2O6) and the glass became dominated by
calcium, aluminum, and silicon. This process was accompanied by a considerable
reduction of glass amount. In the case of CaCO3 addition, however, calcium
magnesium silicates formed to an extent that the glass (low melting material)
finally became dominated by potassium silicate. This process was also accompanied
by a substantial reduction of the amount of glass.
C1 [Xiong, Shaojun; Burvall, Jan; Orberg, Håkan; Kalen, Gunnar; Thyrel, Mikael]
Swedish Univ Agr Sci, Unit Biomass Technol & Chem, SE-90403 Umea, Sweden.
[Ohman, Marcus] Lulea Univ Technol, Div Energy Engn, SE-97187 Lulea, Sweden.
[Bostrom, Dan] Umea Univ, SE-90187 Umea, Sweden.
C3 Swedish University of Agricultural Sciences; Lulea University of
Technology; Umea University
RP Xiong, SJ (corresponding author), Swedish Univ Agr Sci, Unit Biomass Technol &
Chem, SE-90403 Umea, Sweden.
EM shaojun.xiong@btk.slu.se
OI Thyrel, Mikael/0000-0003-4748-2644; Xiong, Shaojun/0000-0001-5700-9493
FU China Kerchin Cattle Industries Ltd.; Swedish Energy Agency [STEM
30040-1]
FX The financial support from China Kerchin Cattle Industries Ltd. and the
Swedish Energy Agency (STEM 30040-1) are gratefully acknowledged. The
help given by Mr. Li He, Li Yi, Li Feng, and Song Yifei at China Kerchin
Cattle Industries Ltd. is very much appreciated. We are grateful to the
editor and four reviewers who provided valuable comments on the
manuscript and to Ann-Sofi Hahlin who helped LIS with optical pi of slag
morphology.
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NR 21
TC 108
Z9 116
U1 0
U2 73
PI WASHINGTON
SN 0887-0624
J9 ENERG FUEL
JI Energy Fuels
PD SEP-OCT
PY 2008
VL 22
IS 5
BP 3465
EP 3470
DI 10.1021/ef700718j
PG 6
GA 350DK
UT WOS:000259332600077
DA 2023-12-05
ER
PT J
AU Francis, AA
AF Francis, AA
TI Conversion of blast furnace slag into new glass-ceramic material
LA English
DT Article
DE devitrification; glass ceramics; slag; waste material
ID COAL ASH; CRYSTALLIZATION; MIXTURES; WASTE; BULK
AB The devitrification behavior of different sizes of slag-derived glass was
investigated using differential thermal analysis, X-ray diffraction and scanning
electron microscopy to determine the possibility of preparing glass-ceramic
materials. The crystalline phases were identified as gehlenite, diopside pyroxene
and barium aluminium silicate. The degree of crystallization was determined by
evaluation the changes of density at different temperatures where a maximum density
was achieved at 900 degreesC. A remarkable difference in the glass-ceramic texture
was observed by treating the sample at different crystallization temperatures. Both
acicular and dendritic morphology have been identified in the sample heat-treated
at 1050 degreesC. A slight variation in peak crystallization temperature with
particle size indicated a bulk crystallization mechanism. (C) 2003 Elsevier Ltd.
C1 CMRDI, Cairo, Egypt.
C3 Egyptian Knowledge Bank (EKB); Central Metallurgical Research &
Development Institute (CMRDI)
RP Francis, AA (corresponding author), CMRDI, POB 87, Cairo, Egypt.
EM adel_francis@hotmail.com
RI Francis, Adel/I-4575-2019
OI Francis, Adel/0000-0001-8542-2912
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PU ELSEVIER SCI LTD
PI OXFORD
SN 0955-2219
J9 J EUR CERAM SOC
JI J. European Ceram. Soc.
PD AUG
PY 2004
VL 24
IS 9
BP 2819
EP 2824
PG 6
GA 830JD
UT WOS:000222117300031
DA 2023-12-05
ER
PT J
AU Wetzel, A
Middendorf, B
AF Wetzel, A.
Middendorf, B.
TI Influence of silica fume on properties of fresh and hardened ultra-high
performance concrete based on alkali-activated slag
LA English
DT Article
DE UHPC; Rheology; Geopolymer; Ground granulated blast furnace slag;
Water/binder ratio
AB Based on the principles of ultra-high performance concrete (UHPC) a Portland
cement free, alkali-activated material was optimized in order to enhance strength
and durability. The formulation is based on ground granulated blast furnace slag
and as an activator a combination of potassium water-glass and potassium hydroxide
was used. Furthermore, silica fume and metakaolin as inorganic fines were used to
increase the packing density of the mixture. Quartz sand (0-2 mm) and quartz powder
were added as aggregates. The results comprise an enhancement of the rheological
properties by the stepwise increase of silica fume. A w/b ratio of less than 0.25
was realised using a certain mixing procedure with a high intensity mixer. The
compressive strength reaches values comparable with the strength range of an UHPC.
The already low capillary porosity could further be decreased by the substitution
of slag with a small amount of metakaolin, which is leading to a higher
polymerisation degree due to an incorporation of aluminium in the reaction
products. The enhanced polymerisation degree was estimated by FTIR and XRD.
Although no effective superplasticizer can be used in this high alkaline material,
the low w/b ratio and a good workability can be achieved by using certain amounts
of silica fume.
C1 [Wetzel, A.; Middendorf, B.] Univ Kassel, Fac Civil & Environm Engn, Inst Struct
Engn, Dept Struct Mat & Construct Chem, Kassel, Germany.
C3 Universitat Kassel
RP Wetzel, A (corresponding author), Univ Kassel, Fac Civil & Environm Engn, Inst
Struct Engn, Dept Struct Mat & Construct Chem, Kassel, Germany.
EM alexander.wetzel@uni-kassel.de
RI Wetzel, Alexander/M-1386-2015
OI Abdellatief, Mohammed/0000-0002-4182-9996; /0000-0003-2680-9708
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TC 107
Z9 109
U1 10
U2 164
PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
PD JUL
PY 2019
VL 100
BP 53
EP 59
DI 10.1016/j.cemconcomp.2019.03.023
PG 7
GA HZ2WG
UT WOS:000468708900005
DA 2023-12-05
ER
PT J
AU Capuzzi, S
Timelli, G
AF Capuzzi, Stefano
Timelli, Giulio
TI Preparation and Melting of Scrap in Aluminum Recycling: A Review
SO METALS
LA English
DT Review
DE recycling; scrap upgrading; secondary aluminum; furnace selection; slag
treatment
ID X-RAY TRANSMISSION; PROCESS PARAMETERS; SIZE-REDUCTION; BEVERAGE CANS;
COMMINUTION; FURNACE; METALS; ENERGY; IDENTIFICATION; BENEFITS
AB This work provides an overview of the aluminum (Al) recycling process, from the
scrap upgrading to the melting process. Innovations and new trends regarding the Al
recycling technologies are highlighted. Aluminum recycling offers advantages in
terms of environmental and economic benefits. The presence of deleterious
impurities in recycled Al alloys is increasing and this is the main drawback if
compared to primary alloys. The continuous growth of undesired elements can be
mitigated by different technologies, preliminary operations and treatments, and by
the optimization of the melting process. Downgrading and dilution are possible
solutions to reduce the rate of impurities, but they are not sustainable if the
final use of Al alloy continuously increases. The main objectives in the
development of the Al recycling are shown and discussed. In particular, the
evolution of preliminary treatments of the scrap, as sorting, comminution and de-
coating, is reported and a review of the melting technologies is also presented.
However, the choice of performing preliminary operations to the melting stage, thus
improving the operating conditions during the furnace running, is a trade-off
between costs and process efficiency.
C1 [Capuzzi, Stefano; Timelli, Giulio] Univ Padua, Dept Management & Engn, Str S
Nicola 3, I-36100 Vicenza, Italy.
C3 University of Padua
RP Timelli, G (corresponding author), Univ Padua, Dept Management & Engn, Str S
Nicola 3, I-36100 Vicenza, Italy.
EM capuzzi@gest.unipd.it; timelli@gest.unipd.it
RI Timelli, Giulio/K-3892-2015
OI Timelli, Giulio/0000-0002-7549-6499
FU EIT-Raw Materials; Padova University within the Summer and Winter School
programme (4L-Alloys)
FX This work was developed within the European Project 4-L Alloys (Life
Long Learning on Light Alloy: from Raw Materials to Sustainable
Products, funded by EIT-Raw Materials) and with the financial support of
the Padova University within the Summer and Winter School programme
(4L-Alloys). The authors would like to acknowledge the Italian
Association of Aluminum Refiners and Remelters (ASSIRAL).
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NR 86
TC 107
Z9 111
U1 19
U2 88
PU MDPI
PI BASEL
PA ST ALBAN-ANLAGE 66, CH-4052 BASEL, SWITZERLAND
EI 2075-4701
J9 METALS-BASEL
JI Metals
PD APR
PY 2018
VL 8
IS 4
AR 249
DI 10.3390/met8040249
PG 24
Engineering
GA GI9XA
UT WOS:000434882800052
OA Green Published, gold
DA 2023-12-05
ER
PT J
AU Rossen, JE
Scrivener, KL
AF Rossen, J. E.
Scrivener, K. L.
TI Optimization of SEM-EDS to determine the C-A-S-H composition in matured
cement paste samples
SO MATERIALS CHARACTERIZATION
LA English
DT Article
DE Cement; Calcium silicate hydrate (C-S-H); Scanning electron microscopy
(SEM); Transmission electron microscopy (TEM); Energy-dispersive
spectrometry (EDS)
ID X-RAY-MICROANALYSIS; BETA-DICALCIUM SILICATE; TRICALCIUM SILICATE;
PORTLAND-CEMENT; NMR; ALUMINUM; SLAG; TEM
AB Microanalysis of characteristic X-rays in the SEM is a powerful method to assess
the chemical composition of phases in cement pastes, in particular the calcium
silicate hydrate containing aluminium (C-A-S-H). Nevertheless, many variables may
influence the results obtained, due mainly to the intimate mixing of C-A-S-H with
other hydrate phases and the susceptibility of this phase to damage by the electron
beam. In this study the effect of various acquisition parameters was examined,
along with methods to determine an "average" C-A-S-H composition. The results
acquired in the SEM were compared with the analysis of the same samples in the TEM,
where phases can be analyzed without intermixing. A simple method was used to
obtain compositions from SEM based analysis that are very close to those which can
be obtained in the TEM. (C) 2016 Elsevier Inc. All rights reserved.
C1 [Rossen, J. E.; Scrivener, K. L.] Ecole Polytech Fed Lausanne, Lab Construct
Mat, CH-1015 Lausanne, Switzerland.
C3 Swiss Federal Institutes of Technology Domain; Ecole Polytechnique
Federale de Lausanne
RP Rossen, JE (corresponding author), Ecole Polytech Fed Lausanne, Lab Construct
Mat, CH-1015 Lausanne, Switzerland.
EM john.rossen@alumni.epfl.ch
FU Swiss National Science Foundation (SNF) [130419]; Nagra (National
Cooperative for the Disposal of Radioactive Waste) for LCS (long-term
cement study)
FX Thanks are due to the following CIME staff: Marco Cantoni, Amelie
Bazzoni and Daniele Laub for help on TEM sample preparation and
experiments. Thanks are also due to Prof. Jacques Lemaitre from LTP and
Cyrille Dunant from LMC for helpful insights into more critical
treatment of the data. The research leading to these results has
received funding from both the Swiss National Science Foundation (SNF)
under Sinergia grant no130419 and from Nagra (National Cooperative for
the Disposal of Radioactive Waste) for the LCS (long-term cement study).
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X
NR 35
TC 107
Z9 114
U1 12
U2 72
PI NEW YORK
SN 1044-5803
EI 1873-4189
J9 MATER CHARACT
JI Mater. Charact.
PD JAN
PY 2017
VL 123
BP 294
EP 306
DI 10.1016/j.matchar.2016.11.041
PG 13
Engineering; Materials Science, Characterization & Testing
GA EI7LD
UT WOS:000392678400033
OA hybrid
DA 2023-12-05
ER
PT J
AU Shirvanimoghaddam, K
Khayyam, H
Abdizadeh, H
Akbari, MK
Pakseresht, AH
Ghasali, E
Naebe, M
AF Shirvanimoghaddam, K.
Khayyam, H.
Abdizadeh, H.
Akbari, M. Karbalaei
Pakseresht, A. H.
Ghasali, E.
Naebe, M.
TI Boron carbide reinforced aluminium matrix composite: Physical,
mechanical characterization and mathematical modelling
SO MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES
MICROSTRUCTURE AND PROCESSING
LA English
DT Article
DE Metal matrix composite; B4C; Artificial neural network; Thin plate
spline
ID PARTICLE DISTRIBUTION; ENERGY MANAGEMENT; MOLTEN ALUMINUM;
NEURAL-NETWORK; WEAR BEHAVIOR; SIC PARTICLES; SPARK PLASMA; PREDICTION;
MICROSTRUCTURE; MICROWAVE
AB This paper investigates the manufacturing of aluminium boron carbide composites
using the stir casting method. Mechanical and physical properties tests to obtain
hardness, ultimate tensile strength (UTS) and density are performed after
solidification of specimens. The results show that hardness and tensile strength of
aluminium based composite are higher than monolithic metal. Increasing the volume
fraction of B4C, enhances the tensile strength and hardness of the composite;
however over-loading of B4C caused particle agglomeration, rejection from molten
metal and migration to slag. This phenomenon decreases the tensile strength and
hardness of the aluminium based composite samples cast at 800 degrees C. For Al-15
vol% B4C samples, the ultimate tensile strength and Vickers hardness of the samples
that were cast at 1000 degrees C, are the highest among all composites. To predict
the mechanical properties of aluminium matrix composites, two key prediction
modelling methods including Neural Network learned by Levenberg-Marquardt Algorithm
(NN-LMA) and Thin Plate Spline (TPS) models are constructed based on experimental
data. Although the results revealed that both mathematical models of mechanical
properties of Al-B4C are reliable with a high level of accuracy, the TPS models
predict the hardness and tensile strength values with less error compared to NN-LMA
models. (C) 2016 Elsevier B.V. All rights reserved.
C1 [Shirvanimoghaddam, K.; Khayyam, H.; Naebe, M.] Deakin Univ, Inst Frontier Mat,
Geelong, Vic 3216, Australia.
[Abdizadeh, H.] Univ Tehran, Sch Met & Mat Engn, POB 11365-4563, Tehran, Iran.
[Akbari, M. Karbalaei] Semnan Univ, Fac Met & Mat Engn, POB 35131-19111, Semnan,
Iran.
[Pakseresht, A. H.; Ghasali, E.] Mat & Energy Res Ctr, POB 31787-316, Karaj,
Iran.
C3 Deakin University; University of Tehran; Semnan University; Materials &
Energy Research Center (MERC)
RP Shirvanimoghaddam, K; Naebe, M (corresponding author), Deakin Univ, Inst
Frontier Mat, Geelong, Vic 3216, Australia.
EM kshirvan@deakin.edu.au; minoo.naebe@deakin.edu.au
RI Ghasali, Ehsan/ABB-1676-2021; Pakseresht, Amirhossein/Y-2290-2019;
Shirvanimoghaddam, Kamyar/ABF-5501-2020; abdizadeh, Hossein/W-3235-2018;
ghasali, ehsan/S-3764-2019
OI Ghasali, Ehsan/0000-0003-4010-2506; Pakseresht,
Amirhossein/0000-0001-6548-8113; Kara, Gheffar/0000-0003-1589-5778;
Khayyam, Hamid/0000-0001-9784-1452; Naebe, Minoo/0000-0002-0607-6327;
Karbalaei akbari, Mohammad/0000-0001-9367-8475; Shirvani Moghaddam,
Kamyar/0000-0002-8136-8389
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NR 64
TC 107
Z9 109
U1 3
U2 76
PI LAUSANNE
SN 0921-5093
EI 1873-4936
J9 MAT SCI ENG A-STRUCT
JI Mater. Sci. Eng. A-Struct. Mater. Prop. Microstruct. Process.
PD MAR 21
PY 2016
VL 658
BP 135
EP 149
DI 10.1016/j.msea.2016.01.114
PG 15
WC Nanoscience & Nanotechnology; Materials Science, Multidisciplinary;
Metallurgy & Metallurgical Engineering
SC Science & Technology - Other Topics; Materials Science; Metallurgy &
GA DH1QU
UT WOS:000372560800016
DA 2023-12-05
ER
PT J
AU Le Saoût, G
Ben Haha, M
Winnefeld, F
Lothenbach, B
AF Le Saout, Gwenn
Ben Haha, Mohsen
Winnefeld, Frank
Lothenbach, Barbara
TI Hydration Degree of Alkali-Activated Slags: A 29Si NMR Study
LA English
DT Article
ID BLAST-FURNACE SLAG; SI-29 MAS NMR; C-S-H; HIGH-RESOLUTION NMR; PORTLAND
CEMENTS; AL-27 NMR; SELECTIVE DISSOLUTION; PART I; ALUMINUM; CHEMISTRY
AB A commercial blast furnace slag was activated using either sodium hydroxide or
hydrous sodium metasilicate, and the degree of hydration was determined by 29Si
magic angle spinning nuclear magnetic resonance (NMR). The results are compared
with measurements made using scanning electron microscopy image analysis (SEM-IA).
The results from both 29Si NMR and the SEM-IA measurements indicated a fast initial
reaction with the alkali, and similar degrees of hydration throughout the reaction.
The 29Si NMR results were analyzed using two different methods for fitting the
residual slag in the decomposition of the 29Si NMR spectra: the first method used
the spectrum of the anhydrous slag, whereas the second method used the spectrum of
the dissolution residue of the hydrated sample. Only the first method provided a
satisfactory simulation. The degree of hydration and the Al/Si atomic ratio within
the CSH, deduced by 29Si NMR were in agreement with SEM-IA and EDX analyses.
C1 [Le Saout, Gwenn; Ben Haha, Mohsen; Winnefeld, Frank; Lothenbach, Barbara] Empa,
Swiss Fed Labs Mat Sci & Technol, Concrete & Construct Chem Lab, CH-8600 Dubendorf,
Switzerland.
RP Le Saoût, G (corresponding author), Empa, Swiss Fed Labs Mat Sci & Technol,
Concrete & Construct Chem Lab, Uberlandstr 129, CH-8600 Dubendorf, Switzerland.
EM gwenn.lesaout@empa.ch
RI Le Saout, Gwenn/H-9886-2019; Ben Haha, Mohsen/AAC-4859-2020; Winnefeld,
Frank/B-5335-2009; Lothenbach, Barbara/C-6275-2013
OI Le Saout, Gwenn/0000-0002-2761-0584; Ben Haha,
Mohsen/0000-0001-7570-326X; Winnefeld, Frank/0000-0002-6864-6196;
Lothenbach, Barbara/0000-0002-9020-6488
10.1016/j.cemconres.2005.04.010
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[Anonymous], NUCL MAGNETIC RESONA
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10.1016/j.cemconres.2010.02.012
NR 40
TC 107
Z9 115
U1 6
U2 109
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD DEC
PY 2011
VL 94
IS 12
BP 4541
EP 4547
DI 10.1111/j.1551-2916.2011.04828.x
PG 7
GA 859BC
UT WOS:000297848100073
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Zhao, Y
Wang, J
Luan, ZK
Peng, XJ
Liang, Z
Shi, L
AF Zhao, Ying
Wang, Jun
Luan, Zhaokun
Peng, Xianjia
Liang, Zhen
Shi, Li
TI Removal of phosphate from aqueous solution by red mud using a factorial
design
LA English
DT Article
DE Phosphate removal; Red mud; Sorption; Factorial design
ID FLY-ASH; ALUMINUM-INDUSTRY; ADSORPTION; WASTEWATERS; BAUXITE; WASTE;
WATER; SLAG; MECHANISMS; ADSORBENT
AB The purpose of the work is to study the adsorption of phosphate on red mud from
aqueous solutions using 21 full factorial designs. The important parameters, which
affect the removal efficiency of phosphate and final pH Of Solution (pH(f)), such
as phosphate concentration, initial pH of solution (pH(i)) and the red mud dosage
were investigated. The effects of individual variables and their interaction
effects for dependent variables, namely, phosphate removal efficiency and pH(f)
were determined. The results of the study showed that phosphate removal efficiency
and pHf were found to be 97.6% and 10.9 with optimal reaction conditions initial
phosphate concentration 25 mg l(-1), red mud dosage 1.5 g l(-1), pH(i) 3.0,
respectively. It was found that adequate amount of calcium ions and higher final pH
than 9 are ideal conditions for maximum phosphate removal. (c) 2008 Published by
Elsevier B.V.
C1 [Zhao, Ying; Wang, Jun; Luan, Zhaokun; Peng, Xianjia; Liang, Zhen; Shi, Li]
Chinese Acad Sci, State Key Lab Environm Aquat Chem, Ecoenvironm Sci Res Ctr,
C3 Chinese Academy of Sciences; Research Center for Eco-Environmental
Sciences (RCEES)
RP Luan, ZK (corresponding author), Chinese Acad Sci, State Key Lab Environm Aquat
Chem, Ecoenvironm Sci Res Ctr, POB 2871, Beijing 100085, Peoples R China.
EM zhao_ying005@yahoo.com.cn; Luanzk@rcees.ac.cn
RI Zhao, Ying/GRJ-6516-2022; Wang, Jing/B-3198-2009; Zhao,
Ying/S-3612-2016; Ying, Zhao/JFJ-7079-2023; Liang, Zhen/S-8028-2019
OI Zhao, Ying/0000-0002-9414-2717; wang, jun/0000-0001-5841-0289
FU National Key Technology RD Program [2006BAJ0SB00]; Ministry of Science &
Technology of China [2007AA06Z344]; Public Industry Research for
National Environmental Protection [200709037]
FX The research work was financially supported by National Key Technology
R&D Program (2006BAJ0SB00), National High Technology R&D Program (863)
from Ministry of Science & Technology of China (2007AA06Z344) and Public
Industry Research for National Environmental Protection (200709037). The
authors thank Research Institute of Shandong Aluminium Co. Ltd., for
providing the red mud. Thanks are due to the editors and anonymous
reviewers for their helpful suggestions and enlightening comments.
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U1 2
U2 49
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
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VL 165
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BP 1193
EP 1199
DI 10.1016/j.jhazmat.2008.10.114
PG 7
GA 446KY
UT WOS:000266121700160
PM 19091463
OA Green Published
DA 2023-12-05
ER
PT J
AU Celik, E
Nalbantoglu, Z
AF Celik, Ece
Nalbantoglu, Zalihe
TI Effects of ground granulated blastfurnace slag (GGBS) on the swelling
properties of lime-stabilized sulfate-bearing soils
SO ENGINEERING GEOLOGY
LA English
DT Article
DE Lime; Expansive soil; Swell; Sulfate-bearing soils; Ettringite; Slag
ID MICROSTRUCTURE
AB The use of calcium-based stabilizers such as calcium oxide (lime) in sulfate-
bearing clay soils has historically caused structural distress due to the formation
of ettringite, an expansive mineral which develops in the presence of sulfate,
calcium, and aluminum compounds of clay fraction. In this work, a research was
conducted to study the effectiveness of ground granulated blastfurnace slag (GGBS),
an industrial by-product, for providing better stabilization of sulfate bearing
soils. Laboratory tests were first performed on the lime-treated expansive soil
containing different concentrations of added sulfate and then the same tests were
repeated on the lime-treated soil, containing the same concentration of sulfate but
this time adding 6% slag. Three different sulfate concentrations (2000, 5000, and
10,000 ppm) were used in the study and the compaction relationships, Atterberg
limits, linear shrinkage and swell potentials were investigated. Test results
indicated that the presence of sulfate in the soil resulted in abnormal increase in
the plasticity and the swell potential of the lime-treated soil with 5000 and
10,000 ppm sulfate concentrations. The swell potential of the lime-treated soil
with 10,000 ppm sulfate concentration became three times higher than that of the
natural soil. The scanning electron micrograph of this higher swell potential soil
confirmed the growth of the ettringite minerals. On the other hand, test results
indicated that the use of lime with GGBS in stabilizing sulfate bearing clays
produced significant improvements in the plasticity as well as the swell potential.
Addition of 6% slag into the lime treated soil eliminated the harmful effect of
sulfate in the soils. In the presence of 6% slag, the swell potential of the lime-
treated soil with 10,000 ppm sulfate concentration decreased from 8% to 1%, whereas
the lime-treated soil with 5000 ppm sulfate concentration showed no swelling. (c)
C1 [Celik, Ece; Nalbantoglu, Zalihe] Eastern Mediterranean Univ, Dept Civil Engn,
Gazimagusa 10, Mersin, Turkey.
C3 Eastern Mediterranean University
RP Celik, E (corresponding author), Eastern Mediterranean Univ, Dept Civil Engn,
Gazimagusa 10, Mersin, Turkey.
EM ece.celik@emu.edu.tr; zalihe.nalbantoglu@emu.edu.tr
RI Nalbantoglu, Zalihe/AAC-1639-2020; Celik, Ece/J-1251-2019
OI Nalbantoglu, Zalihe/0000-0002-1524-6594
CR Abduljauwad S.N., 1993, ASCE GEOTECHNICAL SP, V36, P100
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NR 23
TC 105
Z9 112
U1 8
U2 56
PU ELSEVIER
PI AMSTERDAM
SN 0013-7952
EI 1872-6917
J9 ENG GEOL
JI Eng. Geol.
PD AUG 19
PY 2013
VL 163
BP 20
EP 25
DI 10.1016/j.enggeo.2013.05.016
PG 6
WC Engineering, Geological; Geosciences, Multidisciplinary
SC Engineering; Geology
GA 204VI
UT WOS:000323399000003
DA 2023-12-05
ER
PT J
AU Kim, DH
Shin, MC
Choi, HD
Seo, CI
Baek, K
AF Kim, Do-Hyung
Shin, Min-Chul
Choi, Hyun-Doc
Seo, Chang-Il
Baek, Kitae
TI Removal mechanisms of copper using steel-making slag: adsorption and
precipitation
SO DESALINATION
LA English
CT Conference of the European-Desalination-Society and
Center-for-Research-and-Technology-Hellas
CY APR 22-25, 2007
CL Halkidiki, GREECE
DE adsorption; precipitation; copper; relative contribution
ID WATER; SORPTION; NICKEL; IONS
AB Slag, which consists of calcium oxide, aluminium oxide, and other metal oxides,
is an abundant by-product in steel-making process. It has been used as adsorbents
to remove various heavy metals and the major removal mechanisms are precipitation
and adsorption on the surface of metal oxide. However, the relative contribution of
two removal mechanisms has not reported. In this study, the removal characteristics
of copper were investigated in terms of sorption kinetics and sorption isotherms.
As initial pH of solution increased, the sorption capacity of slags increased
dramatically. We evaluated the relative contribution of two mechanisms in the
copper removal by steel-making slag. At above pH 3.0, contribution of adsorption to
overall removal of copper was less than 12%. As a result, most of copper was
removed by slag as a form or copper hydroxide.
C1 [Kim, Do-Hyung; Shin, Min-Chul; Choi, Hyun-Doc; Baek, Kitae] Kumoh Natl Inst
Technol, Dept Environm Engn, Gumi 730701, Kyeong Buk, South Korea.
[Seo, Chang-Il] Environm Management Corp, Dept Soil & Groundwater, Inchon
404708, South Korea.
C3 Kumoh National University Technology
RP Baek, K (corresponding author), Kumoh Natl Inst Technol, Dept Environm Engn, 1
Yangho Dong, Gumi 730701, Kyeong Buk, South Korea.
EM kbaek@kumoh.ac.kr
RI Baek, Kitae/F-1515-2011
OI Baek, Kitae/0000-0002-7976-6484
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Yan JY, 2000, WASTE MANAGE, V20, P217, DOI 10.1016/S0956-053X(99)00318-9
NR 14
TC 105
Z9 117
U1 1
U2 55
PU ELSEVIER
PI AMSTERDAM
SN 0011-9164
EI 1873-4464
J9 DESALINATION
JI Desalination
PD MAR 1
PY 2008
VL 223
IS 1-3
BP 283
EP 289
DI 10.1016/j.desal.2007.01.226
PG 7
WC Engineering, Chemical; Water Resources
SC Engineering; Water Resources
GA 281PI
UT WOS:000254510200037
DA 2023-12-05
ER
PT J
AU Dai, Z
Tran, TT
Skibsted, J
AF Dai, Zhuo
Tran, Thuan T.
Skibsted, Jorgen
TI Aluminum Incorporation in the C-S-H Phase of White Portland
Cement-Metakaolin Blends Studied by 27Al and 29Si
MAS NMR Spectroscopy
LA English
DT Article
ID NUCLEAR-MAGNETIC-RESONANCE; THERMAL TRANSFORMATION; TRICALCIUM SILICATE;
POZZOLAN METAKAOLIN; HARDENED PASTES; ETTRINGITE; HYDRATION; SLAG; OPC;
QUANTIFICATION
AB The composition and structure of the calcium-silicate-hydrate (C-S-H) phases
formed by hydration of white portland cement-metakaolin (MK) blends have been
investigated using Al-27 and Si-29 MAS NMR. This includes blends with 0, 5, 10, 15,
20, 25, 30 wt% MK, following their hydration from 1 d to 1 yr. (29) Si MAS NMR
reveals that the average Al/Si ratio for the C-S-H phases, formed by hydration of
the portland cement-MK blends, increases almost linearly with the MK content but is
invariant with the hydration time for a given MK content. Correspondingly, the
average aluminosilicate chain lengths of the C-S-H increase with increasing MK
content, reflecting the formation of a C-S-H with a lower Ca/Si ratio. The increase
in Al/Si ratio with increasing MK content is supported by Al-27 MAS NMR which also
allows detection of stratlingite and fivefold coordinated aluminum, assigned to
AlO5 sites in the interlayer of the C-S-H structure. Stratlingite is observed after
prolonged hydration for MK substitution levels above 10 wt% MK. This is at a
somewhat lower replacement level than expected from thermodynamic considerations
which predict the formation of stratlingite for MK contents above 15 wt% after
prolonged hydration for the actual portland cement-MK blends. The increase in
fivefold coordinated Al with increasing MK content suggests that these sites may
contribute to the charge balance of the charge deficit associated with the
incorporation of Al3+ ions in the silicate chains of the C-S-H structure.
C1 [Skibsted, Jorgen] Aarhus Univ, Dept Chem, DK-8000 Aarhus C, Denmark.
Aarhus Univ, Interdisciplinary Nanosci Ctr iNANO, Instrument Ctr Solid State NMR
Spect, DK-8000 Aarhus C, Denmark.
C3 Aarhus University; Aarhus University
RP Skibsted, J (corresponding author), Aarhus Univ, Dept Chem, DK-8000 Aarhus C,
Denmark.
EM jskib@chem.au.dk
FU Danish Natural Science Research Council; Danish Technical Science
Research Council; Carlsbergfondet; Danish National Advanced Technology
Foundation
FX The use of the facilities at the Instrument Centre for Solid-State NMR
Spectroscopy, Department of Chemistry, Aarhus University, sponsored by
the Danish Natural Science Research Council, the Danish Technical
Science Research Council, and Carlsbergfondet, is acknowledged. We thank
the Danish National Advanced Technology Foundation for financial support
to the SCM project. Aalborg Portland A/S, Cementia Holding ApS is
acknowledged for providing the white portland cements used in this
study.
10.1016/j.cemconres.2005.04.010
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NR 50
TC 103
Z9 105
U1 4
U2 73
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD AUG
PY 2014
VL 97
IS 8
BP 2662
EP 2671
DI 10.1111/jace.13006
PG 10
GA AN4AE
UT WOS:000340529200055
DA 2023-12-05
ER
PT J
AU Saikia, N
Cornelis, G
Mertens, G
Elsen, J
Van Balen, K
Van Gerven, T
Vandecasteele, C
AF Saikia, Nabajyoti
Cornelis, Geert
Mertens, Gilles
Elsen, Jan
Van Balen, Koenraad
Van Gerven, Tom
Vandecasteele, Carlo
TI Assessment of Pb-slag, MSWI bottom ash and boiler and fly ash for using
as a fine aggregate in cement mortar
LA English
DT Article
DE MSWI ash; Pb-slag; fine aggregate; mineralogy; leaching
ID MUNICIPAL SOLID-WASTE; PORTLAND-CEMENT; BLENDED CEMENT; SLUDGE ASH;
INCINERATION; CONCRETE; LEAD; CONSTRUCTION; PERFORMANCE; MANAGEMENT
AB Three types of wastes, metallurgical slag from Pb production (SLG), the sand-
sized (0.1-2mm) fraction of MSWI bottom ash from a grate furnace (SF), and boiler
and fly ash from a fluidised bed incinerator (BFA), were characterized and used to
replace the fine aggregate during preparation of cement mortar. The chemical and
mineralogical behaviour of these wastes along with the reactivities of the wastes
with lime and the hydration behaviour of ordinary Portland cement paste with and
without these wastes added were evaluated by various chemical and instrumental
techniques. The compressive strengths of the cement mortars containing waste as a
partial substitution of fine aggregates were also assessed. Finally, leaching
studies of the wastes and waste containing cement mortars were conducted. SLG
addition does not show any adverse affect during the hydration of cement, or on the
compressive strengths behaviours of mortars. Formation of expansive products like
ettringite, aluminium hydroxide and H-2 gas due to the reaction of some
constituents of BFA and SF with alkali creates some cracks in the paste as well as
in the cement mortars, which lower the compressive strength of the cement mortars.
However, utilization of all materials in cement-based application significantly
improves the leaching behaviour of the majority of the toxic elements compared to
the waste as such. (c) 2007 Elsevier B.V. All rights reserved.
C1 [Saikia, Nabajyoti; Cornelis, Geert; Van Gerven, Tom; Vandecasteele, Carlo]
Katholieke Univ Leuven, Dept Chem Engn, B-3001 Louvain, Belgium.
[Mertens, Gilles; Elsen, Jan] Katholieke Univ Leuven, Dept Geog & Geol, Appl
Geol & Mineral Res Grp, B-3001 Heverlee, Belgium.
[Van Balen, Koenraad] Katholieke Univ Leuven, Dept Civil Engn, B-3001 Heverlee,
Belgium.
C3 KU Leuven; KU Leuven; KU Leuven
RP Vandecasteele, C (corresponding author), Katholieke Univ Leuven, Dept Chem Engn,
Croylaan 46, B-3001 Louvain, Belgium.
EM saikianj@yahoo.co.uk; Carlo.Vandecasteele@cit.kuleuven.be
RI elsen, jan/AAB-9873-2021; Van Balen, Koenraad EP/C-2063-2012; Saikia,
Nabajyoti/AHD-4911-2022; Van Balen, Koenraad/Q-6350-2019; Saikia,
Nabajyoti/N-7769-2015; Cornelis, Geert/A-1556-2008; Van Gerven,
Tom/B-5806-2015; elsen, jan/AAE-2352-2021
OI Van Balen, Koenraad EP/0000-0001-6595-2051; Van Balen,
Koenraad/0000-0001-6595-2051; Cornelis, Geert/0000-0003-0078-6798; Van
Gerven, Tom/0000-0003-2051-5696; Saikia, Nabajyoti/0000-0003-3585-4092;
elsen, jan/0000-0002-4370-3852
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NR 53
TC 103
Z9 107
U1 1
U2 56
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD JUN 15
PY 2008
VL 154
IS 1-3
BP 766
EP 777
DI 10.1016/j.jhazmat.2007.10.093
PG 12
GA 304LO
UT WOS:000256111200099
PM 18068299
DA 2023-12-05
ER
PT J
AU Todoroki, H
Mizuno, K
AF Todoroki, H
Mizuno, K
TI Effect of silica in slag on inclusion compositions in 304 stainless
steel, deoxidized with aluminum
LA English
DT Article
DE spinel; magnesia; alumina; aluminum; deoxidation; stainless steel;
inclusion; silica; slag
ID FE-CR ALLOYS; LIQUID-IRON; DEOXIDATION EQUILIBRIA; STAINLESS-STEEL;
THERMODYNAMICS; MAGNESIUM; CHROMIUM; CALCIUM; MGO; NI
AB Experiments were carried out to determine the effect of silica in the slag of
CaO-SiO2-Al2O3-MgO-F system on the formation of MgO (.) Al2O3 spinel inclusion in
304 stainless steel deoxidized with Al. Immediately after the addition of Al into
the molten steel, alumina clusters formed. Simultaneously, reduction of MgO in the
slag occurred to raise Mg content in the steel. This resulted in the change in
inclusion composition to MgO (.) Al2O3 spinel which did not further change. In the
previous experiments with CaO-Al2O3-MgO-F slag, however, spinel inclusions changed
to MgO or liquid CaO-Al2O3-MgO system. The difference in behavior was caused by the
existence of silica in the slag. Silica in the slag was considered to prevent the
extensive reduction of MgO or CaO in the slag by Al to supply soluble Mg or Ca into
the molten steel. A stability diagram of inclusions corresponding to Mg and Al
contents in the steel was calculated employing available thermodynamic data. The
inclusion compositions experimentally obtained well agreed with the diagram. This
implies that spinel inclusions were the most stable in the molten 304 stainless
steel deoxidized with Al under the presence of 10mass% silica in the slag. As a
result, it was concluded that silica in the slag enhanced the formation of spinel
inclusions.
C1 Yakin Kawasaki Co Ltd, Technol Dev Dept, Nippon Yakin Kogyo Grp, Kawasaki
2108558, Japan.
RP Todoroki, H (corresponding author), Yakin Kawasaki Co Ltd, Technol Dev Dept,
Nippon Yakin Kogyo Grp, 4-2 Kojimacho, Kawasaki 2108558, Japan.
EM todoroki@nyk.co.jp
OI TODOROKI, HIDEKAZU/0009-0007-2654-1584
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NR 22
TC 103
Z9 118
U1 0
U2 23
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2004
VL 44
IS 8
BP 1350
EP 1357
PG 8
GA 848GD
UT WOS:000223454700010
OA gold
DA 2023-12-05
ER
PT J
AU Chappex, T
Scrivener, K
AF Chappex, Theodore
Scrivener, Karen
TI Alkali fixation of C-S-H in blended cement pastes and its relation to
alkali silica reaction
LA English
DT Article
DE Alkali silica reaction (C); Supplementary cementitious materials; Pore
solution (B); SEM (B)
ID FLY-ASH; PART II; FUME; METAKAOLIN; CONCRETE; EXPANSION; CHEMISTRY;
SYSTEMS; ABILITY; SLAG
AB Supplementary cementitious materials (SCM) are known to reduce or even stop
expansion due to alkali silica reaction (ASR) in concretes with reactive
aggregates. Studies indicate that the main reason for this is the decrease in
alkalinity of the pore solution of the cement paste, which in turn is attributed to
the change in composition of the C-S,H. In this paper we study the effect of
aluminium and silicon incorporation in C-S-H on the composition of the pore
solution in cement pastes containing SCMs. Different blended pastes of silica fume
and metakaolin were cast, in order to obtain the same Si/Ca ratio of the C-S-H but
with different aluminium contents. EDS micro analysis was made to determine the C-
S-H compositions. In parallel pore solutions were extracted and analysed. It is
found that the incorporation of aluminium does not increase the alkali fixation of
the C-S-H found in real cementitious materials, suggesting that the greater
effectiveness of SCMs containing alumina is due to other reasons. (C) 2012 Elsevier
Ltd. All rights reserved.
C1 [Chappex, Theodore; Scrivener, Karen] Ecole Polytech Fed Lausanne EPFL Lausanne,
Lab Construct Mat, Lausanne, Switzerland.
C3 Swiss Federal Institutes of Technology Domain; Ecole Polytechnique
Federale de Lausanne
RP Chappex, T (corresponding author), Ecole Polytech Fed Lausanne EPFL Lausanne,
Lab Construct Mat, Lausanne, Switzerland.
EM theodore.chappex@epfl.ch; karen.scrivener@epfl.ch
OI Scrivener, Karen/0000-0003-2640-1497
FU Sika Technology A.G.; B&G Ingenieurs Conseils
FX We thank Sika Technology A.G. and B&G Ingenieurs Conseils for the
financial support and Burgess Pigment for providing metakaolin.
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8846(01)00538-5
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10.1016/j.cemconres.2010.09.013
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9465(00)00097-4
6
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10.1016/j.cemconres.2003.12.026
8846(99)00168-4
10.1016/j.cemconres.2004.05.034
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8846(00)00283-0
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8846(99)00096-4
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10.1016/j.cemconres.2010.11.003
Villeneuve V., 2011, GEOLOGIE GENIE GEOLO
Zhang X, 2007, QUANTITATIVE MICROST
NR 23
TC 102
Z9 118
U1 1
U2 60
PI OXFORD
SN 0008-8846
JI Cem. Concr. Res.
PD AUG
PY 2012
VL 42
IS 8
BP 1049
EP 1054
DI 10.1016/j.cemconres.2012.03.010
PG 6
GA 978DB
UT WOS:000306719700002
DA 2023-12-05
ER
PT J
AU Zhao, RD
Yuan, Y
Cheng, ZQ
Wen, T
Li, J
Li, FH
Ma, ZJ
AF Zhao, Renda
Yuan, Yuan
Cheng, Zhengqing
Wen, Tian
Li, Jian
Li, Fuhai
Ma, Zhongguo John
TI Freeze-thaw resistance of Class F fly ash-based geopolymer concrete
LA English
DT Article
DE Class F fly ash-based geopolymer concrete; Slag; Freeze-thaw resistance;
Microstructure; Mineralogy; Inflection point
ID HIGH-PERFORMANCE; DURABILITY; SLAG; TECHNOLOGY
AB A set of Class F fly ash-based geopolymer concrete with slag gradient, namely,
GPC-10 (10% slag content), GPC-30 (30% slag content) and GPC-50 (50% slag content),
was prepared to study its freeze-thaw resistance. GPC-10 was wrapped in aluminum
foil and cured at 80 degrees C for 24 h to accelerate strength development. The
others were cured under standard conditions (20 +/- 2 degrees C, relative humidity
>= 95%). Rapid freeze-thaw cycle testing was carried out according to ASTM C666,
and an ordinary Portland cement concrete (OPCC) sample was used as the control. The
freeze-thaw resistance was evaluated by mass loss, relative dynamic elasticity
modulus and compressive strength loss. In addition, the microstructure and
mineralogy were characterized using scanning electron microscopy (SEM), mercury
intrusion porosimetry (MIP), energy dispersive X-ray spectrosocpy (EDS) and X-ray
diffraction (XRD). The results show that GPC-10 is damaged after five freeze-thaw
cycles, although high temperature curing improves its freeze-thaw resistance. GPC-
30 is damaged in 50 freeze-thaw cycles, while GPC-50 can withstand 225 freeze-thaw
cycles, which is comparable to the freeze-thaw resistance of the OPCC. Also, 125
freeze-thaw cycles marks an inflection point for the freeze-thaw resistance of GPC-
50, which is verified by the SEM and MIP results. The effect of adding slag on the
enhanced freeze-thaw resistance was analyzed by EDS and XRD. (C) 2019 Elsevier Ltd.
C1 [Zhao, Renda; Yuan, Yuan; Cheng, Zhengqing; Wen, Tian; Li, Jian; Li, Fuhai; Ma,
Zhongguo John] Southwest Jiaotong Univ, Sch Civil Engn, Chengdu 610031, Sichuan,
Peoples R China.
[Li, Fuhai] Southwest Jiaotong Univ, Key Lab High Speed Railway Engn, Minist
Educ, Chengdu 610031, Sichuan, Peoples R China.
[Ma, Zhongguo John] Univ Tennessee, Dept Civil & Environm Engn, Knoxville, TN
37916 USA.
C3 Southwest Jiaotong University; Southwest Jiaotong University; University
of Tennessee System; University of Tennessee Knoxville
RP Li, FH (corresponding author), Southwest Jiaotong Univ, Sch Civil Engn, Chengdu
610031, Sichuan, Peoples R China.; Li, FH (corresponding author), Southwest
Jiaotong Univ, Key Lab High Speed Railway Engn, Minist Educ, Chengdu 610031,
Sichuan, Peoples R China.
EM Lifuhai2007@home.swjtu.edu.cn
RI Ma, Zhongguo John/J-8595-2014
OI Ma, Zhongguo John/0000-0001-8246-7605; Cheng,
Zhengqing/0000-0002-1588-9952
FX The authors wish to acknowledge the financial support from the National
Natural Science Foundation of China (51778531).
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NR 37
TC 101
Z9 105
U1 24
U2 159
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 20
PY 2019
VL 222
BP 474
EP 483
DI 10.1016/j.conbuildmat.2019.06.166
PG 10
GA IU3BS
UT WOS:000483454300041
DA 2023-12-05
ER
PT J
AU Hajimohammadi, A
Ngo, T
Mendis, P
Sanjayan, J
AF Hajimohammadi, Ailar
Ngo, Tuan
Mendis, Priyan
Sanjayan, Jay
TI Regulating the chemical foaming reaction to control the porosity of
geopolymer foams
LA English
DT Article
DE Geopolymer foam; Chemical foaming; Aluminium powder; Embodied energy;
Sustainability
ID BLAST-FURNACE SLAG; SITU ATR-FTIR; FLY-ASH; ALKALINE ACTIVATION;
THERMAL-PROPERTIES; STRENGTH; ALUMINUM; CONCRETE; METAKAOLIN;
MICROSTRUCTURE
AB High percentage of aluminium foaming agent is not desirable in geopolymer foams
made with aluminium powder. Therefore, the kinetics of aluminium reaction is
regulated to increase the porosity of geopolymer foams without increasing the
extent of aluminium usage. In geopolymer foams made by Al powder, the
geopolymerization reaction and aluminium foaming reaction occur simultaneously. By
adjusting the ratio of alkali activators, the high degree of aluminium reaction has
been coupled with faster setting of geopolymers, and therefore, the extent of
porosity and the pore size distribution has been increased in geopolymer foams
without the need to add more Aluminium powder. Aluminium powder has high embodied
energy, and this study helps to minimise the negative environmental footprint of
geopolymer foams which are aerated by aluminium powder.
C1 [Hajimohammadi, Ailar; Ngo, Tuan; Mendis, Priyan] Univ Melbourne, Dept
Infrastruct Engn, Victoria 3010, Australia.
[Sanjayan, Jay] Swinburne Univ Technol, Fac Sci Engn & Technol, Victoria 3122,
Australia.
C3 University of Melbourne; Swinburne University of Technology
RP Hajimohammadi, A (corresponding author), Univ Melbourne, Dept Infrastruct Engn,
Victoria 3010, Australia.
EM ailar.hm@unimelb.edu.au
RI Sanjayan, Jay/AAD-1432-2020; Ngo, Tuan/P-8184-2014; Sanjayan,
Jay/AAE-1468-2019; Goodall, Liz J/O-9809-2016; Hajimohammadi,
Ailar/H-1822-2015
OI Ngo, Tuan/0000-0002-9831-8580; Sanjayan, Jay/0000-0002-5400-5988;
Goodall, Liz J/0000-0001-5354-574X; Hajimohammadi,
Ailar/0000-0002-2013-0668; Mendis, Priyan/0000-0003-4068-8201
FU ARC [LP140100504]
FX The authors would like to acknowledge the financial support from the ARC
Linkage Grant LP140100504 [grant number LP140100504, 2014]. This work is
performed in part at the Materials Characterisation and Fabrication
Platform (MCFP) at the University of Melbourne and the Victorian Node of
the Australian National Fabrication Facility (ANFF).
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NR 66
TC 101
Z9 104
U1 8
U2 84
PU ELSEVIER SCI LTD
PI OXFORD
SN 0264-1275
EI 1873-4197
J9 MATER DESIGN
JI Mater. Des.
PD APR 15
PY 2017
VL 120
BP 255
EP 265
DI 10.1016/j.matdes.2017.02.026
PG 11
GA EP4QM
UT WOS:000397365000026
DA 2023-12-05
ER
PT J
AU Yang, JK
Zhang, DD
Hou, J
He, BP
Xiao, B
AF Yang, Jiakuan
Zhang, Dudu
Hou, Jian
He, Baoping
Xiao, Bo
TI Preparation of glass-ceramics from red mud in the aluminium industries
LA English
DT Article
DE glass-ceramics; red mud; fly ash; crystallization; verification; wastes
recovery
ID SEWAGE-SLUDGE; FLY-ASH; SLAG; BEHAVIOR; WASTE
AB The feasibility of recycling red mud and fly ash in the aluminium industries by
producing glasses and glass-ceramics has been investigated. The crystallization
behavior of glass-ceramics mostly produced from red mud and fly ash was studied by
DTA, XRD, optical microscopy techniques. According to DTA curve, nucleation
experiments were carried out at various nucleation temperatures at the same
crystallization temperature of 900 degrees C for 2 h, and crystallization
experiments were performed at the same nucleation temperature of 697 degrees C for
2 h followed by crystallization at various temperatures. The nucleation results
show that optimum nucleation temperature is near 697 degrees C, and the
crystallization experiments show that the crystallization at a high temperature of
over 900 degrees C results in denser grain size. The major crystallized phases were
gehlenite (Ca2Al2SiO7), and augite (Ca(Fe,Mg)Si2O6). The XRD results show that with
the increase of crystallization temperature, the amount of gehlenite increases, and
augite decreases, which is the result of augite transformation into gehlenite. (C)
2006 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
C1 [Yang, Jiakuan; Zhang, Dudu; He, Baoping; Xiao, Bo] Huazhong Univ Sci & Technol,
Coll Environm Sci & Engn, Wuhan 430074, Peoples R China.
[Hou, Jian] Shandong Aluminum Co Ltd, Shandong 255100, Peoples R China.
C3 Huazhong University of Science & Technology
RP Yang, JK (corresponding author), Huazhong Univ Sci & Technol, Coll Environm Sci
& Engn, Wuhan 430074, Peoples R China.
EM yjiakuan@hotmail.com
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TC 101
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U1 1
U2 48
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
J9 CERAM INT
JI Ceram. Int.
PY 2008
VL 34
IS 1
BP 125
EP 130
DI 10.1016/j.ceramint.2006.08.013
PG 6
GA 244IB
UT WOS:000251858500020
DA 2023-12-05
ER
PT J
AU de Silva, NDG
Cholewa, E
Ryser, P
AF de Silva, Nayana Dilini Gardiyehewa
Cholewa, Ewa
Ryser, Peter
TI Effects of Combined Drought and Heavy Metal Stresses on Xylem Structure
and Hydraulic Conductivity in Red Maple (Acer rubrum L.)
SO JOURNAL OF EXPERIMENTAL BOTANY
LA English
DT Article
DE Acer rubrum; Cu; heavy metals; hydraulic conductivity; leaf-specific
conductivity; multiple stresses; Ni; water stress; xylem
ID DIFFERENTIAL ALUMINUM TOLERANCE; CADMIUM-INDUCED DECREASE; L CV
CONTENDER; WATER-STRESS; ABIOTIC STRESS; WHITE BIRCH; VESSEL SIZE;
GROWTH; ROOT; RESISTANCE
AB The effects of heavy metal stress, drought stress, and their combination on
xylem structure in red maple (Acer rubrum) seedlings were investigated in an
outdoor pot experiment. As metal-contaminated substrate, a mixture of 1.5% slag
with sand was used, with Ni, Cu, Co, and Cr as the main contaminants. Plants grown
on contaminated substrate had increased leaf metal concentrations. The two stresses
reduced plant growth in an additive manner. The effects of metal and drought
stresses on xylem characteristics were similar to each other, with a reduced
proportion of xylem tissue, reduced conduit density in stems, and reduced conduit
size in the roots. This resulted, in both stems and roots, in reductions in
hydraulic conductance, xylem-specific conductivity, and leaf-specific conductivity.
The similarity of the responses to the two stresses suggests that the plants'
response to metals was actually a drought response, probably due to the reduced
water uptake capacity of the metal-exposed roots. The only plant responses specific
to metal stress were decreasing trends of stomatal density and chlorophyll content.
In conclusion, the exposure to metals aggravates water stress in an additive
manner, making the plants more vulnerable to drought.
C1 [de Silva, Nayana Dilini Gardiyehewa; Ryser, Peter] Laurentian Univ, Dept Biol,
Sudbury, ON P3E 2C6, Canada.
[Cholewa, Ewa] Nipissing Univ, Dept Biol, N Bay, ON P1B 8L7, Canada.
C3 Laurentian University; Nipissing University
RP Ryser, P (corresponding author), Laurentian Univ, Dept Biol, 935 Ramsey Lake Rd,
Sudbury, ON P3E 2C6, Canada.
EM pryser@laurentian.ca
RI Ryser, Peter/G-7772-2011
OI Ryser, Peter/0000-0002-9495-9508
FU Natural Sciences and Engineering Research Council of Canada (NSERC)
[CRDPJ 372568-08]; Vale; Centre for Excellence in Mining Innovation
(CEMI)
FX We thank Luc Boileau for his great help with the set-up of the
experiment. The work was supported by a Collaborative Research and
Development Grant (CRDPJ 372568-08) of the Natural Sciences and
Engineering Research Council of Canada (NSERC) with Vale and the Centre
for Excellence in Mining Innovation (CEMI).
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TC 99
Z9 104
U1 2
U2 96
PU OXFORD UNIV PRESS
PI OXFORD
PA GREAT CLARENDON ST, OXFORD OX2 6DP, ENGLAND
SN 0022-0957
EI 1460-2431
J9 J EXP BOT
JI J. Exp. Bot.
PD OCT
PY 2012
VL 63
IS 16
BP 5957
EP 5966
DI 10.1093/jxb/ers241
PG 10
WC Plant Sciences
SC Plant Sciences
GA 021XR
UT WOS:000309919500018
PM 22966005
OA hybrid
DA 2023-12-05
ER
PT J
AU Sun, Y
Yao, MS
Zhang, JP
Yang, G
AF Sun, Yong
Yao, Ming-Shun
Zhang, Jing-Ping
Yang, Gang
TI Indirect CO2 mineral sequestration by steelmaking slag with
NH4Cl as leaching solution
SO CHEMICAL ENGINEERING JOURNAL
LA English
DT Article
DE Steelmaking slag; Mineralization; CO2 sequestration
ID CARBON-DIOXIDE; ACETIC-ACID; CAPTURE; STORAGE
AB The steelmaking slag (SL) is used for indirect CO2 mineral sequestration. The
optimized carbonation conditions include: initial pressure 10 bar, 60 degrees C,
400 rpm/min, 60 min duration. The high purity (96 +/- 2 wt%) calcium carbonate is
obtained under the optimized carbonation condition. The crystallite magnesium
carbonate together with other impurities such as aluminum oxide, ferrous oxide,
silica oxide, also exists in the precipitate with composition percentage below 2 wt
%. The characterization of the obtained precipitates at different temperatures by
SEM shows the gradual morphological changes from scalenohedral to rhombohedral
crystal with increase of carbonation temperature (within 20-80 degrees C). The
kinetic shows a fast reaction rate with 11.8 kJ/mol apparent activation energy,
indicating a diffusion determined core-shrinking reaction during carbonation. The
CO2 capture capacity was compared to different sequestration routes using different
industrial wastes. The maximum capacity from our experimental result could reach
211 kg CO2/ton SL with the contribution of CaCO3/MgCO3 together with Mg(HCO3)(2) in
capturing CO2. (C) 2011 Elsevier B.V. All rights reserved.
C1 [Zhang, Jing-Ping; Yang, Gang] Chinese Acad Sci, Inst Proc Engn, Beijing 100081,
Peoples R China.
[Sun, Yong; Yao, Ming-Shun; Yang, Gang] Anpeng Alkaline High Tech Co Ltd,
Beijing, Peoples R China.
C3 Chinese Academy of Sciences; Institute of Process Engineering, CAS
RP Yang, G (corresponding author), Chinese Acad Sci, Inst Proc Engn, Beijing
EM gangyangipecas@gmail.com
RI Sun, Yong/AAO-3995-2020; SUN, YONG/O-1126-2019; Zhang,
Jingping/D-8057-2017; Sun, Yong/F-7285-2012
OI Sun, Yong/0000-0002-4888-156X; Zhang, Jingping/0000-0002-3205-0470; Sun,
Yong/0000-0002-4888-156X
FU National High Technology Research and Development Program 863
[2011AA060703]
FX The National High Technology Research and Development Program 863
(2011AA060703) is highly appreciated for financial support. The kind
work undertaken in An-Shan Steelmaking Co Ltd. and Anpeng High-Tech
Alkaline Production Co Ltd. are appreciated as well. The critical
comments from anonymous reviewers are highly appreciated.
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TC 99
Z9 108
U1 3
U2 65
PI LAUSANNE
SN 1385-8947
J9 CHEM ENG J
JI Chem. Eng. J.
PD SEP 15
PY 2011
VL 173
IS 2
BP 437
EP 445
DI 10.1016/j.cej.2011.08.002
PG 9
WC Engineering, Environmental; Engineering, Chemical
SC Engineering
GA 831TJ
UT WOS:000295753700022
DA 2023-12-05
ER
PT J
AU Park, JH
Kim, DS
AF Park, JH
Kim, DS
TI Effect of CaO-Al2O3-MgO slags on the formation of
MgO-Al2O3 inclusions in ferritic stainless steel
LA English
DT Article
ID LIQUID-IRON; DEOXIDATION EQUILIBRIUM; ALUMINUM DEOXIDATION; AL
DEOXIDATION; MG; THERMODYNAMICS; CHROMIUM; ALLOYS
AB A thermodynamic equilibrium between the Fe-16Cr melts and the CaO-Al2O3-MgO
slags at 1823 K as well as the morphology of inclusions was investigated to
understand the formation behavior of the MgO-Al2O3 spinel-type inclusions in
ferritic stainless steel. The calculated and observed activities of magnesium in
Fe-16Cr melts are qualitatively in good agreement with each other, while those of
aluminum in steel melts exhibit some discrepancies with scatters. In the
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Al3+ ions at the metal/intermediate layer interface, (3) diffusion of Al3+ ions and
electrons through the intermediate layer, and (4) magnesium aluminate (MgAl2O4
spinel, for example) formation by the ionic reaction.
C1 POSCO, Stainless Steel Res Grp, Tech Res Labs, Pohang 790785, South Korea.
C3 POSCO
RP Park, JH (corresponding author), POSCO, Stainless Steel Res Grp, Tech Res Labs,
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[No title captured]
NR 26
TC 99
Z9 107
U1 2
U2 33
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2005
VL 36
IS 4
BP 495
EP 502
DI 10.1007/s11663-005-0041-0
PG 8
Engineering
GA 975CT
UT WOS:000232639300009
DA 2023-12-05
ER
PT J
AU Shih, PH
Wu, ZZ
Chiang, HL
AF Shih, PH
Wu, ZZ
Chiang, HL
TI Characteristics of bricks made from waste steel slag
SO WASTE MANAGEMENT
LA English
DT Article
ID FURNACE
AB The characteristics of bricks made from steel slag were investigated in this
research. Slag addition was shown to reduce the required firing temperature. When
the firing temperature was greater than 1050 degreesC and the slag addition less
than 10%, the bricks met ROC national standard CNS 3319 third-class brick for
builders. The percentage of slag increased as the quartz and kaolin decreased in
the sintered samples while the magnesium aluminum silicate and calcium silicate
increased. There were no new crystal phases observed in these samples. (C) 2004
C1 Fooyin Univ, Dept Environm Engn, Kaohsiung 831, Taiwan.
C3 Fooyin University
RP Chiang, HL (corresponding author), Fooyin Univ, Dept Environm Engn, Kaohsiung
831, Taiwan.
EM hlchiang@mail.fy.edu.tw
RI Hunglung, Chiang/O-3719-2015
OI Hunglung, Chiang/0000-0002-2186-628X
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TC 99
Z9 106
U1 1
U2 17
PI OXFORD
SN 0956-053X
J9 WASTE MANAGE
JI Waste Manage.
PY 2004
VL 24
IS 10
BP 1043
EP 1047
DI 10.1016/j.wasman.2004.08.006
PG 5
GA 878RL
UT WOS:000225664200009
PM 15567669
DA 2023-12-05
ER
PT J
AU Silva, ALVDE
AF Vasconcellos da Costa e Silva, Andre Luiz
TI Non-metallic inclusions in steels - origin and control
SO JOURNAL OF MATERIALS RESEARCH AND TECHNOLOGY-JMR&T
LA English
DT Review
DE Non-metallic inclusions; Ladle metallurgy; Steelmaking; Computational
thermodynamics; Kinetics
ID FERRITIC STAINLESS-STEEL; OF-THE-ART; SUBMERGED ENTRY NOZZLE; IN-SITU
OBSERVATION; FE-MN ALLOYS; STEELMAKING PROCESSES; ALUMINUM DEOXIDATION;
LIQUID STEEL; CARBON-STEEL; TIRE CORD
AB Non-metallic inclusions (NMIs) play a key role in many important properties of
steel, influencing both processing and application of steel products. In this work,
the current understanding of the origin and classification of NMIs is reviewed,
highlighting the dramatic development of the last decades. This includes the
discussion of the thermodynamics of inclusion formation and the current knowledge
on the effects of melt shop processing variable on NMIs composition, amount and
size distribution. The development of inclusion engineering - tailoring the process
to obtain the desired NMIs is highlighted and the development in selected areas -
tire cord, springs and bearing steels as well as prevention of nozzle clogging - is
used to illustrate this development. The promising field of "oxide metallurgy" is
also discussed in the context of inclusion engineering. Finally, the difficulties
in meaningfully characterizing and quantifying NMIs are briefly commented. In
summary it is concluded that inclusion control in steels has evolved significantly
in the last decades. This is due to the progress in understanding the interplay
between thermodynamics, steel and slag chemical composition as well as melt shop
processing. This made possible the tailoring of non-metallic inclusions via
processing, to optimize steel properties. Nonetheless, some important problems
remain and must still be solved to improve inclusion control and optimization. (C)
2018 Brazilian Metallurgical, Materials and Mining Association. Published by
Elsevier Editora Ltda. This is an open access article under the CC BY-NC-ND
license.
C1 [Vasconcellos da Costa e Silva, Andre Luiz] EEIMVR UFF, Volta Redonda, RJ,
Brazil.
C3 Universidade Federal Fluminense
RP Silva, ALVDE (corresponding author), EEIMVR UFF, Volta Redonda, RJ, Brazil.
EM andre.costaesilva@gmail.com
RI Costa e Silva, Andre L V/L-5134-2016; Silva, André/HHN-2071-2022
OI Costa e Silva, Andre L V/0000-0002-0513-8338;
FU CNPq; CAPES; FAPERJ
FX The support of CNPq, CAPES and FAPERJ during different stages on the
author's work is also acknowledged.
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NR 192
TC 98
Z9 105
U1 6
U2 60
PU ELSEVIER
PI AMSTERDAM
SN 2238-7854
EI 2214-0697
J9 J MATER RES TECHNOL
JI J. Mater. Res. Technol-JMRT
PD JUL-SEP
PY 2018
VL 7
IS 3
BP 283
EP 299
DI 10.1016/j.jmrt.2018.04.003
PG 17
Engineering
GA GS9IT
UT WOS:000444031700012
OA gold
DA 2023-12-05
ER
PT J
AU Mobasher, N
Bernal, SA
Provis, JL
AF Mobasher, Neda
Bernal, Susan A.
Provis, John L.
TI Structural evolution of an alkali sulfate activated slag cement
SO JOURNAL OF NUCLEAR MATERIALS
LA English
DT Article
DE Alkali-activated slag; Sodium sulfate; Microstructure; X-ray
diffraction; Nuclear magnetic resonance spectroscopy
ID C-S-H; HYDRATED PORTLAND CEMENTS; BLAST-FURNACE SLAG; ALUMINUM; NMR;
AL-27; SI-29; IMMOBILIZATION; ETTRINGITE; CHEMISTRY
AB In this study, the effect of sodium sulfate content and curing duration (from
fresh paste up to 18 months) on the binder structure of sodium sulfate activated
slag cements was evaluated. Isothermal calorimetry results showed an induction
period spanning the first three days after mixing, followed by an acceleration-
deceleration peak corresponding to the formation of bulk reaction products.
Ettringite, a calcium aluminium silicate hydrate (C-A-S-H) phase, and a
hydrotalcite-like Mg-Al layered double hydroxide have been identified as the main
reaction products, independent of the Na2SO4 dose. No changes in the phase
assemblage were detected in the samples with curing from 1 month up to 18 months,
indicating a stable binder structure. The most significant changes upon curing at
advanced ages observed were growth of the AFt phase and an increase in silicate
chain length in the C-A-S-H, resulting in higher strength. (C) 2015 Elsevier B.V.
C1 [Mobasher, Neda; Bernal, Susan A.; Provis, John L.] Univ Sheffield, Dept Mat Sci
& Engn, Immobilisat Sci Lab, Sheffield S1 3JD, S Yorkshire, England.
Immobilisat Sci Lab, Sheffield S1 3JD, S Yorkshire, England.
RI Bernal, Susan A/E-8938-2011; Provis, John/AAR-3260-2020; Provis, John
L/A-7631-2008
OI Provis, John/0000-0003-3372-8922; Provis, John L/0000-0003-3372-8922;
Bernal, Susan A/0000-0002-9647-3106
FU EPSRC through the University of Sheffield/University of Manchester
Doctoral Training Centre 'Nuclear FiRST' [EP/G037140/1]
FX This study has been sponsored by EPSRC through the University of
Sheffield/University of Manchester Doctoral Training Centre 'Nuclear
FiRST', grant number EP/G037140/1. The NMR spectra were collected using
the EPSRC UK National Solid-state NMR Service at Durham University, and
the assistance of Dr David Apperley is gratefully acknowledged. The
assistance of Dr. Oday H. Hussein in the SEM data collection is also
greatly acknowledged. The authors would like to thank Dr Hajime
Kinoshita for his valuable input into the PhD project of NM.
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NR 40
TC 98
Z9 102
U1 3
U2 64
PI AMSTERDAM
SN 0022-3115
EI 1873-4820
J9 J NUCL MATER
JI J. Nucl. Mater.
PD JAN
PY 2016
VL 468
BP 97
EP 104
DI 10.1016/j.jnucmat.2015.11.016
PG 8
WC Materials Science, Multidisciplinary; Nuclear Science & Technology
SC Materials Science; Nuclear Science & Technology
GA DA4HT
UT WOS:000367761700012
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Kim, GH
Sohn, I
AF Kim, Gi-Hyun
Sohn, Il
TI Effect of Al2O3 on the viscosity and structure of
calcium silicate-based melts containing Na2O and
CaF2
SO JOURNAL OF NON-CRYSTALLINE SOLIDS
LA English
DT Article
DE Al2O3; Viscosity; Melt structure; XPS; Raman
ID ALUMINOSILICATE GLASSES; BOROSILICATE GLASSES; RAMAN-SPECTROSCOPY;
SLAGS; ALUMINUM; XPS; PERALKALINE; CAO-AL2O3; CRYSTALS; CAO-SIO2
AB The effect of Al2O3 on viscosity in the calcium silicate melt-based system
containing Na2O and CaF2 was investigated and correlated with the melt structure
using FTIR (Fourier transform infrared) spectroscopy, XPS (X-ray photoelectron
spectroscopy), and Raman spectroscopy. Substituting SiO2 with Al2O3 modified the
dominant silicate network into a highly structured alumino-silicate structure with
the aluminate structure being particularly prevalent at 20 mass% of Al2O3 and
higher. As the melts become increasingly polymerized with higher Al2O3 content, the
fraction of symmetric Al-O degrees stretching vibrations significantly increased
and the viscosity increased. XPS showed a decrease in the amount of non-bridged
oxygen (O-) but an increase in bridged oxygen (O-0) and free oxygen (O2-) with
higher Al2O3. Although changes in the structure and viscosity with higher CaO/(SiO2
+ Al2O3) were not significant, the symmetric Al-O-0 stretching in the [AlO4](5-)-
tetrahedral units decreased. The apparent activation energy for viscous flow varied
from 118 to 190 kJ/mol. (C) 2012 Elsevier B.V. All rights reserved.
C1 [Kim, Gi-Hyun; Sohn, Il] Yonsei Univ, Seoul 120749, South Korea.
RP Sohn, I (corresponding author), Yonsei Univ, 262 Seongsanno, Seoul 120749, South
Korea.
RI SOHN, IL/I-5815-2012
FU Brain Korea 21 (BK21) Project at the Division of the Humantronics
Information Materials; National Science Foundation of Korea
[2010-8-0581]; Ministry of Knowledge Education [2010-8-0972]; National
Research Foundation of Korea [2010-0007442] Funding Source: Korea
Institute of Science & Technology Information (KISTI), National Science
& Technology Information Service (NTIS)
FX This study was partially supported by the Brain Korea 21 (BK21) Project
at the Division of the Humantronics Information Materials, the National
Science Foundation of Korea Project No. 2010-8-0581, and the Ministry of
Knowledge Education Project No, 2010-8-0972.
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PG 8
WC Materials Science, Ceramics; Materials Science, Multidisciplinary
GA 979LR
UT WOS:000306822000021
DA 2023-12-05
ER
PT J
AU Yoldi, M
Fuentes-Ordoñez, EG
Korili, SA
Gil, A
AF Yoldi, M.
Fuentes-Ordonez, E. G.
Korili, S. A.
Gil, A.
TI Zeolite synthesis from industrial wastes
SO MICROPOROUS AND MESOPOROUS MATERIALS
LA English
DT Article
DE Industrial waste valorization; Zeolite synthesis from wastes; Zeolite
environmental applications
ID COAL FLY-ASH; ALUMINUM SALINE SLAGS; NA-X; HIERARCHICAL ZEOLITES; CO2
ADSORPTION; VALORIZATION; MANAGEMENT; CONVERSION; REMOVAL; FUSION
AB Conventional synthesis conditions for each type of zeolite are tabulated and
reported by the International Zeolite Association Structure Commission (IZA) and
most of them are synthesized from commercial reagents, but they can also be
synthesized from industrial by-products rich in Si and/or Al. In zeolite synthesis
from wastes, concentration of alkali source, temperature, reaction time,
liquid/solid ratio and type of waste determine the textural properties, crystal
structure, Si/Al ratio and ion exchange characteristics of the fabricated zeolite
and its applications. This work summarizes the main methods that have been
developed to synthesize zeolites using industrial wastes as Al and/or Si sources,
the parameters of synthesis and the advantages and limitations of each synthesis
process. The main characteristics and the applications of these synthetic waste
zeolites are also reported.
C1 [Yoldi, M.; Fuentes-Ordonez, E. G.; Korili, S. A.; Gil, A.] Univ Publ Navarra,
INAMAT Sci Dept, Los Acebos Bldg,Campus Arrosadia, Pamplona 31006, Spain.
C3 Universidad Publica de Navarra
RP Gil, A (corresponding author), Univ Publ Navarra, INAMAT Sci Dept, Los Acebos
Bldg,Campus Arrosadia, Pamplona 31006, Spain.
EM andoni@unavarra.es
FU Spanish Ministry of Economy, Industry and Competitiveness (AEI/MINECO)
[MAT2016-78863-C2-1-R, PI017 CORRAL]; European Regional Development Fund
[MAT2016-78863-C2-1-R, PI017 CORRAL]; Government of Navarra
[MAT2016-78863-C2-1-R, PI017 CORRAL]; Santander Bank
FX The authors are grateful for financial support from the Spanish Ministry
of Economy, Industry and Competitiveness (AEI/MINECO), the European
Regional Development Fund and the Government of Navarra through projects
MAT2016-78863-C2-1-R and PI017 CORRAL. MY thanks Government of Navarra
for technologist recruitment. AG and EGFO also thank Santander Bank for
funding through the Research Intensification Program.
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NR 46
TC 97
Z9 98
U1 20
U2 144
PI AMSTERDAM
SN 1387-1811
EI 1873-3093
J9 MICROPOR MESOPOR MAT
JI Microporous Mesoporous Mat.
PD OCT
PY 2019
VL 287
BP 183
EP 191
DI 10.1016/j.micromeso.2019.06.009
PG 9
WC Chemistry, Applied; Chemistry, Physical; Nanoscience & Nanotechnology;
Materials Science, Multidisciplinary
SC Chemistry; Science & Technology - Other Topics; Materials Science
GA IJ6ET
UT WOS:000475995600021
DA 2023-12-05
ER
PT J
AU Yang, KH
Song, JK
AF Yang, Keun-Hyeok
Song, Jin-Kyu
TI Workability Loss and Compressive Strength Development of Cementless
Mortars Activated by Combination of Sodium Silicate and Sodium Hydroxide
LA English
DT Article
ID FLY-ASH; HYDRATION; SLAG
AB To explore the significance and shortcomings of an environment-friendly binder
using powder typed activators, 16 alkali-activated (AA) cementless mortars and a
control ordinary Portland cement (OPC) mortar were mixed, cured under room
temperature, and tested. Both fly ash (FA) and ground granulated blast-furnace slag
(GGBS) as the source material were activated by a combination of sodium silicate
and sodium hydroxide powders. The main variables examined were the mixing ratio of
sodium oxide (Na(2)O) of the activators to source material by weight, and the Blain
fineness of the GGBS. The flow loss and compressive strength development of the
mortars tested were examined according to the alkali quality coefficient explaining
the silicon oxide-to-sodium oxide ratio (SiO(2)/Na(2)O) in an alkaline activator,
and the silicon oxide-to-aluminum oxide (SiO(2)/Al(2)O(3)) ratio and calcium
content in the source material. The hydration products and microstructural
characteristics of the AA pastes sampled from AA mortars were also investigated to
evaluate the effect of the type and fineness of source material on the compressive
strength of the AA mortar. The measured compressive strength development of the AA
mortars was compared with an empirical equation for OPC concrete specified in ACI
209. The test results show that the flow loss and compressive strength development
of the AA mortars are significantly dependent on the alkali quality coefficient and
the fineness of the source material. Although no meaningful compressive strength
develops in the FA-based AA mortars, the 28 day compressive strength of the GGBS-
based AA mortars having an alkali quality coefficient of 0.023 is comparable to
that of the control OPC mortar, showing that the higher the fineness of GGBS, the
higher the compressive strength of AA mortars. Scanning electron microscope image
and x-ray diffraction clearly shows that the surface density of the calcium
silicate hydrates gel in the GGBS-based AA pastes increased with the increase of
fineness of the GGBS.
C1 [Yang, Keun-Hyeok] Mokpo Natl Univ, Dept Architectural Engn, Mokpo, Jeonnam,
South Korea.
[Song, Jin-Kyu] Chonnam Natl Univ, Dept Architectural Engn, Kwangju, South
Korea.
C3 Mokpo National University; Chonnam National University
RP Yang, KH (corresponding author), Mokpo Natl Univ, Dept Architectural Engn,
Mokpo, Jeonnam, South Korea.
EM yangkh@mokpo.ac.kr; jgsong@chonnam.ac.kr
FU (Bio-housing Research Institute); the Korean Ministry of Education &
Human Resources Development
FX This work was supported by the Regional Research Center Program
(Bio-housing Research Institute), granted by the Korean Ministry of
Education & Human Resources Development.
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NR 19
TC 97
Z9 104
U1 1
U2 36
PI RESTON
SN 0899-1561
PD MAR
PY 2009
VL 21
IS 3
BP 119
EP 127
DI 10.1061/(ASCE)0899-1561(2009)21:3(119)
PG 9
GA 407YL
UT WOS:000263400100004
DA 2023-12-05
ER
PT J
AU Bertron, A
Duchesne, J
Escadeillas, G
AF Bertron, A
Duchesne, J
Escadeillas, G
TI Accelerated tests of hardened cement pastes alteration by organic acids:
analysis of the pH effect
LA English
DT Article
DE organic acids; stability; pH; electronic microprobe; X-ray diffraction
ID C-S-H; FEED ACIDS; RESISTANCE; CONCRETE
AB Effluents, such as liquid manure and silage effluents, stored in silos often
made of concrete, contain organic acids that are chemically very aggressive for the
cement-based matrix. The pH of liquid manure is comprised between 6 and 8, and the
pH of silage effluent is about 4.
There has already been much research done on manure's effect on concrete using
aggressive solutions with a pH of or inferior to 4, in order to accelerate
alteration kinetics. These studies aimed at simulating liquid manure and silage
effluent, equally.
The goal of this article is to validate the use of solutions with a pH of 4 to
implement accelerated studies on alterations occurring to structures exposed to the
acidic part of liquid manure.
In this study, the alteration mechanisms of the cement-based matrix produced by
two solutions of organic acids with pH of 4 and 6 were compared.
At the end of the experiment, carried out on ordinary Portland cement and slag
cement pastes, the kinetics of alteration of the cement pastes immersed in the
solution with a pH of 4 was ninefold higher than in the solution with a pH of 6.
The chemical and mineralogical modifications of the paste were analyzed by
electron microprobe, XRD and BSE mode observations.
It was shown that the alteration mechanisms of the paste are sensibly identical
for both solutions: almost complete decalcification, the disappearance of the
crystallized or amorphous hydrated phases and the probable formation of a silica
gel containing aluminum and iron, mainly. The differences in alteration mechanisms
between the two solutions are minor and mainly concern the stability of the
anhydrous phascs: C(4)AF and slag grains. (C) 2004 Elsevier Ltd. All rights
reserved.
C1 INSA UPS, Lab Mat & Durabil Construct, F-31077 Toulouse, France.
Univ Laval, Beton Fac Sci & Genie, Ctr Rech Infrastruct, St Foy, PQ G1K 7P4,
Canada.
Toulouse; Institut National des Sciences Appliquees de Toulouse; Laval
University
RP Bertron, A (corresponding author), INSA UPS, Lab Mat & Durabil Construct,
Complexe Sci Rangueil, F-31077 Toulouse, France.
EM bertron@insa-toulouse.fr
RI Bertron, Alexandra/G-3418-2018; Duchesne, Josee/ACO-0812-2022
OI Bertron, Alexandra/0000-0002-6144-6810; Duchesne,
Josee/0000-0002-6327-4864
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TC 95
Z9 103
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U2 26
PI OXFORD
SN 0008-8846
JI Cem. Concr. Res.
PD JAN
PY 2005
VL 35
IS 1
BP 155
EP 166
DI 10.1016/j.cemconres.2004.09.009
PG 12
GA 898ZI
UT WOS:000227114300017
DA 2023-12-05
ER
PT J
AU Vasudevan, S
Sozhan, G
Ravichandran, S
Jayaraj, J
Lakshmi, J
Sheela, SM
Sozhan, Ganapathy
Ravichandran, Subbiah
Jayaraj, Jeganathan
Sheela, Sagayaraj Margrat
TI Studies on the removal of phosphate from drinking water by
electrocoagulation process
SO INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH
LA English
DT Article
PHOSPHORUS REMOVAL; ADSORPTION; ALUMINUM; SLUDGE; RAW
AB The present study provides an electrocoagulation process for the removal of
phosphate from drinking water using mild steel as the anode and stainless steel as
the cathode. The studies were carried out as a function of pH, temperature, current
density, and so forth, and the adsorption capacity was evaluated using both
Langmuir and Freundlich isotherm models. The results showed that the maximum
removal efficiency of 98% was achieved at a current density of 0.05 A center dot
dm(-2) at a pH of 6.5. The adsorption of phosphate preferably fitting the Langmuir
adsorption isotherm suggests monolayer coverage of adsorbed molecules. The
adsorption process follows second-order kinetics. Temperature studies showed that
adsorption was endothermic and spontaneous in nature.
C1 [Vasudevan, Subramanyan; Sozhan, Ganapathy; Ravichandran, Subbiah; Jayaraj,
Jeganathan; Lakshmi, Jothinathan; Sheela, Sagayaraj Margrat] CSIR, Karaikkudi
C3 Council of Scientific & Industrial Research (CSIR) - India
RP Vasudevan, S (corresponding author), CSIR, Karaikkudi 630006, Tamil Nadu, India.
EM vasudevan65@gmail.com
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TC 93
Z9 101
U1 1
U2 57
PI WASHINGTON
SN 0888-5885
J9 IND ENG CHEM RES
JI Ind. Eng. Chem. Res.
PD MAR 19
PY 2008
VL 47
IS 6
BP 2018
EP 2023
DI 10.1021/ie0714652
PG 6
WC Engineering, Chemical
SC Engineering
GA 273QU
UT WOS:000253947600033
DA 2023-12-05
ER
PT J
AU Ohta, H
Suito, H
AF Ohta, H
Suito, H
TI Activities of SiO2 and Al2O3 and
activity coefficients of FetO and MnO in
CaO-SiO2-Al2O3-MgO slags
LA English
DT Article
ID ALUMINUM OXYGEN EQUILIBRIUM; LIQUID-IRON; THERMODYNAMICS; NITROGEN
AB The activities of SiO2 and Al2O3 in CaO-SiO2-Al2O3-MgO slags were determined at
1873 K along the liquidus lines saturated with 2CaO . SiO2, 2(Mg,Ca)O . SiO2, MgO,
and MgO . Al2O3 phases using a slag-metal equilibration technique. Based on these
and previous results obtained in ternary and quaternary slags, the isoactivity
lines of SiO2 and Al2O3 over the liquid region on the 0, 10, 20, 30, and 40 mass
pet Al2O3 planes and those on the 10 and 20 mass pet MgO planes were determined.
The activity coefficients of FetO and MnO, the phase boundary, and the solubility
of MgO were also determined.
C1 Tohoku Univ, Inst Adv Mat Proc, Sendai, Miyagi 980, Japan.
C3 Tohoku University
RP Ohta, H (corresponding author), Tohoku Univ, Inst Adv Mat Proc, Sendai, Miyagi
980, Japan.
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NR 23
TC 93
Z9 107
U1 0
U2 15
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD FEB
PY 1998
VL 29
IS 1
BP 119
EP 129
DI 10.1007/s11663-998-0014-1
PG 11
Engineering
GA YY313
UT WOS:000072134600014
DA 2023-12-05
ER
PT J
AU Jackson, MD
Moon, J
Gotti, E
Taylor, R
Chae, SR
Kunz, M
Emwas, AH
Meral, C
Guttmann, P
Levitz, P
Wenk, HR
Monteiro, PJM
AF Jackson, Marie D.
Moon, Juhyuk
Gotti, Emanuele
Taylor, Rae
Chae, Sejung R.
Kunz, Martin
Emwas, Abdul-Hamid
Meral, Cagla
Guttmann, Peter
Levitz, Pierre
Wenk, Hans-Rudolf
Monteiro, Paulo J. M.
TI Material and Elastic Properties of Al-Tobermorite in Ancient Roman
Seawater Concrete
LA English
DT Article
ID C-S-H; HYDROUS CALCIUM SILICATES; AUTOCLAVING PROCESS;
CRYSTAL-CHEMISTRY; CATION-EXCHANGE; MINERALS; ALUMINUM; EVOLUTION;
AL-27; NMR
AB The material characteristics and elastic properties of aluminum-substituted 11
angstrom tobermorite in the relict lime clasts of 2000-year-old Roman seawater
harbor concrete are described with TG-DSC and Si-29 MAS NMR studies, along with
nanoscale tomography, X-ray microdiffraction, and high-pressure X-ray diffraction
synchrotron radiation applications. The crystals have aluminum substitution for
silicon in tetrahedral bridging and branching sites and 11.49(3)angstrom interlayer
(002) spacing. With prolonged heating to 350 degrees C, the crystals exhibit normal
behavior. The experimentally measured isothermal bulk modulus at zero pressure, K-
0, 55 +/- 5GPa, is less than ab initio and molecular dynamics models for ideal
tobermorite with a double-silicate chain structure. Even so, K-0, is substantially
higher than calcium-aluminum-silicate-hydrate binder (C-A-S-H) in slag concrete.
Based on nanoscale tomographic study, the crystal clusters form a well connected
solid, despite having about 52% porosity. In the pumiceous cementitious matrix, Al-
tobermorite with 11.27 angstrom interlayer spacing is locally associated with
phillipsite, similar to geologic occurrences in basaltic tephra. The ancient
concretes provide a sustainable prototype for producing Al-tobermorite in high-
performance concretes with natural volcanic pozzolans.
C1 [Jackson, Marie D.; Moon, Juhyuk; Taylor, Rae; Chae, Sejung R.; Meral, Cagla;
Monteiro, Paulo J. M.] Univ Calif Berkeley, Dept Civil & Environm Engn, Berkeley,
CA 94720 USA.
[Moon, Juhyuk] SUNY Stony Brook, Dept Mech Engn, Civil Engn Program, Stony
Brook, NY 11794 USA.
[Gotti, Emanuele] CTG Italcementi SpA, I-24126 Bergamo, Italy.
[Kunz, Martin] Univ Calif Berkeley, Lawrence Berkeley Natl Lab, Berkeley, CA
94720 USA.
[Emwas, Abdul-Hamid] King Abdullah Univ Sci & Technol, Thuwal 239556900, Saudi
Arabia.
[Meral, Cagla] Middle E Tech Univ, TR-06800 Ankara, Turkey.
[Guttmann, Peter] Helmholtz Zentrum Mat & Energie GmbH, Inst Soft Matter & Funct
Mat, D-12489 Berlin, Germany.
[Levitz, Pierre] Univ Paris 06, CNRS, Lab PECSA, F-75005 Paris, France.
[Wenk, Hans-Rudolf] Univ Calif Berkeley, Dept Earth & Planetary Sci, Berkeley,
CA 94720 USA.
C3 University of California System; University of California Berkeley;
State University of New York (SUNY) System; State University of New York
(SUNY) Stony Brook; United States Department of Energy (DOE); Lawrence
Berkeley National Laboratory; University of California System;
University of California Berkeley; King Abdullah University of Science &
Technology; Middle East Technical University; Helmholtz Association;
Helmholtz-Zentrum fuer Materialien und Energie GmbH (HZB); Sorbonne
Universite; Centre National de la Recherche Scientifique (CNRS);
University of California System; University of California Berkeley
RP Monteiro, PJM (corresponding author), Univ Calif Berkeley, Dept Civil & Environm
Engn, Berkeley, CA 94720 USA.
EM monteiro@ce.berkeley.edu
RI Jackson, Marie D/C-8463-2012; Meral Akgul, Cagla/K-8590-2013; Emwas,
Abdul-Hamid/AAG-5382-2020; Moon, Juhyuk/B-7009-2016; Guttmann,
Peter/H-9869-2015
OI Meral Akgul, Cagla/0000-0001-8720-1216; Moon,
Juhyuk/0000-0002-7049-892X; Guttmann, Peter/0000-0002-0534-238X;
Jackson, Marie D./0000-0002-5180-3060
FU King Abdullah University of Science and Technology (KAUST)
[KUS-l1-004021]; Office of Science, Department of Energy
[DE-AC02-05CH11231]; Advanced Nanofabrication Imaging and
Characterization Laboratories at King Abdullah University of Science and
Technology; ROMACONS drilling program; Directorate For Geosciences
[836402] Funding Source: National Science Foundation; Division Of Earth
Sciences [836402] Funding Source: National Science Foundation
FX This research was supported by Award No. KUS-l1-004021, from King
Abdullah University of Science and Technology (KAUST). Data were
acquired at beamlines 12.2.2 and 12.3.2 at the Advanced Light Source at
the Lawrence Berkeley Laboratories, supported by the Director of the
Office of Science, Department of Energy, under Contract No.
DE-AC02-05CH11231, and the Advanced Nanofabrication Imaging and
Characterization Laboratories at King Abdullah University of Science and
Technology. We thank CTG Italcementi researchers and staff, especially
B. Zanga, in Bergamo, Italy; G. Vola at Cimprogetti S.p.A., Dalmine,
Italy; S. Clark at the 12.2.2 beamline; and N. Tamura at the 12.3.2
beamline; and the ROMACONS drilling program: J. P. Oleson, C. Brandon,
R. Hohlfelder. T. Teague, D. Hernandez, C. Hargis, I. A. Delaney, and B.
Black provided research support. We thank J. G. Moore, M. Sintubin, G.
Sposito, P.-A. Itty, and J. Kirz for critical discussions, and three
anonymous reviewers whose comments improved the manuscript.
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NR 72
TC 92
Z9 100
U1 1
U2 91
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD AUG
PY 2013
VL 96
IS 8
BP 2598
EP 2606
DI 10.1111/jace.12407
PG 9
GA 199AE
UT WOS:000322965300040
DA 2023-12-05
ER
PT J
AU Fernández-Jiménez, A
Cristelo, N
Miranda, T
Palomo, A
AF Fernandez-Jimenez, Ana
Cristelo, Nuno
Miranda, Tiago
Palomo, Angel
TI Sustainable alkali activated materials: Precursor and activator derived
from industrial wastes
LA English
DT Article
DE Alkaline activation; Cleaning solution; Fly ash; Glass powder
ID RECYCLED ASPHALT PAVEMENT; EARLY AGE HYDRATION; COAL FLY-ASH;
PORTLAND-CEMENT; GEOPOLYMER; SLAG; STRENGTH; ALUMINUM; MICROSTRUCTURE;
TEMPERATURE
AB The aim of the present paper is to analyse the potential application of a
solution used to wash moulds from the aluminium casting industry as an alkali
activator, for inclusion in the production of alkaline cement. To evaluate the
effectiveness of this cleaning solution (CS), two different by-products/wastes were
considered as a precursor: fly ash type F (FA) and glass powder (GP) from the
production of optical lenses. An 8 molar sodium hydroxide commercial solution was
used to establish threshold values for the CS activator. Several mixtures were
prepared and cured for 20 h, at 85 degrees C, at high humidity (>= 90%). Mechanical
behaviour was assessed by uniaxial compression strength tests. The reaction rate
was determined by calorimetry, and the resulting reaction products were
characterized by X-ray diffraction (XRD), electron microscopy (SEM/EDX) and nuclear
magnetic resonance (NMR-MAS). The results show that the cleaning solution has a
high potential to be used as an activator in the manufacturing of alkali activated
cement, especially due to its tetrahedral aluminium content, which is particularly
effective for the activation of low-Al raw materials, since it acts simultaneously
as a cheap aluminium source. (C) 2017 Elsevier Ltd. All rights reserved.
C1 [Fernandez-Jimenez, Ana; Palomo, Angel] CSIC, IETcc, Eduardo Torroja Inst
Construct Sci, E-28033 Madrid, Spain.
[Cristelo, Nuno] Univ Tras Os Montes & Alto Douro, CQVR, Dept Engn, P-5000801
Vila Real, Portugal.
[Miranda, Tiago] Univ Minho, ISISE, Dept Civil Engn, Campus Azurem, P-4800058
Guimaraes, Portugal.
Tras-os-Montes & Alto Douro; Universidade do Minho
RP Cristelo, N (corresponding author), Univ Tras Os Montes & Alto Douro, CQVR, Dept
Engn, P-5000801 Vila Real, Portugal.
EM anafj@ietcc.csic.es; ncristel@utad.pt; tmiranda@civil.uminho.pt;
palomo@ietcc.csic.es
RI Cristelo, Nuno Miguel/B-3636-2010; Miranda, Tiago/ABE-2391-2020;
Miranda, Tiago/AAQ-9479-2021; Fernández, ANA Maria/G-2597-2016
OI Cristelo, Nuno Miguel/0000-0002-3600-1094; Miranda,
Tiago/0000-0003-4054-6860; Fernández, ANA Maria/0000-0002-5721-2923;
PALOMO, ANGEL/0000-0002-6964-2269
FU Spanish Ministry of the Economy and Competitiveness and funds FEDER
[BIA2013-43293-R, BIA2016-76466-R]
FX This research was funded by the Spanish Ministry of the Economy and
Competitiveness and funds FEDER under research projects BIA2013-43293-R
and BIA2016-76466-R. The authors would also like to acknowledge the
contribution of the Portuguese companies W2V - Waste to Value for the
supply of the cleaning solution; and POLO - Produtos Oticos, SA for the
supply of the glass residue.
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NR 65
TC 91
Z9 92
U1 3
U2 78
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD SEP 20
PY 2017
VL 162
BP 1200
EP 1209
DI 10.1016/j.jclepro.2017.06.151
PG 10
& Ecology
GA FC9UB
UT WOS:000407185500105
DA 2023-12-05
ER
PT J
AU Nakajima, K
Takeda, O
Miki, T
Matsubae, K
Nakamura, S
Nagasaka, T
AF Nakajima, Kenichi
Takeda, Osamu
Miki, Takahiro
Matsubae, Kazuyo
Nakamura, Shinichiro
Nagasaka, Tetsuya
TI Thermodynamic Analysis of Contamination by Alloying Elements in Aluminum
Recycling
SO ENVIRONMENTAL SCIENCE & TECHNOLOGY
LA English
DT Article
ID LEAD
AB In previous studies on the physical chemistry of pyrometallurgical processing of
aluminum scrap, only a limited number of thermodynamic parameters, such as the
Gibbs free energy change of impurity reactions and the variation of activity of an
impurity in molten aluminum, were taken into account In contrast, in this study we
thermodynamically evaluated the quantitative removal limit of impurities during the
remelting of aluminum scrap; all relevant parameters, such as the total pressure,
the activity coefficient of the target impurity, the temperature, the oxygen
partial pressure, and the activity coefficient of oxidation product, were
considered. For 45 elements that usually occur in aluminum products, the
distribution ratios among the metal, slag, and gas phases in the aluminum remelting
process were obtained. Our results show that, except for elements such as Mg and
Zn, most of the impurities occurred as troublesome tramp elements that are
difficult to remove, and our results also indicate that the extent to which the
process parameters such as oxygen partial pressure, temperature, and flux
composition can be changed in aluminum production is quite limited compared to that
for iron and copper production, owing to aluminum's relatively low melting point
and strong affinity for oxygen. Therefore, the control of impurities in the
disassembly process and the quality of scrap play important roles in suppressing
contamination in aluminum recycling.
C1 [Nakajima, Kenichi] Natl Inst Environm Studies, Res Ctr Mat Cycles & Waste
Management, Tsukuba, Ibaraki 3058506, Japan.
[Takeda, Osamu; Miki, Takahiro] Tohoku Univ, Grad Sch Engn, Sendai, Miyagi
9808579, Japan.
[Matsubae, Kazuyo; Nagasaka, Tetsuya] Tohoku Univ, Grad Sch Environm Studies,
Sendai, Miyagi 9808579, Japan.
[Nakamura, Shinichiro] Waseda Univ, Grad Sch Econ, Tokyo 1698050, Japan.
C3 National Institute for Environmental Studies - Japan; Tohoku University;
Tohoku University; Waseda University
RP Nakajima, K (corresponding author), Natl Inst Environm Studies, Res Ctr Mat
Cycles & Waste Management, Tsukuba, Ibaraki 3058506, Japan.
RI Nakajima, Kenichi/AAQ-3768-2021; Matsubae, Kazuyo/J-8842-2015
OI Nakajima, Kenichi/0000-0002-7241-7695; Matsubae,
Kazuyo/0000-0002-3816-3898
FU Nippon Steel Corporation; JSPS [22360218]; Grants-in-Aid for Scientific
Research [22360218, 22360387] Funding Source: KAKEN
FX This research was partially supported by Nippon Steel Corporation and
JSPS (KAKENHI 22360218). The authors thank the members of Research Group
of the Development of "Material Vision 2100" of the Iron and Steel
Institute of Japan for valuable comments and encouragement.
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U2 52
PI WASHINGTON
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EI 1520-5851
J9 ENVIRON SCI TECHNOL
JI Environ. Sci. Technol.
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IS 14
BP 5594
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GA 623NF
UT WOS:000279747100048
PM 20536230
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PT J
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KINGERY, WD
COOPER, AR
AF SAMADDAR, BN
KINGERY, WD
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TI DISSOLUTION IN CERAMIC SYSTEMS .2. DISSOLUTION OF ALUMINA, MULLITE,
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U1 0
U2 12
PU AMER CERAMIC SOC
PI WESTERVILLE
PA 735 CERAMIC PLACE, PO BOX 6136, WESTERVILLE, OH 43081-6136
SN 0002-7820
J9 J AM CERAM SOC
PY 1964
VL 47
IS 5
BP 249
EP 254
DI 10.1111/j.1151-2916.1964.tb14405.x
PG 6
GA WX398
UT WOS:A1964WX39800009
DA 2023-12-05
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PT J
AU JENA, BC
DRESLER, W
REILLY, IG
AF JENA, BC
DRESLER, W
REILLY, IG
TI EXTRACTION OF TITANIUM, VANADIUM AND IRON FROM TITANOMAGNETITE DEPOSITS
AT PIPESTONE LAKE, MANITOBA, CANADA
LA English
CT Minerals Engineering 94 Conference
CY SEP 26-28, 1994
CL LAKE TAHOE, NV
DE VANADIUM-BEARING TITANOMAGNETITE; SMELTING; SODA ASH ROASTING; HCL
LEACHING
AB A process has been developed at the laboratory scale for the recovery of
titanium, vanadium and iron from the vanadium bearing titanomagnetite deposit at
Pipestone Lake, Manitoba, by a combined pyro- and hydrometallurgical processing
route. The ore which contains 57.5% Fe, 0.66% V and 16.6% TiO2 was subjected to
selective reduction smelting so that most of the iron reported to the metal phase
and the vanadium and titanium to the slag phase. The iron had a purity of 99%. The
slag contained between 9-35% FeO, 31-46% TiO2, and 1.2-1.6% V. Over 98% of the
titanium and vanadium reported to the slag phase. The slag was roasted with soda
ash at 950 degrees C and then lenched with hot water at 80 degrees C to recover
vanadium. The leach residue was further treated with hydrochloric acid at 105
degrees C in order to upgrade TiO2 content by removing mainly iron, magnesium and
aluminum. The final product contained 82.9% TiO2, 1.5% FeO, 15.6% SiO2, 1% MgO, 2%
Al2O3, and 0.3% CaO with an overall titanium recovery above 90%. This product can
be utilized as feedstock to the pigment industry.
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NR 16
TC 88
Z9 102
U1 0
U2 30
PI OXFORD
PA THE BOULEVARD, LANGFORD LANE, KIDLINGTON, OXFORD, ENGLAND OX5 1GB
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD JAN-FEB
PY 1995
VL 8
IS 1-2
BP 159
EP 168
DI 10.1016/0892-6875(94)00110-X
PG 10
GA QE613
UT WOS:A1995QE61300014
DA 2023-12-05
ER
PT J
AU Lu, BX
Chen, K
Wang, WL
Jiang, BB
AF Lu, Boxun
Chen, Kun
Wang, Wanlin
Jiang, Binbin
TI Effects of Li2O and Na2O on the Crystallization
Behavior of Lime-Alumina-Based Mold Flux for Casting High-Al Steels
LA English
DT Article
ID VISCOSITY; RATIO; SLAGS
AB With the development of advanced high strength steel (AHSS), a large amount of
aluminum was added into steels. The reaction between aluminum in the molten steel
and silica based mold flux in the continuous-casting process would tend to cause a
series of problems and influence the quality of slabs. To solve the above problems
caused by the slag-steel reaction, nonreactive lime-alumina-based mold flux system
has been proposed. In this article, the effect of Li2O and Na2O on the
crystallization behavior of the lime-alumina-silica-based mold flux has been
studied by using the single hot thermocouple technology (SHTT) and double hot
thermocouple technology (DHTT). The results indicated that Li2O and Na2O in the
above mold flux system play different roles as they behaved in traditional lime-
silica based mold flux, which would tend to inhibit general mold flux
crystallization by lowering the initial crystallization temperature and increasing
incubation time, especially in the high-temperature region. However, when their
content exceeds a critical value, the crystallization process of mold fluxes in low
temperature zone would be greatly accelerated by the new phase formation of LiAlO2
and Na (x) Al (y) Si (z) O-4 crystals, respectively. The crystalline phases
precipitated in all samples during the experiments are discussed in the article.
C1 [Lu, Boxun; Chen, Kun; Wang, Wanlin; Jiang, Binbin] Cent S Univ, Sch Met &
Environm, Changsha 410083, Peoples R China.
RP Wang, WL (corresponding author), Cent S Univ, Sch Met & Environm, Changsha
EM wanlin.wang@gmail.com
FU NSFC [51274244, 51322405]; Fundamental Research Funds for the Central
Universities [2011JQ010]
FX The financial support from NSFC (51274244 and 51322405) and the
Fundamental Research Funds for the Central Universities (2011JQ010) is
greatly acknowledged.
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NR 22
TC 86
Z9 99
U1 0
U2 44
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2014
VL 45
IS 4
BP 1496
EP 1509
DI 10.1007/s11663-014-0063-6
PG 14
Engineering
GA AN1SV
UT WOS:000340364800035
DA 2023-12-05
ER
PT J
AU SCHILLING, PJ
BUTLER, LG
ROY, A
EATON, HC
AF SCHILLING, PJ
BUTLER, LG
ROY, A
EATON, HC
TI SI-29 AND AL-27 MAS-NMR OF NAOH-ACTIVATED BLAST-FURNACE SLAG
LA English
DT Article
ID NUCLEAR MAGNETIC-RESONANCE; CALCIUM SILICATE HYDRATE; GLASSES; AL;
SPECTROSCOPY; TOBERMORITES; COORDINATION; ORDER
AB Si-29 and Al-27 MAS.NMR were performed on NaOH-activated blast-furnace slag to
better characterize the amorphous and poorly crystalline phases which occur in this
system. The unreacted glass has a mainly dimeric silicate structure represented by
a broad Si-29 peak (FWHM = 15 ppm) centered at - 74.5 ppm [Q(1)], with aluminum
present exclusively in tetrahedral coordination. Upon reaction with 5M NaOH (w/s =
0.4), three new Si-29 peaks with widths of ca. 2 ppm are formed at -78.5 [Q(1)], -
81.4 [Q(2)(1Al)], and -84.3 [Q(2)]. Relative peak areas indicate a mostly dimeric
silicate structure for the tobermorite-like C-S-H layers, with roughly a third of
the bridging sites occupied by aluminum, and less than 10% by silicon. In addition
to the tetrahedrally coordinated aluminum substituted in the C-S-H structure, Al-27
MAS-NMR reveals the presence of aluminum in octahedral sites, which is attributed
to the aluminate phase (C,M)(4)AH(13). Si-29 results indicate rapid initial
consumption of the glass, with roughly a third of the glass reacting within the
first day and another third consumed over the following 27 days.
C1 LOUISIANA STATE UNIV,DEPT CHEM,BATON ROUGE,LA 70803.
LOUISIANA STATE UNIV,DEPT CIVIL ENGN,BATON ROUGE,LA 70803.
C3 Louisiana State University System; Louisiana State University; Louisiana
State University System; Louisiana State University
RP SCHILLING, PJ (corresponding author), LOUISIANA STATE UNIV,CTR ADV MICROSTRUCT &
DEVICES,DEPT MECH ENGN,BATON ROUGE,LA 70803, USA.
RI Butler, Les/D-1047-2013; Butler, Leslie G/D-1636-2016
OI Butler, Les/0000-0003-1547-608X; Butler, Leslie G/0000-0003-1547-608X
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NR 26
TC 86
Z9 87
U1 0
U2 10
PU AMER CERAMIC SOC
PI WESTERVILLE
PA 735 CERAMIC PLACE, PO BOX 6136, WESTERVILLE, OH 43081-6136
SN 0002-7820
J9 J AM CERAM SOC
PD SEP
PY 1994
VL 77
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BP 2363
EP 2368
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PG 6
GA PH199
UT WOS:A1994PH19900017
DA 2023-12-05
ER
PT J
AU Zheng, K
Zhang, ZT
Yang, FH
Sridhar, S
AF Zheng, Kai
Zhang, Zuotai
Yang, Feihua
Sridhar, Seetharaman
TI Molecular Dynamics Study of the Structural Properties of Calcium
Aluminosilicate Slags with Varying
Al2O3/SiO2 Ratios
LA English
DT Article
DE molecular dynamics; calcium aluminosilicate slag; slag structure;
Al2O3/SiO2 ratio
ID NON-BRIDGING OXYGEN; GLASSES; NMR; AL; MELTS; COORDINATION; ALUMINATE;
MAS; CA; SPECIATION
AB Molecular dynamics simulation was explored to investigate the change of
structure of calcium aluminosilicate slags with varying Al2O3/SiO2 ratios at a
fixed CaO content. In practice the results of the study are relevant to the
significant changes in slag structure caused by the changes in chemical composition
during continuous casting of steels containing high amounts of dissolved aluminum.
It was found that Q(4) tetrahedral species (tetrahedron with four bridging oxygens)
increase while NBOs (non-bridging oxygen) decreases with increasing Al2O3/SiO2 mole
ratio, suggesting that a more polymerized network was formed. The concentration of
oxygen tricluster increased dramatically up to 24% with increasing Al2O3/SiO2 mole
ratio, and the coordination number for Al (CNAl-O) was also observed to increase
from 4.02 for sample CAS1 to 4.11 for sample CAS11, suggesting that high
coordination number of Al presents in the slag melt with the substitution of [AlO4]
for [SiO4]. NBOs prefer to be coordinated with Si and Al tends to be localized in
more polymerized environment as network intermediate phases. The degree of Al
avoidance was calculated and the Al avoidance principle is applicable in the SiO2
rich regions.
C1 [Zheng, Kai; Zhang, Zuotai] Peking Univ, Dept Energy & Resources Engn, Coll
[Yang, Feihua] Beijing Bldg Mat Acad Sci Res, Beijing 100041, Peoples R China.
[Sridhar, Seetharaman] Carnegie Mellon Univ, Dept Mat Sci & Engn, Pittsburgh, PA
15213 USA.
C3 Peking University; Carnegie Mellon University
RP Zheng, K (corresponding author), Peking Univ, Dept Energy & Resources Engn, Coll
EM zhengkai890406@163.com; zuotaizhang@coe.pku.edu.cn;
chyangfeihua@126.com; sridhars@andrew.cmu.edu
RI Zhang, Zuotai/B-1030-2012
OI Zhang, Zuotai/0000-0002-3580-6018
National Key Technology Research and Development Program [2010BAE00316]
FX The authors wish to express their gratitude to Prof. Yongquan Wu for his
help and suggestions during the simulation process. Financial supports
from National Natural Science Foundation of China (50902003,51172003)
and National Key Technology Research and Development Program
(2010BAE00316) are gratefully acknowledged.
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NR 35
TC 85
Z9 94
U1 3
U2 44
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2012
VL 52
IS 3
BP 342
EP 349
PG 8
GA 913VR
UT WOS:000301906000002
OA gold
DA 2023-12-05
ER
PT J
AU Park, HS
Kim, H
Sohn, I
AF Park, Hyun Shik
Kim, Hyuk
Sohn, Il
TI Influence of CaF2 and Li2O on the Viscous Behavior
of Calcium Silicate Melts Containing 12 wt pct Na2O
LA English
DT Article
ID GLASSES; CAO-CAF2-SIO2; SYSTEM; SLAGS; VISCOSITIES; FLUORINE; CAO-SIO2;
MGO
AB Understanding the viscous behavior of silica-based molten fluxes is essential in
maintaining the reliability of steel casting operations and in preventing
breakouts. In particular, high concentrations of aluminum in recently developed
transformation induced plasticity (TRIP) and twinning induced plasticity (TWIP)
steels tend to promote reduction of silica in the mold fluxes that result in the
formation of alumina, which in turn increases the viscosity. To counteract this
effect, significant amounts of fluidizers such as CaF2 and Li2O are required to
ensure that mold fluxes have acceptable lubrication and heat transfer
characteristics. The viscous behavior of the slag system based on CaO-SiO2-12 wt
pct Na2O with various concentrations of CaF2 and Li2O has been studied using the
rotating spindle method to understand the effects on the viscosity with these
additives. CaF2 additions up to 8 wt pct were effective in decreasing the viscosity
by breaking the network structure of molten fluxes, but CaF2 concentrations above
this level had a negligible effect on viscosity. Li2O additions up to 2 wt pct were
also effective in decreasing the viscosity, but the effect was comparatively
negligible above 2 wt pct. Using Fourier transform infrared (FTIR) analysis of as-
quenched slag samples, it was concluded that the viscosity was controlled more
effectively by changing the larger complex silicate structures of rings and chains
than by changing the amounts of simpler dimers and monomers. DOI: 10.1007/s11663-
011-9474-9 (C) The Minerals, Metals & Materials Society and ASM International 2011
C1 [Park, Hyun Shik] Yonsei Univ, Res Inst Iron & Steel Technol, Seoul 120749,
South Korea.
[Kim, Hyuk; Sohn, Il] Yonsei Univ, Dept Mat Sci & Engn, Seoul 120749, South
Korea.
C3 Yonsei University; Yonsei University
RP Park, HS (corresponding author), Yonsei Univ, Res Inst Iron & Steel Technol,
Seoul 120749, South Korea.
RI SOHN, IL/I-5815-2012
FU Division of the Humantronics Information Materials; Yonsei University;
National Research Foundation of Korea [2010-0007442] Funding Source:
FX This study was supported partially by the Brain Korea 21 (BK21) Project
at the Division of the Humantronics Information Materials and the Yonsei
University Research Fund of 2009.
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NR 24
TC 85
Z9 88
U1 2
U2 16
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD APR
PY 2011
VL 42
IS 2
BP 324
EP 330
DI 10.1007/s11663-011-9474-9
PG 7
Engineering
GA 765FF
UT WOS:000290688100009
DA 2023-12-05
ER
PT J
AU Machner, A
Zajac, M
Ben Haha, M
Kjellsen, KO
Geiker, MR
De Weerdt, K
AF Machner, Alisa
Zajac, Maciej
Ben Haha, Mohsen
Kjellsen, Knut O.
Geiker, Mette R.
De Weerdt, Klaartje
TI Limitations of the hydrotalcite formation in Portland composite cement
pastes containing dolomite and metakaolin
LA English
DT Article
DE Thermal analysis (B); X-ray diffraction (B); Ca(OH)(2) (D); Blended
cement (D); Dedolomitization reaction
ID ALKALI-ACTIVATED SLAG; C-S-H; HYDRATION; LIMESTONE; KINETICS;
SUBSTITUTION; CARBONATE
AB This study focuses on the reaction of dolomite powder in combination with
metakaolin in Portland composite cement pastes. We studied paste samples cured at
20 degrees C, 38 degrees C, and 60 degrees C for up to 1 year. In these systems,
the only magnesium-containing hydration phase of dolomite observed was
hydrotalcite. Dolomite reacted notably already after 90 days when cured at 60
degrees C, whereas at lower curing temperatures the reaction was limited. The
increased availability of aluminium due to the addition of metakaolin did not
contribute to the formation of hydrotalcite. The refined pore space due to the
metakaolin addition did not inhibit the hydrotalcite formation. However, the almost
total absence of portlandite due to the pozzolanic reaction of the metakaolin
inhibited the dolomite reaction, even in pastes with high porosity. Portlandite
seems to be the driving force for the reaction as its absence is inhibiting the
reaction to take place.
C1 [Machner, Alisa; Kjellsen, Knut O.] Norcem AS, R&D Dept, Setreveien 2,POB 38, N-
3991 Brevik, Norway.
[Machner, Alisa; Geiker, Mette R.; De Weerdt, Klaartje] NTNU, Dept Struct Engn,
Richard Birkelandsvei 1A, N-7491 Trondheim, Norway.
[Zajac, Maciej; Ben Haha, Mohsen] Heidelberg Technol Ctr GmbH, Oberklammweg 2-4,
D-69181 Leimen, Germany.
C3 Norwegian University of Science & Technology (NTNU)
RP Machner, A (corresponding author), NTNU, Dept Struct Engn, Richard Birkelandsvei
1A, N-7491 Trondheim, Norway.
EM alisa.machner@ntnu.no
RI Ben Haha, Mohsen/AAC-4859-2020; Zajac, Maciej/AAP-8225-2020; Machner,
Alisa/ABG-8065-2020; Geiker, Mette/AAY-7734-2021
OI Ben Haha, Mohsen/0000-0001-7570-326X; Machner,
Alisa/0000-0002-6334-5116; De Weerdt, Klaartje/0000-0001-8705-8413
FU Norwegian Research Council; Heidelberg Technology Center [241637]
FX The authors would like to thank the Norwegian Research Council and the
Heidelberg Technology Center (industrial PhD programme, project number:
241637) for their financial support.
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[Anonymous], P 13 INT C CHEM CEM
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10.1016/j.cemconres.2014.07.017
NR 42
TC 84
Z9 85
U1 2
U2 65
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD MAR
PY 2018
VL 105
BP 1
EP 17
DI 10.1016/j.cemconres.2017.11.007
PG 17
GA FW0DS
UT WOS:000424962200001
DA 2023-12-05
ER
PT J
AU Liao, JL
Zhang, YY
Sridhar, S
Wang, XD
Zhang, ZT
AF Liao, Junlin
Zhang, Yingyi
Wang, Xidong
Zhang, Zuotai
TI Effect of Al2O3/SiO2 Ratio on the
Viscosity and Structure of Slags
LA English
DT Article
DE viscosity; activity; structure; TRIP steel
ID SILICATE MELTS; AMPHOTERIC BEHAVIOR; GLASSES; AL; NA2O-AL2O3-SIO2;
TRANSFORMATION; PHOSPHORUS; SPECTRA; MGO
AB The present paper investigates how the mass ratio between Al2O3 and SiO2
(m(Al2O3)/m(SiO2)) in slag compositions influences the structure, viscosity and
crystallization of the slag melts. The objective is to study the variations in
viscosity and structure of slags with increasing m(Al2O3)/m(SiO2) ratio. In
practice the results of the study are relevant to the significant changes in slag
property caused by the changes in chemical composition during continuous casting of
steels containing high amounts of dissolved aluminum.
The viscosity was found to decrease slightly with increasing m(Al2O3)/m(SiO2)
ratio up to 0.56. The degree of polymerization for [SiO4]-tetrahedra was found to
decrease with increasing m(Al2O3)/m(SiO2) ratio based on the Fourier
Transformation-Infrared Spectra (FT-IR) and Raman spectra, which could explain the
observed decrease in viscosity. Atm(Al2O3)/m(SiO2) ratios above 0.56, the viscosity
was found to abruptly increase which could be caused by the presence of spinel
crystals. The activity coefficient was computed and it was found that the activity
coefficient of alumina presents negative deviation when m(Al2O3)/m(SiO2) ratio is
less than 0.35, while it shows a positive deviation when m(Al2O3)/m(SiO2) ratio
exceeds 0.35. This phenomenon may be related to the change of the primary phase
region correlating to the phase diagram to the slag composition.
C1 [Liao, Junlin; Zhang, Yingyi; Wang, Xidong; Zhang, Zuotai] Peking Univ, Coll
Engn, Dept Energy & Resources Engn, Beijing 100871, Peoples R China.
[Sridhar, Seetharaman] Carnegie Mellon Univ, Dept Mat Sci & Engn, Pittsburgh, PA
15213 USA.
C3 Peking University; Carnegie Mellon University
RP Liao, JL (corresponding author), Peking Univ, Coll Engn, Dept Energy & Resources
EM junlin.liao@pku.edu.cn; zhyingyi@gmail.com; ssridhar@andrew.cmu.edu;
xidong@pku.edu.cn; zuotaizhang@coe.pku.edu.cn
RI Zhang, Yingyi/AAG-4336-2020; wang, xidong/B-7788-2013; Zhang,
Zuotai/B-1030-2012
OI Zhang, Yingyi/0000-0002-3294-6525; Zhang, Zuotai/0000-0002-3580-6018
National Key Technology Research and Development Program in 12th
Five-year Plan of China [2010BAE00316, 2011BAB02B05]
FX The authors wish to express their gratitude to Dr. Q. F. Shu for the
thermodynamic calculation. Special thanks are also extended to Dr. L. L.
Liu and Mr. S. L. Tang for their help during the viscosity measurements.
Financial supports from National Natural Science Foundation of China
(50902003, 51172003) and National Key Technology Research and
Development Program in 12th Five-year Plan of China (2010BAE00316,
2011BAB02B05) are gratefully acknowledged.
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NR 43
TC 84
Z9 90
U1 0
U2 47
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2012
VL 52
IS 5
BP 753
EP 758
PG 6
GA 948QD
UT WOS:000304516800001
DA 2023-12-05
ER
PT J
AU Ohta, H
Suito, H
AF Ohta, H
Suito, H
TI Deoxidation equilibria of calcium and magnesium in liquid iron
LA English
DT Article
ID ALUMINUM OXYGEN EQUILIBRIUM; MOLTEN IRON; SLAGS; SOLUBILITY;
THERMODYNAMICS; NITROGEN; MELTS; FE
AB Calcium-oxygen and magnesium-oxygen equilibria in liquid iron saturated with
CaO-SiO(2)-Al(2)O(3)-MgO slags were studied at 1873 K using CaO, Al(2)O(3), and MgO
crucibles. The applicability of the first-order and second-order interaction
coefficients between Ca and O and between Mg and O was studied by comparing the Ca-
O and Mg-O equilibria observed in the present and previous experiments with the
calculated ones from the respective interaction coefficients. As a result, the
interaction coefficients obtained in the present work by using a new method were
found to explain the measured solubilities of CaO and MgO. The phase stability
region in Fe-Al-M (M = Ca, Mg)-O system was described at 1873 K.
C1 Tohoku Univ, Inst Adv Mat Proc, Sendai, Miyagi 98077, Japan.
RP Ohta, H (corresponding author), Tohoku Univ, Inst Adv Mat Proc, Sendai, Miyagi
98077, Japan.
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NR 30
TC 84
Z9 93
U1 1
U2 15
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD DEC
PY 1997
VL 28
IS 6
BP 1131
EP 1139
DI 10.1007/s11663-997-0069-4
PG 9
Engineering
GA YT939
UT WOS:000071661700020
DA 2023-12-05
ER
PT J
AU Li, ZM
Nedeljkovic, M
Chen, BY
Ye, G
AF Li, Zhenming
Nedeljkovic, Marija
Chen, Boyu
Ye, Guang
TI Mitigating the autogenous shrinkage of alkali-activated slag by
metakaolin
LA English
DT Article
DE Slag; Shrinkage; Mitigation; Metakaolin; Mechanical properties
ID BLAST-FURNACE SLAG; C-S-H; CALCIUM-SILICATE-HYDRATE; FLY-ASH; DRYING
SHRINKAGE; REACTION-KINETICS; MECHANICAL-PROPERTIES; REDUCING
ADMIXTURES; AMBIENT-TEMPERATURE; CEMENT
AB This study investigates the effectiveness of metakaolin (MK) in mitigating the
autogenous shrinkage of alkali activated slag (AAS). It is found that the
autogenous shrinkage of AAS paste can be reduced by 40% and 50% when replacing 10%
and 20% slag with MK, respectively. By providing additional Si and Al, and
decreasing the pH of the pore solution, the incorporation of MK retards the
formation of aluminium-modified calcium silicate hydrate (CASH) gels, the main
reaction products in the studied pastes. The chemical shrinkage and pore refinement
are consequently mitigated, resulting in a substantial reduction in the pore
pressure. Meanwhile, the elastic modulus of AAS paste is only slightly influenced
after MK addition. As a result, the autogenous shrinkage of AAS is significantly
mitigated by incorporating MK. In addition, the introduction of MK would extend the
setting time, slightly decrease the compressive strength, but greatly increase the
flexural strength of AAS.
C1 [Li, Zhenming; Nedeljkovic, Marija; Chen, Boyu; Ye, Guang] Delft Univ Technol,
Fac Civil Engn & Geosci, Dept Mat & Environm, Microlab, Delft, Netherlands.
[Ye, Guang] Univ Ghent, Dept Struct Engn, Magnel Lab Concrete Res, Ghent,
Belgium.
C3 Delft University of Technology; Ghent University
RP Li, ZM (corresponding author), Delft Univ Technol, Fac Civil Engn & Geosci, Dept
Mat & Environm, Microlab, Delft, Netherlands.
EM z.li-2@tudelft.nl
RI ye, guang/F-1204-2014; li, zhenming/ABA-8552-2021
OI ye, guang/0000-0001-8566-3863; li, zhenming/0000-0002-6752-6264
FU China Scholarship Council (CSC); Netherlands Organisation for Scientific
Research (NWO)
FX This work is supported in part by the scholarship from China Scholarship
Council (CSC) and the grant from Netherlands Organisation for Scientific
Research (NWO).
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NR 102
TC 83
Z9 86
U1 10
U2 91
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD AUG
PY 2019
VL 122
BP 30
EP 41
DI 10.1016/j.cemconres.2019.04.016
PG 12
GA IF8ZB
UT WOS:000473380700003
OA Green Published
DA 2023-12-05
ER
PT J
AU Gutierrez, A
Miró, L
Gil, A
Rodríguez-Aseguinolaza, J
Barreneche, C
Calvet, N
Py, X
Fernandez, AI
Grágeda, M
Ushak, S
Cabeza, LF
AF Gutierrez, Andrea
Miro, Laia
Gil, Antoni
Rodriguez-Aseguinolaza, Javier
Barreneche, Camila
Calvet, Nicolas
Py, Xavier
Fernandez, A. Ines
Grageda, Mario
Ushak, Svetlana
Cabeza, Luisa F.
TI Advances in the valorization of waste and by-product materials as
thermal energy storage (TES) materials
SO RENEWABLE & SUSTAINABLE ENERGY REVIEWS
LA English
DT Review
DE Thermal energy storage (TES); Industrial waste; Slags; Aluminium dross;
Inorganic TES
ID PHASE-CHANGE MATERIALS; HIGH-TEMPERATURE; HEAT-STORAGE; MOLTEN-SALTS;
STEEL SLAG; SELECTION; CERAMICS; CONCRETE; SYSTEM; COMPATIBILITY
AB Today, one of the biggest challenges our society must face is the satisfactory
supply, dispatchability and management of the energy. Thermal Energy Storage (TES)
has been identified as a breakthrough concept in industrial heat recovery
applications and development of renewable technologies such as concentrated solar
power (CSP) plants or compressed air energy storage (CAES). A wide variety of
potential heat storage materials has been identified depending on the implemented
TES method: sensible, latent or thermochemical. Although no ideal storage material
has been identified, several materials have shown a high potential depending on the
mentioned considerations. Despite the amount of studied potential heat storage
materials, the determination of new alternatives for next generation technologies
is still open. One of the main drawbacks in the development of storage materials is
their cost. In this regard, this paper presents the review of waste materials and
by-products candidates which use contributes in lowering the total cost of the
storage system and the valorization of waste industrial materials have strong
environmental and societal benefits such as reducing the landfilled waste amounts,
reducing the greenhouse emissions and others. This article reviews different
industrial waste materials that have been considered as potential TES materials and
have been characterized as such. Asbestos containing wastes, fly ashes, by-products
from the salt industry and from the metal industry, wastes from recycling steel
process and from copper refining process and dross from the aluminum industry, and
municipal wastes (glass and nylon) have been considered. Themophysical properties,
characterization and experiences using these candidates are discussed and compared.
This review shows that the revalorization of wastes or by-products as TES materials
is possible, and that more studies are needed to achieve industrial deployment of
the idea. (C) 2015 Elsevier Ltd. All rights reserved.
C1 [Gutierrez, Andrea; Grageda, Mario; Ushak, Svetlana] Univ Antofagasta, Ctr Adv
Study Lithium & Ind Minerals CELiMIN, Dept Chem Engn & Mineral Proc, Av Univ
Antofagasta,Campus Coloso, Antofagasta 02800, Chile.
[Miro, Laia; Barreneche, Camila; Cabeza, Luisa F.] Univ Lleida, GREA Innovacio
Concurrent, Edifici CREA,Pere Cabrera S-N, Lleida 25001, Spain.
[Gil, Antoni; Rodriguez-Aseguinolaza, Javier] CIC Energigune, Parque Tecnol
Alava,C Albert Einstein 48,Edif CIC, Minano 01510, Alava, Spain.
[Barreneche, Camila; Fernandez, A. Ines] Univ Barcelona, Dept Mat Sci & Met
Engn, Marti & Franques 1,08028, E-08028 Barcelona, Spain.
[Calvet, Nicolas] Masdar Inst Sci & Technol, Dept Mech & Mat Engn, Inst Ctr
Energy iEnergy, POB 54224, Abu Dhabi, U Arab Emirates.
[Py, Xavier] Univ Perpignan, PROMES CNRS UPR8521, Via Domitia, F-66100
Perpignan, France.
[Grageda, Mario; Ushak, Svetlana] Solar Energy Res Ctr SERC Chile, Av Tupper
2007,Piso 4, Santiago, Chile.
[Gil, Antoni] MIT, Dept Mech Engn, 77 Massachusetts Ave, Cambridge, MA 02139
USA.
C3 Universidad de Antofagasta; Universitat de Lleida; CIC Energigune;
University of Barcelona; Khalifa University of Science & Technology;
Universite Perpignan Via Domitia; Centre National de la Recherche
Scientifique (CNRS); CNRS - Institute for Engineering & Systems Sciences
(INSIS); Massachusetts Institute of Technology (MIT)
RP Ushak, S (corresponding author), Univ Antofagasta, Ctr Adv Study Lithium & Ind
Minerals CELiMIN, Dept Chem Engn & Mineral Proc, Av Univ Antofagasta,Campus Coloso,
Antofagasta 02800, Chile.
EM svetlana.ushak@uantof.cl
RI Aseguinolaza, Javier Rodríguez/U-3191-2019; Ushak,
Svetlana/AAA-2348-2019; Miró, Laia/G-5102-2015; FERNANDEZ, ANA
INES/G-2719-2010; Cabeza, Luisa F./B-4587-2013; Gil,
Antoni/HLW-9218-2023; Barreneche, Camila/AAG-8337-2020; Barreneche,
Camila/L-3100-2014
OI Aseguinolaza, Javier Rodríguez/0000-0001-8676-5108; Ushak,
Svetlana/0000-0002-1933-9624; Miró, Laia/0000-0003-4890-6357; FERNANDEZ,
ANA INES/0000-0001-9212-9714; Cabeza, Luisa F./0000-0001-5086-872X; Gil,
Antoni/0000-0002-4900-1317; Barreneche, Camila/0000-0003-3636-3180;
Calvet, Nicolas/0000-0003-4302-913X; Gutierrez,
Andrea/0000-0002-6313-8264
FU Spanish government [ENE2011-28269-C03-02, ENE2011-22722, ULLE10-4E-1305,
BES-2012-051861]; European Union [PIRSES-GA-2013-610692]; Department of
Industry, Innovation, Commerce and Tourism of the Basque Country
government through the ETORTEK CIC Energigune [IE 13-375]; French
government through the ANR SESCO project; French government through the
ANR SACRE project; CNRS; University of Perpignan Via Domitia;
EUROPLASMA/INERTAM Company; FONDECYT [1120422]; CONICYT/FONDAP
[15110019]; Education Ministry of Chile [PMI ANT 1201, ANT 1106]
FX The work is partially funded by the Spanish government
(ENE2011-28269-C03-02, ENE2011-22722 and ULLE10-4E-1305). The authors
would like to thank the Catalan Government for the quality accreditation
given to their research group GREA (2014 SGR 123) and research group
DIOPMA (2014 SGR 1543). The research leading to these results has
received funding from the European Union's Seventh Framework Programme
(FP7/2007-2013) under Grant agreement no. PIRSES-GA-2013-610692
(INNOSTORAGE). Laia Miro would like to thank the Spanish Government for
her research fellowship (BES-2012-051861). The work at CIC Energigune
was supported by the Department of Industry, Innovation, Commerce and
Tourism of the Basque Country government through the ETORTEK CIC
Energigune-2013 research program no. IE 13-375. Research at Masdar
Institute is supported by the Government of Abu Dhabi to help fulfil the
vision of the late President Sheikh Zayed bin Sultan Al Nayhan for
sustainable development and empowerment of the UAE and humankind under
no. SG2014-000002. Researchers of PROMES address all their gratitude to
the French government for the funding of their work through the ANR
SESCO and SACRE projects within the ANR SEED program. They also
acknowledge the support of the CNRS, the University of Perpignan Via
Domitia and the EUROPLASMA/INERTAM Company. The work at the University
of Antofagasta was supported by FONDECYT (Grant No. 1120422),
CONICYT/FONDAP No. 15110019, and the Education Ministry of Chile Grant
PMI ANT 1201. Andrea Gutierrez would like to acknowledge to the
Education Ministry of Chile her doctorate scholarship ANT 1106 and
CONICYT/PAI No. 7813110010.
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NR 99
TC 83
Z9 86
U1 9
U2 180
PI OXFORD
SN 1364-0321
J9 RENEW SUST ENERG REV
JI Renew. Sust. Energ. Rev.
PD JUN
PY 2016
VL 59
BP 763
EP 783
DI 10.1016/j.rser.2015.12.071
PG 21
WC Green & Sustainable Science & Technology; Energy & Fuels
SC Science & Technology - Other Topics; Energy & Fuels
GA DG3CZ
UT WOS:000371948400054
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Saikia, N
Mertens, G
Van Balen, K
Elsen, J
Van Gerven, T
Vandecasteele, C
AF Saikia, Nabajyoti
Mertens, Gilles
Van Balen, Koenraad
Elsen, Jan
Van Gerven, Tom
Vandecasteele, Carlo
TI Pre-treatment of municipal solid waste incineration (MSWI) bottom ash
for utilisation in cement mortar
LA English
DT Article
DE MSWI ash; Aluminium; Sulphate; Treatment; Fine aggregate; Leaching
ID FLY-ASH; BLENDED CEMENT; RESIDUES; SLAG
AB The removal of elemental aluminium, sulphate and harmful organics from two types
of MSWI ash samples, the sand sized (0.1-2 mm) fraction of MSWI bottom ash from a
grate furnace (SF), and boiler and fly ash from a fluidized bed incinerator (BFA),
were done to use as fine aggregates in preparation of cement mortar. Results
indicate that the chemical treatment by 0.25 M Na2CO3 solution can dissolve the Al
and the sulphate bearing minerals from the BFA and therefore enhance its quality to
use as a fine aggregate in cement mortar preparation. On the other hand, heat
treatment at about 675 degrees C before Na2CO3 treatment is necessary to improve
the quality of SF for using as a fine aggregate. The compressive strengths of
mortars improve significantly due to the partial replacement of sand by heat and
Na2CO3 treated ash samples. The proposed treatment methods slightly change the
toxic element leaching behaviours of the ash samples. The concentrations of toxic
elements in the leachates generated from the treated ash samples as well as the
leachates generated from the mortars containing these ash samples are well within
the regulatory limits. (C) 2015 Elsevier Ltd. All rights reserved.
C1 [Saikia, Nabajyoti] Kaziranga Univ, Sch Basic Sci, Jorhat 785006, Assam, India.
[Saikia, Nabajyoti; Van Gerven, Tom; Vandecasteele, Carlo] Katholieke Univ
Leuven, Dept Chem Engn, B-3001 Louvain, Belgium.
[Mertens, Gilles; Elsen, Jan] Katholieke Univ Leuven, Dept Geol, Appl Geol &
Mineral Res Grp, B-3001 Heverlee, Belgium.
[Van Balen, Koenraad] Katholieke Univ Leuven, Dept Civil Engn, B-3001 Heverlee,
Belgium.
C3 Kaziranga University; KU Leuven; KU Leuven; KU Leuven
RP Saikia, N (corresponding author), Kaziranga Univ, Sch Basic Sci, Jorhat 785006,
Assam, India.
EM saikianj@gmail.com
RI Van Gerven, Tom/B-5806-2015; elsen, jan/AAB-9873-2021; Saikia,
Nabajyoti/N-7769-2015; Van Balen, Koenraad/Q-6350-2019; Saikia,
Nabajyoti/AHD-4911-2022; Van Balen, Koenraad EP/C-2063-2012; elsen,
jan/AAE-2352-2021
OI Van Gerven, Tom/0000-0003-2051-5696; Van Balen,
Koenraad/0000-0001-6595-2051; Van Balen, Koenraad
EP/0000-0001-6595-2051; elsen, jan/0000-0002-4370-3852; Saikia,
Nabajyoti/0000-0003-3585-4092
FU K.U. Leuven
FX The authors are grateful to G. Cornelis, S. Ores, G. Hechtermans and F.
Goethals for their helps. NJS is also grateful to Prof. L.J.J. Catalan,
Lakehead University, Thunder Bay, Canada for his help during analyses of
some samples and to the Research Fund, K.U. Leuven for the grant of a
fellowship. Authors are also grateful to N.V. Indaver for providing the
wastes.
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NR 37
TC 83
Z9 88
U1 6
U2 98
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 15
PY 2015
VL 96
BP 76
EP 85
DI 10.1016/j.conbuildmat.2015.07.185
PG 10
GA CR5RX
UT WOS:000361402700009
DA 2023-12-05
ER
PT J
AU Kubba, Z
Huseien, GF
Sam, ARM
Shah, KW
Asaad, MA
Ismail, M
Tahir, MM
Mirza, J
AF Kubba, Ziyad
Huseien, Ghasan Fahim
Sam, Abdul Rahman Mohd
Shah, Kwok Wei
Asaad, Mohammad Ali
Ismail, Mohammad
Tahir, Mahmood Md
Mirza, Jahangir
TI Impact of curing temperatures and alkaline activators on compressive
strength and porosity of ternary blended geopolymer mortars
LA English
DT Article
DE Geopolymer mortars; Alkaline solution; Compressive strength; Porosity
ID OIL FUEL ASH; BLAST-FURNACE SLAG; CALCIUM SILICATE HYDRATE; FLY-ASH;
REPAIR MATERIAL; CONCRETE; CEMENT; MICROSTRUCTURE; PERFORMANCE;
DURABILITY
AB Impact of changing temperatures of curing (27, 60 and 90 degrees C) and types of
alkaline activator solution on the properties of geopolymer mortars (GPMs) prepared
by combining agricultural and industrial wastes including granulated-blast-furnace-
slag (GBFS), fly-ash (FA), and palm-oil-fuel-ash (POFA) was examined. Sodium
Hydroxide (NH), Sodium Silicate (NS) and NHNS alkaline solutions were used as
alkali activators. Proposed GPMs were synthesized using NH solution of molarity 8
M, ratios of alkaline solution to binder were 0.30, NS to NH was 3.0 and binder to
fine aggregate (sand) was 1.5. The mechanical properties of the studied GPMs and
the products of reaction were greatly sensitive to the variation of mix
compositions, alkaline activators type, and temperatures of curing. Furthermore,
the formation of crystalline calcium silicate hydrate (C-S-H), calcium aluminium
silicate hydrate (C-A-S-H) together with additional amorphous gel led to the
compressive strength enhancement of the GPMs as the content of FA was increased and
activated with NS solution. A linear correlation was established between
compressive strength, ultrasonic pulse velocity and porosity of the proposed GPMs.
(C) 2018 The Author. Published by Elsevier Ltd.
C1 [Kubba, Ziyad] Muthanna Univ, Coll Engn, Dept Civil Engn, Samawa 66001, Iraq.
[Huseien, Ghasan Fahim; Sam, Abdul Rahman Mohd; Tahir, Mahmood Md] Univ Teknol
Malaysia, Ctr Inst Smart Infrastruct & Innovat Construct, UTM Construct Res Ctr,
Sch Civil Engn,Fac Engn, Johor Baharu 81310, Johor, Malaysia.
[Shah, Kwok Wei] Natl Univ Singapore, Sch Design & Environm, Dept Bldg,
Singapore 117566, Singapore.
[Asaad, Mohammad Ali; Ismail, Mohammad] Univ Teknol Malaysia, Fac Engn, Sch
Civil Engn, Johor Baharu 81310, Johor, Malaysia.
[Mirza, Jahangir] Res Inst Hydroquebec, Dept Mat Sci, 1800 Mte Ste Julie,
C3 Al-Muthanna University; Universiti Teknologi Malaysia; National
University of Singapore; Universiti Teknologi Malaysia
RP Huseien, GF (corresponding author), Univ Teknol Malaysia, Ctr Inst Smart
Infrastruct & Innovat Construct, UTM Construct Res Ctr, Sch Civil Engn,Fac Engn,
Johor Baharu 81310, Johor, Malaysia.
EM eng.gassan@yahoo.com
RI Kubba, Ziyad/D-9319-2019; Huseien, Ghasan Fahim/AEC-3508-2022; Mirza,
Jahangir/HOF-8557-2023
OI Kubba, Ziyad/0000-0002-3393-4999; Huseien, Ghasan
Fahim/0000-0002-2963-0335; Mirza, Jahangir/0000-0002-3783-8048; Shah,
Kwok Wei/0000-0002-5649-4105
FU UTM COE research grant [Q.J130000.2409.04G00]; UTM FRGS grant [R.
J130000.7822.4F722]; Universiti Teknologi Malaysia; Ministry of Higher
Education
FX This research was supported and funded by the UTM COE research grant
Q.J130000.2409.04G00 and FRGS grant R. J130000.7822.4F722. The authors
would like to thanks the grants provider, namely Universiti Teknologi
Malaysia and Ministry of Higher Education, staff from Material and
Structure Laboratory, School of Civil Engineering, Universiti Teknologi
Malaysia, and the EM Malaysia Sdn. Bhd. and EMRO Japan for their support
and cooperation in conducting this research.
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NR 66
TC 81
Z9 81
U1 4
U2 8
PU ELSEVIER
PI AMSTERDAM
SN 2214-5095
PD DEC
PY 2018
VL 9
AR e00205
DI 10.1016/j.cscm.2018.e00205
PG 15
GA VJ4ER
UT WOS:000594668600018
OA gold
DA 2023-12-05
ER
PT J
AU Ewais, EMM
Khalil, NM
Amin, MS
Ahmed, YMZ
Barakat, MA
AF Ewais, E. M. M.
Khalil, N. M.
Amin, M. S.
Ahmed, Y. M. Z.
Barakat, M. A.
TI Utilization of aluminum sludge and aluminum slag (dross) for the
manufacture of calcium aluminate cement
LA English
DT Article
DE Aluminum sludge; Aluminum dross; Calcium aluminates; Refractory cement
ID HYDRATION
AB Four calcium aluminate cement mixes were manufactured from aluminum sludge as a
source of calcium oxide and Al2O3 and aluminum slag (dross) as a source of aluminum
oxide with some additions of pure alumina. The mixes were composed of 35-50%
aluminum sludge, 37.50-48.75% aluminum slag (dross) and 12.50-16.25% aluminum
oxide. The mixed were processed then sintered at different firing temperatures up
to 1500 degrees C or 1550 degrees C. The mineralogical compositions of the fired
mixes investigated using X-ray diffraction indicated that the fired mixes composed
of variable contents of calcium aluminate (CA), calciumdialuminate (CA(2)),
calciumhexaaluminate (CA(6)) in addition to some content of magnesium aluminate
spinel (MA). Sintering parameters (bulk density, apparent porosity and linear
change) and mechanical properties (cold crushing strength) of the fired briquettes
were tested at different firing temperature. Refractoriness of the cement samples
manufactured at the optimum firing temperature was detected. Cementing properties
(water of consistency, setting time and compressive strength as a function of
curing time up to 28 days of hydration) of pasted prepared from the manufactured
cement mixes at the selected optimum firing temperatures (1400 degrees C or 1500
degrees C) were also tested. Cement mixes manufactured from 45 to 50% aluminum
sludge, 37.50-41.25% aluminum slag (dross) with 12.50-13.75% alumina were selected
as the optimum mixes for manufacturing calcium aluminate cement since they satisfy
the requirements of the international standard specifications regarding cementing
and refractory properties as a result of their content of CA (the main hydraulic
phase in calcium aluminate cement) and CA(2)(the less hydraulic but more refractory
phase). Although the recognized high refractoriness of CA(6), its formation affect
badly the cementing properties of the other non-optimum mixes. (c) 2009 Elsevier
Ltd and Techna Group S.r.l. All rights reserved.
C1 [Ewais, E. M. M.; Ahmed, Y. M. Z.] CMRDI, RCML, Cairo 11421, Egypt.
[Khalil, N. M.] Sebha Univ, Fac Sci, Dept Chem, Sebha, Libya.
[Amin, M. S.] Ain Shams Univ, Fac Sci, Dept Chem, Cairo, Egypt.
[Barakat, M. A.] Res & Dev Inst CMRDI, Chem & Electrochem Met Lab, Cairo 11421,
Egypt.
Development Institute (CMRDI); Sebha University; Egyptian Knowledge Bank
(EKB); Ain Shams University; Egyptian Knowledge Bank (EKB); Central
Metallurgical Research & Development Institute (CMRDI)
RP Ewais, EMM (corresponding author), CMRDI, RCML, POB 87 Helwan, Cairo 11421,
Egypt.
EM dr_ewais@hotmail.com
RI Ewais, Emad/AAE-4020-2021; Barakat, Mohamed/H-7499-2012; Khalil, Nagy
Mohamed/A-5992-2013
OI Ewais, Emad/0000-0002-5260-4338; Barakat, Mohamed/0000-0001-6244-8394;
Ahmed, Yassser/0000-0001-6152-4471; Khalil, Nagy/0000-0002-3136-3491
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[No title captured]
NR 33
TC 81
Z9 92
U1 5
U2 57
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD DEC
PY 2009
VL 35
IS 8
BP 3381
EP 3388
DI 10.1016/j.ceramint.2009.06.008
PG 8
GA 514BJ
UT WOS:000271368100057
DA 2023-12-05
ER
PT J
AU Nishi, T
Shinme, K
AF Nishi, T
Shinme, K
TI Formation of spinel inclusions in molten stainless steel under Al
deoxidation with slags
SO TETSU TO HAGANE-JOURNAL OF THE IRON AND STEEL INSTITUTE OF JAPAN
LA Japanese
DT Article
DE deoxidation; inclusion; stainless steel; slag; alumina; spinel
AB Morphology change of inclusions were experimentally investigated under Al
deoxidation of molten stainless steel with CaO-SiO2-Al2O3-MgO slags in order to
clarify the morphology control factor of inclusions. lj kg of molten 18mass%Cr-
8mass%Ni stainless steels were deoxidized by aluminum at 1873K, and the samples
were taken at intervals to observe the inclusions by SEM and EDS. As the results,
MgO contents of alumina type inclusions were gradually increased with time and the
maximum contents were affected by a CaO/SiO2 ratio in slags. The formation of MgO-
Al2O3 spinel type inclusions were also observed in case of high CaOiSiO(2) ratio.
The origin of Mg in inclusions was presumed to be deformation of MgO in slags.
C1 Sumitomo Met Ind Ltd, Corp Res & Dev Labs, Hasakimachi, Ibaraki 3140255, Japan.
Sumitomo Met Ind Ltd, Energy & Environm Res Ctr, Hasakimachi, Ibaraki 3140255,
Japan.
C3 Nippon Steel & Sumitomo Metal Corporation; Nippon Steel & Sumitomo Metal
Corporation
RP Nishi, T (corresponding author), Sumitomo Met Ind Ltd, Corp Res & Dev Labs, 16-1
Oaza Sunayama, Hasakimachi, Ibaraki 3140255, Japan.
CR Han Q., 1990, P 6 INT IR STEEL C, VI, P166
KISHI M, 1994, ISIJ INT, V34, P298
Knacke O., 1991, Thermochemical Properties of Inorganic Substances
Li GQ, 1996, STEEL RES, V67, P528, DOI 10.1002/srin.199605532
SOMMERVILLE ID, 1971, CHEM METALL IRON STE, P23
Stull D., 1971, JANAF Thermochemical Tables, V37
NR 8
TC 81
Z9 88
U1 0
U2 10
PI TOKYO
SN 0021-1575
J9 TETSU TO HAGANE
JI Tetsu To Hagane-J. Iron Steel Inst. Jpn.
PD DEC
PY 1998
VL 84
IS 12
BP 837
EP 843
PG 7
GA 147AM
UT WOS:000077466100001
DA 2023-12-05
ER
PT J
AU Grangeon, S
Claret, F
Roosz, C
Sato, T
Gaboreau, S
Linard, Y
AF Grangeon, Sylvain
Claret, Francis
Roosz, Cedric
Sato, Tsutomu
Gaboreau, Stephane
Linard, Yannick
TI Structure of nanocrystalline calcium silicate hydrates: insights from
X-ray diffraction, synchrotron X-ray absorption and nuclear magnetic
resonance
SO JOURNAL OF APPLIED CRYSTALLOGRAPHY
LA English
DT Article
DE calcium silicate hydrates; C-S-H; X-ray diffraction; Si-29 NMR;
synchrotron X-ray absorption
ID C-S-H; TRANSMISSION ELECTRON-MICROSCOPY; LOCAL COMPOSITIONAL ORDER;
BLAST-FURNACE SLAG; PORTLAND-CEMENT; ALUMINUM INCORPORATION; TRICALCIUM
SILICATE; CRYSTAL-STRUCTURE; CELL DIMENSIONS; SOLID-SOLUTIONS
AB The structure of nanocrystalline calcium silicate hydrates (C-S-H) having Ca/Si
ratios ranging between 0.57 +/- 0.05 and 1.47 +/- 0.04 was studied using an
electron probe micro-analyser, powder X-ray diffraction, 29 Si magic angle spinning
NMR, and Fourier-transform infrared and synchrotron X-ray absorption
spectroscopies. All samples can be described as nanocrystalline and defective
tobermorite. At low Ca/Si ratio, the Si chains are defect free and the Si Q(3) and
Q(2) environments account, respectively, for up to 40.2 +/- 1.5% and 55.6 +/- 3.0%
of the total Si, with part of the Q(3) Si being attributable to remnants of the
synthesis reactant. As the Ca/Si ratio increases up to 0.87 +/- 0.02, the Si Q(3)
environment decreases down to 0 and is preferentially replaced by the Q(2)
environment, which reaches 87.9 +/- 2.0%. At higher ratios, Q(2) decreases down to
32.0 +/- 7.6% for Ca/Si = 1.38 +/- 0.03 and is replaced by the Q(1) environment,
which peaks at 68.1 +/- 3.8%. The combination of X-ray diffraction and NMR allowed
capturing the depolymerization of Si chains as well as a two-step variation in the
layer-to-layer distance. This latter first increases from similar to 11.3 angstrom
(for samples having a Ca/Si ratio <similar to 0.6) up to 12.25 angstrom at Ca/Si =
0.87 +/- 0.02, probably as a result of a weaker layer-to-layer connectivity, and
then decreases down to 11 angstrom when the Ca/Si ratio reaches 1.38 +/- 0.03. The
decrease in layer-to-layer distance results from the incorporation of interlayer Ca
that may form a Ca(OH)(2)-like structure, nanocrystalline and intermixed with C-S-H
layers, at high Ca/Si ratios.
C1 [Grangeon, Sylvain; Claret, Francis; Roosz, Cedric; Gaboreau, Stephane] BRGM
French Geol Survey, SVP D3E, 3 Ave Claude Guillemin, F-45060 Orleans, France.
[Roosz, Cedric] Andra, Sci Div, 1-7 Rue Jean Monnet,Parc Croix Blanche, Chatenay
Malabry, France.
[Sato, Tsutomu] Hokkaido Univ, Grad Sch Engn, Engn Div Solid Waste Resources &
Geoenvironm Engn, Lab Environm Geol,Res Grp Geoenvironm Engn, Kita 13 Nishi 8,
Sapporo, Hokkaido, Japan.
[Linard, Yannick] Andra, Ctr Meuse Haute Marne, F-55290 Bure, France.
C3 Bureau de Recherches Geologiques et Minieres (BRGM); Hokkaido University
RP Grangeon, S (corresponding author), BRGM French Geol Survey, SVP D3E, 3 Ave
Claude Guillemin, F-45060 Orleans, France.
EM s.grangeon@brgm.fr
RI Claret, Francis/A-1232-2010; Sato, Tsutomu/A-5233-2012; gaboreau,
stephane/AAK-1884-2021; Grangeon, Sylvain/AAR-7024-2020
OI Claret, Francis/0000-0002-6203-7795; Sato, Tsutomu/0000-0002-3279-3696;
gaboreau, stephane/0000-0003-2472-6992; Grangeon,
Sylvain/0000-0002-5018-3015; Roosz, Cedric/0000-0002-6151-1002
FU French national research agency (Agence Nationale de la Recherche - ANR)
[ANR-14-CE01-0006]; Grants-in-Aid for Scientific Research [15H04222]
Funding Source: KAKEN; Agence Nationale de la Recherche (ANR)
[ANR-14-CE01-0006] Funding Source: Agence Nationale de la Recherche
(ANR)
FX The authors are grateful to Dr A. Lahfid for fruitful discussions, to Dr
V. Montouillout for NMR data acquisition, to Dr C. Lerouge for
acquisition of EPMA and FTIR data, and to C. Numako for XANES data
acquisition. SG acknowledges funding by the French national research
agency (Agence Nationale de la Recherche - ANR; NACRE project; grant
ANR-14-CE01-0006). This article benefited from comments and suggestions
made by three anonymous reviewers.
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TC 80
Z9 85
U1 2
U2 58
PU INT UNION CRYSTALLOGRAPHY
PI CHESTER
PA 2 ABBEY SQ, CHESTER, CH1 2HU, ENGLAND
SN 1600-5767
J9 J APPL CRYSTALLOGR
JI J. Appl. Crystallogr.
PD JUN
PY 2016
VL 49
BP 771
EP 783
DI 10.1107/S1600576716003885
PN 3
PG 13
WC Chemistry, Multidisciplinary; Crystallography
SC Chemistry; Crystallography
GA DN4GB
UT WOS:000377020600006
PM 27275135
OA Green Published, hybrid
DA 2023-12-05
ER
PT J
AU Park, JH
AF Park, Joo Hyun
TI Formation mechanism of spinel-type inclusions in high-alloyed stainless
steel melts
LA English
DT Article
ID DEOXIDATION EQUILIBRIUM; LIQUID-IRON; SOLIDIFICATION; TEMPERATURES;
CHROMIUM; ALUMINUM; WELDS; NI; SI
AB Fundamental thermodynamics of the relationship between high-alloyed stainless
steel melts (Fe-20 mass pet Cr-13 mass pct Ni-3 mass pct Si) and the inclusions
were investigated. The formation mechanism of the inclusions containing the spinel
crystals was developed based on the experimental results and from the compositions
of the inclusions in the steel samples taken during plant operations. The molar
content of alumina in the inclusions was found to be linearly proportional to the
increase of aluminum content, indicating that the inclusions could contain alumina
even with less than about 200 ppm aluminum in the steel melt, e.g., steel melts
that were mainly deoxidized by silicon. Furthermore, the composition of the
inclusions is shown to be a function of the activity of the deoxidizers such as
aluminum and silicon in the steel melt. From the analysis of the plant samples, it
was found that the contents of MgO and Al2O3 in the calcium silicate type
inclusions increased continuously as the steel melt transfers from the argon oxygen
decarburization (AOD) converter to the tundish. This composition change in the
inclusions originated from the reduction of MgO and Al2O3 in the slags or
refractories by silicon in the steel melt. Increases of MgO and Al2O3 contents were
prominent in tundish samples, and thus, the spinel phase could be crystallized in
the calcium silicate inclusion matrix in the tundish; and finally the spinel
crystals grew during cooling of the steel melt through the continuous casting (CC)
mold and in the slabs. On the other hand, manganese silicate type inclusions
containing chromium oxide were observed after tapping of the molten steel to the
ladle. The MnO and Cr2O3 in these inclusions was initially reduced by silicon in
the steel melt in the ladle treatment (LT) process, followed by further reduction
by aluminum through the LT to the CC mold. The fractions of inclusions containing
spinel crystals in cast slabs were negligible at the alumina content of less than
about 20 mass pct, while they critically increased at alumina contents greater than
about 20 mass pct.
C1 POSCO, Stainless Steel Res Grp, Tech Res Labs, Pohang 790785, South Korea.
C3 POSCO
RP Park, JH (corresponding author), POSCO, Stainless Steel Res Grp, Tech Res Labs,
EM basicity@posco.com
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NR 26
TC 80
Z9 92
U1 0
U2 46
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2007
VL 38
IS 4
BP 657
EP 663
DI 10.1007/s11663-007-9066-x
PG 7
Engineering
GA 215ZP
UT WOS:000249847800018
DA 2023-12-05
ER
PT J
AU Phair, JW
van Deventer, JSJ
AF Phair, JW
van Deventer, JSJ
TI Characterization of fly-ash-based geopolymeric binders activated with
sodium aluminate
SO INDUSTRIAL & ENGINEERING CHEMISTRY RESEARCH
LA English
DT Article
ID MAS NMR; INFRARED-SPECTRA; AL-27; PRECIPITATION; SI-29; IR
AB Properties and characteristics of sodium silicate activated fly-ash-based
geopolymers have been extensively investigated., but,the utilization of sodium
aluminate activation has received little attention. The present works therefore,
examines the properties of the starting materials and sodium aluminate solutions
and their effect on the final material properties and microstructure of fly-ash-
based geopolymers. To achieve this, starting sodium aluminate solutions were
characterized with ATR-FTIR and Al-27 NMR spectroscopies to determine the
coordination state of aluminum as a function of solution concentration and
[OH]/[Al] ratio. Various fly-ash-based geopolymeric. matrixes were synthesized
utilizing fly ash, kaolinite, K-feldspar, and slag as the mineral aluminum!
sources. The,matrixes were activated with alkali silicate or alkali aluminate
solutions as a function of pH, concentration, and alkali ion (Na+ or K+). FTIR and
XRD studies combined with compressive strength tests demonstrated that in certain
cases aluminate activated geopolymers were mechanically superior to traditional
silicate activated geopolymers. Of specific interest was whether the superior
properties could be related to a polysialate or calcium-aluminate-hydrate phase,
which both contain 6-coordinate aluminum. A discussion of commercially viable
industrial aluminate waste sources as potential large-scale feedstock for
geopolymers was included.
C1 Univ Melbourne, Dept Chem Engn, Melbourne, Vic 3010, Australia.
RP van Deventer, JSJ (corresponding author), Univ Melbourne, Dept Chem Engn,
Melbourne, Vic 3010, Australia.
EM jannie@unimelb.edu.au
OI Phair, John W./0000-0002-3521-3642
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NR 32
TC 80
Z9 97
U1 4
U2 28
PI WASHINGTON
SN 0888-5885
J9 IND ENG CHEM RES
JI Ind. Eng. Chem. Res.
PD AUG 21
PY 2002
VL 41
IS 17
BP 4242
EP 4251
DI 10.1021/ie010937o
PG 10
SC Engineering
GA 585KB
UT WOS:000177523000012
DA 2023-12-05
ER
PT J
AU Shi, CB
Seo, MD
Cho, JW
Kim, SH
AF Shi, Cheng-Bin
Seo, Myung-Duk
Cho, Jung-Wook
Kim, Seon-Hyo
TI Crystallization Characteristics of CaO-Al2O3-Based
Mold Flux and Their Effects on In-Mold Performance during High-Aluminum
TRIP Steels Continuous Casting
LA English
DT Article
ID HEAT-TRANSFER; AL; BEHAVIORS; SLAG; TEMPERATURE; OXIDATION; BASICITY;
PHASE; SI
AB Crystallization behaviors of the newly developed lime-alumina-based mold fluxes
for high-aluminum transformation induced plasticity (TRIP) steels casting were
experimentally studied, and compared with those of lime-silica-based mold fluxes.
The effects of mold flux crystallization characteristics on heat transfer and
lubrication performance in casting high-Al TRIP steels were also evaluated. The
results show that the crystallization temperatures of lime-alumina-based mold
fluxes are much lower than those of lime-silica-based mold fluxes. Increasing B2O3
addition suppresses the crystallization of lime-alumina-based mold fluxes, while
Na2O exhibits an opposite effect. In continuous cooling of lime-alumina-based mold
fluxes with high B2O3 contents and a CaO/Al2O3 ratio of 3.3, faceted cuspidine
precipitates first, followed by needle-like CaO center dot B2O3 or 9CaO center dot
3B(2)O(3)center dot CaF2. In lime-alumina-based mold flux with low B2O3 content
(5.4 mass pct) and a CaO/Al2O3 ratio of 1.2, the formation of fine CaF2 takes place
first, followed by blocky interconnected CaO center dot 2Al(2)O(3) as the dominant
crystalline phase, and rod-like 2CaO center dot B2O3 precipitates at lower
temperature during continuous cooling of the mold flux. In B2O3-free mold flux,
blocky interconnected 3CaO center dot Al2O3 precipitates after CaF2 and 3CaO center
dot 2SiO(2) formation, and takes up almost the whole crystalline fraction. The
casting trials show that the mold heat transfer rate significantly decreases near
the meniscus during the continuous casting using lime-alumina-mold fluxes with
higher crystallinity, which brings a great reduction of surface depressions on cast
slabs. However, excessive crystallinity of mold flux causes poor lubrication
between mold and solidifying steel shell, which induces various defects such as
drag marks on cast slab. Among the studied mold fluxes, lime-alumina-based mold
fluxes with higher B2O3 contents and a CaO/Al2O3 ratio of 3.3 show comparatively
improved performance.
C1 [Shi, Cheng-Bin; Seo, Myung-Duk; Kim, Seon-Hyo] Pohang Univ Sci & Technol
POSTECH, Dept Mat Sci & Engn, Pohang 790784, South Korea.
[Cho, Jung-Wook] Pohang Univ Sci & Technol POSTECH, Grad Inst Ferrous Technol,
C3 Pohang University of Science & Technology (POSTECH); Pohang University
of Science & Technology (POSTECH)
RP Cho, JW (corresponding author), Pohang Univ Sci & Technol POSTECH, Grad Inst
Ferrous Technol, Pohang 790784, South Korea.
RI Shi, Chengbin/J-1262-2016; Cho, Jung-Wook/A-8142-2013
OI Shi, Chengbin/0000-0001-8127-3382; Cho, Jung-Wook/0000-0003-2364-1938
FU Global Excellent Technology Innovation - Ministry of Trade, Industry &
Energy (MOTIE) of Korea [10045029]; Korea Evaluation Institute of
Industrial Technology (KEIT) [10045029] Funding Source: Korea Institute
of Science & Technology Information (KISTI), National Science &
Technology Information Service (NTIS)
FX The authors would like to express sincere thanks to Mr. Seung-ho Shin
and Mr. Min-su Kim of Graduate Institute of Ferrous Technology, POSTECH
for their help in preparing mold flux samples. This work was financially
supported by the Global Excellent Technology Innovation (Grant No.
10045029) funded by the Ministry of Trade, Industry & Energy (MOTIE) of
Korea.
CR Baum TL, 2007, METALL MATER TRANS B, V38, P287, DOI 10.1007/s11663-007-9023-8
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NR 28
TC 79
Z9 82
U1 3
U2 47
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD JUN
PY 2014
VL 45
IS 3
BP 1081
EP 1097
DI 10.1007/s11663-014-0034-y
PG 17
Engineering
GA AI6JW
UT WOS:000336980900030
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Jiang, M
Wang, XH
Chen, B
Wang, WJ
AF Jiang, Min
Wang, Xinhua
Chen, Bin
Wang, Wanjun
TI Formation of MgO•Al2O3 inclusions in high strength
alloyed structural steel refined by
CaO-SiO2-Al2O3-MgO slag
LA English
DT Article
DE MgO center dot Al2O3 spinel; slag; inclusion; equilibrium; high strength
alloyed structural steel
ID LONG CYCLE FATIGUE; NONMETALLIC INCLUSION; LIQUID STEEL; THERMODYNAMICS;
304-STAINLESS-STEEL; MGO-AL2O3; MECHANISM; FAILURE; MGO
AB Present paper focused on the formation of MgO center dot Al2O3 inclusions in
high strength 42CrMo alloyed structural steel refined by CaO-SiO2-Al2O3-MgO slag.
Soluble aluminum contents in molten steel were less than 0.0100 % when steel/slag
equilibrium was established.
It is found by pre-equilibrium experiments that 90 min are sufficient for the
attainment of equilibrium of slag-metal at 1 873 K. Spinel inclusions dispersed
widely in the steel, with sizes between 2 pm and 4 pm. Magnesium content in molten
steel influences the morphology of spinel inclusions greatly. With the rise of
magnesium content in steel, globular spinel inclusions were modified into angular
ones. However, trace amount of Ca in inclusions is effective to change the spinels
from angular shape to globular shape. Solubility of MgO in slag was also discussed.
It is shown that MgO in slags are saturated and activities of MgO can be considered
as unity, Observed log(X-MgO/X-Al2O3) of inclusions increases with the growth of
observed log[a([Mg])/(a([Al])(2)center dot a([O])(2))] of molten steel as well as
the rise of observed log(a(MgO)/a(Al2O3)) in slag, both exhibiting good linear
relation.
MgO-MgO center dot Al2O3-Al2O3 stability phase diagram was obtained. It is found
that aluminum and magnesium contents in molten steel mainly position in the MgO
center dot Al2O3 formation zone, which is essentially pre-requisite for the
formation MgO center dot Al2O3 in steel. Silica in slag is helpful to stabilize MgO
center dot Al2O3 phase, because it would react with calcium and aluminum in molten
steel. In the scope of soluble aluminum contents, magnesium content influences the
transformation among MgO-MgO center dot Al2O3-Al2O3 ternary phases greatly, which
is the reason for the formation of rectangular MgO inclusions.
C1 [Jiang, Min; Wang, Xinhua; Chen, Bin; Wang, Wanjun] Univ Sci & Technol Beijing,
Sch Met & Ecol Engn, Beijing 100083, Peoples R China.
C3 University of Science & Technology Beijing
RP Jiang, M (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol
EM jiangmin820429@yahoo.com.cn
CR Chapetti MD, 2003, MAT SCI ENG A-STRUCT, V356, P236, DOI 10.1016/S0921-
5093(03)00136-9
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5093(03)00135-7
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NR 20
TC 79
Z9 91
U1 4
U2 43
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2008
VL 48
IS 7
BP 885
EP 890
PG 6
GA 330IJ
UT WOS:000257933900002
OA gold
DA 2023-12-05
ER
PT J
AU Zhang, ZT
Wen, GH
Tang, P
Sridhar, S
AF Zhang, Zuotai
Wen, Guanghua
Tang, Ping
TI The influence of Al2/SiO2 ratio on the viscosity
of mold fluxes
LA English
DT Article
DE TRIP steel; mold fluxes; X(Al2O3)/X(SiO2) ratio; viscosity
ID TRANSFORMATION-INDUCED-PLASTICITY; SILICATE MELTS; TRIP STEELS; SLAGS;
BEHAVIOR; AL2O3; ALUMINUM; CAF2
AB The present paper investigates how the X(Al2O3)/X(SiO2) ratio in mold siag
compositions in a range between 0.06 and 2.14 influences the viscosity of the melt.
The objective was to study the variation in viscosity of mould slags if they get
enriched in Al(2)O(3) as a result of reactions during continuous casting with high
Al containing steel melts for manufacturing TRIP steels.
The viscosity was found to increase with increasing X(Al2O3)/X(SiO2) ratio but a
change in the degree of increase was noted at a ratio of 0.57 The effect of
increasing temperature was investigated and it was shown that viscosity decreased,
as expected, with increasing temperature. An available model in literature for
predicting the mold-slag viscosity was empirically modified to account for high
Al(2)O(3) contents investigated in this study.
Increasing X(Al2O3)/X(SiO2) did not appear to influence the vaporization loss of
F but increasing the ratio did influence crystallization by promoting the
precipitation of CaF(2) during slow cooling of samples with a high X(Al2O3)/X(SiO2)
ratio (0.84 and 2.14).
C1 [Zhang, Zuotai; Wen, Guanghua; Sridhar, Seetharaman] Carnegie Mellon Univ, Dept
Mat Sci & Engn, Pittsburgh, PA 15213 USA.
[Wen, Guanghua; Tang, Ping] Chongqing Univ, Dept Mat Sci & Engn, Chongqing
[Sridhar, Seetharaman] Natl Energy Technol Lab, Pittsburgh, PA 15236 USA.
C3 Carnegie Mellon University; Chongqing University; United States
Department of Energy (DOE); National Energy Technology Laboratory - USA
RP Zhang, ZT (corresponding author), Carnegie Mellon Univ, Dept Mat Sci & Engn,
Pittsburgh, PA 15213 USA.
EM sridhars@andrew.cmu.edu
OI Zhang, Zuotai/0000-0002-3580-6018
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NR 43
TC 79
Z9 87
U1 0
U2 18
PI TOKYO
JAPAN
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2008
VL 48
IS 6
BP 739
EP 746
PG 8
GA 318LN
UT WOS:000257093300003
OA gold
DA 2023-12-05
ER
PT J
AU Heikal, M
AF Heikal, M
TI Effect of temperature on the physico-mechanical and mineralogical
properties of Homra pozzolanic cement pastes
LA English
DT Article
DE heat treatment; Homra pozzolanic cement; compressive strength; phase
composition; microstructure
ID PHASE-COMPOSITION; SILICA FUME; MICROSTRUCTURE; CONCRETE
AB The effect of temperature on the phase composition and physico-mechanical
properties of cement pastes is vital for fire resistance. Addition of fine, divided
materials, such as dehydrated aluminum silicate (fired clay), natural hydrated
aluminum silicate (clay), chromite, sintered magnesite, slag, silica, fly ash,
diatomaceous earth, and Homra (crushed clay bricks), to Portland cement is known to
increase heat resistance by combining with lime. Homra is a pozzolanic material
that can react with lime liberated from the hydration of ordinary Portland cement
(OPC). This reaction improves the microstructure of cement pastes. In this study,
OPC was partially substituted by Homra in the ratios of 10, 20, and 30 wt.%. The
cement pastes were fired for 3 h without any load at increasing temperatures from
100 degreesC to 600 degreesC by increment of 100 degreesC. The results show that
the replacement of OPC by 20 wt.% Homra improves the compressive strength by about
25.0%, but replacement by 10 and 30 wt.%, the strength increases by 4.0% and 8.5%
at 600 degreesC. This result is also due to the pozzolanic reaction of Homra with
liberated lime to produce additional amounts of calcium silicate hydrates. (C) 2000
Elsevier Science Ltd. All rights reserved.
C1 Zagazig Univ, Inst Efficient Prod, Zagazig, Egypt.
C3 Egyptian Knowledge Bank (EKB); Zagazig University
RP Heikal, M (corresponding author), Zagazig Univ, Inst Efficient Prod, Zagazig,
Egypt.
RI Heikal, Mohamed/AAJ-3345-2021
OI Heikal, Mohamed/0000-0002-8122-4019
CR [Anonymous], MANSOURA SCI B
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NR 10
TC 79
Z9 79
U1 1
U2 11
PI OXFORD
SN 0008-8846
JI Cem. Concr. Res.
PD NOV
PY 2000
VL 30
IS 11
BP 1835
EP 1839
DI 10.1016/S0008-8846(00)00403-8
PG 5
GA 385YC
UT WOS:000166031900019
DA 2023-12-05
ER
PT J
AU Huseien, GF
Sam, ARM
Shah, KW
Asaad, MA
Tahir, MM
Mirza, J
Sam, Abdul Rahman Mohd
Shah, Kwok Wei
Asaad, Mohammad Ali
Tahir, Mahmood Md
Mirza, Jahangir
TI Properties of ceramic tile waste based alkali-activated mortars
incorporating GBFS and fly ash
LA English
DT Article
DE Alkali activated mortar; Ceramic waste; GBFS; Fly ash; Strength;
Microstructure
ID OIL FUEL ASH; MECHANICAL-PROPERTIES; CORROSION-RESISTANCE; STRENGTH
PROPERTIES; GEOPOLYMER MORTARS; CONCRETE; SLAG; POWDER; CEMENT;
EMISSIONS
AB This paper presents the experimental findings of a study on the performance of
waste ceramic powder (WCP) as binder on the mechanical and microstructure
properties of alkali activated mortars (AAMs) containing ground blast furnace slag
(GBFS) and fly ash (FA). In this study, the ternary blend was activated with low
concentration of alkaline solution (4 M). WCP was kept with high content of 50%,
60% and 70% for the total binder. After casting operation, the specimens were cured
at ambient temperature of 27 degrees C and tested at eight different ages of 1, 3,
7, 28, 56, 90, 180 and 360 days. Microstructure tests such as Xray diffraction
(XRD), scanning electron microscope (SEM) and Fourier transform infrared
spectroscopy (FTIR) were conducted to evaluate the effect of high content of WCP on
the formulation of sodium aluminium silicate hydrate (N-A-S-H), calcium aluminium
silicate hydrate (C-A-S-H) and calcium silicate hydrate (C-S-H) gels. Test results
indicated that high volume WCP produced environmental friendly alkali activated
mortars with compressive strength higher than 70 MPa at age of 28 days. The results
also showed that the workability and setting time of alkali activated mortars
enhanced with the increase in WCP content. (C) 2019 Elsevier Ltd. All rights
reserved.
C1 [Huseien, Ghasan Fahim; Sam, Abdul Rahman Mohd; Asaad, Mohammad Ali; Tahir,
Mahmood Md] Univ Teknol Malaysia, Inst Smart Infrastruct & Innovat Construct, UTM
Construct Res Ctr, Sch Civil Engn,Fac Engn, Johor Baharu 81310, Johor, Malaysia.
[Shah, Kwok Wei] Natl Univ Singapore, Sch Design & Environm, Dept Bldg,
[Mirza, Jahangir] Res Inst Hydro Quebec, Dept Perennite Actifs, 1800 Lionel
Boulet, Varennes, PQ J3X 1S1, Canada.
C3 Universiti Teknologi Malaysia; National University of Singapore;
Hydro-Quebec
RP Huseien, GF (corresponding author), Univ Teknol Malaysia, Inst Smart Infrastruct
& Innovat Construct, UTM Construct Res Ctr, Sch Civil Engn,Fac Engn, Johor Baharu
81310, Johor, Malaysia.; Mirza, J (corresponding author), Res Inst Hydro Quebec,
Dept Perennite Actifs, 1800 Lionel Boulet, Varennes, PQ J3X 1S1, Canada.
EM fhghassan@utm.my; mirza@ireq.ca
RI Mirza, Jahangir/HOF-8557-2023; Huseien, Ghasan Fahim/AEC-3508-2022
OI Mirza, Jahangir/0000-0002-3783-8048; Huseien, Ghasan
Fahim/0000-0002-2963-0335
FU UTM COE research grant [Q.J130000.2409.04G00]; FRGS grant
[R.J130000.7822.4F722]; Universiti Teknologi Malaysia; Centre of
Excellence; Ministry of Higher Education; EM Malaysia Sdn. Bhd.; EMRO
Japan
FX This research was supported and funded by the UTM COE research grant
Q.J130000.2409.04G00 and FRGS grant R.J130000.7822.4F722. The authors
would like to thank the grants provider, namely Universiti Teknologi
Malaysia, Centre of Excellence and Ministry of Higher Education, staff
from Material and Structure Laboratory, School of Civil Engineering,
Universiti Teknologi Malaysia, and the EM Malaysia Sdn. Bhd. and EMRO
Japan for their support and cooperation in conducting this research.
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NR 60
TC 78
Z9 78
U1 3
U2 38
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUL 30
PY 2019
VL 214
BP 355
EP 368
DI 10.1016/j.conbuildmat.2019.04.154
PG 14
GA IE9MA
UT WOS:000472697300033
DA 2023-12-05
ER
PT J
AU Li, YC
Min, XB
Ke, Y
Chai, LY
Shi, MQ
Tang, CJ
Wang, QW
Liang, YJ
Lei, J
Liu, DG
AF Li, Yuan-Cheng
Min, Xiao-Bo
Ke, Yong
Chai, Li-Yuan
Shi, Mei-Qing
Tang, Chong-Jian
Wang, Qing-Wei
Liang, Yan-Jie
Lei, Jie
Liu, De-Gang
TI Utilization of red mud and Pb/Zn smelter waste for the synthesis of a
red mud-based cementitious material
LA English
DT Article
DE Red mud; Arsenic sludge; Unconfined compressive strength; Red mud-based
cementitious material
ID FLY-ASH; HYDROTHERMAL SULFIDATION; BAUXITE RESIDUE; IMMOBILIZATION;
REMOVAL; SLUDGE; SLAG; FLOTATION; CALCIUM; CEMENTS
AB A new method in Which Pb/Zn smelter waste containing arsenic and heavy metals
(arsenic sludge), red mud and lime are utilized to prepare red mud-based
cementitious material (RCM) is proposed in this study. XRD, SEM, FTIR and
unconfined compressive strength (UCS) tests were employed to assess the
physicochemical properties of RCM. In addition, ettringite and iron oxide-
containing ettringite were used to study the hydration mechanism of RCM. The
results show that the UCS of the RCM (red mud + arsenic sludge + lime) was higher
than that of the binder (red mud + arsenic sludge). When the mass ratio of m
(binder): m (lime) was 94:6 and then maintained 28 days at ambient temperature, the
UCS reached 12.05 MPa. The red mud has potential cementitious characteristics, and
the major source of those characteristics was the aluminium oxide. In the red mud-
arsenic sludge-lime system, aluminium oxide was effectively activated by lime and
gypsum to form complex hydration products. Some of the aluminium in ettringite was
replaced by iron to form calcium sulfoferrite hydrate. The BCR and leaching
toxicity results show that the leaching concentration was strongly dependent on the
chemical speciation of arsenic and the hydration products. Therefore, the
investigated red mud and arsenic sludge can be successfully utilized in cement
composites to create a red mud-based cementitious material. (C) 2017 Elsevier B.V.
C1 [Li, Yuan-Cheng; Min, Xiao-Bo; Chai, Li-Yuan; Shi, Mei-Qing; Tang, Chong-Jian;
Wang, Qing-Wei; Liang, Yan-Jie; Lei, Jie; Liu, De-Gang] Cent South Univ, Sch Met &
Environm, Changsha 410083, Hunan, Peoples R China.
[Min, Xiao-Bo; Ke, Yong; Chai, Li-Yuan; Shi, Mei-Qing; Tang, Chong-Jian; Wang,
Qing-Wei] Chinese Natl Engn Res Ctr Control & Treatment Hea, Changsha 410083,
Hunan, Peoples R China.
[Ke, Yong] Cent South Univ, Sch Mat Sci & Engn, Changsha 410083, Hunan, Peoples
R China.
C3 Central South University; Central South University
RP Min, XB (corresponding author), Cent South Univ, Sch Met & Environm, Changsha
EM mxbcsu@163.com
RI Li, yuancheng/IUO-3866-2023
OI LI, Yuancheng/0000-0001-8458-4645
FU Special Program on Environmental Protection for Public Welfare
[201509050]; Natural Science Foundation of China [51634010, 51474247];
Key research and development project of Hunan Province, China
[2015SK2084]; Central South University [2015CX001]; China Postdoctoral
Science Foundation [2017M612583]; Science and Technology Project of
Hunan, China [2017RS3010]
FX The authors gratefully acknowledge the Special Program on Environmental
Protection for Public Welfare (201509050), the Natural Science
Foundation of China (51634010 and 51474247), Key research and
development project of Hunan Province, China (2015SK2084), the Grants
from the project of Innovation-driven Plan in Central South University
(2015CX001), the China Postdoctoral Science Foundation (2017M612583),
and Science and Technology Project of Hunan, China (2017RS3010).
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NR 32
TC 78
Z9 83
U1 15
U2 152
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD FEB 15
PY 2018
VL 344
BP 343
EP 349
DI 10.1016/j.jhazmat.2017.10.046
PG 7
GA FT6EI
UT WOS:000423246700035
PM 29080487
DA 2023-12-05
ER
PT J
AU Pettersson, A
Åmand, LE
Steenari, BM
AF Pettersson, Anita
Amand, Lars-Erik
Steenari, Britt-Marie
TI Chemical fractionation for the characterisation of fly ashes from
co-combustion of biofuels using different methods for alkali reduction
SO FUEL
LA English
DT Article
DE Alkali; Olivine; BFS; Zeolite; Fluidized bed
ID FLUIDIZED-BED COMBUSTION; AGGLOMERATION CHARACTERISTICS; BIOMASS;
BEHAVIOR; FIELD; SULFATE; CAPTURE; KAOLIN; FUELS
AB Chemical fractionation, SEM-EDX and XRD was used for characterisation of fly
ashes from different co-combustion tests in a 12 MW circulating fluidized bed
boiler. The fuels combusted were wood pellets as base fuel and straw pellets as co-
fuel in order to reach a fuel blend with high alkali and chlorine concentrations.
This fuel blend causes severe problems with both agglomeration of bed material if
silica sand is used and with deposits in the convection section of the boiler.
Counter measures to handle this situation and avoiding expensive shut downs, tests
with alternative bed materials and additives were performed. Three different bed
materials were used; silica sand, Olivine sand and blast furnace slag (BFS) and
different additives were introduced to the furnace of the boiler; Kaolin, Zeolites
and Sulphur with silica sand as bed material. The results of the study are that BFS
gives the lowest alkali load in the convection pass compared with Silica and
Olivine sand. in addition less alkali and chlorine was found in the fly ashes in
the BFS case. The Olivine sand however gave a higher alkali load in the convection
section and the chemical fractionation showed that the main part of the alkali in
the fly ashes was soluble, thus found as KCl which was confirmed by the SEM-EDX and
XRD.
The comparison of the different additives gave that addition of Kaolin and
Zeolites containing aluminium-silicates captured 80% of the alkali in the fly ash
as insoluble alkali-aluminium-silikates and reduced the KCl load on the convection
section. Addition of sulphur reduced the KCl load in the flue gas even more but the
K2SO4 concentration was increased and KCl was found in the fly ashes anyhow. The
chemical fractionation showed that 65% of the alkali in the fly ashes of the
Sulphur case was soluble. (C) 2009 Elsevier Ltd. All rights reserved.
C1 [Pettersson, Anita] Univ Coll Boras, SE-50190 Boras, Sweden.
[Amand, Lars-Erik] Chalmers Univ Technol, Environm & Energy Dept, SE-41296
Gothenburg, Sweden.
[Steenari, Britt-Marie] Chalmers Univ Technol, Dept Chem & Biol Engn, SE-41296
Gothenburg, Sweden.
C3 University of Boras; Chalmers University of Technology; Chalmers
RP Pettersson, A (corresponding author), Univ Coll Boras, SE-50190 Boras, Sweden.
EM anita.pettersson@hb.se
FU Swedish Energy Administration; VarmeForsk Service AB; Angpanneforeningen
FX Main support for this work was provided by the Swedish Energy
Administration. The large scale tests were partly performed as part of
Contract No. A5-509 from VarmeForsk Service AB which is gratefully
acknowledged. Vattenfall Power Consultant supplied the IACM instrument
and Angpanneforeningen contributed with fundings for additional
analyses. Further, the authors acknowledge Akademiska Hus AB for
maintaining and operating the boiler and the research staff employed by
Chalmers University of Technology for carrying out the combustion tests.
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NR 23
TC 78
Z9 83
U1 0
U2 57
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD SEP
PY 2009
VL 88
IS 9
BP 1758
EP 1772
DI 10.1016/j.fuel.2009.03.038
PG 15
GA 464TW
UT WOS:000267531100031
OA Green Published
DA 2023-12-05
ER
PT J
AU SUITO, H
INOUE, H
INOUE, R
AF SUITO, H
INOUE, H
INOUE, R
TI ALUMINUM OXYGEN EQUILIBRIUM BETWEEN CAO-AL2O3 MELTS AND LIQUID-IRON
LA English
DT Article
DE CAO-AL2O3 SLAGS; ALUMINUM OXYGEN EQUILIBRIUM; DEOXIDATION; ACTIVITY OF
AL2O3; SUPERSATURATION
ID SYSTEM; FE; AL
AB Aluminium-oxygen equilibria between CaO-Al2O3 melts and liquid iron were studied
in the temperature range of 1 823 to 1 923 K, using an alumina and lime crucibles.
The equilibrium constant K for the reaction: 2Al + 30 = Al2O3 was discussed with
reference to the supersaturation for nucleation of alumina, and compared with the
previous experimental and thermodynamic data. The supersaturation was observed in
the experiments in which an Fe-Al alloy with low concentrations of initial oxygen
was used under the condition of no stirring. Supersaturation increased with a
decrease of oxygen content in liquid iron. Two types of alumina inclusions with a
size of 2-5-mu-m and below 0.1-mu-m were observed by SEM.
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NR 17
TC 78
Z9 81
U1 0
U2 6
PI TOKYO
PA 9-4 OTEMACHI 1-CHOME CHIYODA-KU, TOKYO 100, JAPAN
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 1991
VL 31
IS 12
BP 1381
EP 1388
PG 8
GA GV097
UT WOS:A1991GV09700002
OA gold
DA 2023-12-05
ER
PT J
AU Ren, GX
Xiao, SW
Xie, MQ
Pan, B
Chen, J
Wang, FG
Xia, X
AF Ren, Guo-xing
Xiao, Song-wen
Xie, Mei-qiu
Pan, Bing
Chen, Jian
Wang, Feng-gang
Xia, Xing
TI Recovery of valuable metals from spent lithium ion batteries by smelting
reduction process based on
FeO-SiO2-Al2O3 slag system
SO TRANSACTIONS OF NONFERROUS METALS SOCIETY OF CHINA
LA English
DT Article
DE lithium ion battery; smelting reduction; cobalt; nickel; copper slag;
fayalite
ID NICKEL; COBALT; ACID; EQUILIBRIUM; VISCOSITY; ALUMINUM
AB A novel smelting reduction process based on FeO-SiO2-Al2O3 slag system for spent
lithium ion batteries with Al cans was developed, while using copper slag as the
only slag former. The feasibility of the process and the mechanism of copper loss
in slag were investigated. 98.83% Co, 98.39% Ni and 93.57% Cu were recovered under
the optimum conditions of slag former/battery mass ratio of 4.0: 1, smelting
temperature of 1723 K, and smelting mass ratio of time of 30 min. The FeO-SiO2-
Al2O3 slag system for the smelting process is appropriate under the conditions of
m(FeO): m(SiO2)= 0.58: 1-1.03: 1, and 17.19%-21.52% Al2O3 content. The obtained
alloy was mainly composed of Fe-Co-Cu-Ni solid solution including small amounts of
matte. The obtained slag mainly consisted of fayalite and hercynite. Meanwhile, the
mechanism of copper loss is the mechanical entrainment from strip-like fayalite
particles in the main form of copper sulfide and metallic copper.
C1 [Ren, Guo-xing; Xiao, Song-wen; Xie, Mei-qiu; Pan, Bing; Chen, Jian; Wang, Feng-
gang; Xia, Xing] Changsha Res Inst Min & Met Co Ltd, Changsha 410012, Hunan,
Peoples R China.
RP Xiao, SW (corresponding author), Changsha Res Inst Min & Met Co Ltd, Changsha
EM swinxiao@126.com
FU State-Owned Enterprise Electric Vehicle Industry Alliance, China
[JS-211]
FX Project (JS-211) supported by the State-Owned Enterprise Electric
Vehicle Industry Alliance, China
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NR 25
TC 77
Z9 87
U1 9
U2 111
PU ELSEVIER
PI AMSTERDAM
SN 1003-6326
EI 2210-3384
J9 T NONFERR METAL SOC
JI Trans. Nonferrous Met. Soc. China
PD FEB
PY 2017
VL 27
IS 2
BP 450
EP 456
DI 10.1016/S1003-6326(17)60051-7
PG 7
GA EP3FT
UT WOS:000397268900024
DA 2023-12-05
ER
PT J
AU Pauliuk, S
Kondo, Y
Nakamura, S
Nakajima, K
AF Pauliuk, Stefan
Kondo, Yasushi
Nakajima, Kenichi
TI Regional distribution and losses of end-of-life steel throughout
multiple product life cycles Insights from the global multiregional
MaTrace model
LA English
DT Article
DE Circular economy; MaTrace; Steel recycling; Closed-loop recycling;
Circularity metric
ID EMBODIED RESOURCE FLOWS; ALLOYING ELEMENTS; CIRCULAR ECONOMY; ENERGY;
ALUMINUM; TIME; IRON; AUTOMOBILES; METHODOLOGY; COMMODITIES
AB Substantial amounts of post-consumer scrap are exported to other regions or lost
during recovery and remelting, and both export and losses pose a constraint to
desires for having regionally closed material cycles. To quantify the challenges
and trade-offs associated with closed-loop metal recycling, we looked at the
material cycles from the perspective of a single material unit and trace a unit of
material through several product life cycles. Focusing on steel, we used current
process parameters, loss rates, and trade patterns of the steel cycle to study how
steel that was originally contained in high quality applications such as machinery
or vehicles with stringent purity requirements gets subsequently distributed across
different regions and product groups such as building and construction with less
stringent purity requirements. We applied MaTrace Global, a supply-driven
multiregional model of steel flows coupled to a dynamic stock model of steel use.
We found that, depending on region and product group, up to 95% of the steel
consumed today will leave the use phase of that region until 2100, and that up to
50% can get lost in obsolete stocks, landfills, or slag piles until 2100. The high
losses resulting from business-as-usual scrap recovery and recycling can be
reduced, both by diverting postconsumer scrap into long-lived applications such as
buildings and by improving the recovery rates in the waste management and remelting
industries. Because the lifetimes of high-quality (cold-rolled) steel applications
are shorter and remelting occurs more often than for buildings and infrastructure,
we found and quantified a tradeoff between low losses and high-quality applications
in the steel cycle. Furthermore, we found that with current trade patterns, reduced
overall losses will lead to higher fractions of secondary steel being exported to
other regions. Current loss rates, product lifetimes, and trade patterns impede the
closure of the steel cycle. (C) 2016 Elsevier B.V. All rights reserved.
C1 [Pauliuk, Stefan] Univ Freiburg, Fac Environm & Nat Resources, D-79106 Freiburg,
Germany.
[Kondo, Yasushi; Nakamura, Shinichiro] Waseda Univ, Grad Sch Econ, Tokyo, Japan.
[Nakajima, Kenichi] Natl Inst Environm Studies, Ctr Mat Cycles & Waste
Management Res, Tsukuba, Ibaraki, Japan.
C3 University of Freiburg; Waseda University; National Institute for
Environmental Studies - Japan
RP Pauliuk, S (corresponding author), Univ Freiburg, Fac Environm & Nat Resources,
D-79106 Freiburg, Germany.
EM stefan.pauliuk@indecol.uni-freiburg.de
RI Nakajima, Kenichi/AAQ-3768-2021; Pauliuk, Stefan/AAC-8274-2022; Kondo,
Yasushi/B-9219-2013
OI Nakajima, Kenichi/0000-0002-7241-7695; Kondo,
Yasushi/0000-0002-6855-2691; Pauliuk, Stefan/0000-0002-6869-1405
FU European Commission under the DESIRE Project [308552]; JSPS KAKENHI
[25281065, 15K00641]; Grants-in-Aid for Scientific Research [25281065,
15K00641, 26281059] Funding Source: KAKEN
FX The work of S.P. was funded in part by the European Commission under the
DESIRE Project (grant number 308552). The work of Y.K. and S.N. was
financially supported by JSPS KAKENHI (grant numbers 25281065 and
15K00641). The research was conducted without involvement of the funding
sources. The authors thank Richard Wood for his comments and for
providing data from EXIOBASE. The authors also thank Wataru Takayanagi
for drawing the graphical abstract.
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TC 76
Z9 77
U1 2
U2 56
PU ELSEVIER
PI AMSTERDAM
SN 0921-3449
EI 1879-0658
PD JAN
PY 2017
VL 116
BP 84
EP 93
DI 10.1016/j.resconrec.2016.09.029
PG 10
WE Science Citation Index Expanded (SCI-EXPANDED); Social Science Citation Index
(SSCI)
GA ED3VI
UT WOS:000388776200008
PM 28216806
DA 2023-12-05
ER
PT J
AU Jung, IH
Eriksson, G
Wu, P
Pelton, A
AF Jung, In-Ho
Eriksson, Gunnar
Wu, Ping
Pelton, Arthur
TI Thermodynamic Modeling of the
Al2O3-Ti2O3-TiO2
System and Its Applications to the Fe-Al-Ti-O Inclusion Diagram
LA English
DT Article
DE thermodynamic modeling; Al2O3-Ti2O3-TiO2; Al-Ti deoxidation; inclusion;
FactSage
ID QUASI-CHEMICAL MODEL; ALUMINUM; TEMPERATURE; TITANIUM; OPTIMIZATION;
EQUILIBRIA; TITANATES; OXIDES
AB All available thermodynamic and phase diagram data have been critically
evaluated and optimized for the liquid slag phase and for all solid phases at 1 bar
pressure from 298 K to above the liquidus temperatures for the systems Al2O3-TiO2,
Al2O3-Ti2O3, and Al2O3-Ti2O3-TiO2, and a database of model parameters has been
prepared. The Modified Quasichemical Model was employed for the molten oxide phase.
The thermodynamic modeling predicts the existence of a liquid oxide Al2O3-Ti2O3-
TiO2 phase at secondary steelmaking conditions. The database was used to calculate
the inclusion diagram for Al-Ti deoxidation at 1600 degrees C.
C1 [Jung, In-Ho] McGill Univ, Dept Min & Mat Engn, Montreal, PQ H3A 2B2, Canada.
[Eriksson, Gunnar] GTT Technol, D-52134 Herzogenrath, Germany.
[Wu, Ping] Inst High Performance Comp, Singapore 138632, Singapore.
[Pelton, Arthur] Ecole Polytech, CRCT, Dept Chem Engn, Montreal, PQ H3C 3A7,
Canada.
C3 McGill University; Agency for Science Technology & Research (A*STAR);
A*STAR - Institute of High Performance Computing (IHPC); Universite de
Montreal; Polytechnique Montreal
RP Jung, IH (corresponding author), McGill Univ, Dept Min & Mat Engn, HW Wong
Bldg,3610 Univ St, Montreal, PQ H3A 2B2, Canada.
EM in-ho.jung@mcgill.ca
RI Wu, Ping/AAX-3767-2020; Jung, In-Ho/H-6838-2018
OI Wu, Ping/0000-0002-0788-6268; Jung, In-Ho/0000-0002-9744-7276
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NR 42
TC 75
Z9 85
U1 3
U2 41
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2009
VL 49
IS 9
BP 1290
EP 1297
PG 8
GA 498HC
UT WOS:000270127000003
OA gold
DA 2023-12-05
ER
PT J
AU Gil, A
Korili, SA
AF Gil, A.
Korili, S. A.
TI Management and valorization of aluminum saline slags: Current status and
future trends
LA English
DT Review
DE Aluminum saline slag; Industrial waste valorization; Nonmetallic
products; High-value-added product
ID SALT CAKE; HAZARDOUS-WASTE; CEMENT MORTARS; DROSS; RECOVERY; BEHAVIOR;
ALPO4-5
AB The current situation as regards the management and valorization of aluminum
saline slags, also known as aluminum salt cake or salt slag, is reviewed in this
work. Aluminum saline slags are produced by the secondary aluminum industry and
formed during the aluminum scrap/dross melting processes. The amount of saline slag
generated in these operations can vary between 30% and 60% of the metal produced,
that is, between 300 and 600 kg per ton of aluminum produced. This waste contains
about 3-9 wt.% metallic aluminum, 20-50 wt.% oxides, such as aluminum oxide (also
referred to as nonmetallic products), 20-75 wt.% flux brines, and other components
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saline slags are classified as hazardous waste and are included in the European
List of Wastes, which means that they must be deposited in landfills or in secure
deposits. Similarly, salt cake is a byproduct which could be recovered provided the
process is economically viable. Direct applications such as inert filling for
construction, road paving, morter components, aluminum salts, inert filler in
polymer composites, adsorbents, mineral wood, have been reported. Aluminum, by
chemical dissolution from the nonmetallic fraction, can also be recovered as a
high-value-added product and used to synthesize materials such as pure alumina,
salts, and hydroxides. This work reviews current methods for treating saline slags,
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(C) 2015 Elsevier B.V. All rights reserved.
C1 [Gil, A.; Korili, S. A.] Univ Publ Navarra, Dept Appl Chem, Los Acebos
RP Gil, A (corresponding author), Univ Publ Navarra, Dept Appl Chem, Los Acebos
FU Seventh Framework Programme through project RecycAl
FX This work was funded by Seventh Framework Programme through the project
RecycAl.
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NR 68
TC 74
Z9 75
U1 6
U2 101
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD APR 1
PY 2016
VL 289
BP 74
EP 84
DI 10.1016/j.cej.2015.12.069
PG 11
SC Engineering
GA DF7TG
UT WOS:000371559900009
DA 2023-12-05
ER
PT J
AU Ye, JY
Zhang, WS
Shi, D
AF Ye, Jiayuan
Zhang, Wensheng
Shi, Di
TI Effect of elevated temperature on the properties of geopolymer
synthesized from calcined ore-dressing tailing of bauxite and
ground-granulated blast furnace slag
LA English
DT Article
DE Geopolymer; Bauxite; Ore-dressing tailing; Slag; Elevated temperature;
Linear length; Strength; Porosity; Crystallization
ID C-S-H; THERMAL-BEHAVIOR; FLY-ASH; METAKAOLIN GEOPOLYMERS; EVOLUTION;
STRENGTH; EXPOSURE; PERFORMANCE; TECHNOLOGY; CONCRETE
AB A geopolymer was prepared using calcined ore-dressing tailing of bauxite and
ground-granulated blast furnace slag. To explore the effect on its properties of
heating the geopolymer to 1200 degrees C, the physical evolutions, including the
appearance, length, compressive strength and porosity, and the chemical processes
involving the decomposition and crystallization of specimens after heating were
investigated. After exposure to elevated temperatures up to 1000 degrees C, the
studied geopolymer mortars exhibited the following changes. The linear length
initially showed shrinkage, responding to free water loss and gel dehydration, and
then, it exhibited expansion, resulting from a volume increase due to the
displacive and reconstructive phase transition of quartz in the mortars. The
compressive strength of the mortars decreased due to the increasing cracks and
porosity arising from the dehydration, dehydroxylation and thermal mismatch between
the contracting gels and expanding quartz. Additional conversion of the X-ray
amorphous gels, which exhibit excellent thermal stability below 800 degrees C, into
such crystalline phases as calcium aluminum oxide and anorthite (CaAl2(SiO4)(2))
was found at 1000 degrees C, resulting in a severe deterioration of strength and a
reduction of approximately 40.0 MPa. After exposure to 1200 degrees C, a strength
gain was observed as a result of the densification and self-healing caused by the
viscous sintering and the formation of ceramic phases, such as anorthite (sodian,
ordered, (Ca,Na)(Al,Si)(2)Si2O8). (C) 2014 Elsevier Ltd. All rights reserved.
C1 [Ye, Jiayuan; Zhang, Wensheng; Shi, Di] China Bldg Mat Acad, State Key Lab Green
Bldg Mat, Beijing 100024, Peoples R China.
RP Zhang, WS (corresponding author), China Bldg Mat Acad, State Key Lab Green Bldg
Mat, 1 Guanzhuang Dongli Chaoyang Dist, Beijing 100024, Peoples R China.
EM wensheng_zhang01@163.com
FU National High Technology Research and Development Program ("863"
Program) of China [2009AA03Z506]; National Natural Science Foundation of
China [51102222]
FX The financial help of the National High Technology Research and
Development Program ("863" Program) of China (Project No. 2009AA03Z506)
and National Natural Science Foundation of China (Project No. 51102222)
is gratefully acknowledged.
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NR 37
TC 74
Z9 84
U1 6
U2 97
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 30
PY 2014
VL 69
BP 41
EP 48
DI 10.1016/j.conbuildmat.2014.07.002
PG 8
GA AQ1NU
UT WOS:000342548900006
DA 2023-12-05
ER
PT J
AU Park, JH
Kang, YB
AF Park, Joo Hyun
Kang, Youn-Bae
TI Effect of ferrosilicon addition on the composition of inclusions in
16Cr-14Ni-Si stainless steel melts
LA English
DT Article
ID DEOXIDATION EQUILIBRIUM; AL DEOXIDATION; LIQUID-IRON; FE-NI; SI;
ALUMINUM; SLAGS; THERMODYNAMICS; TEMPERATURES; ALLOYS
AB The silicon deoxidation equilibrium between the 16Cr-14Ni-1.5Mn-Si melts and the
CaO-SiO2-8MgO-5CaF(2) (basicity = 1.8) slag at 1743 K was investigated to
understand the effect of aluminum and silicon contents on the composition of
inclusions. Therefore, the ferrosilicon alloys with different aluminum content were
chosen based on the preceding objective. In addition, the phase stability diagram
of the inclusions was computed using commercial thermodynamic software based on the
Gibbs energy minimization principles. The content of MnO in the inclusions sharply
decreases with increasing silicon content when the steel melts were deoxidized by
the ferrosilicon alloys containing high aluminum (FeSi-H). The content Of SiO2 in
the inclusions slightly increases with increasing silicon content when the FeSi-L
is used, while a maximum value is shown at [Si] = 1.5 pct when the FeSi-H is used.
The content of MgO in the inclusions increases by increasing the content of
silicon, regardless of the kinds of ferrosilicon alloys. The use of the FeSi-L as a
deoxidizer could suppress the formation of Al2O3 in the inclusions, while the
content of Al2O3 increases with increasing silicon content when the FeSi-H is used.
When the FeSi-H is used as a deoxidizer, the inclusions are the glassy type with
the composition of Mn-silicates at [Si] <= 1.3 pct, while the Mg(Ca)-silicates with
the composition of the forsterite phase are observed in the steel composition of
[Si] = 3.3 pct. When the steel melts were deoxidized by the FeSi-L alloys, the
inclusions are the glassy-type Mn-silicates at [Si] = 0.8 pct, while the Mn-
silicates containing the cristobalite phase are observed at [Si] = 1.5 to 2.4 pct.
In the composition of [Si] = 3.3 pct, the Mg-silicates with the composition of the
rhodonite phase are observed. The log(X-SiO2/X-MnO) of the inclusions linearly
increases by increasing the log [a(Si) . a(O) / a(Mn)] with the slope close to
unity when the FeSi-L is used as a deoxidizer, while the slope of the line is about
2 times greater than that of the expected value when FeSi-H is used. The log (X-
MgO/X-MnO) of the inclusions linearly increases by increasing the log [a(Mg)/a(Mn)]
with slopes greater than the expected value of unity.
C1 POSCO, Tech Res Labs, Stainless Steel Res Grp, Pohang 790785, South Korea.
C3 POSCO
RP Park, JH (corresponding author), POSCO, Tech Res Labs, Stainless Steel Res Grp,
RI Kang, Youn-Bae/AAU-5544-2021
OI Kang, Youn-Bae/0000-0003-0615-0168
CR *19 COMM STEELM, 1988, STEELM DAT SOURC JAP, P273
Choi CH, 2004, METALL MATER TRANS B, V35, P115, DOI 10.1007/s11663-004-0101-x
MEHTA SR, 1965, J IRON STEEL I, V203, P524
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10.2355/tetsutohagane1955.89.12_1183
TODOROKI H, 2001, 2001 STEELMAKING C P, P331
[No title captured]
[No title captured]
NR 21
TC 74
Z9 80
U1 0
U2 25
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD OCT
PY 2006
VL 37
IS 5
BP 791
EP 797
DI 10.1007/s11663-006-0061-4
PG 7
Engineering
GA 089YD
UT WOS:000240916900010
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Ahmed, IM
Nayl, AA
Daoud, JA
AF Ahmed, I. M.
Nayl, A. A.
Daoud, J. A.
TI Leaching and recovery of zinc and copper from brass slag by sulfuric
acid
SO JOURNAL OF SAUDI CHEMICAL SOCIETY
LA English
DT Article
DE Recovery; Brass slag; Zinc; Copper; H2SO4 leaching
ID HYDROMETALLURGICAL TREATMENT; DUST
AB Leaching and recovery processes for zinc and copper from brass slag by sulfuric
acid were carried out and iron and aluminum were also precipitated as hydroxides in
addition to silica gel. The factors affecting the performance and efficiency of the
leaching process; such as agitation rate, leaching time, acid concentration and
temperature were separately investigated. The results obtained revealed that zinc
and copper are successfully recovered from these secondary resources, where the
percent recovery amounts to 95% and 99% for zinc and copper, respectively. The
experimental data of this leaching process were well interpreted with the shrinking
core model under chemically controlled processes. The apparent activation energy
for the leaching of zinc has been evaluated using the Arrhenius expression. Based
on the experimental results, a separation method and a flow sheet were developed
and tested to separate zinc, copper, iron, aluminum and silica gel from the brass
slag. (C) 2012 Production and hosting by Elsevier B.V. on behalf of King Saud
University. This is an open access article under the CC BY-NC-ND license
(http://creativecommons.org/licenses/by-nc-nd/4.0/).
C1 [Ahmed, I. M.; Nayl, A. A.; Daoud, J. A.] Atom Energy Author, Hot Labs Ctr,
Cairo 13759, Egypt.
[Nayl, A. A.] Atom Energy Author, Hot Labs Ctr, PO 13759, Cairo, Egypt.
[Nayl, A. A.] Al Jouf Univ, Dept Chem, Coll Sci, Sakakh 2014, Saudi Arabia.
C3 Egyptian Knowledge Bank (EKB); Egyptian Atomic Energy Authority (EAEA);
Egyptian Knowledge Bank (EKB); Egyptian Atomic Energy Authority (EAEA);
Al Jouf University
RP Nayl, AA (corresponding author), Atom Energy Author, Hot Labs Ctr, Cairo 13759,
Egypt.; Nayl, AA (corresponding author), Atom Energy Author, Hot Labs Ctr, PO
13759, Cairo, Egypt.; Nayl, AA (corresponding author), Al Jouf Univ, Dept Chem,
Coll Sci, Sakakh 2014, Saudi Arabia.
EM aanayl@yahoo.com
RI Braese, Stefan/B-9057-2008; Nayl, AbdElAziz A./U-8246-2018
OI Braese, Stefan/0000-0003-4845-3191; Nayl, AbdElAziz
A./0000-0003-0531-5194
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1
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NR 18
TC 73
Z9 73
U1 0
U2 17
PI AMSTERDAM
SN 1319-6103
EI 2212-4640
J9 J SAUDI CHEM SOC
JI J. Saudi Chem. Soc.
PD SEP
PY 2016
VL 20
SU 1
BP S280
EP S285
DI 10.1016/j.jscs.2012.11.003
PG 6
WC Chemistry, Multidisciplinary
SC Chemistry
GA EO0FL
UT WOS:000396373600037
OA gold
DA 2023-12-05
ER
PT J
AU Ryu, HG
Zhang, ZT
Cho, JW
Wen, GH
Sridhar, S
AF Ryu, H. G.
Zhang, Z. T.
Cho, J. W.
Wen, G. H.
Sridhar, S.
TI Crystallization Behaviors of Slags through a Heat Flux Simulator
LA English
DT Article
DE mold slag; TRIP steel; crystallization behavior; heat flux
ID MOLD; TRANSFORMATION; POWDERS
AB This paper investigates how the basicity and alumina content in synthetic slags
influence the crystallization behavior that takes place in a heat flux simulator
for mold slags. The purpose is to elucidate the variation in crystallization
behavior for model slags that are expected to be glassy, partly crystalline and
fully crystalline in order to correlate the changes in heat flux to the dynamic
solid evolution that occurs in the simulator. Three levels of alumina content (3,
15 and 25 wt%) were chosen to investigate the heat transfer behavior through slag
film which have different tendency of reaction with molten steel during continuous
casting of high aluminum containing Transformation Induced Plasticity (TRIP)
steels. A Confocal Scanning Laser Microscopy (CSLM) was used to develop TTT
diagrams for the slags. XRD and SEM were also used to analyze the micro-structures
of the crystalline phases.
The measured heat fluxes through the mold slags tested were found to increase,
as the crystallinity of the slag film decreased with decreasing basicity and
alumina content. It was found that the crystallization temperature increased, while
the incubation time for crystallization decreases with increasing basicity and
alumina content. The increase in alumina content induced the precipitation of CaF2
during cooling process and hence a change in the crystalline phase from Ca4Si2O7F2
to Ca2Al2SiO7.
C1 [Ryu, H. G.; Zhang, Z. T.; Sridhar, S.] Carnegie Mellon Univ, Dept Mat Sci &
Engn, Pittsburgh, PA 15213 USA.
[Zhang, Z. T.] Peking Univ, Coll Engn, Dept Energy & Recourses Engn, Beijing
[Ryu, H. G.; Cho, J. W.] POSCO, Cheonnam 547711, South Korea.
[Wen, G. H.] Chongqing Univ, Coll Mat Sci & Engn, Dept Met, Chongqing 400044,
Peoples R China.
C3 Carnegie Mellon University; Peking University; Chongqing University
RP Ryu, HG (corresponding author), Carnegie Mellon Univ, Dept Mat Sci & Engn,
EM zuotaizhang@coe.pku.edu.cn; sridhars@andrew.cmu.edu
RI Zhang, Zuotai/B-1030-2012; Cho, Jung-Wook/A-8142-2013
OI Zhang, Zuotai/0000-0002-3580-6018; Cho, Jung-Wook/0000-0003-2364-1938
FU Center for Iron and Steelmaking Research, Carnegie Mellon University
(CISR); National Natural Science Foundation of China [50902003];
National Basic Research Program (2007CB613608) [2007CB613608]
FX Financial supports from the Center for Iron and Steelmaking Research,
Carnegie Mellon University (CISR) and from National Natural Science
Foundation of China (50902003) as well as The National Basic Research
Program (2007CB613608) are gratefully acknowledged.
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NR 33
TC 73
Z9 80
U1 1
U2 20
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2010
VL 50
IS 8
BP 1142
EP 1150
PG 9
GA 644BI
UT WOS:000281345000012
OA gold
DA 2023-12-05
ER
PT J
AU Boccaccini, AR
Hamann, B
AF Boccaccini, AR
Hamann, B
TI In situ high-temperature optical microscopy
LA English
DT Review
ID GLASS-POWDER COMPACTS; MATRIX COMPOSITES; HOT-STAGE; ANISOTROPIC
SHRINKAGE; SINTERING SHRINKAGE; CERAMIC COMPOSITE; MOLTEN ALUMINUM;
DENSIFICATION; WETTABILITY; KINETICS
AB High-temperature optical microscopy is an essential in situ characterisation and
monitoring technique with wide applications in different areas of materials
science. The devices used include commercial available instruments, known as
heating microscopes, and custom-made devices, usually called "high-temperature
processing microscopes'' or "thermo-optical instruments''. The different areas of
applications of high-temperature optical microscopy are discussed on the basis of
practical examples drawn from the literature. Besides the classical use of the
technique to study the melting and softening behaviour of glass, slags, ashes and
other silicate and ceramic materials, this review covers alternative applications,
in particular the use of heating microscopes as "optical dilatometers'' to
investigate the sintering kinetics of powder compacts. In this regard, the
advantages of the technique over conventional dilatometry are emphasised. A variety
of custom-made devices is described, developed to investigate particular problems,
such as delamination and curling of laminate composites during densification,
cosintering of multilayer metal-ceramic and ceramic-ceramic systems, and wetting
behaviour of liquid phases on rigid substrates. As a particular example of such a
custom-made equipment, a novel, multi-purpose high-temperature processing
microscope is described, and its application potential, which is well beyond that
of commercial devices, is outlined. This instrument is unique in that it combines
both vertical and horizontal sample observation capability, as well as the
possibility to investigate samples of relatively large sizes (65 mm(3)), i.e. about
10 times larger than those suitable for commercial heating microscopes. (C) 1999
Kluwer Academic Publishers.
C1 Tech Univ Ilmenau, Inst Werkstofftech, D-98684 Ilmenau, Germany.
C3 Technische Universitat Ilmenau
RP Boccaccini, AR (corresponding author), Tech Univ Ilmenau, Inst Werkstofftech, D-
98684 Ilmenau, Germany.
RI Boccaccini, Aldo R./N-9782-2019; Boccaccini, Aldo R/C-7905-2013
OI Boccaccini, Aldo R./0000-0002-7377-2955;
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NR 126
TC 73
Z9 76
U1 1
U2 53
PU KLUWER ACADEMIC PUBL
PI DORDRECHT
PA SPUIBOULEVARD 50, PO BOX 17, 3300 AA DORDRECHT, NETHERLANDS
SN 0022-2461
J9 J MATER SCI
JI J. Mater. Sci.
PD NOV
PY 1999
VL 34
IS 22
BP 5419
EP 5436
DI 10.1023/A:1004706922530
PG 18
GA 244RQ
UT WOS:000083064900001
DA 2023-12-05
ER
PT J
AU Yang, J
Hu, HC
He, XY
Su, Y
Wang, YB
Tan, HB
Pan, H
AF Yang, Jin
Hu, Huachao
He, Xingyang
Su, Ying
Wang, Yingbin
Tan, Hongbo
Pan, Han
TI Effect of steam curing on compressive strength and microstructure of
high volume ultrafine fly ash cement mortar
LA English
DT Article
DE Wet-grinding; Ultrafine fly ash; Steam curing; Compressive strength;
Microstructure
ID DELAYED ETTRINGITE FORMATION; BLAST-FURNACE SLAG; PORE STRUCTURE;
HYDRATION CHARACTERISTICS; LITHIUM SLAG; NANO-SILICA; CONCRETE;
TEMPERATURE; FINENESS; PRODUCTS
AB Utilization of high volume fly ash is generally limited in steam-cured concrete
products due to the delayed strength development. In present work, ultrafine fly
ash (UFA) with a median particle size of 2.3 um was prepared with wet-grinding
technology. The influence of different FA fineness, UFA content (30-70%) and curing
regimes on the compressive strength and microstructure of steam-cured high volume
fly ash cement composites were studied. Both the early and late compressive
strength of steamcured FA blended composites were enhanced by wet-milled UFA with
replacement level as high as 50%, and the strength was even higher than that of
pure cement group. Pore structure of steam-cured high volume FA blended composites
was effectively refined by UFA. The amount of CH after steam curing was generally
lower than that with standard curing. Furthermore, the main chain length and Al/Si
of C-S-H gels under steam curing were improved by UFA. Compared with prolonging the
curing duration, increasing the curing temperature seems more efficient for the
incorporation of aluminum from fly ash into the calcium silicate hydrates. (C) 2020
C1 [Yang, Jin; Hu, Huachao; He, Xingyang; Su, Ying; Wang, Yingbin] Hubei Univ
Technol, Sch Civil Engn Architecture & Environm, Wuhan 430068, Peoples R China.
[Yang, Jin; He, Xingyang; Su, Ying; Wang, Yingbin] Hubei Univ Technol, Bldg
Waterproof Engn & Technol Res Ctr Hubei Prov, Wuhan 430068, Peoples R China.
[Tan, Hongbo] Wuhan Univ Technol, State Key Lab Silicate Mat Architecture, Wuhan
[Pan, Han] China Construct Third Bur Green Ind Investment Co, Wuhan 430100,
Peoples R China.
C3 Hubei University of Technology; Hubei University of Technology; Wuhan
Environm, Wuhan 430068, Peoples R China.
EM hexycn@163.com
RI cheng, shu/IZE-4788-2023
OI Yang, Jin/0000-0002-5332-7862
FU National Key Research and Development Program of China [2019YFC1907103];
Major Technology Innovation of Hubei Province [2019ACA146]; Natural
Science Foundation of Hubei Province [2019CFB170]
FX The authors would like to acknowledge the help of Mr. C. Zhang (Graduate
student, Hubei Univ. Technol.) for the assistance during the
experiments. The authors also like to acknowledge the National Key
Research and Development Program of China (2019YFC1907103), the Major
Technology Innovation of Hubei Province (2019ACA146) and the Natural
Science Foundation of Hubei Province (2019CFB170).
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NR 61
TC 72
Z9 73
U1 10
U2 84
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JAN 10
PY 2021
VL 266
AR 120894
DI 10.1016/j.conbuildmat.2020.120894
PN A
PG 13
GA PI0LU
UT WOS:000600793000013
DA 2023-12-05
ER
PT J
AU Song, H
Jeong, Y
Bae, S
Jun, Y
Yoon, S
Oh, JE
AF Song, Haemin
Jeong, Yeonung
Bae, Sungchul
Jun, Yubin
Yoon, Seyoon
Oh, Jae Eun
TI A study of thermal decomposition of phases in cementitious systems using
HT-XRD and TG
LA English
DT Article
DE Thermal decomposition; TG; HT-XRD; Cementitious; GGBFS
ID STRENGTH DEVELOPMENT; FLY-ASH; TEMPERATURE; HYDRATION; ALUMINUM; LIME;
CAO
AB Significant variations have been reported on the temperature range of thermal
decomposition of cementitious phases. Thus, this study identified temperature
ranges on the phases in actual cementitious systems (portland cement (OPC) pastes,
blended pastes of ground granulated blast furnace slag (GGBFS) with OPC, and Ca(OH)
(2)-activated GGBFS) by simultaneously using thermogravimetry (TG) and high-
temperature X-ray diffraction (HT-XRD) as follows: (1) 81 degrees-91 degrees C for
dehydration of ettringite, (2) similar to 80 degrees-240 degrees C for major
dehydration of C-S-H, (3) similar to 241 degrees-244 degrees C for hydrogarnet, (4)
similar to 129 degrees-138 degrees C for Al2O3-Fe2O3-mono phase (AFm), (5) similar
to 411 degrees-427 degrees C for Ca(OH)(2), and (6) similar to 648 degrees-691
degrees C for CaCO3. The CaO layers and SiO2 chains of C-S-H likely started to
decompose from 615 degrees-630 degrees C, and eventually transformed to new
crystalline phases. This study also demonstrated that (a) the quantity of calcite
could be overestimated due to additional carbonation when Ca(OH)(2) is plentifully
present in samples, and (b) the quantification of phases would be greatly affected
by sample particle size when GGBFS is used in the system. (C) 2018 Elsevier Ltd.
C1 [Song, Haemin; Jeong, Yeonung; Jun, Yubin; Yoon, Seyoon; Oh, Jae Eun] Ulsan Natl
Inst Sci & Technol UNIST, Sch Urban & Environm Engn, UNIST Gil 50, Ulsan 689798,
South Korea.
[Bae, Sungchul] Hanyang Univ, Dept Architectural Engn, Seoul 04763, South Korea.
[Yoon, Seyoon] Kyonggi Univ, Dept Civil Engn, Suwon 16227, South Korea.
C3 Ulsan National Institute of Science & Technology (UNIST); Hanyang
University; Kyonggi University
RP Yoon, S; Oh, JE (corresponding author), Ulsan Natl Inst Sci & Technol UNIST, Sch
Urban & Environm Engn, UNIST Gil 50, Ulsan 689798, South Korea.; Yoon, S
(corresponding author), Ulsan Natl Inst Sci & Technol UNIST, Sch Urban & Environm
Engn, Ulsan 44919, South Korea.
EM yoonseyoon@kyonggi.ac.kr; ohjaeeun@unist.ac.kr
RI Jeong, Yeonung/J-5598-2014; Bae, Sungchul/AFO-4083-2022; Yoon,
Seyoon/N-5936-2014
OI Jeong, Yeonung/0000-0002-1956-9577; Bae, Sungchul/0000-0002-8511-6939;
Yoon, Seyoon/0000-0002-3451-5518; Song, Haemin/0000-0003-2760-400X
FU National Research Foundation of Korea (NRF) - Ministry of Education,
Republic of Korea [NRF-2016R1D1A1B03932908, NRF-2016R1D1A1B03934007];
NRF-Global Ph.D. Fellowship Program through the National Research
Foundation of Korea (NRF) - Ministry of Education, Republic of Korea;
National Research Foundation of Korea [2016R1D1A1B03934007,
2016R1D1A1B03932908, 2017H1A2A1046371, 22A20152613333] Funding Source:
FX This study was supported by the Basic Science Research Programs
(NRF-2016R1D1A1B03932908 and NRF-2016R1D1A1B03934007) and
NRF-2017-Global Ph.D. Fellowship Program through the National Research
Foundation of Korea (NRF), funded by the Ministry of Education, Republic
of Korea.
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TC 71
Z9 72
U1 1
U2 53
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD APR 30
PY 2018
VL 169
BP 648
EP 661
DI 10.1016/j.conbuildmat.2018.03.001
PG 14
GA GE1RP
UT WOS:000430994700063
DA 2023-12-05
ER
PT J
AU Ogundiran, MB
Nugteren, HW
Witkamp, GJ
AF Ogundiran, M. B.
Nugteren, H. W.
Witkamp, G. J.
TI Immobilisation of lead smelting slag within spent aluminate-fly ash
based geopolymers
LA English
DT Article
DE Lead smelting slag; Aluminium etching solution; Geopolymer; Coal fly
ash; Immobilisation
ID INORGANIC POLYMERS; CONTAMINATED SOILS; HEAVY-METALS; PART II;
REMEDIATION; WASTE; PB; TECHNOLOGY; STRENGTH; MATRICES
AB This study presents the solidification/stabilisation and immobilisation of lead
smelting slag (LSS) by its incorporation in coal fly ash - blast furnace slag based
geopolymers. It also explores the use of a spent aluminium etching solution (AES)
as geopolymer activator instead of the commonly used silicate solutions. The
compressive strength of the geopolymers produced with the AES was lower than when
applying a K-silicate solution as activator (100 MPa versus 80 MPa after 28 days).
Compressive strength was not affected when up to 10% of the FA was replaced by LSS.
NEN 12457-4, TCLP, SPLP and NEN 7375 leaching tests indicated that mobile Pb from
LSS was highly immobilised. The diffusion leaching test NEN 7375 revealed exceeding
of the Dutch Soil Quality Regulation threshold limits only for Se and Sb. On the
condition that the remaining excess leaching can be reduced by further refinement
of the mixture recipes, the proposed process will have the potential of producing
waste-based construction materials that may be applied under controlled conditions
in specific situations. (C) 2012 Elsevier B.V. All rights reserved.
C1 [Ogundiran, M. B.; Nugteren, H. W.] Delft Univ Technol, Dept Chem Engn, Prod &
Proc Engn Grp, NL-2628 BL Delft, Netherlands.
[Witkamp, G. J.] Delft Univ Technol, Dept Biotechnol, NL-2628 BC Delft,
Netherlands.
C3 Delft University of Technology; Delft University of Technology
RP Ogundiran, MB (corresponding author), Univ Ibadan, Dept Chem, Ibadan, Nigeria.
EM mbogundiran@yahoo.com; h.w.nugteren@tudelft.nl; g.j.witkamp@tudelft.nl
FU Organisation for Prohibition of Chemical Weapons (OPCW)
FX The financial support of the Organisation for Prohibition of Chemical
Weapons (OPCW) is highly acknowledged. The authors thank the Dutch
Aluminium Anodising Company ALUMET BV for providing the spent etching
solutions. Michel van den Brink (Delft University of Technology,
Department of Process and Energy) is acknowledged for performing the ICP
analyses.
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TC 71
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U1 2
U2 97
PI AMSTERDAM
SN 0304-3894
J9 J HAZARD MATER
PD MAR 15
PY 2013
VL 248
BP 29
EP 36
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PG 8
GA 124DK
UT WOS:000317443800003
PM 23339881
DA 2023-12-05
ER
PT J
AU DUTRE, V
VANDECASTEELE, C
AF DUTRE, V
VANDECASTEELE, C
TI SOLIDIFICATION STABILIZATION OF HAZARDOUS ARSENIC-CONTAINING WASTE FROM
A COPPER REFINING PROCESS
LA English
DT Article
ID BARIUM ARSENATE; SOLUBILITY
AB An industrial waste, originating from a metallurgical process in which copper is
refined and containing large amounts of arsenic (42 wt%), was studied. A suitable
treatment method, solidification/stabilisation (S/S), allowing a reduction of the
leachability of arsenic from the waste was studied and optimised by measurement of
the influence of all additives (waste acid, blast-furnance slag, slaked lime,
cement) used in the process. The S/S process could thus be simplified
considerably. The addition of lime to the waste was the most important factor in
reducing the arsenic concentration in the leachate by formation of a hardly soluble
calcium-arsenic compound. To reduce the arsenic concentration in the leachate even
further, by formation of other insoluble compounds, the addition of aluminium and
barium salts was investigated.
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VLAREM I BESLUIT VLA
[No title captured]
NR 11
TC 71
Z9 82
U1 0
U2 18
PI AMSTERDAM
SN 0304-3894
J9 J HAZARD MATER
PD JAN
PY 1995
VL 40
IS 1
BP 55
EP 68
DI 10.1016/0304-3894(94)00080-Z
PG 14
GA QB289
UT WOS:A1995QB28900005
DA 2023-12-05
ER
PT J
AU Martins, ACP
de Carvalho, JMF
Costa, LCB
Andrade, HD
de Melo, TV
Ribeiro, JCL
Pedroti, LG
Peixoto, RAF
AF Martins, Ana Carolina Pereira
de Carvalho, Jose Maria Franco
Costa, Lafs Cristina Barbosa
Andrade, Humberto Dias
de Melo, Taina Varela
Ribeiro, Jose Carlos Lopes
Pedroti, Leonardo Goncalves
Peixoto, Ricardo Andre Fiorotti
TI Steel slags in cement-based composites: An ultimate review on
characterization, applications and performance
LA English
DT Review
DE Steel slag; Cement-based composites; Basic oxygen furnace slag (BOFS);
Electric arc furnace slag (EAFS); Recycled aggregates; Supplementary
cementitious material (SCM)
ID BASIC OXYGEN FURNACE; SELF-COMPACTING CONCRETE; MECHANICAL-PROPERTIES;
BLAST-FURNACE; BOF SLAG; COARSE AGGREGATE; FINE AGGREGATE; STRUCTURAL
CHARACTERISTICS; ACCELERATED CARBONATION; DIMENSIONAL STABILITY
AB Steel slags are by-products generated in high volumes in the steel industry.
Their main constituents are calcium, silicon, ferric, aluminum, and magnesium
oxides. Larnite, alite, brownmillerite, and ferrite are also found. The presence of
expansive compounds cause concern when used in cement-based compos-ites; however,
mitigating routes have been proposed. Activation techniques improve the binding
proper-ties of steel slag powder, potentiating its use as a supplementary
cementitious material (SCM). As an aggregate, steel slag presents good
morphological and mechanical properties. Promising mechanical and durability
performances in cement-based composites encourage further research to promote the
use of steel slag.
(c) 2021 Elsevier Ltd. All rights reserved.
C1 [Martins, Ana Carolina Pereira; de Carvalho, Jose Maria Franco; Ribeiro, Jose
Carlos Lopes] Univ Fed Vicosa, Dept Civil Engn, Lab Composite Mat, BR-36570900
Vicosa, MG, Brazil.
[Costa, Lafs Cristina Barbosa; Andrade, Humberto Dias; de Melo, Taina Varela;
Peixoto, Ricardo Andre Fiorotti] Univ Fed Ouro Preto, Dept Civil Engn, Lab
Construct Mat, BR-35400000 Ouro Preto, MG, Brazil.
[Pedroti, Leonardo Goncalves] Univ Fed Vicosa, Dept Civil Engn, Lab Construct
Mat, BR-36570900 Vicosa, MG, Brazil.
C3 Universidade Federal de Vicosa; Universidade Federal de Ouro Preto;
Universidade Federal de Vicosa
RP Martins, ACP (corresponding author), Univ Fed Vicosa, Dept Civil Engn, Lab
Composite Mat, BR-36570900 Vicosa, MG, Brazil.
EM ana.martins5@ufv.br; josemaria.carvalho@ufv.br;
lais.cristina.costa@gmail.com; andrade.hdias@gmail.com;
tainavarela@hotmail.com; jcarlos.ribeiro@ufv.br;
leonardo.pedroti@ufv.br; fiorotti.ricardo@gmail.com
RI Franco de Carvalho, José Maria/HCI-3711-2022; Ribeiro,
José/AAD-6064-2021; Fiorotti, Ricardo/R-8399-2019; Franco de Carvalho,
José Maria/AHE-7855-2022; Pereira Martins, Ana Carolina/HTQ-3478-2023
OI Franco de Carvalho, José Maria/0000-0001-5785-3213;
FU Coordencao de Aperfeicoamento de Pessoal de Nivel Superior - Brasil
(CAPES) [001]; Fundacao de Amparo a Pesquisa do Estado de Minas Gerais
(FAPEMIG); Conselho Nacional de Desenvolvimento Cientifico e Tecnologico
(CNPq); Federal University of Vicosa (UFV); Federal University of Ouro
Preto (UFOP)
FX This study was financed in part by the Coordencao de Aperfeicoamento de
Pessoal de Nivel Superior -Brasil (CAPES) Finance code 001. The authors
also acknowledge the support provided by the Fundacao de Amparo a
Pesquisa do Estado de Minas Gerais (FAPEMIG), Conselho Nacional de
Desenvolvimento Cientifico e Tecnologico (CNPq), Federal University of
Vicosa (UFV) and Federal University of Ouro Preto (UFOP). Thanks are
also due to the Brazilian research groups SICon-CNPq/UFV and
RECICLOSCNPq/UFOP for the infrastructure and collaboration.
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PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUL 12
PY 2021
VL 291
AR 123265
DI 10.1016/j.conbuildmat.2021.123265
EA APR 2021
PG 19
GA SQ3XD
UT WOS:000660288600001
DA 2023-12-05
ER
PT J
AU Dai, XD
Aydin, S
Yardimci, MY
Lesage, K
De Schutter, G
AF Dai, Xiaodi
Aydin, Serdar
Yardimci, Mert Yucel
Lesage, Karel
De Schutter, Geert
TI Effects of activator properties and GGBFS/FA ratio on the structural
build-up and rheology of AAC
LA English
DT Article
DE Alkali activated cement (D); Ground blast-furnace slag (D); Fly ash (D);
Rheology (A); Pore solution (B); Structural build-up
ID AGE REACTION-KINETICS; BLAST-FURNACE SLAG; FLY-ASH; MICROSTRUCTURAL
DEVELOPMENT; CEMENTITIOUS MATERIALS; STRENGTH PROPERTIES; HYDRATION
KINETICS; INORGANIC POLYMER; SILICATE HYDRATE; PART II
AB The effects of ground granulated blast furnace slag/fly ash (GGBFS/FA) ratio,
mass ratio of SiO2 to Na2O (M s ) of activator solution and sodium silicate dosage
on structural build-up, flow properties and setting characteristics of alkali-
activated cement (AAC) mixtures were investigated. The solid-like behavior becomes
more dominant with increasing GGBFS/FA ratio. M, value had significant effect on
the structural build-up. Significantly higher initial storage modulus with a low
increasing rate was observed for the M, values lower than 0.8. However, for higher
M, values, a sudden increase in storage modulus was observed after negligible
initial structuration. An increase in sodium silicate dosage caused a considerable
delay in the abrupt increase in the structural formation. It was observed that flow
curves of AAC fit the Herschel-Bulkley model with shear-thickening behavior. ICP-
OES tests revealed the lower release of aluminum and calcium into the pore solution
of GGBFS/FA mixtures with low M, values.
C1 [Dai, Xiaodi; Aydin, Serdar; Yardimci, Mert Yucel; Lesage, Karel; De Schutter,
Geert] Univ Ghent, Magnel Vandepitte Lab, Dept Struct Engn & Bldg Mat, Ghent,
Belgium.
[Aydin, Serdar] Dokuz Eylul Univ, Dept Civil Engn, TR-35160 Izmir, Turkey.
[Yardimci, Mert Yucel] Istanbul Okan Univ, Dept Civil Engn, Tuzla Campus, TR-
34959 Istanbul, Turkey.
C3 Ghent University; Dokuz Eylul University; Okan University
RP De Schutter, G (corresponding author), Univ Ghent, Magnel Vandepitte Lab, Dept
Struct Engn & Bldg Mat, Ghent, Belgium.; Aydin, S (corresponding author), Dokuz
Eylul Univ, Dept Civil Engn, TR-35160 Izmir, Turkey.
EM serdar.aydin@deu.edu.tr; Geert.DeSchutter@Ugent.be
RI Yardimci, Mert Yucel/AAN-8109-2021; Dai, Xiaodi/HNC-1504-2023; Yardimci,
Mert/AAD-1942-2021; aydın, serdar/AAA-2821-2022
FU FWO-EOS [30439691]
FX This paper is the result of research actions performed in the framework
of the FWO-EOS project 30439691 'INTERdisciplinary multiscale Assessment
of a new generation of Concrete with alkali-activated maTerials'
(INTERACT). The financial support by FWO-EOS is gratefully acknowledged.
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PI OXFORD
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EI 1873-3948
JI Cem. Concr. Res.
PD DEC
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AR 106253
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PG 14
GA OS1BY
UT WOS:000589900300014
DA 2023-12-05
ER
PT J
AU Alam, S
Das, SK
Rao, BH
AF Alam, Shamshad
Das, Sarat Kumar
Rao, B. Hanumantha
TI Strength and durability characteristic of alkali activated GGBS
stabilized red mud as geo-material
LA English
DT Article
DE Red mud; GGBS; Alkali activation; Compressive strength; Durability;
Microstructure; Leachate analysis
ID FLY-ASH; SLAKE-DURABILITY; SOIL STABILIZATION; GEOPOLYMER; LIME
AB Red mud (bauxite residue) is generated during the Bayer's process of aluminium
production in the ratio of one part aluminium to 0.8-1.5 part red mud and is
considered as an industrial waste. The storage of unutilised red mud creates a
geoenvironmental problem due to its highly alkaline nature (pH > 11) as it
contaminates the groundwater as well as surface water. The present paper discusses
the strength and durability properties of the stabilized red mud using alkali
(Na2SiO3) activated ground granulated blast furnace slag (GGBS) and its
microstructural property for possible application as a geo-material. One of the
major problems associated with the geo-materials is the strength loss and
weathering due to the exposure to adverse environment. So, the emphasis has been
given to the durability of the stabilized red mud by keeping in mind its various
uses in geotechnical construction. The durability studies are performed by
considering the effect of wet-dry cycles on compressive strength. In addition, the
results of slake durability test and impact strength index are also discussed. The
microstructural and chemical investigations are performed using scanning electron
microscope (SEM) and X-ray diffraction (XRD), respectively, to correlate with the
strength and durability characteristics. The chemistry of leachate in terms of
heavy toxic metals (Hg, As, Pb, and Cr) as identified by EPA is also studied and it
was found that the stabilized red mud is non-toxic. (C) 2019 Elsevier Ltd. All
rights reserved.
C1 [Alam, Shamshad] Natl Inst Technol, Dept Civil Engn, Rourkela 769008, Odisha,
India.
[Das, Sarat Kumar] Indian Inst Technol, Dept Civil Engn, Dhanbad 826004,
Jharkhand, India.
[Rao, B. Hanumantha] Indian Inst Technol, Sch Infrastruct, Bhubaneswar 751013,
Odisha, India.
C3 National Institute of Technology (NIT System); National Institute of
Technology Rourkela; Indian Institute of Technology System (IIT System);
Indian Institute of Technology (Indian School of Mines) Dhanbad; Indian
Institute of Technology System (IIT System); Indian Institute of
Technology (IIT) - Bhubaneswar
RP Das, SK (corresponding author), Indian Inst Technol, Dept Civil Engn, Dhanbad
826004, Jharkhand, India.
EM safzal88@gmail.com; saratdas@iitism.ac.in; bhrao@iitbbs.ac.in
RI DAS, SARAT/P-4828-2017; Alam, Shamshad/T-6451-2017; Rao, B.
Hanumantha/AAY-9129-2020
OI DAS, SARAT/0000-0002-5627-4233; Alam, Shamshad/0000-0002-9839-9157;
FU Department of Science and Technology (DST), India under the SERB program
[SB/S3/CEE/036/2013]
FX The authors would like to acknowledge the financial support of present
work from Department of Science and Technology (DST), India under the
SERB program SB/S3/CEE/036/2013.
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U2 119
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUN 30
PY 2019
VL 211
BP 932
EP 942
DI 10.1016/j.conbuildmat.2019.03.261
PG 11
GA HW9GP
UT WOS:000466999500081
DA 2023-12-05
ER
PT J
AU Azimi, B
Tahmasebpoor, M
Sanchez-Jimenez, PE
Perejon, A
Valverde, JM
AF Azimi, Babak
Tahmasebpoor, Maryam
Sanchez-Jimenez, Pedro E.
Perejon, Antonio
Valverde, Jose Manuel
TI Multicycle CO2 capture activity and fluidizability of
Al-based synthesized CaO sorbents
LA English
DT Article
DE CO2 capture; Al-based synthesized CaO sorbents; Calcium-Looping;
Fluidization
ID CIRCULATING FLUIDIZED-BED; CRYSTAL-STRUCTURE; SOLID SORBENTS; TRICALCIUM
ALUMINATE; LOOPING PROCESS; ENERGY-STORAGE; CARBIDE SLAG; GAS;
ENHANCEMENT; PERFORMANCE
AB CaO-based materials have been identified as promising sorbents for highly
efficient pre-combustion and post-combustion CO2 capture in fluidized beds operated
at high temperatures by means of the Calcium Looping (CaL) process. However, Ca-
based sorbents suffer from a decline of the capture capacity over multiple
sorption/desorption cycles, mainly due to sintering, and from a markedly
heterogeneous fluidization behavior due to the strength of interparticle attractive
forces as compared to particle weight. The present study is focused on the
development of novel synthetic CaO/Al2O3 sorbents for CO2 capture with enhanced CaL
performance and fluidizability by dry mixing with flow conditioner nanopowders. The
influence of initial precursors on the sorbents multicycle activity at realistic
CaL conditions has been investigated. The formation of a stable Ca9Al6O18 mixed-
phase during the preparation of the sorbents promotes the multicycle capture
capacity. The type of Ca and Al precursors, either soluble or insoluble, can
significantly affect the dispersion of this stabilizer (Ca9Al6O18) in the sorbent
matrix and, consequently, may affect the carbonation activity of the materials. The
sorbent prepared from soluble aluminum nitrate and calcium nitrate precursors by
sol-gel method exhibits a very stable multicycle capture capacity with a capture
capacity around 0.2 g of CO2/g of sorbent after 21 cycles keeping a 72% of its
initial capture capacity. The fluidizability of this promising sorbent was also
investigated as affected by the addition of three different flow conditioners.
Fluidization experiments confirmed the positive effect of using hydrophilic alumina
and hydrophobic silica nanoparticles on improving the fluidizability of the
synthesized sorbents.
C1 [Azimi, Babak; Tahmasebpoor, Maryam] Univ Tabriz, Fac Chem & Petr Engn, POB
51666-16471, Tabriz, Iran.
[Sanchez-Jimenez, Pedro E.; Perejon, Antonio] Univ Seville, Inst Ciencia Mat
Sevilla, CSIC, C Americo Vespucio 49, Seville 41092, Spain.
[Perejon, Antonio] Univ Seville, Dept Quim Inorgan, Fac Quim, Seville 41071,
Spain.
[Valverde, Jose Manuel] Univ Seville, Fac Fis, Ave Reina Mercedes S-N, E-41012
Seville, Spain.
C3 University of Tabriz; University of Sevilla; Consejo Superior de
Investigaciones Cientificas (CSIC); Instituto de Ciencia de Materiales
de Sevilla (ICMS-CSIC); University of Sevilla; University of Sevilla
RP Tahmasebpoor, M (corresponding author), Univ Tabriz, Fac Chem & Petr Engn, POB
51666-16471, Tabriz, Iran.
EM tahmasebpoor@tabrizu.ac.ir
RI Tahmasebpoor, Maryam/AAV-1388-2020; Perejon, Antonio/K-1165-2014; Azimi,
Babak/JCP-1881-2023; Valverde, Jose Manuel/C-2918-2008; Sanchez Jimenez,
Pedro E/J-3187-2016
OI Tahmasebpoor, Maryam/0000-0001-6000-2233; Perejon,
Antonio/0000-0002-5525-2227; Azimi, Babak/0000-0002-4032-6414; Valverde,
Jose Manuel/0000-0002-2345-8888; Sanchez Jimenez, Pedro
E/0000-0001-6982-1411
FU MINECO-FEDER [CTQ2014-52763-C2, CTQ2017-83602-C2]
FX The Spanish team acknowledges financial support from Projects
CTQ2014-52763-C2 and CTQ2017-83602-C2 (MINECO-FEDER).
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NR 73
TC 70
Z9 72
U1 6
U2 144
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD FEB 15
PY 2019
VL 358
BP 679
EP 690
DI 10.1016/j.cej.2018.10.061
PG 12
SC Engineering
GA HA2WH
UT WOS:000450105700065
DA 2023-12-05
ER
PT J
AU Claveau-Mallet, D
Wallace, S
Comeau, Y
AF Claveau-Mallet, Dominique
Wallace, Scott
Comeau, Yves
TI Removal of phosphorus, fluoride and metals from a gypsum mining leachate
using steel slag filters
SO WATER RESEARCH
LA English
DT Article
DE Wastewater treatment; Slag filters; Mining remediation; Hydroxyapatite
growth
ID OIL-SHALE ASH; WASTE-WATER; PHOSPHATE; SATURATION; SYSTEMS
AB The objective of this work was to evaluate the capacity of steel slag filters to
treat a gypsum mining leachate containing 11-107 mg P/L ortho-phosphates, 9-37 mg/L
fluoride, 0.24-0.83 mg/L manganese, 0.20-3.3 zinc and 1.7-8.2 mg/L aluminum. Column
tests fed with reconstituted leachates were conducted for 145-222 days and sampled
twice a week. Two types of electric arc furnace (EAF) slags and three filter
sequences were tested. The voids hydraulic retention time (HRTv) of columns ranged
between 4.3 and 19.2 h. Precipitates of contaminants present in columns were
sampled and analyzed with X-ray diffraction at the end of tests. The best removal
efficiencies over a period of 179 days were obtained with sequential filters that
were composed of Fort Smith EAF slag operated at a total HRTv of 34 h which removed
99.9% of phosphorus, 85.3% of fluoride, 98.0% of manganese and 99.3% of zinc. Mean
concentration at this system's effluent was 0.04 mg P/L ortho-phosphates, 4 mg/L
fluoride, 0.02 mg/L manganese, 0.02 zinc and 0.5 mg/L aluminum. Thus, slag filters
are promising passive and economical systems for the remediation of mining
effluents. Phosphorus was removed by the formation of apatite (hydroxyapatite, Ca-
5(PO4)(3)OH or fluoroapatite, Ca-5(PO4)(3)F as confirmed by visual and X-ray
diffraction analyses. The growth rate of apatite was favored by a high phosphorus
concentration. Calcite crystals were present in columns and appeared to be
competing for calcium and volume needed for apatite formation. The calcite crystal
growth rate was higher than that of apatite crystals. Fluoride was removed by
precipitation of fluoroapatite and its removal was favored by a high ratio of
phosphorus to fluoride in the wastewater. (C) 2012 Elsevier Ltd. All rights
reserved.
C1 [Claveau-Mallet, Dominique; Comeau, Yves] Polytechn Montreal, Montreal, PQ H3C
3A7, Canada.
[Wallace, Scott] Nat Wallace Consulting, Stillwater, MN 55082 USA.
C3 Universite de Montreal; Polytechnique Montreal
RP Claveau-Mallet, D (corresponding author), Polytechn Montreal, CP 6079,Succ Ctr
Ville, Montreal, PQ H3C 3A7, Canada.
EM dominique.claveau-mallet@polymtl.ca; scott.wallace@naturallywallace.com
RI Dhoble, Yogesh/I-3720-2013; Comeau, Yves/F-6743-2010
OI Comeau, Yves/0000-0002-0560-1732
FU Natural Sciences and Engineering Research Council of Canada; Missouri
Remediation Trust; Fonds de recherche du Quebec Nature et technologies
FX The authors thank Kalle Kirsimae, Riho Motlep and Martin Liira from the
University of Tartu for the XRD analysis of slags, Denis Bouchard,
Aurore Bordier and Marie Ferland from Polytechnique Montreal for
technical assistance and Mark Finney from Shaw Environmental for
scientific support and data concerning the mine. Tube City (Arkansas)
and Harsco Minerals (Arkansas) provided samples of Fort Smith slag and
Blytheville slag respectively. This project was funded by the Natural
Sciences and Engineering Research Council of Canada, the Missouri
Remediation Trust and the Fonds de recherche du Quebec Nature et
technologies.
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TC 69
Z9 79
U1 4
U2 140
PI OXFORD
SN 0043-1354
J9 WATER RES
JI Water Res.
PD MAR 15
PY 2013
VL 47
IS 4
BP 1512
EP 1520
DI 10.1016/j.watres.2012.11.048
PG 9
GA 104FJ
UT WOS:000315977000002
PM 23305683
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Vasudevan, S
Lakshmi, J
Sozhan, G
Sozhan, Ganapathi
TI Optimization of electrocoagulation process for the simultaneous removal
of mercury, lead, and nickel from contaminated water
SO ENVIRONMENTAL SCIENCE AND POLLUTION RESEARCH
LA English
CT 15th International Symposium on Toxicity Assessment (ISTA)
CY JUL 03-08, 2011
CL City Univ Hong Kong, Hong Kong, PEOPLES R CHINA
HO City Univ Hong Kong
DE Electrocoagulation; Heavy metal; Adsorption; Kinetics; Thermodynamics
ID BAGASSE FLY-ASH; AQUEOUS-SOLUTIONS; ACTIVATED SLAG; DRINKING-WATER;
HAZARDOUS DYE; WASTE; ADSORPTION; CADMIUM; ZINC; CHROMIUM
AB The present study provides an optimization of electrocoagulation process for the
simultaneous removal of heavy metals such as mercury, lead, and nickel from water.
In doing so, the thermodynamic, adsorption isotherm and kinetic studies were also
carried out.
Magnesium alloy, magnesium, aluminum, and mild steel sheet of size 2 dm(2) were
used as anode and galvanized iron as cathode. To optimize the maximum removal
efficiency, different parameters like effect of initial concentration, effect of
temperature, pH, and effect of current density were studied. Mercury-, lead-, and
nickel-adsorbed magnesium hydroxide coagulant was characterized by SEM and EDAX.
The results showed that the maximum removal efficiency was achieved for mercury,
lead, and nickel with magnesium alloy as anode and galvanized iron as cathode at a
current density of 0.15 /dm(2) and pH of 7.0. The adsorption of mercury, lead, and
nickel are preferably fitting the Langmuir adsorption isotherm suggests monolayer
coverage of adsorbed molecules. The adsorption process follows second-order
kinetics. Temperature studies showed that adsorption was endothermic and
spontaneous in nature.
The magnesium hydroxide generated in the cell removes the heavy metals present
in the water and reduces to a permissible level, making it drinkable.
C1 [Vasudevan, Subramanyan; Lakshmi, Jothinathan; Sozhan, Ganapathi] CSIR Cent
Electrochem Res Inst, Karaikkudi 630006, Tamil Nadu, India.
RP Vasudevan, S (corresponding author), CSIR Cent Electrochem Res Inst, Karaikkudi
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NR 46
TC 69
Z9 71
U1 0
U2 47
PU SPRINGER HEIDELBERG
PI HEIDELBERG
PA TIERGARTENSTRASSE 17, D-69121 HEIDELBERG, GERMANY
SN 0944-1344
EI 1614-7499
J9 ENVIRON SCI POLLUT R
JI Environ. Sci. Pollut. Res.
PD AUG
PY 2012
VL 19
IS 7
BP 2734
EP 2744
DI 10.1007/s11356-012-0773-8
PG 11
GA 979BP
UT WOS:000306790200028
PM 22307898
DA 2023-12-05
ER
PT J
AU Shi, ZG
Shi, CJ
Wan, S
Zhang, ZH
AF Shi, Zhenguo
Shi, Caijun
Wan, Shu
Zhang, Zuhua
TI Effects of alkali dosage and silicate modulus on alkali-silica reaction
in alkali-activated slag mortars
LA English
DT Article
DE Alkali-aggregate reaction; Alkali activated cement; Waterglass; Silicate
modulus; Pore solution alkalinity
ID AGGREGATE REACTION; AMORPHOUS SILICA; PORTLAND-CEMENT; FLY-ASH;
CONCRETE; STRENGTH; WATER; EXPANSION; ALUMINUM
AB The effects of silicate modulus and alkali dosage on alkali-silica reaction
(ASR) of alkali-activated slag (AAS) mortars are investigated under accelerated
mortar bar testing conditions as specified in ASTM C1260. At a given alkali dosage,
an intermediate silicate modulus with respect to highest ASR expansion is observed,
which increases from 1.0 to > 2.0 with increase of alkali dosage. The effect of
silicate modulus on ASR expansion is found to be governed by the pore solution
alkalinity. At a given higher silicate modulus such as 1.5 and 2.0 at 14 day, the
ASR expansion tends to increase with increase of alkali dosage, whereas it
decreases with increase of alkali dosage at a given lower silicate modulus such as
0-0.5 at 28 day. The mechanism governing the effect of alkali dosage on ASR
expansion is more complicated and cannot be explained by only the pore solution
alkalinity.
C1 [Shi, Zhenguo; Shi, Caijun; Wan, Shu; Zhang, Zuhua] Hunan Univ, Coll Civil Engn,
Key Lab Green & Adv Civil Engn Mat & Applicat Tec, Changsha 410082, Hunan, Peoples
R China.
[Shi, Zhenguo] Swiss Fed Labs Mat Sci & Technol Empa, Lab Concrete & Construct
Chem, CH-8600 Dubendorf, Switzerland.
[Zhang, Zuhua] Univ Southern Queensland, Ctr Future Mat, Toowoomba, Qld 4350,
Australia.
C3 Hunan University; Swiss Federal Institutes of Technology Domain; Swiss
Federal Laboratories for Materials Science & Technology (EMPA);
University of Southern Queensland
RP Shi, CJ; Zhang, ZH (corresponding author), Hunan Univ, Coll Civil Engn, Changsha
EM zhenguo.shi@empa.ch; cshi@hnu.edu.cn; zuhuazhang@hnu.edu.cn
RI Zhang, Zuhua/AAK-5391-2020; Shi, Zhenguo/E-4894-2018
OI Zhang, Zuhua/0000-0002-7153-5120; Shi, Zhenguo/0000-0003-0000-6560
FU National Natural Science Foundation of China [51638008]; Australian
Research Council DECRA [DE170101070]; Australian Research Council
Discovery project [DP160104149]
FX The financial supports from the National Natural Science Foundation of
China under contract No. 51638008 are gratefully acknowledged. The
participation of Z. Zhang is partially fund by Australian Research
Council DECRA (DE170101070) and Discovery project (DP160104149).
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SN 0008-8846
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VL 111
BP 104
EP 115
DI 10.1016/j.cemconres.2018.06.005
PG 12
GA GP0VM
UT WOS:000440529500009
DA 2023-12-05
ER
PT J
AU Nazari, A
Sanjayan, JG
AF Nazari, Ali
Sanjayan, Jay G.
TI Synthesis of geopolymer from industrial wastes
LA English
DT Article
DE Slag mixtures; Alkali-activated materials; Waste management; Compressive
strength; Workability
ID ALKALI-ACTIVATED SLAG; FLY-ASH; COMPRESSIVE STRENGTH;
MECHANICAL-PROPERTIES; MICROSTRUCTURE; WORKABILITY; CONCRETE; RATIO; AGE
AB Aluminium and grey cast iron slags are produced in small industries and in spite
of blastfurnace slag are considered as wastes. In this work, synthesis possibility
of geopolymeric paste and concrete through alkali activation of different mixes of
these slags is studied. Workability of the mixtures was achieved immediately after
mixing and compressive strength tests were conducted on specimens cured at room
temperature. Workability of all pastes and concrete specimens were in acceptable
range for use in constructions. Maximum compressive strength for both paste and
concrete specimens was achieved by using silica/alumina weight ratio of 3.0. By
increasing the value of parameters of this study including sodium hydroxide
concentration, age of curing and silica/alumina weight ratio, more silicon and
aluminium ions dissolve from slag mixture into alkali activator and hence,
compressive strength increases. It was concluded that among the considered
parameters, silica/alumina weight ratio is the most important factor. The results
indicated the possibility of production of geopolymers by utilizing appropriate
ratios of aluminium slag (alumina source) and grey cast iron slag (silica source).
In most related works reported in the literature, an aluminosilicate source or a
mixture of two aluminosilicate sources with defined silica/alumina weight ratio are
evaluated for possibility of geopolymerization. In the current study, each alumina
and silica is provided from an individual source, and geopolymerization is
performed by manipulating silica/alumina weight ratio. (C) 2015 Elsevier Ltd. All
rights reserved.
C1 [Nazari, Ali; Sanjayan, Jay G.] Swinburne Univ Technol, Fac Sci Engn & Technol,
Hawthorn, Vic 3722, Australia.
C3 Swinburne University of Technology
RP Nazari, A (corresponding author), Swinburne Univ Technol, Fac Sci Engn &
Technol, Hawthorn, Vic 3722, Australia.
EM alinazari@swin.edu.au
RI Sanjayan, Jay/AAE-1468-2019; Sanjayan, Jay/AAD-1432-2020; Nazari,
Ali/I-5340-2019
OI Sanjayan, Jay/0000-0002-5400-5988; Nazari, Ali/0000-0001-9461-3753
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10.1016/j.conbuildmat.2014.06.016
10.1016/j.conbuildmat.2012.09.056
NR 33
TC 68
Z9 70
U1 1
U2 64
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD JUL 15
PY 2015
VL 99
BP 297
EP 304
DI 10.1016/j.jclepro.2015.03.003
PG 8
& Ecology
GA CK4LJ
UT WOS:000356195000025
DA 2023-12-05
ER
PT J
AU Guéguin, M
Cardarelli, F
AF Gueguin, Michel
Cardarelli, Francois
TI Chemistry and mineralogy of titania-rich slags.: Part 1 -:
Hemo-ilmenite, sulphate, and upgraded titania slags
LA English
DT Article
DE titanium; titania slag; titanates; pseudobrookite; karrooite
ID MAGNETIC-PROPERTIES; CRYSTAL-STRUCTURE; PHASE-EQUILIBRIA;
NEUTRON-DIFFRACTION; HIGH-TEMPERATURE; HIGH-PRESSURE; SYSTEM;
PSEUDOBROOKITE; OXIDES; FEO-FE2O3-TIO2
AB Titania-rich slags with 80 mass percent TiO2 are produced in the electric arc
furnaces of QIT-Fer & Titane, Inc., by the continuous smelting of hemo-ilmenite ore
with anthracite coal. Titania slag represents an important feedstock for the
manufacture of titanium dioxide pigment by the sulphate process. Moreover, part of
the production of the titania-rich slag is further acid-leached under a high-
pressure and mode rate-temperature hydrometallurgical process to yield an upgraded
titania slag with 94.5 mass percent TiO2, which is used in the chloride process.
After describing in detail the beneficiation, chemistry, and mineralogy of the
hemo-ilmenite ore, this article reviews the unique crystallochemistry and
mineralogy of the titanate phases with pseudobrookite-karrooite structure and to a
lesser extent silicates and oxides present in these titania-rich feedstocks,
focusing on the chemical reactions occurring at each step of the pyro- and hydro-
metallurgical processes. The behavior of major elements such as titanium, iron,
magnesium, calcium, aluminum, and silicon along with that of minor elements such as
vanadium, chromium, and manganese are particularly detailed. A general discussion
of the methods specifically developed for the study of the synthetic minerals
present in these materials is also presented.
C1 Rio Tinto Iron & Titanium Inc, Dept Technol, Sorel Tracy, PQ J3R 1M6, Canada.
C3 Rio Tinto
RP Guéguin, M (corresponding author), Rio Tinto Iron & Titanium Inc, Dept Technol,
1625 Route Marie Victorin, Sorel Tracy, PQ J3R 1M6, Canada.
EM francois.cardarelli@rtit.com
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NR 70
TC 68
Z9 80
U1 2
U2 27
PI PHILADELPHIA
SN 0882-7508
EI 1547-7401
PD JAN-MAR
PY 2007
VL 28
IS 1
BP 1
EP 58
DI 10.1080/08827500600564242
PG 58
GA 124LG
UT WOS:000243368700001
DA 2023-12-05
ER
PT J
AU Bernal, SA
San Nicolas, R
van Deventer, JSJ
Provis, JL
AF Bernal, Susan A.
San Nicolas, Rackel
Provis, John L.
TI Alkali-activated slag cements produced with a blended sodium
carbonate/sodium silicate activator
LA English
DT Article
ID C-S-H; ACCELERATED CARBONATION; HYDRATION; NMR; GEOPOLYMERS;
PERFORMANCE; REACTIVITY; EVOLUTION; MAGNESIUM; MORTARS
AB An alkali-activated slag cement produced with a blend of sodium carbonate/sodium
silicate activator was characterised. This binder hardened within 12 h and achieved
a compressive strength of 20 MPa after 24 h of curing under ambient conditions,
which is associated with the formation of an aluminium substituted calcium silicate
hydrate as the main reaction product. Carbonates including pirssonite, vaterite,
aragonite and calcite were identified along with the zeolites hydroxysodalite and
analcime at early times of reaction. The partial substitution of sodium carbonate
by sodium silicate reduces the concentration of carbonate ions in the pore
solution, increasing the alkalinity of the system compared with a solely carbonate-
activated paste, accelerating the kinetics of reaction and supplying additional
silicate species to react with the calcium dissolving from the slag as the reaction
proceeds. These results demonstrate that this blend of activators can be used
effectively for the production of high-strength alkali-activated slag cements, with
a microstructure comparable to what has been identified in aged sodium-carbonate-
activated slag cements but without the extended setting time reaction usually
identified when using this salt as an alkali activator.
C1 [Bernal, Susan A.; Provis, John L.] Univ Sheffield, Dept Mat Sci & Engn,
Sheffield, S Yorkshire, England.
3010, Australia.
[San Nicolas, Rackel; van Deventer, Jannie S. J.] Univ Melbourne, Dept Chem &
Biomol Engn, Melbourne, Vic 3010, Australia.
[van Deventer, Jannie S. J.] Zeobond Pty Ltd, Docklands, Vic, Australia.
Melbourne
RP Bernal, SA (corresponding author), Univ Sheffield, Dept Mat Sci & Engn,
RI Provis, John/AAR-3260-2020; Provis, John L/A-7631-2008; Bernal, Susan
A/E-8938-2011; Goodall, Liz J/O-9809-2016
Goodall, Liz J/0000-0001-5354-574X; Bernal, Susan A/0000-0002-9647-3106
FU Australian Research Council, through a Linkage Project - Zeobond Pty
Ltd; European Research Council under the European Union's Seventh
Framework Programme (FP)/ERC grant [335928]; Australian Research Council
through the Particulate Fluids Processing Centre
FX This work was funded by the Australian Research Council, through a
Linkage Project co-sponsored by Zeobond Pty Ltd, including partial
funding through the Particulate Fluids Processing Centre. The authors
thank Adam Kilcullen and David Brice for producing the specimens tested
and Dr John D. Gehman for assistance with the NMR spectroscopy. The work
of JLP and SAB received funding from the European Research Council under
the European Union's Seventh Framework Programme (FP/2007-2013)/ERC
grant agreement 335928 (GeopolyConc).
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NR 44
TC 67
Z9 69
U1 7
U2 76
PU ICE PUBLISHING
PI WESTMINISTER
SN 0951-7197
EI 1751-7605
J9 ADV CEM RES
JI Adv. Cem. Res.
PY 2016
VL 28
IS 4
BP 262
EP 273
DI 10.1680/jadcr.15.00013
PG 12
GA DG9ZO
UT WOS:000372442500007
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Ribeiro, DV
Labrincha, JA
Morelli, MR
AF Ribeiro, D. V.
Labrincha, J. A.
Morelli, M. R.
TI Effect of the addition of red mud on the corrosion parameters of
reinforced concrete
LA English
DT Article
DE Concrete; Red mud; Diffusion; Corrosion; Electrochemical properties
ID CHLORIDE DIFFUSION-COEFFICIENTS; DURABILITY CHARACTERISTICS;
ELECTRICAL-CONDUCTIVITY; EAF SLAG; PERMEABILITY; CEMENTS; BAUXITE; WASTE
AB Red mud, the main waste generated in aluminum and alumina production by the
Bayer process, is considered "hazardous" due to its high pH. The characteristic of
high alkalinity associated with the presence of alumino-silicates facilitates the
assimilation and formation of compounds by reaction with chloride ions. The high pH
also provides greater protection of rebars, which is reflected in the low corrosion
potential and high electrical resistivity (filler effect) of concrete. In this
study, the chloride concentration was monitored by measuring the conductivity of
the anolyte. Red mud proved to be a promising additive for concrete to inhibit the
corrosion process. The corrosion potential was monitored by electrochemical
measurements and the electrical resistivity was evaluated using sensors embedded in
concrete test specimens. The results showed that the addition of red mud is
beneficial to concrete, reducing its chloride migration rate (diffusion
coefficients) and corrosion potential and increasing its electrical resistivity.
C1 [Ribeiro, D. V.] Univ Fed Bahia, Dept Mat Sci & Technol, BR-40210630 Salvador,
BA, Brazil.
[Labrincha, J. A.] Univ Aveiro, Ceram & Glass Engn Dept, P-3810193 Aveiro,
Portugal.
[Labrincha, J. A.] Campus Univ Santiago, CICECO, P-3810193 Aveiro, Portugal.
[Morelli, M. R.] Univ Fed Sao Carlos, Dept Mat Engn, BR-13566550 Sao Carlos, SP,
Brazil.
C3 Universidade Federal da Bahia; Universidade de Aveiro; Universidade de
Aveiro; Universidade Federal de Sao Carlos
RP Ribeiro, DV (corresponding author), Univ Fed Bahia, Dept Mat Sci & Technol, Rua
Aristides Novis,02 Federacao, BR-40210630 Salvador, BA, Brazil.
EM verasribeiro@hotmail.com
RI Ribeiro, Daniel Véras/O-1976-2013; Morelli, Márcio R/M-3601-2014;
Labrincha, J./B-3984-2010
OI Ribeiro, Daniel Véras/0000-0003-3328-1489; Labrincha,
J./0000-0003-4782-1685
FU UA/DECV - Department of Ceramics and Glass Engineering, University of
Aveiro & CICECO (Portugal) [FCT-PTDC/CTM/65243/2006]
FX The authors wish to thank CNPq - National Council for Scientific and
Technological Development (Brazil), PPGCEM/UFSCar - Postgraduate Program
in Materials Science and Engineering at the Federal University of Sao
Carlos (Brazil), and UA/DECV - Department of Ceramics and Glass
Engineering, University of Aveiro & CICECO (Portugal) - Project
FCT-PTDC/CTM/65243/2006.
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NR 30
TC 67
Z9 76
U1 5
U2 43
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD JAN
PY 2012
VL 42
IS 1
BP 124
EP 133
DI 10.1016/j.cemconres.2011.09.002
PG 10
GA 862EB
UT WOS:000298071500015
DA 2023-12-05
ER
PT J
AU Brunet, F
Charpentier, T
Chao, CN
Peycelon, H
Nonat, A
AF Brunet, F.
Charpentier, T.
Chao, C. N.
Peycelon, H.
Nonat, A.
TI Characterization by solid-state NMR and selective dissolution techniques
of anhydrous and hydrated CEM V cement pastes
LA English
DT Article
DE Hydration (A); Amorphous material (B); Blended cement (D); NMR
spectroscopy
ID SI-29 MAS NMR; C-S-H; FURNACE SLAG CEMENT; HIGH-RESOLUTION NMR; AL-27
NMR; PORTLAND CEMENTS; SILICATE PHASES; CALCIUM; ALUMINUM;
QUANTIFICATION
AB The long term behaviour of cement based materials is strongly dependent on the
paste microstructure and also on the internal chemistry. A CEM V blended cement
containing pulverised fly ash (PFA) and blastfurnace slag (BFS) has been studied in
order to understand hydration processes which influence the paste microstructure.
Solid-state NMR spectroscopy with complementary X-ray diffraction analysis and
selective dissolution techniques have been used for the characterization of the
various phases (C3S, C2S, C(3)A and C(4)AF) of the clinker and additives and then
for estimation of the degree of hydration of these same phases. Their
quantification after simulation of experimental Si-29 and Al-27 MAS NMR spectra has
allowed us to follow the hydration of recent (28 days) and old (10 years) samples
that constitutes a basis of experimental data for the prediction of hydration
model. (C) 2009 Elsevier Ltd. All rights reserved.
C1 [Brunet, F.; Charpentier, T.] CEA, IRAMIS, Serv Interdisciplinaire Syst Mol &
Mat, LSDRM, F-91191 Gif Sur Yvette, France.
[Chao, C. N.; Peycelon, H.] CEA, DPC, Serv Corros & Comportement Mat Leur
Environm, F-91191 Gif Sur Yvette, France.
[Nonat, A.] Univ Bourgogne, CNRS, UMR 5209, Inst Carnot Bourgogne, F-21078
Dijon, France.
C3 Universite Paris Saclay; CEA; Centre National de la Recherche
Scientifique (CNRS); CEA; Universite Paris Saclay; Centre National de la
Recherche Scientifique (CNRS); Universite de Bourgogne; Universite de
Technologie de Belfort-Montbeliard (UTBM)
RP Brunet, F (corresponding author), CEA, IRAMIS, Serv Interdisciplinaire Syst Mol
& Mat, LSDRM, F-91191 Gif Sur Yvette, France.
EM francine.brunet@cea.fr
RI Charpentier, Thibault/A-3557-2010
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Andre/0000-0002-6710-5638
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NR 49
TC 67
Z9 73
U1 1
U2 47
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD FEB
PY 2010
VL 40
IS 2
BP 208
EP 219
DI 10.1016/j.cemconres.2009.10.005
PG 12
GA 551PN
UT WOS:000274221600004
DA 2023-12-05
ER
PT J
AU KWAN, S
LAROSA, J
GRUTZECK, MW
AF KWAN, S
LAROSA, J
GRUTZECK, MW
TI SI-29 AND AL-27 MASNMR STUDY OF STRATLINGITE
LA English
DT Article
ID S-H GEL; PASTES
AB Stratlingite (2CaO . Al2O3 . SiO2 . 8H(2)O) is a complex calcium aluminosilicate
hydrate commonly associated with the hydration of slag-containing cements or other
cements enriched in alumina, Stratlingite can coexist with the hydrogarnet solid
solution [hydrogarnet (3CaO . Al2O2 . 6H(2)O)-katoite (3CaO . Al2O3 . SiO2 . 4H2O)]
and calcium silicate hydrate (C-S-H). Since stratlingite is present in many blended
cements, the knowledge of stratlingite's characteristic silicate anion structure
and how aluminum is accommodated by the structure is important, Phase pure
stratlingite samples have been synthesized from oxides in the presence of excess
water and from metakaolinite, calcium aluminate cement, CaO, NaOH, and water, The
samples were characterized using X-ray diffraction (XRD), scanning electron
microscopy (SEM), and thermogravimetric analysis (TGA) and then further examined
using Si-29, With and without cross-polarization (CP), and Al-27 solid-state magic
angle nuclear magnetic resonance spectroscopy (MASNMR), For the most part, NMR data
for these stratlingites corroborate structural information available in the
literature, The aluminum atoms are both tetrahedrally and octahedrally coordinated,
and the silicon atoms exist predominantly as Q(2), Q(2)(1A1), and Q(2)(2AI)
species, The presence of alkali affects the structure of stratlingite in subtle
ways, significantly reducing the AI(/)(IV)AI(VI) ratio.
RP KWAN, S (corresponding author), PENN STATE UNIV,INTERCOLL MAT RES LAB,UNIVERSITY
PK,PA 16802, USA.
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NR 11
TC 67
Z9 71
U1 0
U2 21
PU AMER CERAMIC SOC 735 CERAMIC PLACE
PI WESTERVILLE
PA PO BOX 6136, WESTERVILLE, OH 43081-6136
SN 0002-7820
J9 J AM CERAM SOC
PD JUL
PY 1995
VL 78
IS 7
BP 1921
EP 1926
DI 10.1111/j.1151-2916.1995.tb08910.x
PG 6
GA RJ680
UT WOS:A1995RJ68000031
DA 2023-12-05
ER
PT J
AU Gomes, HI
Funari, V
Mayes, WM
Rogerson, M
Prior, TJ
AF Gomes, Helena, I
Funari, Valerio
Mayes, William M.
Rogerson, Mike
Prior, Timothy J.
TI Recovery of Al, Cr and V from steel slag by bioleaching: Batch and
column experiments
LA English
DT Article
DE Acidophilic bacteria; Mixed culture; Ion exchange resins; Resource
recovery; Circular economy
ID ACIDITHIOBACILLUS-FERROOXIDANS; ION-EXCHANGE; SULFIDE OXIDATION;
VANADIUM REMOVAL; WASTE; COPPER; BACTERIA; CATALYSTS; SEPARATION;
LEACHATES
AB Steel slag is a major by-product of the steel industry and a potential resource
of technology critical elements. For this study, a basic oxygen furnace (BOF) steel
slag was tested for bacterial leaching and recovery of aluminium (Al), chromium
(Cr), and vanadium (V). Mixed acidophilic bacteria were adapted to the steel slag
up to 5% (w/v). In the batch tests, Al, Cr, and V were bioleached significantly
more from steel slag than in control treatments. No statistical difference was
observed arising from the duration of the leaching (3 vs 6 d) in the batch tests.
Al and Cr concentrations in the leachate were higher for the smaller particle size
of the steel slag (< 75 mu m), but no difference was observed for V. In the column
tests, no statistical difference was found for pH, Al, Cr and V between the live
culture (one-step bioleaching) and the supernatant (two-step bioleaching). The
results show that the culture supernatant can be effectively used in an upscaled
industrial application for metal recovery. If bioleaching is used in the 170-250
million tonnes of steel slag produced per year globally, significant recoveries of
metals (100% of Al, 84% of Cr and 8% of V) can be achieved, depending on the slag
composition. The removal and recovery percentages of metals from the leachate with
Amberlite. IRA-400 are relatively modest (< 67% and < 5%, respectively), due to the
high concentration of competing ions (SO42-, PO43-) in the culture medium. Other
ion exchange resins can be better suited for the leachate or methods such as
selective precipitation could improve the performance of the resin. Further
research is needed to minimise interference and maximise metal recovery.
C1 [Gomes, Helena, I; Mayes, William M.; Rogerson, Mike] Univ Hull, Sch Environm
Sci, Cottingham Rd, Kingston Upon Hull HU6 7RX, N Humberside, England.
[Funari, Valerio] Univ Bologna, Dept Biol Geol & Environm Sci, Piazza Porta San
Donato 1, I-40126 Bologna, Italy.
[Prior, Timothy J.] Univ Hull, Sch Math & Phys Sci, Chem, Cottingham Rd,
Kingston Upon Hull HU6 7RX, N Humberside, England.
[Gomes, Helena, I] Univ Nottingham, Fac Engn, Dept Chem & Environm Engn, Univ
Pk, Nottingham NG7 2RD, England.
C3 University of Hull; University of Bologna; University of Hull;
University of Nottingham
RP Gomes, HI (corresponding author), Univ Hull, Sch Environm Sci, Cottingham Rd,
Kingston Upon Hull HU6 7RX, N Humberside, England.; Gomes, HI (corresponding
author), Univ Nottingham, Fac Engn, Dept Chem & Environm Engn, Univ Pk, Nottingham
NG7 2RD, England.
EM helena.gomes@nottingham.ac.uk
RI Mayes, William/ABA-8647-2021; Funari, Valerio/E-4027-2016; Prior,
Timothy J/D-1658-2018; Gomes, Helena I./H-7557-2019
OI Mayes, William/0000-0002-1864-9057; Funari, Valerio/0000-0002-8280-8518;
Prior, Timothy J/0000-0002-7705-2701; Gomes, Helena
I./0000-0003-1131-7604; Rogerson, Mike/0000-0001-6016-0549
FU UK Natural Environment Research Council; Economic and Social Research
Council; Department for Environment, Food and Rural Affairs under the
Resource Recovery from Waste [NE/L014211/1]; Accademia Nazionale dei
Lincei [104/2016]; SIMP; NERC [NE/L01405X/1, NE/L014211/1] Funding
Source: UKRI
FX This project was funded by the UK Natural Environment Research Council,
Economic and Social Research Council and the Department for Environment,
Food and Rural Affairs under the Resource Recovery from Waste theme via
grant NE/L014211/1. The financial support from Accademia Nazionale dei
Lincei (Sc/Sc prot n. 104/2016) and SIMP (www.socminpet.it) to V.F. are
acknowledged. Thanks to Bob Knight and Mike Thompson who performed the
ICP analysis. We also thank Martina Cappelletti and Stefano Fedi from
the FaBit Department (University of Bologna) for their assistance in the
preliminary microbial profiling analysis.
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NR 48
TC 66
Z9 69
U1 1
U2 61
PI LONDON
SN 0301-4797
EI 1095-8630
J9 J ENVIRON MANAGE
PD SEP 15
PY 2018
VL 222
BP 30
EP 36
DI 10.1016/j.jenvman.2018.05.056
PG 7
GA GM8LE
UT WOS:000438479300005
PM 29800862
OA Green Accepted, Green Submitted, hybrid
DA 2023-12-05
ER
PT J
AU Jiang, ZH
Hou, D
Dong, YW
Cao, YL
Cao, HB
Gong, W
AF Jiang, Zhou-Hua
Hou, Dong
Dong, Yan-Wu
Cao, Yu-Long
Cao, Hai-Bo
Gong, Wei
TI Effect of Slag on Titanium, Silicon, and Aluminum Contents in Superalloy
During Electroslag Remelting
LA English
DT Article
ID THERMODYNAMIC MODEL; ALLOYS; STEELS
AB Many factors influence the chemical composition in electroslag remelting (ESR)
steel, including atmosphere in crucible, melting rate, slag composition,
deoxidation, and so on. Fluoride-based slag, which is exposed to liquid metal
directly, influences the chemical composition of ESR ingots to a large extent. The
present paper focuses on the effect of slag on the titanium, silicon, and aluminum
contents in ingots based on the interaction of the slag and metal. In present work,
superalloy of GH8825 and several slags containing different CaO contents have been
employed for investigating the effect of slag on titanium, silicon, and aluminum
contents in an electrical resistance furnace under argon atmosphere. Results
indicate that the higher CaO content in slag has better capacity for avoiding loss
of titanium caused by the reaction of titanium with silica in slag, especially in
case of remelting superalloy with high titanium and low silicon content. The CaO
has a great effect on the activities of TiO2, SiO2, and Al2O3. Thermodynamic
analysis is applied to investigate the CaO behavior. Based on the ion and molecule
coexistence theory of slag, activity model is established to calculate the
activities of components containing titanium, silicon, and aluminum elements in a
six-component slag consisting of CaO-CaF2-Al2O3-SiO2-TiO2-MgO. The components
containing titanium, silicon, and aluminum in slag are mainly CaO center dot TiO2,
2CaO center dot SiO2, CaO center dot SiO2, CaO center dot Al2O3, and MgO center dot
Al2O3. With the increase of CaO mass fraction in slag, the activity coefficient of
SiO2 decreases significantly, whereas slightly change happens for Al2O3. As a
result, the lg(gamma SiO2/gamma TiO2) decreases with increasing CaO content, which
is better for preventing loss of titanium caused by the reaction of titanium with
silica in slag. The slag with high CaO and appropriate TiO2 content is suitable for
electroslag remelting of GH8825. (C) The Minerals, Metals & Materials Society and
ASM International 2016
C1 [Jiang, Zhou-Hua; Hou, Dong; Dong, Yan-Wu; Cao, Yu-Long; Cao, Hai-Bo; Gong, Wei]
Northeastern Univ, Sch Met & Mat, Shenyang 110819, Liaoning, Peoples R China.
RP Jiang, ZH (corresponding author), Northeastern Univ, Sch Met & Mat, Shenyang
110819, Liaoning, Peoples R China.
EM jiangzh@smm.neu.edu.cn
OI Jiang, Zhouhua/0000-0001-8887-7250
FU National Nature Science Foundation of China [51274266]; National Nature
Science Foundation of China; Baosteel Group Corporation [U1360103];
Liaoning Excellent Talents in University [LR2013009]
FX This project supported by the National Nature Science Foundation of
China with the Grant No. 51274266 and supported by Joint Research Fund
of National Nature Science Foundation of China and Baosteel Group
Corporation with the Grant No. U1360103. In addition, this project is
supported by Liaoning Excellent Talents in University with the Grant No.
LR2013009.
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EI 1543-1916
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PG 10
Engineering
GA DL2HN
UT WOS:000375454700064
DA 2023-12-05
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PT J
AU Allahverdi, A
Skvára, F
AF Allahverdi, A
Skvára, F
TI Nitric acid attack on hardened paste of geopolymeric cements -: Part 2
SO CERAMICS-SILIKATY
LA English
DT Article
DE geopolymeric cement; acid attack; fly ash; blast furnace slag
ID RESOLUTION SI-29 NMR; INFRARED ABSORPTION SPECTRA; Y-ZEOLITES;
SILICATES; SPECTROSCOPY; CORROSION; GLASSES
AB Mechanism of nitric acid attack on hardened paste of geopolymeric cements, in
addition to the leaching process discussed in part 1 [1], consists of an
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ejection of tetrahedral aluminium from the aluminosilicate framework. The framework
vacancies are mostly re-occupied by silicon atoms resulting in the formation of an
imperfect highly siliceous framework that is relatively hard but brittle. The
ejected aluminium converted to octahedrally coordinated aluminium mostly
accumulates in the intraframework space.
C1 Inst Chem Technol, Dept Glass & Ceram, CR-16628 Prague, Czech Republic.
C3 University of Chemistry & Technology, Prague
RP Allahverdi, A (corresponding author), Inst Chem Technol, Dept Glass & Ceram,
Tech 5, CR-16628 Prague, Czech Republic.
EM Ali.Allahvredi@vscht.cz
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XINCHENG P, 1999, P 2 INT C KYIEV UKR, P717
NR 34
TC 66
Z9 70
U1 0
U2 9
PU INST CHEMICAL TECHNOLOGY, DEPT GLASS CERAMICS
PI PRAGUE
PA TECHNICKA 5, PRAGUE 166 28, CZECH REPUBLIC
SN 0862-5468
J9 CERAM-SILIKATY
JI Ceram.-Silik.
PY 2001
VL 45
IS 4
BP 143
EP 149
PG 7
GA 510LR
UT WOS:000173210000004
DA 2023-12-05
ER
PT J
AU Radenovic, A
Malina, J
Sofilic, T
AF Radenovic, Ankica
Malina, Jadranka
Sofilic, Tahir
TI Characterization of Ladle Furnace Slag from Carbon Steel Production as a
Potential Adsorbent
SO ADVANCES IN MATERIALS SCIENCE AND ENGINEERING
LA English
DT Article
ID ADSORPTION; REMOVAL; WASTES; IONS
AB A promising type of steel slag for applications is the ladle furnace (LF) slag,
which is also known as the basic slag, the reducing slag, the white slag, and the
secondary refining slag. The LF slag is a byproduct from further refining molten
steel after coming out of a basic oxygen furnace (BOF) or an electric arc furnace
(EAF). The use of the LF slag in further applications requires knowledge of its
characteristics. The LF slag characterization in this paper has been performed
using the following analytical methods: chemical analysis by energy dispersive
spectrometry (EDS), mineralogical composition by X-ray diffraction (XRD), surface
area properties by the Brunauer-Emmett-Teller (BET) and the Barrett-Joyner-Halenda
(BJH) methods, surface chemistry by infrared absorption (FTIR) spectroscopy, and
morphological analysis by scanning electron microscopy (SEM). The results showed
that the main compounds are calcium, silicon, magnesium, and aluminium oxides, and
calcium silicates under their various allotropic forms are the major compounds in
the LF slag. Surface area properties have shown that the LF slag is a mesoporous
material with relatively great BET surface area. The ladle furnace slag is a
nonhazardous industrial waste because the ecotoxicity evaluation by its eluate has
shown that the LF slag does not contain constituents which might in any way affect
the environment harmfully.
C1 [Radenovic, Ankica; Malina, Jadranka; Sofilic, Tahir] Univ Zagreb, Fac Met,
Sisak 44000, Croatia.
C3 University of Zagreb
RP Radenovic, A (corresponding author), Univ Zagreb, Fac Met, Aleja Narodnih Heroja
3, Sisak 44000, Croatia.
EM radenova@simet.hr
FU Ministry of Science, Education, and Sports of the Republic of Croatia
[124-124 1565-1524]
FX This work was supported by the Ministry of Science, Education, and
Sports of the Republic of Croatia, under Project no. 124-124 1565-1524.
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NR 27
TC 65
Z9 67
U1 2
U2 36
PU HINDAWI LTD
PI LONDON
PA ADAM HOUSE, 3RD FLR, 1 FITZROY SQ, LONDON, W1T 5HF, ENGLAND
SN 1687-8434
EI 1687-8442
J9 ADV MATER SCI ENG
JI Adv. Mater. Sci. Eng.
PY 2013
VL 2013
AR 198240
DI 10.1155/2013/198240
PG 6
GA 218GB
UT WOS:000324419700001
DA 2023-12-05
ER
PT J
AU Cong, XY
Lu, S
Yao, Y
Wang, Z
AF Cong, X. Y.
Lu, S.
Yao, Y.
Wang, Z.
TI Fabrication and characterization of self-ignition coal gangue autoclaved
aerated concrete
LA English
DT Article
DE Self-ignition coal gangue; Autoclaved aerated concrete; Orthogonal
experiment; Tobermorite
ID ASH; ACTIVATION; CHINA; SLAG
AB By conducting the orthogonal design for the best mechanical properties of the
matrix parts without introducing air pores in advance, the self-ignition coal
gangue: lime: cement: gypsum = 54: 23: 20: 3 accompany with 1.3 parts per thousand
aluminum powder is determined as the optimal mix proportion of the self-ignition
coal gangue aerated concrete. Meanwhile, the reasonable Ca/Si ratio of the elements
is found to be 0.82. XRD results show that the hydration products of self-ignition
coal gangue autoclaved aerated concrete (SCGAAC) are mainly consisted by CSH gel
and tobermorite phase, moreover, SEM approved that a higher Ca/Si ratio is
conducive to form the tobermorite phase under the autoclaved conditions. The
induced pores in SCGAAC are mainly interconnected open cell structure with middle
characteristic latitudinal dimension between 0.5 and 2 mm. (C) 2016 Elsevier Ltd.
C1 [Cong, X. Y.; Lu, S.; Wang, Z.] Minist Educ, Key Lab Struct Dynam Behav &
Control, Harbin 150090, Peoples R China.
[Cong, X. Y.; Lu, S.; Yao, Y.; Wang, Z.] Harbin Inst Technol, Sch Civil Engn,
Harbin 150090, Peoples R China.
[Yao, Y.] China Bldg Mat Acad, Beijing 100000, Peoples R China.
C3 Harbin Institute of Technology
RP Lu, S (corresponding author), Minist Educ, Key Lab Struct Dynam Behav & Control,
Harbin 150090, Peoples R China.; Lu, S (corresponding author), Harbin Inst Technol,
Sch Civil Engn, Harbin 150090, Peoples R China.
EM hitlu@126.com
RI lu, shuang/M-1863-2017
OI lu, shuang/0000-0001-8700-0254
FU "Solid waste reuse for building materials state key laboratory"
[SWR-2013-008]; National Natural Science Foundation of China [51572251]
FX The work is supported by fund No. SWR-2013-008 provided by "Solid waste
reuse for building materials state key laboratory". And the work is also
supported by the National Natural Science Foundation of China No.
51572251.
CR Cong XD, 1996, ADV CEM BASED MATER, V3, P144, DOI 10.1016/S1065-7355(96)90046-2
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NR 16
TC 64
Z9 71
U1 5
U2 113
PU ELSEVIER SCI LTD
PI OXFORD
SN 0261-3069
EI 1873-4197
J9 MATER DESIGN
JI Mater. Des.
PD MAY 5
PY 2016
VL 97
BP 155
EP 162
DI 10.1016/j.matdes.2016.02.068
PG 8
GA DH0XD
UT WOS:000372506500020
DA 2023-12-05
ER
PT J
AU Manzano, H
Dolado, JS
Ayuela, A
AF Manzano, H.
Dolado, J. S.
Ayuela, A.
TI Aluminum Incorporation to Dreierketten Silicate Chains
SO JOURNAL OF PHYSICAL CHEMISTRY B
LA English
DT Article
ID C-S-H; HYDRATED PORTLAND CEMENTS; TRICALCIUM SILICATE;
MOLECULAR-DYNAMICS; AL-27; NMR; SI-29; PASTES; MODELS; SLAG
AB This work explores, from a theoretical viewpoint, the aluminum incorporation
into silicate chains with dreierketten conformation relevant in the cementitious
calcium-silicate-hydrate (C-S-H) gel and in other minerals, such as wollastonite
and hillebrandite. To this end, we have investigated by means of ab initio
calculations both the stability and the formation of aluminosilicate chains. Our
results show that only certain aluminosilicate chains are stable, namely, those
whose tetrahedra length m obey the m = 3n - 1 rule with n = 1, 2, 3,..., in
agreement with experiments. Moreover, our detailed analyses explain why Al ions
prefer the bridging sites and introduce new insights on the growth process.
C1 [Ayuela, A.] CSIC UPV EHU, Ctr Fis Mat, Fac Quim, Dept Fis Mat, San Sebastian
20018, Spain.
[Manzano, H.; Dolado, J. S.] LABEIN Tecnalia, Derio 49160, Spain.
[Dolado, J. S.] CSIC, Associated Unit LABEIN Tecnalia, Nanostruct & Ecoefficient
Mat Construct Unit, Madrid, Spain.
[Ayuela, A.] Donostia Int Phys Ctr, San Sebastian 20018, Spain.
C3 Consejo Superior de Investigaciones Cientificas (CSIC); University of
Basque Country; CSIC - UPV EHU - Centro de Fisica de Materiales (CFM);
Consejo Superior de Investigaciones Cientificas (CSIC)
RP Ayuela, A (corresponding author), CSIC UPV EHU, Ctr Fis Mat, Fac Quim, Dept Fis
Mat, San Sebastian 20018, Spain.
EM swxayfea@sw.ehu.es
RI Manzano, Hegoi/A-2984-2010; Dolado, Jorge Sanchez/ABF-9005-2020; Ayuela,
Andres/Y-9598-2019; Dolado, Jorge S/Q-1815-2016
OI Manzano, Hegoi/0000-0001-7992-2718; Dolado, Jorge
Sanchez/0000-0003-3686-1438; Dolado, Jorge S/0000-0003-3686-1438;
Ayuela, Andres/0000-0001-9611-9556
FU EITE association; Basque Government; Intramural Special Project
[20006601242]; Spanish MEC [MAT2005-03890, FIS2007-66711-C02-C01];
European Network of Excellence NANO-QUANTA [NM-CT-2004-500198)]
FX H. Manzano acknowledges the grant received from the EITE association.
Thanks are due to the Basque Government for funding the NANOMATERIALES
project, under the ETORTEK program. We also wish to acknowledge the
Intramural Special Project (Ref. 20006601242), the Spanish MEC Grants
MAT2005-03890 and FIS2007-66711-C02-C01, and the European Network of
Excellence NANO-QUANTA (NM-CT-2004-500198). The computing resources from
the Supercomputation Center of Galicia (CESGA) and the Universidad del
Pais Vasco (SGIker ARINA) are gratefully acknowledged. Finally, we thank
Prof. N. H. March for reading this manuscript.
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NR 34
TC 64
Z9 70
U1 0
U2 39
PI WASHINGTON
SN 1520-6106
EI 1520-5207
J9 J PHYS CHEM B
JI J. Phys. Chem. B
PD MAR 5
PY 2009
VL 113
IS 9
BP 2832
EP 2839
DI 10.1021/jp804867u
PG 8
WC Chemistry, Physical
SC Chemistry
GA 412NY
UT WOS:000263732700035
PM 19708114
DA 2023-12-05
ER
PT J
AU Xiao, YP
Reuter, MA
Boin, U
AF Xiao, YP
Reuter, MA
Boin, U
TI Aluminium recycling and environmental issues of salt slag treatment
SO JOURNAL OF ENVIRONMENTAL SCIENCE AND HEALTH PART A-TOXIC/HAZARDOUS
SUBSTANCES & ENVIRONMENTAL ENGINEERING
LA English
CT 2nd International Conference on Environmental Concerns
CY OCT 12-15, 2004
CL Xiamen, PEOPLES R CHINA
DE aluminum cycle; scrap recycling; metal yield; recyclability; salt slag;
environmental impact
AB Environmental friendly recycling is the trend toward total recycling of
aluminium metal. In the secondary aluminium industry, due to the complexity of
compositions and contaminants in the various types of aluminium scraps, an
understanding of the behavior of different scraps during melting is crucial in the
recycling process. Salt slags are the byproducts of the secondary aluminium
industry, which should be recycled and processed in a proper way by taking the
environmental impact into consideration. This article provides qualitative
assessment on 10 different commercial aluminium scraps for their relative
recyclability via well-designed and controlled laboratory experiments. It confirms
that more nonmetallic contaminants, smaller size, and higher ratio of surface area
to body volume generally lead to a lower metal recovery. Recycling the scraps with
lower recyclability normally generates more salt slags. High slag viscosity leads
to more fine aluminum metal entrapped in the salt slag and thus increases the load
of salt slag recycling. It was found that viscosity of the salt flux is increased
with the amount of entrapped nonmetallic components, which affect the settling of
heavier materials. In addition, the slag samples from the melting tests were
leached and analyzed to evaluate the behavior of carbon containing scrap. The
elevated carbon content in the scrap resulted in more-carbide formation in salt
slags and thus more methane generation in salt slag recycling with a higher
environmental impact.
C1 Delft Univ Technol, NL-2628 RX Delft, Netherlands.
C3 Delft University of Technology
RP Xiao, YP (corresponding author), Delft Univ Technol, Mijnbouwstr 120, NL-2628 RX
Delft, Netherlands.
EM y.xiao@ta.tudelft.nl
RI Reuter, Markus A/D-2839-2015; Reuter, Markus/M-5565-2019
OI Reuter, Markus A/0000-0003-0500-4863; Reuter, Markus/0000-0003-0500-4863
CR Janz G. J., 1968, MOLTEN SALTS ELECT C, V1
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Xiao Y, 2000, FOURTH INTERNATIONAL SYMPOSIUM ON RECYCLING OF METALS AND
Ye JA, 1996, MATER T JIM, V37, P170, DOI 10.2320/matertrans1989.37.170
NR 7
TC 64
Z9 68
U1 1
U2 38
PI PHILADELPHIA
SN 1093-4529
EI 1532-4117
J9 J ENVIRON SCI HEAL A
JI J. Environ. Sci. Health Part A-Toxic/Hazard. Subst. Environ. Eng.
PY 2005
VL 40
IS 10
BP 1861
EP 1875
DI 10.1080/10934520500183824
PG 15
GA 969ZX
UT WOS:000232276100004
PM 16194908
DA 2023-12-05
ER
PT J
AU Chen, X
Sutrisno, A
Struble, LJ
AF Chen, Xu
Sutrisno, Andre
Struble, Leslie J.
TI Effects of calcium on setting mechanism of metakaolin-based geopolymer
LA English
DT Article
DE calcium; C-A-S-H; dissolution; geopolymer; NMR; setting; Si/Al
ID A-S-H; ALKALINE ACTIVATION; FLY-ASH; SILICATE HYDRATE; GEL; ALUMINUM;
ALUMINOSILICATE; DISSOLUTION; HYDROXIDE; SLAG
AB Geopolymer setting is seen to be substantially accelerated by addition of
calcium and the objective of this study was to determine the mechanism for this
effect by examining metakaolin geopolymers with and without calcium. Solid-state
Al-27 NMR tests were used to examine the dissolution extent both qualitatively and
quantitatively. Solid-state Si-29 NMR tests were conducted to determine the amount
and structure of each phase. Prior to the quantitative tests, chemical extractions
were used to facilitate assignment of peaks in each spectrum. On addition of
calcium, it was found that both the rate and the extent of metakaolin dissolution
were enhanced. Accelerating dissolution increases the Al concentration in solution,
thus reducing Si/Al available for geopolymer gel formation and further accelerating
the gel formation to cause faster setting. Although C-A-S-H was observed in the
calcium mix, no evidence indicated that it is directly involved in setting.
C1 [Chen, Xu; Struble, Leslie J.] Univ Illinois, Dept Civil & Environm Engn,
Urbana, IL USA.
[Sutrisno, Andre] Univ Illinois, NMR EPR Lab, Sch Chem Sci, Urbana, IL USA.
C3 University of Illinois System; University of Illinois Urbana-Champaign;
University of Illinois System; University of Illinois Urbana-Champaign
RP Chen, X (corresponding author), Univ Delaware, Dept Civil & Environm Engn,
Newark, DE 19716 USA.
EM xuchen@udel.edu
RI Sutrisno, Andre/N-9908-2015
OI Sutrisno, Andre/0000-0003-2308-5708; Chen, Xu/0000-0002-6813-2849
FU National Science Foundation [DMR 10-08109]
FX National Science Foundation, Grant/Award Number: DMR 10-08109
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10.1016/j.cemconres.2007.11.001
10.1016/j.cemconres.2004.10.042
NR 56
TC 63
Z9 66
U1 11
U2 95
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD FEB
PY 2018
VL 101
IS 2
BP 957
EP 968
DI 10.1111/jace.15249
PG 12
GA FO5WW
UT WOS:000416933700048
DA 2023-12-05
ER
PT J
AU Wang, C
Verma, N
Kwon, Y
Tiekink, W
Kikuchi, N
Sridhar, S
AF Wang, Cong
Verma, Neerav
Kwon, Youjong
Tiekink, Wouter
Kikuchi, Naoki
TI A Study on the Transient Inclusion Evolution during Reoxidation of a
Fe-Al-Ti-O Melt
LA English
DT Article
DE inclusions; reoxidation; transient stage
ID ALUMINUM OXIDE; SOLID SOLUTION; MOLTEN STEEL; TITANIUM; BEHAVIOR;
SYSTEM; NOZZLE; AL2O3; SLAGS
AB The effect of a simulated reoxidizing environment on the chemical and
morphological evolution of nonmetallic oxide inclusions was studied. Additions of
545 ppm and 274 ppm of soluble oxygen were introduced to an Al killed melt
containing approximately 600 ppm of Ti and 600 ppm of Al. It was found that
inclusion chemistry evolved from Al(2)O(3), Al(2)TiO(5) and eventually to Ti(3)O(5)
for the higher oxygen addition case and to Al-Ti complex oxides for the lower
oxygen addition one. Morphologically, it was observed that irregular inclusions
gradually were replaced by spherical ones during the reoxidation process. These
changes are discussed through the coupling of thermodynamic prediction and
experimental conditions, and considerations on the local variations of O and
metallic element activities.
C1 [Wang, Cong; Verma, Neerav; Kwon, Youjong; Sridhar, Seetharaman] Carnegie Mellon
Univ, Dept Mat Sci & Engn, Ctr Iron & Steelmaking Res, Pittsburgh, PA 15213 USA.
[Tiekink, Wouter] Tata Steel Res Dev & Technol, NL-1970 CA Ijmuiden,
Netherlands.
[Kikuchi, Naoki] JFE Steel Corp, Steelmaking Res Dept, Steel Res Lab, Hiroshima
7218510, Japan.
[Sridhar, Seetharaman] Natl Energy Technol Lab, Pittsburgh, PA 15236 USA.
C3 Carnegie Mellon University; JFE Holdings, Inc.; JFE Steel; United States
Department of Energy (DOE); National Energy Technology Laboratory - USA
RP Wang, C (corresponding author), Carnegie Mellon Univ, Dept Mat Sci & Engn, Ctr
Iron & Steelmaking Res, 5000 Forbes Ave, Pittsburgh, PA 15213 USA.
EM sridhars@andrew.cmu.edu
RI Wang, Cong/E-8156-2011
OI Wang, Cong/0000-0002-1684-1184
FU Center for Iron and Steelmaking Research (CISR)
FX The authors would like to acknowledge the Center for Iron and
Steelmaking Research (CISR) for financial support.
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NR 30
TC 63
Z9 68
U1 0
U2 10
PI TOKYO
JAPAN
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2011
VL 51
IS 3
BP 375
EP 381
PG 7
GA 742FS
UT WOS:000288927300006
OA gold
DA 2023-12-05
ER
PT J
AU Tsai, CJ
Huang, R
Lin, WT
Wang, HN
AF Tsai, Chia-Jung
Huang, Ran
Lin, Wei-Ting
Wang, His-Ning
TI Mechanical and cementitious characteristics of ground granulated blast
furnace slag and basic oxygen furnace slag blended mortar
LA English
DT Article
ID STEEL SLAG; PORTLAND-CEMENT; HYDRATION; STRENGTH; IRON; REPLACEMENT;
DURABILITY; CONCRETE
AB Reusing waste materials and reducing carbon emissions are crucial environmental
concerns. Ground granulated basic oxygen furnace slag (GGBOS) and ground granulated
blast furnace slag (GGBS) are the by-products of the steel industry and has
positive effects on the environment because it reduces the problems associated
waste disposal. This study reused these two products to completely replace
cementitious materials, thus contributing to waste recycling, reducing the
production demand for cement, and mitigating carbon emissions. Twelve mixture
proportions were designed in this study, including an ordinary Portland mortar
(OPM) as the control group and 11 steel/iron slag blended mortar (SISBM)
experimental groups for the mechanical and cementitious characteristic experiments.
The optimal mixing ratio for SISBM compressive strength ranged from GGBOS (steel
slag): GGBS (iron slag) = 3: 7 to 5: 5 (by weight). At the age of 91 days, the
compressive strength of SISBM reached 80-90% compared with that of the control
group. Based on the pH values, free-CaO, and microanalysis results, the
cementitious characteristics were mainly generated because the GGBOS increased the
free-CaO or Ca(OH)(2) concentrations in the SISBM curing water and provided
alkaline environments for Ca(OH)(2) to engage in the pozzolanic reaction with the
SiO2 and Al2O3 in GGBS, forming crystals such as calcium aluminum silicate hydrate,
(C-A-S-H), calcium silicate hydrate (C-S-H), and calcium-magnesium-alumina-
silicate (C-M-A-S), which generated strength and strengthened microstructure. (C)
C1 [Tsai, Chia-Jung; Wang, His-Ning] Natl Taiwan Ocean Univ, Inst Mat Engn, Keelung
20224, Taiwan.
[Huang, Ran] Natl Taiwan Ocean Univ, Dept Harbor & River Engn, Keelung 20224,
Taiwan.
[Lin, Wei-Ting] Natl Ilan Univ, Dept Civil Engn, Ilan 26047, Taiwan.
[Lin, Wei-Ting] Atom Energy Council, Inst Nucl Energy Res, Taoyuan 32546,
Taiwan.
C3 National Taiwan Ocean University; National Taiwan Ocean University;
National Ilan University; Institute of Nuclear Energy Research - Taiwan
RP Lin, WT (corresponding author), Natl Ilan Univ, Dept Civil Engn, Ilan 26047,
Taiwan.
EM wtlin@niu.edu.tw
RI Lin, Wei-Ting/AAE-4900-2021
OI Lin, Wei-Ting/0000-0003-4792-4457; Tsai, Chia-Jung/0000-0003-4872-3147
CR [Anonymous], 2009, CEMENT SUSTAINABILIT
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10.1016/j.conbuildmat.2011.06.018
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10.1016/j.ijggc.2008.06.001
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10.1016/j.jenvman.2010.04.008
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10.1016/j.cemconres.2007.03.008
10.1016/j.cemconcomp.2008.05.005
Lee CL, 2012, MATER DESIGN, V37, P28, DOI 10.1016/j.matdes.2011.12.030
Li JX, 2011, CEMENT CONCRETE RES, V41, P324, DOI 10.1016/j.cemconres.2010.11.018
10.1016/j.conbuildmat.2008.02.015
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8846(99)00028-9
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9465(98)00032-8
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10.5923/J.JCE.20120206.07]
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Samet B, 2004, CEMENT CONCRETE RES, V34, P1153, DOI
10.1016/j.cemconres.2003.12.021
Siddique R, 2012, RESOUR CONSERV RECY, V69, P29, DOI
10.1016/j.resconrec.2012.09.002
Wang G, 2010, CONSTR BUILD MATER, V24, P1961, DOI
10.1016/j.conbuildmat.2010.04.004
Wang Q, 2012, CONSTR BUILD MATER, V35, P8, DOI 10.1016/j.conbuildmat.2012.02.085
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10.1016/j.conbuildmat.2009.12.028
Wee TH, 1999, CEMENT CONCRETE COMP, V21, P59, DOI 10.1016/S0958-9465(98)00039-0
Wu XQ, 1999, CEMENT CONCRETE RES, V29, P1103
10.1016/j.conbuildmat.2012.06.023
10.1016/j.resconrec.2011.09.003
NR 31
TC 62
Z9 66
U1 1
U2 53
PU ELSEVIER SCI LTD
PI OXFORD
SN 0264-1275
EI 1873-4197
J9 MATER DESIGN
JI Mater. Des.
PD AUG
PY 2014
VL 60
BP 267
EP 273
DI 10.1016/j.matdes.2014.04.002
PG 7
GA AI2DQ
UT WOS:000336668000033
DA 2023-12-05
ER
PT J
AU Zhu, X
Hou, HB
Huang, XQ
Zhou, M
Wang, WX
AF Zhu Xi
Hou Haobo
Huang Xuquan
Zhou Min
Wang Weixing
TI Enhance hydration properties of steel slag using grinding aids by
mechanochemical effect
LA English
DT Article
DE Steel slag; Grinding aids; Mechanochemical effect; Hydration
AB Basic oxygen furnace steel slag is a kind of cementitious material with low
activity and hard for grinding. The objective of this work was to validate specious
grinding aids F1 made in lab which was effective for the grinding of steel slag,
thus enhancing the hydration properties. By using 0.05% F1, the Blaine value of
steel slag was added up to 361.3 m(2)/kg, the portion of size which is normally
smaller than 30 mu m was increased and its particle size distribution turned
homogeneous. The exothermic rate was increased after 8 h, and the enhancement of
hydration properties was more obvious at early age. More calcium aluminum hydrate
was generated at 3 days, and the pastes structure tissue became dense after 28
days. (C) 2011 Elsevier Ltd. All rights reserved.
C1 [Zhu Xi; Hou Haobo; Huang Xuquan; Zhou Min; Wang Weixing] Wuhan Univ, Sch
Resource & Environm Sci, Wuhan 430072, Hubei, Peoples R China.
C3 Wuhan University
RP Zhu, X (corresponding author), Wuhan Univ, Sch Resource & Environm Sci, Wuhan
EM zhuxi_whu@163.com
CR Binici H, 2007, POWDER TECHNOL, V177, P140, DOI 10.1016/j.powtec.2007.03.033
Choi WS, 2004, INT J MINER PROCESS, V74, pS165, DOI 10.1016/j.minpro.2004.07.025
Dressel D, 2010, ZKG INT, V63, P43
Feng Shuxia, 2010, J CHIN CER SOC, V38, P39
Katsioti M, 2009, CONSTR BUILD MATER, V23, P1954, DOI
10.1016/j.conbuildmat.2008.09.003
Luckman M., 2009, CEMENT CONCRETE RES, V39, P102
10.1016/j.conbuildmat.2007.03.019
Shen WG, 2009, J HAZARD MATER, V164, P99, DOI 10.1016/j.jhazmat.2008.07.125
Teoreanu I, 1999, CEMENT CONCRETE RES, V29, P9, DOI 10.1016/S0008-8846(98)00180-
X
10.1016/j.conbuildmat.2009.12.028
NR 10
TC 62
Z9 67
U1 2
U2 70
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD APR
PY 2012
VL 29
BP 476
EP 481
DI 10.1016/j.conbuildmat.2011.10.064
PG 6
GA 903XS
UT WOS:000301156800059
DA 2023-12-05
ER
PT J
AU Li, JY
Wang, N
Xu, RK
Tiwari, D
AF Li Jiu-Yu
Wang Ning
Xu Ren-Kou
Tiwari, D.
TI Potential of Industrial Byproducts in Ameliorating Acidity and Aluminum
Toxicity of Soils Under Tea Plantation
SO PEDOSPHERE
LA English
DT Article
DE acid soil; alkaline slag; amelioration; coal fly ash; red mud
ID AQUEOUS-SOLUTIONS; RED MUD; PHOSPHOGYPSUM; ADSORPTION; AMENDMENTS;
FLUORIDE; RESIDUE
AB It is imperative to choose some low cost, available and effective ameliorants to
correct soil acidity in southern China for sustainable agriculture. The present
investigation dealt with the possible role of industrial byproducts, i.e., coal fly
ash (CFA), alkaline slag (AS), red mud (RM) and phosphogypsum (PG) in correcting
acidity and aluminum (Al) toxicity of soils under tea plantation using an indoor
incubation experiment. Results indicated that CFA, AS and RM increased soil pH,
while PG decreased the pHs of an Ultisol and an Alfisol. The increment of soil pH
followed the order of RM > AS > CFA. All the industrial byproducts invariably
decreased exchangeable Al and hence increased exchangeable Ca, Mg, K and Na and
effective cation exchange capacity. RM, AS and lime decreased total soluble Al,
exchangeable Al and organically bound Al. Formation and retention of hydroxyl-Al
polymers were the principal mechanism through which Al phytotoxicity was alleviated
by application of these amendments. In addition, the heavy metal contents in the
four industrial byproducts constituted a limited environmental hazard in a short
time at the rates normally used in agriculture. Therefore, the short-term use of
the byproducts, especially AS and RM, as amendments for soil acidity and Al
toxicity in acid soils may be a potential alternative to the traditional use of
mined gypsum and lime.
C1 [Li Jiu-Yu; Wang Ning; Xu Ren-Kou] Chinese Acad Sci, Inst Soil Sci, State Key
Lab Soil & Sustainable Agr, Nanjing 210008, Peoples R China.
[Tiwari, D.] Mizoram Univ, Dept Chem, Aizawl 796009, India.
[Li Jiu-Yu] Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China.
C3 Chinese Academy of Sciences; Institute of Soil Science, CAS; Mizoram
University; Chinese Academy of Sciences; University of Chinese Academy
of Sciences, CAS
RP Xu, RK (corresponding author), Chinese Acad Sci, Inst Soil Sci, State Key Lab
EM rkxu@issas.ac.cn
FU International Foundation of Science [C/4073-1]; National "Eleventh Five
Years Plan" Key Project on Science and Technology of China
[2006BAD05B02, 2009BADC6B02]
FX Supported by the International Foundation of Science (No. C/4073-1) and
the National "Eleventh Five Years Plan" Key Project on Science and
Technology of China (Nos. 2006BAD05B02 and 2009BADC6B02).
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NR 38
TC 62
Z9 82
U1 5
U2 82
PU SCIENCE PRESS
PI BEIJING
PA 16 DONGHUANGCHENGGEN NORTH ST, BEIJING 100717, PEOPLES R CHINA
SN 1002-0160
EI 2210-5107
J9 PEDOSPHERE
JI Pedosphere
PD OCT
PY 2010
VL 20
IS 5
BP 645
EP 654
DI 10.1016/S1002-0160(10)60054-9
PG 10
WC Soil Science
SC Agriculture
GA 670FW
UT WOS:000283407600011
DA 2023-12-05
ER
PT J
AU Thy, P
Jenkins, BM
Lesher, CE
Grundvig, S
AF Thy, P
Jenkins, BM
Lesher, CE
Grundvig, S
TI Compositional constraints on slag formation and potassium volatilization
from rice straw blended wood fuel
SO FUEL PROCESSING TECHNOLOGY
LA English
DT Article
DE biomass fuel; combustion; rice straw; wood; ash; slag; high temperature;
phase relations; liquidus; solidus; freezing point depression; potassium
loss
ID TEMPERATURE ELEMENTAL LOSSES; INORGANIC-CHEMISTRY; BIOMASS; COMBUSTION;
ASH; BEHAVIOR
AB Experimental melting of biomass ash blends demonstrates that the addition of
rice straw to a dominantly wood-based fuel causes a marked freezing point
depression in the liquidus temperature of the inorganic slag from well above 2000 C
to a minimum of about 1260 C. The minimum temperature is achieved for ash blends
with about 30% rice straw ash. The melting interval (liquidus to solidus) for the
ash blends is typically 100-200 degrees C. The solidus shows a systematic decrease
from about 1350 degrees C to as low as 800 degrees C for pure rice straw ash.
Potassium is completely lost from slag for blends with less than 30% rice straw ash
content. The addition of more than 30% rice straw ash results in an enhanced
retention of potassium in the solid slag. Potassium loss for fuel blends with above
30% rice straw ash is further positively correlated with melting temperature. As
the temperature approaches the solidus, potassium is increasingly bound in the melt
as well as in potassium-aluminum silicate minerals (leucite) and, therefore,
partially retained in the slag. There are indications that melting temperatures
above the 'true' liquidus for rice straw-rich blends cause partial potassium loss
and consequently a rise in the liquidus. This will result in an apparent extending
of the melting interval for blends with above 30% rice straw ash. The liquidus
silicate mineralogy of the slag changes as a function of increasing rice straw ash
from larnite, to akermanite, wollastonite, and diopside. This mineralogical
sequence reflects an increase in the Si/Ca ratio and polymerization of the melt.
The experimental slag shows favorable similarities to the mineralogy and
composition of slag formed in commercial biomass-fueled boilers, suggesting that
the simplified conditions of the experimental melting study can be used to predict
combustion conditions in commercial biomass-fueled boilers. Thus, small additions
of straw to a predominantly wood fuel should have the effect of lowering slag
melting temperature and relatively reducing potassium loss to the flue gas. If
combustion temperature can be controlled to within, or below, the melting interval
of the ash (< 1260 degrees C), the relatively loss of potassium can be minimized.
Boiler operation below the minimum solidus temperature (similar to 1050 degrees C)
will further strongly restrict loss of potassium. (c) 2005 Elsevier B.V. All rights
reserved.
C1 Univ Calif Davis, Dept Geol, Davis, CA 95616 USA.
Univ Calif Davis, Dept Biol & Agr Engn, Davis, CA 95616 USA.
Aarhus Univ, Dept Earth Sci, DK-8000 Aarhus, Denmark.
C3 University of California System; University of California Davis;
University of California System; University of California Davis; Aarhus
University
RP Thy, P (corresponding author), Univ Calif Davis, Dept Geol, 1 Shields Ave,
Davis, CA 95616 USA.
EM thy@geology.ucdavis.edu
RI Lesher, Charles E/A-2468-2015
OI Lesher, Charles E/0000-0003-4033-4809; Jenkins,
Bryan/0000-0002-0490-3210; Thy, Peter/0000-0002-9267-5798
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NR 27
TC 62
Z9 68
U1 0
U2 27
PI AMSTERDAM
SN 0378-3820
J9 FUEL PROCESS TECHNOL
JI Fuel Process. Technol.
PD MAY
PY 2006
VL 87
IS 5
BP 383
EP 408
DI 10.1016/j.fuproc.2005.08.015
PG 26
WC Chemistry, Applied; Energy & Fuels; Engineering, Chemical
SC Chemistry; Energy & Fuels; Engineering
GA 024RE
UT WOS:000236212900002
DA 2023-12-05
ER
PT J
AU Ohta, H
Suito, H
AF Ohta, H
Suito, H
TI Thermodynamics of aluminum and manganese deoxidation equilibria in Fe-Ni
and Fe-Cr alloys
LA English
DT Article
DE Al deoxidation; interaction coefficient; Mn distribution; iron-nickel
alloy; iron-chromium alloy
ID LIQUID-IRON; OXYGEN; SLAGS; MELTS; NICKEL; AL; CHROMIUM; MNO; CO; MG
AB Aluminum deoxidation equilibrium and manganese distribution have been studied at
1 873 K in the equilibrium experiment between CaO-Al2O3 slags and Fe-10, 20, 40 and
60mass%Ni alloys or Fe-10, 20 and 40mass%Cr alloys containing Mn and Al. On the
basis of these results, the effect of Ni or Cr on the activity coefficients of Al
and Mn based on liquid iron is discussed and the interaction coefficient between Al
and 0 in liquid iron has been estimated. Some experiments in which Fe-18mass%Cr-
8mass%Ni alloy containing Al and Mn was equilibrated with CaO-Al2O3 slags have been
carried out at 1 873 K. It was found that the observed values for the oxygen
content and the Mn distribution ratio in Fe-18mass%Cr-8 mass%Ni alloy are in good
agreement with the calculated values by using the activity coefficients of Al and
Mn obtained in this study.
C1 Tohoku Univ, Inst Multidisciplinary Res Adv Mat, Aoba Ku, Sendai, Miyagi
9808577, Japan.
RP Ohta, H (corresponding author), Tohoku Univ, Inst Multidisciplinary Res Adv Mat,
Aoba Ku, Sendai, Miyagi 9808577, Japan.
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NR 30
TC 62
Z9 70
U1 0
U2 17
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2003
VL 43
IS 9
BP 1301
EP 1308
PG 8
GA 724RC
UT WOS:000185499700002
OA gold
DA 2023-12-05
ER
PT J
AU Marion, M
Chauveau, C
Gokalp, I
AF Marion, M
Chauveau, C
Gokalp, I
TI Studies on the ignition and burning of levitated aluminum particles
SO COMBUSTION SCIENCE AND TECHNOLOGY
LA English
DT Article
DE aluminum combustion; high pressure combustion; electrodynamic
levitation; solid rocket motors; slag accumulation
ID SINGLE METAL-PARTICLE; COMBUSTION PHASE; DROPLET
AB An experimental set-up is developed to investigate the burning of levitated
aluminum particles ignited by a CO2 laser in air under high pressure conditions.
Residence times of aluminum particles burning in the electrodynamic levitator are
long enough to observe the total burning process, under normal and high pressures.
Experiments allow to measure the ignition delay and the burning times of aluminum
particles. These measurements and the accompanying high speed images give useful
information on the burning processes of aluminum particles under Various regimes. A
numerical model is also developed to predict the burning rates of aluminum
particles and the sizes of the alumina residues.
RP Marion, M (corresponding author), CNRS,LAB COMBUST & SYST REACTIFS,F-45071
ORLEANS 2,FRANCE.
RI Chauveau, Christian/A-4907-2010
OI Chauveau, Christian/0000-0001-9042-6256; GOKALP,
ISKENDER/0000-0002-2684-9622; Marion, Michael/0000-0002-1179-8666
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NR 36
TC 62
Z9 77
U1 1
U2 27
PU GORDON BREACH SCI PUBL LTD
PI READING
PA C/O STBS LTD, PO BOX 90, READING, BERKS, ENGLAND RG1 8JL
SN 0010-2202
J9 COMBUST SCI TECHNOL
JI Combust. Sci. Technol.
PY 1996
VL 115
IS 4-6
BP 369
EP &
DI 10.1080/00102209608935537
PG 23
Engineering, Chemical
GA WF999
UT WOS:A1996WF99900008
DA 2023-12-05
ER
PT J
AU Hung, TC
Huang, JS
Wang, YW
Lin, KY
AF Hung, Tu-Cheng
Huang, Jong-Shin
Wang, Yi-Wen
Lin, Kuei-Yi
TI Inorganic polymeric foam as a sound absorbing and insulating material
LA English
DT Article
DE Water absorption; Sound absorption coefficient; Sound transmission loss;
Inorganic polymeric foam
ID ALUMINUM FOAM; ACOUSTIC ABSORPTION; SANDWICH PANELS; IMMOBILIZATION;
GEOPOLYMERS; PROPERTY; SINGLE; PB
AB A mixture of 70% metakaolin and 30% blast furnace slag powders is used as the
raw material in the production of inorganic polymeric foams (IPF) with various
densities ranging from 0.4 to 1.0 g/cm(3) and different thicknesses of 6, 10 and 14
cm using a mechanical foaming method. The water absorptions, sound absorption
coefficients and sound transmission losses of the IPF specimens were measured and
then compared with each other to evaluate the effects of their density and
thickness. It was found that the variation of water absorption with respect to
density was similar to that of the noise reduction coefficient. In addition, the
sound transmission losses of sandwich panels with different-thickness and various-
density IPF cores were measured to determine if two faces of calcium silicate
boards can enhance their noise reducing effects. As a result, the feasibility of
using inorganic polymeric foam as a sound absorption and insulation material can be
evaluated. (C) 2013 Elsevier Ltd. All rights reserved.
C1 [Hung, Tu-Cheng; Huang, Jong-Shin; Wang, Yi-Wen] Natl Cheng Kung Univ, Dept
Civil Engn, Tainan 70101, Taiwan.
[Lin, Kuei-Yi] Council Labor Affairs, Inst Occupat Safety & Hlth, Taipei,
Taiwan.
C3 National Cheng Kung University
RP Huang, JS (corresponding author), Natl Cheng Kung Univ, Dept Civil Engn, Tainan
70101, Taiwan.
EM jshuang@mail.ncku.edu.tw
RI wang, yixuan/GXW-2866-2022; Wang, Yixuan/GZK-6559-2022; Wang,
Yijun/GXW-1763-2022; Wang, Yiru/JMB-2281-2023; Wang,
yanru/JAX-5241-2023; wang, yi/GVT-8516-2022
FU Institute of Occupational Safety and Health, Council of Labor Affairs,
Taiwan, R.O.C. through NCKU Research and Development Foundation [97C080]
FX The financial support of the Institute of Occupational Safety and
Health, Council of Labor Affairs, Taiwan, R.O.C., under contract number
97C080 through NCKU Research and Development Foundation is gratefully
acknowledged.
10.1016/j.cemconres.2004.06.005
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NR 21
TC 61
Z9 68
U1 1
U2 94
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JAN 15
PY 2014
VL 50
BP 328
EP 334
DI 10.1016/j.conbuildmat.2013.09.042
PG 7
GA 300UJ
UT WOS:000330489200038
DA 2023-12-05
ER
PT J
AU Feichtinger, S
Michelic, SK
Kang, YB
Bernhard, C
AF Feichtinger, Stefan
Michelic, Susanne K.
Kang, Youn-Bae
Bernhard, Christian
TI In Situ Observation of the Dissolution of SiO2
Particles in CaO-Al2O3-SiO2 Slags and
Mathematical Analysis of its Dissolution Pattern
LA English
DT Article
ID CALCIUM-ALUMINUM-SILICATE; CERAMIC SYSTEMS; MOLD FLUXES; DIFFUSION;
STEEL; INCLUSIONS; BEHAVIOR; AL2O3; MELTS; OPTIMIZATION
AB The dissolution of amorphous SiO2 particles in CaO-Al2O3SiO2 slags was
investigated at 1450 degrees C by high-temperature confocal scanning laser
microscopy (HT-CSLM) and thermodynamic/kinetic analyses. The SiO2 particles used in
this experimental study had a spherical form so that any rotation of the particle
did not cause errors in the determination of the particle size during the
dissolution. Moreover, a wide composition range of the slag could be chosen without
forming any solid reaction layer which could distort the evaluation of the
dissolution mechanism. The evolution of the diameter of the spherical SiO2 particle
was measured by image analysis of pictures obtained from the HT-CSLM. It was found
that the dissolution curve of the SiO2 particle (size as a function of time)
exhibited either a parabolic-like curve or an S-shaped curve depending on the slag
composition. The patterns were compared with a well-known shrinking core model
(SCM), and it was shown that the SCM could not represent the dissolution behavior
of the SiO2 particle observed in this study. It was experimentally found that the
shape of the dissolution curves varies as a function of the slag composition. The
curve exhibited a parabolic-like shape for low SiO2-containing slags and changed to
an S-type shape with increasing SiO2 concentration in the slag. To elucidate the
dissolution mechanism, a model based on approximations for the diffusion near the
particle was proposed by modifying the previously available model [M. J. Whelan,
Met. Sci. J., 3, 95-97 (1969)]. From the experimental data and the model
calculations, the viscosity of the slag was shown to be the major factor affecting
both dissolution rate and mechanism. Effective binary diffusion coefficients were
estimated using the model and experimental data. Those were shown to be in the
range of literature data.
C1 [Feichtinger, Stefan; Michelic, Susanne K.; Bernhard, Christian] Univ Leoben,
Chair Ferrous Met, A-8700 Leoben, Austria.
[Kang, Youn-Bae] Pohang Univ Sci & Technol POSTECH, Grad Inst Ferrous Technol,
Pohang 790784, Kyungbuk, South Korea.
C3 University of Leoben; Pohang University of Science & Technology
(POSTECH)
RP Kang, YB (corresponding author), Pohang Univ Sci & Technol POSTECH, Grad Inst
Ferrous Technol, Pohang 790784, Kyungbuk, South Korea.
EM ybkang@postech.ac.kr
RI Bernhard, Christian/AAS-9233-2020; Kang, Youn-Bae/AAU-5544-2021;
Michelic, Susanne/U-4610-2019
OI Bernhard, Christian/0000-0003-3976-9725; Kang,
Youn-Bae/0000-0003-0615-0168; Michelic, Susanne/0000-0002-4325-8648
FU Austrian Federal Government; Styrian Provincial Government; Steirische
Wirtschaftsfoerderungsgesellschaft mbH; POSCO Ltd.; Bundesministerium
fur Verkehr, Innovation und Technologie and the Bundesministerium fur
Wirtschaft, Familie und Jugend
FX The authors thank Prof. Chong Soo Lee, Prof. Hae-Geon Lee, Mr. In-Hyeon
Jeong, and other students of Graduate Institute of Ferrous Technology,
POSTECH, for their support for staying and carrying out the experiments
in Pohang, Republic of Korea. The contribution of Mr. Siegfried Schider
through assisting the experiments and evaluations in Leoben, Austria is
highly acknowledged. Financial support by the Austrian Federal
Government (in particular from the Bundesministerium fur Verkehr,
Innovation und Technologie and the Bundesministerium fur Wirtschaft,
Familie und Jugend) and the Styrian Provincial Government, represented
by Oesterreichische Forschungsfoerderungsgesellschaft mbH and by
Steirische Wirtschaftsfoerderungsgesellschaft mbH, within the research
activities of the K2 Competence Centre on "Integrated Research in
Materials, Processing and Product Engineering", operated by the
Materials Center Leoben Forschung GmbH in the framework of the Austrian
COMET Competence Centre Programme, is gratefully acknowledged. One of
the authors (YBK) also thanks POSCO Ltd. for the financial support
through Steel Innovation Program.
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NR 45
TC 61
Z9 66
U1 2
U2 44
PU WILEY-BLACKWELL
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD JAN
PY 2014
VL 97
IS 1
BP 316
EP 325
DI 10.1111/jace.12665
PG 10
GA 282UJ
UT WOS:000329198800039
DA 2023-12-05
ER
PT J
AU Pinto, ISS
Soares, HMVM
AF Pinto, Isabel S. S.
Soares, Helena M. V. M.
TI Selective leaching of molybdenum from spent hydrodesulphurisation
catalysts using ultrasound and microwave methods
SO HYDROMETALLURGY
LA English
DT Article
DE Spent catalysts; Molybdenum; Leaching; Ultrasound; Microwaves
ID SULFURIC-ACID BAKING; HYDROPROCESSING CATALYSTS; METAL RECOVERY;
EXTRACTION; DISSOLUTION; SLUDGE; COPPER; SLAG
AB Spent hydrodesulphurisation (HDS) catalysts from petroleum refineries, mostly
constituted by aluminium (Al), molybdenum (Mo), nickel (Ni) and cobalt (Co), are
classified as hazardous wastes and disposal is restricted by environmental
regulations; thus, the recovery of valuable metals is the most attractive option in
the processing of these residues. Selective Mo leaching from two spent HDS (Ni-Mo
or Co-Mo) catalysts, roasted at 500 degrees C, was studied using three different
approaches: conventional, ultrasound- and microwave-assisted methods. For the Ni-Mo
or Co-Mo catalysts, 77% and 84% of Mo extraction, respectively, was achieved when a
conventional (10 g/L NaOH. 80 degrees C, 120 min, S/L = 50 g/L) approach was used.
For both catalysts, ultrasound-assisted leaching (pulse 0.5 s and 20% amplitude)
with 10 g/L NaOH and S/L = 50 g/L led to 66% Mo dissolution after 10 min. Under
microwave-assisted (four cycles of 30 s) conditions, Mo leaching reached 89% and
91% for Ni-Mo and Co-Mo catalysts, respectively. The latter conditions represent
the best compromise between Mo extraction and selectivity, since Al dissolution was
between 6% and 9%. (C) 2012 Elsevier B.V. All rights reserved.
C1 [Pinto, Isabel S. S.; Soares, Helena M. V. M.] Univ Porto, Dept Engn Quim, Fac
Engn, REQUIMTE, P-4200465 Oporto, Portugal.
C3 Universidade do Porto
RP Soares, HMVM (corresponding author), Fac Engn Porto, Dept Engn Quim, Rua Dr
Roberto Frias, P-4200465 Oporto, Portugal.
EM hsoares@fe.up.pt
RI Soares, Helena/M-7466-2019; Soares, Helena MVM/D-5343-2013
OI Soares, Helena/0000-0002-5768-9182; Soares, Helena
MVM/0000-0002-5768-9182; Pinto, Isabel/0000-0001-8851-1515
FU FEDER funds through the Programa Operacional Factores de Competividade
(COMPETE); national funds from Fundacao para a Ciencia e Tecnologia
(FCT) [PEst-C/EQB/LA0006/2011]; FCT [SFRH/BD/70450/2010]; Fundação para
a Ciência e a Tecnologia [SFRH/BD/70450/2010] Funding Source: FCT
FX This work was financially supported by FEDER funds through the Programa
Operacional Factores de Competividade (COMPETE) and national funds from
Fundacao para a Ciencia e Tecnologia (FCT) within the project
PEst-C/EQB/LA0006/2011. I. Pinto acknowledges a grant scholarship
(SFRH/BD/70450/2010) financed by FCT.
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U1 3
U2 65
PI AMSTERDAM
SN 0304-386X
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD NOV
PY 2012
VL 129
BP 19
EP 25
DI 10.1016/j.hydromet.2012.08.008
PG 7
GA 049JE
UT WOS:000311978000004
DA 2023-12-05
ER
PT J
AU Park, DC
Jung, IH
Rhee, PCH
Lee, HG
AF Park, DC
Jung, IH
Rhee, PCH
Lee, HG
TI Reoxidation of Al-Ti containing steels by
CaO-Al2O3-MgO-SiO2 slag
LA English
DT Article
DE reoxidation; supersaturation; self-dissociation of SiO2; inclusion with
two-layer structure
ID MOLTEN STEEL; OXIDATION RATE; LIQUID STEEL; EQUILIBRIA; ALUMINUM
AB Reoxidation of liquid steel containing Al and Ti by 14%CaO-35%Al2O3-10%MgO-
41%SiO2 (in mass%) slag was investigated at 1 823 K with initial Al content of 820
mass ppm and Ti content varied from 100 to 500 mass ppm. It was observed that Al
and Ti in the steel were simultaneously oxidized by SiO2 in the slag, and the
soluble oxygen was supersaturated during the course, particularly with respect to
Al. Based on the experimental results, a new mechanism of the reoxidation reaction
was proposed, which involves chemical reactions both at the metal/slag interface
and in the bulk metal. Self-dissociation of SiO2 into Si and O at the slag/metal
interface was found to play an important role in both supersaturation of oxygen,
and subsequent formation of complex oxide inclusions. Formation of inclusions
having a two-layer structure where an Al2O3 core was enclosed by complex Al-Ti-O
oxide was explained in relation with supersaturation of oxygen in the steel.
C1 Pohang Univ Sci & Technol, Dept Mat Sci & Engn, Pohang 790784, South Korea.
Res Inst Sci & Technol, Pohang 790600, South Korea.
C3 Pohang University of Science & Technology (POSTECH)
RP Park, DC (corresponding author), Pohang Univ Sci & Technol, Dept Mat Sci & Engn,
San 31 Hyoja Dong, Pohang 790784, South Korea.
RI Jung, In-Ho/H-6838-2018
OI Jung, In-Ho/0000-0002-9744-7276
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NR 16
TC 61
Z9 64
U1 0
U2 15
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2004
VL 44
IS 10
BP 1669
EP 1678
PG 10
GA 864ZH
UT WOS:000224671400008
OA gold
DA 2023-12-05
ER
PT J
AU Gijbels, K
Pontikes, Y
Samyn, P
Schreurs, S
Schroeyers, W
AF Gijbels, Katrijn
Pontikes, Yiannis
Samyn, Pieter
Schreurs, Sonja
Schroeyers, Wouter
TI Effect of NaOH content on hydration, mineralogy, porosity and strength
in alkali/sulfate-activated binders from ground granulated blast furnace
slag and phosphogypsum
LA English
DT Article
DE Ground granulated blast furnace slag; Phosphogypsum; Supersulfated
cement; Alkali-activated binder
ID C-S-H; QUANTITATIVE PHASE-ANALYSIS; BUILDING-MATERIALS; CEMENT PASTE;
CALCIUM; ETTRINGITE; FTIR; WATER; LIME; CARBONATION
AB This study investigates the effect of NaOH content on alkali/sulfate-activated
binders from 90 wt% ground granulated blast furnace slag (GGBFS) and 10 wt%
phosphogypsum (PG). Alkali activators were prepared with a NaOH molarity ranging
from 0 M to 4 M. The hydration was monitored using in-situ X-ray diffraction (XRD)
and isothermal calorimetry. The hydration product assemblage was investigated using
XRD, thermogravimetric analysis (TGA), Fourier-transformed infrared (FTIR)
spectroscopy, nitrogen adsorption/desorption and compressive strength tests. A
molarity of 0 M NaOH gave rise to the highest porosity and highest strength,
although setting occurred only after 7 days. From a molarity of 2 M NaOH and
higher, ettringite disappeared and got replaced by a monosulfate phase (i.e.,
NaCa4Al2O6(SO4)(1)(.5)center dot 15H(2)O) and amorphous aluminum-hydroxide. This
study shows the potential of using GGBFS and PG for the development of novel by-
product based cementitious binders.
C1 [Gijbels, Katrijn; Schreurs, Sonja; Schroeyers, Wouter] Hasselt Univ, CMK, Nucl
Technol Ctr, Agoralaan,Gebouw H, B-3590 Diepenbeek, Belgium.
[Pontikes, Yiannis] Katholieke Univ Leuven, Dept Mat Engn, Kasteelpk Arenberg
44, B-3001 Leuven, Belgium.
[Samyn, Pieter] Hasselt Univ, IMO IMOMEC, Appl & Analyt Chem, Agoralaan,Gebouw
D, B-3590 Diepenbeek, Belgium.
C3 Hasselt University; KU Leuven; Hasselt University
RP Gijbels, K (corresponding author), Hasselt Univ, CMK, Nucl Technol Ctr,
Agoralaan,Gebouw H, B-3590 Diepenbeek, Belgium.
EM katrijn.gijbels@uhasselt.be; yiannis.pontikes@kuleuven.be;
pieter.samyn@uhasselt.be; sonja.schreurs@uhasselt.be;
wouter.schroeyers@uhasselt.be
RI Samyn, Pieter/ABE-8557-2020; Schroeyers, Wouter/ADI-6064-2022
OI Samyn, Pieter/0000-0002-2180-7925; Schreurs, Sonja/0000-0002-6816-8737;
Schroeyers, Wouter/0000-0001-9899-5269
FU Fund for Scientific Research Flanders (FWO); COST Action [TU1301]
FX This work was supported by the Fund for Scientific Research Flanders
(FWO). The authors would like to thank the networking support of the
COST Action TU1301, www.norm4building.org.Marcin Selent (University of
Oulu, Finland) and Kristof Van Hecke (University of Ghent, Belgium) are
gratefully acknowledged for their valuable feedback with respect to XRD.
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NR 92
TC 60
Z9 61
U1 10
U2 85
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD JUN
PY 2020
VL 132
AR 106054
DI 10.1016/j.cemconres.2020.106054
PG 13
GA LU6EK
UT WOS:000537846000018
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Ji, ZH
Pei, YS
AF Ji, Zehua
Pei, Yuansheng
TI Immobilization efficiency and mechanism of metal cations
(Cd2+, Pb2+ and Zn2+) and anions
(AsO43- and
Cr2O72-) in wastes-based geopolymer
LA English
DT Article
DE Drinking water treatment residual; Heavy metals; Immobilization
mechanism; MAS-NMR
ID ORE PROCESSING RESIDUE; ASH-BASED GEOPOLYMER; HEAVY-METALS; FLY-ASH;
ALKALI-ACTIVATION; RISK-ASSESSMENT; SEDIMENTS; ADSORPTION; STRENGTH;
REMOVAL
AB In this study, a composite geopolymer based on solid wastes (drinking water
treatment residue (DWTR) and granulated blast furnace slag (GBFS)) were used in
immobilization of heavy metals cations (Cd2+, Pb2+ and Zn2+) and anions (AsO43- and
Cr2O72-). For evaluating the immobilization effect for heavy metals, the mechanical
strength and leaching properties of geopolymers were investigated. Meanwhile,
different characterization methods were used to research the immobilization
mechanisms. The results indicated that the mechanical strength of geopolymers
containing heavy metals was effectively improved by 37.11% with addition of DWTR.
The stability of metals in geopolymer were increased and the release risk was
decreased under the effect of DWTR. Characterization results verified the uniform
distribution of heavy metals in geopolymer, and the adding of Pb2+, AsO43- and
Cr2O72- caused the formation of crystalline phases. After the adding of heavy
metals, the chemical environment change of Al 2p is more significant than Si 2p.
Based on Si-29 and Al-27 MAS-NMR results, the different metals show various
influences on the silicon and aluminum species in geopolymer matrix, and the
strength of polymerized structure is mainly based on the Q(4)(mAl).
C1 [Ji, Zehua; Pei, Yuansheng] Beijing Normal Univ, Minist Educ, Sch Environm, Key
Lab Water & Sediment Sci, Beijing 100875, Peoples R China.
C3 Beijing Normal University
RP Pei, YS (corresponding author), Beijing Normal Univ, Minist Educ, Sch Environm,
Key Lab Water & Sediment Sci, Beijing 100875, Peoples R China.
EM yspei@bnu.edu.cn
FU Major Science and Technology Program for Water Pollution Control and
Treatment [2018ZX07110004]; National Natural Science Foundation of China
[51579009, 51879012]; Beijing municipal science and technology plan
projects [Z181100005518005]
FX This work was financially supported by the Major Science and Technology
Program for Water Pollution Control and Treatment (Project no.
2018ZX07110004), the National Natural Science Foundation of China
(Project no. 51579009, 51879012) and the Beijing municipal science and
technology plan projects (Project no. Z181100005518005).
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NR 48
TC 60
Z9 65
U1 19
U2 148
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD FEB 15
PY 2020
VL 384
AR 121290
DI 10.1016/j.jhazmat.2019.121290
PG 11
GA LR2YM
UT WOS:000535561100073
PM 31581019
DA 2023-12-05
ER
PT J
AU Park, JS
Park, JH
AF Park, Jun Seok
Park, Joo Hyun
TI Effect of Slag Composition on the Concentration of
Al2O3 in the Inclusions in Si-Mn-killed Steel
LA English
DT Article
ID FERRITIC STAINLESS-STEEL; 1 873 K; CAO-SIO2-MNO SLAG; DEOXIDATION
EQUILIBRIUM; SULFIDE CAPACITY; DISSOLUTION MECHANISM; ALUMINUM
DEOXIDATION; INTERFACIAL REACTION; RAMAN-SPECTRA; BEHAVIOR
AB The thermodynamic equilibria between CaO-Al2O3-SiO2-CaF2-MgO(-MnO) slag and Fe-
1.5 mass pct Mn-0.5 mass pct Si-0.5 mass pct Cr melt was investigated at 1873 K
(1600 A degrees C) in order to understand the effect of slag composition on the
concentration of Al2O3 in the inclusions in Si-Mn-killed steels. The composition of
the inclusions were mainly equal to (mol pct MnO)/(mol pct SiO2) = 0.8(+/- 0.06)
with Al2O3 content that was increased from about 10 to 40 mol pct by increasing the
basicity of slag (CaO/SiO2 ratio) from about 0.7 to 2.1. The concentration ratio of
the inclusion components, , and the activity ratio of the steel components, ,
showed a good linear relationship on a logarithmic scale, indicating that the
activity coefficient ratio of the inclusion components, , was not significantly
changed. From the slag-steel-inclusion multiphase equilibria, the concentration of
Al2O3 in the inclusions was expressed as a linear function of the activity ratio of
the slag components, on a logarithmic scale. Consequently, a compositional window
of the slag for obtaining inclusions with a low liquidus temperature in the Si-Mn-
killed steel treated in an alumina ladle is recommended. (C) The Minerals, Metals &
Materials Society and ASM International 2013
C1 [Park, Jun Seok] Univ Ulsan, Sch Mat Sci & Engn, Ulsan 680749, South Korea.
[Park, Joo Hyun] Hanyang Univ, Dept Mat Engn, Ansan 426791, South Korea.
C3 University of Ulsan; Hanyang University
RP Park, JH (corresponding author), Hanyang Univ, Dept Mat Engn, Ansan 426791,
South Korea.
EM basicity@hanyang.ac.kr
RI Park, Jun/HPH-3570-2023
FU National Research Foundation of Korea [22A20130012792] Funding Source:
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10.1016/j.jeurceramsoc.2010.07.020
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NR 47
TC 60
Z9 68
U1 2
U2 35
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD JUN
PY 2014
VL 45
IS 3
BP 953
EP 960
DI 10.1007/s11663-013-9998-2
PG 8
Engineering
GA AI6JW
UT WOS:000336980900019
DA 2023-12-05
ER
PT J
AU Valeev, D
Kunilova, I
Alpatov, A
Mikhailova, A
Goldberg, M
Kondratiev, A
AF Valeev, D.
Kunilova, I.
Alpatov, A.
Mikhailova, A.
Goldberg, M.
Kondratiev, A.
TI Complex utilisation of ekibastuz brown coal fly ash: Iron & carbon
separation and aluminum extraction
LA English
DT Article
DE Coal fly ash; Magnetic separation; Flotation; Autoclave acid leaching;
Aluminum extraction; Fly ash treatment
ID ACID-LEACHING METHOD; AMMONIUM-SULFATE; POWER-PLANT; KINETICS; GANGUE;
AL2O3; SIO2; SLAG; NANOPARTICLES; ADDITIVES
AB Fly ash landfills that accumulate a by-product of coal combustion and
gasification represent a permanent threat to the surrounding environment due to
many factors (air and water pollution, soil contamination, wildlife poisoning,
etc). Moreover, disposed coal fly ash may contain significant amounts of valuable
elements that are not extracted and potentially wasted. To improve the above
situation, a combined ash treatment process was developed for utilisation of the
coal fly ash waste from coal-fired power stations. The ash treatment includes three
stages: 1) magnetic separation of an iron-containing fraction, 2) carbon separation
by floatation, and 3) extraction of aluminum by the autoclave hydrochloric acid
leaching. The lab-scale results of the ash treatment applied to the Ekibastuz brown
coal fly ash from the Omsk power stations (Russia) were presented and discussed.
The XRD analysis showed that the fly ash consists primarily of quartz, mullite and
magnetite. It was found that the magnetic fraction separated at the first stage is
enriched in magnetite (over 20 wt %), the carbon content in the concentrate after
flotation increases to 27 wt %, and 90-95% of aluminum can be extracted during the
autoclave acid leaching. The SEM analysis showed that the magnetite phase is grown
on the surface of alumosilicate spheres as similar to 1 mu m cubic crystals. The
effect of the autoclave temperature and exposure time on the Al extraction
efficiency was also investigated and analysed in the present paper. The optimal
autoclave temperature and exposure time were found to achieve the maximum Al
extraction efficiency. It was also found by the SEM microanalysis that further
extraction of aluminum is not economically feasible since the remaining Al is
evenly surrounded by SiO2 in the fly ash particles. (C) 2019 Elsevier Ltd. All
rights reserved.
C1 [Valeev, D.] Russian Acad Sci, IP Bardin Lab Problems Met Complex Ores, Baikov
Inst Met & Mat Sci, Leninsky Prosp 49, Moscow 119334, Russia.
[Kunilova, I.] Russian Acad Sci, Lab 4 2 Complex Proc Nontradit Mineral Mat, Res
Inst Comprehens Exploitat Mineral Resources I, Kryukovskii Tupik 4, Moscow 111020,
Russia.
[Alpatov, A.] Russian Acad Sci, Lab Mat Diagnost, Baikov Inst Met & Mat Sci,
Leninsky Prosp 49, Moscow 119334, Russia.
[Mikhailova, A.] Russian Acad Sci, Lab Crystal Struct Studies, Baikov Inst Met &
Mat Sci, Leninsky Prosp 49, Moscow 119334, Russia.
[Goldberg, M.] Russian Acad Sci, Lab Ceram Composite Mat, Baikov Inst Met & Mat
Sci, Leninsky Prosp 49, Moscow 119334, Russia.
[Kondratiev, A.] Natl Univ Sci & Technol MISIS, Sci Res Ctr Thermochem Mat,
Leninsky Prosp 4, Moscow 119991, Russia.
C3 Russian Academy of Sciences; Baikov Institute of Metallurgy & Materials
Science (IMET RAS); Russian Academy of Sciences; Russian Academy of
Sciences; Baikov Institute of Metallurgy & Materials Science (IMET RAS);
Russian Academy of Sciences; Baikov Institute of Metallurgy & Materials
Science (IMET RAS); Russian Academy of Sciences; Baikov Institute of
Metallurgy & Materials Science (IMET RAS); National University of
Science & Technology (MISIS)
RP Valeev, D (corresponding author), Russian Acad Sci, IP Bardin Lab Problems Met
Complex Ores, Baikov Inst Met & Mat Sci, Leninsky Prosp 49, Moscow 119334, Russia.
EM dvaleev@imet.ac.ru; ecoreagent@yandex.ru; avalpatov@imet.ac.ru;
amikhailov@imet.ac.ru; mgoldberg@imet.ac.ru; al.v.kondratiev@gmail.com
RI Kunilova, Irina/AAA-6622-2022; Goldberg, Margarita A./D-8884-2017;
Kondratiev, Alex/G-9598-2015; Valeev, Dmitry/A-9683-2016; Kondratiev,
Alex/ABH-5376-2020; Kunilova, Irina/F-2960-2013; Mikhailova, Alexandra
A.B./M-4660-2017
OI Goldberg, Margarita A./0000-0003-1794-1889; Kondratiev,
Alex/0000-0001-6658-0421; Valeev, Dmitry/0000-0002-8820-7502;
Kondratiev, Alex/0000-0001-6658-0421; Kunilova,
Irina/0000-0002-7775-085X
FU Russian Science Foundation [18-79-00305]; Russian Government State Task
for Basic Research [075-00746-19-00]; Ministry of Education and Science
of the Russian Federation [11.7971.2017/6.7]; Russian Science Foundation
[18-79-00305] Funding Source: Russian Science Foundation
FX The present study was funded by the Russian Science Foundation project
No 18-79-00305. The analytical part of the work (X-ray, XRD, SEM, C and
S analysis) was carried out in accordance with the Russian Government
State Task for Basic Research No. 075-00746-19-00. One of the authors
(Kondratiev Alex) was financially supported by the Ministry of Education
and Science of the Russian Federation in the framework of the basic part
of the state program 'Organisation of the Research Work' for higher
educational institutions in 2017-2019 no. 11.7971.2017/6.7.
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NR 56
TC 59
Z9 62
U1 9
U2 118
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAY 1
PY 2019
VL 218
BP 192
EP 201
DI 10.1016/j.jclepro.2019.01.342
PG 10
& Ecology
GA HQ0UL
UT WOS:000462110400018
DA 2023-12-05
ER
PT J
AU Yaghoubi, M
Arulrajah, A
Disfani, MM
Horpibulsuk, S
Darmawan, S
Wang, J
AF Yaghoubi, Mohammadjavad
Arulrajah, Arul
Disfani, Mahdi Miri
Horpibulsuk, Suksun
Darmawan, Stephen
Wang, James
TI Impact of field conditions on the strength development of a geopolymer
stabilized marine clay
LA English
DT Article
DE Marine clay; Geopolymer; Strength; Curing conditions; Mineralogy
ID SOLIDS-TO-LIQUID; FLY-ASH; ACTIVATOR RATIOS; SOIL-GEOPOLYMER; ACID-RAIN;
CEMENT; SLAG; GEL
AB A soft marine clay was stabilized with fly-ash (FA) and slag (S) based
geopolymers. FA and S with combined contents of 10, 20 and 30% were added to the
soft clay and activated with a liquid alkaline activator (L) at various contents.
The clay was a marine clay which was dominated by quartz, illite and feldspar. The
effect of a number of preparation and curing factors including water content and
temperature variation, wetting-drying cycles and mixing time and method were
evaluated. The objective of this research was to evaluate the effect of these
factors that are likely to occur in ground improvement applications, such as deep
soil mixing, on the unconfined compressive strength (UCS), microstructure and
mineralogy of the mixtures. Results showed that increasing the FA + S content
increased the UCS values significantly through the geopolymerization process, which
was evident when increasing the FA + S content from 10% to 20%. Moreover, higher
UCS values were achieved when the curing temperature was increased and the strength
development was accelerated as a result of accelerated precipitation of FA and S.
Furthermore, strength development was enhanced when the L/(FA + S) ratio was
increased from 0.75 to 1.0, followed by a decrease at L/(FA + S) ratio of 1.25.
Similar trends of strength development were observed by varying the water contents
of 0.75, 1.0 and 1.25 liquid limit (LL) of the soil. The increased amount of
liquid, L and water, caused less favorable environment, such as lower L molarity
and less particle contact, for proper strength development. The UCS values
decreased for up to 6 cycles of wetting and drying, where the geopolymeric network
was not sufficiently stable, and remained almost constant afterwards. Increasing
the mixing time caused more dissolution of FA and S, which resulted in enhancement
of the UCS values. Adding FA + S and L to the soil separately resulted in higher
UCS values compared to when FA + S and L were mixed together initially and then
added to the soil. The microstructure and mineralogy analyses indicated that
increasing the curing temperature, as well as the L/(FA + S) ratio resulted in more
dissolution of FA and S and formation of calcium sodium aluminum silicate hydrate
(CNASH) products.
C1 [Yaghoubi, Mohammadjavad; Arulrajah, Arul] Swinburne Univ Technol, Dept Civil &
Construct Engn, Melbourne, Vic, Australia.
[Disfani, Mahdi Miri] Univ Melbourne, Dept Infrastruct Engn, Melbourne, Vic,
Australia.
[Horpibulsuk, Suksun] Suranaree Univ Technol, Ctr Excellence Innovat Sustainable
Infrastruct De, Sch Civil Engn, Nakhon Ratchasima, Thailand.
[Darmawan, Stephen] Geotesta Pty Ltd, Melbourne, Vic, Australia.
[Wang, James] Swinburne Univ Technol, Dept Mech Engn & Prod Design Engn,
Melbourne, Vic, Australia.
C3 Swinburne University of Technology; University of Melbourne; Suranaree
University of Technology; Swinburne University of Technology
RP Arulrajah, A (corresponding author), Swinburne Univ Technol, Dept Civil &
Construct Engn, Melbourne, Vic, Australia.
EM myaghoubi@swin.edu.au; aarulrajah@swin.edu.au;
mahdi.miri@unimelb.edu.au; suksun@g.sut.ac.th; sd@geotesta.com.au;
jawang@swin.edu.au
RI Disfani, M/F-8713-2015; Wang, James/JAD-0675-2023; Yaghoubi,
Mohammadjavad/AAL-8693-2020
OI Disfani, M/0000-0002-9231-8598; Yaghoubi,
Mohammadjavad/0000-0003-2246-0430; Wang, James/0000-0002-8497-9943;
Arulrajah, Arul/0000-0003-1512-9803; Darmawan,
Stephen/0000-0002-3013-1453; Horpibulsuk, Suksun/0000-0003-1965-8972
FU Australian Research Councils [LP150100043]; Thailand Research Fund under
the TRF Senior Research Scholar program [RTA5980005]; Suranaree
University of Technology; Australian Research Council [LP150100043]
Funding Source: Australian Research Council
FX This research was supported under Australian Research Councils Linkage
Projects funding scheme (project number LP150100043). The fourth author
is grateful to the financial support from the Thailand Research Fund
under the TRF Senior Research Scholar program Grant No. RTA5980005 and
Suranaree University of Technology.
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NR 50
TC 59
Z9 59
U1 1
U2 52
PU ELSEVIER
PI AMSTERDAM
SN 0169-1317
EI 1872-9053
J9 APPL CLAY SCI
JI Appl. Clay Sci.
PD JAN
PY 2019
VL 167
BP 33
EP 42
DI 10.1016/j.clay.2018.10.005
PG 10
GA HA0LV
UT WOS:000449900400004
DA 2023-12-05
ER
PT J
AU Kim, WH
Sohn, I
Min, DJ
AF Kim, W. H.
Sohn, I.
Min, D. J.
TI A Study on the Viscous Behaviour with K2O Additions in the
CaO-SiO2-Al2O3-MgO-K2O
Quinary Slag System
SO STEEL RESEARCH INTERNATIONAL
LA English
DT Article
DE Viscosity; BF slag; K2O; FT-IR; Ion compensation; Critical temperature
ID BLAST-FURNACE OPERATION; FULLY LIQUID SLAGS; SILICATE MELTS; VISCOSITY;
ALUMINUM; SPECTRA; MODEL; FEO; MGO
AB The viscosities of CaO-SiO2-20wt%Al2O3-10 wt%MgO-K2O quinary slags with CaO/SiO2
from 0.8 to 1.2 at 1773K with 1-5 wt% K2O additions were measured to estimate the
effect of K2O on the viscous behaviour of the slags. The measured viscosity at 1773
K increased with K2O addition at a fixed CaO/SiO2, which is contrary to the effect
of Na2O on the viscosity of BF slags. To qualitatively verify the changes in slag
structure, FT-IR spectroscopy was used. It was found that K2O induces Al2O3 to
behave as an acidic oxide by forming [AlO4](5-)-tetrahedral units by the ionic
compensation effect of K+ cations. However, regarding the effect of K2O on the
silicate structure, it is observed that K2O has a negligible effect due to the
consumption of O-2(-) with the formation of [AlO4](5-)-tetrahedral units.
Furthermore, it is also found that Si-O-Al bending became more complicated with K2O
additions, which supports the selective effect of K2O on the aluminate structure of
the slag. In spite of the more complicated structure with K2O additions, the
critical temperature (T-CR) decreased due to the gradual reduction of the liquidus
temperature (T-LO) of the slags.
C1 [Kim, W. H.; Sohn, I.; Min, D. J.] Yonsei Univ, Dept Mat Sci & Engn, Seoul
RP Min, DJ (corresponding author), Yonsei Univ, Dept Mat Sci & Engn, Seoul 120749,
South Korea.
EM chemical@yonsei.ac.kr
RI Min, DongJoon/G-7724-2012; SOHN, IL/I-5815-2012
FU Brain Korea 21 Project; Korea Evaluation Institute of Industrial
Technology (KEIT) [K0001343] Funding Source: Korea Institute of Science
& Technology Information (KISTI), National Science & Technology
Information Service (NTIS); National Research Foundation of Korea
[2010-0007442] Funding Source: Korea Institute of Science & Technology
Information (KISTI), National Science & Technology Information Service
(NTIS)
FX The authors appreciate H. Kim for his good discussion and the partial
funding provided by the Second Stage of Brain Korea 21 Project.
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NR 38
TC 59
Z9 61
U1 3
U2 31
PU WILEY-V C H VERLAG GMBH
PI WEINHEIM
PA BOSCHSTRASSE 12, D-69469 WEINHEIM, GERMANY
SN 1611-3683
EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD SEP
PY 2010
VL 81
IS 9
BP 735
EP 741
DI 10.1002/srin.201000067
PG 7
GA 651FS
UT WOS:000281912200006
DA 2023-12-05
ER
PT J
AU Tan, HB
Li, MG
He, XY
Su, Y
Yang, J
Zhao, H
AF Tan, Hongbo
Li, Maogao
He, Xingyang
Su, Ying
Yang, Jin
Zhao, Huang
TI Effect of wet grinded lithium slag on compressive strength and hydration
of sulphoaluminate cement system
LA English
DT Article
DE Lithium slag; Wet grinding; Nano particles; Accelerator; Early
compressive strength
ID BLAST-FURNACE SLAG; SURFACE FRACTAL DIMENSION; PORE STRUCTURE;
SODIUM-SULFATE; ASH; MICROSTRUCTURE; PERFORMANCE; EXTRACTION; CARBONATE;
CONCRETE
AB As a by-products of lithium carbonate industry, emission of lithium slag (LS)
was increasingly increased due to the huge market demand of lithium salt.
Therefore, LS disposal faces great challenge. In the study, a new approach to use
LS in sulphoaluminate cement (SAC) system to improve the early compressive strength
was proposed. Nano-lithium slag (nano-LS) was prepared via wet grinding, and the
effect of nano-LS on hydration mechanism of SAC was investigated. The results
indicated that nano-LS with D50 of 300 nm was prepared. In comparison with the
Blank, 4.0% nano-LS promoted the 7 h compressive strength from 4.5 MPa to 24.3 MPa,
with an increase by more than 4 times, and an increase by 28% at 1 d age; it also
reduced the initial and final setting time to 16 min and 23 min, being reduced by
33.3% and 37.5%. This phenomenon was because nano-LS accelerated the hydration of
SAC, and 4.0% dosage even made the inducing period disappear. The reason for the
accelerated hydration was that the nano particles in nano-LS slurry acted as
excellent nucleation seeds for speeding of the formation of hydration products.
Additionally, the promoted dissolution of lithium salt during the process of wet
milling also facilitated precipitation of aluminum phase to accelerate the SAC
hydration. Consequently, nano-LS was expected as an excellent accelerator in SAC
system. All of findings suggested an innovation new way to utilize LS in SAC
system. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Tan, Hongbo; Li, Maogao] Wuhan Univ Technol, State Key Lab Silicate Mat
Architectures, Wuhan 430070, Peoples R China.
[He, Xingyang; Su, Ying; Yang, Jin] Hubei Univ Technol, Sch Civil Engn
Architecture & Environm, Wuhan 430070, Peoples R China.
[Zhao, Huang] China Construct Third Bur Green Ind Investment Co, Wuhan 430100,
Peoples R China.
[Tan, Hongbo] Zhengzhou Univ, Sch Mat Sci & Engn, Zhengzhou 450052, Peoples R
China.
C3 Wuhan University of Technology; Hubei University of Technology;
Zhengzhou University
Environm, Wuhan 430070, Peoples R China.
EM hexycn@163.com
OI Yang, Jin/0000-0002-5332-7862
FU National Natural Science Foundation of China [51978544]; Major Technical
Innovation Project in Hubei Province of China [2019ACA146]
FX It was appreciated it that the fund aid of National Natural Science
Foundation of China (51978544) and Major Technical Innovation Project in
Hubei Province of China (2019ACA146).
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NR 59
TC 58
Z9 58
U1 16
U2 83
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JAN 18
PY 2021
VL 267
AR 120465
DI 10.1016/j.conbuildmat.2020.120465
PG 11
GA PN6FP
UT WOS:000604573000004
DA 2023-12-05
ER
PT J
AU Shi, RY
Li, JY
Ni, N
Xu, RK
AF Shi Ren-yong
Li Jiu-yu
Ni Ni
Xu Ren-kou
TI Understanding the biochar's role in ameliorating soil acidity
SO JOURNAL OF INTEGRATIVE AGRICULTURE
LA English
DT Review
DE aluminum toxicity; crop residue biochars; pH buffering capacity; soil
acidity
ID PH BUFFERING CAPACITY; CATION-EXCHANGE CAPACITY; VARIABLE CHARGE SOILS;
PYROLYSIS TEMPERATURE; ALUMINUM TOXICITY; CLIMATE-CHANGE; ALKALINE SLAG;
CROP RESIDUES; BY-PRODUCTS; ACIDIFICATION
AB Extensive acidic soils, which suffer from accelerated soil acidification, are
found in southern China. Soil acidity, aluminum toxicity, and nutrient deficiencies
severely limited crop productivity in acidic soils. It has been widely reported
that crop residue biochars can ameliorate acidic soils and increase crop
productivity. Here, we summarized the positive effects and mechanisms involved in
the correction of soil acidity, the alleviation of aluminum toxicity and the
increase of soil pH buffering capacity by crop residue biochars. The carbonate,
oxygen-containing functional groups and silicates in biochars are the major
components responsible for their efficacy in amending acidic soils and resisting
soil re-acidification. We conclude that application of crop residue biochars may be
a better option than traditional liming to ameliorate acidic soils. Nonetheless,
further researches into soil acidification are still required to address some
issues that are controversial and poorly understood.
C1 [Shi Ren-yong; Li Jiu-yu; Xu Ren-kou] Chinese Acad Sci, Inst Soil Sci, State Key
Lab Soil & Sustainable Agr, Nanjing 210008, Jiangsu, Peoples R China.
[Ni Ni] Nanjing Inst Environm Sci, Minist Ecol & Environm, Nanjing 210042,
[Ni Ni] Minist Ecol & Environm, Key Lab Pesticide Environm Assessment & Pollut
Co, Nanjing 210042, Jiangsu, Peoples R China.
C3 Chinese Academy of Sciences; Institute of Soil Science, CAS
Soil & Sustainable Agr, Nanjing 210008, Jiangsu, Peoples R China.
EM ryshi@issas.ac.cn; rkxu@issas.ac.cn
FU National Key Research and Development of China [2016YFD0200302];
National Key Basic Research Program of China [2014CB441003]
FX The study was funded by the National Key Research and Development of
China (2016YFD0200302) and the National Key Basic Research Program of
China (2014CB441003).
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NR 88
TC 58
Z9 70
U1 18
U2 111
PU ELSEVIER SCI LTD
PI OXFORD
SN 2095-3119
J9 J INTEGR AGR
JI J. Integr. Agric.
PD JUL
PY 2019
VL 18
IS 7
BP 1508
EP 1517
DI 10.1016/S2095-3119(18)62148-3
PG 10
WC Agriculture, Multidisciplinary
SC Agriculture
GA IH4HG
UT WOS:000474451900012
OA hybrid
DA 2023-12-05
ER
PT J
AU Novais, RM
Ascensao, G
Ferreira, N
Seabra, MP
Labrincha, JA
AF Novais, Rui M.
Ascensao, G.
Ferreira, N.
Seabra, M. P.
Labrincha, J. A.
TI lInfluence of water and aluminium powder content on the properties of
waste-containing geopolymer foams
LA English
DT Article
DE Inorganic polymer; Biomass fly ash; Calorimetry; Foam
ID FLY-ASH; STRUCTURAL-ANALYSIS; REACTION-KINETICS; CO2 EMISSIONS;
ACTIVATION; METAKAOLIN; SLAG; PERFORMANCE
AB The production of low thermal conductivity geopolymers has attracted increasing
attention over the past years due to their low cost and green processing
technology. In this work, light and porous geopolymers were produced by the proper
association of aluminium content and solid-to-liquid ratio. This allowed the
production of very low thermal conductivity geopolymers (78.6 mW/m K) exhibiting
homogeneous pore size distribution which suggests their use in thermal insulating
applications. Moreover this study also reduced the existing knowledge gap
concerning the fresh-state characterization of foamed geopolymer slurries. The
influence of aluminium powder, curing temperature and solid-to-liquid ratio on the
calorimetric response of biomass fly ash containing geopolymer slurries was
evaluated. The calorimetric response of geopolymer slurries shows that the time
needed to reach the maximum temperature decreases when the aluminium powder rises,
thus shortening the open time before in situ application. It was also found that
the geopolymerization rate is governed by the curing temperature.
C1 [Novais, Rui M.; Ascensao, G.; Ferreira, N.; Seabra, M. P.; Labrincha, J. A.]
Univ Aveiro, Aveiro Inst Mat, Dept Mat & Ceram Engn, CICECO, Campus Univ Santiago,
P-3810193 Aveiro, Portugal.
C3 Universidade de Aveiro
RP Novais, RM (corresponding author), Univ Aveiro, Aveiro Inst Mat, Dept Mat &
Ceram Engn, CICECO, Campus Univ Santiago, P-3810193 Aveiro, Portugal.
EM ruimnovais@ua.pt
RI Labrincha, J./B-3984-2010; Ascensão, Guilherme/AAT-3833-2020; Seabra,
Maria Paula/H-3640-2013; Novais, Rui M./X-2771-2019
OI Labrincha, J./0000-0003-4782-1685; Ascensão,
Guilherme/0000-0002-6003-4486; Seabra, Maria Paula/0000-0002-5174-7433;
Novais, Rui M./0000-0001-5698-9135
FU FCT/MEC [POCI-01-0145-FEDER-007679, UID/CTM/50011/2013]; FEDER
FX This work was developed within the scope of the project CICECO-Aveiro
Institute of Materials, POCI-01-0145-FEDER-007679 (FCT Ref.
UID/CTM/50011/2013), financed by national funds through the FCT/MEC and
when appropriate co-financed by FEDER under the PT2020 Partnership
Agreement. Guilherme Ascensao collaboration with this work was performed
before his integration in the NEW-MINE project.
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NR 35
TC 58
Z9 62
U1 1
U2 59
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD APR 15
PY 2018
VL 44
IS 6
BP 6242
EP 6249
DI 10.1016/j.ceramint.2018.01.009
PG 8
GA FY9VN
UT WOS:000427215100057
DA 2023-12-05
ER
PT J
AU Gil, A
Arrieta, E
Vicente, MA
Korili, SA
AF Gil, A.
Arrieta, E.
Vicente, M. A.
Korili, S. A.
TI Synthesis and CO2 adsorption properties of hydrotalcite-like
compounds prepared from aluminum saline slag wastes
LA English
DT Article
DE Aluminum saline slag; Hydrotalcite; CO2 adsorption
ID LAYERED DOUBLE HYDROXIDES; HIGH-TEMPERATURE ADSORPTION; CARBON-DIOXIDE;
PROMOTED HYDROTALCITE; HAZARDOUS-WASTE; ANIONIC CLAYS; SORPTION;
CAPTURE; ADSORBENTS; VALORIZATION
AB This study describes the synthesis of hydrotalcite-like materials by the co-
precipitation method using aluminum extracted from saline slags wastes. Saline
slags were chemically treated with 2 mol/dm(3) aqueous solutions of NaOH for 2 h
using a reflux system. The aluminum aqueous solutions were used as precursors with
cobalt, magnesium and nickel nitrates, and Na2CO3, to obtain hydrotalcite-like
materials with two mole M2+/Al3+ ratios, 2: 1 and 4:1. The resulting solids were
characterized by X-ray diffraction, termogravimetric analyses, nitrogen adsorption
at -196 degrees C and scanning electron microscopy. After thermal treatment at 200
degrees C, the CO2 adsorption at 50, 100 and 200 degrees C was evaluated under dry
conditions. The results showed a remarkable sorption capacity of 5.26 mmol/g at a
pressure of 80 kPa and at a temperature of 50 degrees C for the MgAl-2: 1 sample,
with sorption capacities considerably higher than those reported in the literature
for hydrotalcites under similar conditions. The Henry's law constants were obtained
directly from the adsorption isotherms at low pressures and the values found are
between 0.01 and 4.20 mmol/kPa.g. The isosteric heats of CO2 adsorption found,
using the Clausius-Clapeyron equation, were in the range of 5.2 to 16.8 kJ/mol.
C1 [Gil, A.; Arrieta, E.; Korili, S. A.] Univ Publ Navarra, Dept Quim Aplicada,
Edificio Los Acebos,Campus Arrosadia, E-31006 Pamplona, Spain.
[Gil, A.; Korili, S. A.] Univ Publ Navarra, Inst Mat Avanzados INAMAT, Campus
Arrosadia, Pamplona 31006, Spain.
[Vicente, M. A.] Univ Salamanca, Dept Quim Inorgan, GIR QUESCAT, E-37008
Salamanca, Spain.
C3 Universidad Publica de Navarra; Universidad Publica de Navarra;
University of Salamanca
RP Gil, A (corresponding author), Univ Publ Navarra, Dept Quim Aplicada, Edificio
Los Acebos,Campus Arrosadia, E-31006 Pamplona, Spain.
RI Vicente, Miguel Angel/L-5298-2014
OI Vicente, Miguel Angel/0000-0002-6714-0249
FU Spanish Ministry of Economy, Industry and Competitiveness (AEI/MINECO);
European Regional Development Fund (ERDF) [MAT2016-78863-C2-2-R]
of Economy, Industry and Competitiveness (AEI/MINECO), and the European
Regional Development Fund (ERDF) through project MAT2016-78863-C2-2-R.
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X
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NR 44
TC 58
Z9 62
U1 4
U2 66
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD FEB 15
PY 2018
VL 334
BP 1341
EP 1350
DI 10.1016/j.cej.2017.11.100
PG 10
SC Engineering
GA FQ7HL
UT WOS:000418533400134
OA Green Published
DA 2023-12-05
ER
PT J
AU Ren, CZ
Wang, WL
Li, GL
AF Ren, Changzai
Wang, Wenlong
Li, Guolin
TI Preparation of high-performance cementitious materials from industrial
solid waste
LA English
DT Article
DE Industrial solid wastes; Sulfoaluminate clinker; Mechanical properties;
X-ray diffraction; Clinker phases
ID CALCIUM SULFOALUMINATE CEMENT; BELITE CEMENT; CONCRETE
AB Sulfoaluminate cement exhibits a good dimensional stability, an early strength,
a high strength, a high resistance to chemical attack (from seawater, sulfates and
chlorides), a low energy consumption and low carbon-dioxide emissions during
production. However, sulfoaluminate cement factories traditionally use limestone,
bauxite and gypsum as materials, which places significant pressure on these natural
resources. This study aimed to investigate the feasibility of substituting
traditional raw materials with industrial solid wastes in sulfoaluminate clinker
production. It was achieved by sintering a mixture of industrial solid wastes (coal
gangue: 8%-15%, flue gas desulfurization gypsum: 25%-35%, aluminum slag: 30%-35%,
carbide slag: 30%-35%) at 1150-1300 degrees C. The mineralogical composition of the
clinker was C(4)A(3)(S) over bar, C2S and C(4)AF. The compressive strength of
hydrated specimens reached as high as 75 MPa after a 28 d curing. This research
provides a feasible and promising way to produce high-value products using
industrial solid wastes and may promote their large-scale utilization. (C) 2017
C1 [Ren, Changzai; Wang, Wenlong; Li, Guolin] Shandong Univ, Natl Engn Lab Coal
Fired Pollutants Emiss Reduct, Jinan 250061, Shandong, Peoples R China.
[Ren, Changzai] Xinjiang Inst Engn, Dept Elect Power Engn, Urumqi 830091,
Peoples R China.
C3 Shandong University; Xinjiang Institute of Engineering
RP Wang, WL (corresponding author), Shandong Univ, Natl Engn Lab Coal Fired
Pollutants Emiss Reduct, Jinan 250061, Shandong, Peoples R China.
EM wwenlong@sdu.edu.cn
RI wang, wenlong/L-2239-2013
Shandong Provincial Science Fund for Distinguished Young Scholars
[JQ201514]; Primary Research & Development Plan of Shandong Province
[2016GSF116006]
FX The authors thank the support of The National Key Research and
Development Program of China (2017YFC0703100), Shandong Provincial
Science Fund for Distinguished Young Scholars (No. JQ201514), and
Primary Research & Development Plan of Shandong Province
(2016GSF116006).
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NR 27
TC 58
Z9 62
U1 13
U2 141
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 15
PY 2017
VL 152
BP 39
EP 47
DI 10.1016/j.conbuildmat.2017.06.124
PG 9
GA FH9QA
UT WOS:000411545600004
DA 2023-12-05
ER
PT J
AU Shuva, MAH
Rhamdhani, MA
Brooks, GA
Masood, S
Reuter, MA
AF Shuva, M. A. H.
Rhamdhani, M. A.
Brooks, G. A.
Masood, S.
Reuter, M. A.
TI Thermodynamics data of valuable elements relevant to e-waste processing
through primary and secondary copper production: a review
LA English
DT Review
DE Thermodynamics; Precious metals distribution; Valuable metals
distribution; Black copper smelting; E-waste recycling; WEEE recycling
ID DISSOLUTION BEHAVIOR; DISTRIBUTION EQUILIBRIA; LIQUID COPPER;
FEOX-CAO-SIO2 SLAGS; MINOR ELEMENTS; TELLURIUM DISTRIBUTION; ELECTRONIC
WASTE; PHASE-EQUILIBRIA; PRECIOUS METALS; MOLTEN COPPER
AB Waste of electronics and electrical equipment (WEEE or e-waste) can be viewed as
a resource for metals, as it does not only contain the common metals like iron
(Fe), aluminium (Al), lead (Pb) and copper (Cu) but also traces of precious and
rare elements such as gold (Au), silver (Ag), tin (Sn), selenium (Se), tellurium
(Te), platinum (Pt), palladium (Pd), tantalum (Ta), cobalt (Co) and indium (In).
The recovery of these trace elements is vital, not just because it has high
commercial values, but also for resources efficiency. One of the existing
industrial routes for processing of e-waste is through the primary and secondary Cu
smelting processes. During these processes, the trace elements are distributed in
different phases, i.e. in metal/matte, slag and gas. Different elements have
different thermodynamic properties that govern the partitioning behaviour during
the process. There has been a number of studies on the distribution behaviour of
the trace elements relevant to primary Cu smelting (extraction of metals from
virgin ores). However, there are only limited thermodynamics data relevant to
secondary Cu smelting (extraction of metals from secondary/recycled sources). This
paper reviews the thermodynamics data relevant for recovering the trace valuable
elements from the primary Cu as well as secondary Cu smelting. These data and
knowledge provide the basis for determining the optimum conditions favourable for
recovering the trace valuable elements in e-waste through the industrial Cu
pyrometallurgical processing. (C) 2016 Elsevier Ltd. All rights reserved.
C1 [Shuva, M. A. H.; Rhamdhani, M. A.; Brooks, G. A.; Masood, S.] Swinburne Univ
Technol, Hawthorn, Vic 3122, Australia.
[Shuva, M. A. H.; Rhamdhani, M. A.; Brooks, G. A.; Masood, S.] Wealth Waste Res
Cluster, Brisbane St Lucia, Qld, Australia.
[Reuter, M. A.] Helmholtz Inst Freiberg Resource Technol, Freiberg, Germany.
C3 Swinburne University of Technology; Helmholtz Association;
Helmholtz-Zentrum Dresden-Rossendorf (HZDR)
RP Rhamdhani, MA (corresponding author), Swinburne Univ Technol, Hawthorn, Vic
3122, Australia.
EM ARhamdhani@swin.edu.au
RI Masood, Syed/AAI-9769-2020; Rhamdhani, Muhammad Akbar/ACM-2274-2022;
Reuter, Markus/M-5565-2019
OI Rhamdhani, Muhammad Akbar/0000-0002-9457-3808; Reuter,
Markus/0000-0003-0500-4863; Brooks, Geoffrey/0000-0002-8499-780X;
Masood, Syed/0000-0001-9472-1527
FU Wealth from Waste Research Cluster; Australian CSIRO (Commonwealth
Scientific Industrial Research Organisation); University of Technology,
Sydney; University of Queensland, USA; Swinburne University of
Technology, USA; Monash University, USA; Yale University, USA; Swinburne
Research for the Swinburne University Postgraduate Research Award
(SUPRA)
FX The authors would like to acknowledge Swinburne Research for the
Swinburne University Postgraduate Research Award (SUPRA) support. The
authors would like to also acknowledge the support of the Wealth from
Waste Research Cluster, a collaborative program between the Australian
CSIRO (Commonwealth Scientific Industrial Research Organisation);
University of Technology, Sydney; The University of Queensland,
Swinburne University of Technology, Monash University and Yale
University, USA.
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NR 112
TC 58
Z9 61
U1 6
U2 206
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD SEP 10
PY 2016
VL 131
BP 795
EP 809
DI 10.1016/j.jclepro.2016.04.061
PG 15
& Ecology
GA DQ5UP
UT WOS:000379270900076
DA 2023-12-05
ER
PT J
AU Salih, MA
Farzadnia, N
Ali, AAA
Demirboga, R
AF Salih, Moslih Amer
Farzadnia, Nima
Ali, Abang Abdullah Abang
Demirboga, Ramazan
TI Development of high strength alkali activated binder using palm oil fuel
ash and GGBS at ambient temperature
LA English
DT Article
DE POFA; GGBS; High strength alkali activated binder; Geopolymers; C-S-H;
C-A-S-H
ID CALCIUM SILICATE HYDRATE; RICE HUSK ASH; FLY-ASH; COMPRESSIVE STRENGTH;
GEOPOLYMER; SLAG; CEMENT; CONCRETE; MICROSTRUCTURE; GEL
AB This study focused on production of high strength alkali activated binder by
alkali activation of binary mix of palm oil fuel ash (POFA) and ground granulated
blast furnace slag (GGBS) at ambient temperature. Compression test was performed to
assess mechanical properties of the mixture. Chemical tests were also conducted to
investigate the role of calcium and aluminum ions from GGBS in the strength
development. Formation of aluminum-substituted calcium silicate hydrate (C-A-S-H)
gel with a higher degree of crystallinity was observed when GGBS was added.
Replacement of 50% POFA with GGBS increased the strength up to 92 MPa at 90 days.
C1 [Salih, Moslih Amer] Al Furat Al Awsat Tech Univ, Babylon Tech Inst, Al Musaib
City, Babylon Provinc, Iraq.
[Salih, Moslih Amer; Farzadnia, Nima; Ali, Abang Abdullah Abang] Univ Putra
Malaysia, Fac Engn, Dept Civil Engn, Housing Res Ctr, Serdang 43400, Selangor,
Malaysia.
[Demirboga, Ramazan] King Abdulaziz Univ, Dept Civil Engn, Jeddah, Saudi Arabia.
C3 Al-Furat Al-Awsat Technical University; Universiti Putra Malaysia; King
Abdulaziz University
RP Salih, MA (corresponding author), Al Furat Al Awsat Tech Univ, Babylon Tech
Inst, Al Musaib City, Babylon Provinc, Iraq.
EM moslih_salih@yahoo.com
RI Salih, Dr. Moslih Amer/AAD-3931-2019; Farzadnia, Nima/B-2411-2010
OI Salih, Dr. Moslih Amer/0000-0002-5824-1689; Farzadnia,
Nima/0000-0002-9396-4102
FU Academy of Science Malaysia (ASM) [06-05-13-SF0004]; YTL Cement
Marketing Sdn Bhd (Company) [455804-M]; Slag Cement Sdn Bhd (Company)
[368743-P]
FX The authors wish to gratefully acknowledge the Academy of Science
Malaysia (ASM) for the financial support of this study under Project
Number (06-05-13-SF0004). Also, the authors would like to thank YTL
Cement Marketing Sdn Bhd (Company No: 455804-M) and Slag Cement Sdn Bhd
(Company No. 368743-P) for their support in donating GGBS for the
project.
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NR 75
TC 58
Z9 61
U1 0
U2 32
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD SEP 15
PY 2015
VL 93
BP 289
EP 300
DI 10.1016/j.conbuildmat.2015.05.119
PG 12
GA CO4YE
UT WOS:000359166000031
DA 2023-12-05
ER
PT J
AU Eschlböck-Fuchs, S
Haslinger, MJ
Hinterreiter, A
Kolmhofer, P
Huber, N
Rössler, R
Heitz, J
Pedarnig, JD
AF Eschlboeck-Fuchs, S.
Haslinger, M. J.
Hinterreiter, A.
Kolmhofer, P.
Huber, N.
Roessler, R.
Heitz, J.
Pedarnig, J. D.
TI Influence of sample temperature on the expansion dynamics and the
optical emission of laser-induced plasma
SO SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY
LA English
DT Article
DE Laser induced breakdown spectroscopy (LIBS); Calibration free LIBS;
Time-resolved plasma photography; Sample temperature; Plasma expansion
dynamics
ID INDUCED BREAKDOWN SPECTROSCOPY; DOUBLE-PULSE; MINERAL MELT; CALIBRATION;
SPECTROMETRY; ABLATION; SENSOR; STEEL
AB We investigate the influence of sample temperature on the dynamics and optical
emission of laser induced plasma for various solid materials. Bulk aluminum alloy,
silicon wafer, and metallurgical slag samples are heated to temperature T-S <= 500
degrees C and ablated in air by Nd:YAG laser pulses (wavelength 1064 nm, pulse
duration approx. 7 ns). The plasma dynamics is investigated by fast time-resolved
photography. For laser-induced breakdown spectroscopy (LIBS) the optical emission
of plasma is measured by Echelle spectrometers in combination with intensified CCD
cameras. For all sample materials the temporal evolution of plume size and
broadband plasma emission vary systematically with T-S. The size and brightness of
expanding plumes increase at higher T-S while the mean intensity remains
independent of temperature. The intensity of emission lines increases with
temperature for all samples. Plasma temperature and electron number density do not
vary with T-S. We apply the calibration-free LIBS method to determine the
concentration of major oxides in slag and find good agreement to reference data up
to T-S = 450 degrees C. The LIBS analysis of multi-component materials at high
temperature is of interest for technical applications, e.g. in industrial
production processes. (C) 2013 Elsevier B.V. All rights reserved.
C1 [Eschlboeck-Fuchs, S.; Haslinger, M. J.; Hinterreiter, A.; Kolmhofer, P.; Huber,
N.; Heitz, J.; Pedarnig, J. D.] Johannes Kepler Univ Linz, Christian Doppler Lab
Laser Assisted Diagnost, Inst Appl Phys, A-4040 Linz, Austria.
[Roessler, R.] Voestalpine Stahl GmbH, A-4031 Linz, Austria.
C3 Johannes Kepler University Linz; Voestalpine AG
RP Pedarnig, JD (corresponding author), Johannes Kepler Univ Linz, Christian
Doppler Lab Laser Assisted Diagnost, Inst Appl Phys, A-4040 Linz, Austria.
EM johannes.pedarnig@jku.at
RI Heitz, Johannes/O-8637-2015; Pedarnig, Johannes D/A-8500-2016; Huber,
Norbert/B-9271-2017
OI Heitz, Johannes/0000-0002-5608-5133; Pedarnig, Johannes
D/0000-0002-7842-3922; Haslinger, Michael/0000-0002-0127-5554; Huber,
Norbert/0000-0002-0684-3629
FU Austrian Federal Ministry of Economy, Family and Youth; National
Foundation for Research, Technology and Development (Christian Doppler
Laboratory LAD)
FX Financial support by the Austrian Federal Ministry of Economy, Family
and Youth and the National Foundation for Research, Technology and
Development (Christian Doppler Laboratory LAD) is gratefully
acknowledged. We thank the B & C Privatstiftung for the Houska
Recognition Award 2011 presented to the Christian Doppler Laboratory.
CR [Anonymous], 2006, Handbook of Laser-Induced Breakdown Spectroscopy
Bauerle D., 2013, LASER PROCESSING CHE
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NR 37
TC 58
Z9 64
U1 3
U2 86
PI OXFORD
SN 0584-8547
J9 SPECTROCHIM ACTA B
JI Spectroc. Acta Pt. B-Atom. Spectr.
PD SEP 1
PY 2013
VL 87
BP 36
EP 42
DI 10.1016/j.sab.2013.05.023
PG 7
WC Spectroscopy
SC Spectroscopy
GA 210ZN
UT WOS:000323874000005
DA 2023-12-05
ER
PT J
AU Wu, T
Wang, Q
He, SP
Xu, JF
Long, X
Lu, YJ
AF Wu, Ting
Wang, Qian
He, Shengping
Xu, Jianfei
Long, Xiao
Lu, Yongjian
TI Study on Properties of Alumina-Based Mould Fluxes for High-Al Steel Slab
Casting
LA English
DT Article
DE crystalline; dynamic reduction; high-Al steel; mould fluxes
ID TRANSFORMATION
AB During the continuous casting of high-Al steel, the dynamic reduction of silica-
based mould fluxes by the aluminium in the steel leads to changes in their
composition and physical properties. The alumina-based mould flux has been
suggested as an alternative to alleviate this reduction problem. However, until
now, the smooth running of high-Al steel continuous casting has been impeded by the
lack of systematic investigation of properties of this slag. In this paper, the
effects of typical components on the properties of alumina-based mould fluxes are
discussed. The experimental results show that: (a) an increase in F- can reduce the
viscosity while increasing the melting and break temperatures; (b) with increasing
Li2O, the viscosity, melting temperature, and break temperature first decrease and
then increase; (c) with the addition of BaO, the viscosity, melting temperature,
and break temperature remain at a low level, while a further increase in BaO causes
a decrease in viscosity, an increase in melting temperature, and the stabilization
of the break temperature; (d) BaO is favorable to stabilize the properties of mould
fluxes for the dissolution of additional Al2O3; (e) the crystalline phases of the
mould fluxes mainly contain 12CaO center dot 7Al(2)O(3) and 11CaO center dot
7Al(2)O(3)center dot CaF2, and 12CaO center dot 7Al(2)O(3) has great potential as a
substitute for cuspidine.
C1 [Wu, Ting; Wang, Qian; He, Shengping; Xu, Jianfei; Long, Xiao; Lu, Yongjian]
Chongqing Univ, Chongqing Key Lab Met Engn, Coll Mat Sci & Engn, Chongqing 400045,
Peoples R China.
C3 Chongqing University
RP Wu, T (corresponding author), Chongqing Univ, Chongqing Key Lab Met Engn, Coll
Mat Sci & Engn, Chongqing 400045, Peoples R China.
EM wuting@cqu.edu.cn
OI Long, Xiao/0000-0001-7141-4102
FU Fundamental Research Funds for the Central Universities in China
[CDJZR11130004]
FX The authors greatly appreciate the funding support from the Fundamental
Research Funds for the Central Universities in China (Project No.
CDJZR11130004).
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[No title captured]
NR 15
TC 58
Z9 63
U1 2
U2 27
PI WEINHEIM
SN 1611-3683
J9 STEEL RES INT
JI Steel Res. Int.
PD DEC
PY 2012
VL 83
IS 12
BP 1194
EP 1202
DI 10.1002/srin.201200092
PG 9
GA 051UM
UT WOS:000312153200010
DA 2023-12-05
ER
PT J
AU Vermeulen, Y
Coletti, B
Blanpain, B
Wollants, P
Vleugels, J
AF Vermeulen, Y
Coletti, B
Blanpain, B
Wollants, P
Vleugels, J
TI Material evaluation to prevent nozzle clogging during continuous casting
of Al killed steels
LA English
DT Article
DE continuous casting; aluminium killed low carbon steel; clogging; nozzle;
refractory materials
ID GRAPHITE IMMERSION NOZZLE; MECHANISM; WEAR
AB Al2O3-carbon composite submerged entry nozzles (SEN) are used for continuous
casting of steels. Although this material has excellent mechanical and thermal
properties, it frequently leads to clogging. The purpose of our research is to find
a suitable refractory material that can be used to coat SENs. This paper reports on
the chemical compatibility of a number of potential refractory materials: Al2O3,
ZrO2, Al2O3-carbon, SiO2 and MgO with liquid steel, an amount of simulated
inclusions and synthetic slag. For this purpose, an experimental laboratory
procedure was optimised to simulate the nozzle behaviour during continuous casting.
Al2O3 was found to give satisfactory results, and therefore a Al2O3 plasma coated
Al2O3-carbon material was also tested in the laboratory with good results.
C1 Catholic Univ Louvain, Dept Met & Mat Engn, B-3001 Heverlee, Belgium.
C3 Universite Catholique Louvain
RP Vermeulen, Y (corresponding author), Catholic Univ Louvain, Dept Met & Mat Engn,
Kasteelpk Arenberg 44, B-3001 Heverlee, Belgium.
RI Vleugels, Jozef/C-8262-2017; Blanpain, Bart/ABW-6334-2022
OI Vleugels, Jozef/0000-0003-4432-4675; Blanpain, Bart/0000-0002-5603-3456
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NR 19
TC 58
Z9 60
U1 1
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PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2002
VL 42
IS 11
BP 1234
EP 1240
PG 7
GA 617TJ
UT WOS:000179376700007
OA gold
DA 2023-12-05
ER
PT J
AU Tayeh, BA
Hakamy, A
Amin, M
Zeyad, AM
Agwa, IS
AF Tayeh, Bassam A.
Hakamy, Ahmad
Amin, Mohamed
Zeyad, Abdullah M.
Agwa, Ibrahim Saad
TI Effect of air agent on mechanical properties and microstructure of
lightweight geopolymer concrete under high temperature
LA English
DT Article
DE Lightweight geopolymer concrete; Ferrosilicon; Aluminum powder;
Mechanical properties; High temperatures; Microstructure
ID FLY-ASH; COMPRESSIVE STRENGTH; ELEVATED-TEMPERATURE; CURING TEMPERATURE;
ALKALI ACTIVATION; PART I; FOAMS; AGGREGATE; HYDRATION; BEHAVIOR
AB Recent innovations in the field of concrete have contributed to the development
of lightweight geopolymer concrete (LGC), which can be produced by adding an air
agent. This study investigates the possibility of producing an air agent from the
powder slag of ferrosilicon (FSS), an industrial waste. A class F fly ash (FA) was
used for GC synthesis, and aluminium powder (AP) and FSS were added as air agents
for LGC synthesis. The performance of FSS and AP as an air agents was compared by
studying the properties of LGC produced under the same conditions. Air agents with
0%, 0.1%, 0.2%, 0.3%, 0.4%, 0.5% and 1.0% mass of FA were adopted to produce LGC.
Thirteen mixtures were prepared to evaluate unit weight, the fresh and mechanical
properties and the microstructure of LGC with PA and FSS air agents. Influence of
high temperature of 200-800 degrees C for 2hrs on LGC was also investigated. The
results show the possibility of using FSS waste powder as an air agent in LGC
production. In terms of workability and unit weight, FSS was better compared to AP
at the same percentage addition. The slump flow and unit weight, were 548 mm, 1830
kg/m(3), and 569 mm and 1740 kg/m(3), while compressive strength was 24.7 and 21.8
MPa for LGC containing 1% AP and 1% FSS, respectively.
C1 [Tayeh, Bassam A.] Islamic Univ Gaza, Fac Engn, Civil Engn Dept, POB 108, Gaza,
Palestine.
[Hakamy, Ahmad] Umm Al Qura Univ, Fac Appl Sci, Dept Phys, Mecca 21955, Saudi
Arabia.
[Amin, Mohamed; Agwa, Ibrahim Saad] Suez Univ, Fac Technol & Educ, Civil &
Architectural Constructions Dept, Suez, Egypt.
[Zeyad, Abdullah M.] Jazan Univ, Fac Engn, Civil Engn Dept, Jazan, Saudi Arabia.
[Zeyad, Abdullah M.] Univ Sci & Technol, Fac Engn, Civil Engn Dept, Aden, Yemen.
C3 Islamic University Gaza; Umm Al Qura University; Egyptian Knowledge Bank
(EKB); Suez University; Jazan University
RP Tayeh, BA (corresponding author), Islamic Univ Gaza, Fac Engn, Civil Engn Dept,
POB 108, Gaza, Palestine.
EM btayeh@iugaza.edu.ps
RI Hakamy, Ahmad/CAF-8325-2022; Agwa, Ibrahim Saad/IYT-2832-2023; Agwa,
Ibrahim saad/ABG-1347-2021; Tayeh, Bassam/IYJ-5641-2023; Zeyad, Abdullah
M./J-2063-2016; Amin, Mohamed/HLV-7796-2023
OI Agwa, Ibrahim Saad/0009-0009-8048-3164; Tayeh,
Bassam/0009-0003-7522-333X; Zeyad, Abdullah M./0000-0003-0023-8249;
Amin, Mohamed/0000-0001-6858-3773; Saad Agwa,
Ibrahim/0000-0001-5925-6666
FU Umm Al-Qura University [22UQU4250045DSR01]
FX "The authors would like to thank the Deanship of Scientific Research at
Umm Al-Qura University for supporting this work by Grant Code:
(22UQU4250045DSR01) ".
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NR 89
TC 57
Z9 57
U1 8
U2 24
PU ELSEVIER
PI AMSTERDAM
SN 2214-5095
PD JUN
PY 2022
VL 16
AR e00951
DI 10.1016/j.cscm.2022.e00951
EA FEB 2022
PG 19
GA 0V3SC
UT WOS:000788264900006
OA gold
DA 2023-12-05
ER
PT J
AU Du, CM
Shang, C
Gong, XJ
Ting, W
Wei, XG
AF Du Changming
Shang Chao
Gong, Xiangjie
Wang Ting
Wei Xiange
TI Plasma methods for metals recovery from metal-containing waste
SO WASTE MANAGEMENT
LA English
DT Article
DE Plasma; Metal waste; Metal; Recovery
ID DIELECTRIC-BARRIER DISCHARGES; MUNICIPAL SOLID-WASTE;
METALLURGICAL-GRADE SILICON; IN-FLIGHT TREATMENT; THERMAL PLASMA;
ELECTROPLATING SLUDGE; VALUABLE METALS; CIRCUIT BOARDS; IRON RECOVERY;
GLIDING ARC
AB Metal-containing waste, a kind of new wastes, has a great potential for
recycling and is also difficult to deal with. Many countries pay more and more
attention to develop the metal recovery process and equipment of this kind of waste
as raw material, so as to solve the environmental pollution and comprehensively
utilize the discarded metal resources. Plasma processing is an efficient and
environmentally friendly way for metal-containing waste. This review mainly discuss
various metal-containing waste types, such as printed circuit boards (PCBs), red
mud, galvanic sludge, Zircon, aluminium dross and incinerated ash, and the
corresponding plasma methods, which include DC extended transferred arc plasma
reactor, DC non-transferred arc plasma torch, RF thermal plasma reactor and argon
and argon-hydrogen plasma jets. In addition, the plasma arc melting technology has
a better purification effect on the extraction of useful metals from metal-
containing wastes, a great capacity of volume reduction of waste materials, and a
low leaching toxicity of solid slag, which can also be used to deal with all kinds
of metal waste materials, having a wide range of applications. (C) 2018 Elsevier
C1 [Du Changming; Shang Chao; Gong, Xiangjie; Wang Ting; Wei Xiange] Sun Yat Sen
Univ, Sch Environm Sci & Engn, Guangzhou 510275, Guangdong, Peoples R China.
C3 Sun Yat Sen University
RP Du, CM; Wei, XG (corresponding author), Sun Yat Sen Univ, Sch Environm Sci &
Engn, Guangzhou 510275, Guangdong, Peoples R China.
EM duchm@mail.sysu.edu.cn; 1220805600@qq.corn; eeswxg@mail.sysu.edu.cn
FU Guangdong Applied Science and Technology Research Project, China
[2015B020237005]; Natural Science Foundation of GuangDong, China
[2016A030313221]
FX The project is supported by the Guangdong Applied Science and Technology
Research Project, China (2015B020237005), and Natural Science Foundation
of GuangDong, China (2016A030313221).
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TC 57
Z9 57
U1 9
U2 124
PI OXFORD
SN 0956-053X
J9 WASTE MANAGE
JI Waste Manage.
PD JUL
PY 2018
VL 77
BP 373
EP 387
DI 10.1016/j.wasman.2018.04.026
PG 15
GA GO8YR
UT WOS:000440389600040
PM 29709310
DA 2023-12-05
ER
PT J
AU Delannoy, Y
AF Delannoy, Yves
TI Purification of silicon for photovoltaic applications
SO JOURNAL OF CRYSTAL GROWTH
LA English
CT 5th International Workshop on Crystal Growth Technology (IWCGT)
CY JUN 26-30, 2011
CL Berlin, GERMANY
DE Purification; Segregation; Stirring; Silicon; Solar cells
ID MOLTEN SILICON; GRADE SILICON; BORON REMOVAL
AB Solar grade silicon, as a starting material for crystallization to produce solar
cells, is discussed here in terms of impurities whose maximum content is estimated
from recent literature and conferences. A review of the production routes for each
category of solar-grade silicon (undoped, compensated or heavily compensated) is
proposed with emphasis on the metallurgical route.
Some recent results are proposed concerning segregation, showing that
directional solidification systems can be used for solidification even at high
solidification rate (15 cm/h). Results on inductive plasma purification, where
boron is evacuated as HBO in a gas phase blown from an inductive plasma torch, are
shown to apply as well to arc plasmas and purification by moist gas.
Special attention is paid to the history of impurities in the purification
processes, showing that impure auxiliary phases (silicon tetrachloride, slag,
aluminum, etc.) often need their own purification process to enable their
recycling, which has to be considered to evaluate the cost (financial, energetic
and environmental) of the purification route. (C) 2011 Elsevier B.V. All rights
reserved.
C1 Grenoble INP SIMAP, F-38402 St Martin Dheres, France.
C3 Communaute Universite Grenoble Alpes; Institut National Polytechnique de
Grenoble; Universite Grenoble Alpes (UGA); Centre National de la
Recherche Scientifique (CNRS)
RP Delannoy, Y (corresponding author), Grenoble INP SIMAP, F-38402 St Martin
Dheres, France.
EM Yves.Delannoy@inpg.fr
RI Delannoy, Yves/D-5593-2016
OI Delannoy, Yves/0000-0003-4906-0736
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TC 57
Z9 57
U1 1
U2 51
PU ELSEVIER
PI AMSTERDAM
SN 0022-0248
EI 1873-5002
J9 J CRYST GROWTH
JI J. Cryst. Growth
PD DEC 1
PY 2012
VL 360
SI SI
BP 61
EP 67
DI 10.1016/j.jcrysgro.2011.12.006
PG 7
WC Crystallography; Materials Science, Multidisciplinary; Physics, Applied
SC Crystallography; Materials Science; Physics
GA 035JL
UT WOS:000310942500013
DA 2023-12-05
ER
PT J
AU Esmaily, H
Nuranian, H
AF Esmaily, H.
Nuranian, H.
TI Non-autoclaved high strength cellular concrete from alkali activated
slag
LA English
DT Article
DE Cellular concrete; Alkali activated slag; Pore structure
ID TEMPERATURE
AB In this study, the use of alkali activated slag (AAS) in place of usual
cementitious materials in the production of autoclave aerated concrete (AAC) was
studied. This substitution altered autoclave curing stage by steam curing in MC
production process. In this way, after mixing of AAS paste with aluminum powder.
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70, 78 and 87 degrees C. To achieve the best results, microscopic pore structure,
compressive strength of the body and mini-slump of initial paste were studied. The
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C1 [Esmaily, H.; Nuranian, H.] Mat & Energy Res Ctr, Tehran, Iran.
C3 Materials & Energy Research Center (MERC)
RP Esmaily, H (corresponding author), Mat & Energy Res Ctr, POB 14155-4777, Tehran,
Iran.
EM hossein_esmaily@merc.ac.ir
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NR 25
TC 57
Z9 61
U1 1
U2 34
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JAN
PY 2012
VL 26
IS 1
BP 200
EP 206
DI 10.1016/j.conbuildmat.2011.06.010
PG 7
GA 831TO
UT WOS:000295754200024
DA 2023-12-05
ER
PT J
AU Janke, D
Ma, ZT
Valentin, P
Heinen, A
AF Janke, D
Ma, ZT
Valentin, P
Heinen, A
TI Improvement of castability and anality of continuously cast steel
LA English
DT Article
DE thermodynamics; Ca metallurgy; RH treatment; inclusions; castability;
steel quality
ID LIQUID-IRON; OXYGEN EQUILIBRIUM; CALCIUM; MELTS; ALUMINUM; SOLUBILITY
AB Thermodynamic fundamentals on the systems Fe-Al-O and Fe-Al-Ca-S-O being
important to metallurgy of Ca-treated Al-killed steels are analysed and discussed.
The formation of liquid Ca aluminates for the improvement of castability is pursued
in view of the production of Ca-treated Al-killed steels. The "Liquid window" is
theoretically analysed and experimentally investigated. The top slag is formed
after tapping and its composition is fairly constant during ladle treatment for
both with and without RH treatment, respectively. However, the top slag of the
degassed heats shows a lower oxygen level compared to the non-degassed heats. It is
found that there exists an "inclusion path" during the ladle treatment. The
inclusion path for the heats with RH treatment considerably differs from that of
the heats without RH treatment and it greatly influences the efficiency of Ca
treatment.
C1 TU Freiburg, Inst Iron & Steel Technol, D-09599 Freiburg, Germany.
Saarstahl AG, Betriebschef Stahlerzeugung Sekundarmet, D-66330 Volklingen,
Germany.
RP Janke, D (corresponding author), TU Freiburg, Inst Iron & Steel Technol,
Leipziger Str 34, D-09599 Freiburg, Germany.
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NR 45
TC 57
Z9 59
U1 0
U2 4
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2000
VL 40
IS 1
BP 31
EP 39
PG 9
GA 290DX
UT WOS:000085661900005
OA gold
DA 2023-12-05
ER
PT J
AU Kong, J
Xing, PF
Liu, Y
Wang, JQ
Jin, X
Feng, ZB
Luo, XT
AF Kong, Jian
Xing, Pengfei
Liu, Yang
Wang, Jingqiang
Jin, Xing
Feng, Zhongbao
Luo, Xuetao
TI An Economical Approach for the Recycling of High-Purity Silicon from
Diamond-Wire Saw Kerf Slurry Waste
SO SILICON
LA English
DT Article
DE Diamond-wire; Kerf slurry waste; Acid leaching; Induction furnace;
Melting; SoG-Si
ID METALLURGICAL GRADE SILICON; BORON REMOVAL; DIRECTIONAL SOLIDIFICATION;
POLYCRYSTALLINE SILICON; MOLTEN SILICON; IRON REMOVAL; PHOSPHORUS;
SEPARATION; KINETICS; CARBIDE
AB Large amounts of solar-grade silicon were wasted as silicon powder waste (SPW)
during the diamond-wire saw slicing process. In this paper, the SPW was purified by
acid leaching, and the purified SPW was pelletized. Then the pellets were melted in
induction furnace in air atmosphere to produce high-purity silicon ingots. Firstly,
the SPW as raw material was characterized. The results show that the particle size
of the powder is mainly in the range of 0.14 approximate to 8.71 m, the powder has
a shape of thin flake, the contents of SPW are Si 83.99 wt%, silicon oxide 13.5 wt
%, others 2.51 wt%, of which B (boron) 0.2 ppmw, P (phosphorus) 4.32 ppmw, and
metallic impurities 16412 ppmw, respectively. Secondly, the SPW was purified by
acid leaching and the leaching parameters were optimized, i.e. leaching time 80
min, temperature 60 degrees, acid concentration 25%, liquid-solid ratio 10 mL/g and
agitation speed 200 rpm. Thirdly, the purified SPW was pelletized and then melted
in induction furnace in air atmosphere. High-purity silicon ingots with Si 99.99%,
B 0.16 ppmw and P 1.1 ppmw were produced. The slag mainly consists of 48.63 wt% Si,
43.51 wt% SiO2 and 7.86 wt% SiC. The high-purity silicon ingots can be used to
produce aluminum silicon alloy and silicon nitride. And it is prospective to use
the high-purity silicon ingots as the feedstock to produce solar grade silicon
(SoG-Si).
C1 [Kong, Jian; Xing, Pengfei; Liu, Yang; Wang, Jingqiang; Jin, Xing; Feng,
Zhongbao] Northeastern Univ, Sch Met, Shenyang 110819, Liaoning, Peoples R China.
[Luo, Xuetao] Xiamen Univ, Dept Mat Sci & Engn, Xiamen 361005, Peoples R China.
C3 Northeastern University - China; Xiamen University
RP Xing, PF (corresponding author), Northeastern Univ, Sch Met, Shenyang 110819,
Liaoning, Peoples R China.
EM xingpf@smm.neu.edu.cn
RI Kong, Jian/HZH-7744-2023
FU State Key Program of National Natural Science Foundation of China
[51334004]; National Natural Science Foundation of China [51074043];
Fundamental Research Funds for the Central University
FX This work was financially supported by the State Key Program of National
Natural Science Foundation of China (Grant No.51334004), the National
Natural Science Foundation of China (Grant No.51074043) and the
Fundamental Research Funds for the Central University (Grant
No.N120409004).
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NR 50
TC 56
Z9 59
U1 14
U2 65
PU SPRINGER
PI DORDRECHT
SN 1876-990X
EI 1876-9918
J9 SILICON-NETH
JI Silicon
PD FEB
PY 2019
VL 11
IS 1
BP 367
EP 376
DI 10.1007/s12633-018-9889-x
PG 10
WC Chemistry, Physical; Materials Science, Multidisciplinary
GA HK4GV
UT WOS:000457881700035
DA 2023-12-05
ER
PT J
AU Dri, M
Sanna, A
Maroto-Valer, MM
AF Dri, Marco
Sanna, Aimaro
Maroto-Valer, M. Mercedes
TI Dissolution of steel slag and recycled concrete aggregate in ammonium
bisulphate for CO2 mineral carbonation
LA English
DT Article
DE Mineral carbonation; Ammonium bisulphate; Dissolution; Steel slag;
Recycled concrete aggregate
ID KINETICS; PHASE; CAPTURE; ORE
AB Recent research on mineral carbonation has focused attention on multi-step
processes which appear more attractive than single-step processes due to the higher
purity of the final products. Recent studies on mineral carbonation have indicated
that industrial wastes can require a lower degree of pre-treatment and less energy-
intensive carbonation conditions, in comparison to mineral rocks. In light of this,
a closed-loop, multi-step process which allows precipitation of calcium carbonate
(CaCO3) from Ca-rich waste streams has been developed. The main objective of this
work is to focus on mineral dissolution kinetics for steel slag and recycled
concrete aggregate, to confirm the formation of CaSO4(s) for the following
carbonation reaction. Dissolution studies using ammonium bisulphate (NH4HSO4)
solutions were carried out at three different temperatures (25-50-90 degrees C).
For the steel slag sample, solid crystals of CaSO4 were produced on the surface of
the reacted particles of the starting material. Mg and Fe, instead, dissolved into
solution and their efficiencies of dissolution, after 3 h at 90 degrees C, were 85%
and 90% respectively. Kinetic analyses found that the Avrami model, which explains
the diffusion process for systems in which crystallization occurs on the sample
surface, can accurately represent the kinetics of steel slag dissolution. The
calculated activation energy was 42 kJ/mol. Dissolution of recycled concrete
aggregate into an NH4HSO4 solution, as for steel slag, produced precipitated CaSO4,
while aluminium, the other main metal present, dissolved partially (40% at 25
degrees C) into solution. For the recycled concrete aggregate, the Avrami model
fitted best the results from dissolution experiments. However, because of the low
values of R-2 at 25 degrees C and 90 degrees C, the Avrami model cannot be
considered valid in terms of the kinetic of the reaction and further investigations
are needed to corroborate precipitation of crystals of CaSO4 on the surface of RCA
samples. (C) 2013 Elsevier B.V. All rights reserved.
C1 [Dri, Marco; Sanna, Aimaro; Maroto-Valer, M. Mercedes] Heriot Watt Univ, Sch
Engn & Phys Sci, Ctr Innovat Carbon Capture & Storage CICCS, Edinburgh EH14 4AS,
Midlothian, Scotland.
C3 Heriot Watt University
RP Maroto-Valer, MM (corresponding author), Heriot Watt Univ, Sch Engn & Phys Sci,
Edinburgh EH14 4AS, Midlothian, Scotland.
EM m.maroto-valer@hw.ac.uk
RI Maroto-Valer, Mercedes/F-5016-2014
OI Maroto-Valer, Mercedes/0000-0003-1643-2863
FU Caterpillar UK Engines Company Limited; Centre for Innovation in Carbon
Capture and Storage (Engineering and Physical Sciences Research Council)
[EP/F012098/2]; EPSRC [EP/F012098/2] Funding Source: UKRI; Engineering
and Physical Sciences Research Council [EP/F012098/2] Funding Source:
researchfish
FX The authors acknowledge Caterpillar UK Engines Company Limited and the
Centre for Innovation in Carbon Capture and Storage (Engineering and
Physical Sciences Research Council grant EP/F012098/2) for the support
to the project, and Tarmac Ltd UK and Roger Bullivant Ltd UK for
providing the samples.
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[No title captured]
[No title captured]
NR 26
TC 56
Z9 61
U1 3
U2 85
PI AMSTERDAM
SN 0378-3820
EI 1873-7188
PD SEP
PY 2013
VL 113
BP 114
EP 122
DI 10.1016/j.fuproc.2013.03.034
PG 9
GA 154YT
UT WOS:000319713300016
DA 2023-12-05
ER
PT J
AU Xu, K
Deng, T
Liu, JT
Peng, WG
AF Xu, Ke
Deng, Tong
Liu, Juntan
Peng, Weigong
TI Study on the phosphate removal from aqueous solution using modified fly
ash
SO FUEL
LA English
DT Article
DE Fly ash; Modification; Sulfuric acid; Phosphate; Removal
ID CONSTRUCTED WETLAND SYSTEMS; IMMOBILIZATION; SLAG
AB In this work the fly ash was modified by sulfuric acid for the removal of
phosphate. It was found that modification of fly ash could significantly enhance
the phosphate immobilization ability of the fly ash. The specific surface area of
the fly ash increased from 8.8 to 32.5 m(2)/g after treated with sulfuric acid. The
modification of the fly ash also resulted in the mobilization of acid-soluble metal
ions due to partial or complete dissolution of the metals under the acidic
conditions. Both adsorption and precipitation contributed to the removal of
phosphate by the modified fly ash but precipitation was a major mechanism of
phosphate removal. The experimental results showed that adsorption of phosphate by
the modified fly ash was rapid, the removal percentage of phosphate could reach
maximum in 5 min. In the range of 5-9, pH did not significantly affect the removal
of phosphate and the removal percentage of phosphate increased with the increase of
adsorbent dosage. The adsorption of phosphate by the modified fly ash could be
described well by Langmuir isotherm equation, the Langmuir constant Q(0) was 9.15
mg g (1). The XRD patterns and the SEM images of modified fly ash after sorption
revealed that CaHPO(4)center dot 2H(2)O was formed in the removal of phosphate. In
addition, phosphate also formed precipitate with aluminum and iron. (C) 2010
C1 [Xu, Ke; Liu, Juntan; Peng, Weigong] Zhengzhou Inst Aeronaut Ind Management,
Zhengzhou 450015, Peoples R China.
[Deng, Tong] Chinese Acad Sci, Inst Proc Engn, Beijing 100080, Peoples R China.
C3 Chinese Academy of Sciences; Institute of Process Engineering, CAS
RP Xu, K (corresponding author), Zhengzhou Inst Aeronaut Ind Management, Zhengzhou
EM xuke72@tom.com
FU Natural Science Foundation of the Education Department of Henan Province
of China [2008B610013]
FX This work was supported by the Natural Science Foundation of the
Education Department of Henan Province of China (No. 2008B610013).
8846(02)00888-8
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NR 16
TC 56
Z9 81
U1 6
U2 57
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
J9 FUEL
JI Fuel
PD DEC
PY 2010
VL 89
IS 12
BP 3668
EP 3674
DI 10.1016/j.fuel.2010.07.034
PG 7
GA 653JK
UT WOS:000282086200009
DA 2023-12-05
ER
PT J
AU Anuwattana, R
Khummongkol, P
AF Anuwattana, Rewadee
Khummongkol, Pojanie
TI Conventional hydrothermal synthesis of Na-A zeolite from cupola slag and
aluminum sludge
LA English
DT Article
DE Cupola slag; Zeolite; Synthesis; Fusion method; Hydrothermal
ID COAL FLY-ASH
AB Na-A type zeolites were prepared from two industrial wastes: the solid by-
product of cupola slag and aluminum sludge from an aluminum plating plant. Two
preparation methods using the same starting material compositions were carried out.
In the first method, alkaline fusion was introduced, followed by the hydrothermal
treatment to obtain sodium aluminosilicate which was then crystallized in NaOH
solution under the condition of 90 +/- 3 degrees C for 1-9 h with different
H2O/SiO2 ratios. The result shows that higher H2O/SiO2 ratio increases the rate of
crystallization. The largest amount of crystallinity for Na-A was found at 3 h. In
the second method, alkaline hydrothermal treatment without fusion was carried out
in the same condition as the first method. No Na-A zeolite was obtained by this
method. The changes of the dissolved amounts of Si4+ and Al3+ in 3 M NaOH were
investigated during the hydrothermal reaction. (C) 2008 Elsevier B.V. All rights
reserved.
C1 [Anuwattana, Rewadee; Khummongkol, Pojanie] King Mongkuts Univ Technol Thonburi,
Sch Energy & Mat, Environm Technol Div, Bangkok 10140, Thailand.
C3 King Mongkuts University of Technology Thonburi
RP Khummongkol, P (corresponding author), King Mongkuts Univ Technol Thonburi, Sch
Energy & Mat, Environm Technol Div, Bangkok 10140, Thailand.
EM Pojanie.khu@kmutt.ac.th
FU Thailand Research Fund
FX This research was supported by Thailand Research Fund under the Royal
Golden jubilee award (TRF-RGJ).
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PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD JUL 15
PY 2009
VL 166
IS 1
BP 227
EP 232
DI 10.1016/j.jhazmat.2008.11.020
PG 6
GA 453MQ
UT WOS:000266615100030
PM 19111982
DA 2023-12-05
ER
PT J
AU Wang, L
Skjevrak, G
Hustad, JE
Gronli, MG
AF Wang, Liang
Skjevrak, Geir
Hustad, Johan E.
Gronli, Morten G.
TI Effects of Sewage Sludge and Marble Sludge Addition on Slag
Characteristics during Wood Waste Pellets Combustion
SO ENERGY & FUELS
LA English
DT Article
ID BIOMASS PELLETS; MELTING BEHAVIOR; ASH; KAOLIN; FUELS; TEMPERATURE;
TRANSFORMATIONS; TENDENCIES; PREVENTION; REDUCTION
AB The objectives of the present work were to investigate the effects of sewage
sludge and marble sludge addition on slagging tendency and obtain better
understandings for slag formation processes during the combustion of problematic
wood waste pellets. Wood waste pellets produced with and without additives were
combusted in a boiler (1.2 MW(th)) with continuous measurements of the combustion
temperature and flue gas composition. The chemical composition, mineral phase, and
microchemistry of the collected bottom ash and slag were examined by X-ray
fluorescence (XRF), X-ray diffraction (XRD), and scanning electron microscopy
coupled with energy dispersive X-ray analysis (SEM/EDX). Reference wood waste
pellets showed a high slagging tendency with 34 wt % of the ingoing fuel ash formed
as slag on the grate. XRF and SEM/EDX analyses revealed high contents of Si, K, and
Na in the slag and a clear correlation among the three elements. It implies melted
fractions of the slag consist of alkali silicates indirectly observed as glass
phases by XRD analysis. The severe slagging of wood waste pellets was reduced
distinctly upon addition of marble sludge. For two marble sludge added combustion
tests, less than 3 wt % of the ingoing fuel ash formed as low sintering degrees
slag. The mineral compositions of the resultant slag were changed from low melting
point silicates to high temperature melting calcium based silicates, oxides, and
hydroxides. SEM/EDX revealed enhancement of Ca and Mg in the melted slag, which
were possibly originated from marble sludge and dissolved in ash melts. This may
lead to release of alkali metals from the ash melts thereby reducing the formed
melt amount. In addition, marble sludge addition restrained sintering and
accumulation of melted ash into a continuous phase and resulted in fragile slag
particles. Addition of 4 wt % sewage sludge has a minor effect on the slag
formation of wood waste pellets combustion. The sizes and sintering degrees of the
formed slag were considerably decreased and the mineral compositions in the slag
were dominated by high temperature melting corundum and calcium silicates. The
enrichment of kalsilite observed in the slag was probably caused by the reactions
of aluminum silicates in the sewage sludge with potassium from the fuel. The
corundum, calcium silicates, and kalsilite have higher melting temperatures and
thus gave a lower ash melt fraction in the slag. However, as a result of the
addition of sewage sludge, both the ash content and the Si level of ingoing fuel
pellets were enhanced. Thereby the formed slag amount increased slightly for the
combustion of the 8 wt % sewage sludge blended wood waste pellets.
C1 [Wang, Liang; Skjevrak, Geir; Hustad, Johan E.; Gronli, Morten G.] Norwegian
Univ Sci & Technol, Dept Energy & Proc Engn, N-7034 Trondheim, Norway.
RP Wang, L (corresponding author), Norwegian Univ Sci & Technol, Dept Energy & Proc
Engn, N-7034 Trondheim, Norway.
EM liang.wang@sintef.no
RI Wang, Liang/L-3759-2019
OI Gronli, Morten Gunnar/0000-0003-1788-7499; Wang,
Liang/0000-0002-1458-7653
FU Research Council of Norway; More Biovarme AS; Ekornes ASA
FX The financial support from the Research Council of Norway is gratefully
acknowledged. The support given by Johnny Winsjansen (More Biovarme AS),
Fred Anton Alvestad and Hakon Eikemo (Ekornes ASA), during the
experiments is gratefully appreciated. Finally, we thank two reviewers
for their insightful comments on our work.
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TC 55
Z9 57
U1 0
U2 52
PI WASHINGTON
SN 0887-0624
J9 ENERG FUEL
JI Energy Fuels
PD DEC
PY 2011
VL 25
IS 12
BP 5775
EP 5785
DI 10.1021/ef2007722
PG 11
GA 860KF
UT WOS:000297946500026
DA 2023-12-05
ER
PT J
AU Ogirigbo, OR
Black, L
AF Ogirigbo, Okiemute Roland
Black, Leon
TI Chloride binding and diffusion in slag blends: Influence of slag
composition and temperature
LA English
DT Article
DE Chloride binding; Granulated blast-furnace slag; Temperature; Diffusion;
Microstructure
ID BLAST-FURNACE SLAG; HYDRATION PRODUCTS; HYDRAULIC ACTIVITY; PORE
SOLUTION; CEMENT; PORTLAND; CONCRETE; DURABILITY; STRENGTH; INGRESS
AB This study has investigated the impact of a change in GGBS chemical composition
on the chloride ingress resistance of slag blended cements under different
temperature regimes. Two slags, having alumina contents of 12.23 and 7.77%
respectively, were combined with a CEM I 52.5 R at 30 wt% replacement. Chloride
binding and diffusion tests were conducted on paste and mortar samples
respectively. All tests were carried out at temperatures of 20 degrees C and 38
degrees C. The higher temperature resulted in an increase in chloride binding;
attributed to greater degrees of slag hydration. Despite this, chloride ingress was
greater at 38 degrees C; attributed to changes in the pore structure and the
chloride binding capacities of the slag blends. The more reactive, aluminium-rich
slag performed better in terms of chloride binding and resistance to chloride
penetration, especially at the high temperature and this was attributed to its
higher alumina content and greater degree of reaction at 38 degrees C. (C) 2017
C1 [Ogirigbo, Okiemute Roland] Univ Benin, Dept Civil Engn, Fac Engn, Benin,
Nigeria.
[Ogirigbo, Okiemute Roland; Black, Leon] Univ Leeds, Inst Resilient Infrastruc,
Sch Civil Engn, Woodhouse Lane, Leeds LS2 9JT, W Yorkshire, England.
C3 University of Benin; University of Leeds
RP Ogirigbo, OR (corresponding author), Univ Benin, Dept Civil Engn, Fac Engn,
Benin, Nigeria.
EM okiemute.ogirigbo@uniben.edu; L.Black@leeds.ac.uk
RI Black, Leon/B-5840-2008; Ogirigbo, Okiemute Roland/O-9514-2018
OI Black, Leon/0000-0001-8531-4989; Ogirigbo, Okiemute
Roland/0000-0002-4119-2892
FU Petroleum Technology Development Fund (PTDF) of Nigeria
FX The authors would like to thank the Petroleum Technology Development
Fund (PTDF) of Nigeria for providing the funds for this research.
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NR 61
TC 54
Z9 55
U1 2
U2 40
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD SEP 15
PY 2017
VL 149
BP 816
EP 825
DI 10.1016/j.conbuildmat.2017.05.184
PG 10
GA FA6ET
UT WOS:000405536800076
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Fernández-González, D
Ruiz-Bustinza, I
Mochón, J
González-Gasca, C
Verdeja, LF
AF Fernandez-Gonzalez, D.
Ruiz-Bustinza, I.
Mochon, J.
Gonzalez-Gasca, C.
Verdeja, L. F.
TI Iron Ore Sintering: Process
LA English
DT Review
DE Agglomeration; CAP process; flame front; HPS process; iron ore; MEBIOS
process; sintering; softening and melting
ID COMPOSITE AGGLOMERATION; MINERAL PHASES; QUASI-PARTICLE; CALCIUM
FERRITE; SILICO-FERRITES; COMBUSTION-RATE; ALUMINUM SFCA; BED STRUCTURE;
RAW-MATERIALS; COKE BREEZE
AB Sintering is a thermal agglomeration process that is applied to a mixture of
iron ore fines, recycled ironmaking products, fluxes, slag-forming agents, and
solid fuel (coke). The purpose of the sintering process is manufacturing a product
with the suitable characteristics (thermal, mechanical, physical and chemical) to
be fed to the blast furnace. The process has been widely studied and researched in
the iron and steelmaking industry to know the best parameters that allow one to
obtain the best sinter quality. The present article reviews the sintering process
that the mixture follows, once granulated, when it is loaded onto the sinter
strand. There, the sinter mixture is partially melted at a temperature between
1300-1480 degrees C and undergoes a series of reactions that forms the sinter cake
to be loaded into the blast furnace to produce pig iron.
C1 [Fernandez-Gonzalez, D.; Verdeja, L. F.] Univ Oviedo, Sch Mines Energy & Mat,
Dept Mat Sci & Met Engn, Oviedo 33004, Asturias, Spain.
[Ruiz-Bustinza, I.; Mochon, J.] Natl Ctr Met Res CENIM CSIC, Dept Primary Met &
Recycling, Madrid, Spain.
[Gonzalez-Gasca, C.] European Univ Madrid Laureate Int Univ, Madrid, Spain.
C3 University of Oviedo; Consejo Superior de Investigaciones Cientificas
(CSIC); Centro Nacional de Investigaciones Metalurgicas (CENIM);
European University of Madrid
RP Fernández-González, D (corresponding author), Univ Oviedo, Sch Mines Energy &
Mat, Dept Mat Sci & Met Engn, Oviedo 33004, Asturias, Spain.
EM fernandezgdaniel@uniovi.es
RI ruiz-bustinza, inigo/AFV-2095-2022; Fernández-González,
Daniel/AAA-7211-2020; González, Daniel Fernández/K-6869-2019;
Ruiz-Bustinza, Inigo/L-5899-2014
OI Fernández-González, Daniel/0000-0001-6957-4764; Ruiz-Bustinza,
Inigo/0000-0002-8571-1105
FU Spanish Ministry of Education, Culture and Sports via an FPU (Formacion
del Profesorado Universitario) [FPU014/02436]
FX This research was supported by the Spanish Ministry of Education,
Culture and Sports via an FPU (Formacion del Profesorado Universitario)
grant to Daniel Fernandez Gonzalez (FPU014/02436).
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NR 104
TC 54
Z9 56
U1 7
U2 97
PI PHILADELPHIA
SN 0882-7508
EI 1547-7401
PY 2017
VL 38
IS 4
BP 215
EP 227
DI 10.1080/08827508.2017.1288115
PG 13
GA EX7JU
UT WOS:000403425300001
DA 2023-12-05
ER
PT J
AU Yang, L
Yan, Y
Hu, ZH
AF Yang, Lin
Yan, Yun
Hu, Zhihua
TI Utilization of phosphogypsum for the preparation of non-autoclaved
aerated concrete
LA English
DT Article
DE Aerated concrete; Phosphogypsum; Compressive strength; Shrinking
ID ASH; BINDER; CEMENT; WASTE
AB Phosphogypsum (PG) was used as raw material for the preparation of non-
autoclaved aerated concrete, a series of technological parameters, such as water to
solid ratio (W/S), quick lime content, steam temperature, and chemical activators,
were investigated based on the density and compressive strength of specimens in
this paper and the performances of products were also tested. The optimal mix
proportion for preparing PG non-autoclaved aerated concrete (about 700 kg/m(3)) is
as follows: cement 15%, Ground Granulated Blast Furnace Slag (GGBFS) 30%, PG 55%,
quick lime 7%, Na2SO4 1.6%, aluminum powder 0.074%, W/S 0.45. The best steam
temperature used for curing the specimens is 90 degrees C. The compressive
strength, frost-resistance and thermal conductivity of products meet the
requirements of Chinese autoclaved aerated concrete blocks standard, however, the
shrinking of non-autoclaved aerated concrete is still a challenge and the
durability also must be observed in the next work. The results also show that
phosphogypsum not only plays the role of filler but also plays the role of
activator. (C) 2013 Elsevier Ltd. All rights reserved.
C1 [Yang, Lin; Yan, Yun; Hu, Zhihua] Southwest Univ Sci & Technol, State Key Lab
Cultivat Base Nonmetal Composites &, Mianyang 621010, Sichuan, Peoples R China.
C3 Southwest University of Science & Technology - China
RP Yan, Y (corresponding author), Southwest Univ Sci & Technol, State Key Lab
Cultivat Base Nonmetal Composites &, Mianyang 621010, Sichuan, Peoples R China.
EM yanglin06142@163.com; yanyun@swust.edu.cn
OI Yan, Yun/0000-0003-4628-120X
FU National High-Tech. R&D Program (863program) of China [2011AA06A106];
Open Project of State Key Laboratory Cultivation Base for Nonmetal
Composites and Functional Materials [11zxfk26]; Southwest University of
Science and Technology [11ycjj03]
FX The authors acknowledge the financial support of the National High-Tech.
R&D Program (863program) (2011AA06A106) of China, the Open Project of
State Key Laboratory Cultivation Base for Nonmetal Composites and
Functional Materials (11zxfk26) and Postgraduate Innovation Fund
sponsored by Southwest University of Science and Technology(11ycjj03),
and thank the administrators of the fund for their support in our
research.
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NR 16
TC 54
Z9 58
U1 4
U2 94
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
PD JUL
PY 2013
VL 44
BP 600
EP 606
DI 10.1016/j.conbuildmat.2013.03.070
PG 7
GA 161PG
UT WOS:000320205200069
DA 2023-12-05
ER
PT J
AU Mahedi, M
Cetin, B
Dayioglu, AY
AF Mahedi, Masrur
Cetin, Bora
Dayioglu, Asli Y.
TI Leaching behavior of aluminum, copper, iron and zinc from cement
activated fly ash and slag stabilized soils
SO WASTE MANAGEMENT
LA English
DT Article
DE Leaching; Metals; pH-dependent; Fly ash; Slag; Geochemical modeling
ID PERFORMANCE PROPERTIES; TRACE-ELEMENTS; BY-PRODUCTS; BOTTOM ASH; COAL
ASH; PH; METALS; WASTES; STEEL; LEACHABILITY
AB The use of industrial by-products such as fly ash and slag have become very
prevalent in soil stabilization owing to its suitable physical and mechanical
properties, and economical advantages. However, fly ash and slag have been
identified as the potential source of toxic substances, and may pose environmental
risk by leaching heavy and trace metals into soil, surface and groundwater.
Toxicity characteristic leaching procedure (TCLP) tests were conducted to
investigate the environmental hazards associated with the leaching of aluminum
(Al), copper (Cu), iron (Fe) and zinc (Zn) from fly ashes, slag, type I/II cement
and cement activated fly ash and slag stabilized soils. Sulfate (SO4), dissolved
inorganic carbon (DIC) and dissolved organic carbon (DOC) concentrations were also
quantified to evaluate their influence on metal leaching. To understand the effect
of pH on the leaching behavior, pH-dependent leach tests were conducted at the pH
ranges of 2-14. Results indicated that an increase in fly ash or slag content may
not necessarily increase the effluent metal concentrations. Al, Cu, Zn and DOC
followed an amphoteric leaching pattern where concentrations increased in both
acidic and basic conditions. In contrast, maximum DIC concentrations occurred at
neutral or near neutral pH values. Fe and SO4 showed cationic leaching behavior
where concentrations decreased with an increase in effluent pH. Additionally, the
leaching controlling mechanisms of the metals were identified by implementing
geochemical modeling program Visual MINTEQ. The geochemical analyses indicated that
the solubility of Al3+ and Fe3+ were controlled by precipitation/dissolution
reactions of oxide/hydroxide minerals at all pH values. Leaching of Cu2+ was only
solubility controlled at pH higher than 7, whereas Zn2+ leaching was solubility
controlled in the pH range of 8-12. (C) 2019 Elsevier Ltd. All rights reserved.
C1 [Mahedi, Masrur; Cetin, Bora] Iowa State Univ, Dept Civil Construct & Environm
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[Dayioglu, Asli Y.] Istanbul Tech Univ, Dept Civil Engn, Ayazaga Campus,Civil
Engn Bldg, TR-34469 Istanbul, Turkey.
C3 Iowa State University; Istanbul Technical University
RP Cetin, B (corresponding author), Iowa State Univ, Dept Civil Construct &
Environm Engn, 813 Bissell Rd,Town Engn Bldg, Ames, IA 50011 USA.
EM mmahedi@iastate.edu; bcetin@iastate.edu; yalcinas@itu.edu.tr
RI DAYIOGLU, ASLI YALCIN/S-5330-2017; Mahedi, Masrur/U-9786-2019
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NR 79
TC 53
Z9 56
U1 9
U2 83
PI OXFORD
SN 0956-053X
EI 1879-2456
J9 WASTE MANAGE
JI Waste Manage.
PD JUL 15
PY 2019
VL 95
BP 334
EP 355
DI 10.1016/j.wasman.2019.06.018
PG 22
GA JR9EX
UT WOS:000499920700033
PM 31351620
DA 2023-12-05
ER
PT J
AU Yi, C
Ma, HQ
Zhu, HG
Li, WJ
Xin, ML
Liu, YL
Guo, YD
AF Yi, Cheng
Ma, Hongqiang
Zhu, Hongguang
Li, Weijian
Xin, Minglang
Liu, Yilei
Guo, Yongdong
TI Study on chloride binding capability of coal gangue based cementitious
materials
LA English
DT Article
DE High-aluminum coal gangue; Slag; Chloride binding; Freundlich equation;
Friedel's salt
ID FLY-ASH CONCRETE; HYDRATION PRODUCTS; BLENDED CEMENTS; CAPACITY;
ENVIRONMENT; METAKAOLIN; DIFFUSION; LIMESTONE; MIXTURES; MORTARS
AB The addition of supplementary cementitious materials containing Al2O3 can
improve the chloride binding capability of hardened cement paste to varying
degrees, thereby enhancing the durability of reinforced concrete structures. This
work was designed to investigate the high-aluminum coal gangue based cementitious
materials chloride binding capability, including coal gangue content, coal gangue-
slag combined addition and coal gangue calcination temperature. The phase
composition and Friedel's salt contents in the specimens were evaluated by XRD and
TG-DTG analysis. The results showed that the specimens chloride binding isotherms
could be described by Freundlich equation. The coal gangue optimal content was
between 20% and 30% and the maximum content was 40%. The chloride binding
capability of slag was stronger than that of coal gangue, which promoted the
formation of Friedel's salt. In the content range of this study, the chloride
binding capability of coal gangue specimens increased at first and then decreased
with the increase of the molar ratios of Ca/Si and Si/Al. When the coal gangue-slag
composite was added, the chloride binding capability increased with the increase of
the mole ratios of Ca/Si and Si/Al, presenting a positive linear relationship. (C)
C1 [Yi, Cheng; Ma, Hongqiang; Zhu, Hongguang; Li, Weijian; Xin, Minglang; Liu,
Yilei; Guo, Yongdong] China Univ Min & Technol Beijing, Coll Mech & Architectural
C3 China University of Mining & Technology
RP Ma, HQ (corresponding author), China Univ Min & Technol Beijing, Coll Mech &
Architectural Engn, Beijing 100083, Peoples R China.
EM 745323692@qq.com
OI Ma, Hongqiang/0000-0002-9076-0147
FU National Natural Science Foundation of China (NSFC) [51578539]; Beijing
Natural Science Foundation [8164061]
FX This research was sponsored by the National Natural Science Foundation
of China (NSFC, NO.51578539) and Beijing Natural Science Foundation
funded projects (NO.8164061). The authors gratefully acknowledge test
support from materials and durability laboratory of China University of
Mining and Technology (Beijing).
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NR 36
TC 53
Z9 58
U1 13
U2 126
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD APR 10
PY 2018
VL 167
BP 649
EP 656
DI 10.1016/j.conbuildmat.2018.02.071
PG 8
GA GE0IJ
UT WOS:000430897200059
DA 2023-12-05
ER
PT J
AU Cristelo, N
Tavares, P
Lucas, E
Miranda, T
Oliveira, D
AF Cristelo, Nuno
Tavares, Pedro
Lucas, Ernesto
Miranda, Tiago
Oliveira, Daniel
TI Quantitative and qualitative assessment of the amorphous phase of a
Class F fly ash dissolved during alkali activation reactions - Effect of
mechanical activation, solution concentration and temperature
LA English
DT Article
DE Alkaline activation; Strength; Chemical properties; Microstructures
ID DISSOLUTION KINETICS; COMPRESSIVE STRENGTH; HYDRAULIC-PROPERTIES;
PORTLAND-CEMENT; CALCIUM CONTENT; HYBRID CEMENTS; SLAG
AB A detailed analysis of the effects of mechanical activation and temperature on
the dissolution process of a Portuguese Class F fly ash was developed. The
evolution of the silica and alumina dissolved and transferred to the
aluminosilicate gel was characterised. Quantification of bulk vitreous mass was
performed using X-ray diffraction, together with the identification of the most
relevant amorphous phases dissolved. The breakage process is responsible for
further modifications of the original particle than just the exposure of additional
surface area and increased structural disorder. X-ray diffraction and Rietveld
amorphous bulk quantification proved to be an inadequate methodology to quantify
the effects of mechanical activation. Increasing dissolution temperature proved to
be very effective in terms of bulk mass dissolved, with higher dissolution values
after 16 h, at 80 degrees C, than after 90 days, at 20 degrees C. The semi
empirical Avrami model was found to be satisfactorily fitted to the experimental
data regarding the dissolution percentage as a function of time. Compressive
strength evolution was found to be related to the release of amorphous bulk phases,
and in particular to the transfer of aluminium into the aluminosilicate gel,
throughout the entire curing period of 90 days. (C) 2016 Elsevier Ltd. All rights
reserved.
C1 [Cristelo, Nuno; Lucas, Ernesto] Univ Tras Os Montes & Alto Douro, Dept Engn,
CQVR, P-5000801 Vila Real, Portugal.
[Tavares, Pedro] Univ Tras Os Montes & Alto Douro, Dept Chem, CQVR, P-5000801
[Miranda, Tiago; Oliveira, Daniel] Univ Minho, Dept Civil Engn, ISISE, Campus
Azurem, P-4800058 Guimaraes, Portugal.
C3 University of Tras-os-Montes & Alto Douro; University of Tras-os-Montes
& Alto Douro; Universidade do Minho
RP Cristelo, N (corresponding author), Univ Tras Os Montes & Alto Douro, Dept Engn,
CQVR, P-5000801 Vila Real, Portugal.
EM ncristel@utad.pt; ptavares@utad.pt; elucas@utad.pt;
tmiranda@civil.uminho.pt; danvco@civil.uminho.pt
RI Miranda, Tiago/ABE-2391-2020; Tavares, Pedro B/B-8253-2013; Miranda,
Tiago/AAQ-9479-2021; Oliveira, Daniel V./I-3804-2012; Cristelo, Nuno
Miguel/B-3636-2010
OI Tavares, Pedro B/0000-0001-7589-1299; Miranda,
Tiago/0000-0003-4054-6860; Oliveira, Daniel V./0000-0002-8547-3805;
Cristelo, Nuno Miguel/0000-0002-3600-1094
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NR 56
TC 53
Z9 54
U1 5
U2 29
PU ELSEVIER SCI LTD
PI OXFORD
SN 1359-8368
EI 1879-1069
PD OCT 15
PY 2016
VL 103
BP 1
EP 14
DI 10.1016/j.compositesb.2016.08.001
PG 14
GA DW8WM
UT WOS:000383936200001
DA 2023-12-05
ER
PT J
AU Xiao, D
Wang, WL
Lu, BX
AF Xiao, Dan
Wang, Wanlin
Lu, Boxun
TI Effects of B2O3 and BaO on the Crystallization
Behavior of CaO-Al2O3-Based Mold Flux for Casting
High-Al Steels
LA English
DT Article
ID VISCOSITY; RATIO; SLAGS; TI
AB The non-reactive lime-alumina-based mold flux has been proposed to overcome the
aluminum introduced slag/steel interaction problems during the casting of high
aluminum bearing steels. In this article, a new mold flux with CaO/Al2O3 (C/A)
ratio of 2 was designed, and the effects of BaO substituting for CaO to replace
B2O3 on the mold flux crystallization behaviors have been investigated through the
using of single hot thermocouple technology and double hot thermocouple technology
(DHTT). The results suggested that BaO shows the stronger tendency to inhibit
crystallization of mold flux comparing with B2O3; however, the synergic effect of
the combination of BaO and B2O3 tends to improve the mold flux crystallization in
this non-reactive mold flux system. The analysis of the crystallized phases for
different samples and the crystallization behaviors under simulated thermal
gradient through DHTT were also conducted to support the reliability of above
conclusions. (C) The Minerals, Metals & Materials Society and ASM International
2015
C1 [Xiao, Dan; Wang, Wanlin; Lu, Boxun] Cent S Univ, Sch Met & Environm, Changsha
FU NSFC [51274244, 51322405]; Hunan Excellent Young Scholar Funding
[14JJ1005]
FX The financial support from NSFC (51274244, 51322405) and Hunan Excellent
Young Scholar Funding (14JJ1005) is greatly acknowledged.
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NR 17
TC 53
Z9 55
U1 1
U2 53
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD APR
PY 2015
VL 46
IS 2
BP 873
EP 881
DI 10.1007/s11663-014-0286-6
PG 9
Engineering
GA CE5GW
UT WOS:000351860300037
DA 2023-12-05
ER
PT J
AU Li, M
Utigard, T
Barati, M
AF Li, Mark
Utigard, Torstein
Barati, Mansoor
TI Removal of Boron and Phosphorus from Silicon Using
CaO-SiO2-Na2O-Al2O3 Flux
LA English
CT Symposium on CFD Modeling and Simulation in Materials Processing held
during the TMS Annual Meeting and Exhibition
CY MAR 11-15, 2012
CL Orlando, FL
ID THERMODYNAMIC PROPERTIES; IMPURITY GETTER; GRADE-SILICON; LIQUID COPPER;
SI; SOLIDIFICATION; PURIFICATION; IRON; TITANIUM; ALUMINUM
AB A combination of solvent refining and flux treatment was employed to remove
boron and phosphorus from crude silicon to acceptable levels for solar
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examined under a range of slag compositions, varying in CaO:SiO2 and SiO2:Al2O3
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substantial increase of boron distribution coefficient. The highest boron and
phosphorus distribution coefficients are 47 and 1.1, respectively. Using these
optimum slags to reduce boron and phosphorus in MG-Si to solar grade level, a slag
mass about 0.3 times and 17 times mass of alloy would be required, respectively.
C1 [Li, Mark; Utigard, Torstein; Barati, Mansoor] Univ Toronto, Dept Mat Sci &
Engn, Toronto, ON M5S 3E4, Canada.
C3 University of Toronto
RP Li, M (corresponding author), Univ Toronto, Dept Mat Sci & Engn, Toronto, ON M5S
3E4, Canada.
EM mark.li@mail.utoronto.ca
FU NSERC
FX The present study was partially supported by NSERC.
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NR 46
TC 53
Z9 62
U1 1
U2 47
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD FEB
PY 2014
VL 45
IS 1
BP 221
EP 228
DI 10.1007/s11663-013-0011-x
PG 8
Engineering
GA 304GN
UT WOS:000330735200026
DA 2023-12-05
ER
PT J
AU Varacalle, DJ
Guillen, DP
Deason, DM
Rhodaberger, W
Sampson, E
AF Varacalle, Dominic J., Jr.
Guillen, Donna Post
Deason, Douglas M.
Rhodaberger, William
Sampson, Elliott
TI Effect of grit-blasting on substrate roughness and coating adhesion
SO JOURNAL OF THERMAL SPRAY TECHNOLOGY
LA English
DT Article
DE bond strength; grit blasting; statistical design of experiments;
substrate preparation; surface roughness; twin-wire electric arc
AB Statistically designed experiments were performed to compare the surface
roughness produced by grit blasting A36/1020 steel using different abrasives. Grit
blast media, blast pressure, and working distance were varied using a Box-type
statistical design of experiment (SDE) approach. The surface textures produced by
four metal grits (HG16, HG18, HG25, and HG40) and three conventional grits (copper
slag, coal slag, and chilled iron) were compared. Substrate roughness was measured
using surface profilometry and correlated with operating parameters. The HG16 grit
produced the highest surface roughness of all the grits tested. Aluminum and zinc-
aluminum coatings were deposited on the grit-blasted substrates using the twin-wire
electric arc (TWEA) process. Bond strength of the coatings was measured with a
portable adhesion tester in accordance with ASTM standard D 4541. The coatings on
substrates roughened with steel grit exhibit superior bond strength to those
prepared with conventional grit. For aluminum coatings sprayed onto surfaces
prepared with the HG16 grit, the bond strength was most influenced by current,
spray distance, and spray gun pressure (in that order). The highest bond strength
for the zinc-aluminum coatings was attained on surfaces prepared using the metal
grits.
C1 Vartech Inc, Idaho Falls, ID USA.
Idaho Natl Engn Lab, Idaho Falls, ID 83415 USA.
USA, Space & Missile Def Command, Huntsville, AL USA.
Ervin Ind, Ann Arbor, MI USA.
Praxair Tafa, Bow, NH USA.
C3 United States Department of Energy (DOE); Idaho National Laboratory
RP Varacalle, DJ (corresponding author), Vartech Inc, Idaho Falls, ID USA.
EM Donna.Guillen@inl.gov
RI Guillen, Donna P/B-9681-2017
OI Guillen, Donna P/0000-0002-7718-4608
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NR 14
TC 53
Z9 59
U1 1
U2 29
PU ASM INTERNATIONAL
PI MATERIALS PARK
PA SUBSCRIPTIONS SPECIALIST CUSTOMER SERVICE, MATERIALS PARK, OH 44073-0002
USA
SN 1059-9630
J9 J THERM SPRAY TECHN
JI J. Therm. Spray Technol.
PD SEP
PY 2006
VL 15
IS 3
BP 348
EP 355
DI 10.1361/105996306X124347
PG 8
WC Materials Science, Coatings & Films
GA 084GK
UT WOS:000240520400007
DA 2023-12-05
ER
PT J
AU Seo, WG
Han, WH
Kim, JS
Pak, JJ
AF Seo, WG
Han, WH
Kim, JS
Pak, JJ
TI Deoxidation equilibria among Mg, Al and O in liquid iron in the presence
of MgO • Al2O3 spinel
LA English
DT Article
DE liquid iron; deoxidation equilibria; spinel; magnesium; aluminum
ID NONMETALLIC INCLUSION; MAGNESIUM; THERMODYNAMICS; CALCIUM; STEEL;
OXYGEN; SLAGS
AB The deoxidation equilibria among Mg, Al and O in liquid iron in the presence of
MgO.Al2O3 spinel was studied at 1 873 K by adding Al and Mg alloys into liquid iron
in MgO and Al2O3 crucibles. From the experimental results, the equilibrium
constant, K-Mg, for the reaction, MgO (s)=Mg+O, and the first- and second-order
interaction parameters including cross-product terms between Mg and O have been
determined. Using these thermodynamic parameters, the relations between a(Mg) vs.
a(O), a(Mg) vs. a(Al) in liquid iron could be well represented with respective
oxide activities in MgO.Al2O3 spinel. A stability diagram for MgO, MgO.Al2O3 and
Al2O3 phases was constructed at 1 873 K as a function of dissolved Mg, Al and O
contents in liquid iron to examine the condition for the formation of MgO.Al2O3
spinel during the deoxidation process.
C1 POSCO, Tech Res Labs, Pohang 790690, South Korea.
Hanyang Univ, Div Mat & Chem Engn, Ansan 425791, South Korea.
C3 POSCO; Hanyang University
RP Seo, WG (corresponding author), Univ Tokyo, Grad Sch Frontier Sci, Dept Adv Mat
Sci, Bunkyo Ku, Tokyo 1130033, Japan.
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U1 1
U2 23
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2003
VL 43
IS 2
BP 201
EP 208
PG 8
GA 649FX
UT WOS:000181197500010
OA gold
DA 2023-12-05
ER
PT J
AU Tian, LY
He, DP
Zhao, JN
Wang, HG
AF Tian Lingyu
He Dongpo
Zhao Jianing
Wang Hongguang
TI Durability of geopolymers and geopolymer concretes: A review
SO REVIEWS ON ADVANCED MATERIALS SCIENCE
LA English
DT Review
DE geopolymer; preparation; carbonation resistance; fire resistance;
corrosion resistance; permeation properties
ID ASH-BASED GEOPOLYMER; PORTLAND-CEMENT CONCRETE; BLAST-FURNACE SLAG;
FLY-ASH; MECHANICAL-PROPERTIES; RECYCLED AGGREGATE; THERMAL-BEHAVIOR;
METHYLENE-BLUE; METAKAOLIN; RESISTANCE
AB Geopolymers are green materials with three-dimensional silicon and aluminum
tetrahedral structures that can be serving as environmentally friendly construction
materials and therefore have the potential to contribute to sustainable
development. In this paper, the mechanism and research progress regarding the
carbonation resistance, structural fire resistance, corrosion resistance,
permeation properties and frost resistance of geopolymer concretes are reviewed,
and the main problems with the durability of geopolymer concretes are discussed.
Geopolymers possess the superb mechanic property and their compression strengths
could be higher than 100 MPa. Generally, the higher the GPC strength, the better
the carbonation-resistant. GPC has excellent fire resistance, due to geopolymers
are acquired an inorganic skeleton which is affected by the alkali content, alkali
cation, and Si/Ai ratio. There are a large number of Al-O and Si-O structures in
geopolymers. Geopolymers do not react with acids at room temperature and can be
used to make acid-resistant materials. Besides, GPC owning low porosity volume
shows good resistance to permeability. The freezing-thawing failure mechanism of
geopolymer concretes is mainly based on hydrostatic and osmotic pressure theory.
GPC has poor frost resistance, and the freezing-thawing limit is less than 75
times.
C1 [Tian Lingyu; He Dongpo; Zhao Jianing; Wang Hongguang] Northeast Forestry Univ,
Sch Civil Engn, Harbin 150040, Peoples R China.
[Wang Hongguang] Northeast Forestry Univ, Minist Educ, Key Lab Biobased Mat Sci
& Technol, Harbin 150040, Peoples R China.
C3 Northeast Forestry University - China; Northeast Forestry University -
China
RP Wang, HG (corresponding author), Northeast Forestry Univ, Sch Civil Engn, Harbin
150040, Peoples R China.; Wang, HG (corresponding author), Northeast Forestry Univ,
Minist Educ, Key Lab Biobased Mat Sci & Technol, Harbin 150040, Peoples R China.
EM wanghongguang@nefu.edu.cn
RI Sabo, Kashi University Talwandi/AAO-3938-2021; WANG,
Hongguang/N-8426-2015
OI WANG, Hongguang/0000-0002-7620-614X
FU National Natural Science Foundation of China [51708092]; China
Postdoctoral Science Fund Project [2018M631894]
FX The research in this paper has been supported by the National Natural
Science Foundation of China (Grant No. 51708092) and China Postdoctoral
Science Fund Project (Grant No. 2018M631894).
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NR 78
TC 52
Z9 54
U1 22
U2 111
PU DE GRUYTER POLAND SP Z O O
PI WARSAW
PA BOGUMILA ZUGA 32A STR, 01-811 WARSAW, MAZOVIA, POLAND
SN 1606-5131
EI 1605-8127
J9 REV ADV MATER SCI
JI Rev. Adv. Mater. Sci.
PD JAN
PY 2021
VL 60
IS 1
BP 1
EP 14
DI 10.1515/rams-2021-0002
PG 14
WC Nanoscience & Nanotechnology; Materials Science, Multidisciplinary
SC Science & Technology - Other Topics; Materials Science
GA QE7AO
UT WOS:000616357300001
OA gold
DA 2023-12-05
ER
PT J
AU Zierold, KM
Odoh, C
AF Zierold, Kristina M.
Odoh, Chisom
TI A review on fly ash from coal-fired power plants: chemical composition,
regulations, and health evidence
SO REVIEWS ON ENVIRONMENTAL HEALTH
LA English
DT Review
DE air pollution; coal ash; coal-fired power plants; fly ash; particles
ID INORGANIC ARSENIC EXPOSURE; BLOOD LEAD CONCENTRATIONS; TYPE-2
DIABETES-MELLITUS; COMBUSTION BY-PRODUCTS; TRACE-ELEMENTS; OXIDATIVE
STRESS; LEACHING BEHAVIOR; ENVIRONMENTAL IMPACTS; DRINKING-WATER;
PRENATAL EXPOSURE
AB Throughout the world, coal is responsible for generating approximately 38% of
power. Coal ash, a waste product, generated from the combustion of coal, consists
of fly ash, bottom ash, boiler slag, and flue gas desulfurization material. Fly
ash, which is the main component of coal ash, is composed of spherical particulate
matter with diameters that range from 0.1 mu m to >100 mu m. Fly ash is
predominately composed of silica, aluminum, iron, calcium, and oxygen, but the
particles may also contain heavy metals such as arsenic and lead at trace levels.
Most nations throughout the world do not consider fly ash a hazardous waste and
therefore regulations on its disposal and storage are lacking. Fly ash that is not
beneficially reused in products such as concrete is stored in landfills and surface
impoundments. Fugitive dust emissions and leaching of metals into groundwater from
landfills and surface impoundments may put people at risk for exposure. There are
limited epidemiological studies regarding the health effects of fly ash exposure.
In this article, the authors provide an overview of fly ash, its chemical
composition, the regulations from nations generating the greatest amount of fly
ash, and epidemiological evidence regarding the health impacts associated with
exposure to fly ash.
C1 [Zierold, Kristina M.] Univ Alabama Birmingham, Environm Hlth Sci, Birmingham,
AL 35294 USA.
[Odoh, Chisom] Univ North Texas, Rehabil & Hlth Serv, Denton, TX 76203 USA.
C3 University of Alabama System; University of Alabama Birmingham;
University of North Texas System; University of North Texas Denton
RP Zierold, KM (corresponding author), Univ Alabama Birmingham, Environm Hlth Sci,
Birmingham, AL 35294 USA.
EM kzierold@uab.edu
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NR 228
TC 52
Z9 53
U1 23
U2 215
PU WALTER DE GRUYTER GMBH
PI BERLIN
PA GENTHINER STRASSE 13, D-10785 BERLIN, GERMANY
SN 0048-7554
EI 2191-0308
J9 REV ENVIRON HEALTH
JI Rev. Environ. Health
PD DEC
PY 2020
VL 35
IS 4
BP 401
EP 418
DI 10.1515/reveh-2019-0039
PG 18
WC Environmental Sciences; Public, Environmental & Occupational Health
SC Environmental Sciences & Ecology; Public, Environmental & Occupational
Health
GA OY5VP
UT WOS:000594314700009
PM 32324165
DA 2023-12-05
ER
PT J
AU Zhang, W
Yao, X
Yang, T
Zhang, ZH
AF Zhang, Wei
Yao, Xiao
Yang, Tao
Zhang, Zuhua
TI The degradation mechanisms of alkali-activated fly ash/slag blend
cements exposed to sulphuric acid
LA English
DT Article
DE Alkali-activated cement; Acid attack; Pore structure; Slag; Fly ash
ID ASH-BASED GEOPOLYMERS; BLAST-FURNACE SLAG; HARDENED PASTE;
PORTLAND-CEMENT; PORE STRUCTURE; PART 1; ATTACK; RESISTANCE; CORROSION;
CONCRETE
AB In the present work alkali-activated fly ash/slag cements (AACs) are synthesized
and exposed to sulphuric acid (pH = 1.0) to investigate their anti-corrosion
properties. The mineralogical compositions, pore structure and microstructure of
different layers of the corroded samples are examined, along with the compressive
strength change. The results show that with fly ash/slag ratio varying from 100/0
to 0/100, the compressive strengths of all of the samples decrease during acid
attack: the most anti-corrosion mixture is found in the pure fly ash binder, which
retains 83.5% strength after 28 days of exposure. Gypsum is only observed in the
surface layer (0-5 mm) of samples. In terms of pore structure, the acid attack
results in higher porosities in the corroded layers than their corresponding
uncorroded layers. The samples with slag addition show a notably pore structure
change. The sulphuric acid attack on the AACs binders has certainly led to the
increase of porosity, regardless of the compact level of AACs (slag addition leads
to compacter microstructure). The Al/Si atomic ratios in the corroded layer
decrease after acid attack, and the reduction ratios become smaller as slag content
increases, suggesting a dense matrix is advantage to impede the loss of aluminum
from gel structures. (C) 2018 Elsevier Ltd. All rights reserved.
C1 [Zhang, Wei; Yao, Xiao] Nanjing Tech Univ, Coll Mat Sci & Engn, Nanjing 210009,
[Yang, Tao] Yancheng Inst Technol, Sch Mat Sci & Engn, Yancheng 224051, Jiangsu,
Peoples R China.
[Zhang, Zuhua] Hunan Univ, Coll Civil Engn, Key Lab Green & Adv Civil Engn Mat &
Applicat Tec, Changsha 410082, Hunan, Peoples R China.
[Zhang, Zuhua] Univ Southern Queensland, Ctr Future Mat, Toowoomba, Qld 4350,
Australia.
C3 Nanjing Tech University; Yancheng Institute of Technology; Hunan
University; University of Southern Queensland
RP Yao, X; Zhang, ZH (corresponding author), Hunan Univ, Coll Civil Engn, Key Lab
Green & Adv Civil Engn Mat & Applicat Tec, Changsha 410082, Hunan, Peoples R China.
EM htmpaper@sina.com; Zuhua.Zhang@usq.edu.au
RI Zhang, Zuhua/AAK-5391-2020; Zhang, Wei/D-6503-2015
OI Zhang, Zuhua/0000-0002-7153-5120; Zhang, Wei/0000-0002-8564-5558; Yang,
Tao/0000-0002-4879-8256
FU Jiangsu Higher Education Institutions for Priority Academic Program
Development (PAPD); National Natural Science Foundation of China
[51702278]; Collaborative Innovation Center for Ecological Building
Materials of Jiangsu Province [CP201506]; Australian Research Council
[DE170101070, DP160104149]; Australian Research Council [DE170101070]
Funding Source: Australian Research Council
FX The authors thank the financial support of the Jiangsu Higher Education
Institutions for Priority Academic Program Development (PAPD). The work
by Yang is supported by the National Natural Science Foundation of China
(No. 51702278) and the Collaborative Innovation Center for Ecological
Building Materials of Jiangsu Province (CP201506). The technical support
provided by Chen Yue from the Modern Analysis and Testing Centre,
Nanjing Tech University is also acknowledged. The participation of Z.
Zhang is supported by Australian Research Council projects DE170101070
and DP160104149.
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NR 47
TC 52
Z9 53
U1 3
U2 35
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 20
PY 2018
VL 186
BP 1177
EP 1187
DI 10.1016/j.conbuildmat.2018.08.050
PG 11
GA GV3GV
UT WOS:000445983300101
DA 2023-12-05
ER
PT J
AU Zhou, LJ
Li, H
Wang, WL
Xiao, D
Zhang, L
Yu, J
AF Zhou, Lejun
Li, Huan
Wang, Wanlin
Xiao, Dan
Zhang, Lei
Yu, Jie
TI Effect of Li2O on the Behavior of Melting, Crystallization,
and Structure for CaO-Al2O3-Based Mold Fluxes
LA English
DT Article
ID INDUCED-PLASTICITY STEELS; HIGH AL STEEL; VISCOUS BEHAVIOR;
INFRARED-SPECTRA; VISCOSITY; ALUMINUM; SLAGS; PERFORMANCE; GLASSES;
SYSTEM
AB The effect of Li2O content on the behavior of melting, crystallization, and
molten structure for CaO-Al2O3-based mold fluxes was investigated in this article,
through use of single hot thermocouple technology (SHTT), Fourier transform
infrared spectroscopy (FTIR), Raman spectroscopy, and X-ray diffraction (XRD). The
SHTT results showed that the melting temperature range of the designed mold fluxes
decreases and the crystallization of mold fluxes is inhibited first and then
becomes enhanced when the Li2O content increases from 1 to 6 mass pct. The FTIR and
Raman spectroscopy results suggested that Li2O could release O2- ions to break the
complex Al-O-Al structural unit into Al-O- structure. Meanwhile, Li2O could also
stabilize the structural unit of Si-O-Al by link aluminate and Q(0)(Si) structure
through providing Li+ ions to merge into the network and compensate for the charges
between Al3+ and Si4+. Besides, the XRD results indicated that the precipitation of
LiAlO2 in molten slag would enhance the crystallization behavior of mold flux when
Li2O content is over 4.5 mass pct.
C1 [Zhou, Lejun; Li, Huan; Wang, Wanlin; Xiao, Dan; Zhang, Lei; Yu, Jie] Cent S
Univ, Sch Met & Environm, Changsha 410083, Peoples R China.
[Zhou, Lejun; Li, Huan; Wang, Wanlin; Xiao, Dan; Zhang, Lei; Yu, Jie] Cent S
Univ, Natl Ctr Int Res Clean Met, Changsha 410083, Peoples R China.
C3 Central South University; Central South University
RI zhou, lejun/HJZ-1171-2023; Zhang, Lei/ABA-4375-2021
OI Zhang, Lei/0000-0002-1758-5733; Zhou, Lejun/0000-0003-3127-6942
FU National Science Foundation of China [U1760202, 51504294]; Opening
Foundation from the Ministry of Education Key Laboratory of
Metallurgical Emission Reduction & Resources Recycling (Anhui University
of Technology)
FX Financial support from the National Science Foundation of China (Grant
Nos. U1760202 and 51504294) and the Opening Foundation from the Ministry
of Education Key Laboratory of Metallurgical Emission Reduction &
Resources Recycling (Anhui University of Technology) are greatly
acknowledged.
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NR 32
TC 52
Z9 54
U1 6
U2 71
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD OCT
PY 2018
VL 49
IS 5
BP 2232
EP 2240
DI 10.1007/s11663-018-1327-3
PG 9
Engineering
GA GT8DR
UT WOS:000444765500012
DA 2023-12-05
ER
PT J
AU Du, MJ
Huang, JJ
Liu, ZY
Zhou, X
Guo, S
Wang, ZQ
Fang, YT
AF Du, Meijie
Huang, Jiejie
Liu, Zheyu
Zhou, Xing
Guo, Shuai
Wang, Zhiqing
Fang, Yitian
TI Reaction characteristics and evolution of constituents and structure of
a gasification slag during acid treatment
SO FUEL
LA English
DT Article
DE Gasification slag; Acetic acid; Hydrochloric acid; Acid treatment;
Composition; Structure evolution
ID COAL FLY-ASH; FT-IR; ADSORPTION; GREEN
AB Gasification slag is a potential resource of high value, which can be utilized
as a porous material by acidification. To have a deep understanding of the
composition and structural characteristics of the acidified slag, the gasification
slag was treated using different concentrations of acetic acid (HAc) and HCl,
respectively. The slag samples, in both an untreated and an acidified form, were
characterized by AAS, XRD, FT-IR, BET, and TG. The results show that the reaction
between the slag and a higher concentration of HAc could generate crystal minerals
like alumohydrocalcite (CaAl2(CO3)(2)(OH)(4)center dot 3H(2)O) and aluminum acetate
hydroxide ((CH3COO)(2)Al(OH)). Meanwhile, HAc treatment results in an increase of
crystallinity, but HCl treatment exerts the opposite effect. In addition, compared
to the untreated, the specific surface area of the slag treated by HAc and HCl
increases 20 times and 86 times, respectively. Acid treatment would make more
mesoporous due to the extraction of Ca.
C1 [Du, Meijie; Huang, Jiejie; Liu, Zheyu; Zhou, Xing; Guo, Shuai; Wang, Zhiqing;
Fang, Yitian] Chinese Acad Sci, Inst Coal Chem, Taiyuan 030001, Shanxi, Peoples R
China.
[Du, Meijie; Zhou, Xing; Guo, Shuai] Univ Chinese Acad Sci, Beijing 100049,
Peoples R China.
[Fang, Yitian] Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal Convers,
Taiyuan 030001, Shanxi, Peoples R China.
C3 Chinese Academy of Sciences; Institute of Coal Chemistry, CAS; Chinese
Academy of Sciences; University of Chinese Academy of Sciences, CAS;
Chinese Academy of Sciences; Institute of Coal Chemistry, CAS
RP Huang, JJ (corresponding author), Chinese Acad Sci, Inst Coal Chem, Taiyuan
030001, Shanxi, Peoples R China.
EM huangjj@sxicc.ac.cn
RI Huang, Jie/GWQ-5005-2022
OI Wang, Zhiqing/0000-0001-9009-9785
FU National Science Foundation of China [21676289]; Teams and Youth
Innovation Promotion Association [2014156]
FX The work is financially supported by the National Science Foundation of
China (21676289), and Teams and Youth Innovation Promotion Association
(2014156).
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NR 43
TC 52
Z9 59
U1 20
U2 114
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD JUL 15
PY 2018
VL 224
BP 178
EP 185
DI 10.1016/j.fuel.2018.03.073
PG 8
GA GG8AV
UT WOS:000432920900018
OA hybrid
DA 2023-12-05
ER
PT J
AU Soleimani, S
Rajaei, S
Jiao, PC
Sabz, A
Soheilinia, S
AF Soleimani, Sepehr
Rajaei, Shabnam
Jiao, Pengcheng
Sabz, Arash
Soheilinia, Sina
TI New prediction models for unconfined compressive strength of geopolymer
stabilized soil using multi-gen genetic programming
SO MEASUREMENT
LA English
DT Article
DE Soil stabilization; Geopolymer; Genetic programming; Prediction
ID CALCIUM CARBIDE RESIDUE; BEARING CAPACITY; FLY; PARAMETERS
AB This study presents new models for the prediction of unconfined compressive
strength (UCS) of geopolymer stabilized clayey soils using a modified branch of
genetic programming, called multi- gen genetic programming (MGGP). The proposed
MGGP models incorporate several parameters affecting the behavior of the UCS of the
clayey stabilized soil. UCS is formulated in terms of percentages of fly ash,
ground granulated blast furnace slag, liquid limit, plastic limit, plasticity
index, molar concentration, alkali to binder ratio, and ratios of sodium and
silicon to aluminum. The importance of each predictor variable is measured through
a sensitivity analysis. The validity of the models and the trend of the results are
verified by performing parametric study. The parametric study results are also in
good agreement with previous studies. The results indicate that the proposed
equations are capable of evaluating UCS accurately.
C1 [Soleimani, Sepehr] Univ Tehran, Coll Civil & Environm Engn, Tehran, Iran.
[Rajaei, Shabnam] Politecn Milan, Dept Civil & Environm Engn, Milan, Italy.
[Jiao, Pengcheng] Univ Penn, Dept Mech Engn & Appl Mech, Philadelphia, PA 19104
USA.
[Sabz, Arash] Texas A&M Univ, Zachry Dept Civil Engn, College Stn, TX 77843 USA.
[Soheilinia, Sina] Univ Tafresh, Coll Civil & Environm Engn, Tehran, Iran.
C3 University of Tehran; Polytechnic University of Milan; University of
Pennsylvania; Texas A&M University System; Texas A&M University College
Station
RP Jiao, PC (corresponding author), Univ Penn, Dept Mech Engn & Appl Mech,
Philadelphia, PA 19104 USA.
EM pjiao@seas.upenn.edu
RI Jiao, Pengcheng/AAY-8438-2020
OI Jiao, Pengcheng/0000-0002-9577-3828
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NR 58
TC 52
Z9 52
U1 3
U2 47
PU ELSEVIER SCI LTD
PI OXFORD
SN 0263-2241
EI 1873-412X
J9 MEASUREMENT
JI Measurement
PD JAN
PY 2018
VL 113
BP 99
EP 107
DI 10.1016/j.measurement.2017.08.043
PG 9
WC Engineering, Multidisciplinary; Instruments & Instrumentation
SC Engineering; Instruments & Instrumentation
GA FI2KK
UT WOS:000411767300011
DA 2023-12-05
ER
PT J
AU Wu, JJ
Li, YL
Ma, WH
Wei, KX
Yang, B
Dai, YN
AF Wu, Ji-jun
Li, Yan-long
Ma, Wen-hui
Wei, Kui-xian
Yang, Bin
Dai, Yong-nian
TI Boron removal in purifying metallurgical grade silicon by
CaO-SiO2 slag refining
LA English
DT Article
DE metallurgical grade silicon; boron removal; thermodynamics; distribution
coefficient; slag refining
ID SOLAR-CELLS; ALUMINUM
AB Boron removal from metallurgical grade silicon (MG-Si) using a calcium silicate
slag was studied. The results show that it is impossible basically to remove boron
using a pure SiO2 refining. The oxidizing ability of CaO-SiO2 slag for boron
removal was characterized by establishing the thermodynamic relationship between
the distribution coefficient of boron (L-B) and the activities of SiO2 and CaO. The
experimental results show that the distribution coefficient and the removal
efficiency of boron are greatly improved with the increase of CaO proportion in the
slag. The maximal value of LB reaches 1.57 with a slag composition of 60% CaO-40%
SiO2 (mass fraction). The boron content in the refined silicon is reduced from
18x10(-6) to 1.8x10(-6) using slag refining at 1600 degrees C for 3 h with a CaO-
SiO2/MG-Si ratio of 2.5, and the removal efficiency of boron reaches 90%.
C1 [Wu, Ji-jun; Li, Yan-long; Ma, Wen-hui; Wei, Kui-xian; Yang, Bin; Dai, Yong-
nian] Kunming Univ Sci & Technol, State Key Lab Complex Nonferrous Met Resources
Cl, Natl Engn Lab Vacuum Met, Kunming 650093, Peoples R China.
[Wu, Ji-jun; Ma, Wen-hui; Wei, Kui-xian; Yang, Bin; Dai, Yong-nian] Kunming Univ
Sci & Technol, Yunnan Prov Key Lab Nonferrous Vacuum Met, Kunming 650093, Peoples R
China.
[Wu, Ji-jun; Li, Yan-long; Ma, Wen-hui; Wei, Kui-xian; Dai, Yong-nian] Kunming
Univ Sci & Technol, Engn Res Ctr Silicon Met & Silicon Mat Yunnan Pro, Kunming
C3 Kunming University of Science & Technology; Kunming University of
Science & Technology; Kunming University of Science & Technology
RP Wu, JJ (corresponding author), Kunming Univ Sci & Technol, State Key Lab Complex
Nonferrous Met Resources Cl, Natl Engn Lab Vacuum Met, Kunming 650093, Peoples R
China.
EM dragon_wu213@126.com
RI ma, wenhui/GQZ-0052-2022
FU National Natural Science Foundation of China [51104080, u1137601];
Personnel Training Foundation of Kunming University of Science and
Technology in China [14118557]
FX Projects (51104080, u1137601) supported by the National Natural Science
Foundation of China; Project (14118557) supported by the Personnel
Training Foundation of Kunming University of Science and Technology in
China
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NR 25
TC 52
Z9 56
U1 1
U2 29
PI AMSTERDAM
SN 1003-6326
EI 2210-3384
PD APR
PY 2014
VL 24
IS 4
BP 1231
EP 1236
DI 10.1016/S1003-6326(14)63183-6
PG 6
GA AL6XJ
UT WOS:000339276700042
DA 2023-12-05
ER
PT J
AU Sakata, K
AF Sakata, Kimiaki
TI Technology for production of austenite type clean stainless steel
LA English
CT 12th ISIJ-VDEh Seminar
CY NOV 21-22, 2005
CL Kitakyushu, JAPAN
DE secondary refining; Si deoxidation; desulfurization; spinel inclusion;
immersion nozzle clogging; magnesia inclusion; alumina inclusion
ID FE-NI; SLAGS; DEOXIDATION; ALUMINUM
AB We established the refining technology for cleanliness in regard to austenite
type stainless steel. But immersion nozzle clogging in continuous casting occurred
by formation of spinel (MgO-Al2O3) type inclusions in strong reduction refining for
cleanliness. Therefore, we estimated the conditions for formation of spinel and it
was possible to improve the castability while keeping cleanliness by controlling of
inclusion compositions.
C1 Aichi Steel Co Ltd, Specialty Steel Engn Dept, Prod Engn Div 1, Tokai, Aichi
4768666, Japan.
RP Sakata, K (corresponding author), Aichi Steel Co Ltd, Specialty Steel Engn Dept,
Prod Engn Div 1, 1 Wanowari,Arao Machi, Tokai, Aichi 4768666, Japan.
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NR 16
TC 52
Z9 58
U1 2
U2 14
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2006
VL 46
IS 12
BP 1795
EP 1799
PG 5
GA 121TL
UT WOS:000243179800011
OA gold
DA 2023-12-05
ER
PT J
AU Rhamdhani, MA
Brooks, GA
Coley, KS
AF Rhamdhani, MA
Brooks, GA
Coley, KS
TI Kinetics of metal/slag reactions during spontaneous emulsification
LA English
DT Article
ID INTERFACIAL PHENOMENA; SLAG; LIQUID; IRON; GAS
AB An approach for accommodating the interfacial area changes in kinetic equations
for heterogeneous reactions in the presence of spontaneous emulsification has been
proposed. The kinetics were analyzed by incorporating time-averaged interfacial
areas in the rate equations. The approach was found to be applicable for the
experimental data and to satisfactorily describe the reaction kinetics. In the case
of a high-temperature reaction between 2.35 g Fe-5 wt pct Al alloy metal droplets
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first-order relationship with respect to aluminum in the metal, and it was
concluded that they were controlled by mass transport in the metal phase. The
calculated metal mass-transfer coefficient k(m) was 1.7 x 10(-6) m/s.
C1 McMaster Univ, Dept Mat Sci & Engn, Hamilton, ON L8S 4L7, Canada.
CSIRO Minerals, Clayton, Vic 3169, Australia.
C3 McMaster University; Commonwealth Scientific & Industrial Research
Organisation (CSIRO)
RP Rhamdhani, MA (corresponding author), McMaster Univ, Dept Mat Sci & Engn,
Hamilton, ON L8S 4L7, Canada.
EM rhamdhma@mcmaster.ca
RI Rhamdhani, Muhammad Akbar/ACM-2274-2022
OI Rhamdhani, Muhammad Akbar/0000-0002-9457-3808; Brooks,
Geoffrey/0000-0002-8499-780X
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NR 20
TC 52
Z9 55
U1 0
U2 12
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD APR
PY 2005
VL 36
IS 2
BP 219
EP 227
DI 10.1007/s11663-005-0023-2
PG 9
Engineering
GA 911XV
UT WOS:000228041000007
DA 2023-12-05
ER
PT J
AU Ünlü, N
Drouet, MG
AF Ünlü, N
Drouet, MG
TI Comparison of salt-free aluminum dross treatment processes
LA English
DT Article
DE Dross recycling; aluminum; salt-free dross processing; alcan plasma
torch process; Droscar process; alurec process; ecocent process;
Drosrite process
AB Dross is an unavoidable by-product of the aluminum production. It forms at the
surface of the molten metal as the latter reacts with the furnace atmosphere.
Depending on the process, it contains, on average, about 50% free aluminum metal
dispersed in an oxide layer. Since the aluminum production is highly energy-
intensive, dross recycling is very attractive from both the energy and the economic
standpoints. The conventional recycling process using salt rotary furnaces is
thermally inefficient and environmentally non-acceptable because of the production
of salt slags. Several salt-free dross treatment processes have been proposed in
the last few years, their operation, energy consumption and metal yield will be
described in detail and compared in the present paper. (C) 2002 Elsevier Science
C1 Istanbul Tech Univ, Fac Chem Met, Dept Met Engn & Mat Sci, TR-80626 Istanbul,
Turkey.
C3 Istanbul Technical University
RP Ünlü, N (corresponding author), Univ Virginia, Dept Mat Sci & Engn, 116
Engineers Way, Charlottesville, VA 22904 USA.
RI Ünlü, Necip/A-5830-2016
OI Ünlü, Necip/0000-0001-5850-6272
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NR 10
TC 52
Z9 61
U1 4
U2 48
PI AMSTERDAM
SN 0921-3449
PD JUL
PY 2002
VL 36
IS 1
BP 61
EP 72
AR PII S0921-3449(02)00010-1
DI 10.1016/S0921-3449(02)00010-1
PG 12
GA 593KW
UT WOS:000177991300004
DA 2023-12-05
ER
PT J
AU Ismail, N
El-Hassan, H
AF Ismail, Najif
El-Hassan, Hilal
TI Development and Characterization of Fly Ash-Slag Blended Geopolymer
Mortar and Lightweight Concrete
LA English
DT Article
DE Dune sand; Rheological; Mechanical; Lightweight; Geopolymer;
Microstructure
ID MECHANICAL-PROPERTIES; STRENGTH PROPERTIES; THERMAL-BEHAVIOR; PART I;
CEMENT; WORKABILITY; TEMPERATURE; HYDRATION; OPTIMIZATION; PERFORMANCE
AB A synopsis of an experimental program on the development of a sustainable fly
ash-slag blended geopolymer mortar (GPM) and lightweight geopolymer concrete (LGPC)
is presented. Geopolymer mortar mixes were prepared incorporating industrial by-
products and sustainable desert dune sand to study the effect of different mixing
variables, including binding materials, curing temperature, and alkaline activator
solution composition and content, on the rheological and mechanical performance.
Optimum mix designs were then formulated into producing LGPC samples with different
binding materials and curing temperature. Lightweight geopolymer concrete specimens
exhibited a brittle behavior with a weakened structure due to low-strength
lightweight aggregates. Lightweight geopolymer concrete made with dune sand and a
fly ash to slag ratio of 3:1 resulted in the highest compressive strength when
cured for 24h at 60 degrees C. Microstructure characterization of LGPC specimens
was also conducted. Scanning electron microscopy and differential scanning
calorimetry showed the coexistence of an aluminosilicate hydrate geopolymer gel and
aluminum-modified C S H gel as the main polymerization reaction products in an
amorphous geopolymeric microstructure.
C1 [Ismail, Najif; El-Hassan, Hilal] United Arab Emirates Univ, Dept Civil &
Environm Engn, POB 15551, Al Ain, U Arab Emirates.
C3 United Arab Emirates University
RP El-Hassan, H (corresponding author), United Arab Emirates Univ, Dept Civil &
EM helhassan@uaeu.ac.ae
RI Hassan, Hilal El/S-4832-2019; Ismail, Najif/G-3754-2011
OI Hassan, Hilal El/0000-0001-9349-350X; Ismail, Najif/0000-0003-1671-529X
FU United Arab Emirates University (UAEU) [31N249, 31N241]
FX Financial support for this study was provided by the United Arab
Emirates University (UAEU) under Grants 31N249 and 31N241. Participation
of students and assistance of laboratory staff at UAEU is gratefully
acknowledged. Ashtech International supplied the fly ash and Emirates
Cement Factory provided the ground-granulated blast-furnace slag used in
the study.
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NR 57
TC 51
Z9 52
U1 3
U2 84
PI RESTON
SN 0899-1561
EI 1943-5533
PD APR
PY 2018
VL 30
IS 4
AR 04018029
DI 10.1061/(ASCE)MT.1943-5533.0002209
PG 14
GA FW8YM
UT WOS:000425622900010
DA 2023-12-05
ER
PT J
AU Guo, XY
Liu, JX
Qin, H
Liu, Y
Tian, QH
Li, D
AF Guo, Xueyi
Liu, Jingxin
Qin, Hong
Liu, Yang
Tian, Qinghua
Li, Dong
TI Recovery of metal values from waste printed circuit boards using an
alkali fusion-leaching-separation process
SO HYDROMETALLURGY
LA English
DT Article
DE Waste printed circuit boards; Alkali fusion process; Copper; Amphoteric
metals
ID PRECIOUS METALS; COPPER CATHODE; TITANIUM; END; PYROLYSIS; STABILITY;
VANADIUM; SCRAP; GOLD; SLAG
AB An efficient alkali fusion-leaching-separation process is developed to recover
metals in crushed metal enrichment (CME) which originated from waste printed
circuit boards (PCBs). Impacts of fusion parameters on metals conversions were
systematically investigated. In the fusion-leaching process, amphoteric metals such
as tin, lead, zinc and aluminum in the CME were leached out, while leaving copper
and precious metals in the residue. Subsequently, metals in solution were further
extracted via precipitation processes, and metals in the residue were recovered
using an add leaching-electrowinning process. Cathode copper, nano-Cu2O,
CaSnO3/CaSn(OH)(6) crystal and mixture of PbS-ZnS were obtained as the final
products of this process. By optimizing the experimental conditions, recoveries of
98.66% for Cu, 91.08% for Sn, 91.25% for Zn, 78.78% for Pb were achieved,
respectively. And all precious metals were enriched in the final residue with
grades of Au 613 g/t, and Ag 2157 g/t. (C) 2015 Elsevier B.V. All rights reserved.
C1 [Guo, Xueyi; Liu, Jingxin; Qin, Hong; Liu, Yang; Tian, Qinghua; Li, Dong] Cent S
Univ, Sch Met & Environm, Changsha 410083, Hunan, Peoples R China.
[Guo, Xueyi; Tian, Qinghua; Li, Dong] Nonferrous Met Ind China, Cleaner Met Engn
Res Ctr, Changsha 410083, Hunan, Peoples R China.
RP Guo, XY (corresponding author), Cent S Univ, Sch Met & Environm, Changsha
EM xyguo@csu.edu.cn
OI Liu, Jingxin/0000-0001-6882-2228; Guo, Xueyi/0000-0003-0660-3024
International Cooperation program of Ministry of Science & Technology of
China [2014DFA90520]
FX The work presented in this paper is supported by the National Natural
Science Foundation of China (Project No.51074190 and No.51234009), the
International Cooperation program of Ministry of Science & Technology of
China (Project No.2014DFA90520).
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NR 40
TC 51
Z9 56
U1 3
U2 77
PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD JUL
PY 2015
VL 156
BP 199
EP 205
DI 10.1016/j.hydromet.2015.06.011
PG 7
GA CR5RE
UT WOS:000361400800026
DA 2023-12-05
ER
PT J
AU CHO, SW
SUITO, H
AF CHO, SW
SUITO, H
TI ASSESSMENT OF ALUMINUM OXYGEN EQUILIBRIUM IN LIQUID-IRON AND ACTIVITIES
IN CAO-AL2O3-SIO2 SLAGS
LA English
DT Article
DE SLAG METAL EQUILIBRIUM; ACTIVITY; DEOXIDATION; DISTRIBUTION RATIO;
CAO-AL2O3-SIO2 SLAG; NITROGEN; SULFUR
ID GALVANIC CELLS; MELTS; SYSTEM; NITROGEN; CAO-SIO2
AB The equilibrium constant K(Al) for the reaction: 2Al+30=Al2O3(s) and the first-
order interaction parameter e(Al)O were estimated at 1 873 K by using the values
for the contents of oxygen, aluminum and other components obtained in slag-metal
equilibrium experiments and those for activity of alumina, along with the
respective interaction parameters. The values for log K(Al) and e(Al)O were found
to be 13.3 +/- 0.59 and -6.83 +/- 0.07, respectively.
Activities of slag components in the CaO-Al2O3-SiO2 system were also evaluated
at 1 873 K from the values for nitride and sulfide capacities coupled with nitrogen
and sulfur distribution ratios. These results were discussed by comparing with
previous values.
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NR 29
TC 51
Z9 51
U1 0
U2 3
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 1994
VL 34
IS 2
BP 177
EP 185
PG 9
GA MX335
UT WOS:A1994MX33500007
OA gold
DA 2023-12-05
ER
PT J
AU Phiri, TC
Singh, P
Nikoloski, AN
AF Phiri, Tina Chanda
Singh, Pritam
Nikoloski, Aleksandar N.
TI The potential for copper slag waste as a resource for a circular
economy: A review-Part II
LA English
DT Review
DE Copper slag waste; Circular economy; Characterisation; Metal recovery;
Utilisation
ID RUDAWY JANOWICKIE MOUNTAINS; HISTORICAL CU-SLAGS; CONVERTER SLAG;
SMELTER SLAG; METAL VALUES; BASE METALS; HYDROMETALLURGICAL RECOVERY;
MECHANICAL-PROPERTIES; ENVIRONMENTAL-IMPACT; FLOTATION TAILINGS
AB Copper slag waste has continued to cause increasing concerns due to the huge
volumes being produced annually worldwide. This paper presents a review of copper
slag as a potential resource for cobalt and copper metals for a circular economy.
An overview of the chemical and mineralogical characterisation of copper slag from
21 major producing countries is discussed. Characterisation is an important
consideration in understanding the nature and environmental behaviour of copper
slag. Copper smelter slags are highly heterogeneous and chemically diverse. The
principal slag constituents are silica, ferrous oxide, ferric oxide, limestone, and
alumina. The slag also contains high concentrations of valuable metals and
metalloids such as copper, cobalt, zinc, calcium, aluminium, silver, magnesium, and
lead. The variation in the chemical and mineralogical composition of copper slag is
mainly influenced by the type of concentrate, type of fluxes, furnace type and
cooling rates during and following the smelting and converting processes.
Furthermore, the various processing strategies for metal recovery, such as
flotation, pyrometallurgy and hydrometallurgy is presented. Finally, utilisation of
the copper slag waste in the concrete industry to promote environmental
sustainability is discussed. This review demonstrates that processing and
repurposing of copper slag waste has benefits of a circular economy such as
increasing critical metal supply, lowering the cost of concrete, and reducing
environmental harm.
C1 [Phiri, Tina Chanda; Singh, Pritam; Nikoloski, Aleksandar N.] Murdoch Univ, Fac
Energy & Engn, 90 South St, Murdoch, WA, Australia.
C3 Murdoch University
RP Nikoloski, AN (corresponding author), Murdoch Univ, Fac Energy & Engn, 90 South
St, Murdoch, WA, Australia.
EM a.nikoloski@murdoch.edu.au
OI Nikoloski, Aleksandar/0000-0002-5267-7262
FU Schlumberger Foundation Faculty for the Future Fellowship
FX The authors would like to thank the Schlumberger Foundation Faculty for
the Future Fellowship for the financial support.
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Z9 51
U1 16
U2 74
PI OXFORD
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD OCT 1
PY 2021
VL 172
AR 107150
DI 10.1016/j.mineng.2021.107150
EA AUG 2021
PG 16
GA US6GU
UT WOS:000697526100008
DA 2023-12-05
ER
PT J
AU Singh, J
Singh, SP
AF Singh, Jagmeet
Singh, S. P.
TI Geopolymerization of solid waste of non-ferrous metallurgy - A review
LA English
DT Review
DE Construction; Geopolymerization; etallurgy; Non-ferrous; Solid waste
ID RED MUD; COPPER SLAG; FLY-ASH; MINE TAILINGS; GEOPOLYMERISATION
KINETICS; MECHANICAL-PROPERTIES; ZINC SLAG; STRENGTH; CEMENT; LEAD
AB The growing demand for non-ferrous metals (Aluminium, Copper, Nickle, Lead and
Zinc) has grown the non-ferrous metallurgical industry, which generate huge amount
of solid waste. Most common method for the disposal of these solid wastes is
dumping at sites, which pollutes the soil and water and covers the useful land.
Geopolymerization technique can be very helpful for the safe disposal of these
solid wastes, which converts the solid wastes into valuable construction materials
such as binders, mortar, bricks, paving blocks and concrete etc. However, to
commercialize the use of these construction products, some key aspects require
detailed examination. Alternative techniques and materials will have to be
identified to increase their reactivity in geopolymerization and in-depth knowledge
of reaction mechanism, mix design, strength and durability characteristics of
resulting geopolymer will have to be studied. The present paper reviews the
important studies on geopolymerization of different solid wastes produced from non-
ferrous industry. The optimum synthesis parameters such as alkali activators,
curing temperature, curing time and molar ratio etc. for the geopolymerization of
these solid wastes are reported and exiting gaps and future trends are also
discussed.
C1 [Singh, Jagmeet; Singh, S. P.] Dr BR Ambedkar Natl Inst Technol, Jalandhar,
Punjab, India.
C3 National Institute of Technology (NIT System); Dr B R Ambedkar National
Institute of Technology Jalandhar
RP Singh, SP (corresponding author), Dr BR Ambedkar Natl Inst Technol, Dept Civil
Engn, Jalandhar 144011, Punjab, India.
EM jagmeet.dhanoa.99@gmail.com; spsingh@nitj.ac.in
RI dhanoa, jagmeet/AAG-7230-2021
OI dhanoa, jagmeet/0000-0002-5326-0223; Singh, S P/0000-0002-0508-7171
FU Ministry of Human Resource Development (MHRD), Government of India
FX The authors acknowledge financial assistance in the form of a fellowship
to the first author from the Ministry of Human Resource Development
(MHRD), Government of India.
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U2 127
PI LONDON
SN 0301-4797
EI 1095-8630
J9 J ENVIRON MANAGE
PD DEC 1
PY 2019
VL 251
AR 109571
DI 10.1016/j.jenvman.2019.109571
PG 12
GA JJ3HM
UT WOS:000494052300024
PM 31546140
DA 2023-12-05
ER
PT J
AU Irbe, L
Beddoe, RE
Heinz, D
AF Irbe, L.
Beddoe, R. E.
Heinz, D.
TI The role of aluminium in C-A-S-H during sulfate attack on concrete
LA English
DT Article
ID HYDRATED PORTLAND CEMENTS; BLAST-FURNACE SLAG; GYPSUM FORMATION; ALKALI
BINDING; AL-27 NMR; ETTRINGITE; SI-29; TEMPERATURE; CHEMISTRY
AB Storage tests with C-A-S-H phases in Na2SO4 solutions (3 and 30 g/L SO4) were
carried out to study changes in the C-A-S-H nanostructure during sulfate attack on
concrete. Particular attention was paid to the availability of aluminium in C-A-S-H
for ettringite formation. Ettringite only formed above the saturation pH of
portlandite. The removal of aluminium from C-A-S-H decreased the Al/Si ratio and
mean chain length (MCL) of the C-A-S-H phases. No ettringite formed in solutions
below the saturation pH of portlandite. Here, decalcification of the C-A-S-H phases
resulted in an increase in MCL. The formation of ettringite from aluminium in C-A-
S-H exposed to Na2SO4 solutions is controlled by the availability of calcium.
Sodium is adsorbed on deprotonated silanol groups in C-A-S-H. At 3 g/L SO4, the
SO42- ions are adsorbed with calcium on deprotonated silanol groups, but at 30 g/L
SO4, they are also bonded to other sites in C-A-S-H.
C1 [Irbe, L.; Beddoe, R. E.; Heinz, D.] Tech Univ Munich, Ctr Bldg Mat, Baumbachstr
7, D-81245 Munich, Germany.
C3 Technical University of Munich
RP Irbe, L (corresponding author), Tech Univ Munich, Ctr Bldg Mat, Baumbachstr 7,
D-81245 Munich, Germany.
EM linda.irbe@tum.de
FU German Research Foundation (DFG)
FX The authors thank the German Research Foundation (DFG) for financially
supporting this work. Special thanks are due to Dr. E. Griesshaber from
the Department of Earth and Environmental Sciences and GeoBioCenter,
Ludwig-Maximilians-Universitat Munchen for SEM measurements.
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TC 50
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U1 9
U2 103
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD FEB
PY 2019
VL 116
BP 71
EP 80
DI 10.1016/j.cemconres.2018.11.012
PG 10
GA HK1LX
UT WOS:000457667500010
DA 2023-12-05
ER
PT J
AU Shi, ZG
Shi, CJ
Wan, S
Ou, ZH
AF Shi, Zhenguo
Shi, Caijun
Wan, Shu
Ou, Zhihua
TI Effect of alkali dosage on alkali-silica reaction in sodium hydroxide
activated slag mortars
LA English
DT Article
DE Alkali-silica reaction; Alkali-activated slag; Alkali activator;
Compressive strength; Pore structure
ID BLAST-FURNACE SLAG; AGGREGATE REACTION; HYDRATION PRODUCTS; AMORPHOUS
SILICA; PORTLAND-CEMENT; CONCRETE; STRENGTH; CALCIUM; ASR; DISSOLUTION
AB Alkali-silica reaction (ASR) is one of the durability factors limiting the
commercial use of alkali-activated slag (MS) concrete. The effect of alkali dosage
is of great importance and barely studied for ASR in AAS system. This study
investigates the effect of alkali dosage on ASR in sodium hydroxide (NaOH)
activated slag mortars. In addition to ASR expansion, the changes in sample weight,
compressive strength, pore structure, and pore solution chemistry are also
investigated for better understanding the factors controlling the ASR in AAS
mortars. The present study shows that the pore solution alkalinity increases with
increasing the alkali dosage of the activator. However, the ASR expansion decreases
with increasing the alkali dosage. The SEM/EDX results show no significant
difference in both morphology and chemical composition of the ASR products. The
lower ASR expansion at higher alkali dosage may be attributed to the relatively
higher concentration of aluminum in the pore solution due to higher degree of slag
hydration, which is expected to mitigate the dissolution of silica from the
reactive aggregate. (C) 2017 Elsevier Ltd. All rights reserved.
C1 [Shi, Zhenguo; Shi, Caijun; Wan, Shu] Hunan Univ, Coll Civil Engn, Changsha
[Shi, Zhenguo] Univ Aarhus, Interdisciplintay Nanosci Ctr iNANO, DK-8000 Aarhus
C, Denmark.
[Shi, Zhenguo] Univ Aarhus, Dept Chem, DK-8000 Aarhus C, Denmark.
[Ou, Zhihua] Hunan Univ Technol, Sch Civil Engn, Zhuzhou 412007, Peoples R
China.
C3 Hunan University; Aarhus University; Aarhus University; Hunan University
of Technology
RP Shi, CJ (corresponding author), Hunan Univ, Coll Civil Engn, Changsha 410082,
EM zshi@chem.au.dk; cshi@hnu.edu.cn
RI Shi, Zhenguo/E-4894-2018
OI Shi, Zhenguo/0000-0003-0000-6560
FU National Natural Science Foundation of China [51638008, 51461135001]
FX The financial supports from the National Natural Science Foundation of
China under contract Nos. 51638008 and 51461135001 are gratefully
acknowledged.
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NR 38
TC 50
Z9 54
U1 5
U2 72
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUL 15
PY 2017
VL 143
BP 16
EP 23
DI 10.1016/j.conbuildmat.2017.03.125
PG 8
GA EU4ZW
UT WOS:000401042400002
DA 2023-12-05
ER
PT J
AU Schöler, A
Winnefeld, F
Ben Haha, M
Lothenbach, B
AF Schoeler, Axel
Winnefeld, Frank
Ben Haha, Mohsen
Lothenbach, Barbara
TI The effect of glass composition on the reactivity of synthetic glasses
LA English
DT Article
DE blended cements; degree of reaction; glass dissolution; kinetics;
supplementary cementitious materials
ID BLAST-FURNACE SLAG; SUPPLEMENTARY CEMENTITIOUS MATERIALS; SILICEOUS
FLY-ASH; PORTLAND-CEMENT; PHYSICAL-PROPERTIES; LIMESTONE POWDER;
HYDRATION; CALCIUM; BLENDS; QUANTIFICATION
AB The reactivity of synthetic glasses depends on their chemical compositions. In
far from equilibrium dissolution experiments, the reactivity of Ca-rich glasses
with compositions similar to blast-furnace slag is found to be much higher (up to
similar to 60wt.% after 7days) compared to Si-rich glasses with compositions
similar to type F fly ash (up to similar to 20wt.% after 7days). Isothermal
calorimetry and TGA experiments conducted on model systems containing portlandite
and calcite and on glass-blended Portland cement confirmed the higher reactivity of
the Ca-rich glasses. The degree of glass reaction after 91days ranged from 7 to
20wt.%. The results showed also a higher reactivity of the glasses containing more
aluminum (both for Ca-rich and Si-rich glasses) indicating that not only calcium
but also aluminum acted rather as network modifier than as network former. The
results confirm a strong dependence of the glass reactivity on the degree of
polymerization of the glass network.
C1 [Schoeler, Axel; Winnefeld, Frank; Lothenbach, Barbara] Empa, Swiss Fed Labs Mat
Sci & Technol, Lab Concrete & Construct Chem, Dubendorf, Switzerland.
[Ben Haha, Mohsen] HeidelbergCement Technol Ctr GmbH, Leimen, Germany.
RP Schöler, A (corresponding author), Empa, Swiss Fed Labs Mat Sci & Technol, Lab
Concrete & Construct Chem, Dubendorf, Switzerland.
EM axel.schoeler@freenet.de
RI Winnefeld, Frank/B-5335-2009; Lothenbach, Barbara/C-6275-2013; Ben Haha,
Mohsen/AAC-4859-2020
Barbara/0000-0002-9020-6488; Ben Haha, Mohsen/0000-0001-7570-326X;
Scholer, Axel/0000-0002-2463-0926
FU HeidelbergCement
FX HeidelbergCement
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NR 56
TC 50
Z9 51
U1 1
U2 34
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD JUN
PY 2017
VL 100
IS 6
BP 2553
EP 2567
DI 10.1111/jace.14759
PG 15
GA EW6HR
UT WOS:000402610900028
DA 2023-12-05
ER
PT J
AU Yao, XL
Wang, WL
Liu, M
Yao, YG
Wu, S
AF Yao, Xingliang
Wang, Wenlong
Liu, Min
Yao, Yonggang
Wu, Shuang
TI Synergistic use of industrial solid waste mixtures to prepare
ready-to-use lightweight porous concrete
LA English
DT Review
DE Ready-to-use lightweight porous concrete; Industrial solid wastes;
Synergistic effect; High early compressive strength; Life cycle
assessment
ID AUTOCLAVED AERATED CONCRETE; FOAMED CONCRETE; HYDRATION; BUILDINGS;
STRENGTH; ENERGY; CEMENT; GYPSUM; ASH
AB Lightweight porous concrete is a popular energy-saving building material.
However, the raw materials required to prepare this concrete paste are extracted
from natural resources, and its early compressive strength is so low that it cannot
be used for applications with a short casting time. In order to improve the early
compressive strength and reduce energy and resource consumption during preparation,
this study proposes using only solid wastes to prepare the pastes for lightweight
porous concrete that can be ready to use in a short time. This was achieved by
sintering a mixture of aluminum dust, flue-gas desulfurization gypsum, carbide
slag, and red mud to obtain a cementitious material (CM). Then, other solid wastes
(14.26 wt% flue-gas desulfurization gypsum, 9.9 wt% fly ash, and 1 wt% carbide
slag) were blended with the CM to prepare ready-to-use lightweight porous concrete
(RLPC), which was successfully prepared using only industrial solid wastes as the
raw materials. The minimum thermal conductivity obtained was 0.15 W/m.K, and the
maximum 28-d compressive strength obtained was 3.57 MPa for an RLPC dry density of
similar to 600 kg/m(3). In addition, the 4-h and 1-d compressive strengths were up
to 1.31 MPa and 1.57 MPa, respectively, which is even higher than the 28-d
compressive strength of most conventional foamed concretes. Finally, our life cycle
assessment showed that the preparation of RLPC has a lower environmental impact
than that of conventional foamed concrete. (C) 2018 Elsevier Ltd. All rights
reserved.
C1 [Yao, Xingliang; Wang, Wenlong; Yao, Yonggang; Wu, Shuang] Shandong Univ, Natl
Engn Lab Coal Fired Pollutants Emiss Reduct, Jinan 250061, Shandong, Peoples R
China.
[Liu, Min] UCL, Civil Environm & Geomat Engn, London WC1E 6BT, England.
C3 Shandong University; University of London; University College London
RP Wang, WL (corresponding author), Shandong Univ, Natl Engn Lab Coal Fired
Pollutants Emiss Reduct, Jinan 250061, Shandong, Peoples R China.
EM yaoxl1991@163.com; wwenlong@sdu.edu.cn; min.liu.13@ucl.ac.uk;
501779594@qq.com; 1652756099@qq.com
RI wang, wenlong/L-2239-2013; Yao, Xingliang/AAG-2215-2021
OI Yao, Xingliang/0000-0001-5355-905X; Wu, Shuang/0000-0001-9125-8741
FU National Key Research & Development Program of China [2017YFC0703100];
Shandong Provincial Science Fund for Distinguished Young Scholars
[JQ201514]; Natural Science Foundation Major Primary Research Program of
Shandong Province [ZR2017ZC0734]
FX The authors acknowledge the support of the National Key Research &
Development Program of China (No. 2017YFC0703100), the Shandong
Provincial Science Fund for Distinguished Young Scholars (No. JQ201514),
and the Natural Science Foundation Major Primary Research Program of
Shandong Province (No. ZR2017ZC0734).
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10.1016/j.conbuildmat.2015.10.112
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10.1016/j.conbuildmat.2013.03.091
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NR 32
TC 49
Z9 51
U1 12
U2 153
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD FEB 20
PY 2019
VL 211
BP 1034
EP 1043
DI 10.1016/j.jclepro.2018.11.252
PG 10
& Ecology
GA HK4SC
UT WOS:000457952400089
DA 2023-12-05
ER
PT J
AU Hu, JP
Liu, WZ
Wang, L
Liu, Q
Chen, F
Yue, HR
Liang, B
Lü, L
Wang, Y
Zhang, GQ
Li, C
AF Hu, Jinpeng
Liu, Weizao
Wang, Lin
Liu, Qiang
Chen, Fang
Yue, Hairong
Liang, Bin
Lu, Li
Wang, Ye
Zhang, Guoquan
Li, Chun
TI Indirect mineral carbonation of blast furnace slag with
(NH4)2SO4 as a recyclable extractant
SO JOURNAL OF ENERGY CHEMISTRY
LA English
DT Article
DE Blast furnace slag; CO2; Mineral carbonation; CO2 sequestration
ID CO2 SEQUESTRATION; WOLLASTONITE CARBONATION; THERMAL-DECOMPOSITION;
AMMONIUM BISULFATE; STEELMAKING SLAGS; MG EXTRACTION; FIXATION;
DISSOLUTION; SERPENTINE; SULFATE
AB Large quantities of CO2 and blast furnace slag are discharged in the iron and
steel industry. Mineral carbonation of blast furnace slag can offer substantial CO2
emission reduction and comprehensive utilisation of the solid waste. In this study,
a recyclable extractant, (NH4)(2)SO4, was used to extract calcium and magnesium
from blast furnace slag (main phases of gehlenite and akermanite) by using low-
temperature roasting to fix CO2 through aqueous carbonation. The process parameters
and efficiency of the roasting extraction, mineralisation, and Al recovery were
investigated in detail. The results showed that the extractions of Ca, Mg, and Al
can reach almost 100% at an (NH4)(2)SO4-to-slag mass ratio of 3: 1 and at 370
degrees C in 1 h. Adjusting the pH value of the leaching solution of the roasted
slag to 5.5 with the NH3 released during the roasting resulted in 99% Al
precipitation, while co-precipitation of Mg was lower than 2%. The Mg-rich leachate
after the depletion of Al and the leaching residue (main phases of CaSO4 and SiO2)
were carbonated using (NH4)(2)CO3 and NH4HCO3 solutions, respectively, under mild
conditions. Approximately 99% of Ca and 89% of Mg in the blast furnace slag were
converted into CaCO3 and (NH4)(2)Mg(CO3)(2)center dot 4H(2)O, respectively. The
latter can be selectively decomposed to magnesium carbonate at 10 0-20 0 degrees C
to recover the NH3 for reuse. In the present route, the total CO2 sequestration
capacity per tonne of blast furnace slag reached up to 316 kg, and 313 kg of Al-
rich precipitate, 10 0 0 kg of carbonated product containing CaCO3 and SiO2, and
304 kg of carbonated product containing calcium carbonate and magnesium carbonate
were recovered simultaneously. These products can be used, respectively, as raw
materials for the production of electrolytic aluminium, cement, and light magnesium
carbonate to replace natural resources. (C) 2017 Science Press and Dalian Institute
of Chemical Physics, Chinese Academy of Sciences. Published by Elsevier B.V. and
Science Press. All rights reserved.
C1 [Hu, Jinpeng; Liu, Weizao; Wang, Lin; Liu, Qiang; Chen, Fang; Yue, Hairong;
Liang, Bin; Lu, Li; Wang, Ye; Zhang, Guoquan; Li, Chun] Sichuan Univ, Coll Chem
Engn, Chengdu 610065, Sichuan, Peoples R China.
C3 Sichuan University
RP Li, C (corresponding author), Sichuan Univ, Coll Chem Engn, Chengdu 610065,
EM lic@scu.edu.cn
RI yue, Hairong/D-1874-2013; Liu, Weizao/K-5038-2019; Liang,
Bin/JHU-0581-2023
OI Liu, Weizao/0000-0003-0976-2864;
FU National Key R&D Program of China [2016YFB0600904]
FX The authors are grateful for the financial support of the National Key
R&D Program of China (2016YFB0600904).
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NR 31
TC 49
Z9 53
U1 9
U2 81
PI AMSTERDAM
SN 2095-4956
J9 J ENERGY CHEM
JI J. Energy Chem.
PD SEP
PY 2017
VL 26
IS 5
BP 927
EP 935
DI 10.1016/j.jechem.2017.06.009
PG 9
WC Chemistry, Applied; Chemistry, Physical; Energy & Fuels; Engineering,
Chemical
GA FM9NV
UT WOS:000415598900012
DA 2023-12-05
ER
PT J
AU Segui, P
Aubert, JE
Husson, B
Measson, M
AF Segui, P.
Aubert, J. E.
Husson, B.
Measson, M.
TI Characterization of wastepaper sludge ash for its valorization as a
component of hydraulic binders
LA English
DT Article
DE Wastepaper sludge ash; Characterization; Valorization; Hydraulic binder
ID MSWI FLY-ASH; BLENDED CEMENT; PAPER; STRENGTH; BEHAVIOR; PULP; SLAG
AB This paper deals with the physical, chemical and mineralogical characterization
of WSA in order to evaluate the interest of its potential reuse as a component in
hydraulic binders. The results show that WSA contains hydraulic minerals such as
lime (CaO), mayenite (Ca12Al14O33) and alpha'-Ca2SiO4 in addition to gehlenite, the
main mineral. WSA can also be considered as a hydraulic mineral admixture, which is
very encouraging for the potential reuse of this material in hydraulic binders.
However, WSA has some characteristics that could be worrying for its reuse.
Firstly, SEM observations show that its particles are very porous, and that could
lead to problems of workability of cement-based materials containing WSA. Secondly,
the presence of both lime and metallic aluminium could be responsible for swelling
when WSA is introduced into cement-based materials. No swelling was observed
visually during the hydration of WSA-containing paste in this study but this first
qualitative test is not sufficient and further investigations of this specific
characteristic will be necessary. Finally, the presence of lime in the WSA could be
considered as a problem for its use in binder for construction (risk of expansion)
but, from another point of view, it would be very interesting for applications in
road works, especially for the stabilization of soil, in which lime is regularly
employed because it has useful properties (drying and reinforcement of the
mechanical strength of the soils). (C) 2012 Elsevier B.V. All rights reserved.
C1 [Segui, P.; Aubert, J. E.; Husson, B.] Univ Toulouse, UPS, INSA, LMDC, F-31077
Toulouse, France.
[Segui, P.; Measson, M.] Eiffage Travaux Publ Rech & Dev, F-69960 Corbas,
France.
Toulouse; Institut National des Sciences Appliquees de Toulouse;
Universite Toulouse III - Paul Sabatier
RP Aubert, JE (corresponding author), Univ Toulouse, UPS, INSA, LMDC, 135 Ave
Rangueil, F-31077 Toulouse, France.
EM jean-emmanuel.aubert@univ-tlse3.fr
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10.1016/j.cemconcomp.2005.10.007
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10.1016/j.cemconres.2009.07.001
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NR 28
TC 49
Z9 50
U1 0
U2 27
PU ELSEVIER
PI AMSTERDAM
SN 0169-1317
EI 1872-9053
J9 APPL CLAY SCI
JI Appl. Clay Sci.
PD MAR
PY 2012
VL 57
BP 79
EP 85
DI 10.1016/j.clay.2012.01.007
PG 7
GA 911AI
UT WOS:000301689300011
DA 2023-12-05
ER
PT J
AU Pereira, DA
Aguiar, J
Castro, F
Almeida, MF
Labrincha, JA
AF Pereira, DA
Aguiar, J
Castro, F
Almeida, MF
Labrincha, JA
TI Mechanical behaviour of Portland cement mortars with incorporation of
Al-containing salt slags
LA English
DT Article
DE waste management; mortar; Portland cement; salt slag; mechanical
properties
AB Recovery of a salt cake slag produced from aluminum scrap re-melted in rotary
furnaces, at the lowest cost, while complying with all environmental laws is the
main objective of this study. The characterisation of the slag residue involved
determinations of the water leaching conditions, toxicological analysis, chemical
analysis of the leaching waste, and mineralogical composition. A two-phase study
was made to determine the effect of waste additions on mechanical properties of
cement mortars, involving partial replacements of either sand or cement. SEM
characterisation of fracture surfaces was also made. Partial substitution of
cement, which is the most expensive component of the mortar, by salt slag has both
environmental and economical advantages. However, only small amounts (up to 10 wt.
%) can be replaced by washed slag without significant damage to mortar
characteristics. Sand substitution by slag is less problematic and 30-50 wt.%
replacement levels are easily achieved. However, the direct economical impact is
less relevant. The incorporation of unwashed slag in impracticable, as a result of
noxious gases released and significant volumetric expansion effects. (C) 2000
C1 Univ Aveiro, Dep Eng Ceram & Vidro, P-3810193 Aveiro, Portugal.
Inst Super Engn, Dep Eng Mecan, P-4200 Oporto, Portugal.
Univ Minho, Dept Civil Engn, P-4810 Guimaraes, Portugal.
Univ Minho, Dept Eng Mecan, P-4810 Guimaraes, Portugal.
Univ Porto, Dept Engn Met, P-4000 Oporto, Portugal.
C3 Universidade de Aveiro; Instituto Politecnico do Porto; Universidade do
Minho; Universidade do Minho; Universidade do Porto
RP Labrincha, JA (corresponding author), Univ Aveiro, Dep Eng Ceram & Vidro, P-
3810193 Aveiro, Portugal.
EM jal@cv.ua.pt
RI Castro, Fernando A.P./H-6642-2015; Labrincha, J./B-3984-2010; Aguiar,
José/B-6597-2009; Almeida, Manuel Fonseca/I-7072-2015
OI Castro, Fernando A.P./0000-0002-6674-3988; Labrincha,
J./0000-0003-4782-1685; Aguiar, José/0000-0003-3954-5721; Almeida,
Manuel Fonseca/0000-0001-9326-7043
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NR 9
TC 49
Z9 50
U1 0
U2 6
PI OXFORD
SN 0008-8846
JI Cem. Concr. Res.
PD JUL
PY 2000
VL 30
IS 7
BP 1131
EP 1138
DI 10.1016/S0008-8846(00)00272-6
PG 8
GA 356KQ
UT WOS:000089442800015
OA Green Published
DA 2023-12-05
ER
PT J
AU Guo, Y
Zhang, TS
Tian, WL
Wei, JX
Yu, QJ
AF Guo, Yiqun
Zhang, Tongsheng
Tian, Wenli
Wei, Jiangxiong
Yu, Qijun
TI Physically and chemically bound chlorides in hydrated cement pastes: a
comparison study of the effects of silica fume and metakaolin
LA English
DT Article
ID C-S-H; BLAST-FURNACE SLAG; PORTLAND-CEMENT; FLY-ASH; BLENDED CEMENTS;
COMPRESSIVE STRENGTH; TRICALCIUM SILICATE; POZZOLANIC REACTION; HARDENED
PASTES; SODIUM-CHLORIDE
AB Increasing the chloride binding capacity of hydration products is an effective
countermeasure to improve the chloride resistance of cement-based materials. The
alumina content of binder is usually adopted to evaluate the chloride binding
capacity, in terms of Friedel's salt. However, the influences of aluminum on the
characteristics of C-S-H and finally on physically bound chloride are not taken
into account. In the present study, the characteristics of hydration products were
widened by introducing silica fume and metakaolin into Portland cement pastes,
respectively; then, the consequent chloride binding capacity was followed using
Freundlich binding isotherms; chemically and physically bound chlorides were
further distinguished. The results show that the chloride binding capacity of
cement pastes reduced with the increase of SF addition, but proportionally
increased with the increasing MK addition. The amount of chemically bound chloride
was doubled by adding 16% MK (15.07mg/g), which was about 6 times as high as that
of cement paste with 16% SF. The chemically bound chloride through formation of
Friedel's salt by ion-exchange mainly related to the monocarboaluminate content,
whereas the physically bound chloride was largely depended on the specific surface
area of cement pastes. Moreover, MK promoted the substitution of Al3+ for Si4+ in
C-S-H, resulting in more sites for chloride binding and then a higher amount of
physically bound chloride. In contrast, SF increased the protonation degree of C-S-
H, leading to a lower positive charge density on the surface of C-S-H and finally a
lower amount of physically bound chloride due to poor electrostatic adsorption.
C1 [Guo, Yiqun; Zhang, Tongsheng; Tian, Wenli; Wei, Jiangxiong; Yu, Qijun] South
China Univ Technol, Sch Mat Sci & Engn, Guangzhou 510640, Guangdong, Peoples R
China.
[Zhang, Tongsheng] UCL, Dept Civil Environm & Geomat Engn, London WC1E 6BT,
England.
[Zhang, Tongsheng; Wei, Jiangxiong; Yu, Qijun] Guangdong Low Carbon Technol &
Engn Ctr Bldg Mat, Guangzhou 510640, Guangdong, Peoples R China.
C3 South China University of Technology; University of London; University
College London
RP Zhang, TS (corresponding author), South China Univ Technol, Sch Mat Sci & Engn,
Guangzhou 510640, Guangdong, Peoples R China.; Zhang, TS (corresponding author),
UCL, Dept Civil Environm & Geomat Engn, London WC1E 6BT, England.; Zhang, TS
(corresponding author), Guangdong Low Carbon Technol & Engn Ctr Bldg Mat, Guangzhou
510640, Guangdong, Peoples R China.
EM mstszhang@scut.edu.cn
RI Guo, Yiqun/AAJ-9370-2020; wei, jiang/GRX-7907-2022
OI Zhang, Tongsheng/0000-0001-5783-2367
FU National Key Research and Development Program [2016YFB0303502];
Guangdong Science and Technology Program [2016A020221009]; Water
Resource Science and Technology Innovation Program of Guangdong Province
[2016-23]; Guangdong Special Support for Youth Science and Technology
Innovation Talents [2015TQ01C312]; Pearl River Science and Technology
Nova Program of Guangzhou [201610010098]
FX This work was funded by the National Key Research and Development
Program (2016YFB0303502), Guangdong Science and Technology Program
(2016A020221009), the Water Resource Science and Technology Innovation
Program of Guangdong Province (2016-23), the Guangdong Special Support
for Youth Science and Technology Innovation Talents (2015TQ01C312), and
the Pearl River Science and Technology Nova Program of Guangzhou
(201610010098). Their financial supports are gratefully acknowledged.
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NR 72
TC 48
Z9 50
U1 4
U2 85
PU SPRINGER
PI NEW YORK
SN 0022-2461
EI 1573-4803
J9 J MATER SCI
JI J. Mater. Sci.
PD FEB
PY 2019
VL 54
IS 3
BP 2152
EP 2169
DI 10.1007/s10853-018-2953-5
PG 18
GA HA1VP
UT WOS:000450016100019
DA 2023-12-05
ER
PT J
AU Guo, XL
Meng, FJ
Shi, HS
AF Guo, Xiaolu
Meng, Fanjie
Shi, Huisheng
TI Microstructure and characterization of hydrothermal synthesis of
Al-substituted tobermorite
LA English
DT Article
DE Tobermorite; Aluminum; Hydrothermal synthesis; Microstructure
ID C-S-H; BLAST-FURNACE SLAG; SI-29 NMR; AL-27; SPECTROSCOPY; ALUMINUM;
SOLIDIFICATION; PHASES; ASH
AB Tobermorite is an important mineral analog of calcium silicate hydrate (C-S-H),
the main phase formed by hydration of Portland cement, due to the structural
similarity. As part of a broader study on the effect of aluminum substitution C-S-
H, the synthesis and characterization of tobermorite with and without aluminum were
conducted. The X-ray diffraction pattern indicated that a suitable synthesis time
for tobermorite with or without aluminum was 5 h in an autoclave at 180 degrees C
and Saturated steam pressure around 1 MPa. In both samples the mineral is 11
angstrom-tobermorite. X-ray fluorescehce showed that the sample with aluminum had a
higher molar ratio of Ca/(Si + Al). Thermogravimetry-differential scanning
calorimetry showed the same general changes, loss of free water at 55 degrees C,
loss of interlayer water at 187 degrees C, dehydroxylation at 664 degrees C, and
conversion to wollastonite at 841 C. With the incorporation of aluminum, 29Si and
27Al magic angle spinning-nuclear magnetic resonance spectra showed aluminum
addition increases the mean chain length, Al mainly occupies Q(2) bridging and Q(3)
branching sites. Scanning electron Micrographs indicated that tobermorite crystals
are larger than those of sample without alumina. This work is beneficial for
understanding the implication of the use of admixtures containing aluminum in
concrete on its micro- and atomic-scale properties. (C) 2016 Published by Elsevier
Ltd.
C1 [Guo, Xiaolu; Shi, Huisheng] Tongji Univ, Minist Educ, Key Lab Adv Civil Engn
Mat, Shanghai 201804, Peoples R China.
[Guo, Xiaolu; Meng, Fanjie; Shi, Huisheng] Tongji Univ, Sch Mat Sci & Engn, 4800
Caoan Rd, Shanghai 201804, Peoples R China.
C3 Tongji University; Tongji University
RP Guo, XL (corresponding author), Tongji Univ, Sch Mat Sci & Engn, 4800 Caoan Rd,
Shanghai 201804, Peoples R China.
EM guoxiaolu@tongji.edu.cn
FU National Natural Science Foundation of China [51478328]; Fundamental
Research Funds for the Central Universities of China [0500219225]
FX The authors acknowledge the financial supports received from the
National Natural Science Foundation of China (No. 51478328), the
Fundamental Research Funds for the Central Universities of China (No.
0500219225). The authors also appreciate the helps from Professor Leslie
J. Struble, Professor Paramita Mondal, and Wiliam A. Hunnicutt in the
Department of Civil and Environmental Engineering, University of
Illinois at Urbana Champaign, USA.
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NR 46
TC 48
Z9 52
U1 5
U2 84
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD FEB 15
PY 2017
VL 133
BP 253
EP 260
DI 10.1016/j.conbuildmat.2016.12.059
PG 8
GA EJ1XC
UT WOS:000393002800027
DA 2023-12-05
ER
PT J
AU Cheng, J
Zhou, F
Xuan, XX
Liu, JZ
Zhou, JH
Cen, KF
AF Cheng, Jun
Zhou, Fan
Xuan, Xiaoxu
Liu, Jianzhong
Zhou, Junhu
Cen, Kefa
TI Comparison of the catalytic effects of eight industrial wastes rich in
Na, Fe, Ca and Al on anthracite coal combustion
SO FUEL
LA English
DT Article
DE Industrial waste; Combustion; Anthracite coal; Catalysis; Ignition
temperature
ID HIGH ASH COAL; THERMOGRAVIMETRIC ANALYSIS; BURNING ADDITIVES;
THERMAL-ANALYSIS; PULVERIZED COAL; GRAPHITE
AB The catalytic effects of eight industrial wastes rich in Na, Fe, Ca and Al on
Jincheng anthracite coal combustion were compared. The thermogravimetric
experiments showed that Na-rich brine sludge (BS) and salt sludge (SS) exhibited
better catalytic effects on coal combustion than Fe-rich iron mud (IM) and steel
residue (SR). However, IM and SR exhibited better catalytic effects than Ca-rich
white lime mud (WLM) and calcium carbide residue (CCR). Among the eight industrial
wastes, Al-rich alumina residue (AR) and aluminium slag (AS) demonstrated the worst
catalytic effects. BS, which contains more Na (mainly in the form of NaCl, which
was equivalent to Na2O with a content of 13.14%) than SS (mainly in the form of
NaCl and Na3Mg(CO3)(2)Cl, which were equivalent to Na2O with a content of 7.64%)
does, reduced the ignition temperature of Jincheng coal from 582 degrees C to 561
degrees C because of the promoted transfer of oxygen to the carbon surface through
the cyclic oxidation and reduction reactions between Na2O and Na2O2. IM, which
contains more Fe (mainly in the form of gamma-Fe2O3, which was equivalent to Fe2O3
with a content of 92.22%) than SR (mainly in the form of Fe2SiO4 and alpha-Fe,
which were equivalent to Fe2O3 with a content of 8.29%) does, reduced the ignition
temperature of Jincheng coal to 569 degrees C as a consequence of the enhanced
transfer of oxygen to the carbon surface through the cyclic oxidation and reduction
reactions between FeO and Fe2O3. (C) 2016 Elsevier Ltd. All rights reserved.
C1 [Cheng, Jun; Zhou, Fan; Xuan, Xiaoxu; Liu, Jianzhong; Zhou, Junhu; Cen, Kefa]
Zhejiang Univ, State Key Lab Clean Energy Utilizat, Hangzhou 310027, Zhejiang,
Peoples R China.
C3 Zhejiang University
RP Cheng, J (corresponding author), Zhejiang Univ, State Key Lab Clean Energy
Utilizat, Hangzhou 310027, Zhejiang, Peoples R China.
EM juncheng@zju.edu.cn
RI Xuan, Xiaoxu/GLV-2493-2022
OI Xuan, Xiaoxu/0000-0002-8818-7134; Zhou, Junhu/0000-0002-5043-2288
FU National Natural Science Foundation of China [51476141]; National Basic
Research Program of China [201203214906]; Zhejiang Provincial Natural
Science Foundation of China [LR14E060002]
FX This work was supported by the National Natural Science Foundation of
China (51476141), the National Basic Research Program of China
(201203214906) and the Zhejiang Provincial Natural Science Foundation of
China (LR14E060002).
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NR 21
TC 48
Z9 51
U1 1
U2 78
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD JAN 1
PY 2017
VL 187
BP 398
EP 402
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PG 5
GA DZ9HY
UT WOS:000386187100043
DA 2023-12-05
ER
PT J
AU Gaurav, M
Ramakrishna, PA
AF Gaurav, M.
Ramakrishna, P. A.
TI Effect of mechanical activation of high specific surface area aluminium
with PTFE on composite solid propellant
SO COMBUSTION AND FLAME
LA English
DT Article
DE PTFE; Aluminium combustion; Solid propellant combustion; Agglomeration;
Thermal conductivity
ID BURNING RATE; THERMAL-CONDUCTIVITY; COMBUSTION
AB This study deals with the mechanical activation of pyral with PTFE. Pyral is a
flake-like aluminium particle with a large specific surface area (similar to 22.5
m(2)/g). This paper, through a variety of tests like the TGA, DSC, particle size
analysis, SEM analysis and other tests tries to establish that this mechanically
activated aluminium is a good replacement for conventional aluminium used in a
solid propellant. Burn rates were also measured at pressures ranging from 10 to 70
bar using a modified Crawford bomb. The burn rates of solid propellants prepared
with this mechanically activated pyral powder were found to be higher than that of
non-activated pyral powder and much higher than that of those reported in
literature with similar mechanically activated aluminium. This has been explained
to be due the large specific surface area of aluminium used in these experiments
which undergo exothermic fluorination reactions with PTFE. Two phase losses and
slag accumulation are the two problems encountered when aluminium is used in
composite solid propellants. Slag accumulation has shown a significant reduction
with the use of this activated powder over non-activated pyral. (C) 2016 The
Combustion Institute. Published by Elsevier Inc. All rights reserved.
C1 [Gaurav, M.; Ramakrishna, P. A.] Indian Inst Technol Madras, Dept Aerosp Engn,
Madras 600036, Tamil Nadu, India.
Technology (IIT) - Madras
RP Gaurav, M (corresponding author), Indian Inst Technol Madras, Dept Aerosp Engn,
Madras 600036, Tamil Nadu, India.
EM gauray.marothiya29@gmail.com
OI Marothiya, Gaurav/0000-0003-4951-6457; Ramakrishna,
P.A./0000-0003-3228-7897
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NR 41
TC 48
Z9 53
U1 2
U2 43
PI NEW YORK
SN 0010-2180
EI 1556-2921
J9 COMBUST FLAME
JI Combust. Flame
PD APR
PY 2016
VL 166
BP 203
EP 215
DI 10.1016/j.combustflame.2016.01.019
PG 13
Engineering, Chemical; Engineering, Mechanical
GA DH4PQ
UT WOS:000372768300019
DA 2023-12-05
ER
PT J
AU Li, CC
Qiao, XC
Yu, JG
AF Li, Chen-chen
Qiao, Xiu-chen
Yu, Jian-guo
TI Large surface area MCM-41 prepared from acid leaching residue of coal
gasification slag
SO MATERIALS LETTERS
LA English
DT Article
DE Coal gasification slag; MCM-41; Silicon; Porous material; Coal fly ash;
Sol-gel preparation
ID MESOPOROUS MATERIALS; SILICA
AB Acid leaching residue of coal gasification slag (ALR-CGS) is a by-product of the
aluminum extraction process of CGS. Its amount increased with the industrialization
of the CGS aluminum extraction process. Thanks to the high silica content of ALR-
CGS, this research evaluated the synthesis of MCM-41 using this discarded material.
Highly ordered MCM-41 with hexagonal shaped pore diameters of 2.91-3.65 nm was
synthesized using ALR-CGS following a non-hydrothermal sol-gel method. The
synthesized sample had a BET specific surface area of 1347 m(2)/g. ALR-CGS is a
very competitive alternative silica source in the synthesis of MCM-41. (C) 2016
Elsevier B.V. All rights reserved.
C1 [Li, Chen-chen; Qiao, Xiu-chen] E China Univ Sci & Technol, Sch Resource &
Environm Engn, 130 Meilong Rd, Shanghai 200237, Peoples R China.
[Yu, Jian-guo] E China Univ Sci & Technol, State Key Lab Chem Engn, Meilong Rd
130, Shanghai 200237, Peoples R China.
C3 East China University of Science & Technology; East China University of
Science & Technology
RP Qiao, XC (corresponding author), E China Univ Sci & Technol, Sch Resource &
Environm Engn, 130 Meilong Rd, Shanghai 200237, Peoples R China.
EM xiuchenqiao@ecust.edu.cn
FU National High Technology Research and Development Program (863 Program)
[2011AA06A102]; National Natural Science Foundation of China [21176082];
Specialized Research Fund for the Doctoral Program of Higher Education
[20110074110002]
FX This work was funded by the National High Technology Research and
Development Program (863 Program) (2011AA06A102), the National Natural
Science Foundation of China (21176082) and the Specialized Research Fund
for the Doctoral Program of Higher Education (20110074110002).
CR Adjdir M, 2009, APPL CLAY SCI, V46, P185, DOI 10.1016/j.clay.2008.11.009
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NR 13
TC 48
Z9 52
U1 7
U2 149
PI AMSTERDAM
SN 0167-577X
EI 1873-4979
J9 MATER LETT
JI Mater. Lett.
PD MAR 15
PY 2016
VL 167
BP 246
EP 249
DI 10.1016/j.matlet.2015.12.125
PG 4
WC Materials Science, Multidisciplinary; Physics, Applied
SC Materials Science; Physics
GA DC8SW
UT WOS:000369491000063
DA 2023-12-05
ER
PT J
AU Chen, DS
Zhao, LS
Qi, T
Hu, GP
Zhao, HX
Li, J
Wang, LN
AF Chen, De-sheng
Zhao, Long-sheng
Qi, Tao
Hu, Guo-ping
Zhao, Hong-xin
Li, Jie
Wang, Li-na
TI Desilication from titanium-vanadium slag by alkaline leaching
LA English
DT Article
DE desilication; titanium-vanadium slag; alkaline leaching; kinetics
ID RECOVERY
AB A hydrometallurgical process for the selective removal of silicon from titanium-
vanadium slag by alkaline leaching was investigated. X-ray diffraction, scanning
electron microscopy and electron dispersive spectroscopy were used to characterize
the samples. The results show that anosovite, pyroxene and metallic iron are the
major components of the titanium-vanadium slag. Anosovite is presented in granular
and plate shapes, and pyroxene is distributed in the anosovite crystals. Metallic
iron is spheroidal and wrapped in anosovite. Silicon is mainly in the pyroxene, and
titanium and vanadium are mainly in the anosovite. The effects of agitation speed,
leaching temperature, leaching time, sodium hydroxide concentration and liquid-
solid (L/S) mass ratio on the leaching behavior of silica from titanium-vanadium
slag were investigated. The leaching temperature and L/S mass ratio played
considerable role in the desilication process. Under the optimal conditions, 88.2%
silicon, 66.3% aluminum, 27.3% manganese, and only 1.2% vanadium were leached out.
The desilication kinetics of the titanium-vanadium slag was described by the
chemical control model. The apparent activation energy of the desilication process
was found to be 46.3 kJ/mol.
C1 [Chen, De-sheng; Zhao, Long-sheng; Qi, Tao; Hu, Guo-ping; Zhao, Hong-xin; Li,
Jie; Wang, Li-na] Chinese Acad Sci, Inst Proc Engn, Natl Engn Lab Hydromet Cleaner
Prod Technol, Beijing 100190, Peoples R China.
[Chen, De-sheng; Zhao, Long-sheng; Qi, Tao; Hu, Guo-ping; Zhao, Hong-xin; Li,
Jie; Wang, Li-na] Chinese Acad Sci, Inst Proc Engn, Key Lab Green Proc & Engn,
C3 Institute of Process Engineering, CAS; Chinese Academy of Sciences;
Chinese Academy of Sciences; Institute of Process Engineering, CAS
RP Wang, LN (corresponding author), Chinese Acad Sci, Inst Proc Engn, Natl Engn Lab
Hydromet Cleaner Prod Technol, Beijing 100190, Peoples R China.
EM linawang@home.ipe.ac.cn
RI Hu, Guoping/L-4423-2019; Wang, Jin/GYA-2019-2022; Wang,
Liangshi/Q-8323-2017
OI Hu, Guoping/0000-0002-7480-8411; Wang, Liangshi/0000-0003-4432-0842
FU Major Program of the National Natural Science Foundation of China
[51090380]; National Science Foundation for Distinguished Young Scholars
of China [51125018]; National Natural Science Foundation of China
[51374191, 51104139, 21006115]
FX Foundation item: Project (51090380) supported by the Major Program of
the National Natural Science Foundation of China; Project (51125018)
supported by the National Science Foundation for Distinguished Young
Scholars of China; Projects (51374191, 51104139, 21006115) supported by
the National Natural Science Foundation of China
CR Chen DS, 2011, MINER ENG, V24, P864, DOI 10.1016/j.mineng.2011.03.018
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NR 16
TC 48
Z9 54
U1 3
U2 43
PU ELSEVIER
PI AMSTERDAM
SN 1003-6326
EI 2210-3384
PD OCT
PY 2013
VL 23
IS 10
BP 3076
EP 3082
DI 10.1016/S1003-6326(13)62836-8
PG 7
GA 273WN
UT WOS:000328567100036
DA 2023-12-05
ER
PT J
AU HINO, M
KITAGAWA, S
BANYA, S
AF HINO, M
KITAGAWA, S
BANYA, S
TI SULFIDE CAPACITIES OF CAO-AL2O3-MGO AND CAO-AL2O3-SIO2 SLAGS
LA English
DT Article
DE SULFIDE CAPACITY; SULFUR DISTRIBUTION RATIO; SECONDARY STEELMAKING;
SLAG; PHYSICAL CHEMISTRY
ID S DISTRIBUTION; LIQUID-IRON; SULFUR
AB The sulphide capacities of CaO-Al2O3, CaO-Al2O3-MgO and CaO-Al2O3-SiO2 slags
were studied at 1 823 to 1 923 K to estimate the sulphur distribution ratio between
secondary steelmaking slag and liquid steel.
From the obtained results, it was confirmed that substitution of MgO or SiO2 for
CaO at a given N(Al2O3) decreased the sulphide capacities in both systems of CaO-
Al2O3-MgO and CaO-Al2O3-SiO2. The evaluated maximum values of sulphur distribution
ratio for both slags were higher than 1 000 at 1 873 K on the condition of CaO-
saturation if the dissolved aluminium content in steel was assumed to be 0.01 mass
%.
C1 TOHOKU UNIV,GRAD SCH,SENDAI,MIYAGI 980,JAPAN.
RP HINO, M (corresponding author), TOHOKU UNIV,FAC ENGN,AOBA KU,SENDAI,MIYAGI
980,JAPAN.
[Anonymous], 1988, STEELMAKING DATA SOU
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NR 23
TC 48
Z9 50
U1 0
U2 3
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 1993
VL 33
IS 1
BP 36
EP 42
PG 7
GA KH294
UT WOS:A1993KH29400006
OA gold
DA 2023-12-05
ER
PT J
AU Shen, DJ
Liu, KG
Wen, CY
Shen, YQ
Jiang, GQ
AF Shen, Dejian
Liu, Kaigi
Wen, Chuyuan
Shen, Yongqiang
Jiang, Guoqing
TI Early-age cracking resistance of ground granulated blast furnace slag
concrete
LA English
DT Article
DE High-performance concrete; Ground granulate blast furnace slag; Cracking
resistance; Residual stress; Stress relaxation; Stress rate
ID HIGH-PERFORMANCE CONCRETE; RESIDUAL-STRESS DEVELOPMENT; SUPER ABSORBENT
POLYMERS; HIGH-STRENGTH CONCRETE; SHRINKAGE CRACKING; AUTOGENOUS
SHRINKAGE; RESTRAINED CONCRETE; COMPRESSIVE STRENGTH; CURING
TEMPERATURE; MINERAL ADMIXTURES
AB High-performance concrete (HPC) generally experiences rather high autogenous
shrinkage. If restrained, residual tensile stress will be induced which may be
sufficient to cause cracking. Ground granulated blast furnace slag (GGBFS) has been
utilized as a mineral admixture to reduce shrinkage cracking in HPC. The restrained
shrinkage cracking of concrete containing GGBFS appears to be less than that of
concrete without slag. However, the data is limited, and the effect of the GGBFS on
the restrained cracking resistance needs to be further investigated. Restrained
ring tests on cracking resistance of HPC using GGBFS as 0%, 20%, 35%, and 50% by
weight replacements of cement were performed. Four concrete mixtures with the same
w/b ratio of 0.32 were placed in a 23 +/- 1 degrees C, 60 +/- 5% RH environment,
and covered with vinyl and aluminum adhesive tape. The outer rings were removed at
24 h after casting to allow water evaporation through the height of the specimen.
Test results showed that: (1) the residual tensile stress at the age of 14.25 days
after casting decreased by 18.6%, 33.2%, and 40.9% when the amount of GGBFS
increased from 0% to 20%, 35%, and 50%, respectively; (2) the stress rate decreased
by 58.9%, 62.5%, and 66.8% when the amount of GGBFS increased from 0% to 20%, 35%,
and 50%, respectively, indicating that the cracking resistance based on stress rate
increased with increasing GGBFS replacement. (C) 2019 Elsevier Ltd. All rights
reserved.
C1 [Shen, Dejian; Liu, Kaigi; Wen, Chuyuan; Shen, Yongqiang] Hohai Univ, Coll Civil
& Transportat Engn, 1 Xikang Rd, Nanjing 210098, Jiangsu, Peoples R China.
[Shen, Dejian; Liu, Kaigi; Wen, Chuyuan; Shen, Yongqiang] Jiangsu Engn Res Ctr
Crack Control Concrete, 1 Xikang Rd, Nanjing 210098, Jiangsu, Peoples R China.
[Shen, Dejian; Liu, Kaigi; Wen, Chuyuan; Shen, Yongqiang; Jiang, Guoqing]
Nanjing Engn Res Ctr Prefabricated Construct, 1 Xikang Rd, Nanjing 210098, Jiangsu,
Peoples R China.
[Jiang, Guoqing] Nanjing Construct Grp CO Ltd, 200 Ruanjian Ave, Nanjing 210012,
C3 Hohai University
RP Shen, DJ (corresponding author), Hohai Univ, Coll Civil & Transportat Engn, 1
Xikang Rd, Nanjing 210098, Jiangsu, Peoples R China.
EM shendjn@163.com
OI Shen, Dejian/0000-0002-0283-6835
FU National Natural Science Foundation of China [51578215]; Qing Lan
Project of Jiangsu Province; Fundamental Research Funds for Central
Universities [2018B664X14]; Postgraduate Research & Practice Innovation
Program of Jiangsu Province [KYCX18_0568]
FX The financial support of the National Natural Science Foundation of
China (Grant No. 51578215) is gratefully acknowledged. This work is also
sponsored by Qing Lan Project of Jiangsu Province. The support of the
Fundamental Research Funds for Central Universities (Grant No.
2018B664X14) is also gratefully acknowledged. The Postgraduate Research
& Practice Innovation Program of Jiangsu Province (Grant No.
KYCX18_0568) is also gratefully acknowledged.
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NR 78
TC 47
Z9 47
U1 4
U2 34
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 20
PY 2019
VL 222
BP 278
EP 287
DI 10.1016/j.conbuildmat.2019.06.028
PG 10
GA IU3BS
UT WOS:000483454300025
DA 2023-12-05
ER
PT J
AU Whittaker, M
Zajac, M
Ben Haha, M
Black, L
AF Whittaker, Mark
Zajac, Maciej
Ben Haha, Mohsen
Black, Leon
TI The impact of alumina availability on sulfate resistance of slag
composite cements
LA English
DT Article
DE Sulfate attack; Cement; Slag; Characterisation; Durability
ID C-S-H; BLAST-FURNACE SLAG; PORTLAND-CEMENT; GYPSUM FORMATION; ATTACK;
HYDRATION; CONCRETE; MORTARS; CRYSTALLIZATION; MICROSTRUCTURE
AB Slag cement pastes prepared with either 40% or 70% of slags by weight were
prepared (W/B = 0.5) and subsequently exposed to a 3 g L-1 Na2SO4 solution. The
slag cements were shown to be more resistant. Initially, ettringite levels rose,
then plateaued upon carbonate AFm consumption, although monosulfate was also found
to be in equilibrium with ettringite when using an Al-rich slag. Portlandite was
initially consumed, to form ettringite, but leached out after prolonged attack
until it was fully depleted, or nearly, with subsequently C-A-S-H being
decalcified. Any excess aluminium released by the slag was bound to a calcium
deficient C-A-S-H phase and hydrotalcite, sheltering the aluminates from ingressing
sulfates. Mass balance further revealed that, if the slag in the blends were to
fully dissolve to form C-A-S-H and hydrotalcite, there would have been insufficient
aluminium and calcium to combine with sulfates to form ettringite. Rather, calcium
from C-A-S-H would have continuously leached, leaving behind a silicate skeleton.
C1 [Whittaker, Mark] Univ Aberdeen, Kings Coll, Aberdeen AB24 3FX, Scotland.
[Whittaker, Mark; Black, Leon] Univ Leeds, Woodhouse Lane, Leeds LS2 9JT, W
Yorkshire, England.
[Zajac, Maciej; Ben Haha, Mohsen] Heidelberg Technol Ctr GmbH, Rohrbacher Str
95, D-69181 Leimen, Germany.
C3 University of Aberdeen; University of Leeds
RP Black, L (corresponding author), Univ Leeds, Woodhouse Lane, Leeds LS2 9JT, W
Yorkshire, England.
EM l.black@leeds.ac.uk
RI Ben Haha, Mohsen/AAC-4859-2020; Zajac, Maciej/AAP-8225-2020; Black,
Leon/B-5840-2008
OI Ben Haha, Mohsen/0000-0001-7570-326X; Black, Leon/0000-0001-8531-4989
FU University Research Scholarship from the University Of Leeds;
HeidelbergCement Technology Centre GmbH
FX This work was funded by a University Research Scholarship from the
University Of Leeds for Mark Whittaker, with additional funding and
materials provided by HeidelbergCement Technology Centre GmbH. The
authors also wish to express their gratitude to Barbara Lothenbach and
the referees who provided very constructive feedback.
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10.1016/j.cemconres.2014.07.018
NR 56
TC 47
Z9 53
U1 1
U2 29
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD AUG 30
PY 2016
VL 119
BP 356
EP 369
DI 10.1016/j.conbuildmat.2016.05.015
PG 14
GA DQ1JF
UT WOS:000378956600035
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Jha, AK
Sivapullaiah, PV
AF Jha, Arvind Kumar
Sivapullaiah, P. V.
TI Volume change behavior of lime treated gypseous soil - influence of
mineralogy and microstructure
LA English
DT Article
DE Cementitious; Compressibility; Ettringite; Hydration; Swell
ID FURNACE SLAG GGBS; SULFATE ATTACK; COMPRESSIBILITY BEHAVIOR;
GEOTECHNICAL PROPERTIES; STABILIZED KAOLINITE; FLY-ASH; ETTRINGITE;
STRENGTH; HYDRATION
AB Series of oedometer tests and micro-analytical studies (XRD, SEM and EDAX) have
been carried out to investigate the influence of varying gypsum content on swell,
compressibility and permeability of lime treated montmorillonitic soil after curing
for different period. Immediate swell is observed on inundation of compacted
samples with water and continuously increased with gypsum content. However, changes
in swell are found to be marginal with curing. This is attributed to the formation
and growth of ettringite crystals by ionic reactions of aluminum calcium-sulfate in
the presence of water which is confirmed through detailed micro-analysis. The
higher swell in uncured specimens and gradual reduction in swell with increase in
curing periods are due to relative dominance of formation and growth of ettringite
and cementitious compounds, respectively. Also, the ionic reaction products are
found to bear a significant influence on the compressibility and permeability
behavior. (C) 2015 Elsevier B.V. All rights reserved.
C1 [Jha, Arvind Kumar; Sivapullaiah, P. V.] Indian Inst Sci, Dept Civil Engn,
Bangalore 566012, Karnataka, India.
C3 Indian Institute of Science (IISC) - Bangalore
RP Sivapullaiah, PV (corresponding author), Indian Inst Sci, Dept Civil Engn,
Bangalore 566012, Karnataka, India.
EM arvind@civil.iisc.ernet.in; siva@civil.iisc.ernet.in
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NR 51
TC 47
Z9 49
U1 0
U2 33
PI AMSTERDAM
SN 0169-1317
EI 1872-9053
J9 APPL CLAY SCI
JI Appl. Clay Sci.
PD JAN
PY 2016
VL 119
BP 202
EP 212
DI 10.1016/j.clay.2015.09.017
PN 2
PG 11
GA CY6SL
UT WOS:000366539000003
DA 2023-12-05
ER
PT J
AU Magallanes-Rivera, RX
Juarez-Alvarado, CA
Valdez, P
Mendoza-Rangel, JM
AF Magallanes-Rivera, R. X.
Juarez-Alvarado, C. A.
Valdez, P.
Mendoza-Rangel, J. M.
TI Modified gypsum compounds: An ecological-economical choice to improve
traditional plasters
LA English
DT Article
DE Hemihydrate; Gypsum; Blast furnace slag; Hydration; Silica Fume; Fly
ash; Dimensional stability; Absorption; Low density
ID CEMENTITIOUS BINDER; WASTE GYPSUM; FLY-ASH; HYDRATION; STRENGTH; WATER;
SLAG; PERFORMANCE; REACTIVITY; ACTIVATION
AB An investigation was performed on the improvement of properties for commercial
hemihydrate by means of low additions of granulated blast furnace slag and
pozzolanas like silica fume or fly ash. Results after 180 days for pastes cured
under water at 20 degrees C showed that it is possible to triplicate the
compressive strength of plain plaster. The reaction mechanism can be summarized by
the total reaction of the hemihydrate in the first 24 h, followed by the slower
slag and pozzolanas hydration and interaction of the sulfates with aluminium to
form ettringite. Excellent dimensional stability and low density was also observed.
C1 [Magallanes-Rivera, R. X.; Juarez-Alvarado, C. A.; Valdez, P.; Mendoza-Rangel,
J. M.] Univ Autonoma Nuevo Leon UANL, Fac Ingn Civil, Acad Grp Concrete Technol,
San Nicolas De Los Garza 66450, NL, Mexico.
C3 Universidad Autonoma de Nuevo Leon
RP Magallanes-Rivera, RX (corresponding author), Univ Autonoma Nuevo Leon UANL, Fac
Ingn Civil, Acad Grp Concrete Technol, Ciudad Univ S-N, San Nicolas De Los Garza
66450, NL, Mexico.
EM rxmagallanes@gmail.com
RI Juaréz, Cesar/AGG-9540-2022; Magallanes-Rivera, Ricardo/B-4817-2019;
Mendoza-Rangel, Jose Manuel/O-4464-2019; UANL, FIC-UANL/O-5444-2015;
Magallanes-Rivera, Ricardo/AAH-7820-2020
OI Magallanes-Rivera, Ricardo/0000-0002-3504-720X; Mendoza-Rangel, Jose
Manuel/0000-0002-5896-6006; Magallanes-Rivera,
Ricardo/0000-0002-3504-720X; Valdez-Tamez, Pedro
Leobardo/0000-0002-1298-2051
FU PROMEP
FX Thanks are due to PROMEP for the scholarship of Magallanes-Rivera to
develop this research and Jose Luis Lopez from RHI-Refmex for the silica
fume used.
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NR 23
TC 47
Z9 50
U1 3
U2 43
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
PD DEC
PY 2012
VL 37
BP 591
EP 596
DI 10.1016/j.conbuildmat.2012.07.054
PG 6
GA 083AF
UT WOS:000314434400068
DA 2023-12-05
ER
PT J
AU Anjos, C
Magalhaes, MCF
Abreu, MM
AF Anjos, Carla
Magalhaes, M. Clara F.
Abreu, Maria Manuela
TI Metal (Al, Mn, Pb and Zn) soils extractable reagents for available
fraction assessment: Comparison using plants, and dry and moist soils
from the Bracal abandoned lead mine area, Portugal
SO JOURNAL OF GEOCHEMICAL EXPLORATION
LA English
DT Article
DE Abandoned lead mine; Available extraction methods; Metals
phytoavailability; Spontaneous shrubs
ID RHIZOSPHERE-BASED METHOD; TRACE-ELEMENTS; COEXISTING SPHALERITE;
SAO-DOMINGOS; HEAVY-METALS; PHYTOAVAILABILITY; BIOAVAILABILITY;
MANGANESE; ENVIRONMENTS; REMEDIATION
AB Eleven composite soil samples, developed either on schist materials or fine
heterogeneous waste materials and coarse metallurgical slags, were collected in the
Bracal (Portugal) abandoned lead mine. Plants growing in each sampling area were
identified. A total of 49 plant samples of eight species -Acacia dealbata Link,
Acacia melanoxilon R. Br., Cistus inflows Pourr. ex Demoly, Erica arborea L.
Eucalyptus globulus Labill., Pinus pinaster Aiton, Quercus robur L, and Ulex minor
Roth - were collected. This study intends to evaluate the available fraction of
aluminium, lead, manganese, and zinc in the soils using dry and moist samples in
contact with five extractant solutions, degasified distilled water, and calcium
chloride, calcium nitrate, ammonium acetate and DTPA aqueous solutions, and to
compare together these results with the total elemental amounts in the aboveground
part of the plant species. The available fraction is higher in moist than in the
dry soil samples. The correlations between the soil available fraction of the
elements and its concentration in the plants suggest that DTPA is not the best
extractant for lead bioavailability evaluation. Variable results were observed for
the bioavailable fraction of the elements evaluation suggesting that, in
multielemental contaminated soils, calcium chloride seems to be a good extractant
medium, once it correlates with the higher number of plant species. (C) 2011
C1 [Anjos, Carla; Magalhaes, M. Clara F.] Univ Aveiro, CICECO, Dept Quim, P-3800
Aveiro, Portugal.
[Abreu, Maria Manuela] Univ Tecn Lisboa, UIQA, Inst Super Agron, Lisbon,
Portugal.
C3 Universidade de Aveiro; Universidade de Lisboa
RP Anjos, C (corresponding author), Univ Aveiro, CICECO, Dept Quim, P-3800 Aveiro,
Portugal.
EM c.anjos@ua.pt
RI Abreu, Maria Manuela/AAK-9721-2021; Magalhães, Maria Clara F/B-3055-2014
OI Abreu, Maria Manuela/0000-0002-6650-1161; Magalhães, Maria Clara
F/0000-0002-3359-850X
FU Portuguese Foundation for Science and Technology of CICECO
FX We would like to thank the Portuguese Foundation for Science and
Technology for financial research support of CICECO.
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NR 53
TC 47
Z9 53
U1 0
U2 63
PU ELSEVIER
PI AMSTERDAM
SN 0375-6742
EI 1879-1689
J9 J GEOCHEM EXPLOR
JI J. Geochem. Explor.
PD FEB
PY 2012
VL 113
SI SI
BP 45
EP 55
DI 10.1016/j.gexplo.2011.07.004
PG 11
GA 903AT
UT WOS:000301086300006
DA 2023-12-05
ER
PT J
AU Shen, X
Chen, M
Wang, N
Wang, D
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Chen, Min
Wang, Nan
Wang, Dong
TI Viscosity Property and Melt Structure of
CaO-MgO-SiO2-Al2O3-FeO Slag System
LA English
DT Article
DE quinary slag system; smelting reduction; viscosity; structure;
polymerization degree
ID ALUMINOSILICATE MELTS; CALCIUM ALUMINATE; SILICATE MELTS; RAMAN;
GLASSES; BEHAVIOR; BEARING; MGO; IR
AB For the purpose to describe the change of the viscosity properties of the
converter slag during smelting reduction process using aluminum ash as reductant
and provide basis for technology development, the viscosity of CaO-MgO-SiO2-Al2O3-
FeO slag system at a fixed basicity of 3 was measured with the various ratio of
A/(A+F) (w(Al2O3)/w(Al2O3+FeO)) by the cylinder method, and the structural of the
melt was analyzed based on the FTIR and Raman spectroscopy to further explain the
evolution behavior of viscosity. The results showed that viscosity of the slag was
increased with increasing the ratio of A/(A+F). When this ratio increased from 0.17
to 0.5, the simple network units of the molten slag were polymerized into more
complex network structure, resulting in a slow increase in viscosity from 0.65
dPa.s to 0.91 dPa.s at 1 873 K. With further increasing this ratio to 1.0, the main
structure was converted from silicate structure to aluminate structure. In
addition, the polymerization degrees of aluminate units and silicate units both
increased, which eventually led to an rapid increase in the viscosity from 0.91
dPa.s to 1.94 dPa.s.
C1 [Shen, Xiang; Chen, Min; Wang, Nan; Wang, Dong] Northeastern Univ, Sch Met, 3-11
Wen Hua Rd, Shenyang 110819, Liaoning, Peoples R China.
RP Chen, M (corresponding author), Northeastern Univ, Sch Met, 3-11 Wen Hua Rd,
Shenyang 110819, Liaoning, Peoples R China.
EM chenm@smm.neu.edu.cn
RI Wang, Nan/HLV-7836-2023; Wang, Nan/JLL-3980-2023; Wang,
Nan/GRY-3150-2022
FU National Natural Science Foundation of China [51574065, 51574066,
51774073, 51774072]; National Key R&D Program of China [2017YFB0304201,
2017YFB0304203, 2016YFB0300602]
FX The authors gratefully acknowledge the National Natural Science
Foundation of China (Grant numbers 51574065, 51574066, 51774073 and
51774072) and the National Key R&D Program of China (Grant numbers
2017YFB0304201, 2017YFB0304203 and 2016YFB0300602) which has made this
research possible.
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NR 34
TC 46
Z9 48
U1 6
U2 34
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2019
VL 59
IS 1
BP 9
EP 15
DI 10.2355/isijinternational.ISIJINT-2018-479
PG 7
GA HJ3KK
UT WOS:000457069600002
OA gold
DA 2023-12-05
ER
PT J
AU Gao, JX
Wen, GH
Huang, T
Bai, BW
Tang, P
Liu, Q
AF Gao, Jinxing
Wen, Guanghua
Huang, Ting
Bai, Binwen
Tang, Ping
Liu, Qiang
TI Effect of Al Speciation on the Structure of High-Al Steels Mold Fluxes
Containing Fluoride
LA English
DT Article
DE calcium silicate; microstructure; spectroscopy; aluminosilicates
ID MQ-MAS NMR; CALCIUM ALUMINOSILICATE; CRYSTALLIZATION BEHAVIOR; GLASSES;
ALUMINUM; RAMAN; VISCOSITY; MELTS; CAO-AL2O3; KINETICS
AB To design suitable mold fluxes for the casting of high-Al steels, the structure
of mold fluxes based on CaO-SiO2, CaO-SiO2-Al2O3, and CaO-Al2O3 was examined by
Raman spectroscopy and magic-angle spinning nuclear magnetic resonance. The results
showed that Si atoms are replaced by Al atoms as the network formers with the
increase in Al2O3 in the mold fluxes. This converts the silicate slags (CaO-SiO2
mold fluxes) into aluminosilicates slags (CaO-SiO2-Al2O3 or CaO-Al2O3 mold fluxes).
The F- ions in the mold flux containing Al2O3 are classified into three categories,
according to function: Bridging F's, Nonbridging F's, and Free-F's. The Al3+ ion
holds three distinct coordination environments: IV Al, V Al, and VI Al. The
addition of F affects the coordination environment of Al3+ to form AlO3F and AlO2F2
that accommodate the network structure of slags. The network structure in the CaO-
SiO2 mold fluxes is mainly connected through Si-O-Si linkage. However, the network
structure of the mold fluxes containing elevated content of Al2O3 is mainly
connected through Si-O-Si, Al-OAl, Al-O-Si, and Al-F-Al linkages. Hence, the
structural characteristics of high-Al steels mold fluxes must be considered during
the designing step of the mold fluxes.
C1 [Gao, Jinxing; Wen, Guanghua; Huang, Ting; Bai, Binwen; Tang, Ping; Liu, Qiang]
Chongqing Univ, Coll Mat Sci & Engn, State Key Lab Mech Transmiss, Chongqing
RP Gao, JX (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, State Key
Lab Mech Transmiss, Chongqing 400044, Peoples R China.
EM gaojinxing163@163.com
FX The authors would like to greatly appreciate the funding from the
National Natural Science Foundation of China (grant nos. 51274260 and
51574050).
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NR 38
TC 46
Z9 51
U1 0
U2 19
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD DEC
PY 2016
VL 99
IS 12
BP 3941
EP 3947
DI 10.1111/jace.14444
PG 7
GA EK3RQ
UT WOS:000393844100013
DA 2023-12-05
ER
PT J
AU Dung, NT
Chang, TP
Chen, CT
AF Nguyen Tien Dung
Chang, Ta-Peng
Chen, Chun-Tao
TI Engineering and sulfate resistance properties of slag-CFBC fly ash paste
and mortar
LA English
DT Article
DE Sulfate resistance; Slag; Circulating fluidized bed combustion (CFBC)
fly ash; Hydration product; Compressive strength; Drying shrinkage
ID C-S-H; FLUIDIZED-BED; PORTLAND-CEMENT; HYDRATION; STRENGTH; MECHANISM;
ETTRINGITE; GEOPOLYMER; ANHYDRITE; PRODUCTS
AB This study explores a SCA cement produced by mixing slag (S) and circulating
fluidized bed combustion (CFBC) fly ash (CA). The hydration products of SCA cement
detected by X-ray Diffraction and Thermogravimetric Analysis were ettringite,
calcium silicate hydrate and calcium aluminium silicate hydrate, all of which
produced dense microstructure. The compressive strengths of SCA paste and mortar
specimens reached 75 MPa at 28 days. The expansion of SCA paste and mortar
compensated for drying shrinkage, thereby leading to low ultimate shrinkage. The
SCA mortars had good resistance to sulfate attack with the strength loss about 15%
or less. (C) 2014 Elsevier Ltd. All rights reserved.
C1 [Nguyen Tien Dung; Chang, Ta-Peng; Chen, Chun-Tao] Natl Taiwan Univ Sci &
Technol Taiwan Tech, Dept Construct Engn, Taipei 106, Taiwan.
C3 National Taiwan University of Science & Technology
RP Chang, TP (corresponding author), Natl Taiwan Univ Sci & Technol Taiwan Tech,
Dept Construct Engn, Taipei 106, Taiwan.
EM tpchang@mail.ntust.edu.tw
RI CHen, Chun-Tao/H-9800-2017; Nguyen, Tien-Dung/AAD-9608-2021
OI CHen, Chun-Tao/0000-0003-2038-2205; Nguyen, Dung T./0000-0001-9102-4072
FU National Taiwan University of Science and Technology (NTUST) (Taiwan
Tech)
FX The first author gratefully acknowledges the financial support of this
work from National Taiwan University of Science and Technology (NTUST)
(Taiwan Tech) through the scholarships. The chemical tests were carried
out at the Department of Chemical Engineering of NTUST by a valuable
assistance from Mr. Vo Duc Thang.
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NR 41
TC 46
Z9 48
U1 4
U2 62
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUL 30
PY 2014
VL 63
BP 40
EP 48
DI 10.1016/j.conbuildmat.2014.04.009
PG 9
GA AJ7JW
UT WOS:000337874000005
DA 2023-12-05
ER
PT J
AU Vasudevan, S
Lakshmi, J
Sozhan, G
Sozhan, Ganapathy
TI Optimization of the process parameters for the removal of phosphate from
drinking water by electrocoagulation
SO DESALINATION AND WATER TREATMENT
LA English
DT Article
DE Electrocoagulation; Phosphate; Removal; Adsorption; Kinetics; Isotherms
PHOSPHORUS REMOVAL; ADSORPTION; FLUORIDE; ALUMINUM; SLUDGE; RAW
AB The present Studies provide the purification of drinking water containing
phosphate by electrocoagulation process using zinc as the anode and stainless steel
as the cathode. The experimental parameters like electrolyte pH, temperature and
current density, and so forth, on the removal efficiency of phosphate were carried
out. The adsorption capacity was evaluated using both Langmuir and Freundlich
isotherm models. The kinetic studies show that the adsorption obeys second-order
kinetics. The maximum removal efficiency of 98.8% was achieved at a current density
of 0.05 A/dm(2), at a pH of 7.0. Thermodynamic parameters were evaluated. Overall
adsorption process was endo-thermic and spontaneous. The adsorption of phosphate
preferably fitting the Langmuir adsorption isotherm suggests monolayer coverage of
adsorbed molecules.
C1 [Vasudevan, Subramanyan; Lakshmi, Jothinathan; Sozhan, Ganapathy] Cent
Electrochem Res Inst CSIR, Karaikkudi, Tamil Nadu, India.
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Tamil Nadu, India.
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TC 46
Z9 47
U1 0
U2 23
PU DESALINATION PUBL
PI HOPKINTON
PA 36 WALCOTT VALLEY DRIVE,, HOPKINTON, MA 01748 USA
SN 1944-3994
EI 1944-3986
J9 DESALIN WATER TREAT
JI Desalin. Water Treat.
PD DEC
PY 2009
VL 12
IS 1-3
BP 407
EP 414
DI 10.5004/dwt.2009.971
PG 8
GA 541OF
UT WOS:000273424700054
DA 2023-12-05
ER
PT J
AU Zhang, LF
AF Zhang, LF
TI State of the art in the control of inclusions in tire cord steels - a
review
LA English
DT Article
DE inclusions; tire cord steel; steel refining; tundish; synthetic slag
treatment
ID OXIDE INCLUSIONS; TUNDISH; CLEANLINESS; BEHAVIOR; FLOW
AB The control of inclusions in tire cord steels and techniques used in the
production process are extensively reviewed. Inclusion and segregation requirements
for the tire cord steel are discussed. The deformability of an inclusion is
significantly affected by its Al2O3 content. Inclusions containing 20% Al2O3 has
best deformability. The undeformable inclusions can be avoided by controlling the
dissolved aluminum in the steel. Low basicity slags favour the generation of
deformable inclusions. When the basicity R (=CaO/SiO2) = 0.8-1.5, the dissolved
aluminum in the steel should be 1-5ppm to achieve 20% Al2O3 in inclusions. With
R=1.0-1.4, in order to control [Al] in the range of 1-5ppm, the slag should contain
approximately 8% Al2O3. The technologies to control inclusions in tire cord steels
are reviewed including steel deoxidizer choice, steel refining method, slag carry
over from BOF to the ladle, ladle stirring practice, control of nitrogen pickup and
caster curvature. Control methods to decrease the central segregation in the tire
cord steel are briefly reviewed, such as electromagnetic stirring during continuous
casting.
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RP Zhang, LF (corresponding author), Norwegian Univ Sci & Technol, Dept Mat Sci &
Engn, Alfred Getz Vei 2, N-7491 Trondheim, Norway.
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[No title captured]
[No title captured]
NR 91
TC 46
Z9 50
U1 3
U2 29
PI WEINHEIM
PA POSTFACH 101161, 69451 WEINHEIM, GERMANY
SN 1611-3683
EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD MAR
PY 2006
VL 77
IS 3
BP 158
EP 169
DI 10.1002/srin.200606370
PG 12
GA 037OZ
UT WOS:000237157800003
DA 2023-12-05
ER
PT J
AU Olson, RA
Martins, LCB
AF Olson, RA
Martins, LCB
TI Cellular ceramics in metal filtration
SO ADVANCED ENGINEERING MATERIALS
LA English
DT Review
AB In most molten metal processing operations, the acts of melting, transporting
and alloying the metal in preparation for casting into desired shapes introduces
undesirable non-metallic inclusions to the melt. Molten metals are highly reactive
and tend to interact with gases and refractories during processing steps;
undesirable phases are absorbed either as liquid or solid. Such examples of
inclusion introduction are molten aluminum reacting with oxygen in air to form
solid aluminum oxide, or molten cast iron reacting with oxygen in air to form
liquid slag phases.
C1 SELEE Corp, Hendersonville, NC USA.
RP Olson, RA (corresponding author), SELEE Corp, Hendersonville, NC USA.
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PD APR
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IS 4
BP 187
EP 192
DI 10.1002/adem.200500021
PG 6
GA 935AZ
UT WOS:000229752500005
DA 2023-12-05
ER
PT J
AU Homayoonmehr, R
Ramezanianpour, AA
Mirdarsoltany, M
AF Homayoonmehr, Reza
Ramezanianpour, Ali Akbar
Mirdarsoltany, Mohammadamin
TI Influence of metakaolin on fresh properties, mechanical properties and
corrosion resistance of concrete and its sustainability issues: A review
SO JOURNAL OF BUILDING ENGINEERING
LA English
DT Review
DE Metakaolin; Mechanical strength; Chloride-induce corrosion;
Chloride-binding; Carbonation; Sustainability
ID SUPPLEMENTARY CEMENTING MATERIALS; HIGH-STRENGTH CONCRETE; PORE-SIZE
DISTRIBUTION; BLAST-FURNACE SLAG; HIGH-PERFORMANCE METAKAOLIN; HIGH
REACTIVITY METAKAOLIN; FIBER-REINFORCED CONCRETE; SELF-COMPACTING
CONCRETE; OIL FUEL ASH; C-S-H
AB As an available and high-quality supplementary cementing materials (SCMs),
Consumption of Metakaolin (MK) was proposed by many research to replace Portland
cement to improve concrete quality and reduce the negative effects of cement
industry on the environment. With that being said, it is necessary to summarize the
recent finding and gaps on the effect of replacing Portland-cement by MK in
different replacement levels on various fresh and hardened properties of concrete.
This review paper presents an overview of recent investigations on MK effect on
fresh properties, mechanical strength, and corrosion resistance of concrete and
mortars. Besides, the synergic effect of MK and other SCMs, its optimum replacement
level for different purposes, and application of in different types of concretes
are discussed as well. The literature indicates that using MK, up to a certain
replacement level, improves the pore structure of concrete; consequently, increases
its durability against chloride-induced corrosion. Because of the high aluminum
(Al) composition of MK, using MK increases chloride binding as well. In the case of
carbonation, using MK was reported to increase the carbonation depth mostly under
high CO2 concentrations. Nevertheless, under the conventional concentration of CO2,
MK containing specimens show acceptable performance against carbonation, especially
combined to the limestone. From another perspective, MK can play a major role to
reduce the direct and indirect CO2 emission of cement industry, and using it seems
an inevitable step toward more sustainable cement industry and concrete
construction.
C1 [Ramezanianpour, Ali Akbar] Amirkabir Univ Technol, Dept Civil & Environm Engn,
Concrete Technol & Durabil Res Ctr CTDRc, Tehran, Iran.
[Homayoonmehr, Reza; Mirdarsoltany, Mohammadamin] Amirkabir Univ Technol, Dept
Civil Engn, Tehran, Iran.
C3 Amirkabir University of Technology; Amirkabir University of Technology
RP Homayoonmehr, R (corresponding author), Amirkabir Univ Technol, Dept Civil Engn,
Tehran, Iran.
EM rhomayoonmehr@aut.ac.ir
FU INSF
FX The authors wish to acknowledge INSF for their support of the project.
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NR 241
TC 45
Z9 45
U1 7
U2 29
PU ELSEVIER
PI AMSTERDAM
EI 2352-7102
J9 J BUILD ENG
JI J. Build. Eng.
PD DEC
PY 2021
VL 44
AR 103011
DI 10.1016/j.jobe.2021.103011
EA JUL 2021
PG 22
WC Construction & Building Technology; Engineering, Civil
SC Construction & Building Technology; Engineering
GA UY6OS
UT WOS:000701641500001
DA 2023-12-05
ER
PT J
AU Mabroum, S
Aboulayt, A
Taha, Y
Benzaazoua, M
Semlal, N
Hakkou, R
AF Mabroum, S.
Aboulayt, A.
Taha, Y.
Benzaazoua, M.
Semlal, N.
Hakkou, R.
TI Elaboration of geopolymers based on clays by-products from phosphate
mines for construction applications
LA English
DT Article
DE Phosphate mines; Mine waste; Clayey lithology; Valorization;
Geopolymers; Circular economy
ID ASH-BASED GEOPOLYMER; BLAST-FURNACE SLAG; FLY-ASH; ALKALI ACTIVATION;
METAKAOLIN; TAILINGS; WASTE; SI-29; AL-27; MICROSTRUCTURE
AB Yellow clays from Moroccan phosphate mines are extracted with other waste rocks
lithologies and stored in large dumps within the mine site. The present paper
investigates the use of this by-product as a new aluminosilicate source for
geopolymers elaboration at the laboratory scale. Yellow clays studied are mainly
composed of montmorillonite, dolomite and quartz as major phases. The Toxicity
Characteristic Leaching Procedure (TCLP) showed no existence of contaminant. In
order to reach thermal activation, the raw clays were first calcined at different
temperatures between 500 and 900 degrees C. Raw and calcined clays were
characterized using thermogravimetric analysis (TGA), X-Ray Diffraction (XRD) and
Fourier transformed infrared (FTIR) spectroscopy. For the synthesis of geopolymers,
calcined powder was mixed with an alkaline solution presenting different
NaOH/Na2SiO3 ratios. The compressive strength was measured at 7, 14 and 28 days and
material porosity was determined using Mercury Intrusion Porosimetry method in
order to explain the mechanical behavior. XRD, 27Al and 29Si Magic Angle Spinning
Nuclear Magnetic Resonance (MAS-NMR) spectroscopy, Fourier transformed infrared and
TGA have been used to investigate the gel structure.
The thermal treatment at 900 degrees C allowed the destruction of crystalline
structure of montmorillonite clays, as well as the formation of new phases such as
periclase (MgO) and gehlenite (Ca2Al2SiO7). Furthermore, the Al-27 - Si-29 MAS-NMR
and the XRD analysis of the elaborated materials confirmed the formation of two
cementitious gels C-A-S-H (Calcium aluminum silicate hydrate) and N-A-S-H (Sodium
aluminum silicate hydrate). The compressive strength was around 25 MPa at 28 days.
The obtained results are promising; they have shown that elaborated materials can
be adapted for construction applications. In this case, it is recommended that
economic and commercial study be developed. (C) 2020 Elsevier Ltd. All rights
reserved.
C1 [Mabroum, S.; Aboulayt, A.; Taha, Y.; Benzaazoua, M.; Hakkou, R.] Mohammed VI
Polytech Univ UM6P, Ben Guerir 43150, Morocco.
[Benzaazoua, M.] Inst Rech Mines & Environm IRME UQAT, Rouyn Noranda, PQ,
Canada.
[Semlal, N.] OCP SA, Innovat, BP 118, El Jadida 24000, Morocco.
[Mabroum, S.; Hakkou, R.] Cadi Ayyad Univ UCA, Fac Sci & Technol, Marrakech
40000, Morocco.
C3 Mohammed VI Polytechnic University; Cadi Ayyad University of Marrakech
RP Hakkou, R (corresponding author), Mohammed VI Polytech Univ UM6P, Ben Guerir
43150, Morocco.
EM r.hakkou@uca.ma
RI Semlal, Nawal/AAT-5177-2020; Taha, Yassine/N-3181-2018
OI Taha, Yassine/0000-0003-3193-1046; ABOULAYT,
Abdelilah/0000-0002-6056-6693
FU OCP-SA, Morocco [OCP/UM6P AS03]
FX This work was support by OCP-SA, Morocco, under the specific agreement
OCP/UM6P #AS03. The authors would like to show their gratitude to the
OCP-SA collaborators for the great help concerning the sampling.
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Z9 45
U1 2
U2 55
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD JUL 10
PY 2020
VL 261
AR 121317
DI 10.1016/j.jclepro.2020.121317
PG 11
& Ecology
GA LO3OC
UT WOS:000533537200010
DA 2023-12-05
ER
PT J
AU Yang, LY
Yang, MM
Xu, P
Zhao, XC
Bai, H
Li, H
AF Yang, Liyun
Yang, Maomao
Xu, Ping
Zhao, Xiancong
Bai, Hao
Li, Hong
TI Characteristics of Nitrate Removal from Aqueous Solution by Modified
Steel Slag
SO WATER
LA English
DT Article
DE nitrate; modified steel slag; adsorption; mechanism; regeneration
ID MAKING SLAG; WATER-TREATMENT; ADSORPTION; WASTE; PHOSPHATE; SORPTION;
IONS; ADSORBENTS; PHOSPHORUS; ALUMINA
AB Steel slag, which makes up a gigantic amount of metallurgical industrial solid
waste, was in this experiment successfully synthesized an inexpensive adsorbent
used to remove nitrate pollution from aqueous solution. This adsorbent was obtained
by mixing steel slag, aluminium hydroxide and deionized water, and aging this at a
mass ratio of 3:0.45:2, and then activating it at 800 degrees C. The
physicochemical characteristics of the steel slag before and after modification
were investigated to compare the effect of their surface properties on the
adsorption behaviour of nitrate. The effects of adsorbent dosage, pH, and contact
time on the adsorption process were investigated. The results showed that an
increase in specific surface area and the formation of a positive surface of the
modified steel slag (MSS) compared with the original steel slag (OSS) could
effectively increase the number of the active adsorption sites and nitrate removal
ability. The optimum parameters for nitrate removal were as follows: the
concentration of nitrate was 20 mg/L, the dosage was 1 g/100 mL, the pH was four,
and the reaction time was 180 min. The adsorption capacity of the MSS was
approximately 1.9 times that of the OSS. The nitrate adsorption of the MSS was in
accordance with the pseudo-second-order model and the Freundlich model, which
indicated that the adsorption of nitrate on the MSS was mainly single layer
chemical adsorption. The mechanism of nitrate removal mainly included ion exchange,
hydrogen bonding, electrostatic interactions and intermolecular interactions. In
addition, regeneration experiments indicated that the MSS after regeneration still
had the capacity to remove nitrate.
C1 [Yang, Liyun; Yang, Maomao; Xu, Ping; Zhao, Xiancong; Bai, Hao; Li, Hong] Univ
Sci & Technol, Sch Met & Ecol Engn, Beijing 100083, Peoples R China.
RP Yang, LY (corresponding author), Univ Sci & Technol, Sch Met & Ecol Engn,
EM Yangliyun@ustb.edu.cn; yangmm0426@foxmail.com; sensen150107@163.com;
zhaoxiancong319@foxmail.com; baihao@metall.ustb.edu.cn;
lihong@metall.ustb.edu.cn
FU Ten-Year Evaluation Project of the People's Republic of China Ministry
of Environmental Protection [STSN-06]
FX Financial support for this study was provided by the Ten-Year Evaluation
Project of the People's Republic of China Ministry of Environmental
Protection (STSN-06).
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NR 53
TC 45
Z9 45
U1 2
U2 22
PU MDPI AG
PI BASEL
SN 2073-4441
J9 WATER-SUI
JI Water
PD OCT
PY 2017
VL 9
IS 10
AR 757
DI 10.3390/w9100757
PG 17
WC Environmental Sciences; Water Resources
SC Environmental Sciences & Ecology; Water Resources
GA FM1BZ
UT WOS:000414707500034
DA 2023-12-05
ER
PT J
AU Krishna, KCB
Aryal, A
Jansen, T
AF Krishna, K. C. Bal
Aryal, Ashok
Jansen, Troy
TI Comparative study of ground water treatment plants sludges to remove
phosphorous from wastewater
LA English
DT Article
DE Adsorption isotherm; Adsorption kinetics; Alum sludge; Iron sludge;
Phosphorus
ID CONSTRUCTED WETLAND SYSTEM; AQUEOUS-SOLUTION; ALUM SLUDGE; PHOSPHATE
ADSORPTION; STEEL SLAG; MECHANISMS; CAPACITY; SORPTION; PERFORMANCE;
RETENTION
AB Alum- and iron-based sludge obtained from water treatment plant produced during
a unit treatment process (coagulation and flocculation) have been widely tested as
a low-cost adsorbent to remove phosphorous (P) from wastewater. However, the
effectiveness of iron-based sludge generated from the oxidation of iron which
naturally occurs in the ground water has not been investigated. Moreover,
influences of dominant metals ions comprised in the treatment plants sludges on P
adsorption capacity and rate from wastewater are not yet known. This study,
therefore, employed four different groundwater treatment plants sludges iron-based
(from the oxidation of iron) and alum-based (from coagulation and flocculation
process) to determine their P adsorption capacities and adsorption rates from the
synthetic wastewater (SWW) and secondary effluent wastewater (SEWW). Although
metals ions concentrations were the highest in the iron-based sludge amongst the
sludge used in this study, it appeared to have the lowest P adsorption capacity and
adsorption rate. A good correlation between aluminium to iron mass ratio and
adsorption capacity for both types of waters were noted. However, a poor relation
between aluminium to iron mass ratio and adsorption rates for the SEWW was
observed. Further, the tested sludges were found to have a better P removal
efficiency and adsorption capacity from the SEWW than from the SWW. Thus, this
study demonstrates the ground water treatment plants sludges could be a low cost
and effective adsorbent in removing P from wastewater. (C) 2016 Elsevier Ltd. All
rights reserved.
C1 [Krishna, K. C. Bal; Aryal, Ashok] Curtin Univ, Dept Civil Engn, GPO Box U1987,
Perth, WA 6845, Australia.
[Krishna, K. C. Bal] Univ Western Sydney, Inst Infrastruct Engn, Locked Bag
1797, Penrith, NSW 2751, Australia.
[Jansen, Troy] Water Corp, Balcatta, WA, Australia.
[Aryal, Ashok] Infra Tech Pacific Pty Ltd, 32 Honeyeater Circle, Perth, WA 6014,
Australia.
C3 Curtin University; Western Sydney University
RP Krishna, KCB (corresponding author), Univ Western Sydney, Inst Infrastruct Engn,
Locked Bag 1797, Penrith, NSW 2751, Australia.
EM b.kc@westernsydney.edu.au
FU Curtin University; National Centre of Excellence in Desalination,
Australia
FX The authors acknowledge the funding offered by Curtin University and
National Centre of Excellence in Desalination, Australia. The authors
would like to acknowledge Water Corporation, Western Australia for
providing the samples and assisting during the sample collection. The
authors would like to thank Stephen O'Neil from Water Corporation for
his valuable comments.
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NR 32
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Z9 47
U1 3
U2 59
PI LONDON
SN 0301-4797
EI 1095-8630
J9 J ENVIRON MANAGE
PD SEP 15
PY 2016
VL 180
BP 17
EP 23
DI 10.1016/j.jenvman.2016.05.006
PG 7
GA DS1XO
UT WOS:000380418700003
PM 27192387
DA 2023-12-05
ER
PT J
AU Boegelein, T
Louvis, E
Dawson, K
Tatlock, GJ
Jones, AR
AF Boegelein, Thomas
Louvis, Eleftherios
Dawson, Karl
Tatlock, Gordon J.
Jones, Andy R.
TI Characterisation of a complex thin walled structure fabricated by
selective laser melting using a ferritic oxide dispersion strengthened
steel
LA English
DT Article
DE Oxide dispersion strengthened alloys; Rapid prototyping; Additive
manufacturing; Selective laser melting; Transmission electron microscopy
ID BEHAVIOR; POWDER; ALLOY; TEM; ORIENTATION; SUPERALLOYS; PARTICLES;
OXIDATION
AB Oxide dispersion strengthened (ODS) alloys exhibit superior mechanical and
physical properties due to the presence of nanoscopic Y(Al, Ti) oxide precipitates,
but their manufacturing process is complex. The present study is aimed at further
investigation of the application of an alternative, Additive Manufacturing (AM)
technique, Selective Laser Melting (SLM), to the production of consolidated ODS
alloy components. Mechanically alloyed PM2000 (ODS-FeCrAl) powders have been
consolidated and a fine dispersion of Y-containing precipitates were observed in an
as built thin-walled component, but these particles were typically poly-crystalline
and contained a variety of elements including O, Al, Ti, Cr and Fe. Application of
post-build heat treatments resulted in the modification of particle structures and
compositions; in the annealed condition most precipitates were transformed to
single crystal yttrium aluminium oxides. During the annealing treatment,
precipitate distributions homogenised and localised variations in number density
were diminished. The resulting volume fractions of those precipitates were 25-40%
lower than have been reported in conventionally processed PM2000, which was
attributed to Y-rich slag-like surface features and inclusions formed during SLM.
(C) 2015 Elsevier Inc. All rights reserved.
C1 [Boegelein, Thomas; Louvis, Eleftherios; Dawson, Karl; Tatlock, Gordon J.;
Jones, Andy R.] Univ Liverpool, Sch Engn, Ctr Mat & Struct, Liverpool L69 3G,
Merseyside, England.
[Louvis, Eleftherios] Stryker Orthopaed, Addit Mfg Technol Ctr Excellence, IDA
Business & Technol Pk, Carrigtwohill, Cork, Ireland.
C3 University of Liverpool
RP Boegelein, T (corresponding author), Univ Liverpool, Sch Engn, Ctr Mat & Struct,
Liverpool L69 3G, Merseyside, England.
EM t.boegelein@liv.ac.uk
OI Dawson, Karl/0000-0003-3249-8328
FU Advanced Research Materials (ARM) Programme; EPSRC [EP/H018921/1];
Engineering and Physical Sciences Research Council [EP/H018921/1]
Funding Source: researchfish; EPSRC [EP/H018921/1] Funding Source: UKRI
FX The authors are grateful for financial support of the work through the
Advanced Research Materials (ARM) Programme, U.S. Department of Energy,
Office of Fossil Energy managed by U.T.-Battelle, LLC and funding by
EPSRC grant EP/H018921/1 (Materials for Fusion and Fission Power). The
staff at the Nanoinvestigation Centre at Liverpool (NiCaL), led by Dr.
S. Romani, is greatly acknowledged for support and helpful advice. The
hexagon structure was produced in the Manufacturing Science and
Engineering Research Centre at the University of Liverpool, led by Dr.
C.J. Sutcliffe. Members of the group, in particular Dr. J. Singh and Dr.
J. Robinson, gave valuable input.
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NR 53
TC 45
Z9 52
U1 9
U2 158
PI NEW YORK
SN 1044-5803
EI 1873-4189
J9 MATER CHARACT
JI Mater. Charact.
PD FEB
PY 2016
VL 112
BP 30
EP 40
DI 10.1016/j.matchar.2015.11.021
PG 11
GA DD7MR
UT WOS:000370109200004
OA hybrid
DA 2023-12-05
ER
PT J
AU Riley, AL
Mayes, WM
AF Riley, Alex L.
Mayes, William M.
TI Long-term evolution of highly alkaline steel slag drainage waters
SO ENVIRONMENTAL MONITORING AND ASSESSMENT
LA English
DT Article
DE Slag; Hyperalkaline; Trend analysis; Calcite precipitation; Pollution
ID CONSTRUCTED WETLAND; BLAST-FURNACE; GROUND-WATER; LEACHATE; TESTS; PH;
PENNSYLVANIA; REMEDIATION; DOWNSTREAM; TOXICITY
AB The disposal of slag generated by the steel industry can have negative
consequences upon the surrounding aquatic environment by the generation of high pH
waters, leaching of potentially problematic trace metals, and rapid rates of
calcite precipitation which smother benthic habitats. A 36-year dataset was
collated from the long-term ambient monitoring of physicochemical parameters and
elemental concentrations of samples from two steel slag leachate-affected
watercourses in northern England. Waters were typified by elevated pH (> 10), high
alkalinity, and were rich in dissolved metals (e. g. calcium (Ca), aluminium (Al),
and zinc (Zn)). Long-term trend analysis was performed upon pH, alkalinity, and Ca
concentration which, in addition to Ca flux calculations, were used to highlight
the longevity of pollution arising as a result of the dumping and subsequent
leaching of steel slags. Declines in calcium and alkalinity have been modest over
the monitoring period and not accompanied by significant declines in water pH. If
the monotonic trends of decline in alkalinity and calcium continue in the largest
of the receiving streams, it will be in the region of 5080 years before calcite
precipitation would be expected to be close to baseline levels, where ecological
impacts would be negligible.
C1 [Riley, Alex L.; Mayes, William M.] Univ Hull, Ctr Environm & Marine Sci,
Scarborough YO11 3AZ, England.
C3 University of Hull
RP Riley, AL (corresponding author), Univ Hull, Ctr Environm & Marine Sci,
Scarborough YO11 3AZ, England.
EM A.Riley@2014.hull.ac.uk
RI Mayes, William/ABA-8647-2021; Riley, Alex/AAA-6550-2021
OI Mayes, William/0000-0002-1864-9057; Riley, Alex/0000-0001-5086-6636
FU Natural Environment Research Council [NE/K015648/1, NE/L014211/1];
Natural Environment Research Council [NE/L014211/1, NE/K015648/1,
NE/L01405X/1] Funding Source: researchfish; NERC [NE/K015648/1,
NE/L014211/1, NE/L01405X/1] Funding Source: UKRI
FX This work was funded by the Natural Environment Research Council under
grants NE/K015648/1 and NE/L014211/1. The authors would like to thank
the Environment Agency for provision of long-term elemental and rainfall
data, as well as the Centre for Ecology and Hydrology for the issuing of
gauged daily flow data. Bob Knight and Victor Uchenna Oty are thanked
for laboratory analyses. We are also grateful for assistance with field
sampling from Carl Thomas, Aron Anton, Katherine Abel, Alexandra
Harrison, Lorna Nicholson and Thomas Shard.
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NR 60
TC 45
Z9 46
U1 3
U2 30
PU SPRINGER
PI DORDRECHT
SN 0167-6369
EI 1573-2959
J9 ENVIRON MONIT ASSESS
JI Environ. Monit. Assess.
PD JUL
PY 2015
VL 187
IS 7
AR 463
DI 10.1007/s10661-015-4693-1
PG 16
GA CM0AL
UT WOS:000357340500071
PM 26108748
OA Green Submitted, Green Published, hybrid
DA 2023-12-05
ER
PT J
AU Komljenovic, MM
Bascarevic, Z
Marjanovic, N
Nikolic, V
AF Komljenovic, Miroslav M.
Bascarevic, Zvezdana
Marjanovic, Natasa
Nikolic, Violeta
TI Decalcification resistance of alkali-activated slag
LA English
DT Article
DE Alkali-activated slag; Decalcification; Accelerated leaching
ID CEMENT-BASED MATERIALS; C-S-H; CALCIUM SILICATE HYDRATE; BLAST-FURNACE
SLAG; AGGRESSIVE ENVIRONMENTS; ALUMINUM INCORPORATION;
RADIOACTIVE-WASTES; PASTES ALTERATION; STRESS-CORROSION; ORGANIC-ACIDS
AB This paper analyses the effects of decalcification in concentrated 6 M NH4NO3
solution on mechanical and microstructural properties of alkali-activated slag
(AAS). Portland-slag cement (CEM II/A-S 42.5 N) was used as a benchmark material.
Decalcification process led to a decrease in strength, both in AAS and in CEM II,
and this effect was more pronounced in CEM II. The decrease in strength was
explicitly related to the decrease in Ca/Si atomic ratio of C-S-H gel. A very low
ratio of Ca/Si similar to 0.3 in AAS was the consequence of coexistence of C-S-H(I)
gel and silica gel. During decalcification of AAS almost complete leaching of
sodium and tetrahedral aluminum from C-S-H(I) gel also took place. AAS showed
significantly higher resistance to decalcification in relation to the benchmark CEM
II due to the absence of portlandite, high level of polymerization of silicate
chains, low level of aluminum for silicon substitution in the structure of C-S-
H(1), and the formation of protective layer of polymerized silica gel during
decalcification process. In stabilization/solidification processes alkali-activated
slag represents a more promising solution than Portland-slag cement due to
significantly higher resistance to decalcification. (C) 2012 Elsevier B.V. All
rights reserved.
C1 [Komljenovic, Miroslav M.; Bascarevic, Zvezdana; Marjanovic, Natasa; Nikolic,
Violeta] Univ Belgrade, Inst Multidisciplinary Res, Belgrade 11030, Serbia.
C3 University of Belgrade
RP Komljenovic, MM (corresponding author), Univ Belgrade, Inst Multidisciplinary
Res, Kneza Viseslava 1, Belgrade 11030, Serbia.
EM miroslav.komljenovic@imsi.rs; zvezdana@imsi.bg.ac.rs;
natasa@imsi.bg.ac.rs; violeta@imsi.bg.ac.rs
RI Miroslav, Komljenovic/H-8557-2019
OI Miroslav, Komljenovic/0000-0001-5322-6984; Nikolic,
Violeta/0000-0003-0933-3197; Dzunuzovic, Natasa/0000-0001-9548-114X
FU Ministry of Education and Science of the Republic of Serbia; [TR34026]
FX This work was carried out within the project TR34026. The authors are
grateful to the Ministry of Education and Science of the Republic of
Serbia for financial support. We thank Dr. Aleksandra Rosic (Faculty of
Mining and Geology, Belgrade University) for XRD analysis.
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NR 66
TC 45
Z9 49
U1 3
U2 58
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD SEP 30
PY 2012
VL 233
BP 112
EP 121
DI 10.1016/j.jhazmat.2012.06.063
PG 10
GA 998ZB
UT WOS:000308277800015
PM 22818592
DA 2023-12-05
ER
PT J
AU Shu, QF
AF Shu, Qifeng
TI A Viscosity Estimation Model for Molten Slags in
Al2O3-CaO-MgO-SiO2 System
LA English
DT Article
DE viscosity; estimation model; aluminosilicate melts
ID SILICATE MELTS; ALUMINOSILICATE MELTS; STRUCTURAL ROLE; ALUMINUM
AB A model for viscosity estimation of molten slags in the Al2O3-CaO-MgO-SiO2
system is presented in this work. The model is an extension to the viscosity
estimation model of molten slags in the CaO-FeO-MgO-MnO-SiO2 system developed
before by the present author. The present model has explicitly taken charge
compensation into consideration. It is postulated that AI exists in a structural
unit MAl2O4 when MO/ Al2O3 > 1 for the Al2O3-MO-SiO2 system (MO=CaO, MgO). MAl2O4
has a similar behaviour as SiO2, i.e. it can form an Al-O-Al network and be
depolymerised by network modifying oxides (CaO, MgO). The present model is applied
in viscosity estimation of some slags within the Al2O3-CaO-MgO-SiO2 system. A mean
deviation of less than 25% is achieved for the present model.
C1 Beijing Univ Sci & Technol, Dept Phys Chem Met, Sch Met & Ecol Engn, Beijing
RP Shu, QF (corresponding author), Beijing Univ Sci & Technol, Dept Phys Chem Met,
EM Shuqifeng@gmail.com
RI Shu, Qifeng/AGO-3293-2022
OI Shu, Qifeng/0000-0001-5434-3314
FU NSFC [50704002]
FX The financial support froth NSFC (No. 50704002) is gratefully
acknowledged.
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LA English
DT Article
ID CALCIUM ALUMINOSILICATE GLASSES; COORDINATION; NMR
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glasses. This leads to a reactivity reduction.
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PU THOMAS TELFORD SERVICES LTD
PI LONDON
PA THOMAS TELFORD HOUSE, 1 HERON QUAY, LONDON E14 4JD, ENGLAND
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PD JAN
PY 2004
VL 16
IS 1
BP 1
EP 7
DI 10.1680/adcr.16.1.1.36257
PG 7
GA 800YS
UT WOS:000220064200001
DA 2023-12-05
ER
PT J
AU El-Mahallawy, N
Taha, MA
Jarfors, AEW
Fredriksson, H
AF El-Mahallawy, N
Taha, MA
Jarfors, AEW
Fredriksson, H
TI On the reaction between aluminium, K2TiF6 and
KBF4
LA English
DT Article
DE metal matrix composites; Al-based MMC; processing
ID METAL-MATRIX COMPOSITES; FIBROUS PREFORMS; PURE METAL; INFILTRATION; AL;
ALLOY
AB The reaction between molten Al and KBF4 and K2TiF6 was analysed. Additions of
the two salts separately, consecutively and simultaneously were made at 800 and
1000 degrees C. The phases formed were identified and their morphology
investigated. When adding K2TiF6 emulsification of the salt occurs. Residual salt
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an emulsified region, a new globular morphology of Al3Ti-type was found. No
evidence of emulsification of KBF4 was found. This implies that the two salts react
individually with Al. A new morphology of A1B(2), in the form of thin plates,
formed presumably at the salt/aluminium interface. was also found. (C) 1999
Published by Elsevier Science S.A. All rights reserved.
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Ain Shams Univ, Fac Engn, Cairo, Egypt.
C3 Royal Institute of Technology; Egyptian Knowledge Bank (EKB); Ain Shams
University
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Stockholm, Sweden.
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U1 0
U2 21
PI LAUSANNE
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PD NOV 15
PY 1999
VL 292
IS 1-2
BP 221
EP 229
DI 10.1016/S0925-8388(99)00294-7
PG 9
GA 253MD
UT WOS:000083559600035
DA 2023-12-05
ER
PT J
AU Li, J
Yu, QJ
Huang, HL
Yin, SH
AF Li, Jing
Yu, Qijun
Huang, Haoliang
Yin, Suhong
TI Effects of Ca/Si Ratio, Aluminum and Magnesium on the Carbonation
Behavior of Calcium Silicate Hydrate
SO MATERIALS
LA English
DT Article
DE C-S-H; Ca/Si ratio; Al/Si ratio; Mg/Si ratio; carbonation behavior
ID C-S-H; STRUCTURAL FEATURES; SLAG CONCRETE; PART II; CEMENT; FRESH;
MODEL; NMR; TOBERMORITE; C-S-H(I)
AB The effects of Ca/Si ratio, aluminum and magnesium on the carbonation behavior
of calcium silicate hydrate (C-S-H) were investigated by using X-ray powder
diffraction (XRD), nuclear magnetic resonance (NMR) and thermogravimetric analyzer
(TGA). The results showed that the Ca/Si ratio, Al/Si ratio and Mg/Si ratio had a
significant influence on the structure, carbonation products and carbonation
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appeared when magnesium uptake in C-S-H. The carbonation product of C-S-H was
vaterite if the Ca/Si ratio was lower than 0.87. The carbonation products of C-S-H
were vaterite and calcite if the Ca/Si ratio was higher than 1.02. C-M-S-H had more
polymerized units, stronger bond strength and better carbonation resistance than C-
S-H.
C1 [Li, Jing; Yu, Qijun; Huang, Haoliang; Yin, Suhong] South China Univ Technol,
Sch Mat Sci & Engn, Guangzhou 510640, Guangdong, Peoples R China.
C3 South China University of Technology
RP Yin, SH (corresponding author), South China Univ Technol, Sch Mat Sci & Engn,
Guangzhou 510640, Guangdong, Peoples R China.
EM Jing-Li@hotmail.com; concyuq@scut.edu.cn; h.l.huang@msn.com;
imshyin@scut.edu.cn
RI Huang, Haoliang/C-8986-2013
OI Li, Jing/0000-0001-7783-3367; Huang, Haoliang/0000-0002-8956-8852; ,
Jing/0000-0003-4531-5631
FU National Natural Science Foundation of China [51561135012]; Open Fund of
State Key Laboratory of High Performance Civil Engineering Materials
[2015CEM002]
FX This research was funded by National Natural Science Foundation of China
with grant number of 51561135012 and Open Fund of State Key Laboratory
of High Performance Civil Engineering Materials with grant number of
2015CEM002. The APC was funded by National Natural Science Foundation of
China (51561135012).
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NR 41
TC 44
Z9 48
U1 5
U2 80
PU MDPI
PI BASEL
SN 1996-1944
J9 MATERIALS
JI Materials
PD APR 2
PY 2019
VL 12
IS 8
AR 1268
DI 10.3390/ma12081268
PG 14
Metallurgical Engineering; Physics, Applied; Physics, Condensed Matter
SC Chemistry; Materials Science; Metallurgy & Metallurgical Engineering;
Physics
GA HX9ZI
UT WOS:000467767400074
PM 31003418
DA 2023-12-05
ER
PT J
AU Wang, L
Liu, WZ
Hu, JP
Liu, Q
Yue, HR
Liang, B
Zhang, GQ
Luo, DM
Xie, HP
Li, C
AF Wang, Lin
Liu, Weizao
Hu, Jingpeng
Liu, Qiang
Yue, Hairong
Liang, Bin
Zhang, Guoquan
Luo, Dongmei
Xie, Heping
Li, Chun
TI Indirect mineral carbonation of titanium-bearing blast furnace slag
coupled with recovery of TiO2 and Al2O3
SO CHINESE JOURNAL OF CHEMICAL ENGINEERING
LA English
DT Article
DE Mineral carbonation; CO2 sequestration; Ti-bearing blast furnace slag;
Ammonium sulphate; Titanium dioxide; Aluminium oxide
ID CO2 SEQUESTRATION; WOLLASTONITE CARBONATION; STEELMAKING SLAGS;
MECHANISMS; DISSOLUTION; SERPENTINE; ACTIVATION; EXTRACTION; GYPSUM
AB Large quantities of CO2 and blast furnace slag are discharged in the iron and
steel industry. Mineral carbonation of blast furnace slag can offer substantial CO2
emission reduction and comprehensive utilization of the solid waste. This paper
describes a novel route for indirect mineral carbonation of titanium-bearing blast
furnace (TBBF) slag, in which the TBBF slag is roasted with recyclable (NH4)(2)SO4
(AS) at low temperatures and converted into the sulphates of various valuable
metals, including calcium, magnesium, aluminium and titanium. High value added Ti-
and Al-rich products can be obtained through stepwise precipitation of the leaching
solution from the roasted slag. The NH3 produced during the roasting is used to
capture CO2 from flue gases. The NH4HCO3 and (NH4)(2)CO3 thus obtained are used to
carbonate the CaSO4-containing leaching residue and MgSO4-rich leaching solution,
respectively. In this study, the process parameters and efficiency for the
roasting, carbonation and Ti and Al recovery were investigated in detail. The
results showed that the sulfation ratios of calcium, magnesium, titanium and
aluminium reached 92.6%, 87% and 84.4%, respectively, after roasting at an AS-to-
TBBF slag mass ratio of 2: 1 and 350 degrees C for 2 h. The leaching solution was
subjected to hydrolysis at 102 degrees C for 4 h with a Ti hydrolysis ratio of
95.7% and the purity of TiO2 in the calcined hydrolysate reached 98 wt%. 99.7% of
aluminium in the Ti-depleted leaching solution was precipitated by using NH3. The
carbonation products of Ca and Mg were CaCO3 and (NH4)(2)Mg(CO3)(2) center dot
4H(2)O, respectively. The latter can be decomposed into MgCO3 at 100-200 degrees
Cwith simultaneous recovery of the NH3 for reuse. In this process, approximately
82.1% of Ca and 84.2% of Mg in the TBBF slag were transformed into stable
carbonates and the total CO2 sequestration capacity per ton of TBBF slag reached up
to 239.7 kg. The TiO2 obtained can be used directly as an end product, while the
Al-rich precipitate and the two carbonation products can act, respectively, as raw
materials for electrolytic aluminium, cement and light magnesium carbonate
production for the replacement of natural resources. (C) 2017 The Chemical Industry
and Engineering Society of China, and Chemical Industry Press. All rights reserved.
C1 [Wang, Lin; Liu, Weizao; Hu, Jingpeng; Liu, Qiang; Yue, Hairong; Liang, Bin;
Zhang, Guoquan; Luo, Dongmei; Xie, Heping; Li, Chun] Sichuan Univ, Coll Chem Engn,
Chengdu 610065, Sichuan, Peoples R China.
EM lic@scu.edu.cn
RI Liu, Weizao/K-5038-2019; Liang, Bin/JHU-0581-2023; yue,
Hairong/D-1874-2013
OI Liu, Weizao/0000-0003-0976-2864; Xie, Heping/0000-0002-1686-7827
FU National Key Projects for Fundamental Research and Development of China
[2016YFB0600904]
FX Supported by the National Key Projects for Fundamental Research and
Development of China (2016YFB0600904).
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NR 40
TC 44
Z9 49
U1 9
U2 96
PU CHEMICAL INDUSTRY PRESS
PI BEIJING
PA NO. 3 HUIXINLI CHAOYANGQU, BEIJING 100029, PEOPLES R CHINA
SN 1004-9541
EI 2210-321X
J9 CHINESE J CHEM ENG
JI Chin. J. Chem. Eng.
PD MAR
PY 2018
VL 26
IS 3
BP 583
EP 592
DI 10.1016/j.cjche.2017.06.012
PG 10
SC Engineering
GA GC0UG
UT WOS:000429492800020
DA 2023-12-05
ER
PT J
AU Huang, XH
Liao, JL
Zheng, K
Hu, HH
Wang, FM
Zhang, ZT
AF Huang, X. H.
Liao, J. L.
Zheng, K.
Hu, H. H.
Wang, F. M.
Zhang, Z. T.
TI Effect of B2O3 addition on viscosity of mould slag
containing low silica content
LA English
DT Article
DE Viscosity; B2O3; Break temperature; FTIR
ID BORATE GLASSES; RAMAN; TRANSFORMATION; BEHAVIOR; SPECTRA; FLUXES; MELTS;
AL; SI
AB The viscosity of SiO2-30Al(2)O(3)-B2O3-12Na(2)O-CaO slag system (CaO/SiO2=2.68-
7.35, B2O3=0-9 wt-%) was investigated in the present study. The objective is to
study the influence of B2O3 on the viscosity and structure of mould slags
containing low silica content. The research of the low silica slag system is
meaningful because of it is less reactive with Al during continuous casting of
steels containing high amounts of dissolved aluminium, such as transformation
induced plasticity assisted steels. The viscosities of these quinternary slags
decreased slightly with an increase in the content of additive B2O3 above the break
temperature. The apparent activation energy of viscous flow was found to decrease
with increasing B2O3 content. The break temperature also decreased with increasing
B2O3 content. Based on the experimental data, the decrease in break temperature per
mol.-% B2O3 Delta T-br is 15.23 K. An empirical model was then established to
predict the break temperature of mould slags containing B2O3, and the deviation is
between 225 and +25 K. Based on the viscosity and Fourier transform infrared
analysis, it is proposed that the three-coordinated boron is dominated in these
slags over the entire compositional range, and the borosilicate networks are
loosened with increasing B2O3 content in the present study. The Riboud model was
modified empirically based on the present experimental data, and the mean deviation
is similar to 13%.
C1 [Huang, X. H.] China Univ Min & Technol, Fac Resources & Safety Engn, Beijing
[Liao, J. L.; Zheng, K.; Zhang, Z. T.] Peking Univ, Beijing Key Lab Solid Waste
Utilizat & Management, Coll Engn, Beijing 100871, Peoples R China.
[Liao, J. L.] Aluminum Corp China, Beijing 100082, Peoples R China.
[Hu, H. H.; Wang, F. M.] Univ Sci & Technol Beijing, Dept Phys Chem, Beijing
C3 China University of Mining & Technology; Peking University; Aluminum
Corporation of China (CHALCO); University of Science & Technology
Beijing
RP Zhang, ZT (corresponding author), Peking Univ, Beijing Key Lab Solid Waste
Utilizat & Management, Coll Engn, Beijing 100871, Peoples R China.
EM zuotaizhang@pku.edu.cn
OI Zhang, Zuotai/0000-0002-3580-6018
FU Common Development Fund of Beijing; National Natural Science Foundation
of China [50902003, 51172003]; National High Technology Research and
Development Program of China (863 Program) [2012AA06A114]; Key Projects
in the National Science & Technology Pillar Program [2011BAB03B02,
2011BAB02B05]
FX The authors gratefully acknowledge financial support by the Common
Development Fund of Beijing and the National Natural Science Foundation
of China (grant nos. 50902003 and 51172003). Supports by the National
High Technology Research and Development Program of China (863 Program,
grant no. 2012AA06A114) and Key Projects in the National Science &
Technology Pillar Program (grant nos. 2011BAB03B02 and 2011BAB02B05) are
also acknowledged.
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NR 27
TC 44
Z9 46
U1 0
U2 30
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD JAN
PY 2014
VL 41
IS 1
BP 67
EP 74
DI 10.1179/1743281213Y.0000000107
PG 8
GA AE6OZ
UT WOS:000334114700011
DA 2023-12-05
ER
PT J
AU Giannopoulou, I
Dimas, D
Maragkos, I
Panias, D
AF Giannopoulou, I.
Dimas, D.
Maragkos, I.
Panias, D.
TI UTILIZATION OF METALLURGICAL SOLID BY-PRODUCTS FOR THE DEVELOPMENT OF
INORGANIC POLYMERIC CONSTRUCTION MATERIALS
SO GLOBAL NEST JOURNAL
LA English
CT 2nd International Conference on Engineering for Waste Valorisation
(WasteEng 2008)
CY JUN 03-05, 2008
CL Patras, GREECE
DE geopolymerization; geopolymers; red mud; ferronickel slag
ID F FLY-ASH; GEOPOLYMERIC MATERIALS; METALS
AB This paper deals with the geopolymerization of the red mud generated in the
primary aluminium production and the slag generated in the ferronickel production,
in order to develop inorganic polymeric materials with advanced mechanical and
physical properties. In particular, the effect of the main synthesis parameters of
the inorganic polymeric materials on their mechanical strength and water absorption
was investigated. Moreover, the structure of the inorganic polymeric materials was
studied according to X-ray Diffraction analysis, Fourier Transform Infra Red
spectroscopy and Scanning Electronic Microscopy. The inorganic polymeric materials
produced by the geopolymerization of the red mud developed compressive strength up
to 21 MPa and presented water absorption lower than 3 %, while the
geopolymerization of the ferronickel slag resulted in materials with compressive
strength higher than 110 MPa and extremely low water absorption (< 1 %). According
to these results, the developed materials may be viewed as alternatives in the
industrial sectors of construction and building materials.
C1 [Giannopoulou, I.; Dimas, D.; Maragkos, I.; Panias, D.] Natl Tech Univ Athens,
Sch Min & Met Engn, Met Lab, Athens 15780, Greece.
RP Panias, D (corresponding author), Natl Tech Univ Athens, Sch Min & Met Engn, Met
Lab, Iroon Polytech 9, Athens 15780, Greece.
EM panias@metal.ntua.gr
RI Giannopoulou, Ioanna/AAL-5169-2021; Panias, Dimitrios/AAO-1296-2021
OI Giannopoulou, Ioanna/0000-0003-2528-919X
10.1016/j.cemconres.2004.06.031
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GIANNOPOULOU I, 2008, P 1 PANH C BUILD MAT, P1733
8846(98)00243-9
10.1016/j.colsurfa.2006.12.064
NR 17
TC 44
Z9 46
U1 0
U2 8
PU GLOBAL NETWORK ENVIRONMENTAL SCIENCE & TECHNOLOGY
PI ATHENS
PA 30 VOULGAROKTONOU STR, ATHENS, GR 114 72, GREECE
SN 1790-7632
J9 GLOBAL NEST J
JI Glob. Nest. J.
PD JUL
PY 2009
VL 11
IS 2
SI SI
BP 127
EP 136
PG 10
GA 545SS
UT WOS:000273757700003
DA 2023-12-05
ER
PT J
AU Yilmaz, S
Kutmen-Kalpakli, Y
Yilmaz, E
AF Yilmaz, Suat
Kutmen-Kalpakli, Yasemen
Yilmaz, Ersan
TI Synthesis and characterization of boehmitic alumina coated graphite by
sol-gel method
LA English
DT Article
DE Sol-gel coating; Alumina; Graphite; TG analysis
ID OXIDATION RESISTANCE
AB Non-wettability property makes graphite a good protecting material against the
molten metal and/or slag. Properties like high oxidation potential between 600 and
1200 degrees C and non-wettability with water at room temperatures limits the usage
of graphite in castable refractory applications. In this study, sol-gel method,
which is a relatively cheaper process, was used. Boehmitic sol was obtained by
hydrolyzing and peptiziting the alkoxide AIP (aluminum isopropoxide) used as
alumina source. Then natural flake graphite was mixed with the boehmitic solution
for coating of graphite. At 120 degrees C boehmitic sol coated graphite was dried
and gelled. Then heat threaded at 550 degrees C for gamma-Al2O3 transformation of
boehmite. Products that obtained from the studies were characterized with FTIR and
XRD tests. Alumina coated graphite samples were made by repeating the same steps
and TG analysis were made to investigate the oxidation behaviour of the samples.
Finally, SEM-EDS analyses were carried out to investigate the microscopic
properties of the alumina coated graphite powders. (C) 2008 Elsevier Ltd and Techna
Group S.r.l. All rights reserved.
C1 [Yilmaz, Suat; Yilmaz, Ersan] Istanbul Univ, Dept Met & Mat Engn, TR-34320
Avcilar, Turkey.
[Kutmen-Kalpakli, Yasemen] Yildiz Tech Univ, Dept Chem Engn, Davutpasa, Turkey.
C3 Istanbul University; Yildiz Technical University
RP Yilmaz, S (corresponding author), Istanbul Univ, Dept Met & Mat Engn, TR-34320
Avcilar, Turkey.
EM syilmaz@istanbul.edu.tr
RI YILMAZ, Suat/D-4731-2019; YILMAZ, SUAT/HPG-4444-2023; Kalpakli, Yasemen
Kutmen/AAG-5511-2019
OI YILMAZ, Suat/0000-0002-6092-9319; Kalpakli, Yasemen
Kutmen/0000-0002-1300-2289
FU TUBITAK (The Scientific and Technological Research Council of Turkey)
[106M318]; Research Fund of Istanbul University [UDP 2391]; METAMIN Inc.
in Istanbul
FX This work was supported by TUBITAK (The Scientific and Technological
Research Council of Turkey) with Project Nr.: 106M318, by Research Fund
of Istanbul University with Project Nr.: UDP 2391 and by METAMIN Inc. in
Istanbul.
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NR 19
TC 44
Z9 48
U1 0
U2 46
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD JUL
PY 2009
VL 35
IS 5
BP 2029
EP 2034
DI 10.1016/j.ceramint.2008.11.006
PG 6
GA 452FE
UT WOS:000266524700043
DA 2023-12-05
ER
PT J
AU Sheibani, S
Najafabadi, MF
AF Sheibani, S.
Najafabadi, M. Fazel.
TI In situ fabrication of Al-TiC metal matrix composites by reactive slag
process
LA English
DT Article
ID PART I; ALUMINUM; SOLIDIFICATION
AB The possibility of in situ fabrication of Al-TiC composite using reactive slag
process is studied in the present paper. Commercial pure aluminum, cryolite,
titanium oxide and graphite have been used. Aluminum was melted by an induction
furnace and then a mixture of salts powder was added to it. Specimens of aluminum
matrix composites containing various percentages of TiCs were prepared.
Microstructure, mechanical properties and phase analysis of specimens were
examined. Results obtained showed that, in situ fabrication of TiC reinforcement in
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shape rather than as a particle. (C) 2006 Elsevier Ltd. All rights reserved.
C1 Univ Tehran, Dept Met & Mat Engn, Fac Engn, Tehran, Iran.
C3 University of Tehran
RP Sheibani, S (corresponding author), Univ Tehran, Dept Met & Mat Engn, Fac Engn,
POB 14395-553, Tehran, Iran.
EM Sheibani_s@engmail.ut.ac.ir
RI Sheibani, Saeed/C-5222-2018
OI Sheibani, Saeed/0000-0002-6124-3386
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PU ELSEVIER SCI LTD
PI OXFORD
SN 0261-3069
J9 MATER DESIGN
JI Mater. Des.
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BP 2373
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DA 2023-12-05
ER
PT J
AU Bamigboye, GO
Bassey, DE
Olukanni, DO
Ngene, B
Adegoke, D
Odetoyan, AO
Kareem, MA
Enabulele, DO
Nworgu, AT
AF Bamigboye, Gideon O.
Bassey, Daniel E.
Olukanni, David O.
Ngene, Ben U.
Adegoke, Dunmininu
Odetoyan, Abimbola O.
Kareem, Mutiu A.
Enabulele, David O.
Nworgu, Austin T.
TI Waste materials in highway applications: An overview on generation and
utilization implications on sustainability
LA English
DT Article
DE Construction materials; Sustainable materials; Pavement performance;
Compressive strength; Economic impact analysis; Recycled waste materials
ID LIFE-CYCLE ASSESSMENT; CEMENT KILN DUST; FURNACE STEEL SLAG; ASPHALT
MIXTURES; CRUMB RUBBER; RECYCLED MATERIALS; ALUMINUM DROSS; MINE
TAILINGS; BOTTOM ASH; BIO-BINDER
AB The rate at which the construction industry explores and consumes non-renewable
natural aggregates and other industrial products such as bitumen, lime, and cement
during construction and rehabilitation of road pavements has over time proven to be
environmentally degrading and non-sustainable. This, alongside the issues of high
solid waste generation and inadequate disposal, has led to series of studies by
various researchers to find methods to integrate these solid wastes as alternative
materials in road construction and maintenance. This paper provides a simple yet
detailed review of recent relevant studies conducted to understand the alarming
rate of generation and the effects of reusing these waste materials in both
flexible and rigid pavements. The review further outlines the advantages and
disadvantages of the selected waste materials and compare the results with that of
conventional materials in accordance with relevant standards while highlighting the
performance, and life cycle environmental and economic sustainability implications.
The study shows that the adoption of these materials offers efficiency in waste
disposal while reducing the demand for natural aggregates and consequently,
significantly reducing life cycle impacts and costs. The challenges limiting the
effective practical implementation of these waste recycling techniques in the
construction industry were discussed and possible solutions were suggested to
encourage and ensure its utilization in road construction. (C) 2020 Elsevier Ltd.
C1 [Bamigboye, Gideon O.; Bassey, Daniel E.; Olukanni, David O.; Ngene, Ben U.;
Adegoke, Dunmininu; Odetoyan, Abimbola O.; Enabulele, David O.; Nworgu, Austin T.]
Covenant Univ, Dept Civil Engn, Ota, Ogun State, Nigeria.
[Kareem, Mutiu A.] Osun State Univ, Dept Civil Engn, Osogbo, Nigeria.
C3 Covenant University
RP Bamigboye, GO (corresponding author), Covenant Univ, Dept Civil Engn, Ota, Ogun
State, Nigeria.
EM gideon.bamigboye@covenantuniversity.edu.ng
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NR 214
TC 43
Z9 44
U1 7
U2 59
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD FEB 10
PY 2021
VL 283
AR 124581
DI 10.1016/j.jclepro.2020.124581
EA JAN 2021
PG 33
& Ecology
GA PU0XD
UT WOS:000609032200011
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Huseien, GF
Ismail, M
Tahir, MM
Mirza, J
Khalid, NHA
Asaad, MA
Husein, AA
Sarbini, NN
Ismail, Mohammad
Tahir, Mahmood Md.
Mirza, Jahangir
Khalid, Nur Hafizah A.
Asaad, Mohammad Ali
Husein, Ahmed Abdulameer
Sarbini, Noor Nabilah
TI Synergism between palm oil fuel ash and slag: Production of
environmental-friendly alkali activated mortars with enhanced properties
LA English
DT Article
DE Alkali activated mortar; POFA; GBFS; Alkaline solution;
Envirmental-friendly mortar
ID FLY-ASH; COMPRESSIVE STRENGTH; GEOPOLYMER MORTAR; MICROSTRUCTURAL
ANALYSIS; PERFORMANCE
AB Environmental concern raised by the production of ordinary Portland cement
(OPC), is behind the search for greener construction materials and remediation. One
such material is alkali activated mortars (AAMs). It is well known that the high
molarity of sodium hydroxide (12-16 M) and high content of sodium silicate (sodium
silicate to sodium hydroxide higher than 2.5) have negative impacts on the
environment. Driven by this idea, we prepared some binary alkali activated mortars
by combining palm oil fuel ash (POFA) and ground blast furnace slag (GBFS) at
varying ratios. The effect of low concentration alkaline solution on the fresh,
mechanical and durable properties of alkali activated was determined. The ratio of
sodium hydroxide (molarity 4 M) (NH) to sodium silicate (NS) in the mixture was
kept at 0.75. Microstructures of the prepared alkali activated mortars were
analyzed using SEM, XRD and FTIR measurements. The achieved high strength
(approximate to 72 MPa at age of 28 days) of the alkali activated mortars was
attributed to the synergy between GBFS and POFA. Partial replacement of GBFS with
POFA was demonstrated to be beneficial for improving the compressive strength,
durability and resistance against sulphuric acid attack. Meanwhile, calcium
aluminium silicate hydrate (CASH) gel was discerned to be the main reaction product
of POFA and GBFS in these binary systems. It was established that the proposed AAMs
can contribute towards the development of sustainable materials. (C) 2018 Elsevier
C1 [Huseien, Ghasan Fahim; Tahir, Mahmood Md.] Univ Teknol Malaysia, Inst Smart
Infrastruct & Innovat Construct, Fac Civil Engn, Skudai, Johor Bahru, Malaysia.
[Huseien, Ghasan Fahim; Ismail, Mohammad; Khalid, Nur Hafizah A.; Asaad,
Mohammad Ali; Husein, Ahmed Abdulameer; Sarbini, Noor Nabilah] Univ Teknol
Malaysia, Fac Civil Engn, Utm Johor Bahru 81310, Johor, Malaysia.
[Mirza, Jahangir] Hydro Quebec Res Inst, Dept Mat Sci, 1800 Mte Ste Julie,
C3 Universiti Teknologi Malaysia; Universiti Teknologi Malaysia;
Hydro-Quebec
RP Ismail, M (corresponding author), Univ Teknol Malaysia, Fac Civil Engn, Utm
Johor Bahru 81310, Johor, Malaysia.
EM mohammad@utm.my
RI Khalid, Nur Hafizah Abd/AAR-6404-2020; Huseien, Ghasan
Fahim/AEC-3508-2022; Mirza, Jahangir/HOF-8557-2023; SARBINI, NOOR
NABILAH BINTI/ABH-2659-2020; Ismail, Mohammad/F-9868-2011
OI Huseien, Ghasan Fahim/0000-0002-2963-0335; Mirza,
Jahangir/0000-0002-3783-8048; Ismail, Mohammad/0000-0002-0264-6476; Abd
Khalid, Nur Hafizah/0000-0002-1728-3313
FU UTM, Johor Bahru, Malaysia [16H94]; Malaysian Ministry of Education
[4B322, 15JO8, 4Y117]; MOSTI Grant [4S090]
FX The authors are grateful to UTM, Johor Bahru, Malaysia for their
financial support Grant no 16H94 and also The Malaysian Ministry of
Education for their financial support through, Grant no 4B322, 15JO8 and
4Y117 and MOSTI Grant no 4S090.
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NR 31
TC 43
Z9 43
U1 0
U2 20
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD MAY 10
PY 2018
VL 170
BP 235
EP 244
DI 10.1016/j.conbuildmat.2018.03.031
PG 10
GA GE4BB
UT WOS:000431158200023
DA 2023-12-05
ER
PT J
AU Yliniemi, J
Kinnunen, P
Karinkanta, P
Illikainen, M
AF Yliniemi, Juho
Kinnunen, Paivo
Karinkanta, Pasi
Illikainen, Mirja
TI Utilization of Mineral Wools as Alkali-Activated Material Precursor
SO MATERIALS
LA English
DT Article
DE geopolymer; alkali activation; mineral wool; rock wool; glass wool;
mmmf: man-made mineral fibre
ID SLAG; TEMPERATURE; IMMOBILIZATION; GEOPOLYMERS; WASTE; GELS
AB Mineral wools are the most common insulation materials in buildings worldwide.
However, mineral wool waste is often considered unrecyclable because of its fibrous
nature and low density. In this paper, rock wool (RW) and glass wool (GW) were
studied as alkali-activated material precursors without any additional co-binders.
Both mineral wools were pulverized by a vibratory disc mill in order to remove the
fibrous nature of the material. The pulverized mineral wools were then alkali-
activated with a sodium aluminate solution. Compressive strengths of up to 30.0 MPa
and 48.7 MPa were measured for RWandGW, respectively, with high flexural strengths
measured for both (20.1 MPa for RW and 13.2 MPa for GW). The resulting alkali-
activated matrix was a composite-type in which partly-dissolved fibers were
dispersed. In addition to the amorphous material, sodium aluminate silicate
hydroxide hydrate and magnesium aluminum hydroxide carbonate phases were identified
in the alkali-activated RW samples. The only crystalline phase in the GW samples
was sodium aluminum silicate. The results of this study show that mineral wool is a
very promising raw material for alkali activation.
C1 [Yliniemi, Juho; Kinnunen, Paivo; Karinkanta, Pasi; Illikainen, Mirja] Univ
Oulu, Fiber & Particle Engn Res Unit, Oulu 90014, Finland.
C3 University of Oulu
RP Yliniemi, J (corresponding author), Univ Oulu, Fiber & Particle Engn Res Unit,
Oulu 90014, Finland.
EM juho.yliniemi@oulu.fi; paivo.kinnunen@oulu.fi; pasi.karinkanta@oulu.fi;
mirja.illikainen@oulu.fi
RI Kinnunen, Paivo/I-3430-2012
OI Kinnunen, Paivo/0000-0001-8490-1890; Yliniemi, Juho/0000-0003-0013-8598;
Illikainen, Mirja/0000-0001-7545-4574
FU Ekokem Environmental Stipend Fund
FX The authors would like to thank the Ekokem Environmental Stipend Fund
for its financial support. Kalle Hyypio, is acknowledged for his
completion of a part of the experimental work as a part of his
bachelor's thesis. Jarno Karvonen, Elisa Wirkkala and Jani Osterlund are
acknowledged for their contributions to the laboratory analyses. The
personnel of the Center of Microscopy and Nanotechnology are
acknowledged for their contributions to the FESEM and XRD analyses.
Special thanks to Arie van Riessen for the valuable advice for the
experiments.
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NR 41
TC 43
Z9 44
U1 6
U2 27
PU MDPI
PI BASEL
SN 1996-1944
J9 MATERIALS
JI Materials
PD MAY
PY 2016
VL 9
IS 5
AR 312
DI 10.3390/ma9050312
PG 12
Physics
GA DP6SG
UT WOS:000378628500007
PM 28773435
OA Green Published, Green Submitted, gold
DA 2023-12-05
ER
PT J
AU Sanchez-Segado, S
Makanyire, T
Escudero-Castejon, L
Hara, Y
Jha, A
AF Sanchez-Segado, S.
Makanyire, T.
Escudero-Castejon, L.
Hara, Y.
Jha, A.
TI Reclamation of reactive metal oxides from complex minerals using alkali
roasting and leaching - an improved approach to process engineering
SO GREEN CHEMISTRY
LA English
DT Review
ID CHROMITE ORE; RED MUD; SELECTIVE SEPARATION; CLEANER PRODUCTION;
ILMENITE ORE; KINETICS; REDUCTION; CONSTITUTION; IMPURITIES; EXTRACTION
AB In nature, the commonly occurring reactive metal oxides of titanium, chromium,
aluminium, and vanadium often chemically combine with the transition metal oxides
such as iron oxides and form complex minerals. Physico-chemical separation of
transition metal oxides from the remaining reactive metal oxides is therefore an
important step in the purification of reactive oxide constituents. Each
purification step has quite a high energy requirement at present. Current practice
in industry yields sulphate and neutralized chloride waste from titanium dioxide
enrichment, red mud from bauxite refining, slag and leach residues from vanadium
extraction and chromite ore process residue (COPR) from chromate processes. In this
review article, a novel alkali-based oxidative roasting and aqueous leaching for
the extraction of mineral oxides is explained in the context of the original work
of Le Chatelier in 1850, which was unsuccessful in the industrialization of bauxite
processing for alumina extraction. However, much later in the 19th century the
alkali-based oxidative mineral roasting was successfully developed for industrial
scale manufacturing of chromate chemicals, which yields COPR. The crystal chemistry
of mineral oxides, namely alumina, titanium dioxide, and chromium oxide in
naturally occurring minerals is briefly reviewed in the context of chemical
extraction, which is then developed as a model for developing thermodynamic
chemical equilibrium principles for analyzing the physical separation and
enrichment of such reactive metal oxides by forming water-soluble and water-
insoluble alkali complexes. The involvement of the alkali roasting chemistry of
non-magnetic titaniferous mineral waste is also reported in the initial separation
of rare-earth oxide mixtures for subsequent separation of individual oxides. The
paper concludes with a generic approach to process chemistry which minimizes waste
generation and therefore helps in reducing the overall process and energy costs.
Examples of recovering alkali from high pH solution using carbon dioxide are also
demonstrated.
C1 [Sanchez-Segado, S.; Makanyire, T.; Escudero-Castejon, L.; Hara, Y.; Jha, A.]
Univ Leeds, Inst Mat Res, Leeds LS2 9JT, W Yorkshire, England.
C3 University of Leeds
RP Sanchez-Segado, S (corresponding author), Univ Leeds, Inst Mat Res, Leeds LS2
EM a.jha@leeds.ac.uk
RI Jha, Animesh/A-3808-2009; NERC, NERC SoS Minerals/Y-4428-2018
OI Jha, Animesh/0000-0003-3150-5645; Sanchez Segado,
Sergio/0000-0002-3511-0723; Makanyire, Terence/0000-0001-9781-4518
FU consortium of UK industry; EPSRC [GR/T19889/01, GR/L95977/01]; European
Union's Marie Curie Fellowship grant; NERC's Catalyst Grant
[NE/L002280/1]; Engineering and Physical Sciences Research Council
[GR/T08074/01, GR/T19889/01, 1149064] Funding Source: researchfish;
Natural Environment Research Council [NE/M01147X/1, NE/L002280/1]
Funding Source: researchfish; NERC [NE/M01147X/1, NE/L002280/1] Funding
Source: UKRI
FX The authors acknowledge the financial support from a consortium of UK
industry and the EPSRC standard grants (GR/T19889/01 and GR/L95977/01)
and PhD studentships for research which was initiated in 1997 at the
University of Leeds. A. Jha also acknowledges the support from the
European Union's Marie Curie Fellowship grant for Dr Sanchez-Segado and
from the NERC's Catalyst Grant reference NE/L002280/1.
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NR 73
TC 43
Z9 44
U1 9
U2 98
PI CAMBRIDGE
ENGLAND
SN 1463-9262
EI 1463-9270
J9 GREEN CHEM
JI Green Chem.
PY 2015
VL 17
IS 4
BP 2059
EP 2080
DI 10.1039/c4gc02360a
PG 22
GA CF7GL
UT WOS:000352724200008
OA Green Accepted, hybrid
DA 2023-12-05
ER
PT J
AU Li, R
He, C
He, YL
AF Li, Ran
He, Chao
He, Yanling
TI Preparation and characterization of poly-silicic-cation coagulants by
synchronous-polymerization and co-polymerization
LA English
DT Article
DE Poly-silicic-cation coagulant; Synchronous-polymerization;
Co-polymerization; Coagulation performance; Industrial wastes;
Papermaking wastewater
ID METAL-POLYSILICATE COAGULANTS; REMOVAL EFFICIENCY; ALUMINUM; SULFATE;
PERFORMANCE; MECHANISM; ASH; FE
AB Poly-silicic-cation coagulants (PSiCs) were prepared from industrial wastes such
as fly ash, pyrite slag and wasted sulfuric acid by synchronous-polymerization and
co-polymerization, and were denoted as PSiCs and PSiCc respectively. Their
structures and morphologies were characterized and compared by X-ray diffraction
(XRD), infrared spectra (IR), ultraviolet/visible absorption (UVA) scanning and
microscopic imaging, and their coagulation performances were evaluated by
papermaking wastewater treatment. The results show that new complexed compounds are
formed in both PSiCs and PSiCc, but the polymerizations and conformations of Fe, Al
and Si are different between the two coagulants. Compared with PSiCs, the contents
of high polymers and ionic polymerized bonds are decreased obviously, and the
cross-copolymerization between Fe(III) and Al(III) hydroxyl polymers disappeared in
PSiCc. Morphologic analysis shows that PSiCc has fewer branch-like units than
PSiCs, and coagulation experiments indicate that PSiCs exhibits higher coagulation
efficiency in removing COD. (C) 2013 Elsevier B.V. All rights reserved.
C1 [Li, Ran] Xi An Jiao Tong Univ, Sch Life Sci & Technol, Xian 710049, Peoples R
China.
[He, Chao] Xi An Jiao Tong Univ, Sch Mech Engn, Xian 710049, Peoples R China.
[He, Yanling] Xi An Jiao Tong Univ, Sch Human Settlement & Civil Engn, Xian
C3 Xi'an Jiaotong University; Xi'an Jiaotong University; Xi'an Jiaotong
University
RP He, YL (corresponding author), Xi An Jiao Tong Univ, Sch Human Settlement &
Civil Engn, Xian 710049, Peoples R China.
EM heyl@mail.xjtu.edu.cn
FU National Science and Technology Major Special "Water Pollution Control
and Governance" Project, China [2009ZX07212-002-002]; Key Technology of
Oily Wastewater Treatment Project, China [2011KTCL03-06]
FX This study was supported by the National Science and Technology Major
Special "Water Pollution Control and Governance" Project, China (No.
2009ZX07212-002-002) and Key Technology of Oily Wastewater Treatment
Project, China (No. 2011KTCL03-06).
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NR 25
TC 43
Z9 45
U1 4
U2 75
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD MAY 1
PY 2013
VL 223
BP 869
EP 874
DI 10.1016/j.cej.2013.03.010
PG 6
SC Engineering
GA 167KP
UT WOS:000320631200099
DA 2023-12-05
ER
PT J
AU WEISS, T
SCHWERDTFEGER, K
AF WEISS, T
SCHWERDTFEGER, K
TI CHEMICAL-EQUILIBRIA BETWEEN SILICON AND SLAG MELTS
LA English
DT Article
AB The equilibria between silicon and slags of the systems CaO-SiO2, Na2O-SiO2, and
CaO-SiO2-Y with Y being Al2O3, MgO, TiO(x), B2O3, and Na2O have been investigated
in silica crucibles. The calcium content under silica-saturated CaO-SiO2 slag is
262 parts per million (ppm) at 1500-degrees-C. The aluminum and magnesium contents
increase with increasing alumina or magnesium oxide contents, respectively,
reaching about 1800 ppm Al at silica/mullite or about 390 ppm Mg at
silica/protoenstatite saturation. Boron has a distribution ratio [B]/(B2O3) of
0.18. The sodium content under silica-saturated Na2O-SiO2 slag is 25 ppm at 1500-
degrees-C. In contrast, the titanium content of the silicon, if Y is TiO(x) and
(Ti) is in the percent range, is high and varies with the titanium content of the
slag according to [wt pct Ti] = 2.7 square-root (wt pct Ti). In other experiments.
it is shown that metallurgical grade (MG) silicon can be purified from aluminum,
magnesium, and calcium by treatment with suitable silicate slags.
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NR 11
TC 43
Z9 49
U1 0
U2 4
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD AUG
PY 1994
VL 25
IS 4
BP 497
EP 504
DI 10.1007/BF02650071
PG 8
Engineering
GA PA275
UT WOS:A1994PA27500004
DA 2023-12-05
ER
PT J
AU MAEDA, M
YAHATA, T
MITUGI, K
IKEDA, T
AF MAEDA, M
YAHATA, T
MITUGI, K
IKEDA, T
TI ALUMINOTHERMIC REDUCTION OF TITANIUM-OXIDE
SO MATERIALS TRANSACTIONS JIM
LA English
DT Article
DE TITANIUM; TITANIA; ALUMINUM; ALUMINA; ALUMINOTHERMIC REDUCTION; OXYGEN;
SLAG
AB The aluminothermic reduction of titanium oxide was studied at 1973 K in an
atmosphere of argon and alumina crucible. The overall reaction,
TiO2+4/3Al=Ti+2/3Al2O3, was finished within about 10 min.
When the molar ratio of aluminum to titanium oxide (X(Al)/X(TiO2)) was 4/3
(which corresponds to the stoichiometric ratio), an alloy containing 5 mass% oxygen
and 15 mass% aluminum was obtained. If the ratio was increased, aluminum content
increased and oxygen decreased. For an intermetallic composition where 36 mass% of
aluminum is necessary, oxygen content was 1.5 mass%. The possibility of reducing
oxygen content was demonstrated by decreasing the activity of alumina in the slag.
RP MAEDA, M (corresponding author), UNIV TOKYO,INST IND SCI,7-22-1 ROPPONGI,MINATO
KU,TOKYO 106,JAPAN.
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NR 9
TC 43
Z9 44
U1 0
U2 14
PU JAPAN INST METALS
PI SENDAI
PA AOBA ARAMAKI, SENDAI 980, JAPAN
SN 0916-1821
J9 MATER T JIM
JI Mater. Trans. JIM
PD JUL
PY 1993
VL 34
IS 7
BP 599
EP 603
DI 10.2320/matertrans1989.34.599
PG 5
Engineering
GA LR937
UT WOS:A1993LR93700005
OA gold
DA 2023-12-05
ER
PT J
AU Chang, J
Xiong, C
Zhang, YY
Wang, D
AF Chang, Jun
Xiong, Cang
Zhang, Yangyang
Wang, Dan
TI Foaming characteristics and microstructure of aerated steel slag block
prepared by accelerated carbonation
LA English
DT Article
DE Steel slag; Foaming; Carbonation; Microstructure
ID C-S-H; MECHANICAL-PROPERTIES; CALCIUM-CARBONATE; QUANTITATIVE-ANALYSIS;
PORTLAND-CEMENT; FLY-ASH; HYDRATION; CONCRETE; SULFOALUMINATE; PRODUCTS
AB The present paper discusses investigated the foaming behaviors and
microstructure of three aerated steel slag block (ASSB) samples prepared with three
different foaming agents (namely animal protein, hydrogen peroxide, aluminum
powder) and by accelerated carbonation. The composition and microstructure of the
ASSB samples before and after accelerated carbonation were characterized using X-
ray diffraction (XRD), Rietveld method, thermogravimetric analysis (TGA), fourier
transform infrared spectroscopy (FT-IR) and field emission scanning electron
microscopy (FE-SEM). It is an advisable method for foamed steel slag products to
use the aluminum powder and accelerated carbonation technology. The aluminum powder
favored a good foaming behavior for steel slag owing to (i) a high porosity and low
dry density, (ii) a high hydration degree of minerals in steel slag, including
brownmillerite, larnite, and lime, which was confirmed by the analysis of mineral
compositions using Rietveld method, and (iii) the interlaced lamellas of
monocarboaluminate and calcium silicate hydrate (C-S-H) gel strengthen the bubbles
wall, which was confirmed by morphology analysis using FE-SEM. After accelerated
carbonation, the monocarboaluminate shifted to aragonite, vaterite, calcite and
amorphous aluminum hydroxide (Al(OH)(3)), which was confirmed by XRD, TGA and FT-
IR. The network skeleton formed by aragonite crystals improved the compressive
strength of ASSB prepared by aluminum powder. In addition, the reactions of the
formation and carbonation of monocarboaluminate phase were proved to be
thermodynamically possible in this work. (C) 2019 Elsevier Ltd. All rights
reserved.
C1 [Chang, Jun; Xiong, Cang; Zhang, Yangyang; Wang, Dan] Dalian Univ Technol, Sch
Civil Engn, Dalian 116024, Liaoning, Peoples R China.
C3 Dalian University of Technology
RP Wang, D (corresponding author), Dalian Univ Technol, Sch Civil Engn, Dalian
EM wangdan1991430@mail.dlut.edu.cn
RI zhang, yangyang/GZG-7467-2022
FX This work was financially supported by the National Natural Science
Foundation of China (51172096).
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NR 64
TC 42
Z9 44
U1 8
U2 76
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUN 10
PY 2019
VL 209
BP 222
EP 233
DI 10.1016/j.conbuildmat.2019.03.077
PG 12
GA HZ2XV
UT WOS:000468713000022
DA 2023-12-05
ER
PT J
AU Rivera, RM
Xakalashe, B
Ounoughene, G
Binnemans, K
Friedrich, B
Van Gerven, T
AF Rivera, Rodolfo Marin
Xakalashe, Buhle
Ounoughene, Ghania
Binnemans, Koen
Friedrich, Bernd
Van Gerven, Tom
TI Selective rare earth element extraction using high-pressure acid
leaching of slags arising from the smelting of bauxite residue
SO HYDROMETALLURGY
LA English
DT Article
DE High-pressure acid leaching; Bauxite residue; Rare earths; Red mud;
Slag; Smelting
ID RED MUD; VALUABLE METALS; RECOVERY; SILICA; IRON; TEMPERATURE; KINETICS;
SCANDIUM; ALUMINUM; OPTIMIZATION
AB During acid leaching of bauxite residue (red mud), the increase in dissolution
of rare-earth elements (REEs) is associated with a substantial co-dissolution of
iron; this poses problems in the downstream processing (i.e. solvent extraction or
ion exchange). Six different slags generated by reductive smelting of the same
bauxite residue sample were treated by high-pressure acid leaching (HPAL) with HCl
and H2SO4 to selectively extract REEs. Thus, up to 90 wt% of scandium was extracted
from the slags using H2SO4 at 150 degrees C, while with HCl the extraction of
scandium reached up to 80 wt% at 120 degrees C. The extraction of yttrium,
lanthanum and neodymium was above 95 wt% when HCl was used as a reagent, but it was
much lower ( < 20 wt%) with H2SO4, presumably due to the formation of a double
sulfate (NaLn(SO4)(2).nH(2O)) and/or due to the adsorption on the surface of
silicon/aluminium-oxides compounds. In addition, HPAL of bauxite residue slags led
to a significant co-dissolution of aluminium ( > 90 wt%, 18 g L-1), while the
concentration of the remaining iron ( > 60 wt%) was of 3 g L-1 in the leachate. The
co-dissolution of silicon and titanium was lower than 5 wt%.
C1 [Rivera, Rodolfo Marin; Ounoughene, Ghania; Van Gerven, Tom] Katholieke Univ
Leuven, Dept Chem Engn, Celestijnenlaan 200F, B-3001 Heverlee, Belgium.
[Xakalashe, Buhle; Friedrich, Bernd] Rhein Westfal TH Aachen, Inst Proc Met &
Met Recycling, D-52056 Aachen, Germany.
[Binnemans, Koen] Katholieke Univ Leuven, Dept Chem, Celestijnenlaan 200F, B-
3001 Heverlee, Belgium.
C3 KU Leuven; RWTH Aachen University; KU Leuven
RP Van Gerven, T (corresponding author), Katholieke Univ Leuven, Dept Chem Engn,
Celestijnenlaan 200F, B-3001 Heverlee, Belgium.
EM tom.vangerven@kuleuven.be
RI Van Gerven, Tom/B-5806-2015; Friedrich, Bernd/AAM-7029-2021; Rivera,
Rodolfo Marin/AAF-8783-2019; Friedrich, Bernd/AAM-7005-2021; Binnemans,
Koen/O-3242-2013
OI Van Gerven, Tom/0000-0003-2051-5696; Friedrich,
Bernd/0000-0002-2934-2034; Rivera, Rodolfo Marin/0000-0002-0169-2032;
Binnemans, Koen/0000-0003-4768-3606
FU European Community [636876]
FX The research leading to these results has received funding from the
European Community's Horizon 2020 Programme (H2020/2014-2019) under
Grant Agreement No. 636876 (MSCA- ETN REDMUD). This publication reflects
only the authors' view, exempting the Community from any liability.
Project website: http://www.etn.redmud.org. The authors thank Aluminium
of Greece for providing the bauxite residue sample.
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NR 65
TC 42
Z9 46
U1 0
U2 64
PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD MAR
PY 2019
VL 184
BP 162
EP 174
DI 10.1016/j.hydromet.2019.01.005
PG 13
GA HP1EM
UT WOS:000461408200019
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Park, T
Ampunan, V
Maeng, S
Chung, E
AF Park, Taejun
Ampunan, Vanvimol
Maeng, Sungkyu
Chung, Eunhyea
TI Application of steel slag coated with sodium hydroxide to enhance
precipitation-coagulation for phosphorus removal
SO CHEMOSPHERE
LA English
DT Article
DE Phosphorus removal; Slag; Coating; Precipitation and coagulation
ID PHOSPHATE REMOVAL; FURNACE SLAG; WATER; MECHANISMS; FILTERS; MODEL
AB Phosphorus removal has been studied for decades to reduce the environmental
impact of phosphorus in natural waterbodies. Slag has been applied for the
phosphorus removal by several mechanisms. In this study, sodium hydroxide coating
was applied on the slag surface to enhance the efficiency of precipitation-
coagulation process.
In the batch test, it was found that the capacity of the slag to maintain high
pH decreases with increasing its exposure time to the aqueous solution. In the
column test, the coarse-grained coated slag showed higher phosphorus removal
efficiency than the fine-grained uncoated slag. The coated slag maintained pH
higher than uncoated slag and, accordingly, the removal efficiency of phosphorus
was higher. Especially, when pH was less than 8, the removal efficiency decreased
significantly. However, coated slag provided an excess amount of aluminum and
sodium. Thus, a return process to reuse aluminum and sodium as a coagulant was
introduced. The return process yields longer lifespan of slag with higher
phosphorus removal and lower concentration of cations in the effluent. With the
return process, the phosphorus removal efficiency was kept higher than 60% until
150 bed volumes; meanwhile, the efficiency without return process became lower than
60% at 25 bed volumes. (C) 2016 Elsevier Ltd. All rights reserved.
C1 [Park, Taejun; Ampunan, Vanvimol; Chung, Eunhyea] Seoul Natl Univ, Dept Energy
Syst Engn, Gwanak Ro 1, Seoul 08826, South Korea.
[Maeng, Sungkyu] Sejong Univ, Dept Civil & Environm Engn, Neungdong Ro 209,
C3 Seoul National University (SNU); Sejong University
RP Chung, E (corresponding author), Seoul Natl Univ, Dept Energy Syst Engn, Gwanak
Ro 1, Seoul 08826, South Korea.
EM echung@snu.ac.kr
FU KIST Institutional Program [2E24280]; Brain Korea 21 Plus Project
[21A20130012821]
FX This work was supported by the KIST Institutional Program (Project No.
2E24280). This work was also partly supported by the Brain Korea 21 Plus
Project (Project No. 21A20130012821).
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NR 28
TC 42
Z9 47
U1 1
U2 49
PI OXFORD
SN 0045-6535
EI 1879-1298
J9 CHEMOSPHERE
JI Chemosphere
PD JAN
PY 2017
VL 167
BP 91
EP 97
DI 10.1016/j.chemosphere.2016.09.150
PG 7
GA ED0PC
UT WOS:000388543400011
PM 27710847
DA 2023-12-05
ER
PT J
AU Setiadi, A
Milestone, NB
Hill, J
Hayes, M
AF Setiadi, A.
Milestone, N. B.
Hill, J.
Hayes, M.
TI Corrosion of aluminium and magnesium in BFS composite cements
SO ADVANCES IN APPLIED CERAMICS
LA English
CT 25th Cement and Concrete Science Conference
CY SEP 15-16, 2005
CL Royal Holloway Coll, London, ENGLAND
HO Royal Holloway Coll
DE bayerite; stratlingite; corrosion; cement; brucite
ID STRATLINGITE
AB Legacy radioactive wastes arising from reprocessing of nuclear fuels in the UK
are classified as intermediate level waste ( ILW), which contain things such as
aluminium and magnesium. Blast furnace slag ( BFS) composite cements are used to
encapsulate ILW. These cements have a high pH which is advantageous to limit the
mobility of some of the radioactive species but can cause corrosion of metals. The
present paper describes some fundamental aspects of corrosion of aluminium and
magnesium in BFS composite cements.
The corrosion of aluminium produced an interface between aluminium and cement
which was porous with a series of zones containing bayerite (Al(OH)(3)) and
stratlingite ( 2CaO(center dot)Al(2)O(3 center dot)SiO(2 center dot)8H(2)O). With
magnesium, the main corrosion product was found to be brucite (Mg(OH)(2)) and the
porous zone was less pronounced. The hydration of the bulk cement did not appear to
be affected by the corrosion of these metals.
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Yorkshire, England.
UK Nirex Ltd, Harwell OX11 0RH, Oxon, England.
BNFL NSTS, Seascale CA20 1PG, Cumbria, England.
RP Setiadi, A (corresponding author), Univ Sheffield, Dept Mat Engn, Immobilisat
Sci Lab, Mappin St, Sheffield S1 3JD, S Yorkshire, England.
EM a.setiadi@sheffield.ac.uk
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PA HUDSON RD, LEEDS LS9 7DL, ENGLAND
SN 1743-6753
J9 ADV APPL CERAM
JI Adv. Appl. Ceram.
PD AUG
PY 2006
VL 105
IS 4
BP 191
EP 196
DI 10.1179/174367606X120142
PG 6
GA 078YG
UT WOS:000240142100006
DA 2023-12-05
ER
PT J
AU Kiventera, J
Perumal, P
Yliniemi, J
Illikainen, M
AF Kiventera, Jenni
Perumal, Priyadharshini
Yliniemi, Juho
Illikainen, Mirja
TI Mine tailings as a raw material in alkali activation: A review
SO INTERNATIONAL JOURNAL OF MINERALS METALLURGY AND MATERIALS
LA English
DT Review
DE mine tailings; alkali activation; thermal treatment; mechanical
activation; alkaline fusion; heavy metal immobilization
ID IMMOBILIZE TOXIC METALS; GOLD MINE; FLY-ASH; GEOPOLYMERIC MATERIALS;
THERMAL-STABILITY; POTENTIAL USE; FUSION METHOD; WASTE; STRENGTH; SLAG
AB The mining industry produces billions of tons of mine tailings annually.
However, because of their lack of economic value, most of the tailings are
discarded near the mining sites, typically under water. The primary environmental
concerns of mine tailings are related to their heavy metal and sulfidic mineral
content. Oxidation of sulfidic minerals can produce acid mine drainage that leaches
heavy metals into the surrounding water. The management of tailing dams requires
expensive construction and careful control, and there is the need for stable,
sustainable, and economically viable management technologies. Alkali activation as
a solidification/stabilization technology offers an attractive way to deal with
mine tailings. Alkali activated materials are hardened, concrete-like structures
that can be formed from raw materials that are rich in aluminum and silicon, which
fortunately, are the main elements in mining residues. Furthermore, alkali
activation can immobilize harmful heavy metals within the structure. This review
describes the research on alkali activated mine tailings. The reactivity and
chemistry of different minerals are discussed. Since many mine tailings are poorly
reactive under alkaline conditions, different pretreatment methods and their
effects on the mineralogy are reviewed. Possible applications for these materials
are also discussed.
C1 [Kiventera, Jenni; Perumal, Priyadharshini; Yliniemi, Juho; Illikainen, Mirja]
Univ Oulu, Fibre & Particle Engn Res Unit, Pentti Kaiteran Katu 1, Oulu 90014,
Finland.
RP Kiventera, J (corresponding author), Univ Oulu, Fibre & Particle Engn Res Unit,
Pentti Kaiteran Katu 1, Oulu 90014, Finland.
EM jenni.kiventera@oulu.fi
RI P, Priyadharshini/P-7995-2018
OI P, Priyadharshini/0000-0002-7731-2016; Illikainen,
Mirja/0000-0001-7545-4574; Yliniemi, Juho/0000-0003-0013-8598
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NR 67
TC 41
Z9 43
U1 18
U2 99
PU SPRINGER
PI NEW YORK
SN 1674-4799
EI 1869-103X
J9 INT J MIN MET MATER
JI Int. J. Miner. Metall. Mater.
PD AUG
PY 2020
VL 27
IS 8
BP 1009
EP 1020
DI 10.1007/s12613-020-2129-6
PG 12
Engineering; Mining & Mineral Processing
SC Materials Science; Metallurgy & Metallurgical Engineering; Mining &
Mineral Processing
GA NC0VH
UT WOS:000560929800002
DA 2023-12-05
ER
PT J
AU Li, FH
Yu, B
Wang, GX
Fan, HL
Wang, T
Guo, MX
Fang, YT
AF Li, Fenghai
Yu, Bing
Wang, Guixiu
Fan, Hongli
Wang, Tao
Guo, Mingxi
Fang, Yitian
TI Investigation on improve ash fusion temperature (AFT) of low-AFT coal by
biomass addition
LA English
DT Article
DE Low AFT SM coal; Biomass; Effects; AFT variation; Mineral transformation
ID FLUIDIZED-BED GASIFICATION; FUSIBILITY CHARACTERISTICS; RICE HUSK;
TORREFIED BIOMASS; ALUMINUM COAL; FLOW BEHAVIOR; VISCOSITY; SLAG;
COMBUSTION; PREDICTION
AB The co-gasification of coal and biomass is of importance for coal clean
conversion and biomass utilization on a large scale. To investigate the effecting
behaviors of biomass on ash fusion characteristics of low ash-fusiontemperature
(AFT) coal, the ash chemical properties of three materials (Shenmu coal (SM),
chestnut shell (CS), and rice husk (RH)), the variations in SM mixed AFT with
increasing CS or RH mass ratio and their mechanisms were explored through silicate-
network structure theory, X-ray powder diffractometry, and FactSage software. The
formations of anorthite, gehlenite and their eutectics caused SM with low AFT. An
increased CS mass ratio led to the increasing contents of high melting-point (MP)
kalsilite, lime and magnesia and the decreasing contents of low MP nepheline,
olivine, and gehlenite, this made SM mixed AFTs increased gradually. Increasing
high MP tridymite content led to SM mixed AFT mostly increased with increasing RH
mass ratio. The temperature that all minerals changed into liquid phase based on
FactSage calculation could reflect the AFT variation of samples.
C1 [Li, Fenghai; Wang, Guixiu; Fan, Hongli; Wang, Tao; Guo, Mingxi] Heze Univ, Sch
Chem & Chem Engn, Heze 274015, Shandong, Peoples R China.
[Li, Fenghai; Yu, Bing] Henan Polytech Univ, Sch Chem & Chem Engn, Jiaozuo
454003, Henan, Peoples R China.
[Li, Fenghai; Fang, Yitian] Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal
Convers, Taiyuan 030001, Shanxi, Peoples R China.
C3 Heze University; Henan Polytechnic University; Chinese Academy of
Sciences; Institute of Coal Chemistry, CAS
RP Li, FH; Wang, T (corresponding author), Heze Univ, Sch Chem & Chem Engn, Heze
274015, Shandong, Peoples R China.
EM hzlfh@163.com; quser@qq.com
RI LI, feng/HIR-1703-2022; guo, mingxi/ABB-3916-2020
FU Natural Science Foundation of China [21875059]; Natural Science
Foundation of Shandong Province, China [ZR2018MB037, ZR2017BB063,
ZR2015BL014, ZR2014BM014]
FX This work was financially supported by the Natural Science Foundation of
China (21875059), and the Natural Science Foundation of Shandong
Province, China (ZR2018MB037, ZR2017BB063, ZR2015BL014, and
ZR2014BM014).
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NR 56
TC 41
Z9 44
U1 3
U2 48
PI AMSTERDAM
SN 0378-3820
EI 1873-7188
PD AUG
PY 2019
VL 191
BP 11
EP 19
DI 10.1016/j.fuproc.2019.03.005
PG 9
GA IA9VI
UT WOS:000469904600002
DA 2023-12-05
ER
PT J
AU Shin, JH
Park, JH
AF Shin, Jae Hong
Park, Joo Hyun
TI Modification of Inclusions in Molten Steel by Mg-Ca Transfer from Top
Slag: Experimental Confirmation of the 'Refractory-Slag-Metal-Inclusion
(ReSMI)' Multiphase Reaction Model
LA English
DT Article
ID NONMETALLIC INCLUSIONS; FORMATION MECHANISM; CALCIUM TREATMENT; SPINEL;
EVOLUTION; ALUMINUM; SULFUR
AB High-temperature experiments and Refractory-Slag-Metal-Inclusion (ReSMI)
multiphase reaction simulations were carried out to determine the effect of the
ladle slag composition on the formation behavior of non-metallic inclusions in
molten steel. Immediately after the slag-metal reaction, magnesium migrated to the
molten steel and a MgAl2O4 spinel inclusion was formed due to a reaction between
magnesium and alumina inclusions. However, the spinel inclusion changed entirely
into a liquid oxide inclusion via the transfer of calcium from slag to metal in the
final stage of the reaction. Calcium transfer from slag to metal was more enhanced
for lower SiO2 content in the slag. Consequently, the spinel inclusion was modified
to form a liquid CaO-Al2O3-MgO-SiO2 inclusion, which is harmless under steelmaking
conditions. The modification reaction was more efficient as the SiO2 content in the
slag decreases.
C1 [Shin, Jae Hong; Park, Joo Hyun] Hanyang Univ, Dept Mat Engn, Ansan 15588, South
Korea.
C3 Hanyang University
RP Shin, JH (corresponding author), Hanyang Univ, Dept Mat Engn, Ansan 15588, South
Korea.
OI Shin, JaeHong/0000-0001-7737-4375
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NR 29
TC 41
Z9 44
U1 2
U2 29
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD DEC
PY 2017
VL 48
IS 6
BP 2820
EP 2825
DI 10.1007/s11663-017-1080-z
PG 6
Engineering
GA FN2FJ
UT WOS:000415806100002
DA 2023-12-05
ER
PT J
AU Perná, I
Hanzlícek, T
AF Perna, Ivana
Hanzlicek, Tomas
TI The solidification of aluminum production waste in geopolymer matrix
LA English
DT Article
DE Aluminum waste; Solidification; Recycling; Geopolymer
ID INDUSTRIAL-WASTES; FLY-ASH; RED MUD
AB The solidification of highly alkaline, generally semi-liquid red waste and gray
slag from the aluminum production inhibits toxic properties. The chemical and
mineralogical compositions of waste materials were determined and both materials
were transformed to the solids (compact and foamed materials) through the
geopolymer technology. The described method of solidification distinguishes by the
inhibition of waste alkalinity, lowering the waste hazardous effect. The resulting
solids have sufficient mechanical properties and do not produce any hazardous
gasses when heated. The presented work studies the solidification of waste
materials from aluminum production and results inform about insulating properties
of products when both waste types are reacting with geopolymer precursors. (C) 2014
C1 [Perna, Ivana; Hanzlicek, Tomas] Acad Sci Czech Republ, Inst Rock Struct & Mech,
Vvi, Dept Mat Struct & Properties, Prague 18209 8, Czech Republic.
C3 Czech Academy of Sciences; Institute of Rock Structure & Mechanics of
the Czech Academy of Sciences
RP Perná, I (corresponding author), Acad Sci Czech Republ, Inst Rock Struct & Mech,
Vvi, Dept Mat Struct & Properties, V Holesovickach 41, Prague 18209 8, Czech
Republic.
EM perna@irsm.cas.cz
RI Perná, Ivana/G-9810-2014
OI Perná, Ivana/0000-0002-5946-8885
FU Institute of Rock Structure and Mechanics, v.v.i., Academy of Sciences
of the Czech Republic [USMH-130/135/2011]
FX This work has been supported by the Research Program for the years
2012-2017, Institute of Rock Structure and Mechanics, v.v.i., Academy of
Sciences of the Czech Republic, #USMH-130/135/2011.
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3449(98)00048-2
10.1016/j.resconrec.2013.03.003
NR 35
TC 41
Z9 42
U1 4
U2 56
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD DEC 1
PY 2014
VL 84
BP 657
EP 662
DI 10.1016/j.jclepro.2014.04.043
PG 6
& Ecology
GA AU6SB
UT WOS:000345731000069
DA 2023-12-05
ER
PT J
AU Harada, A
Maruoka, N
Shibata, H
Kitamura, S
AF Harada, Akifumi
Maruoka, Nobuhiro
Shibata, Hiroyuki
Kitamura, Shin-ya
TI A Kinetic Model to Predict the Compositions of Metal, Slag and
Inclusions during Ladle Refining: Part2. Condition to Control the
Inclusion Composition
LA English
DT Article
DE ladle metallurgy; kinetic simulation; inclusion; spinel; slag; Ca
treatment
ID DEOXIDATION EQUILIBRIUM; FE-NI; MAGNESIUM; ALUMINUM
AB A kinetic model to simulate the reactions in a ladle furnace was developed in
the previous paper. The following parameters were considered in this model; (1)
ratio of the entrapment of slag in the molten steel, (2) ratio of the floatation of
the deoxidation products and inclusions originating from the slag, (3) ratio of the
agglomeration of deoxidation products with inclusions originating from the slag and
(4) ratio of the volume of the bulk zone to the total volume of molten steel and
that of slag phase. These parameters were optimized using sensitivity calculation
by comparison with operational results as the parameters affected the amount and
composition of inclusions.
Then, the method to suppress the formation of MgO center dot Al2O3 spinel-type
inclusion was discussed using the optimized parameters. The calculated results
showed that the formation of MgO center dot Al2O3 spinel-type inclusion could be
suppressed by optimizing the additional amount of Al, initial content of MgO in the
slag, and slag basicity in addition to the Ca treatment. The changes in the
inclusions calculated using the kinetic model were in good agreement with those
predicted by the phase stability diagram. The developed model was useful for
optimizing the operation of a ladle furnace.
C1 [Harada, Akifumi] Tohoku Univ, Grad Sch Engn, Dept Met, Aoba Ku, Sendai, Miyagi
9808577, Japan.
[Maruoka, Nobuhiro; Shibata, Hiroyuki; Kitamura, Shin-ya] Tohoku Univ, Inst
Multidisciplinary Res Adv Mat, Aoba Ku, Sendai, Miyagi 9808577, Japan.
C3 Tohoku University; Tohoku University
RP Harada, A (corresponding author), Tohoku Univ, Grad Sch Engn, Dept Met, Aoba Ku,
2-1-1 Katahira, Sendai, Miyagi 9808577, Japan.
EM a.harada@mail.tagen.tohoku.ac.jp
RI Shibata, Hiroyuki/ACO-3534-2022; Kitamura, Shin-ya/AAY-6813-2020;
Maruoka, Nobuhiro N/E-1421-2015
OI Maruoka, Nobuhiro N/0000-0002-7164-9080; Shibata,
Hiroyuki/0000-0002-9965-7285
FU Research Grant of the 19th Committee of Steelmaking; Japan Society for
the Promotion of Science; ISIJ Research Promotion Grant of Iron and
Steel Institute of Japan
FX The authors appreciate the financial support of the Research Grant of
the 19th Committee of Steelmaking, the Japan Society for the Promotion
of Science, and the ISIJ Research Promotion Grant of Iron and Steel
Institute of Japan.
Graham K.-J., 2010, P INT S HIGHL INN NO
Harada A., ISIJ INT IN PRESS
NR 12
TC 41
Z9 44
U1 1
U2 19
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2013
VL 53
IS 12
BP 2118
EP 2125
PG 8
GA 278ZI
UT WOS:000328928000013
OA gold
DA 2023-12-05
ER
PT J
AU Giannopoulou, I
Panias, D
AF Giannopoulou, I.
Panias, D.
TI Hydrolytic stability of sodium silicate gels in the presence of aluminum
LA English
DT Article
ID X-RAY-DIFFRACTION; SYNTHESIS PARAMETERS; SLAG; GEOPOLYMERS; MINERALS;
GLASS
AB Polycondensation in alkali silicate solutions comprises a fundamental process of
the geopolymerization technology. Previous works had shown that the hydrolytic
stability of sodium silicate gels depends on the SiO2/Na2O ratio. Sodium silicate
gels totally insoluble in water can be produced at SiO2/Na2O molar ratios higher
than 4.4. This article aims at elucidating the effect of tetra-coordinated aluminum
addition on the hydrolytic stability of sodium silicate gels. According to the
results, the aluminum addition stabilizes the sodium silicate gels in an aqueous
environment. A sodium silicate gel with SiO2/Na2O molar ratio 3.48, which is
totally soluble in deionized water at ambient temperature, can be transformed to
insoluble sodium hydroaluminosilicates with the addition of tetrahedral aluminum at
Al/Si molar ratios higher than 0.08. In addition, this article studies the
structure of prepared sodium hydroaluminosilicates and draws very useful
conclusions for the geopolymerization technology.
C1 [Giannopoulou, I.; Panias, D.] Natl Tech Univ Athens, Met Lab, Sch Min & Met
Engn, Athens 15780, Greece.
RP Panias, D (corresponding author), Natl Tech Univ Athens, Met Lab, Sch Min & Met
Engn, Athens 15780, Greece.
EM panias@metal.ntua.gr
RI Panias, Dimitrios/AAO-1296-2021; Giannopoulou, Ioanna/AAL-5169-2021
OI Giannopoulou, Ioanna/0000-0003-2528-919X
FU Senator Committee of Basic Research of the National Technical University
of Athens [65/1634]
FX The authors would like to thank the Senator Committee of Basic Research
of the National Technical University of Athens, Programme "PEBE-2007",
R.C. No.:65/1634 for the financial support of this study.
CR [Anonymous], 2008, GEOPOLYMER CHEM APPL
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10.1016/j.conbuildmat.2005.06.052
NR 31
TC 41
Z9 42
U1 2
U2 34
PU SPRINGER
PI NEW YORK
SN 0022-2461
EI 1573-4803
J9 J MATER SCI
JI J. Mater. Sci.
PD OCT
PY 2010
VL 45
IS 19
BP 5370
EP 5377
DI 10.1007/s10853-010-4586-1
PG 8
GA 634QI
UT WOS:000280597600031
DA 2023-12-05
ER
PT J
AU Rha, CY
Kang, SK
Kim, CE
AF Rha, CY
Kang, SK
Kim, CE
TI Investigation of the stability of hardened slag paste for the
stabilization/solidification of wastes containing heavy metal ions
LA English
DT Article
DE hardened slag paste; chromium; lead
ID BLAST-FURNACE SLAG; PORTLAND-CEMENT; SOLIDIFICATION; STABILIZATION;
ACTIVATION; HYDRATION; MATRICES; FTIR
AB We have studied the effect of chromium ions and lead ions on the chemical
stability of hardened slag paste with toxic wastes during the
stabilization/solidification process. The influences of Cr and Pb ions on the
hydration of slag were also investigated. Sodium silicate (Na2SiO3), 5 wt.% of
slag, was used as an alkali activator for slag hydration. The physical stability of
hardened paste containing partial replacement of slag with fry ash and gypsum was
also examined.
When gypsum was added to slag, the compressive strength of hardened slag paste
developed, accompanying the activation of alumino-ferrite-tricalciumsulfate (Al2O3-
Fe2O3-3CaSO(4), AFt) and alumino-ferrite-monocalciumsulfate (Al2O3-Fe2O3-CaSO4,
AFm) phase generation. Those phases caused densification of the microstructure.
Concurrently, the leaching amount of heavy metal ions was decreased. When fly ash
was added to slag, the compressive strength increased and the leaching amount
decreased with both active formation of aluminate hydrates and ion substitution.
Lead ions were mostly stabilized through physical encapsulation by the hardened
slag paste's hydrate matrix. In the case of chromium ions, we observed that it was
mainly solidified through the formation of a substitutional solid solution with
aluminum atoms in the structure of aluminate hydrates. (C) 2000 Elsevier Science
C1 Yonsei Univ, Dept Ceram Engn, Seodaemoon Ku, Seoul 120749, South Korea.
RP Rha, CY (corresponding author), Yonsei Univ, Dept Ceram Engn, Seodaemoon Ku, 134
Shinchon Dong, Seoul 120749, South Korea.
CR [Anonymous], [No title captured]
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NR 18
TC 41
Z9 51
U1 1
U2 39
PU ASPEN LAW & BUSINESS DIV ASPEN PUBLISHERS INC
PI NEW YORK
PA 1185 AVENUE OF THE AMERICAS, NEW YORK, NY 10036 USA
SN 0304-3894
J9 J HAZARD MATER
PD APR 28
PY 2000
VL 73
IS 3
BP 255
EP 267
DI 10.1016/S0304-3894(99)00185-5
PG 13
GA 302YF
UT WOS:000086393500005
PM 10751696
DA 2023-12-05
ER
PT J
AU Sivasakthi, M
Jeyalakshmi, R
Rajamane, NP
AF Sivasakthi, M.
Jeyalakshmi, R.
Rajamane, N. P.
TI Fly ash geopolymer mortar: Impact of the substitution of river sand by
copper slag as a fi ne aggregate on its thermal resistance properties
LA English
DT Article
DE Geopolymer mortar; Copper slag; Fine aggregate; Waste reuse; Thermal
properties; Microstructure
AB Geopolymer materials are increasingly finding application in various settings
because of their excellent mechanical properties and their ability to reduce the
level of CO2 emission in the atmosphere, thus contributing to a sustainable
environment. Mortars containing an alkali-activated fly ash binder in which river
sand is used as an aggregate are found to display poor adhesive strength and
incompatibility at elevated temperatures, necessitating researchers to look for
alternate aggregates to be used in geopolymer mortars. In this study, we have
substituted copper slag as an aggregate [C] in place of river sand [R] in a fly ash
geopolymer mortar and investigated its effect on the thermal resistance of the
mortar. We report the results of our investigations in this paper. Our experimental
results show that the mortar using copper slag as an aggregate (C-type mortar)
exhibited good thermal stability in the temperature range of 200e1000 degrees C
without any spalling. Thermal strain was low, and the mortar was found to have a
thermal expansion of just 0.002% and a thermal conductivity value of 0.6 W/m K at
1000 degrees C. Further, the C-type mortar exhibited a compressive strength of 33
MPa on exposure to 1000 degrees C and negligible mass loss even after several
thermal cycles, facilitating the recycling of industrial waste such as copper slag
in thermal applications. In contrast, mortars using river sand as an aggregate (R-
type mortars) exhibited a higher mass loss on thermal treatment. Thermal-induced
changes were studied using field emission scanning electron spectroscopy (FESEM),
X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS). The network
rich in silicon atoms in the crystalline phase was found to contain aluminium as
nepheline along with an amorphous geopolymeric gel in the heated samples. There
were no differences in the binding energy of Si, Al, O and Na atoms of heated and
unheated samples, which confirmed the retention of the desired geopolymeric
microstructural network even at elevated temperatures.(c) 2020 Elsevier Ltd. All
rights reserved.
C1 [Jeyalakshmi, R.] SRM Inst Sci & Technol, Dept Chem, Chennai, Tamil Nadu, India.
[Sivasakthi, M.; Rajamane, N. P.] SRM Inst Sci & Technol, Ctr Adv Concrete Res
CACR, Chennai, Tamil Nadu, India.
C3 SRM Institute of Science & Technology Chennai; SRM Institute of Science
& Technology Chennai
RP Jeyalakshmi, R (corresponding author), SRM Inst Sci & Technol, Dept Chem,
Chennai, Tamil Nadu, India.
EM sivasakthi.msc09@gmail.com; jeyalakr@srmist.edu.in;
rajamanenp@yahoo.co.uk
OI M, Sivasakthi/0000-0002-2485-4962
FU Department of Science and Technolgy, Ministry of Science and Technolgy,
India [DST/TSG/STS/2012/20, DST/TDT/WMT/2017/101]; DSTFIST from the
Department of Chemistry, SRMIST
FX This work was supported by the Department of Science and Technolgy,
Ministry of Science and Technolgy, India [Grant No's DST/TSG/STS/2012/20
and DST/TDT/WMT/2017/101, and the DSTFIST sponsored facilities from the
Department of Chemistry, SRMIST.
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NR 44
TC 40
Z9 41
U1 4
U2 31
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD JAN 10
PY 2021
VL 279
AR 123766
DI 10.1016/j.jclepro.2020.123766
PG 13
& Ecology
GA OZ9SK
UT WOS:000595258500020
DA 2023-12-05
ER
PT J
AU Huang, GD
Yang, K
Sun, YH
Lu, ZY
Zhang, XY
Zuo, L
Feng, YQ
Qian, RC
Qi, Y
Ji, YS
Xu, ZS
AF Huang, Guodong
Yang, Ke
Sun, Yuhua
Lu, Zeyang
Zhang, Xingyu
Zuo, Lin
Feng, Yongqi
Qian, Ruochun
Qi, Yue
Ji, Yongsheng
Xu, Zhishan
TI Influence of NaOH content on the alkali conversion mechanism in MSWI
bottom ash alkali-activated mortars
LA English
DT Article
DE Alkali conversion mechanism; Polymerization reaction; Municipal solid
waste incineration bottom ash; Granulated blast-furnace slag;
Alkali-activated; Mortar
ID FLY-ASH; STRENGTH DEVELOPMENT; BLENDED CEMENT; PORE SOLUTION; SLAG;
CONCRETE; CALCIUM; CARBONATION; METAKAOLIN; SILICA
AB This is a microscopic analysis of the promoting effect that different NaOH
contents exerted on both polymerization reaction and alkali conversion mechanism
between free and union alkali. The study focuses on the strength development of
municipal solid waste incineration bottom ash (BA) alkali-activated mortars. Mixing
with the appropriate amount of NaOH (between 1.8% and 5.6%) formed a good
alkalinity stimulating environment (13.5 < pH < 14.5) in alkali-activated samples
and promoted the process of polymerization. Moreover the formation of high-strength
polymerization products (C-A-S-H and C-S-H gels) was also promoted, which
significantly facilitated the conversion from free alkali to union alkali and
increased the compressive strength. However, excessive addition of NaOH (above
5.6%) cannot further promote the transformation from free alkali to union alkali
and decrease the compressive strength. The polymerization and formation of silicate
(C-S-H gels) were severely affected by the high alkalinity environment (pH > 14.5)
and the excess active sodium competed with active calcium for active silicon and
aluminium. This resulted in a large number of low strength N-A-S-H gels formation,
while the yield of high strength C-S-H gels decreased significantly. (C) 2020
C1 [Huang, Guodong; Sun, Yuhua; Zhang, Xingyu; Zuo, Lin; Feng, Yongqi; Qian,
Ruochun; Qi, Yue] Anhui Univ Sci & Technol, Sch Civil Engn & Construct, Huainan
232001, Anhui, Peoples R China.
[Huang, Guodong; Ji, Yongsheng; Xu, Zhishan] China Univ Min & Technol, State Key
Lab Geomech & Deep Underground Engn, Xuzhou 21116, Jiangsu, Peoples R China.
[Huang, Guodong; Yang, Ke] Anhui Univ Sci & Technol, Sch Energy & Safety,
Huainan 232001, Anhui, Peoples R China.
[Lu, Zeyang] Anhui Univ Sci & Technol, Sch Mech & Optoelect Phys, Huainan
C3 Anhui University of Science & Technology; China University of Mining &
Technology; Anhui University of Science & Technology; Anhui University
of Science & Technology
RP Huang, GD (corresponding author), Anhui Univ Sci & Technol, Sch Civil Engn &
Construct, Huainan 232001, Anhui, Peoples R China.; Huang, GD (corresponding
author), China Univ Min & Technol, State Key Lab Geomech & Deep Underground Engn,
Xuzhou 21116, Jiangsu, Peoples R China.; Huang, GD (corresponding author), Anhui
Univ Sci & Technol, Sch Energy & Safety, Huainan 232001, Anhui, Peoples R China.
OI Ji, Yongsheng/0000-0002-7414-9719
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10.1016/j.cemconres.2017.03.002
10.1016/j.cemconres.2015.04.013
10.1016/j.cemconcomp.2017.10.003
10.1016/j.conbuildmat.2010.12.044
10.1016/j.conbuildmat.2013.05.069
10.1016/j.cemconres.2011.03.016
10.1016/j.cemconres.2017.10.004
Tang P, 2015, CONSTR BUILD MATER, V83, P77, DOI
10.1016/j.conbuildmat.2015.02.033
Tuyan M, 2018, COMPOS PART B-ENG, V135, P242, DOI
10.1016/j.compositesb.2017.10.013
10.1016/j.cemconres.2017.05.006
10.1016/j.conbuildmat.2014.09.059
Yuan B, 2017, CEMENT CONCRETE COMP, V84, P188, DOI
10.1016/j.cemconcomp.2017.09.005
NR 51
TC 40
Z9 40
U1 12
U2 53
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUL 10
PY 2020
VL 248
AR 118582
DI 10.1016/j.conbuildmat.2020.118582
PG 10
GA LK7ZX
UT WOS:000531081200017
DA 2023-12-05
ER
PT J
AU Nguyen, HA
Chang, TP
Shih, JY
Chen, CT
AF Hoang-Anh Nguyen
Chang, Ta-Peng
Shih, Jeng-Ywan
Chen, Chun-Tao
TI Influence of low calcium fly ash on compressive strength and hydration
product of low energy super sulfated cement paste
LA English
DT Article
DE CFBC fly ash; Fly ash; Super-sulfated cement; Compressive strength;
Hydration product
ID C-S-H; BLAST-FURNACE SLAG; ACTIVATION; LIME; ALKALI; COMBUSTION;
RESISTANCE; CA(OH)(2); MORTARS; ATTACK
AB This research aims to explore the effects of low calcium Class F fly ash (FFA)
as an alumina supplier on the compressive strength and hydration products of an
ecological super-sulfated cement (SSC) with fluidized bed combustion (CFBC) fly ash
(CFA) as a crucial activator. Experimental results showed that partial replacement
of ground granulated blast furnace slag (GGBFS/slag) by FFA in range of 10-30 wt%
significantly improved the compressive strength of hardened eco-SSC paste.
Microstructural examination using scanning electron microscope equipped with energy
dispersive X-ray spectrometer (SEM/EDS), X-ray diffraction (XRD), thermogravimetric
and derivative thermogravimetric analysis (TGA), and Fourier transform infrared
(FTIR) spectroscopy obviously proved that the main hydration products of the
hardened paste were ettringite/monosulfate (AFt/AFm) and calcium aluminum silicate
hydrate (C-A-S-H). Increase in FFA resulted in higher degree of AFt/AFm
precipitation and C-A-S-H with lower Ca:(Si + Al) ratio.
C1 [Hoang-Anh Nguyen; Chang, Ta-Peng; Chen, Chun-Tao] Natl Taiwan Univ Sci &
Technol NTUST Taiwan Tech, Dept Civil & Construct Engn, Taipei 106, Taiwan.
[Shih, Jeng-Ywan] Ming Chi Univ Technol, Dept Chem Engn, New Taipei 243, Taiwan.
[Hoang-Anh Nguyen] Cantho Univ, Dept Rural Technol, Coll Rural Dev, Cantho City,
Vietnam.
C3 Ming Chi University of Technology; Can Tho University
RP Chang, TP (corresponding author), Natl Taiwan Univ Sci & Technol NTUST Taiwan
Tech, Dept Civil & Construct Engn, Taipei 106, Taiwan.
Tech); Ministry of Science and Technology, Taiwan, R.O.C.
[103-2221-E-011-078-MY3]; National Foundation for Science and Technology
Development (NAFOSTED), Vietnam [107.99-2018.301]
FX The authors would like to acknowledge the financial aid from the
National Taiwan University of Science and Technology (NTUST) (Taiwan
Tech) and the Ministry of Science and Technology, Taiwan, R.O.C. through
research grant of 103-2221-E-011-078-MY3, and National Foundation for
Science and Technology Development (NAFOSTED), Vietnam, through research
grant of 107.99-2018.301 for this investigation.
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NR 48
TC 40
Z9 40
U1 9
U2 58
PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
PD MAY
PY 2019
VL 99
BP 40
EP 48
DI 10.1016/j.cemconcomp.2019.02.019
PG 9
GA HW6UA
UT WOS:000466824900004
DA 2023-12-05
ER
PT J
AU Chargui, F
Hamidouche, M
Belhouchet, H
Jorand, Y
Doufnoune, R
Fantozzi, G
AF Chargui, Fouzia
Hamidouche, Mohamed
Belhouchet, Hocine
Jorand, Yves
Doufnoune, Rachida
Fantozzi, Gilbert
TI Mullite fabrication from natural kaolin and aluminium slag
SO BOLETIN DE LA SOCIEDAD ESPANOLA DE CERAMICA Y VIDRIO
LA English
DT Article
DE Mullite; Kaolin; Aluminum slag; Phase transformation
ID MICROSTRUCTURAL EVOLUTION; PHASE-TRANSFORMATION; POROUS MULLITE;
CERAMICS; BOEHMITE; COMPOSITES; MIXTURES; ZIRCON; ELABORATION; BEHAVIOR
AB The structural transformations of kaolin-aluminium slag mixtures during heating
were studied using differential thermal analysis (DTA), thermal gravimetric
analysis (TGA), Fourier transform infrared (FTIR) spectroscopy, X-ray diffraction
analysis (XRD) and scanning electron microscopy (SEM). The amount of formed mullite
increases with the firing temperature. At 1500 degrees C, the mullitization of the
mixture is almost complete. The morphology of the formed mullite is bimodal
(primary and secondary phases). The primary mullite, formed from processing of
kaolin by the gradual collapse of metakaolin from 990 degrees C, has a shape of
elongated crystals. The other hand, the secondary mullite formed by solution-
precipitation from the glass phase in the presence of alumina particles has a shape
of acicular grains. (C) 2018 SECV. Published by Elsevier Espana, S.L.U.
C1 [Chargui, Fouzia; Hamidouche, Mohamed; Doufnoune, Rachida] Setif 1 Univ,
Emergent Mat Res Unit, Setif 19000, Algeria.
[Chargui, Fouzia; Hamidouche, Mohamed] Setif 1 Univ, Opt & Precis Mech Inst,
Setif 19000, Algeria.
[Belhouchet, Hocine] Setif 1 Univ, Nonmetall Mat Lab, Opt & Precis Mech Inst,
Setif 19000, Algeria.
[Belhouchet, Hocine] Mohamed Boudiaf Msila Univ, Fac Sci, Phys Dept, Msila
28000, Algeria.
[Jorand, Yves; Fantozzi, Gilbert] Lyon Univ, INSA Lyon, MATEIS Lab, CNRS UMR
5510, F-69621 Villeurbanne, France.
[Doufnoune, Rachida] Setif 1 Univ, Fac Technol, Proc Engn Dept, Setif 19000,
Algeria.
C3 Universite Ferhat Abbas Setif; Universite Ferhat Abbas Setif; Universite
Ferhat Abbas Setif; Centre National de la Recherche Scientifique (CNRS);
CNRS - Institute for Engineering & Systems Sciences (INSIS); Institut
National des Sciences Appliquees de Lyon - INSA Lyon; Universite Ferhat
Abbas Setif
RP Hamidouche, M (corresponding author), Setif 1 Univ, Emergent Mat Res Unit, Setif
19000, Algeria.; Hamidouche, M (corresponding author), Setif 1 Univ, Opt & Precis
Mech Inst, Setif 19000, Algeria.
EM mhamidouche@univ-setif.dz
RI Belhouchet, Hocine/AAM-7519-2021
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NR 32
TC 40
Z9 41
U1 3
U2 21
PI AMSTERDAM
SN 0366-3175
EI 2173-0431
J9 BOL SOC ESP CERAM V
JI Bol. Soc. Esp. Ceram. Vidr.
PD JUL-AUG
PY 2018
VL 57
IS 4
BP 169
EP 177
DI 10.1016/j.bsecv.2018.01.001
PG 9
GA GR7BJ
UT WOS:000442841000006
OA gold
DA 2023-12-05
ER
PT J
AU Yagüe, S
Sánchez, I
de la Villa, RV
García-Giménez, R
Zapardiel, A
Frías, M
AF Yague, Santiago
Sanchez, Isabel
Vigil de la Villa, Raquel
Garcia-Gimenez, Rosario
Zapardiel, Antonio
Frias, Moises
TI Coal-Mining Tailings as a Pozzolanic Material in Cements Industry
SO MINERALS
LA English
DT Article
DE coal-mining tailings; thermally activated tailings; cement; pozzolan;
mineralogy; metakaolinite
ID COALFIELD NW SPAIN; WASTE; WATER; MINE; TRANSFORMATIONS; METAKAOLIN;
SYSTEMS; HEAT; MK
AB The generation of enormous volumes of mine-tailing waste is standard practice in
the mining industry. Large quantities of these tailings are also sources of
kaolinite-rich materials that accumulate in slag heaps, causing significant
environmental degradation and visual impacts on the landscape. The consequences of
coal refuse dumped in slagheaps calls for the study of eco-innovative solutions and
the assessment of waste types. Moreover, the environmental benefits of reusing
large amounts of contaminated waste are also evident. Hence, the objective of this
investigation is to expand current knowledge of new siliceous-aluminium minerals
and their pozzolanic activity. Four raw tailing samples are characterized to
determine their chemical (by ICP/MS analysis), morphological (by SEM/EDX analysis),
and mineralogical (by XRD analysis) compositions prior to their thermal activation
that transforms the inert wastes at various temperatures into materials with
cementitious properties. The results of XRD analysis following activation confirmed
that the kaolinite content is fully transformed into metakaolinite. The coal refuse
samples presented sufficiently reliable levels of pozzolanic activity for use as
additives in industrial cements.
C1 [Yague, Santiago] Univ Nacl Educ Distancia, ETS Ingenieros Ind, E-28040 Madrid,
Spain.
[Sanchez, Isabel; Zapardiel, Antonio] Univ Nacl Educ Distancia, Fac Ciencias, E-
28040 Madrid, Spain.
[Vigil de la Villa, Raquel; Garcia-Gimenez, Rosario] Univ Autonoma Madrid, Dept
Geol & Geoquim, CSIC, Unidad Asociada, E-28049 Madrid, Spain.
[Frias, Moises] Spanish Natl Res Council, CSIC, Eduardo Torroja Inst, Madrid
28033, Spain.
C3 Universidad Nacional de Educacion a Distancia (UNED); Universidad
Nacional de Educacion a Distancia (UNED); Autonomous University of
Madrid; Consejo Superior de Investigaciones Cientificas (CSIC); Consejo
Superior de Investigaciones Cientificas (CSIC); CSIC - Instituto de
Ciencias de la Construccion Eduardo Torroja (IETCC)
RP García-Giménez, R (corresponding author), Univ Autonoma Madrid, Dept Geol &
Geoquim, CSIC, Unidad Asociada, E-28049 Madrid, Spain.
EM santiagooyg@hotmail.com; isa.svigil@gmail.com; raquel.vigil@uam.es;
rosario.garcia@uam.es; azapardiel@ccia.uned.es; mfrias@ietcc.csic.es
RI Garcia, Rosario/B-2113-2008; Frias, Moises/H-3331-2015
OI Frias, Moises/0000-0001-6621-7227
FU Spanish Ministry of Economy and Competitiveness
[BIA2015-65558-C3-1-2-3R]
FX This research was supported by the Spanish Ministry of Economy and
Competitiveness (Project Ref BIA2015-65558-C3-1-2-3R (MINECO/FEDER)).
The authors are also grateful to the Sociedad Anonima Huellera
Vasco-Leonesa and to the Spanish Cement Institute (IECA) for their
assistance with this research.
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[No title captured]
NR 40
TC 40
Z9 42
U1 2
U2 39
PU MDPI
PI BASEL
SN 2075-163X
J9 MINERALS-BASEL
JI Minerals
PD FEB
PY 2018
VL 8
IS 2
AR 46
DI 10.3390/min8020046
PG 13
WC Geochemistry & Geophysics; Mineralogy; Mining & Mineral Processing
SC Geochemistry & Geophysics; Mineralogy; Mining & Mineral Processing
GA FZ4AU
UT WOS:000427534300015
DA 2023-12-05
ER
PT J
AU Keeping, MG
AF Keeping, Malcolm G.
TI Uptake of Silicon by Sugarcane from Applied Sources May Not Reflect
Plant-Available Soil Silicon and Total Silicon Content of Sources
SO FRONTIERS IN PLANT SCIENCE
LA English
DT Article
DE acid soils; aluminum; calcium silicate; liming; plant stress; silicon
uptake; soil pH; thermophosphate
ID BORER ELDANA-SACCHARINA; CALCIUM-MAGNESIUM SILICATE; MEDIATED
ALLEVIATION; SURFACE APPLICATION; WALKER LEPIDOPTERA; ALUMINUM TOXICITY;
AMORPHOUS SILICA; RICE; RESISTANCE; SI
AB Soils of the tropics and sub-tropics are typically acid and depleted of soluble
sources of silicon (Si) due to weathering and leaching associated with high
rainfall and temperatures. Together with intensive cropping, this leads to marginal
or deficient plant Si levels in Si-accumulating crops such as rice and sugarcane.
Although such deficiencies can be corrected with exogenous application of Si
sources, there is controversy over the effectiveness of sources in relation to
their total Si content, and their capacity to raise soil and plant Si
concentrations. This study tested the hypothesis that the total Si content and
provision of plant-available Si from six sources directly affects subsequent plant
Si uptake as reflected in leaf Si concentration. Two trials with potted cane plants
were established with the following Si sources as treatments: calcium silicate
slag, fused magnesium (thermo) phosphate, volcanic rock dust, magnesium silicate,
and granular potassium silicate. Silicon sources were applied at rates intended to
achieve equivalent elemental soil Si concentrations; controls were untreated or
lime-treated. Analyses were conducted to determine soil and leaf elemental
concentrations. Among the sources, calcium silicate produced the highest leaf Si
concentrations, yet lower plant-available soil Si concentrations than the
thermophosphate. The latter, with slightly higher total Si than the slag, produced
substantially greater increases in soil Si than all other products, yet did not
significantly raise leaf Si above the controls. All other sources did not
significantly increase soil or leaf Si concentrations, despite their high Si
content. Hence, the total Si content of sources does not necessarily concur with a
product's provision of soluble soil Si and subsequent plant uptake. Furthermore,
even where soil pH was raised, plant uptake from thermophosphate was well below
expectation, possibly due to its limited liming capacity. The ability of the
calcium silicate to provide Si while simultaneously and significantly increasing
soil pH, and thereby reducing reaction of Si with exchangeable Al3+, is proposed as
a potential explanation for the greater Si uptake into the shoot from this source.
C1 [Keeping, Malcolm G.] South African Sugarcane Res Inst, Mt Edgecombe, South
Africa.
[Keeping, Malcolm G.] Univ Witwatersrand, Sch Anim Plant & Environm Sci,
Johannesburg, South Africa.
C3 University of Witwatersrand
RP Keeping, MG (corresponding author), South African Sugarcane Res Inst, Mt
Edgecombe, South Africa.; Keeping, MG (corresponding author), Univ Witwatersrand,
Sch Anim Plant & Environm Sci, Johannesburg, South Africa.
EM malcolm.keeping@sugar.org.za
RI Keeping, Malcolm G/J-5959-2019
OI Keeping, Malcolm G/0000-0003-2992-4066
FU South African Sugarcane Research Institute (SASRI); National Research
Foundation (NRF), South Africa [IFR2011040700004]
FX Funding and infrastructural support for the research was provided by the
South African Sugarcane Research Institute (SASRI), and additional
financing of research expenses by the Incentive Funding Programme for
Rated Researchers of the National Research Foundation (NRF), South
Africa (Grant No. IFR2011040700004).
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NR 117
TC 40
Z9 42
U1 1
U2 49
PI LAUSANNE
SN 1664-462X
J9 FRONT PLANT SCI
JI Front. Plant Sci.
PD MAY 15
PY 2017
VL 8
AR 760
DI 10.3389/fpls.2017.00760
PG 14
WC Plant Sciences
SC Plant Sciences
GA EU8VG
UT WOS:000401316000002
PM 28555144
DA 2023-12-05
ER
PT J
AU Li, PC
Ning, XJ
AF Li Pengcheng
Ning Xiaojun
TI Effects of MgO/Al2O3 Ratio and Basicity on the
Viscosities of CaO-MgO-SiO2-Al2O3
Slags: Experiments and Modeling
LA English
DT Article
ID SILICATE-BASED SLAGS; AMPHOTERIC BEHAVIOR; VISCOUS-FLOW; MELTS; BINARY;
ALUMINUM; GLASSES; ALKALI; ENERGY; CAO
AB The effects of the MgO/Al2O3 ratio and basicity on the viscosities of CaO-MgO-
SiO2-Al2O3 slags were investigated at 1733 K, 1773 K, and 1823 K (1460 A degrees C,
1500 A degrees C, and 1550 A degrees C) in this study. At a fixed Al2O3 of 15 and
18 mass pct, increasing the basicity from 1 to 1.2 resulted in lowering the
viscosity of slags. At a fixed basicity of 1.0 and 1.2, increasing the MgO from 0
to 15 mass pct decreased the viscosity of slags. The Fourier transform-infrared
spectra analysis of the slag structure was made to discuss the depolymerization
roles of MgO and basicity. Considering the different depolymerization effects of
basic oxides upon the silicate/aluminate network structure as suggested by FT-IT
analysis, a fresh model for predicting the viscosity of CaO-MgO-SiO2-Al2O3 slags
was constructed. A total of 209 viscosity measurements with large compositional
variations showed satisfactory agreement with the results calculated by the present
model. With the aid of the current model, the co-effects of the MgO/Al2O3 ratio and
basicity on the viscosities of CaO-MgO-SiO2-Al2O3 slags (15 to 20 mass pct Al2O3)
were investigated.
C1 [Li Pengcheng; Ning Xiaojun] Univ Sci & Technol Beijing, Sch Met & Ecol Engn,
RP Li, PC (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol Engn,
EM pchlee@outlook.com
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NR 42
TC 40
Z9 42
U1 2
U2 42
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD FEB
PY 2016
VL 47
IS 1
BP 446
EP 457
DI 10.1007/s11663-015-0470-3
PG 12
Engineering
GA DB7JX
UT WOS:000368692300041
DA 2023-12-05
ER
PT J
AU Wang, Q
Qiu, ST
Zhao, P
AF Wang, Qiang
Qiu, Shengtao
Zhao, Pei
TI Kinetic Analysis of Alumina Change in Mold Slag for High Aluminum Steel
during Continuous Casting
LA English
DT Article
AB A kinetic calculation model considering both a molten slag reaction with molten
steel and an Al2O3 inclusion absorption in molten slag was developed to estimate
the change in Al2O3 in molten slag during the continuous casting of high aluminum
steel. Practical casting experiments of high aluminum steel were conducted to
investigate the change in composition in the molten slag and to validate the
proposed model. The calculated results show that the Al2O3 concentration in the
molten slag increases quickly during the initial stage and gradually approaches a
steady-state value after 900 seconds of casting, which agrees well with the
experiment outcome. The change in Al2O3 in molten slag is mainly affected by the
initial Al2O3 concentration w (0) of the mold powder, reaction equilibrium
concentration of Al2O3 w* at the slag-steel interface, mass transfer coefficient
beta in molten slag, Al2O3 inclusion concentration w (M) , and absorption
coefficient beta in molten steel during continuous casting of high aluminum steel.
The experiment result shows that the concentration of Al2O3 in molten slag
increases significantly and that SiO2 decreases strongly, while the other
components in the molten slag can be negligible comparatively. Mold slag properties
at 0, 5, and 45 minutes change greatly, which can deteriorate the performance of
the mold slag.
C1 [Wang, Qiang; Qiu, Shengtao; Zhao, Pei] Cent Iron & Steel Res Inst, Natl Engn
Res Ctr Continuous Casting Technol, Beijing 100081, Peoples R China.
C3 Central Iron & Steel Research Institute
RP Wang, Q (corresponding author), Cent Iron & Steel Res Inst, Natl Engn Res Ctr
Continuous Casting Technol, Beijing 100081, Peoples R China.
EM wangqiang9901@163.com
FU Special Steel Plant of Baosteel; Research Institute of Baosteel
FX The authors thank the Special Steel Plant of Baosteel and the Research
Institute of Baosteel for financial and technical support.
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NR 18
TC 40
Z9 45
U1 1
U2 17
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD APR
PY 2012
VL 43
IS 2
BP 424
EP 430
DI 10.1007/s11663-011-9600-8
PG 7
Engineering
GA 912ET
UT WOS:000301778200022
DA 2023-12-05
ER
PT J
AU Zhang, JD
Shen, ZM
Mei, ZJ
Li, SP
Wang, WH
AF Zhang, Jianda
Shen, Zhemin
Mei, Zhijian
Li, Shanping
Wang, Wenhua
TI Removal of phosphate by Fe-coordinated amino-functionalized 3D
mesoporous silicates hybrid materials
SO JOURNAL OF ENVIRONMENTAL SCIENCES
LA English
DT Article
DE phosphate; mesoporous material; Fe coordinated; adsorption
ID PHOSPHORUS REMOVAL; MOLECULAR-SIEVES; WASTE-WATER; ADSORPTION; MCM-41;
WASTEWATERS; ADSORBENTS; ALUMINUM; SLAG
AB Phosphate removal from aqueous waste streams is an important approach to control
the eutrophication downstream bodies of water. A Fe(III) coordinated amino-
functionalized silicate adsorbent for phosphate adsorption was synthesized by a
post-grafting and metal cation incorporation process. The surface structure of the
adsorbent was characterized by X-ray diffraction, N-2 adsoropion/desoprotion
technique, and Fourier transform infrared spectroscopy. The experimental results
showed that the adsorption equilibrium data were well fitted to the Langmuir
equation. The maximum adsorption capacity of the modified silicate material was
51.8 mg/g. The kinetic data from the adsorption of phosphate were fitted to pseudo
second-order model. The phosphate adsorption was highly pH dependent and the
relatively high removal of phosphate fell within the pH range 3.0-6.0. The
coexistence of other anions in solutions has an adverse effect on phosphate
adsorption; a decrease in adsorption capacity followed the order of exogenous
anions: F- > SO42- > NO3- > Cl-. In addition, the adsorbed phosphate could be
desorbed by NaOH solutions. This silicate adsorbent with a large adsorption
capacity and relatively high selectivity could be utilized for the removal of
phosphate from aqueous waste streams or in aquatic environment.
C1 [Zhang, Jianda; Shen, Zhemin; Mei, Zhijian; Wang, Wenhua] Shanghai Jiao Tong
Univ, Sch Environm Sci & Engn, Shanghai 200240, Peoples R China.
[Li, Shanping] Shandong Univ, Sch Environm Sci & Engn, Jinan 250100, Peoples R
China.
C3 Shanghai Jiao Tong University; Shandong University
RP Wang, WH (corresponding author), Shanghai Jiao Tong Univ, Sch Environm Sci &
Engn, Shanghai 200240, Peoples R China.
EM zjdrf@163.com; wangwh@sjtu.edu.cn
FU National Major Research Plan for Water Pollution Control and Treatment
of China [2009ZX07101-015, 2009ZX07105-003]
FX This work was supported by the National Major Research Plan for Water
Pollution Control and Treatment of China (No. 2009ZX07101-015,
2009ZX07105-003). We also want to thank Dr. David for his valuable work
on our manuscript revision.
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NR 27
TC 40
Z9 44
U1 0
U2 47
PU SCIENCE PRESS
PI BEIJING
SN 1001-0742
EI 1878-7320
J9 J ENVIRON SCI-CHINA
JI J. Environ. Sci.
PY 2011
VL 23
IS 2
BP 199
EP 205
DI 10.1016/S1001-0742(10)60393-2
PG 7
GA 727VO
UT WOS:000287831200004
PM 21516992
DA 2023-12-05
ER
PT J
AU Chan, CF
Argent, BB
Lee, WE
AF Chan, CF
Argent, BB
Lee, WE
TI Influence of additives on slag resistance of
Al2O3-SiO2-SiC-C refractory bond phases
under reducing atmosphere
LA English
DT Article
AB The microstructures of Al2O3-SiO2-SiC-C refractory matrices with aluminum,
silicon, Si3N4, BN, B2O3, and B4C additives are characterized before and after a
crucible slag test, and the phases present are compared to those expected at
thermodynamic equilibrium, The carbon content dominates the resistance to CaO-MgO-
Al2O3-SiO2 slag penetration, while the viscosity of liquid phases present has a
significant influence when the matrix carbon contents are similar. Silicon and
Si3N4 additives reduce slag penetration resistance because of indirect oxidation of
carbon to form SiC. B4C, in particular, and B2O3 also reduce slag penetration
resistance because of formation of a more fluid boron-containing liquid, while
aluminum and BN addition have no significant effect. Carbon and BN hardly react
with the slag, while SiC partially reacts with it, leading to deposition of carbon
as a dense layer, Corundum present in the refractories also readily dissolves in
the slag. Microstructurally, slag penetration resistance is associated with the
dense carbon layer located at the slag-refractory interface.
C1 Univ Sheffield, Dept Mat Engn, Sheffield S1 3JD, S Yorkshire, England.
RP Chan, CF (corresponding author), Univ Sheffield, Dept Mat Engn, Sheffield S1
3JD, S Yorkshire, England.
OI Lee, William/0000-0002-0650-1442
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NR 25
TC 40
Z9 44
U1 1
U2 14
PU AMER CERAMIC SOC
PI WESTERVILLE
PA 735 CERAMIC PLACE, PO BOX 6136, WESTERVILLE, OH 43081-6136 USA
SN 0002-7820
J9 J AM CERAM SOC
PD DEC
PY 1998
VL 81
IS 12
BP 3177
EP 3188
DI 10.1111/j.1151-2916.1998.tb02754.x
PG 12
GA 149CR
UT WOS:000077588000016
DA 2023-12-05
ER
PT J
AU Lee, Y
Nassaralla, CL
AF Lee, Y
Nassaralla, CL
TI Formation of hexavalent chromium by reaction between slag and
magnesite-chrome refractory
LA English
DT Article
AB The goal of this work was to understand how Cr(6+) formation is affected by the
interaction between chromite phases present in magnesite-chrome refractory and
different slag compositions. In addition, the formation of Cr(6+) as a function of
chromite particle Size and cooling rate due to the chromite phase/slag interaction
was investigated. The following slag compositions were studied: calcium aluminate,
calcium aluminum silicate, and calcium silicate. It was found that the presence of
uncombined CaO in the calcium aluminate slags is responsible for a higher yield of
Cr(6+). However, the replacement of Al(2)O(3) by SiO(2) in calcium aluminate slags
decreases the formation of Cr(6+). SiO(2) reacts with CaO to form stable 2CaO .
Al(2)O(3) . SiO(2) and CaO . SiO(2) phases, consequently decreasing the amount of
uncombined CaO available to react with the chromite phase to form Cr(6+). Moreover,
the content of Cr(6+), decreased by increasing chromite particle size and
increasing the cooling rate of magnesite-chrome refractory.
C1 Michigan Technol Univ, Dept Met & Mat Engn, Houghton, MI 49931 USA.
C3 Michigan Technological University
RP Lee, Y (corresponding author), Michigan Technol Univ, Dept Met & Mat Engn,
Houghton, MI 49931 USA.
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NR 10
TC 40
Z9 42
U1 0
U2 8
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD APR
PY 1998
VL 29
IS 2
BP 405
EP 410
DI 10.1007/s11663-998-0117-8
PG 6
Engineering
GA ZJ613
UT WOS:000073234300011
DA 2023-12-05
ER
PT J
AU Kumar, A
Saravanan, TJ
Bisht, K
Kabeer, KISA
AF Kumar, Aman
Saravanan, T. Jothi
Bisht, Kunal
Kabeer, K. I. Syed Ahmed
TI A review on the utilization of red mud for the production of geopolymer
and alkali activated concrete
LA English
DT Review
DE Alkali-activated binder; Fly ash; Ground granulate blast furnace slag;
Rice husk ash; Metakaolin; Silica fume
ID ASH-BASED GEOPOLYMER; F FLY-ASH; COMPRESSIVE STRENGTH; WASTE GLASS; COAL
GANGUE; METAKAOLIN; MICROSTRUCTURE; DURABILITY; BEHAVIOR; CEMENT
AB The production of ordinary Portland cement releases many greenhouse gases, which
have led to adverse environmental changes such as global warming and climate
change. These phenomena have invigorated the utilization of various industrial
waste products to synthesize geopolymer materials and alkali-activated binders
(AAB) to alleviate OPC's use in construction and building materials. Red Mud (RM)
is one such harmful radioactive waste material generated as a by-product in
aluminum production by Bayer's process. This article highlights RM's utilization of
materials such as fly ash, ground granulated blast furnace slag, silica fume,
metakaolin, refuse mudstone, and rice husk ash to synthesize geopolymer and AAB
samples. The heavy metal ions present in the raw materials in their weak acid-
soluble and reducible fraction were in their residual and oxidizable fractions in
the geopolymer, providing better stability and curing a severe threat to the
environment. The freeze-thaw results showed that the mass-loss rate of the
geopolymer was less than that of concrete. The geopolymer samples exhibited
activity concentration levels well within the prescribed limit. Studies also
include the analysis of Fe's role in the ettringite structure using the Mo center
dot ssbauer spectra analysis. Besides, an overview of the recent advances in the
use of RM for geopolymer synthesis has been presented in terms of hardened, fresh,
and thermal properties and geopolymer and AAB's microstructure analysis. The effect
of ambient curing, heat treatment, elevated temperature curing, and autoclave
curing has been briefly outlined, along with the impact of the RM fraction in the
geopolymer samples. The research findings revealed that the RM-based geopolymer and
AAB manifested similar properties to OPC concrete for various civil engineering
applications.
C1 [Kumar, Aman; Saravanan, T. Jothi] Indian Inst Technol Bhubaneswar, Sch
Infrastruct, Bhubaneswar, India.
[Bisht, Kunal] KIET Grp Inst, Dept Civil Engn, Muradnagar, India.
[Kabeer, K. I. Syed Ahmed] SRM Inst Sci & Technol, Sch Architecture & Interior
Design, Sonipat, India.
Technology (IIT) - Bhubaneswar; KIET Group of Institutions; SRM
University Haryana
RP Saravanan, TJ (corresponding author), Indian Inst Technol Bhubaneswar, Sch
Infrastruct, Bhubaneswar, India.
EM tjs@iitbbs.ac.in
RI BISHT, KUNAL/ABG-4834-2021; Kabeer, Syed Ahmed/AAC-2200-2020
OI Kabeer, Syed Ahmed/0000-0002-3243-583X; Kumar, Aman/0000-0003-0935-166X;
Bisht, Dr. Kunal/0000-0002-8849-832X
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NR 60
TC 39
Z9 39
U1 25
U2 125
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 4
PY 2021
VL 302
AR 124170
DI 10.1016/j.conbuildmat.2021.124170
EA JUL 2021
PG 28
GA UK1YN
UT WOS:000691771800002
DA 2023-12-05
ER
PT J
AU Aboulayt, A
Souayfan, F
Roziere, E
Jaafri, R
El Idrissi, AC
Moussa, R
Justino, C
Loukili, A
AF Aboulayt, Abdelilah
Souayfan, Faten
Roziere, Emmanuel
Jaafri, Reda
El Idrissi, Anass Cherki
Moussa, Redouane
Justino, Christophe
Loukili, Ahmed
TI Alkali-activated grouts based on slag-fly ash mixtures: From early-age
characterization to long-term phase composition
LA English
DT Article
DE Grouts; Alkali-activated binder; Fly ash; Ground granulated
blast-furnace slag; NMR; Phase composition
ID BLAST-FURNACE SLAG; A-S-H; SOLID-STATE NMR; REACTION-KINETICS; ACID
ATTACK; GEOPOLYMER; CEMENT; SILICATE; METAKAOLIN; SI-29
AB Alkali-activation and the combination of slag and fly ash are expected to
improve the chemical stability of grouts designed for underground works. Sodium
silicate activated grout mixtures have been designed with a liquid activator volume
fraction of 75%. As the data related to such high water-to-solid ratios are scarce,
a comprehensive study has been designed in order to determine the phase composition
of these grouts and thus understand the influence of fly ash proportion on
engineering properties of grouts at both fresh and hardened states. The reactivity
at early-age is mainly provided by slag with a drop in strength from 60% of fly
ash. Nuclear magnetic resonance (NMR), X-ray diffraction (XRD), and Fourier
transform infrared spectroscopy (FTIR) have been used to investigate the phase
assemblage at long term (700 days). The alkali-activation of slag mainly produces a
calcium silicate hydrate substituted with aluminum (C A S H). From 20% of fly ash
the CASH phase coexists with sodium aluminosilicate gel N-A-S-H, predominant from
60% of fly ash. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Aboulayt, Abdelilah; Souayfan, Faten; Roziere, Emmanuel; Jaafri, Reda; El
Idrissi, Anass Cherki; Loukili, Ahmed] Ecole Cent Nantes, UMR CNRS 6183, Civil Engn
& Mech Res Inst GeM, 1 Rue Noe, F-44321 Nantes, France.
[Aboulayt, Abdelilah] Mohammed VI Polytech Univ, Mat Sci Energy & Nanoengn Dept,
Ben Guerir 43150, Morocco.
[Moussa, Redouane] Univ Hassan II Casablanca, Fac Sci Ain Chock, Lab Phys Chem
Inorgan Mat, Casablanca, Morocco.
[Justino, Christophe] Soletanche Bachy, Chemin Proc, F-77130 Montereau Fault
Yonne, France.
C3 Nantes Universite; Ecole Centrale de Nantes; Centre National de la
Recherche Scientifique (CNRS); Mohammed VI Polytechnic University;
Hassan II University of Casablanca
RP Roziere, E (corresponding author), Ecole Cent Nantes, UMR CNRS 6183, Civil Engn
& Mech Res Inst GeM, 1 Rue Noe, F-44321 Nantes, France.
EM emmanuel.roziere@ec-nantes.fr
OI ABOULAYT, Abdelilah/0000-0002-6056-6693; , LOUKILI/0000-0001-7921-2740
FU Erasmus mundus (Eu-METALIC II) program; Soletanche Bachy company
FX Erasmus mundus (Eu-METALIC II) program is acknowledged for the financial
support of Dr. Abdelilah Aboulayt's post-doctoral mobility. This study
has also been partially funded by Soletanche Bachy company.
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NR 63
TC 39
Z9 39
U1 4
U2 62
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD NOV 10
PY 2020
VL 260
AR 120510
DI 10.1016/j.conbuildmat.2020.120510
PG 13
GA NW4AC
UT WOS:000574950300007
DA 2023-12-05
ER
PT J
AU Ghanim, B
Murnane, JG
O'Donoghue, L
Courtney, R
Pembroke, JT
O'Dwyer, TF
AF Ghanim, Bashir
Murnane, John G.
O'Donoghue, Lisa
Courtney, Ronan
Pembroke, J. Tony
O'Dwyer, Thomas F.
TI Removal of vanadium from aqueous solution using a red mud modified saw
dust biochar
SO JOURNAL OF WATER PROCESS ENGINEERING
LA English
DT Article
DE Modified biochar; Red mud; Saw dust; Vanadium; Adsorption; Bauxite
residue
ID BAUXITE RESIDUE; WASTE-WATER; ADSORPTIVE PERFORMANCE; STEEL SLAG;
SORPTION; MONTMORILLONITE; BATCH; KINETICS; RECOVERY; SEAWATER
AB Adsorption studies were carried out on a red mud modified sawdust biochar
material to assess its capacity in the removal of vanadium (V) from aqueous
solution. In this study, a number of parameters which can potentially influence
V(V) adsorption were investigated including equilibrium V(V) solution
concentration, contact time for effective V(V) removal, temperature of the
adsorption process, solution pH and ionic strength. The uptake of V (V) was shown
to be heavily influenced by solution pH with maximum uptake (16.45 mg g(-1))
achieved in the pH range of 3.5 - 5.5. The adsorption process was best described by
the Langmuir model. The kinetics of the adsorption process indicated that V(V)
uptake occurred within 60 min of contact and that pseudo-second order kinetics best
described the kinetics of the overall adsorption process. There was a clear
increase in V(V) uptake with increasing temperature (range 293-343 K) indicating an
endothermic adsorption process and the level of uptake remained largely unchanged
at solution salt concentrations of up to 0.1 M NaCl and competing cation
concentrations of up to 2000 mg L-1 of sodium and 200 mg L-1 aluminium. The
relatively weak interaction between V(V) and the modified biochar surface may
indicate a possibility of recovery of the bound V(V) and subsequent regeneration of
the adsorbent.
C1 [Ghanim, Bashir; Pembroke, J. Tony; O'Dwyer, Thomas F.] Univ Limerick, Sch Nat
Sci, Dept Chem Sci, Limerick, Ireland.
[Courtney, Ronan] Univ Limerick, Sch Nat Sci, Dept Biol Sci, Limerick, Ireland.
[Murnane, John G.; O'Donoghue, Lisa] Univ Limerick, Sch Engn, Limerick, Ireland.
[Ghanim, Bashir; Courtney, Ronan; Pembroke, J. Tony; O'Dwyer, Thomas F.] Univ
Limerick, Bernal Inst, Limerick, Ireland.
C3 University of Limerick; University of Limerick; University of Limerick;
University of Limerick
RP O'Dwyer, TF (corresponding author), Univ Limerick, Sch Nat Sci, Dept Chem Sci,
Limerick, Ireland.
EM tom.odwyer@ul.ie
RI O'Dwyer, Thomas/CAA-2411-2022; O'Dwyer, Thomas/A-3146-2013; Murnane,
John/D-2456-2017; Pembroke, J Tony/AAJ-2422-2021
OI O'Dwyer, Thomas/0000-0002-2733-9245; Murnane, John/0000-0003-4327-5234;
Pembroke, J Tony/0000-0001-9340-7026
FU Geological Survey of Ireland (GSI) [2018-ERAMIN2-002]; Irish
Environmental Protection Agency (EPA); EU ERA-MIN2 award [86]
FX The authors acknowledge support from the Geological Survey of Ireland
(GSI, project no. 2018-ERAMIN2-002), the Irish Environmental Protection
Agency (EPA) and an EU ERA-MIN2 award to the EU Biomimic Consortium (ID
T86).
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NR 49
TC 39
Z9 41
U1 5
U2 69
PU ELSEVIER
PI AMSTERDAM
SN 2214-7144
J9 J WATER PROCESS ENG
JI J. Water Process. Eng.
PD FEB
PY 2020
VL 33
AR 101076
DI 10.1016/j.jwpe.2019.101076
PG 9
WC Engineering, Environmental; Engineering, Chemical; Water Resources
GA KR4OO
UT WOS:000517599700080
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Liu, Q
Liu, WZ
Hu, JP
Wang, L
Gao, JQ
Liang, B
Yue, HR
Zhang, GQ
Luo, DM
Li, C
AF Liu, Qiang
Liu, Weizao
Hu, Jinpeng
Wang, Lin
Gao, Jianqiu
Liang, Bin
Yue, Hairong
Zhang, Guoquan
Luo, Dongmei
Li, Chun
TI Energy-efficient mineral carbonation of blast furnace slag with high
value-added products
LA English
DT Article
DE Blast furnace slag; Carbon dioxide utilization; Mineral sequestration;
CO2 net-emission reduction
ID WOLLASTONITE CARBONATION; STEELMAKING SLAGS; CALCIUM-CARBONATE; CO2;
FIXATION; SEQUESTRATION; REGENERATION; DISSOLUTION; ELECTRICITY;
GENERATION
AB Large quantities of CO2 and blast furnace (BF) slag are discharged in the iron
and steel industry. Mineral carbonation of blast furnace slag can offer substantial
CO2 emission reduction and comprehensive utilization of the solid waste. An energy-
and cost-efficient mineral carbonation technology combined with NH3 capturing CO2
and simultaneous power generation is presented in this article. In this process,
blast furnace slag was leached with recyclable ammonium bisulphate (ABS) to extract
Ca, Mg and Al. Gaseous ammonia, which is produced during ammonium sulphate (AS)
roasting for ABS regeneration, was used to capture CO2 in flue gases using a CO2
mineralization cell (CMC) to simultaneously generate NH4HCO3 and electricity. The
extracted CaSO4 and MgSO4 reacted with an NH4HCO3/NH3 solution to realize stable
CO2 sequestration while the extracted Al was recovered in the form of aluminium
ammonium sulphate, which is a high value-added product. The process parameters and
efficiency of the leaching, mineralization and Al recovery were investigated in
detail in the present study. The results showed that approximately 91% of Mg and
97% of Ca in the BF slag were converted into corresponding carbonates and 76% of
aluminium was recovered in the form of NH4Al(SO4)(2)12H(2)O with a purity of 99.6
wt.%. 3802 kg of blast furnace slag was required for sequestration of 1000 kg CO2.
A preliminary energy analysis indicated that although the present process was
somewhat energy intensive without a net reduction of CO2 emission, an improved
process, which combined the NH3 capturing CO2 and simultaneous generating of
electrical energy with a mixed ammonium sulphate (AS)+ blast furnace (BF) slag
roasting instead of the separated ammonium sulphate roasting and ammonium
bisulphate aqueous leaching of the blast furnace slag, was energy-efficient with a
567 kg net reduction of CO2 emission during the sequestration of 1000 kg of CO2. An
economic analysis of the process demonstrated that the sales revenue of the primary
products after deducting the cost of raw materials reached up to $427 for
sequestration of 1000 kg of CO2. (C) 2018 Elsevier Ltd. All rights reserved.
C1 [Liu, Qiang; Liu, Weizao; Hu, Jinpeng; Wang, Lin; Gao, Jianqiu; Liang, Bin; Yue,
Hairong; Zhang, Guoquan; Luo, Dongmei; Li, Chun] Sichuan Univ, Coll Chem Engn,
Chengdu 610065, Sichuan, Peoples R China.
EM lic@scu.edu.cn
RI Liang, Bin/JHU-0581-2023; Liu, Weizao/K-5038-2019; yue,
Hairong/D-1874-2013
OI Liu, Weizao/0000-0003-0976-2864;
[2016YFB0600904]; Fundamental Research Funds for the Central
Universities [2012017yjsy112]
Projects for Fundamental Research and Development of China
(2016YFB0600904) and The Fundamental Research Funds for the Central
Universities (2012017yjsy112).
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TC 39
Z9 43
U1 14
U2 107
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD OCT 1
PY 2018
VL 197
BP 242
EP 252
DI 10.1016/j.jclepro.2018.06.150
PN 1
PG 11
& Ecology
GA GQ8JA
UT WOS:000441998400024
DA 2023-12-05
ER
PT J
AU Richardson, IG
Li, S
AF Richardson, I. G.
Li, S.
TI Composition and structure of an 18-year-old 5M KOH-activated ground
granulated blast-furnace slag paste
LA English
DT Article
DE Slag; NMR; TEM; Microstructure; Alkali activation
ID C-S-H; ORDINARY PORTLAND-CEMENT; NMR; ALUMINUM; MICROSTRUCTURE;
MICROANALYSIS; HYDRATION; AL-27
AB The main hydration products were C-A-S-H(I), present in both inner (Ip) and
outer product (Op), and a Mg-Al layered double hydroxide (LDH), present only in the
Ip. The composition of C-A-S-H(I) was the same in Op and Ip. Reduced scatter in the
data with age suggests a tendency towards compositional homogeneity. The mean
length of the aluminosilicate anions in the C-A-S-H(I) increased with age. The
layer spacings of the C-A-S-H(I) and Mg-Al LDH had not changed significantly with
age. The Mg/Al ratio of the LDH was about 2.6 and had not changed between 1 and 18
years. (C) 2018 Elsevier Ltd. All rights reserved.
C1 [Richardson, I. G.; Li, S.] Univ Leeds, Sch Civil Engn, Leeds LS2 9JT, W
Yorkshire, England.
[Li, S.] Haerbin Inst Technol, Sch Civil Engn, Haerbin 150000, Heilongjiang,
Peoples R China.
C3 University of Leeds; Harbin Institute of Technology
EM i.g.richardson@leeds.ac.uk
FU UK's Nuclear Decommissioning Authority
FX Thanks are due to the UK's Nuclear Decommissioning Authority for funding
the work, including the provision of a fully funded studentship for SL
at the University of Leeds.
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U2 22
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD APR 20
PY 2018
VL 168
BP 404
EP 411
DI 10.1016/j.conbuildmat.2018.02.034
PG 8
GA GD8IU
UT WOS:000430756900036
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Wang, KP
Jiang, M
Wang, XH
Wang, Y
Zhao, HQ
Cao, ZM
AF Wang, Kunpeng
Jiang, Min
Wang, Xinhua
Wang, Ying
Zhao, Haoqian
Cao, Zhanmin
TI Formation Mechanism of
CaO-SiO2-Al2O3-(MgO) Inclusions in
Si-Mn-Killed Steel with Limited Aluminum Content During the Low Basicity
Slag Refining
LA English
DT Article
ID SYSTEM
AB Pilot trails were carried out to study the formation mechanism of CaO-SiO2-
Al2O3-(MgO) inclusions in tire cord steel. 48 samples were taken from 8 heats of
liquid steel during secondary refining, which were subsequently examined by an
automatic scanning electron microscope with energy dispersive spectrometer (SEM-
EDS). Characteristics of thousands of oxide inclusions at different refining stages
were obtained, including their compositions, sizes, morphologies, etc. Based on the
obtained information of inclusions, details during formation of CaO-SiO2-Al2O3-
(MgO) inclusions were revealed and a new mechanism was proposed, including their
origin, formation, and evolution during the refining process. It was found that
CaO-SiO2-Al2O3-(MgO) inclusions were initially originated from the CaO-SiO2-MnO-
(MgO) inclusions, which were formed during BOF tapping by the coalescence between
MnO-SiO2 deoxidation products and the emulsified slag particles because of violent
flow of steel. This can be well confirmed by the evaluation of the formation
thermodynamics of CaO-SiO2-MnO-(MgO) inclusions, which was proved very difficult to
be produced by intrinsic reactions inside liquid steel. Because of chemical
reactions between CaO-SiO2-MnO-(MgO) inclusions and molten steel, they were mainly
changed into CaO-SiO2-MnO-Al2O3-(MgO) and partially into CaO-SiO2-Al2O3-(MgO),
which may be detrimental to the cold drawing ability of coils. Based on this
finding, improvements were made in industrial production during BOF tapping and
secondary refining. The results indicated that such (CaO-SiO2)-based inclusions
existed in conventional process were effectively decreased after the improvements.
C1 [Wang, Kunpeng; Jiang, Min; Wang, Xinhua; Cao, Zhanmin] Univ Sci & Technol
Beijing, Sch Met & Ecol Engn, Beijing 100083, Peoples R China.
[Wang, Ying; Zhao, Haoqian] Xingtai Iron & Steel Corp Ltd, Xingtai 054027,
Hebei, Peoples R China.
EM jiangmin@ustb.edu.cn
RI Wang, Xinhua/ISR-8520-2023; Wang, Xiaoqiang/IQS-3727-2023; Wang,
Xin/HZL-4695-2023; Cao, Zhanmin/M-1575-2016; Wang, Xin/JCE-2009-2023;
Wang, Xin/GYU-1129-2022; Wang, Xin/AAN-8435-2021
OI Cao, Zhanmin/0000-0001-7682-5250; Wang, Xin/0000-0002-4457-7376; Wang,
Xin/0000-0002-4457-7376
FU Xingtai Iron and Steel Corp., Ltd.
FX Sincere gratitude and appreciation should be expressed by the authors to
Xingtai Iron and Steel Corp., Ltd. for supporting of the research and
great help during industrial samplings.
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NR 23
TC 39
Z9 46
U1 2
U2 36
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD FEB
PY 2016
VL 47
IS 1
BP 282
EP 290
DI 10.1007/s11663-015-0502-z
PG 9
Engineering
GA DB7JX
UT WOS:000368692300029
DA 2023-12-05
ER
PT J
AU Arbi, K
Palomo, A
Fernández-Jiménez, A
AF Arbi, K.
Palomo, A.
TI Alkali-activated blends of calcium aluminate cement and slag/diatomite
LA English
DT Article
DE Alkaline activation; Geopolymer; Calcium aluminate cement (CAC); Slag;
Diatomite
ID SOLID-STATE AL-27; DIATOMACEOUS-EARTH; FLY-ASH; INORGANIC POLYMERS;
SLAG; METAKAOLIN; HYDRATION; SILICATE; GEOPOLYMERS; CONCRETE
AB The present study deals with the formulation of new cementitious materials via
the alkaline activation of an industrial by-product (blast furnace slag) or a
natural rock (diatomite) in the presence of reactive aluminium sourced from calcium
aluminate cement (CAC). Two blends, one containing 20% CAC and 80% slag and the
other 20% CAC and 80% diatomite, were prepared and activated with sodium sulphate
or a sodium hydroxide solution. The hardened materials were characterised with X-
ray diffraction (XRD) as well as Al-27 and Si-29 nuclear magnetic resonance (NMR)
and tested for their 2-day mechanical strength. The main reaction product was a
cementitious gel that precipitated with crystalline phases such as ettringite, U
phase and katoite. While the slag blend reacted to generate a C-(A)-S-H-like gel
under moderately alkaline conditions, diatomite reactivity proved to be very low
under such conditions. The greater reactivity of both slag and diatomite at high pH
(high alkalinity) favoured their interaction with CAC. (C) 2013 Elsevier Ltd and
Techna Group S.r.l. All rights reserved.
C1 [Arbi, K.; Palomo, A.; Fernandez-Jimenez, A.] CSIC, Inst Eduardo Torroja, Madrid
28033, Spain.
de Ciencias de la Construccion Eduardo Torroja (IETCC)
RP Arbi, K (corresponding author), CSIC, Inst Eduardo Torroja, Madrid 28033, Spain.
EM kamel@ietcc.csic.es
RI Fernández, ANA Maria/G-2597-2016; PALOMO, ANGEL/G-2584-2016
OI Fernández, ANA Maria/0000-0002-5721-2923; Arbi,
kamel/0000-0002-4630-438X; PALOMO, ANGEL/0000-0002-6964-2269
FU Spanish Ministry of the Economy and Competitive Affairs [BIA
2010-17530]; Spanish National Research Council (CSIC); European Social
Fund
FX This study was funded by the Spanish Ministry of the Economy and
Competitive Affairs under Project BIA 2010-17530. K. Arbi worked under a
2009 Post-graduate Studies Council contract, co-funded by the Spanish
National Research Council (CSIC) and the European Social Fund.
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NR 46
TC 39
Z9 41
U1 6
U2 135
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD DEC
PY 2013
VL 39
IS 8
BP 9237
EP 9245
DI 10.1016/j.ceramint.2013.05.031
PG 9
GA 236YJ
UT WOS:000325835100091
DA 2023-12-05
ER
PT J
AU Roy, D
Pistorius, PC
Fruehan, RJ
AF Roy, Debdutta
Pistorius, Petrus Christiaan
Fruehan, Richard J.
TI Effect of Silicon on the Desulfurization of Al-Killed Steels: Part I.
Mathematical Model
LA English
DT Article
AB Recent observations suggest that increased silicon levels improve ladle
desulfurization of aluminum-killed steel. While the overall desulfurization
reaction of Al-killed steels does not show a direct role of silicon in
desulfurization, model calculations are presented which test the idea that silicon
suppresses the reduction of silica which can consume aluminum at the slag/metal
interface. Consumption of aluminum would increase the oxygen potential at the
slag/metal interface and decrease the sulfur partition coefficient between slag and
metal. The model considers the coupled reactions of the reduction of silica, iron
oxide, and manganese oxide in the slag and desulfurization of the steel by
aluminum. The results show that silicon can indeed suppress consumption of aluminum
at the slag/metal interface by side reactions other than desulfurization, with
silicon affecting both the kinetics and the equilibrium of desulfurization. (C) The
Minerals, Metals & Materials Society and ASM International 2013
C1 [Roy, Debdutta; Pistorius, Petrus Christiaan; Fruehan, Richard J.] Carnegie
Mellon Univ, Dept Mat Sci & Engn, Ctr Iron & Steelmaking Res, Pittsburgh, PA 15213
USA.
RP Pistorius, PC (corresponding author), Carnegie Mellon Univ, Dept Mat Sci & Engn,
Ctr Iron & Steelmaking Res, 5000 Forbes Ave, Pittsburgh, PA 15213 USA.
EM pistorius@cmu.edu
RI Pistorius, Petrus Christiaan/A-8247-2011
OI Pistorius, Petrus Christiaan/0000-0002-2966-1879
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NR 16
TC 39
Z9 45
U1 2
U2 27
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD OCT
PY 2013
VL 44
IS 5
BP 1086
EP 1094
DI 10.1007/s11663-013-9813-0
PG 9
Engineering
GA 231QI
UT WOS:000325431900007
DA 2023-12-05
ER
PT J
AU Obenaus-Emler, R
Falah, M
Illikainen, M
AF Obenaus-Emler, R.
Falah, M.
Illikainen, M.
TI Assessment of mine tailings as precursors for alkali-activated materials
for on-site applications
LA English
DT Article
DE Alkali-activated binders; Mine tailings; Alternative raw materials;
Environmental impact
AB Year after year the mining industry generates 5-7 billion metric tons of
tailings worldwide. They are mostly disposed rather than valorised. The substantial
amounts of tailings has led to growing concerns about their ecological and
environmental impacts such as occupation of large areas of land, generation of
windblown dust, and contamination of surface and underground water. Over the past
years the mining industry has been subjected to increase environmental principles.
As the consequence, besides waste rock and water management, tailings management
becomes a progressively important factor for ecologic and economic reasons.
Mine tailings from flotation processes are normally disposed in impoundments on
the surface. This may cause environmental and safety problems including serious
water pollution arising from contamination of surface water, groundwater, and soils
due to the leaching of heavy metals, process reagents, and Sulphur compounds.
Recently the process of alkali-activation and geopolymerisation has been explored
as a potential method for tailings consolidation and heavy metal fixation. The
tailings of many existing mining operations contain the aluminosilicate minerals
needed for alkali-activation at least to some extent. From a sustainability point
of view it makes sense to use alkali-activated products from tailings directly on
the mine site as e.g. (1) backfill material applied to fill open cavities from the
(underground) mining operation and (2) cover materials for surface deposits of
tailings in order to store them ecologically safe and sealed off from the
environment.
Mine tailings from different mining operations around the world have been
investigated regarding their potential use as precursors for alkali-activated
materials. An assessment of the release of gel forming elements into alkaline
solutions was performed by leaching experiments under various conditions (time,
concentration of the solvent, and temperature). Compared to traditional alkali-
activated precursor materials the release of aluminium and silicon is in general
low for the mine tailings investigated. However, results indicate a favourable
ratio of Si/Al for the formation of gels similar to other alkali-activated
products. Additionally, the leached calcium can contribute to the strength of the
resulting products by forming C-S-H gels when a considerable amount of Si is
present in the pore solution either from the activator or dissolved from the
material itself.
The results of the leaching tests were used to facilitate the mix design for
alkali-activated products. In order to increase the mechanical strength of the
final product different approaches were considered: (1) addition of reactive
materials (e.g. blast furnace slag), (2) increasing the reactivity of the tailings
by grinding, and (3) increasing the reactivity by curing at elevated temperature.
Depending on the tailings type, the mix design, and the curing conditions the final
material shows a compressive strength in excess of 30 MPa even for curing at low
temperatures.
The investigated mine tailings can potentially be used for various applications
on the mine site. With regard to specific target applications a further evaluation
of long term properties of the resulting products (e.g. freeze-thaw resistance) has
to be performed. Furthermore, results indicate that products with even higher
strength can be manufactured by further reducing the particle size of the tailings
or by the addition of other reactive materials. (C) 2020 The Authors. Published by
Elsevier Ltd.
C1 [Obenaus-Emler, R.] Univ Leoben, Leoben, Austria.
[Falah, M.; Illikainen, M.] Univ Oulu, Oulu, Finland.
C3 University of Leoben; University of Oulu
RP Obenaus-Emler, R (corresponding author), Univ Leoben, Leoben, Austria.
EM emler@unileoben.ac.at
OI Illikainen, Mirja/0000-0001-7545-4574
FU European Union's Horizon 2020 research and innovation programme
[730480]; H2020 Societal Challenges Programme [730480] Funding Source:
H2020 Societal Challenges Programme
FX The results presented in this paper are part of the research project
ITERAMS -Integrated mineral technologies for more sustainable raw
material supply. This project has received funding from the European
Union's Horizon 2020 research and innovation programme under grant
agreement No 730480.
CR Ahmari S, 2013, CONSTR BUILD MATER, V44, P743, DOI
10.1016/j.conbuildmat.2013.03.075
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10.1016/j.jhazmat.2006.02.044
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10.1016/j.conbuildmat.2011.04.005
NR 15
TC 38
Z9 41
U1 8
U2 43
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUN 20
PY 2020
VL 246
AR 118470
DI 10.1016/j.conbuildmat.2020.118470
PG 10
GA LF3GR
UT WOS:000527309800037
DA 2023-12-05
ER
PT J
AU Zhang, Y
Zhang, JL
Jiang, JY
Hou, DS
Zhang, JR
AF Zhang, Yu
Zhang, Jinglin
Jiang, Jinyang
Hou, Dongshuai
Zhang, Jinrui
TI The effect of water molecules on the structure, dynamics, and mechanical
properties of sodium aluminosilicate hydrate (NASH) gel: A molecular
dynamics study
LA English
DT Article
DE De-polymerization; Hydrolytic reaction; Reactive force field; Sodium
aluminosilicate hydrate gel
ID CALCIUM SILICATE HYDRATE; FLY-ASH; GEOPOLYMER; TEMPERATURE; SIMULATION;
TRANSPORT; SI-29; SLAG
AB Sodium aluminosilicate hydrate (NASH) gel is the primary adhesive constituent in
geopolymer. In the nanostructure of NASH gel, structural water has a great impact
on the structure and mechanical properties of NASH. In this study, molecular
dynamics simulation is utilized to investigate the effect of water on the
structure, dynamics, and mechanical properties of NASH gel. The result shows that
water molecules in NASH gel are physically and chemically bound to Si-Al framework
by the formation of H-bond as well as Si-OH, Al-OH and Na-OH. These hydrolytic
reactions result in the elongation of Al-O bond and the structural transformation
from tetrahedral aluminum to pentahedral aluminum. The structural weakening caused
by hydrolysis for aluminate skeleton leads to an increase in the mobility of
aluminum and a decrease in the stability of Al-O bond. However, the sodium in NASH
structure becomes stabilized as a result of the hydrolysis of aluminate skeleton
and the formation of Na-OH. In contrast, silicate skeleton exhibits hydrophobic
nature and not sensitive to water. Mechanically, hydrolytic reaction weakens the
tensile performance of NASH gel by two mechanisms, which is promoting the de-
polymerization of Si-Al framework during the tensile process, and preventing the
re-polymerization of broken framework. Meanwhile, the de-polymerization of Si-Al
framework can further promote hydrolytic reaction during the tensile testing. (C)
C1 [Zhang, Yu; Zhang, Jinglin; Hou, Dongshuai] Qingdao Univ Technol, Dept Civil
Engn, Qingdao 266033, Peoples R China.
[Zhang, Jinglin] Southeast Univ, Sch Mat Sci & Engn, Jiangsu Key Lab Construct
Mat, Nanjing 211189, Jiangsu, Peoples R China.
[Zhang, Jinrui] Tianjin Univ, Dept Civil Engn, Tianjin, Peoples R China.
C3 Qingdao University of Technology; Southeast University - China; Tianjin
University
RP Hou, DS (corresponding author), Qingdao Univ Technol, Dept Civil Engn, Qingdao
EM dshou@outlook.com
OI Hou, Dongshuai/0000-0002-1252-2987
FU National Natural science foundation of China [51508292]; China Ministry
of Science and Technology [2015CB655100]; Natural science foundation of
Shandong Province [ZR2017JL024, 16-5-1-96-jch]
FX Financial support from National Natural science foundation of China
under Grant 51508292, the China Ministry of Science and Technology under
Grant 2015CB655100, Natural science foundation of Shandong Province
under Grant ZR2017JL024, Qingdao Research Program 16-5-1-96-jch are
gratefully acknowledged.
CR Arbi K, 2016, IND ENG CHEM RES, V55, P5439, DOI 10.1021/acs.iecr.6b00559
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NR 40
TC 38
Z9 40
U1 17
U2 120
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD DEC 30
PY 2018
VL 193
BP 491
EP 500
DI 10.1016/j.conbuildmat.2018.10.221
PG 10
GA HD8NU
UT WOS:000452814600045
DA 2023-12-05
ER
PT J
AU Wang, JY
Huang, XW
Wang, LS
Wang, Q
Yan, YN
Zhao, N
Cui, DL
Feng, ZY
AF Wang, Jinyu
Huang, Xiaowei
Wang, Liangshi
Wang, Qiang
Yan, Yannan
Zhao, Na
Cui, Dali
Feng, Zongyu
TI Kinetics study on the leaching of rare earth and aluminum from FCC
catalyst waste slag using hydrochloric acid
SO HYDROMETALLURGY
LA English
DT Article
DE Rare earths; Aluminum; Leaching kinetics; FCC catalyst; Waste slag
ID METAL HYDRIDE BATTERIES; RECOVERY; ASH; ELEMENTS; SCRAPS; ORE
AB During the industrial production of FCC catalyst, a large amount of FCC catalyst
waste slag (FCC waste slag) containing rare earths and aluminum was generated.
Landfill was commonly used to deal with the slag, which may cause serious
environmental degradation and resources depletion. A novel hydrometallurgical
process consisting of hydrochloric acid leaching and subsequent neutralization is
proposed to recover rare earths and aluminum from the FCC waste slag. The effect of
leaching temperature, hydrochloric acid concentration and leaching time on the
metal extraction are studied. The leaching kinetics of aluminum and rare earths are
also investigated. It is shown that 91.0% of La, 92.2% of Ce, and 94.2% of Al are
extracted under optimum leaching conditions of hydrochloric acid concentration 9.00
mol/L, solid to liquid ratio (S/L ratio) 0.05 g/mL, leaching temperature 293 K and
leaching time 30 min. The leaching behaviors of aluminum and rare earths follow a
shrinking core model which can be expressed as 1 - (1 - x)(1/3) = k(ap)t, and the
overall leaching process is controlled by the surface chemical reaction. The
activation energies for the leaching of Al, La, and Ce are 6.24, 9.71, and 9.10
kJ/mol, respectively. Zeolite Na-Y and FCC catalyst presented in the FCC waste slag
is leached with HCl individually. Only the FCC catalyst has a negative effect on
the leaching of rare earths and aluminum. Finally, selective precipitation is
employed to produce Al(OH)(3) and RE(OH)(3), which can be reused for the industrial
production of FCC catalyst.
C1 [Wang, Jinyu; Huang, Xiaowei; Wang, Liangshi; Wang, Qiang; Yan, Yannan; Zhao,
Na; Cui, Dali; Feng, Zongyu] Gen Res Inst Nonferrous Met, Natl Engn Res Ctr Rare
Earth Mat, Beijing 100088, Peoples R China.
C3 General Research Institute for Nonferrous Metals
RP Huang, XW; Wang, LS (corresponding author), Gen Res Inst Nonferrous Met, Natl
Engn Res Ctr Rare Earth Mat, Beijing 100088, Peoples R China.
EM hxw0129@188.com; wls1657@163.com
RI Wang, Liangshi/Q-8323-2017
OI Wang, Liangshi/0000-0003-4432-0842
FU Ministry of Industry and Information Technology of China; Beijing Nova
Program [Z161100004916108]
FX This work was supported by the Rare-earth Adjustment Upgrade Projects of
Ministry of Industry and Information Technology of China and Beijing
Nova Program (grant number Z161100004916108).
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NR 36
TC 38
Z9 47
U1 4
U2 60
PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD AUG
PY 2017
VL 171
BP 312
EP 319
DI 10.1016/j.hydromet.2017.06.007
PG 8
GA FD9WY
UT WOS:000407874000040
DA 2023-12-05
ER
PT J
AU Mongalo, L
Lopis, AS
Venter, GA
AF Mongalo, Lehlohonolo
Lopis, Anton S.
Venter, Gerhard A.
TI Molecular dynamics simulations of the structural properties and
electrical conductivities of
CaO-MgO-Al2O3-SiO2 melts
LA English
DT Article
DE Aluminosilicate; Molecular dynamics; Structural properties; Diffusion;
Electrical conductivity
ID CALCIUM ALUMINOSILICATE GLASSES; 1500 DEGREES-C; MQ-MAS NMR; AL-O-AL;
SILICATE LIQUIDS; SELF-DIFFUSION; IONIC LIQUIDS; ALUMINUM; SPECTROSCOPY;
TEMPERATURE
AB The structural properties and electrical conductivities of nine CaO-MgO-Al2O3-
SiO2 slags with compositions in the peralkaline region have been calculated using
molecular dynamics simulations. The proportion of nonbridging oxygen (NBO) and
bridging oxygen (BO) atoms were determined from simulation and shown to be in
reasonable agreement with theoretical prediction. Bridging oxygen atoms were
classified into Si-O-Si, Si-O-Al or Al-O-Al linkages and the results used to
establish whether the Al avoidance principle is applicable. The number of bridging
oxygens coordinated to tetrahedral [SiO4](4-) and [AlO4](5-) units, namely the Q(n)
distribution, was determined. Although a good comparison to the theoretical average
Q was found at low basicity, at higher basicity greater deviation was seen.
Electrical conductivities, taking cross-correlations into account, were in
excellent agreement with experimentally measured values, although Nernst-Einstein
conductivities, estimated from self-diffusion coefficients alone, showed large
deviations. Molecular dynamics simulations are therefore able to reliably predict
conductivity, but values calculated indirectly, i.e. using the Nemst-Einstein
relationship, should be used with care. At low basicity theoretical predictions of
structural disorder, based on Zachariasen's Random Network Model, are in reasonable
agreement with simulation, but this agreement worsens as the proportion of network
modifying cations increases. (C) 2016 Elsevier B.V. All rights reserved.
C1 [Mongalo, Lehlohonolo; Venter, Gerhard A.] Univ Cape Town, Sci Comp Res Unit,
ZA-7701 Cape Town, South Africa.
[Mongalo, Lehlohonolo; Venter, Gerhard A.] Univ Cape Town, Dept Chem, ZA-7701
Cape Town, South Africa.
[Lopis, Anton S.] CSIR, Ctr High Performance Comp, 15 Lower Hope St, ZA-7700
Cape Town, South Africa.
C3 University of Cape Town; University of Cape Town; Council for Scientific
& Industrial Research (CSIR) - South Africa
RP Venter, GA (corresponding author), Univ Cape Town, Sci Comp Res Unit, ZA-7701
Cape Town, South Africa.; Venter, GA (corresponding author), Univ Cape Town, Dept
Chem, ZA-7701 Cape Town, South Africa.
EM gerhard.venter@uct.ac.za
RI Venter, Gerhard/GQI-1207-2022; Lopis, Anton/GVU-5441-2022
OI Venter, Gerhard/0000-0003-3993-1198;
FU National Research Foundation (NRF) [IFR1203100525]; DST-NRF Professional
Development Program (PDP) scholarship
FX We would like to thank the Center for High Performance Computing (CHPC)
for computational resources and Quinn Reynolds for his comments on the
manuscript. This work is based on research supported by the National
Research Foundation (NRF) (grant no. IFR1203100525) and funded through a
DST-NRF Professional Development Program (PDP) scholarship awarded to LM
and hosted by Mintek. Any opinion, findings and conclusions or
recommendations expressed in this material are those of the authors and
therefore the NRF does not accept any liability in regard thereto.
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NR 47
TC 38
Z9 40
U1 10
U2 88
PI AMSTERDAM
SN 0022-3093
EI 1873-4812
PD NOV 15
PY 2016
VL 452
BP 194
EP 202
DI 10.1016/j.jnoncrysol.2016.08.042
PG 9
GA EC3TY
UT WOS:000388050800029
DA 2023-12-05
ER
PT J
AU Yan, W
Chen, WQ
Yang, YD
Lippold, C
Mclean, A
AF Yan, Wei
Chen, Weiqing
Yang, Yindong
Lippold, Carsten
Mclean, Alex
TI Effect of Slag Compositions and Additive on Heat Transfer and
Crystallization of Mold Fluxes for High-Al Non-magnetic Steel
LA English
DT Article
DE high-Al steel; heat transfer; crystallization; SHTT; CCT; TTT
ID MEDIUM-CARBON STEELS; HOT THERMOCOUPLE TECHNIQUE; TRANSFER BEHAVIOR;
MECHANISM; VISCOSITY; POWDER; ALLOY; B2O3; NA2O; FILM
AB Intense reaction between silica in mold fluxes and aluminium in liquid steel
during casting of high-Al non-magnetic steel 20Mn23AlV (1.5-2.5 Al in mass percent)
would significantly alter both chemical compositions and properties of mold fluxes.
This would subsequently lead to severe casting problems such as lots of slag rims,
breakout and poor surface quality. Investigation carried out in this paper started
with plant sampling, followed by a look at how the variation of Al2O3/SiO2 ratio
with reaction time can affect the casting process and product quality. Thus, this
work focuses on the study of increasing Al2O3/SiO2 and partial substitution of CaO
with BaO in CaO-SiO2 system mold fluxes in terms of heat transfer and
crystallization behavior. The techniques implemented are heat flux simulator and
single hot thermocouple technique (SHTT). The results showed that an increase in
Al2O3/SiO2 inhibits heat transfer, increases crystallization temperature and
critical cooling rate while shortens incubation time, additionally, accelerates
precipitation of phase with high melting temperature. However, greater substitution
of CaO with BaO accelerates heat transfer, reduces crystallization temperature and
critical cooling rate at the cost of longer incubation time even at elevated
Al2O3/SiO2. Eventually, partial substitution of CaO with BaO, to some extent,
counteracts the effect of increasing Al2O3/SiO2 on heat transfer and
crystallization properties of mold fluxes for casting of high-Al steels.
C1 [Yan, Wei; Chen, Weiqing] Univ Sci & Technol Beijing, State Key Lab Adv Met,
[Yan, Wei; Yang, Yindong; Mclean, Alex] Univ Toronto, Dept Mat Sci & Engn,
Toronto, ON M5S 3E4, Canada.
[Lippold, Carsten] Qingdao Stollberg & Samil Co Ltd, Qingdao 266300, Peoples R
China.
C3 University of Science & Technology Beijing; University of Toronto
RP Yan, W (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
Met, 30 Xueyuan Rd, Beijing 100083, Peoples R China.
EM yanweimetal@gmail.com
RI chen, weiqing/G-3874-2011
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NR 36
TC 38
Z9 40
U1 1
U2 19
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2015
VL 55
IS 5
BP 1000
EP 1009
PG 10
GA CI8YV
UT WOS:000355058500013
DA 2023-12-05
ER
PT J
AU Chiang, YW
Santos, RM
Elsen, J
Meesschaert, B
Martens, JA
Van Gerven, T
AF Chiang, Yi Wai
Santos, Rafael M.
Elsen, Jan
Meesschaert, Boudewijn
Martens, Johan A.
Van Gerven, Tom
TI Towards zero-waste mineral carbon sequestration via two-way valorization
of ironmaking slag
LA English
DT Article
DE Mineral carbonation; Precipitated calcium carbonate; Hydrothermal
conversion; Zeolitic materials; Blast furnace slag; Valorization
ID STEELMAKING SLAGS; HYDROTHERMAL SYNTHESIS; CALCIUM; CO2; ZEOLITES;
DIOXIDE; CAPTURE; STORAGE
AB A three-stage process was developed to transform blast furnace slag (BFS) into
two valuable products: precipitated calcium carbonate (PCC) and zeolitic materials.
The conceptualized process aims to simultaneously achieve sustainable CO2
sequestration and solid waste elimination. Calcium is first selectively extracted
by leaching with an organic acid, followed by carbonation of the leachate to
precipitate CaCO3. In parallel, the hydrothermal conversion of the extracted solid
residues in alkali solution induces the dissolution/precipitation mechanism that
leads to the formation of micro- and meso-porous zeolitic materials. Leaching
selectivity was identified as a key factor in the valorization potential of both
products. Acetic acid satisfactorily limited the leaching of aluminum, required for
the subsequent synthesis of zeolites, and carbonation of the acetic acid leachate
resulted in the production of PCC of varied mineralogy and morphology, depending on
processing conditions. In the hydrothermal conversion stage, the formation of
zeolitic phases was observed, and their characteristics were found to vary
depending on the calcium extraction efficiency in the previous stage, and the
alkali (NaOH) concentration. The zeolitic phases produced, in order of increasing
valorization potential, were: tobermorite, sodalite, lazurite, and analcime. (C)
C1 [Chiang, Yi Wai; Meesschaert, Boudewijn; Martens, Johan A.] Katholieke Univ
Leuven, Dept Microbial & Mol Syst, B-3001 Leuven, Belgium.
[Chiang, Yi Wai] Univ Guelph, Sch Engn, Guelph, ON N1G 2W1, Canada.
[Santos, Rafael M.; Van Gerven, Tom] Katholieke Univ Leuven, Dept Chem Engn, B-
3001 Leuven, Belgium.
[Elsen, Jan] Katholieke Univ Leuven, Dept Earth & Environm Sci, B-3001 Leuven,
Belgium.
C3 KU Leuven; University of Guelph; KU Leuven; KU Leuven
RP Chiang, YW (corresponding author), Katholieke Univ Leuven, Dept Microbial & Mol
Syst, Kasteelpk Arenberg 23, B-3001 Leuven, Belgium.
EM chiange@uoguelph.ca; rafael.santos@alumni.utoronto.ca
RI Chiang, Yi Wai/K-5452-2012; Van Gerven, Tom/B-5806-2015; Meesschaert,
Boudewijn Daniël/B-8420-2015; elsen, jan/AAB-9873-2021; Santos, Rafael
M./G-1657-2011; elsen, jan/AAE-2352-2021
OI Van Gerven, Tom/0000-0003-2051-5696; Meesschaert, Boudewijn
Daniël/0000-0003-2381-7868; Santos, Rafael M./0000-0002-8368-8618;
Chiang, Yi Wai/0000-0002-7798-9166; Martens, Johan/0000-0002-9292-2357;
elsen, jan/0000-0002-4370-3852
FU KU Leuven Industrial Research Fund (IOF); KU Leuven Special Research
Fund (BOF)
FX This work was supported by the KU Leuven Industrial Research Fund (IOF),
through the Knowledge Platform on Sustainable Materialization of
Residues from Thermal Processes into Products (SMaRT-Pro2).
Rafael Santos is grateful for a Postdoctoral Mandate financed by the KU
Leuven Special Research Fund (BOF). The KU Leuven Department of
Metallurgy and Materials Engineering is acknowledged for the use of
WDXRF and SEM-EDX equipment.
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NR 32
TC 38
Z9 41
U1 8
U2 60
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD AUG 1
PY 2014
VL 249
BP 260
EP 269
DI 10.1016/j.cej.2014.03.104
PG 10
SC Engineering
GA AJ3GI
UT WOS:000337554100031
OA Green Submitted, Green Accepted
DA 2023-12-05
ER
PT J
AU Piatak, NM
Seal, RR
AF Piatak, Nadine M.
Seal, Robert R., II
TI Mineralogy and environmental geochemistry of historical iron slag,
Hopewell Furnace National Historic Site, Pennsylvania, USA
LA English
DT Article
ID TRACE-ELEMENTS; BASE-METAL; STABILITY; PYROXENE; RELEASE; SMELTER;
OXYGEN
AB The Hopewell Furnace National Historic Site in southeastern Pennsylvania, which
features an Fe smelter that was operational in the 18th and 19th centuries, is
dominated by three slag piles. Pile 1 slag, from the Hopewell Furnace, and pile 2
slag, likely from the nearby Cornwall Furnace, were both produced in cold-blast
charcoal-fired smelters. In contrast, pile 3 slag was produced in an anthracite
furnace. Ore samples from the nearby Jones and Hopewell mines that fed the smelter
are mainly magnetite-rich with some sulfides (pyrite, chalcopyrite, sphalerite) and
accessory silicates (quartz, garnet, feldspar, and clay minerals). Slag piles 1 and
2 are similar mineralogically containing predominantly skeletal and dendritic
aluminian diopside and augite, skeletal forsteritic olivine, glass, rounded blebs
of metallic Fe, and exotic quartz. Olivine is a major phase in all samples from
pile 2, whereas it occurs in only a few samples from pile 1. Samples of the <2 mm-
size fraction of surface composite slag material or crushed slag from at depth in
piles 1 and 2 are mineralogically similar to the large surface slag fragments from
those piles with the addition of phases such as feldspars, Fe oxides, and clay
minerals that are either secondary weathering products or entrained from the
underlying bedrock. Pile 3 slag contains mostly skeletal forsteritic olivine and
Ti-bearing aluminian diopside, dendritic or fine-grained subhedral melilite, glass,
euhedral spinel, metallic Fe, alabandite-oldhamite solid solution, as well as a
sparse Ti carbonitride phase. The bulk chemistry of the slag is dominated by Al2O3
(8.5-16.2 wt.%), CaO (8.2-26.2 wt.%), MgO (4.2-24.7 wt.%), and SiO2 (36.4-59.8 wt.
%), constituting between 81% and 97% of the mass of the samples. Piles 1 and 2 are
chemically similar; pile 1 slag overall contains the highest Fe2O3, K2O and MnO,
and the lowest MgO concentrations. Pile 3 slag is high in Al2O3, CaO and S, and low
in Fe2O3, K2O and SiO2 compared to the other piles. In general, piles 1 and 2 are
chemically similar to each other, whereas pile 3 is distinct a conclusion that
reflects their mineralogy. The similarities and differences among piles in terms of
mineralogy and major element chemistry result from the different smelting
conditions under which the slag formed and include the fuel source, the composition
of the ore and flux, the type of blast (cold versus hot), which affects the furnace
temperature, and other beneficiation methods.
The three distinct slag piles at Hopewell are enriched in numerous trace
elements, such as As (up to 12 mg/kg), Cd (up to 0.4 mg/kg), Co (up to 31.8 mg/kg),
Cu (up to 647 mg/kg), Mn (up to 0.69 wt.%), Pb (up to 172 mg/kg) and Zn (up to 393
mg/kg), together with Fe (13.9 wt.%), when compared to the average for the
continental crust, with the <2 mm-size fraction commonly containing the highest
concentrations. Enrichments in various elements (e.g., Cd, Co, Cu, Pb, Zn) were
also found in the ore samples. Despite these enrichments, comparison of bulk
chemistry trace-element concentrations to the environmental guidelines suggests
most elements are likely not problematic with the exception of As, Co, Fe and Mn.
Leachate tests that simulate weathering indicate Fe (up to 973 mu g/L) and Mn (up
to 133 mu g/L) are readily released in potentially harmful concentrations compared
to secondary drinking water and some aquatic ecosystem toxicity criteria. Aluminum
and Cu, although not high in the solid compared to environmental guidelines, also
exceed relevant criteria in leachate extracts with maximum concentrations of 2700
mu g/L and 17.7 mu g/L, respectively. In contrast, As and Co, which are significant
in the solids, are not leached in concentrations that exceed guidelines (i.e., 3 mu
g/L or less for both elements). The weathering rates of the Fe metal and Fe oxides,
which host Cu and some Fe, are likely higher than the silicate glass, which hosts
the majority of Al, Mn and some Fe, and the crystalline silicates and spinels
affecting which elements and how much are released into the environment and
surrounding aquatic ecosystem. The mineral assemblages and their chemical
composition, the bulk sample chemistry, and leachability of trace elements are all
important components in understanding the potential environmental impacts of the
slag piles. Published by Elsevier Ltd.
C1 [Piatak, Nadine M.; Seal, Robert R., II] US Geol Survey, Reston, VA 20192 USA.
C3 United States Department of the Interior; United States Geological
Survey
RP Piatak, NM (corresponding author), US Geol Survey, 12201 Sunrise Valley Dr,
Reston, VA 20192 USA.
EM npiatak@usgs.gov
FU NPS/USGS
FX The authors would like to thank Ronald Sloto, Arthur Lilienthal, Jane M.
Hammarstrom, all of the USGS, and Denise M. Levitan, of Virginia Tech
for their assistance in sample collection. Gregory Kolous of Kutztown
University provided the Jones ore samples. We would also like to thanks
the NPS/USGS Water Quality Partnership Program for partially funding the
work. Harvey Belkin of the USGS provided guidance on the SEM and
electron microprobe operations. Ronald Sloto (USGS) and Matthew
Kierstead (PAL Inc.) both provided insight into historical aspects of
the site. The manuscript benefited from reviews by Avery Drake (USGS),
Kathy Rankin (USGS), Ruth Schulte (USGS), Ronald Sloto (USGS), Vojtech
Ettler (Charles University), and an anonymous referee. The use of trade,
product, industry, or firm names in this paper is for descriptive
purposes only and does not constitute endorsement by the US Government.
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NR 46
TC 38
Z9 41
U1 2
U2 54
PI OXFORD
SN 0883-2927
J9 APPL GEOCHEM
JI Appl. Geochem.
PD MAR
PY 2012
VL 27
IS 3
BP 623
EP 643
DI 10.1016/j.apgeochem.2011.12.011
PG 21
GA 894CA
UT WOS:000300403400009
DA 2023-12-05
ER
PT J
AU Tripathi, NN
Nzotta, M
Sandberg, A
Sichen, D
AF Tripathi, NN
Nzotta, M
Sandberg, A
Sichen, D
TI Effect of ladle age on formation of nonmetallic inclusions in ladle
treatment
LA English
DT Article
DE steels; tool steels; ladle metallurgy; inclusions
ID NON-METALLIC INCLUSIONS; DEOXIDATION; STEEL; ALUMINUM; SILICON; SI; AL
AB An experimental study was carried out at Uddeholm Tooling, Hagfors, Sweden to
examine the impact of ladle glaze on the formation of non-metallic inclusions
during the ladle treatment process. Steel samples were taken at various stages of
the process and from ladles of different ages. Inclusion numbers were counted under
an optical microscope. It was found that the total number of inclusions increased
with the ladle age before deoxidation and at the end of the ladle treatment. The
increase was substantial after the ladle had been used more than 18 times.
Inclusions having the smallest sizes were found to make a large contribution to
this increase. This observation was further confirmed by the difference between
total oxygen content and dissolved oxygen content in the steel samples, which also
showed an increase with ladle age. Analysis by SEM-EDX revealed two types of
inclusions before casting, namely, inclusions consisting only of an oxide solution
having a composition very close to 3CaO.Al2O3, and inclusions consisting of the
same oxide solution as well as MgO phase. This finding was in accordance with the
reported result that both 3CaO.Al2O3 and MgO were present in the slag infiltrated
layer of the ladle glaze. It was concluded that ladle glaze is the foremost source
of non-metallic inclusions in tool steel during ladle treatment.
C1 Royal Inst Technol, Div Met, Dept Mat Sci & Engn, SE-10044 Stockholm, Sweden.
Uddeholm Tooling AB, SE-68385 Hagfors, Sweden.
C3 Royal Institute of Technology
RP Sichen, D (corresponding author), Royal Inst Technol, Div Met, Dept Mat Sci &
Engn, SE-10044 Stockholm, Sweden.
EM du@mse.kth.se
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NR 30
TC 38
Z9 41
U1 1
U2 24
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD JUN
PY 2004
VL 31
IS 3
BP 235
EP 240
DI 10.1179/030192304225011025
PG 6
GA 846RX
UT WOS:000223335000008
DA 2023-12-05
ER
PT J
AU Proctor, DM
Shay, EC
Fehling, KA
Finley, BL
AF Proctor, DM
Shay, EC
Fehling, KA
Finley, BL
TI Assessment of human health and ecological risks posed by the uses of
steel-industry slags in the environment
SO HUMAN AND ECOLOGICAL RISK ASSESSMENT
LA English
DT Article
DE steel slag; environmental health risk assessment; metals;
bioavailability; stochastic analysis
ID MANGANESE ABSORPTION; EXPOSURE
AB Steel-industry slag, a co-product of iron and steel production, is produced and
sold for use in a wide range of applications. A comprehensive study of the
potential human health risks associated with the environmental applications (e.g.,
fill, roadbase, landscaping) of iron- and steel-making slag was performed using
characterization data for 73 samples of slag collected from blast furnaces, basic
oxygen furnaces, and electric arc furnaces. Characterization data were compared to
regulatory health-based "screening" benchmarks to determine constituents of
interest. Antimony, beryllium, cadmium, trivalent and hexavalent chromium,
manganese, thallium, and vanadium were measured above screening levels and were
assessed in an application-specific exposure assessment using standard U.S.
Environmental Protection Agency risk assessment methods. A stochastic analysis was
conducted to evaluate the variability and uncertainty in the inhalation exposure
and risk estimates, and the oral bioaccessibility of certain metals in the slag was
quantified. The risk assessment found no significant hazards to human health as a
result of the environmental applications of steel-industry slag. However, site-
specific ecological risk assessment may be required for slag applications in and
around small water bodies with limited dilution volume, because high pH and
aluminum were found to leach at levels that may be harmful to aquatic life.
C1 Exponent, Irvine, CA 92618 USA.
AMEC, Pittsburgh, PA USA.
Exponent, Santa Rosa, CA USA.
C3 Exponent; Exponent
RP Proctor, DM (corresponding author), Exponent, 320 Goddard Way,Suite 200, Irvine,
CA 92618 USA.
EM dproctor@exponent.com
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NR 51
TC 38
Z9 46
U1 1
U2 42
PI PHILADELPHIA
SN 1080-7039
EI 1549-7860
J9 HUM ECOL RISK ASSESS
JI Hum. Ecol. Risk Assess.
PD JUN
PY 2002
VL 8
IS 4
BP 681
EP 711
DI 10.1080/20028091057150
PG 31
WC Biodiversity Conservation; Environmental Sciences
SC Biodiversity & Conservation; Environmental Sciences & Ecology
GA 571CR
UT WOS:000176697700004
DA 2023-12-05
ER
PT J
AU Andersson, MAT
Jonsson, LTI
Jonsson, PG
AF Andersson, MAT
Jonsson, LTI
Jonsson, PG
TI A thermodynamic and kinetic model of reoxidation and desulphurisation in
the ladle furnace
LA English
DT Article
DE ladle treatment; vacuum; reoxidation; desulphurisation; kinetics;
thermodynamics; fluid flow; CFD; model simulation
ID GAS-STIRRED LADLE; SLAGS
AB A thermodynamic and kinetic model of reoxidation and desulphurisation in the
ladle furnace has been developed by using a two-dimensional fluid-flow model
combined with equations expressing the thermodynamics of reoxidation and
desulphurisation. More specifically ladle vacuum treatment of a gas-stirred ladle
has been simulated. In order to describe the activities of the oxide components of
the slag, expressions by Ohta and Suito(1)) were adopted. The thermodynamic model
describes the slag/metal equilibria between Al, Si, O, Mn and S in the molten steel
and Al2O3, SiO2, FeO, MnO and S in the slag. A fluid dynamic model that considers
the slag, steel and argon phases derives the kinetics. Results from an isothermal
calculation have been heuristically compared with industrial plant data and they
show good agreement. The model results have also revealed that the reduction of
silica plays a part in aluminium loss during ladle treatment.
C1 KTH, Div Met, SE-10044 Stockholm, Sweden.
RP Andersson, MAT (corresponding author), KTH, Div Met, SE-10044 Stockholm, Sweden.
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NR 20
TC 38
Z9 42
U1 1
U2 16
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2000
VL 40
IS 11
BP 1080
EP 1088
PG 9
GA 374PB
UT WOS:000165352600005
OA gold
DA 2023-12-05
ER
PT J
AU Wang, YR
Cao, YB
Zhang, ZH
Huang, JZ
Zhang, P
Ma, YW
Wang, H
AF Wang, Yanru
Cao, Yubin
Zhang, Zuhua
Huang, Jizhong
Zhang, Peng
Ma, Yuwei
Wang, Hao
TI Study of acidic degradation of alkali-activated materials using
synthetic C-(N)-A-S-H and N-A-S-H gels
LA English
DT Article
DE Alkali-activated materials; Acid resistance; Aluminosilicates; N-A-S-H;
C-(N)-A-S-H; Durability
ID FLY-ASH; GEOPOLYMERS; CONCRETE; SLAG; RESISTANCE; STRENGTH; MORTARS;
CEMENT
AB Alkali-activated materials (AAMs) are usually recognized having better acid
resistance compared to ordinary Portland cement (OPC), however, the detailed
mechanism has not been well studied due to the complexity of raw materials and
hardened matrix. In this study, two typical binding gels in AAMs, sodium aluminum
silicate hydrate (N-A-S-H) and calcium (sodium) aluminum silicate hydrate (C-(N)-A-
S-H), were chemically prepared by laboratory synthesized aluminosilicate powders.
The microstructure and composition evolution of the two gels exposed to sulfuric
acid were investigated. The results showed that the C-(N)-A-S-H gel had higher
degree of structural order than the N-A-S-H gel, while the N-A-S-H gel showed
higher polymerization. The AlIV in N-A-S-H gel transferred completely to AlV during
sulfuric acid attack, while trace amount of AlIV was still detected in the exposed
C-(N)-A-S-H gels. Both gels had increased silica polymerization degree after
exposure to sulfuric acid solution. Due to rapider dealumination of N-A-S-H gel
than C-(N)-A-S-H gel, the Si/Al ratio increased much higher in the former. The
molecular framework changes of N-A-S-H gel caused by dealumination was found to
have less effect on the integrity though than that of C-(N)-A-S-H gel, in which
coarse gypsum crystalline grains formed and led to destructive stress in hardened
matrix. This paper provides an insight at microstructure level of the two typical
gels, which is essential for the manufacturing and application of alkali-activated
materials.
C1 [Wang, Yanru; Cao, Yubin; Wang, Hao] Univ Southern Queensland, Ctr Future Mat,
Toowoomba, Qld 4350, Australia.
Applicat Tec, Changsha 410082, Peoples R China.
[Zhang, Zuhua] Hunan Univ, Key Lab Bldg Safety & Energy Efficiency Minist Ed,
Changsha 410082, Peoples R China.
[Huang, Jizhong] Shanghai Univ, Inst Conservat Cultural Heritage, Shanghai
[Zhang, Peng] Qingdao Univ Technol, Sch Civil Engn, Qingdao 266033, Peoples R
China.
[Ma, Yuwei] Guangzhou Univ, Res Ctr Wind Engn & Engn Vibrat, Guangzhou 510006,
Peoples R China.
C3 University of Southern Queensland; Hunan University; Hunan University;
Shanghai University; Qingdao University of Technology; Guangzhou
University
RP Wang, H (corresponding author), Univ Southern Queensland, Ctr Future Mat,
Toowoomba, Qld 4350, Australia.; Zhang, ZH (corresponding author), Hunan Univ, Coll
Civil Engn, Key Lab Green & Adv Civil Engn Mat & Applicat Tec, Changsha 410082,
Peoples R China.; Ma, YW (corresponding author), Guangzhou Univ, Res Ctr Wind Engn
& Engn Vibrat, Guangzhou 510006, Peoples R China.
EM zuhuazhang@hnu.edu.cn; yuwei_ma@gzhu.edu.cn; hao.wang@usq.edu.au
RI Wang, Hao/A-7340-2016; Zhang, Zuhua/AAK-5391-2020; wang,
hao/HSE-7975-2023; wang, yixuan/JGM-3893-2023; Wang, yanru/JAX-5241-2023
OI Wang, Hao/0000-0001-8869-9669; Zhang, Zuhua/0000-0002-7153-5120;
FU National Natural Science Foundation of China (NSFC) [U2001225, 51878263,
51638008]; NSFC [51778003]
FX This work is partially supported by the National Natural Science
Foundation of China (NSFC) grants (U2001225, 51878263, 51638008). The
support from NSFC grant (51778003) is acknowledged as well.
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NR 57
TC 37
Z9 38
U1 8
U2 58
PU ELSEVIER SCI LTD
PI OXFORD
SN 1359-8368
EI 1879-1069
PD FEB 1
PY 2022
VL 230
AR 109510
DI 10.1016/j.compositesb.2021.109510
EA DEC 2021
PG 14
GA XW0IV
UT WOS:000735314800004
DA 2023-12-05
ER
PT J
AU Santamaría, L
López-Aizpún, M
García-Padial, M
Vicente, MA
Korili, SA
Gil, A
AF Santamaria, L.
Lopez-Aizpun, M.
Garcia-Padial, M.
Vicente, M. A.
Korili, S. A.
Gil, A.
TI Zn-Ti-Al layered double hydroxides synthesized from aluminum saline slag
wastes as efficient drug adsorbents
LA English
CT Euroclay Conference (EUROCLAY)
CY JUL 01-05, 2019
CL Pierre & Marie Curie Univ, Paris, FRANCE
HO Pierre & Marie Curie Univ
DE Aluminum industrial wastes; Adsorption removal of diclofenac;
Hydrotalcite from saline slags; Layered double hydroxides; Adsorption
removal of salicylic acid
ID SALICYLIC-ACID; THERMOGRAVIMETRIC ANALYSIS; CONTROLLED-RELEASE;
AQUEOUS-SOLUTION; ION-EXCHANGE; HYDROTALCITE; PHARMACEUTICALS;
ADSORPTION; DICLOFENAC; REMOVAL
AB This work reports the synthesis of Zinc-Titanium-Aluminum (ZnTiAl) layered
double hydroxides (LDH) with various proportions of Al-Ti and a Zn/(Al-Ti) molar
ratio of 3:1 by the co-precipitation method. Two series, made with commercial
aluminum (Al) and aluminum extracted from saline slags (Al*), have been considered.
Structural characterization and comparison of the two series has been made using
powder X-ray diffraction (PXRD), Nitrogen physisorption at 77 K, Scanning electron
microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and Thermogravimetry
measurements. The adsorption capacity of diclofenac and salicylic acid, as examples
of emergent pollutants, by the different LDH on batch and fixed-bed column
experiments has been analyzed. The effect of various parameters, such as the pH,
the initial concentration of pollutant, the mass of adsorbent and the contact time,
on the sorption behavior were studied and compared. The contact time to attain
equilibrium for maximum adsorption was found to be between 100 and 400 min. The
kinetic and equilibrium results were correlated to several adsorption and isotherm
equation models. The synthesized materials were more effective in removing
diclofenac than salicylic acid, being Zn6Al*(2) the hydrotalcite that showed the
highest adsorption capacity. The results showed a new application of a material
obtained from the valorization of an industrial waste such as aluminum saline
slags.
C1 [Santamaria, L.; Lopez-Aizpun, M.; Garcia-Padial, M.; Korili, S. A.; Gil, A.]
Univ Publ Navarra, Dept Ciencias Edificio Acebos, INAMAT, Campus Arrosadia, E-31006
Pamplona, Spain.
[Vicente, M. A.] Univ Salamanca, Dept Quim Inorgan, GIR QUESCAT, E-37008
Salamanca, Spain.
C3 Universidad Publica de Navarra; University of Salamanca
RP Gil, A (corresponding author), Univ Publ Navarra, Dept Ciencias Edificio Acebos,
INAMAT, Campus Arrosadia, E-31006 Pamplona, Spain.
RI Santamaría, Leticia/ABD-2455-2020; Santamaría, Leticia/K-2587-2018;
Vicente, Miguel Angel/L-5298-2014
OI Santamaría, Leticia/0000-0003-1248-341X; Santamaría,
Leticia/0000-0003-1248-341X; Vicente, Miguel Angel/0000-0002-6714-0249;
Gil, Antonio/0000-0001-9323-5981
European Regional Development Fund (ERDF) [MAT2016-78863-C2-R];
Government of Navarra [PI017-PI039 CORRAL]; Universidad Publica de
Navarra; Santander Bank
FX This work was funded by the Spanish Ministry of Economy, Industry and
Competitiveness (AEI/MINECO), and the European Regional Development Fund
(ERDF) through project MAT2016-78863-C2-R and the Government of Navarra
through projects PI017-PI039 CORRAL. LS thanks Universidad Publica de
Navarra for a pre-doctoral grant. AG also thanks Santander Bank for
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NR 71
TC 37
Z9 37
U1 2
U2 35
PU ELSEVIER
PI AMSTERDAM
PA RADARWEG 29a, 1043 NX AMSTERDAM, NETHERLANDS
SN 0169-1317
EI 1872-9053
J9 APPL CLAY SCI
JI Appl. Clay Sci.
PD MAR 15
PY 2020
VL 187
AR 105486
DI 10.1016/j.clay.2020.105486
PG 14
GA KW7SV
UT WOS:000521385500021
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Kumar, VRP
Gunasekaran, K
Shyamala, T
AF Kumar, V. R. Prasath
Gunasekaran, K.
Shyamala, T.
TI Characterization study on coconut shell concrete with partial
replacement of cement by GGBS
LA English
DT Article
DE Coconut shell; Ground granulated blast-furnace slag; Compressive
strength; Durability study; Micro-structural characterization
ID HIGH-STRENGTH CONCRETE; BLAST-FURNACE SLAG; PALM KERNEL SHELL; FLY-ASH;
MECHANICAL-PROPERTIES; HIGH-PERFORMANCE; HIGH-VOLUME; MICROSTRUCTURE;
DURABILITY; HYDRATION
AB Increasing demand and depletion of natural resources has brought a need for the
replacement of conventional concrete. This study is conducted by completely
replacing coarse aggregate with coconut shell (CS) an agricultural waste. Though it
achieves the target strength the decrease in quality of coconut shell concrete
(CSC) is enhanced by utilizing a pozzolanic material Ground Granulated Blast-
furnace Slag (GGBS) and its optimum percentage of replacement with cement is found
as 10% by conducing compressive strength for varying percentage of replacement say
0%, 5%, 10%, 15%, and 20%. For the optimum mix, the durability study and
microstructural investigation, say SEM, XRD, EDX, FTIR, and IMM was examined. The
result revealed that incorporating GGBS increases the strength of concrete to
around 15%. The microstructural study has clearly exhibits that the hydration
process has been improved to better formation of Calcium Silicate Hydrate (C-S-H)
and Calcium Aluminium Silicate Hydrate (C-A-S-H) when GGBS is incorporated.
C1 [Kumar, V. R. Prasath; Gunasekaran, K.; Shyamala, T.] SRM Inst Sci & Technol,
Dept Civil Engn, Fac Engn & Technol, Kattankulathur 603203, Tamil Nadu, India.
C3 SRM Institute of Science & Technology Chennai
RP Kumar, VRP (corresponding author), SRM Inst Sci & Technol, Dept Civil Engn, Fac
Engn & Technol, Kattankulathur 603203, Tamil Nadu, India.
EM prasathkumar.v@ktr.srmuniv.ac.in
RI PRASATH KUMAR, V R/ABE-7690-2021; Kandaswamy, Gunasekaran/P-4441-2016
OI PRASATH KUMAR, V R/0000-0001-7292-0963; Kandaswamy,
Gunasekaran/0000-0001-9810-346X
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[Anonymous], P 8 INT C ADV CIV ST
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10.1016/j.conbuildmat.2017.11.034
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10.1016/j.conbuildmat.2019.01.191
Ylmén R, 2013, INT J CONCR STRUCT M, V7, P119
NR 51
TC 37
Z9 38
U1 3
U2 17
PU ELSEVIER
PI AMSTERDAM
EI 2352-7102
J9 J BUILD ENG
JI J. Build. Eng.
PD NOV
PY 2019
VL 26
AR 100830
DI 10.1016/j.jobe.2019.100830
PG 9
GA JV4VK
UT WOS:000502363100014
DA 2023-12-05
ER
PT J
AU Xuan, DX
Tang, P
Poon, CS
AF Xuan, Dongxing
Tang, Pei
Poon, Chi Sun
TI Effect of casting methods and SCMs on properties of mortars prepared
with fine MSW incineration bottom ash
LA English
DT Article
DE Fine incineration bottom ash; Metallic aluminium; Glass; ASR expansion;
SCMs; Casting methods
ID WASTE; AGGREGATE; ENERGY; PERFORMANCE; RESIDUES; CONCRETE; GLASS
AB Fine municipal solid waste incineration bottom ash (MSWIBA) contains more
contaminants (e.g. metallic aluminium, glass and gypsum) that cannot be effectively
removed by current recycling techniques and this thus limits its engineering
application in concrete products. Instead of removing these contaminants, the
objective of this research was to investigate the influences of using different
casting methods and various supplementary cementitious materials (SCMs) on
improving the properties of cement mortar prepared with the fine MSWIBA. In this
study, the mortar bar specimens incorporating 100% fine MSWIBA as sand were
prepared using the conventional wet-mixed method and a dry-mixed method. The SCMs
applied were fly ash (FA), ground-granulated blast-furnace slag (GGBS) and waste
glass powder (GP), with a replacement ratio of 30 wt% of ordinary cement in the
mortar. The curing conditions of the specimens were in the 20 degrees C water, in
the 80 degrees C water and in an 80 degrees C NaOH solution for 28 days,
respectively. The experimental results showed that the dry-mixed method was an
effective method to mitigate the expansion of the mortar prepared with MSWIBA as
well as to enhance its mechanical properties after being subjected to the NaOH
solution. The order of effectiveness of SCMs on the reduction in the expansion of
the mortar prepared with MSWIBA was FA, GGBS and GP. It was indicated that FA was
the most effective in mitigating the alkali-silica expansion as well as the
alkaline-Al reaction. (C) 2018 Elsevier Ltd. All rights reserved.
C1 [Xuan, Dongxing; Tang, Pei; Poon, Chi Sun] Hong Kong Polytech Univ, Dept Civil &
Environm Engn, Kowloon, Hong Kong, Peoples R China.
RP Poon, CS (corresponding author), Hong Kong Polytech Univ, Dept Civil & Environm
Engn, Kowloon, Hong Kong, Peoples R China.
EM cecspoon@polyu.edu.hk
RI XUAN, Dongxing/R-2340-2017; Poon, Chi Sun/JQI-2195-2023; Tang,
Pei/AAR-4082-2020; Poon, Chi Sun/H-4152-2015
OI XUAN, Dongxing/0000-0002-9505-9720; Poon, Chi Sun/0000-0003-4912-3936;
Tang, Pei/0000-0003-4881-6757
FU Hong Kong Polytechnic University Postdoctoral Fellowship Scheme
FX This work was funded by the Hong Kong Polytechnic University
Postdoctoral Fellowship Scheme. We would like to thank Dr. Jiangshan Li
(the Hong Kong Polytechnic University) for his assistance in sourcing
the MSWIBA used in this study.
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NR 25
TC 37
Z9 37
U1 2
U2 23
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD APR 10
PY 2018
VL 167
BP 890
EP 898
DI 10.1016/j.conbuildmat.2018.02.077
PG 9
GA GE0IJ
UT WOS:000430897200081
DA 2023-12-05
ER
PT J
AU Chen, YL
Chang, JE
Lai, YC
Chou, MIM
AF Chen, Ying-Liang
Chang, Juu-En
Lai, Yi-Chieh
Chou, Mei-In Melissa
TI A comprehensive study on the production of autoclaved aerated concrete:
Effects of silica-lime-cement composition and autoclaving conditions
LA English
DT Article
DE Autoclaved aerated concrete; Composition design; Autoclaving conditions;
Bulk density; Compressive strength
ID QUARTZ PARTICLE-SIZE; BLAST-FURNACE SLAG; LIGHTWEIGHT CONCRETE;
HYDROTHERMAL SOLIDIFICATION; MECHANICAL-PROPERTIES; STRENGTH; AGGREGATE;
TAILINGS; ASH; AIR
AB This study describes the effects of raw mix composition, amount of foaming
agent, water-solids ratio, steam pressure, and curing time on the characteristics
of autoclaved aerated concrete (AAC). The bulk density, compressive strength, and
microstructures of AAC specimens were examined, and X-ray diffraction, mercury
intrusion porosimetry, and thermal analyses were employed. The bulk density of AAC
was affected by the amount of aluminum powder added and water-solids ratio, and
especially the latter. An increase in the amount of cement was not beneficial to
the development of compressive strength. In contrast, autoclave curing greatly
enhanced the compressive strength, and the AAC specimen autoclaved at 12 atm for 16
h had the highest compressive strength of 13.3 MPa. Increasing steam pressure can
notably reduce the curing time, based on similar requirements of compressive
strength. In contrast, prolonging curing time was helpful to the development of
compressive strength under low steam pressure conditions. (C) 2017 Elsevier Ltd.
C1 [Chen, Ying-Liang; Chang, Juu-En] Natl Cheng Kung Univ, Dept Environm Engn,
Sustainable Environm Res Labs, 1 Univ Rd, Tainan 70101, Taiwan.
[Lai, Yi-Chieh] Natl Sci & Technol Museum, Technol Educ Div, 720 Jiouru 1st Rd,
Kaohsiung 80765, Taiwan.
[Chou, Mei-In Melissa] Univ Illinois, Illinois State Geol Survey, Dept Nat
Resources & Environm Sci, 615 E Peabody Dr, Champaign, IL 61820 USA.
C3 National Cheng Kung University; University of Illinois System;
University of Illinois Urbana-Champaign
RP Chen, YL (corresponding author), Natl Cheng Kung Univ, Dept Environm Engn,
Sustainable Environm Res Labs, 1 Univ Rd, Tainan 70101, Taiwan.
EM roy.yl.chen@gmail.com
OI Chen, Ying-Liang/0000-0001-5295-9393
FU Ministry of Science and Technology, Taiwan [MOST 102-2221-E-006-005-MY3,
MOST 106-3113-E-007-002]
FX The authors gratefully acknowledge the Ministry of Science and
Technology, Taiwan, for its financial support of this study (Contract
No.: MOST 102-2221-E-006-005-MY3 and MOST 106-3113-E-007-002).
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NR 31
TC 37
Z9 38
U1 2
U2 71
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 30
PY 2017
VL 153
BP 622
EP 629
DI 10.1016/j.conbuildmat.2017.07.116
PG 8
GA FI3HD
UT WOS:000411847700061
DA 2023-12-05
ER
PT J
AU Chaunsali, P
Peethamparan, S
AF Chaunsali, Piyush
Peethamparan, Sulapha
TI Evolution of strength, microstructure and mineralogical composition of a
CKD-GGBFS binder
LA English
DT Article
DE Cement kiln dust (CKD); Ground granulated blast furnace slag (GGBFS);
Characterization; X-ray diffraction; Thermogravimetry; Scanning electron
microscopy
ID BLAST-FURNACE SLAG; CEMENT KILN DUSTS; EARLY HYDRATION; FLY-ASH; ALKALI;
TEMPERATURE; ACTIVATION; GEOPOLYMERS; MORTARS; PASTES
AB Characterization of a nontraditional binding material containing cement kiln
dust (CKD) and ground granulated blast furnace slag (GGBFS) is discussed in this
paper. Significant compressive strength was obtained for a CKD-GGBFS blend with 70%
CKD and 30% GGBFS at a water-to-binder ratio of 0.40 after 2 days of curing at
elevated temperature. Similar strength was also obtained for the samples subjected
to normal moisture curing over a period of 28 days. The compressive strength
increased with additional moist curing in both the cases. The microstructural and
the mineralogical examinations show that the strength development was mainly due to
the formation of calcium silicate hydrate (C-S-H). In addition to normal C-S-H,
aluminum and magnesium incorporated C-S-H phases were also present in the CKD-GGBFS
blends. The formation of ettringite appears to be a contributing factor in early
age strength development of CKD-GGBFS binder. Published by Elsevier Ltd.
C1 [Chaunsali, Piyush; Peethamparan, Sulapha] Clarkson Univ, Dept Civil & Environm
Engn, Potsdam, NY 13699 USA.
C3 Clarkson University
RP Peethamparan, S (corresponding author), Clarkson Univ, Dept Civil & Environm
EM speetham@clarkson.edu
RI Chaunsali, Piyush/O-9759-2019; Chaunsali, Piyush/V-4670-2017
OI Chaunsali, Piyush/0000-0003-2107-6488;
10.1016/j.cemconres.2004.06.015
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SHI CJ, 1989, CEMENT CONCRETE RES, V19, P527
NR 34
TC 37
Z9 40
U1 1
U2 20
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD FEB
PY 2011
VL 41
IS 2
BP 197
EP 208
DI 10.1016/j.cemconres.2010.11.010
PG 12
GA 715DQ
UT WOS:000286861100008
DA 2023-12-05
ER
PT J
AU Park, JH
Zhang, LF
AF Park, Joo Hyun
Zhang, Lifeng
TI Kinetic Modeling of Nonmetallic Inclusions Behavior in Molten Steel: A
Review
LA English
DT Review
ID CONTINUOUS-CASTING MOLD; IN-SITU OBSERVATION; FERRITIC STAINLESS-STEEL;
MGO-CENTER-DOT-AL2O3 SPINEL INCLUSIONS; PROCESS SIMULATION-MODEL;
NON-METALLIC INCLUSIONS; COUPLED TURBULENT-FLOW; ALUMINUM-KILLED STEEL;
OF-THE-ART; FLUID-FLOW
AB The kinetic modeling for the nucleation, size growth, and compositional
evolution of nonmetallic inclusions in steel was extensively reviewed in the
present article. The nucleation and initial growth of inclusion in molten steel
during deoxidation as well as the collision growth, motion, removal, and entrapment
of inclusions in the molten steel in continuous casting (CC) tundish and strand
were discussed. Moreover, the recent studies on the prediction of inclusion
composition in CC semiproducts were introduced. Since the 1990s, the development of
thermodynamic model and relevant databases for inclusion engineering has been
initiated by the steel industry. Later, the commercial software FACTSAGE employing
the FACT database was widely used to predict the gas (atmosphere/bubble)-liquid
(steel/slag/inclusion)-solid (refractory/slag/steel/inclusion) multiphase
equilibria. With the help of the comprehensive thermodynamic database and solution
models in conjunction with the development of user-friendly computing packages, the
kinetics of inclusion evolution in molten steel can be successfully predicted based
on several kinetic models such as the coupled reaction (CR) model, reaction zone
model, and tank series recirculation (TSR) model. However, some parameters are
needed to represent the real processes according to the model employed at different
operational or experimental conditions. The effect of reoxidation on the evolution
of inclusions in the ladle and tundish, which was experimentally confirmed, can be
simulated by the effective equilibrium reaction zone (EERZ) model. The complex
slag-steel interfacial reaction phenomena have been successfully explained by the
interfacial kinetic model based on the dynamic interfacial tension and oxygen
adsorption/desorption characteristics at the slag-steel interface.
C1 [Park, Joo Hyun] Hanyang Univ, Dept Mat Sci & Chem Engn, Ansan 15588, South
Korea.
[Park, Joo Hyun] KTH Royal Inst Technol, Dept Mat Sci & Engn, S-10044 Stockholm,
Sweden.
[Zhang, Lifeng] Yanshan Univ, State Key Lab Metastable Mat Sci & Technol, 438
West Hebei Ave, Qinhuangdao 066004, Hebei, Peoples R China.
C3 Hanyang University; Royal Institute of Technology; Yanshan University
RP Park, JH (corresponding author), Hanyang Univ, Dept Mat Sci & Chem Engn, Ansan
15588, South Korea.; Zhang, LF (corresponding author), Yanshan Univ, State Key Lab
Metastable Mat Sci & Technol, 438 West Hebei Ave, Qinhuangdao 066004, Hebei,
Peoples R China.
EM basicity@hanyang.ac.kr; zhanglifeng@ysu.edu.cn
FU Korea Evaluation Institute of Industrial Technology (KEIT) [20009956];
Ministry of Trade, Industry & Energy (MOTIE), Korea; Korea Evaluation
Institute of Industrial Technology (KEIT) [20009956] Funding Source:
FX This work was partly supported by the Korea Evaluation Institute of
Industrial Technology (KEIT, with Grant No. 20009956), funded by the
Ministry of Trade, Industry & Energy (MOTIE), Korea.
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NR 360
TC 36
Z9 36
U1 9
U2 83
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD DEC
PY 2020
VL 51
IS 6
BP 2453
EP 2482
DI 10.1007/s11663-020-01954-1
EA OCT 2020
PG 30
Engineering
GA PY4VD
UT WOS:000577232100002
OA Bronze
DA 2023-12-05
ER
PT J
AU Isteri, V
Ohenoja, K
Hanein, T
Kinoshita, H
Tanskanen, P
Illikainen, M
Fabritius, T
AF Isteri, Visa
Ohenoja, Katja
Hanein, Theodore
Kinoshita, Hajime
Tanskanen, Pekka
Illikainen, Mirja
Fabritius, Timo
TI Production and properties of ferrite-rich CSAB cement from metallurgical
industry residues
LA English
DT Article
DE CSA cement; Fayalite slag; Fluorellestadite; Jarosite; Steel making
slag; Utilization
ID SULFOALUMINATE-BELITE CEMENT; CRYSTAL-STRUCTURE REFINEMENTS; POWDER
DIFFRACTION DATA; DICALCIUM SILICATE; PORTLAND CLINKERS;
PHASE-TRANSITION; HYDRATION; IRON; BROWNMILLERITE; ALUMINUM
AB Blast furnace slag from the steel industry is commercially utilized as a cement
replacement material without major processing requirements; however, there arc many
unutilizcd steel production slags which differ considerably from the blast furnace
slag in chemical and physical properties In this study, calcium sulfoaluminate Mite
(CSAB) cement clinkers were produced using generally unutilizcd metallurgical
industry residues: AOD (Argon Oxygen Decarburisation) slag from stainless steel
production, Fe slag from zinc production, and fayalitic slag from nickel
production. CSAB clinker with a target composition of ye'elimite-belite-ferrite was
produced by firing raw materials at 1300 degrees C. The phase composition of the
produced clinkers was identified using quantitative XRD analyses, and the chemical
composition of the clinker phases produced was established using FESEM-EDS and
mechanical properties were tested through compressive strength test. It is
demonstrated that these metallurgical residues can be used successfully as
alternative raw materials for the production of CSAB cement that can be used for
special applications. In addition, it is shown that the available quantities of
these side-streams are enough for significant replacement of virgin raw materials
used in cement production. (C) 2020 The Authors. Published by Elsevier B.V.
C1 [Isteri, Visa; Tanskanen, Pekka; Fabritius, Timo] Univ Oulu, Fac Technol, Proc
Met, POB 4300, Oulu 90014, Finland.
[Ohenoja, Katja; Illikainen, Mirja] Univ Oulu, Fibre & Particle Engn, Fac
Technol, POB 4300, Oulu 90014, Finland.
[Hanein, Theodore; Kinoshita, Hajime] Univ Sheffield, Dept Mat Sci & Engn,
C3 University of Oulu; University of Oulu; University of Sheffield
RP Fabritius, T (corresponding author), Univ Oulu, Fac Technol, Proc Met, POB 4300,
Oulu 90014, Finland.
EM timo.fabritius@oulu.fi
OI Kinoshita, Hajime/0000-0001-8805-1774; Fabritius,
Timo/0000-0002-0513-2315; Hanein, Theodore/0000-0002-3009-703X; Isteri,
Visa/0000-0002-9215-1468; Tanskanen, Pekka/0000-0001-6965-9338;
FU Business Finland [1415/31/2015]; Boliden Harjavalta; Boliden Kokkola;
Yara Suomi; Fortum Waste Solutions; Outokumpu Stainless; Renlund
Foundation
FX The CECIRE (1415/31/2015)-project was supported by Business Finland and
the following companies: Boliden Harjavalta, Boliden Kokkola, Yara
Suomi, Fortum Waste Solutions and Outokumpu Stainless. XRD and FESEM
analysis were performed at the Center of Microscopy and Nanotechnology
(University of Oulu). The support of Renlund Foundation is also
appreciated.
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NR 71
TC 36
Z9 41
U1 5
U2 39
PU ELSEVIER
PI AMSTERDAM
SN 0048-9697
EI 1879-1026
PD APR 10
PY 2020
VL 712
AR 136208
DI 10.1016/j.scitotenv.2019.136208
PG 12
GA KJ9JB
UT WOS:000512369600114
PM 31931225
OA hybrid, Green Published, Green Accepted
DA 2023-12-05
ER
PT J
AU Ding, W
Xiao, JH
Peng, Y
Shen, SY
Chen, T
AF Ding Wei
Xiao Jun-Hui
Peng Yang
Shen Si-Yue
Chen Tao
TI Iron Extraction from Red Mud using Roasting with Sodium Salt
LA English
DT Article
DE Red mud; segregation roasting; sodium sulfate; magnetic separation
ID MAGNETIC SEPARATION; REDUCTION; RECOVERY; SULFATE; ORE; BENEFICIATION;
COMPONENTS; RESIDUE
AB Red mud is the main solid waste generated by the aluminum industry for the
extraction of alumina. Considering the environmental problems associated with red
mud, the recovery of iron from bauxite slag is still a promising field. The effect
of sodium sulfate on the red mud separation roasting-magnetic separation process
was studied. The results show that at the roasting temperature of 1100 degrees C
for 65 min, the segregation roasting-magnetic separation is carried out with 8 wt.%
sodium sulfate. The total iron grade of the magnetic separation iron concentrate is
79.32 wt.% and iron recovery rate of 85.43%. X-ray diffraction analysis (XRD),
optical microscopy analysis and scanning electron microscopy-X-ray energy
spectroscopy (SEM-EDS) were used to study the addition of sodium sulfate
segregation roasting products to red mud. The results show that adding the proper
amount of sodium sulfate during the red mud segregation roasting process can
enhance the separation and recovery of iron. During the red mud segregation
roasting process, sodium sulfate reacts with alumina, silica, etc. to form sodium
silicate and sodium aluminosilicate, which inhibits the formation of fayalite and
promotes the chlorination of iron oxide. Element migration and chemical reaction
can destroy the original ore structure, promote the formation of molten phase and
accelerate the aggregation and growth of metallic iron particles. Thus, a metallic
iron concentrate with high quality is obtained.
C1 [Ding Wei; Xiao Jun-Hui; Peng Yang; Shen Si-Yue; Chen Tao] Southwest Univ Sci &
Technol, Sichuan Engn Lab Nonmetall Mineral Powder Modific, Mianyang, Sichuan,
Peoples R China.
[Ding Wei; Xiao Jun-Hui; Peng Yang; Shen Si-Yue; Chen Tao] Southwest Univ Sci &
Technol, Dept Mineral Proc, Sch Environm & Resource, Mianyang, Sichuan, Peoples R
China.
[Xiao Jun-Hui] Minist Land & Resources, Key Lab Radioact & Rare Scattered
Minerals, Shaoguan, Peoples R China.
[Xiao Jun-Hui] Southwest Univ Sci & Technol, Minist Educ, Key Lab Solid Waste
Treatment & Recycling, Mianyang, Sichuan, Peoples R China.
C3 Southwest University of Science & Technology - China; Southwest
University of Science & Technology - China; Ministry of Natural
Resources of the People's Republic of China; Southwest University of
Science & Technology - China
RP Xiao, JH (corresponding author), Southwest Univ Sci & Technol, Sch Environm &
Resource, Mianyang 621010, Sichuan, Peoples R China.
EM xiaojunhui33@163.com
RI Ding, Wei/HII-9240-2022; Xiao, Junhui/GQA-9838-2022; xiao,
junhui/HPF-1922-2023; xiao, junhui/AAQ-1773-2021
OI Ding, Wei/0000-0003-1880-2936; Xiao, Junhui/0000-0002-1256-2196; xiao,
junhui/0000-0002-1256-2196
FU Sichuan Science and Technology Program; Open Foundation of the Key
Laboratory of Radioactive and Rare and Sparse Minerals of the Ministry
of Land and Resources; Key Laboratory of Sichuan Province for
Comprehensive Utilization of Vanadium and Titanium Resources Foundation
[2018FTSZ35]; China Geological Big Survey; Open Foundation of the State
Key Laboratory of Refractories and Metallurgy, Wuhan University of
Science and Technology
FX This work was supported by the Sichuan Science and Technology Program;
Open Foundation of the Key Laboratory of Radioactive and Rare and Sparse
Minerals of the Ministry of Land and Resources; Key Laboratory of
Sichuan Province for Comprehensive Utilization of Vanadium and Titanium
Resources Foundation [2018FTSZ35]; China Geological Big Survey; Open
Foundation of the State Key Laboratory of Refractories and Metallurgy,
Wuhan University of Science and Technology.
CR Akcil A, 2018, MIN PROC EXT MET REV, V39, P145, DOI
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NR 24
TC 36
Z9 37
U1 17
U2 97
PI PHILADELPHIA
SN 0882-7508
EI 1547-7401
PD APR 3
PY 2021
VL 42
IS 3
BP 153
EP 161
DI 10.1080/08827508.2019.1706049
EA DEC 2019
PG 9
GA QT0NW
UT WOS:000504373500001
DA 2023-12-05
ER
PT J
AU Titah, HS
Purwanti, IF
Tangahu, BV
Kurniawan, SB
Imron, MF
Abdullah, SRS
Ismail, NI
AF Titah, Harmin Sulistiyaning
Purwanti, Ipung Fitri
Tangahu, Bieby Voijant
Kurniawan, Setyo Budi
Imron, Muhammad Fauzul
Abdullah, Siti Rozaimah Sheikh
Ismail, Nur 'Izzati
TI Kinetics of aluminium removal by locally isolated Brochothrix
thermosphacta and Vibrio alginolyticus
LA English
DT Article
DE Bacteria; Aluminium recycling; B. thermosphacta; Pseudo first order;
Pseudo second order; V. alginolyticus
ID GROWTH-KINETICS; BACTERIA; DIESEL; BIOSORPTION; IONS; SLAG
AB The emergence of the aluminium recycling industry has led to an increase in
aluminium-containing wastewater discharge to the environment. Biological treatment
of metal is one of the solutions that can be provided as green technology.
Screening tests showed that Brochothrix thermosphacta and Vibrio alginolyticus have
the potential to remove aluminium from wastewater. Brochothrix thermosphacta
removed up to 49.60%, while Vibrio alginolyticus was capable of removing up to
59.72% of 100 mg/L aluminium in acidic conditions. The removal of aluminium by V.
alginolyticus was well fitted with pseudo-first-order kinetics (k(1) =
0.01796/min), while B. thermosphacta showed pseudo-second-order kinetics (k(2) =
0.125612 mg substrate/g adsorbent. hr) in the process of aluminium removal. V.
alginolyticus had a higher rate constant under acidic conditions, while B.
thermosphacta had a higher rate constant under neutral pH conditions.
C1 [Titah, Harmin Sulistiyaning; Purwanti, Ipung Fitri; Tangahu, Bieby Voijant]
Inst Teknol Sepuluh Nopember, Fac Civil Environm & Geo Engn, Dept Environm Engn,
Kampus ITS Sukolilo, Surabaya 60111, Indonesia.
[Kurniawan, Setyo Budi] Politekn Perkapalan Negeri Surabaya, Study Program Waste
Treatment Engn, Jalan Teknik Kimia,Kampus ITS Sukolilo, Surabaya 60111, Indonesia.
[Imron, Muhammad Fauzul] Univ Airlangga, Fac Sci & Technol, Dept Biol, Study
Program Environm Engn, Kampus C UNAIR,Jalan Mulyorejo, Surabaya 6011$, Indonesia.
[Abdullah, Siti Rozaimah Sheikh; Ismail, Nur 'Izzati] Univ Kebangsaan Malaysia,
Fac Engn & Built Environm, Dept Chem & Proc Engn, Ukm Bangi 43600, Selangor,
Malaysia.
C3 Institut Teknologi Sepuluh Nopember; Airlangga University; Universiti
Kebangsaan Malaysia
RP Kurniawan, SB (corresponding author), Politekn Perkapalan Negeri Surabaya, Study
Program Waste Treatment Engn, Jalan Teknik Kimia,Kampus ITS Sukolilo, Surabaya
60111, Indonesia.
EM harminsulis@gmail.com; purwanti@enviro.its.ac.id; voijant@its.ac.id;
setyobudi.kurniawan@gmail.com; fauzul.01@gmail.com; rozaimah@ukm.edu.my;
nurezatyismail@ukm.edu.my
RI Ismail, Nur 'Izzati/AAB-8517-2021; Titah, Harmin
Sulistiyaning/AAD-1805-2021; Imron, Muhammad Fauzul/ISV-1451-2023;
Kurniawan, Setyo Budi/Q-6349-2019; Ismail, Nur 'Izzati/A-2259-2019;
Tangahu, Bieby Voijant/AAD-1735-2021; Imron, Muhammad
Fauzul/Q-7775-2019; Abdullah, Siti Rozaimah Sheikh/M-1970-2016;
Purwanti, Ipung Fitri/CAG-9370-2022
OI Ismail, Nur 'Izzati/0000-0001-6582-5909; Titah, Harmin
Sulistiyaning/0000-0003-4791-8735; Kurniawan, Setyo
Budi/0000-0002-0791-1638; Ismail, Nur 'Izzati/0000-0001-6582-5909;
Tangahu, Bieby Voijant/0000-0003-3306-5735; Imron, Muhammad
Fauzul/0000-0003-2649-2421; Abdullah, Siti Rozaimah
Sheikh/0000-0002-5282-8702; Purwanti, Ipung Fitri/0000-0002-9970-3755
FU Ministry of Research, Technology and Higher Education Indonesia through
the scheme of Penelitian Unggulan Perguruan Tinggi 2017; Indonesia
Endowment Fund for Education; Ministry of Research, Technology and
Higher Education Indonesia [123.14/D2.3/KP/2018]; Universiti Kebangsaan
Malaysia [DIP-2017-022]
FX This work was supported by the Ministry of Research, Technology and
Higher Education Indonesia through the scheme of Penelitian Unggulan
Perguruan Tinggi 2017 and the Indonesia Endowment Fund for Education
through the research grant for the LPDP awardee 2017 for the
corresponding author. Authors would also like to thank Ministry of
Research, Technology and Higher Education Indonesia through the scheme
of World Class Professor Scheme-B No. 123.14/D2.3/KP/2018, and research
grant from Universiti Kebangsaan Malaysia Grant (DIP-2017-022) for
sponsoring this publication.
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NR 40
TC 36
Z9 36
U1 0
U2 8
PI LONDON
SN 0301-4797
EI 1095-8630
J9 J ENVIRON MANAGE
PD MAY 15
PY 2019
VL 238
BP 194
EP 200
DI 10.1016/j.jenvman.2019.03.011
PG 7
GA HT1AM
UT WOS:000464296400022
PM 30851558
DA 2023-12-05
ER
PT J
AU Coudert, E
Paris, M
Deneele, D
Russo, G
Tarantino, A
AF Coudert, Elodie
Paris, Michael
Deneele, Dimitri
Russo, Giacomo
Tarantino, Alessandro
TI Use of alkali activated high-calcium fly ash binder for kaolin clay soil
stabilisation: Physicochemical evolution
LA English
DT Article
DE Soil stabilisation; Alkali activated material; Kaolin; High-calcium fly
ash
ID C-S-H; LATERITIC SOIL; GEOPOLYMER; NMR; AL-27; SLAG
AB This study addresses the use of alkali activated high-calcium fly ash-based
binder to improve engineering characteristics of soft clay-rich soils as an
alternative to common stabilisers. The physico-chemical reaction sequence has been
investigated by considering the binder alone and the binder mixed with kaolin. An
insight into the reactivity evidenced that calcium-containing phases derived from
high-calcium fly ash represent the reactive phases and, hence, pozzolanic activity
is the dominant process. New compounds are formed, thenardite Na2SO4 and an
amorphous silicate consisting of chains combined with calcium probably
incorporating three-dimensional four-fold aluminium environments. (C) 2018 Elsevier
C1 [Coudert, Elodie; Paris, Michael; Deneele, Dimitri] Univ Nantes, CNRS, Inst Mat
Jean Rouxel IMN, 2 Rue Houssiniere,BP 32229, F-44322 Nantes 3, France.
[Coudert, Elodie; Russo, Giacomo] Univ Cassino & Southern Lazio, Dept Civil &
Mech Engn, Via Gaetano di Biasio 43, I-03043 Cassino, FR, Italy.
[Coudert, Elodie; Tarantino, Alessandro] Univ Strathclyde, Dept Civil & Environm
Engn, 75 Montrose St, Glasgow G1 1XJ, Lanark, Scotland.
[Deneele, Dimitri] IFSTTAR, GERS, EE, F-44344 Bouguenais, France.
C3 Centre National de la Recherche Scientifique (CNRS); Nantes Universite;
University of Cassino; University of Strathclyde; Universite
Gustave-Eiffel
RP Deneele, D (corresponding author), IFSTTAR, GERS, EE, F-44344 Bouguenais,
France.
EM Dimitri.Deneele@ifsttar.fr
RI Deneele, Dimitri/AAD-5758-2021; Russo, Giacomo/AAE-6302-2019; Michael,
Paris/B-4644-2009
OI Russo, Giacomo/0000-0003-0073-8331; Michael, Paris/0000-0002-8671-0630;
DENEELE, Dimitri/0000-0003-3332-7424; Tarantino,
Alessandro/0000-0001-6690-748X
FU European Commission via the Marie Sklodowska-Curie Innovative Training
Networks (ITN-ETN) [H2020-MSCA-ITN-2015-675762]
FX The authors wish to acknowledge the support of the European Commission
via the Marie Sklodowska-Curie Innovative Training Networks (ITN-ETN)
project TERRE 'Training Engineers and Researchers to Rethink
geotechnical Engineering for a low carbon future'
(H2020-MSCA-ITN-2015-675762).
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10.1016/j.conbuildmat.2013.06.017
NR 42
TC 36
Z9 36
U1 3
U2 53
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD MAR 20
PY 2019
VL 201
BP 539
EP 552
DI 10.1016/j.conbuildmat.2018.12.188
PG 14
GA HM5PG
UT WOS:000459527000049
OA Green Published, hybrid, Green Accepted
DA 2023-12-05
ER
PT J
AU Zou, FB
Tan, HB
He, XY
Ma, BG
Deng, XF
Zhang, T
Mei, JP
Liu, XH
Qi, HH
AF Zou, Fubing
Tan, Hongbo
He, Xingyang
Ma, Baoguo
Deng, Xiufeng
Zhang, Ting
Mei, Junpeng
Liu, Xiaohai
Qi, Huahui
TI Effect of triisopropanolamine on compressive strength and hydration of
steaming-cured cement-fly ash paste
LA English
DT Article
DE Fly ash; Triisopropanolamine; Early strength; Steam-cured; Dissolution
ID SI-29 MAS-NMR; C-S-H; MECHANICAL-PROPERTIES; POLYCARBOXYLATE
SUPERPLASTICIZER; SODIUM GLUCONATE; PORTLAND-CEMENT; SHRINKAGE; SLAG;
RHEOLOGY; CONCRETE
AB Fly ash (FA) has been accepted as one of the most popular supplementary material
in blends with cement. However, high content of FA added would result in very slow
strength development at the early age, and this problem limits the use of FA in
precast concrete. In this study, an attempt was made to enhance the early strength
of steam-cured high content cement-fly ash paste (SCHF, 50% FA) by incorporating
triisopropanolamine (TIPA), and the underlying mechanism was systematically
investigated in terms of hydration products, pore structure, and ions dissolution
of FA. The early hydration process was assessed with isothermal calorimetry,
thermogravimetric with differential thermo-gravimetric, and scanning electron
microscopy with energy dispersive spectrometer. The pore structure of hardened
paste was characterized with mercury intrusion porosimetry. The solubility of FA
was analyzed with inductive coupled plasma emission spectrometer, nuclear magnetic
resonance, and scanning electron microscopy. The chelating ability of TIPA with
Fe3+ and Al3+ was evaluated with the conductivity. These results show that with the
dosage of TIPA less than 0.10%, the compressive strength will increase with
increasing dosage of TIPA, mainly because of the acceleration of both hydration of
cement and pozzolanic reaction of FA; while with the dosage more than 0.10%, the
compressive strength was sharply decreased owing to its air entraining effect to
increase the harmful pores, with negative effect on mechanical performance. The
reason for the accelerated pozzolanic reaction of FA is that TIPA can accelerate
the dissolution of aluminum, ferric and silicate into solution to participate in
hydration. The findings are expected to provide guidance on promoting the use of FA
in precast concrete. (C) 2018 Elsevier Ltd. All rights reserved.
C1 [Zou, Fubing; Tan, Hongbo; Ma, Baoguo; Deng, Xiufeng; Zhang, Ting; Mei, Junpeng;
Liu, Xiaohai; Qi, Huahui] Wuhan Univ Technol, State Key Lab Silicate Mat
Architectures, Wuhan 430070, Hubei, Peoples R China.
[He, Xingyang] Hubei Univ Technol, Sch Civil Engn Architecture & Environm, Wuhan
[He, Xingyang] Hubei Univ Technol, Bldg Waterproof Engn & Technol Res Ctr Hubei
Prov, Wuhan 430070, Hubei, Peoples R China.
RP Tan, HB (corresponding author), Wuhan Univ Technol, State Key Lab Silicate Mat
Architectures, Wuhan 430070, Hubei, Peoples R China.; He, XY (corresponding
author), Hubei Univ Technol, Sch Civil Engn Architecture & Environm, Wuhan 430070,
Hubei, Peoples R China.
EM thbwhut@whut.edu.cn; hexycn@163.com
RI Qi, Huahui/IUQ-2766-2023; Deng, Xiufeng/GWC-8986-2022; Tan,
Hongbo/Q-5972-2018
OI Liu, Xiaohai/0000-0002-8357-109X; Tan, Hongbo/0000-0003-1706-9939
FU National key R&D program of China [2016YFC0701003-5]; Major Technical
Innovation Project in Hubei Province of China [2018AAA002]
FX Financial supports from National key R&D program of China
(2016YFC0701003-5) and Major Technical Innovation Project in Hubei
Province of China (2018AAA002) are gratefully acknowledged.
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NR 40
TC 36
Z9 37
U1 6
U2 82
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD DEC 20
PY 2018
VL 192
BP 836
EP 845
DI 10.1016/j.conbuildmat.2018.10.087
PG 10
GA HE6DX
UT WOS:000453494600069
DA 2023-12-05
ER
PT J
AU Yang, W
Guo, CB
Zhang, LF
Ling, HT
Li, C
AF Yang, Wen
Guo, Changbo
Zhang, Lifeng
Ling, Haitao
Li, Chao
TI Evolution of Oxide Inclusions in Si-Mn Killed Steels During Hot-Rolling
Process
LA English
DT Article
ID MANGANESE SULFIDE INCLUSIONS; LIMITED ALUMINUM CONTENT; NON-METALLIC
INCLUSIONS; NONMETALLIC INCLUSIONS; FORMATION MECHANISM; DEFORMATION;
BEHAVIOR; MATRIX
AB The evolution of oxide inclusions in Si-Mn killed steels refined by slags of
different basicity during a four-pass industrial hot-rolling process was
investigated using an automated microscopy system. High-basicity refining slag
induced the formation of CaO- and Al2O3-containing inclusions, while refining slag
with 0.8 basicity induced dominant inclusions of SiO2 and MnO-SiO2. CaO-SiO2-Al2O3
inclusions mainly formed endogenously during solidification and cooling of Ca-
containing steels, where Ca originated from slag-steel reactions. However, the
larger-sized higher-CaO inclusions originated from slag entrainment. Different
inclusions presented different hot-rolling behaviors. The inclusion composition
changed by deformation and new phase formation. The dominant oxide types were
unchanged under refinement by low-basicity slag; however, they changed under
refinement with high-basicity slag. The deformation index of inclusions decreased
with increasing accumulated reduction (AR) of the steel. The difference in
deformation index between different inclusion types was the largest in the first
rolling stage and decreased in subsequent stages. SiO2-CaO and SiO2-MnO-CaO
inclusions had larger deformation indices during hot rolling but smaller indices in
the last two stages. High-basicity slag increased inclusion complexity; from the
perspective of cold-drawing performance, low-basicity refining slag is better for
the industrial production of tire-cord steels.
C1 [Yang, Wen; Guo, Changbo; Zhang, Lifeng] Univ Sci & Technol Beijing, Sch Met &
Ecol Engn, Beijing 100083, Peoples R China.
[Guo, Changbo] Qingdao Iron & Steel Grp Co Ltd, Qingdao 266000, Peoples R China.
[Ling, Haitao] Anhui Univ Technol, Sch Met Engn, Maanshan 243002, Anhui, Peoples
R China.
[Li, Chao] HBIS Grp Co Ltd, R&D Inst, Shijiazhuang 050023, Hebei, Peoples R
China.
C3 University of Science & Technology Beijing; Anhui University of
Technology
FU National Science Foundation of China [51274034, 51334002, 51404019,
51604023, 5150 4020]; Beijing Key Laboratory of Green Recycling and
Extraction of Metals (GREM); Laboratory of Green Process Metallurgy and
Modeling (GPM2); High Quality Steel Consortium (HQSC) at the School of
Metallurgical and Ecological Engineering, University of Science and
Technology Beijing (USTB), China
FX The authors are grateful for the support from the National Science
Foundation of China (Grant Nos. 51274034, 51334002, 51404019, 51604023,
and 5150 4020), the Beijing Key Laboratory of Green Recycling and
Extraction of Metals (GREM), the Laboratory of Green Process Metallurgy
and Modeling (GPM2), and the High Quality Steel Consortium (HQSC) at the
School of Metallurgical and Ecological Engineering, University of
Science and Technology Beijing (USTB), China.
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NR 45
TC 36
Z9 45
U1 2
U2 49
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD OCT
PY 2017
VL 48
IS 5
BP 2717
EP 2730
DI 10.1007/s11663-017-1025-6
PG 14
Engineering
GA FF4ST
UT WOS:000408947600047
DA 2023-12-05
ER
PT J
AU Jo, H
Lee, MG
Park, J
Jung, KD
AF Jo, Hoyong
Lee, Min-Gu
Park, Jinwon
Jung, Kwang-Deog
TI Preparation of high-purity nano-CaCO3 from steel slag
SO ENERGY
LA English
DT Article
DE Steel slag; Alkali metal ion dissolution; Mineral carbonation;
Nano-CaCO3
ID LAYERED DOUBLE HYDROXIDES; CO2 MINERAL CARBONATION;
ELECTROCHEMICAL-CELL; SEQUESTRATION; DISSOLUTION; FIXATION; DIOXIDE;
ALKALI; ACID; SERPENTINITE
AB Indirect carbonation is a suitable method for carbon dioxide (CO2) removal from
the environment, and it requires an acid to dissolve the calcium ions and a base to
precipitate the formed calcium carbonate (CaCO3). We herein report a new method to
produce high-purity nano-CaCO3 (nCaCO(3)) from steel slag using hydrochloric acid
(HCl) and sodium hydroxide (NaOH). The rate equation for the dissolution of calcium
(Ca) in the slag was derived using a range of variables, such as temperatures,
solid -to -liquid (S/L) ratio, and HCI concentration. The purified calcium
hydroxide (Ca(OH)(2)) was converted into nCaCO(3) (size: 80-120 nm, purity: 98.5%)
by carbonation with CO2, after impurities, such as iron (Fe), aluminum (Al), and
Mg, were completely removed. An efficiency of 73% was obtained for the dissolution
and precipitation steps when 0.50 M HCI and 1.0 M NaOH were employed to produce 1
ton/h of nano-CaCO3 with a purity of 98.5 wt%. Recently, a sodium chloride (NaCI)
electrolysis system with low energy requirement was proposed to simultaneously
produce HCl and NaOH. Assuming 90% faradic efficiency in the aforementioned NaCI
electrolysis, process energies of 916 kWh/tCaCO(3) and 1462 kWh/tCaCO(3) were
obtained at potentials of 0.83 V and 1.50 V, respectively. (C) 2016 Elsevier Ltd.
C1 [Jo, Hoyong; Jung, Kwang-Deog] Korea Inst Sci & Technol, Clean Energy Res Ctr,
[Jo, Hoyong; Lee, Min-Gu; Park, Jinwon] Yonsei Univ, Dept Chem & Biomol Engn, 50
Yonsei Ro, Seoul 120749, South Korea.
C3 Korea Institute of Science & Technology (KIST); Yonsei University
RP Jung, KD (corresponding author), Korea Inst Sci & Technol, Clean Energy Res Ctr,
EM jkdcat@kist.re.kr
RI Jung, Kwang-deog/AAA-5799-2019
OI Jung, Kwang-Deog/0000-0002-5747-9417
FU Korea Institute of Science and Technology (KIST); Korea CCS R&D Center
by the Ministry of Science, ICT and Future Planning [2014M1A8A1049293]
FX This work was financially supported through the Korea Institute of
Science and Technology (KIST) and the Korea CCS R&D Center
(2014M1A8A1049293) by the Ministry of Science, ICT and Future Planning.
CR [Anonymous], 2013, THESIS U ILLINOIS UR
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NR 38
TC 36
Z9 37
U1 11
U2 75
PI OXFORD
SN 0360-5442
EI 1873-6785
J9 ENERGY
JI Energy
PD FEB 1
PY 2017
VL 120
BP 884
EP 894
DI 10.1016/j.energy.2016.11.140
PG 11
GA EN4BQ
UT WOS:000395953000076
DA 2023-12-05
ER
PT J
AU Yang, GW
Wang, XH
Huang, FX
Yang, D
Wei, PY
Hao, X
AF Yang, Guangwei
Wang, Xinhua
Huang, Fuxiang
Yang, Die
Wei, Pengyuan
Hao, Xin
TI Influence of Calcium Addition on Inclusions in LCAK Steel with Ultralow
Sulfur Content
LA English
DT Article
ID LIQUID-IRON; NONMETALLIC INCLUSIONS; EQUILIBRIUM; DEOXIDATION; ALUMINUM
AB Experiments with different calcium addition were carried out in a MgO crucible
without slag at 1873 K (1600 degrees C) to investigate the variation of inclusion
composition in low carbon Al-killed (LCAK) steel with ultralow sulfur content
(0.028 to 0.0738 pct Al, 7 to 9 ppm S). It was found that total oxygen (T. O)
content in steel decreases whereas [mass pct Ca]/[mass pct T. O] and [mass pct
Mg]/[mass pct T. O] increase with CaSi addition. Inclusions change from spherical
CaO-Al2O3(-CaS-MgO) to irregular CaO-CaS with CaSi addition. The Al2O3 content in
inclusions linearly decreases by increasing [mass pct Ca]/[mass pct T. O] of the
steel and it disappears when [mass pct Ca]/[mass pct T. O] exceeds 3. In addition,
(mass pct CaS)/(mass pct CaO) of the inclusions linearly increases by increasing
[mass pct S]/[mass pct T. O] of the steel. The steel composition for CaO-CaS
formation is obtained. The mechanism of inclusion evolution is discussed.
C1 [Yang, Guangwei; Wang, Xinhua; Huang, Fuxiang; Yang, Die; Wei, Pengyuan; Hao,
Xin] Univ Sci & Technol Beijing, Sch Met & Ecol Engn, Beijing 100083, Peoples R
China.
RP Yang, GW (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol
Engn, 30 Xueyuan Rd, Beijing 100083, Peoples R China.
EM ustb_jack@hotmail.com
RI Wang, Xiaoqiang/IQS-3727-2023; Wang, Xin/JCE-2009-2023; Wang,
Xinhua/ISR-8520-2023; Wang, Xin/AAN-8435-2021; Wang, Xin/GYU-1129-2022
OI Wang, Xin/0000-0002-4457-7376; Wang, Xin/0000-0002-4457-7376;
FU National Basic Research Program of China [2010CB630806]; National
Natural Science Foundation of China [51204014, 51304013]
FX The authors gratefully express their appreciation to the National Basic
Research Program of China (No. 2010CB630806) and National Natural
Science Foundation of China (No. 51204014 and No. 51304013) for
sponsoring this work.
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[No title captured]
NR 31
TC 36
Z9 41
U1 0
U2 16
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD FEB
PY 2015
VL 46
IS 1
BP 145
EP 154
DI 10.1007/s11663-014-0181-1
PG 10
Engineering
GA AZ4NS
UT WOS:000348199900019
DA 2023-12-05
ER
PT J
AU Yu, X
Wen, GH
Tang, P
Ma, FJ
Wang, H
AF Yu Xiong
Wen Guang-hua
Tang Ping
Ma Fan-jun
Wang Huan
TI Behavior of Mold Slag Used for 20Mn23Al Nonmagnetic Steel During Casting
SO JOURNAL OF IRON AND STEEL RESEARCH INTERNATIONAL
LA English
DT Article
DE nonmagnetic steel; continuous casting; mold slag; viscosity; CaF2
ID TRANSFORMERS; FLUXES; PLATES
AB Because of the addition of significant quantities of aluminum and manganese, the
great challenge of casting 20Mn23Al nonmagnetic steel is to design a mold slag that
is chemically compatible with this steel composition. A new mold slag with low
melting point and low basicity was proposed. The initial slag (the base mold slag)
and two corresponding mold slags sampled after 8 min and 15 min were investigated,
and the changes of mold slag composition and properties of molten slag were
discussed. The results showed that the slag quickly changed in chemical composition
to a slag that contained a small quantity of silica and a larger quantity of
alumina, and the basicity increased obviously; the heat flux density through the
slag film decreased slightly compared with the slag film at 0 min, 8 min and 15
min; the mold slag used for nonmagnetic steel was precipitated as CaF2 crystals.
The casting experiment shows that the slab has good surface quality without
longitudinal face cracks and slag inclusions; the Al2O3 content in the molten slag
pool increased with time at the beginning stage, and it can approach equilibrium
state after about 600 s.
C1 [Yu Xiong; Wen Guang-hua; Tang Ping; Ma Fan-jun; Wang Huan] Chongqing Univ, Coll
Mat Sci & Engn, Chongqing 400044, Peoples R China.
RP Yu, X (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
EM yuxiong@cqu.edu.cn
FX Foundation Item: Item Sponsored by National Natural Science Foundation
of China (50874125)
CR Cheng Z, 1998, COMPEL, V17, P347, DOI 10.1108/03321649810203260
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NR 11
TC 36
Z9 39
U1 0
U2 9
PU JOURNAL IRON STEEL RESEARCH EDITORIAL BOARD
PI BEIJING
PA NO. 76 XUEYUAN SOUTH-ROAD, BEIJING 100081, PEOPLES R CHINA
SN 1006-706X
EI 2210-3988
J9 J IRON STEEL RES INT
JI J. Iron Steel Res. Int.
PD JAN
PY 2011
VL 18
IS 1
BP 20
EP 25
PG 6
GA 752QA
UT WOS:000289706200005
DA 2023-12-05
ER
PT J
AU Jansson, S
Brabie, V
Jönsson, P
AF Jansson, S.
Brabie, V.
Jonsson, P.
TI Magnesia-carbon refractory dissolution in Al killed low carbon steel
LA English
DT Article
DE reoxidation; aluminium killed steel; low carbon; inclusions; refractory;
slag
ID BEHAVIOR
AB The effects of rotation speed, steel temperature and steel composition on the
rate of dissolution of MgO-C refractory into Al deoxidised molten steel were
investigated using the rotating cylinder method. Cylinders or rods of MgO-C
refractory material were immersed in an Al deoxidised molten steel. Experiments
were performed for steel temperatures between 1873 and 1973 K and rotation speeds
between 100 and 800 rev min(-1) as well as for different immersion times. For each
case, the dissolution rate of MgO-C material was determined from measurement of the
decrease in the rod radius. The experimental results showed that the dissolution
rate of the MgO-C refractory material increased with an increase in steel
temperature and rotation speed. The findings strongly suggest the diffusion of
magnesium through the slag layer formed around the refractory rods to be a rate
determining step. This thin oxide layer at the steel/refractory interface was found
to be owing to reaction between magnesium vapour and CO generated by the reaction
between MgO and C in the refractory. Oxide inclusions were also found in the steel
melt and they were shown to mainly consist of MgO and Al2O3 or a mixture of the
two.
C1 Royal Inst Technol, Div Appl Proc Met, SE-10044 Stockholm, Sweden.
Dalarna Univ, SE-78188 Borlange, Sweden.
Arvika Gjuteri AB, SE-67182 Arvika, Sweden.
C3 Royal Institute of Technology; Dalarna University
RP Jönsson, P (corresponding author), Royal Inst Technol, Div Appl Proc Met, SE-
10044 Stockholm, Sweden.
EM par@mse.kth.se
RI brabie, voicu/AAY-3195-2021
OI brabie, voicu/0000-0002-5399-4163
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NR 31
TC 36
Z9 42
U1 2
U2 25
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD OCT
PY 2006
VL 33
IS 5
BP 389
EP 397
DI 10.1179/174328106X113977
PG 9
GA 097OJ
UT WOS:000241457300007
DA 2023-12-05
ER
PT J
AU Monaghan, BJ
Chen, L
Sorbe, J
AF Monaghan, BJ
Chen, L
Sorbe, J
TI Comparative study of oxide inclusion dissolution in
CaO-SiO2-Al2O3 slag
LA English
DT Article
DE dissolution; inclusions; alumina; spinel; zirconia
ID ALUMINA-SILICA MELTS; SINTERED ALUMINA; SAPPHIRE; AL2O3
AB The dissolution of alumina, spinel and zirconia inclusions in a liquid CaO-SiO2-
Al2O3 slag has been investigated using laser scanning confocal microscopy. Over the
experimental temperature range 1477-1577 degrees C it is found that alumina
inclusions have a slower dissolution rate than that of spinel, and that zirconia
inclusions form gas bubbles at the inclusion surface during dissolution. The
results have been analysed assuming mass transfer control in the slag phase, and
the slower rate of dissolution of the alumina inclusions is explained by the
observation that they have a greater mass of aluminium oxide, the rate controlling
species, than that of spinel.
C1 Univ Wollongong, Sch Mech Mat & Mechatron Engn, Wollongong, NSW 2522, Australia.
Univ Wollongong, Steel Inst, Wollongong, NSW 2522, Australia.
Inst Natl Sci Appl, F-69621 Villeurbanne, France.
C3 University of Wollongong; University of Wollongong; Institut National
des Sciences Appliquees de Lyon - INSA Lyon
RP Monaghan, BJ (corresponding author), Univ Wollongong, Sch Mech Mat & Mechatron
Engn, Wollongong, NSW 2522, Australia.
EM brian_monaghan@uow.edu.au
OI Monaghan, Brian/0000-0002-6341-3588
CR [Anonymous], THERMOPHYSICAL PROPE
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DEA R, 1993, FUNDAMENTALS STEELMA, P84
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NR 31
TC 36
Z9 38
U1 1
U2 12
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD JUN
PY 2005
VL 32
IS 3
BP 258
EP 264
DI 10.1179/174328105X28793
PG 7
GA 924JS
UT WOS:000228975700015
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Pereira, DA
Couto, DM
Labrincha, JA
AF Pereira, DA
Couto, DM
Labrincha, JA
TI Incorporation of alumina rich residues in refractory bricks
SO CFI-CERAMIC FORUM INTERNATIONAL
LA English
DT Article
AB Properly treated and neutralised sludge or salt slag from the anodising of
aluminium or Al-second melting processes are basically composed of water, colloidal
aluminium hydroxides, and variable minor elements. These residues are often
classified as non-toxic, and their average composition seems favourable for
recycling processes, or for attempting to incorporate them in other products. Ln
this paper, the use of common refractory materials is examined. A detailed
characterisation of residues was made, involving leaching tests, chemical and
mineralogical compositions, drying and firing behaviour, grain size distribution,
and mixing adaptability in wet conditions. Clay-based formulations were also
characterised, and typical industrial processing conditions were preferably
followed. The incorporation of sludges from the waste water of anodising baths is
somewhat limited (up to 5 mass-%), because the characteristics of the fired
material tend to be poorer with increasing sludge contents, as shown by a decrease
of the flexural strength. The inert and refractory characteristics of the sludge
might explain this effect. On the contrary, the incorporation of slag tends to
improve the physical and mechanical characteristics of the ceramic material, due to
its fluxing action. Higher incorporation levels (ca. 10 mass-%) are admissible.
C1 Univ Aveiro, UIMC, Ceram & Glass Engn Dept, P-3810193 Aveiro, Portugal.
CIEA, ISEP, Dept Mech Engn, P-4200 Oporto, Portugal.
C3 Universidade de Aveiro; Instituto Politecnico do Porto
RP Labrincha, JA (corresponding author), Univ Aveiro, UIMC, Ceram & Glass Engn
Dept, P-3810193 Aveiro, Portugal.
RI Labrincha, J./B-3984-2010
OI Labrincha, J./0000-0003-4782-1685
[Anonymous], TILE BRICK INT, DOI DOI 10.1016/S1001-0742(12)60191-0
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NR 13
TC 36
Z9 36
U1 0
U2 5
PU GOLLER VERLAG GMBH
PI BADEN BADEN
PA ASCHMATTSTRASSE 8, D-76532 BADEN BADEN, GERMANY
SN 0173-9913
J9 CFI-CERAM FORUM INT
JI CFI-Ceram. Forum Int.
PD JUL
PY 2000
VL 77
IS 7
BP E21
EP E25
PG 5
GA 340CC
UT WOS:000088514700007
DA 2023-12-05
ER
PT J
AU Zhang, BQ
Fang, HS
Ma, HT
Li, JG
AF Zhang, BQ
Fang, HS
Ma, HT
Li, JG
TI Aluminothermal reaction to prepare Al-Ti-C master alloy
LA English
DT Article
DE Al-Ti-C master alloys; aluminothermal reaction; reaction mechanism;
K2TiF6
ID GRAIN-REFINEMENT; B-TYPE; ALUMINUM; TITANIUM; BORON
AB An investigation was carried out on the reaction process and mechanism between
K2TiF6, graphite powder and aluminum melt with the common Ti concentration of 5 %
similar to 7 % in the grain-refiner AL-Ti-C master alloys and the reaction
temperature of 750 similar to 950 degrees C, aiming at understanding their reaction
mechanism and putting forward the aluminothermal reduction reaction method to
practical use. During experimental investigation, K2TiF6 and graphite wrapped in
aluminum foils were introduced into the aluminum melt at 850 degrees C. Samples of
alloy and slag were investigated by chemical analysis, XRD examination, SEM
observation, and EDS analysis as well. It was found that the reaction was very
vigorous at the beginning of the process and then reached a dynamic equilibrium.
There were 3 particular reactions during the aluminothermal reaction process. At
the beginning stage of the reaction, there emerged the phases of TiC and one type
of metastable intermetallic phase TiAl9 as well as TiAl3 in aluminum melt. At the
late stage of the reaction, the metastable phase TiAl9 disappeared and another
phase of Al4C3 emerged.
C1 Tsing Hua Univ, Dept Mat Sci & Engn, Beijing 100084, Peoples R China.
C3 Tsinghua University
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NR 24
TC 36
Z9 40
U1 0
U2 9
PU ALLERTON PRESS INC
PI NEW YORK
PA 150 FIFTH AVE, NEW YORK, NY 10011 USA
SN 1003-6326
PD FEB
PY 2000
VL 10
IS 1
BP 1
EP 5
PG 5
GA 289GM
UT WOS:000085612200001
DA 2023-12-05
ER
PT J
AU DIMITROV, S
WEYL, A
JANKE, D
AF DIMITROV, S
WEYL, A
JANKE, D
TI CONTROL OF THE ALUMINUM-OXYGEN REACTION IN PURE IRON MELTS
SO STEEL RESEARCH
LA English
DT Article
ID STEEL; EQUILIBRIUM; DEGREESC; SHAPES; OXIDES
AB Modified electrochemical oxygen sensors based on CaO-doped ZrO2 and Y2O3-doped
ThO2 were developed and applied to study the aluminium-oxygen reaction in pure
liquid iron with special regard to the provision of reliable experimental
conditions and the attainment of true chemical equilibrium. The sensors represent
valuable tools particularly for EMF long-term measurements over several hours. At
1600 degrees C, values of the constant K'(Al-O) = 9.77.10(-15) and of the
interaction parameters e(O)(Al) = -5.54 and e(Al)(O) = -9.35 were determined. When
Fe-O-Al melts are covered with a slag phase at an activity a(Al2O3) < 1, e.g., CaO-
saturated CaO-Al2O3 slag, the Al-O relationship in the iron may nevertheless be
controlled by an equilibrium oxide phase at an activity a(Al2O3) = 1, presumably
represented by inclusion particles crossing of pure Al2O3.
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TC 36
Z9 36
U1 0
U2 4
PU VERLAG STAHLEISEN MBH
PI DUSSELDORF
PA SOHNSTRABE 65, D-40237 DUSSELDORF, GERMANY
SN 0177-4832
J9 STEEL RES
JI Steel Res.
PD JAN
PY 1995
VL 66
IS 1
BP 3
EP 7
DI 10.1002/srin.199501762
PG 5
GA QE247
UT WOS:A1995QE24700001
DA 2023-12-05
ER
PT J
AU Komljenovic, M
Tanasijevic, G
Dzunuzovic, N
Provis, JL
AF Komljenovic, M.
Tanasijevic, G.
Dzunuzovic, N.
Provis, J. L.
TI Immobilization of cesium with alkali-activated blast furnace slag
LA English
DT Article
DE Hazardous waste; Solidification; Alkali-activated binder; Leaching;
Nanostructure
ID GAMMA-RAY IRRADIATION; C-S-H; FLY-ASH; METAKAOLIN; GEOPOLYMERS;
CARBONATION; CO-60; RADIONUCLIDES; ENCAPSULATION; TOBERMORITE
AB Alkali-activated binders (AABs), as a promising alternative to Portland cement,
are now being used on a commercial scale in various applications around the world,
including hazardous and radioactive waste immobilization. In this paper, the
leaching resistance, strength, and nanostructural alteration of alkali-activated
blast furnace slag (AABFS) doped with 2 % and 5 % cesium were investigated. The
addition of cesium caused a significant increase in the compressive strength of
AABFS, followed by mild strength reduction after leaching. AABFS can be considered
a potentially efficient matrix for cesium immobilization, since the mean
leachability index in both cases (2 % and 5 % of Cs added) was above the threshold
value of 6. Both doping with Cs and leaching caused the transformation of the AABFS
nanostructure. The majority of the aluminum that was released from the C-A-S-H gel
due to leaching remained within the AABFS matrix, initiating gel reconstruction:
the C-A-S-H gel was converted to C-S-H gel, and an additional N-(C)-A-S-H gel was
also formed. Cesium was preferentially associated with the N-(C)-A-S-H gel rather
than with the C-A-S-H gel. The results of this research seem to be in good
agreement with the Cross-linked Substituted Tobermorite Model (CSTM).
C1 [Komljenovic, M.; Tanasijevic, G.; Dzunuzovic, N.] Univ Belgrade, Inst
Multidisciplinary Res, Kneza Viseslava 1, Belgrade 11030, Serbia.
[Provis, J. L.] Univ Sheffield, Dept Mat Sci & Engn, Mappin St, Sheffield S1
3JD, S Yorkshire, England.
C3 University of Belgrade; University of Sheffield
RP Komljenovic, M (corresponding author), Univ Belgrade, Inst Multidisciplinary
Res, Kneza Viseslava 1, Belgrade 11030, Serbia.
EM miroslav.komljenovic@imsi.rs
RI Provis, John/AAR-3260-2020; Miroslav, Komljenovic/H-8557-2019
OI Provis, John/0000-0003-3372-8922; Miroslav,
Komljenovic/0000-0001-5322-6984; Dzunuzovic, Natasa/0000-0001-9548-114X
FU NATO SPS programme [G5402]; Ministry of Education, Science and
Technological Development of the Republic of Serbia [TR 34,026]
FX This research was financially supported by the NATO SPS programme
(project G5402) and the Ministry of Education, Science and Technological
Development of the Republic of Serbia (project TR 34,026). The authors
would like to thank Dr. Ljiljana Kostic-Kravljanac (Institute for
Multidisciplinary Research, University of Belgrade) for assistance in
acquiring the ICP-OES data, Dr. Marin Tadic (Institute for nuclear
sciences, University of Belgrade) for the XRD data, and Dr. Zoran
Miladinovic (Institute of general and physical chemistry, Belgrade) for
the NMR data.
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NR 57
TC 35
Z9 35
U1 2
U2 25
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD APR 15
PY 2020
VL 388
AR 121765
DI 10.1016/j.jhazmat.2019.121765
PG 16
GA LB2JV
UT WOS:000524462500040
PM 31928790
OA Green Published, Green Accepted, hybrid
DA 2023-12-05
ER
PT J
AU Lau, CK
Rowles, MR
Parnham, GN
Htut, T
Ng, TS
AF Lau, Chee Keong
Rowles, Matthew R.
Parnham, Glenn N.
Htut, Trevor
Ng, Tian Sing
TI Investigation of geopolymers containing fly ash and ground-granulated
blast-furnace slag blended by amorphous ratios
LA English
DT Article
DE Fly ash; Ground-granular blast furnace slag; Geopolymer; Amorphous
material; X-ray diffraction
ID METAKAOLIN-BASED GEOPOLYMERS; SODIUM-SILICATE ACTIVATION;
MICROSTRUCTURAL DEVELOPMENT; COMPRESSIVE STRENGTH; PHASE EVOLUTION;
OPTIMIZATION; WORKABILITY; DIFFRACTION; PERFORMANCE; REACTIVITY
AB A new amorphous phase mix design framework had been successfully developed in
consideration of calcium content through the combination of ground-granular blast-
furnace slag (GGBFS) in fly ash (FA) blended geopolymers. The new framework has
been developed considering the amorphous silicon, aluminium, sodium and calcium
containing phases of the aluminosilicate sources to increase geopolymerisation
reactivity and compressive strength. By utilising this new framework, this study
found that the optimal amorphous Si/Al ratio of FA- and GGBFS-blended geopolymers
are between 2.3 and 3.1. At 40-50% of FA replacement with GGBFS, it had been
observed that blended geopolymers are able to achieve the majority of its 28 days
compressive strength at 7 days. To account for the effect of calcium content, a new
amorphous ratio, (Na + 2Ca)/Al, is proposed, with an optimal ratio of between 3.2
and 3.4. (C) 2019 Elsevier Ltd. All rights reserved.
C1 [Lau, Chee Keong; Parnham, Glenn N.; Htut, Trevor; Ng, Tian Sing] Curtin Univ,
Sch Civil & Mech Engn, Perth, WA, Australia.
[Rowles, Matthew R.] Curtin Univ, John de Laeter Ctr, Perth, WA, Australia.
C3 Curtin University; Curtin University
RP Htut, T (corresponding author), Curtin Univ, Sch Civil & Mech Engn, Perth, WA,
Australia.
EM trevor.htut@curtin.edu.au
RI Rowles, Matthew/AAD-7885-2019
OI Rowles, Matthew/0000-0002-7448-6774; , Chee Keong/0000-0002-5198-6338
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A. International, 2017, C61817A ASTM
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10.1016/j.conbuildmat.2014.05.080
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NR 48
TC 35
Z9 35
U1 4
U2 27
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 20
PY 2019
VL 222
BP 731
EP 737
DI 10.1016/j.conbuildmat.2019.06.198
PG 7
GA IU3BS
UT WOS:000483454300065
DA 2023-12-05
ER
PT J
AU Li, FH
Ma, XW
Xu, ML
Fang, YT
AF Li, Fenghai
Ma, Xiuwei
Xu, Meiling
Fang, Yitian
TI Regulation of ash-fusion behaviors for high ash-fusion-temperature coal
by coal blending
LA English
DT Article
DE Regulation; Ash-fusion behavior; High ash-fusion-temperature coal; Coal
blending
ID FLOW PROPERTIES; SLAG FLOW; FUSIBILITY; BIOMASS; GLASS
AB Blending is a promising method to modify the ash-fusion characteristics of coal
to meet gasification requirements. To investigate the variation in ash-fusion
behavior for high ash-fusion-temperature (AFT) coal through coal blending and its
regulating mechanism, the ash-chemistry characteristics of four coals (Nantun,
Pengzhuang, Biaodian, and Xiangyuan) were analyzed. Mineral-transformation
behaviors in the mixed ashes were investigated by X-ray powder diffractometry using
normalized reference intensity ratio software, scanning electron microscopy
analyzer equipped with energy-dispersive X-ray spectrometry, and FactSage software.
Pengzhuang and Biaodian coals, AFTs meet entrained-flow gasifier requirements when
the Xiangyuan mass ratio reaches 20%. The Nantun requires a Xiangyuan mass ratio of
XY >30% because of its high aluminum oxide content. The required Xiangyuan optimal
blending mass ratio is 40%-70% for the three high AFT coals to meet gasification
requirements in the entrained-flow gasifier. An increased Xiangyuan mass ratio
leads to decreasing contents of high melting-point mullite and silica and
increasing contents of low melting-point anorthite, hercynite, gehienite, and
hedenbergite. Amorphous matter in three mixed ash types resulted in a decrease in
their AFTs. The variation in liquid phase under certain conditions reflects the
change in AFT. (C) 2017 Elsevier B.V. All rights reserved.
C1 [Li, Fenghai; Xu, Meiling] Heze Univ, Dept Chem & Engn, Heze 274015, Peoples R
China.
[Li, Fenghai; Ma, Xiuwei] Henan Polytech Univ, Sch Mat Sci & Engn, Jiaozuo
RP Li, FH (corresponding author), Heze Univ, Dept Chem & Engn, Heze 274015, Peoples
R China.
EM hzlfh@163.com
RI LI, feng/HIR-1703-2022
FU Natural Science Foundation of Shandong Province, China [ZR2014BM014];
Strategic Priority Research Program of the Chinese Academy of Sciences
[XDA07050103]; Youth Natural Science Foundation of Shanxi Province,
China [Y5SJ1A1121]
Shandong Province, China (ZR2014BM014), the Strategic Priority Research
Program of the Chinese Academy of Sciences (XDA07050103), and Youth
Natural Science Foundation of Shanxi Province, China (Y5SJ1A1121).
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NR 44
TC 35
Z9 37
U1 5
U2 76
PU ELSEVIER
PI AMSTERDAM
SN 0378-3820
EI 1873-7188
PD NOV
PY 2017
VL 166
BP 131
EP 139
DI 10.1016/j.fuproc.2017.05.012
PG 9
GA FD2ZG
UT WOS:000407402700015
DA 2023-12-05
ER
PT J
AU Li, C
Gao, JT
Wang, Z
Guo, ZC
AF Li, Chong
Gao, Jintao
Wang, Zhe
Guo, Zhancheng
TI Separation of Fine Al2O3 Inclusion from Liquid
Steel with Super Gravity
LA English
DT Article
ID FUNCTIONALLY GRADED MATERIALS; ROTATING PACKED-BED; BEARING SLAG MELT;
SUPERGRAVITY FIELD; MASS-TRANSFER; IRON-ORE; PHOSPHORUS; REMOVAL; PHASE;
ALUMINUM
AB An innovative approach of super gravity was proposed to separate fine Al2O3
inclusions from liquid steel in this study. To investigate the removal behaviors of
inclusions, the effects of different gravity coefficients and time on separating
the inclusions were studied. The results show that a large amount of Al2O3
inclusions gathered at the top of the sample obtained by super gravity, whereas
there were almost no inclusions appearing at the bottom. The volume fraction and
number density of inclusions presented a gradient distribution along the direction
of the super gravity, which became steeper with increasing gravity coefficient and
separating time. As a result of the collision between inclusions, a large amount of
inclusions aggregated and grew during the moving process, which further decreased
the removal time. The experimental required removal time of inclusions is close to
the theoretical values calculated by Stokes law under gravity coefficient G
ae<currency> 80, t ae<currency> 15 minutes, and the small deviation may be because
the inclusion particles are not truly spherical. Under the condition of gravity
coefficient G = 80, t = 15 minutes, the total oxygen content at the bottom of the
sample (position of 5 cm) is only 8.4 ppm, and the removal rate is up to 95.6 pct
compared with that under normal gravity.
C1 [Li, Chong; Gao, Jintao; Wang, Zhe; Guo, Zhancheng] Univ Sci & Technol Beijing,
State Key Lab Adv Met, Beijing 100083, Peoples R China.
RP Gao, JT (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
Met, Beijing 100083, Peoples R China.
EM jintaogao@ustb.edu.cn
RI Guo, Z. C./AAS-1733-2021
FU National Natural Science Foundations of China [51234001, 51404025];
Fundamental Research Funds for the Central Universities
[FRF-TP-15-009A2]
FX This work is supported by the National Natural Science Foundations of
China (Nos. 51234001 and 51404025) and the Fundamental Research Funds
for the Central Universities (FRF-TP-15-009A2), which is acknowledged
with thanks.
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NR 26
TC 35
Z9 38
U1 3
U2 22
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD APR
PY 2017
VL 48
IS 2
BP 900
EP 907
DI 10.1007/s11663-016-0905-5
PG 8
Engineering
GA EN5EO
UT WOS:000396028600015
DA 2023-12-05
ER
PT J
AU Lu, BX
Wang, WL
AF Lu, Boxun
Wang, Wanlin
TI Effects of Fluorine and BaO on the Crystallization Behavior of
Lime-Alumina-Based Mold Flux for Casting High-Al Steels
LA English
DT Article
ID VISCOSITY; SYSTEM; SLAGS
AB With the development of advanced high-strength steel, the slag/steel reaction
problems introduced by the addition of aluminum into steel become a challenge for
the continuous casting process. An investigation aims to improve the
crystallization property of lime-alumina-based mold flux for casting high Al-
bearing steels which was carried out through the study of effects of fluorine and
BaO on the crystallization behaviors of the mold flux. The single/double hot
thermocouple technique and SEM, EDS were employed in the study. The results
indicated that the decrease of fluorine content would promote the crystallization
behaviors in the lime-alumina-based system which is different to that in the
conventional lime-silica-based system, while BaO substituted for CaO can inhibit
the crystallization of the lime-alumina-based mold flux. Moreover, the
crystallization behavior of mold flux under simulated thermal gradient was in well
accordance with TTT results, including the crystallization process and three-
layered (liquid, crystalline, glassy) distribution of mold flux. (C) The Minerals,
Metals & Materials Society and ASM International 2015
C1 [Lu, Boxun; Wang, Wanlin] Cent S Univ, Sch Met & Environm, Changsha 410083,
Peoples R China.
FU NSFC [51274244, 51322405]; Hunan Excellent Young Scholar Funding
[14JJ1005]
FX The financial support from NSFC (51274244, 51322405) and Hunan Excellent
Young Scholar Funding (14JJ1005) is greatly acknowledged.
CR [Anonymous], 1995, VEREIN DTSCH EISENHU, P105
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Jeffrey J. B., 2005, AISTECH P, V11, P99
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Wang Q., 2012, THESIS CENTRAL IRON
Wang Y., 2007, SPEC STEEL, V28, P22
[No title captured]
NR 21
TC 35
Z9 37
U1 1
U2 43
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD APR
PY 2015
VL 46
IS 2
BP 852
EP 862
DI 10.1007/s11663-014-0285-7
PG 11
Engineering
GA CE5GW
UT WOS:000351860300035
DA 2023-12-05
ER
PT J
AU Seo, J
Kim, S
Park, S
Yoon, HN
Lee, HK
AF Seo, Joonho
Kim, Seonhyeok
Park, Solmoi
Yoon, H. N.
Lee, H. K.
TI Carbonation of calcium sulfoaluminate cement blended with blast furnace
slag
LA English
DT Article
DE Calcium sulfoaluminate; Blast furnace slag; Carbonation:
characterization; Supplementary cementitious material
ID AL-27 MAS NMR; C-S-H; FLY-ASH; HYDRATION KINETICS; BELITE CEMENT; CO2
UPTAKE; ALUMINUM; MICROSTRUCTURE; SILICATE; PERFORMANCE
AB The present study investigated the carbonation of calcium sulfoaluminate (CSA)
cement blended with blast furnace slag. Paste samples were prepared by substituting
CSA cement with slag at dosages of 0, 30, 50, and 70 wt%. The samples were
carbonated for 28 days at a CO2 concentration of 3% after a sufficient pre-curing
period. The test results indicated that slag incorporation did not affect the phase
assemblage of the sample regardless of carbonation, while the incorporated slag
promoted the formation of monosulfate and stratlingite upon carbonation in which
this observation is closely related to the improved reaction degree of Si in the
slag by carbonation. Meanwhile, monosulfate and ettringite were the first phases to
be carbonated, while the C-A-S-H gel formed due to the carbonation of belite,
thereby enhancing the compressive strength by refining the pore size in the gel
pore region. On the other hand, the carbonation degree of the samples vastly
increased as the slag content increased due to a small amount of ettringite formed
along with the low reaction degree of slag which induced the development of
macropores.
C1 [Seo, Joonho; Kim, Seonhyeok; Yoon, H. N.; Lee, H. K.] Korea Adv Inst Sci &
Technol KAIST, Dept Civil & Environm Engn, Daejeon 34141, South Korea.
[Park, Solmoi] Pukyong Natl Univ, Dept Civil Engn, 45 Yongso Ro, Busan 48513,
South Korea.
C3 Korea Advanced Institute of Science & Technology (KAIST); Pukyong
National University
RP Lee, HK (corresponding author), Korea Adv Inst Sci & Technol KAIST, Dept Civil &
Environm Engn, Daejeon 34141, South Korea.
EM haengki@kaist.ac.kr
RI Park, Solmoi/AAA-5658-2022; Park, Solmoi/AAD-5326-2019; Park,
Solmoi/AHE-4311-2022
OI Park, Solmoi/0000-0003-0746-3940; Seo, Joonho/0000-0002-8027-492X
FU National Research Foundation of Korea (NRF) of the Korean government
(Ministry of Science & ICT) through the Smart Submerged Floating Tunnel
System Research Center [2017R1A5A1014883]
FX This study was supported by the National Research Foundation of Korea
(NRF) of the Korean government (Ministry of Science & ICT) [Grant
Number: 2017R1A5A1014883] through the Smart Submerged Floating Tunnel
System Research Center. The authors acknowledge the use of Thermal
Analysis System at the Korea Basic Science Busan Center, and would like
to thank Dr. H.G. Kim for assistance with Thermal Analysis System. The
authors acknowledge the use of Particle and Pore size Analysis System at
the Korea Basic Science Jeonju Center, and would like to thank Dr. S.J.
Lee for assistance with Particle and Pore size Analysis System.
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NR 69
TC 34
Z9 35
U1 4
U2 33
PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
PD APR
PY 2021
VL 118
AR 103918
DI 10.1016/j.cemconcomp.2020.103918
EA FEB 2021
PG 11
GA RC1JK
UT WOS:000632557900003
DA 2023-12-05
ER
PT J
AU Li, J
Sun, P
Li, JX
Lv, Y
Ye, HP
Shao, L
Du, DY
AF Li, Jia
Sun, Peng
Li, Jiaxin
Lv, Ying
Ye, Hengpeng
Shao, Li
Du, Dongyun
TI Synthesis of electrolytic manganese residue-fly ash based geopolymers
with high compressive strength
LA English
DT Article
DE Electrolytic manganese residue; Fly ash; Geopolymer; Compressive
strength
ID LATERITIC SOIL; HEAVY-METALS; RED MUD; CEMENT; CODISPOSAL; SLAG;
PROPERTY; SULFATE; BINDER
AB A large amount of electrolytic manganese residue (EMR) has been produced in
electrolytic manganese industry and caused great damage to the environment. In this
study, industrial solid waste of EMR and fly ash (FA) were used as solid
aluminosilicate raw materials (ASM) to prepare geopolymers with high mechanical
strength and good environmental stability. The influences of EMR/ASM ratio,
Liquid/Solid ratio (L/S) and curing conditions were studied to guide the production
of geopolymers with excellent properties. The results showed that EMR-FA based
geopolymer with acceptable compressive strength (16 MPa), good environmental
stability and low leaching toxicity can be obtained under the conditions of EMR/ASM
= 0.6, L/S = 0.25 and curing at 80 degrees C for 12 h. The mineral composition of
geopolymers was analyzed by X-ray diffraction spectrometer (XRD), which indicated
that the geopolymers were mainly amorphous aluminosilicate. By scanning electron
microscope and energy dispersive spectrometer analysis, the EMR-FA based geopolymer
exhibits a smooth and dense surface of cementitious material with the main elements
of silicon, aluminum, calcium and sodium. The geopolymerization was analyzed by
Fourier transform infrared spectra and the mechanism was discussed. (C) 2020
Published by Elsevier Ltd.
C1 [Li, Jia; Sun, Peng; Li, Jiaxin; Ye, Hengpeng; Shao, Li; Du, Dongyun] South Cent
Univ Nationalities, Sch Resource & Environm Sci, Wuhan 430074, Peoples R China.
[Li, Jia] Yale Univ, Sch Forestry & Environm Studies, New Haven, CT 06511 USA.
[Lv, Ying] GRINM Grp Corp Ltd, Natl Engn Lab Biohydromet, Beijing 101407,
Peoples R China.
[Lv, Ying] GRINM Resources & Environm Tech Co Ltd, Beijing 101407, Peoples R
China.
[Lv, Ying] Gen Res Inst Nonferrous Met, Beijing 100088, Peoples R China.
[Lv, Ying] Univ Sci & Technol Beijing, Sch Met & Ecol Engn, Beijing 100083,
Peoples R China.
C3 South Central Minzu University; Yale University; General Research
Institute for Nonferrous Metals; University of Science & Technology
Beijing
RP Ye, HP (corresponding author), South Cent Univ Nationalities, Sch Resource &
Environm Sci, Wuhan 430074, Peoples R China.
EM yehengpeng@126.com
RI 李, 嘉馨/IWM-4023-2023; wang, qiang/IZW-1751-2023
OI Lv, Ying/0000-0003-3026-0498
FU National Natural Science Foundation of China [51804354]; Scientific
Special of Central Higher Educatiom Institutions [CZZ20003]
FX This project is financially supported by the National Natural Science
Foundation of China (51804354) and the Scientific Special of Central
Higher Educatiom Institutions (No. CZZ20003), which are greatly
appreciated.
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NR 44
TC 34
Z9 35
U1 12
U2 90
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUL 10
PY 2020
VL 248
AR 118489
DI 10.1016/j.conbuildmat.2020.118489
PG 9
GA LK7ZX
UT WOS:000531081200007
DA 2023-12-05
ER
PT J
AU Li, XM
Zhi, LF
Shi, WJ
Kong, LX
Bai, J
Yu, JL
Reinmöller, M
Guhl, S
Meyer, B
Li, W
AF Li, Xiaoming
Zhi, Lifei
Shi, Wenju
Kong, Lingxue
Bai, Jin
Yu, Jianglong
Reinmoeller, Markus
Guhl, Stefan
Meyer, Bernd
Li, Wen
TI Effect of K2O/Na2O on fusion behavior of coal ash
with high silicon and aluminum level
SO FUEL
LA English
DT Article
DE K2O/Na2O; Ash fusibility; Mixed-alkaline effect; High silicon and
aluminium
ID DIRECT LIQUEFACTION; ZHUNDONG COAL; GASIFICATION; SODIUM; SLAG;
TEMPERATURE; VISCOSITY; RICH
AB Ash fusion temperatures (AFTs) are widely used for evaluation of fusibility of
coal ash for combustion and gasification. K2O and Na2O is regarded as the effective
component to enhance the ash fusibility for slag tapping. The combination of K2O
and Na2O may enhance the flux efficiency. In this work, the effect of K2O/Na2O mass
ratio on fusion behavior of coal ash with high silicon and alumina level was
evaluated by the height variation of ash cone during heating. The results showed
that AFTs and theoretical fusion range (T-liq-T-ini) decreased quickly and then
increased slowly as the K2O/Na2O mass ratio in the coal ash was reduced. The sub-
liquidus phase changed from mullite into feldspar, which was responsible for change
of AFTs. Meanwhile, most of K element occurred in leucite (KAlSi2O6) and the rest
existed in nepheline (KAlSiO4), but Na almost existed in nepheline (NaAlSiO4). The
competition effect between K2O and Na2O on AFTs was reflected by KAlSiO4/NaAlSiO4
in nepheline, so the SiO2-KAlSi2O6-NaAlSi2O6 ternary phase diagram was constructed,
which well explained the variation of AFTs caused by K2O/Na2O mass ratio.
Meanwhile, the fusion process was divided into two stages based on variation rate
of ash cone height. At first stage, the amount of liquidus phase is limited and the
viscosity is high, so only a low shrinkage rate of ash cone exhibits. However, at
the second stage, high shrinking rate is caused by not only the rapid increase of
slag content but also the sharp decrease of viscosity besides, the addition of
K2O/Na2O change ash fusion process from "melting-dissolving" into "softening-
melting".
C1 [Li, Xiaoming; Zhi, Lifei] Taiyuan Univ Sci & Technol, Sch Chem & Biol Engn,
Taiyuan, Shanxi, Peoples R China.
[Shi, Wenju; Kong, Lingxue; Bai, Jin; Li, Wen] Chinese Acad Sci, Inst Coal Chem,
State Key Lab Coal Convers, Taiyuan 030001, Peoples R China.
[Shi, Wenju] Univ Chinese Acad Sci, Beijing 100049, Peoples R China.
[Yu, Jianglong] Univ Sci & Technol Liaoning, Sch Chem Engn, Key Lab Adv Coal &
Coking Technol Liaoning Prov, Anshan 114051, Peoples R China.
[Yu, Jianglong] Univ Newcastle, ICCCF, Callaghan, NSW 2308, Australia.
[Yu, Jianglong] Univ Newcastle, Chem Engn, Callaghan, NSW 2308, Australia.
[Reinmoeller, Markus; Guhl, Stefan; Meyer, Bernd] Tech Univ Bergakad Freiberg,
Inst Energy Proc Engn & Chem Engn, D-09599 Freiberg, Germany.
[Meyer, Bernd] Fraunhofer Inst Microstruct Mat & Syst IMWS, Branch Circular
Carbon Technol, Walter Hulse Str 1, D-06120 Halle, Germany.
C3 Taiyuan University of Science & Technology; Chinese Academy of Sciences;
Institute of Coal Chemistry, CAS; Chinese Academy of Sciences;
University of Chinese Academy of Sciences, CAS; University of Science &
Technology Liaoning; University of Newcastle; University of Newcastle;
Technical University Freiberg; Fraunhofer Gesellschaft
RP Shi, WJ; Bai, J (corresponding author), Chinese Acad Sci, Inst Coal Chem, State
Key Lab Coal Convers, Taiyuan 030001, Peoples R China.
EM shiwenju15@mails.ucas.edu.cn; stone@sxicc.ac.cn
RI yu, jiang/IQT-1529-2023; Ran, Chen/JMR-1744-2023
OI Bai, Jin/0000-0002-8623-1656; Reinmoller, Markus/0000-0001-8188-5469;
Yu, Jianglong/0000-0002-5932-0813
FU Natural Science Foundation of Shanxi Province [201801D121050,
201801D121051]; Fund Program for the Scientific Activities of Selected
Returned Overseas Professionals in Shanxi Province [2017006]; Doctoral
Scientific Research Foundation of Taiyuan University of Science and
Technology [20162023]; Joint Foundation of Natural Science Foundation of
China [U1510201]; Joint Foundation of Natural Science Foundation of
Shanxi Province [U1510201]; NSFC-DFG [21761132032]
FX This work was supported by Natural Science Foundation of Shanxi Province
[Grant numbers 201801D121050 and 201801D121051], Fund Program for the
Scientific Activities of Selected Returned Overseas Professionals in
Shanxi Province [Grant number 2017006], Doctoral Scientific Research
Foundation of Taiyuan University of Science and Technology [Grant number
20162023], Joint Foundation of Natural Science Foundation of China and
Shanxi Province [Grant number U1510201], and NSFC-DFG [grant number
21761132032].
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TC 34
Z9 36
U1 7
U2 58
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD APR 1
PY 2020
VL 265
AR 116964
DI 10.1016/j.fuel.2019.116964
PG 9
GA KF0BM
UT WOS:000508914300059
DA 2023-12-05
ER
PT J
AU Mishra, B
Gostu, S
AF Mishra, Brajendra
Gostu, Sumedh
TI Materials sustainability for environment: Red-mud treatment
SO FRONTIERS OF CHEMICAL SCIENCE AND ENGINEERING
LA English
DT Review
DE red-mud processing; waste management; sustainability; valorization
ID MAGNETIC SEPARATION; BAUXITE RESIDUE; IRON RECOVERY; ALUMINA;
EXTRACTION; REDUCTION; SCANDIUM; ELEMENTS; PHASE; RICH
AB Bayer's process revolutionized the extraction of aluminum from the bauxite ores.
However, the hydrothermal extraction of alumina is associated with the generation
of a byproduct, red-mud consisting of undissolved solids composed of iron oxides,
sodium alumino silicates, titania, silica and rare earth elements. The accumulation
of red-mud (or bauxite residue) in the world is 30 billion metric tons produced at
a rate of 125 million tons per annum (2013). Utilization of red-mud for
constructional purposes, wastewater treatment, metallurgical products, and pigments
are listed. Metallurgical processing efforts of red-mud to generate various value
added products such as pig iron, direct reduced iron slag wool, magnetite, titania,
iron carbides are presented in the article.
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USA.
[Gostu, Sumedh] Worcester Polytech Inst, Dept Mat Sci & Engn, Worcester, MA
01609 USA.
C3 Worcester Polytechnic Institute; Worcester Polytechnic Institute
RP Mishra, B (corresponding author), Worcester Polytech Inst, Dept Mech Engn,
Worcester, MA 01609 USA.
EM BMishra@wpi.edu
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NR 49
TC 34
Z9 37
U1 23
U2 167
PU SPRINGER
PI NEW YORK
SN 2095-0179
EI 2095-0187
J9 FRONT CHEM SCI ENG
JI Front. Chem. Sci. Eng.
PD SEP
PY 2017
VL 11
IS 3
BP 483
EP 496
DI 10.1007/s11705-017-1653-z
PG 14
SC Engineering
GA FF5VI
UT WOS:000409067300021
DA 2023-12-05
ER
PT J
AU Piva, SPT
Kumar, D
Pistorius, PC
AF Piva, Stephano P. T.
Kumar, Deepoo
Chris Pistorius, P.
TI Modeling Manganese Silicate Inclusion Composition Changes during Ladle
Treatment Using FactSage Macros
LA English
DT Article
ID DEOXIDIZED STEEL; DESULFURIZATION
AB This work investigated the use of FactSage macros to simulate steel-slag and
steel-inclusion reaction kinetics in silicon-manganese killed steels, and predict
oxide inclusion composition changes during ladle treatment. These changes were
assessed experimentally using an induction furnace to simulate deoxidation and slag
addition. The average steel mass transfer coefficient for the experimental setup
was calculated from the analyzed aluminum pick-up by steel. Average oxide inclusion
composition was measured using scanning electron microscopy and energy-dispersive
X-ray spectroscopy. Confocal laser scanning microscopy was used to assess the
physical state (solid or liquid) of oxide inclusions in selected samples. The
changes in the chemical compositions of the oxide inclusions and the steel agreed
with the FactSage macro simulations.
C1 [Piva, Stephano P. T.; Kumar, Deepoo; Chris Pistorius, P.] Carnegie Mellon Univ,
Dept Mat Sci & Engn, Ctr Iron & Steelmaking Res, Pittsburgh, PA 15213 USA.
[Piva, Stephano P. T.] CAPES Fdn, Minist Educ Brazil, BR-70040020 Brasilia, DF,
Brazil.
C3 Carnegie Mellon University; Coordenacao de Aperfeicoamento de Pessoal de
Nivel Superior (CAPES)
Ctr Iron & Steelmaking Res, Pittsburgh, PA 15213 USA.
RI Pistorius, Petrus Christiaan/A-8247-2011; Kumar, Deepoo/AAP-4932-2021
OI Pistorius, Petrus Christiaan/0000-0002-2966-1879; Kumar,
Deepoo/0000-0002-4396-6097; Papadopoli Tonelli Piva,
Stephano/0000-0002-8013-568X
FU CAPES [BEX 13379/13-5]; [MCF-677785]
FX We are grateful for support of this work by the industrial members of
the Center for Iron and Steelmaking Research. We acknowledge use of the
Materials Characterization Facility at Carnegie Mellon University
supported by Grant MCF-677785. The financial support of Stephano P.T.
Piva by CAPES under the process BEX 13379/13-5-Doutorado Pleno/Ciencia
sem Fronteiras is gratefully acknowledged.
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NR 18
TC 34
Z9 40
U1 3
U2 26
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD FEB
PY 2017
VL 48
IS 1
BP 37
EP 45
DI 10.1007/s11663-016-0764-0
PG 9
Engineering
GA EI2CZ
UT WOS:000392295500008
DA 2023-12-05
ER
PT J
AU Walkley, B
San Nicolas, R
Sani, MA
Gehman, JD
van Deventer, JSJ
Provis, JL
AF Walkley, Brant
San Nicolas, Rackel
Sani, Marc-Antoine
Gehman, John D.
Provis, John L.
TI Synthesis of stoichiometrically controlled reactive aluminosilicate and
calcium-aluminosilicate powders
SO POWDER TECHNOLOGY
LA English
DT Article
DE Amorphous aluminosilicates; Powder synthesis; NMR spectroscopy
ID PORTLAND-CEMENT COMPONENTS; POLY(VINYL ALCOHOL); NMR-SPECTRA; RANGE
ORDER; HIGH-FIELD; AL-27 NMR; FLY-ASH; SI-29; SLAG; STATE
AB Aluminosilicate and calcium-aluminosilicate powders are synthesised via an
organic steric entrapment route under conditions permitting strict stoichiometric
control, utilising polyvinyl alcohol and polyethylene glycol as polymeric carriers.
Polyethylene glycol is superior to polyvinyl alcohol for synthesis of calcium-
aluminosilicate powders via this method, producing a more controllable product
which generated less fine ash during calcination. This paper presents detailed
description of synthesis and characterisation of the powders produced through this
approach, including new insight into the nanostructures within the calcined
powders. Aluminium environments are a mixture of 4-, 5- and 6-coordinated, while
silicon is tetrahedral and shows a broad range of connectivity states. The powders
are X-ray amorphous, display a high degree of homogeneity, and thus offer potential
for utilisation as precursors for synthesis of hydrous aluminosilicates in the
quaternary CaO-Na2O-Al2O3-SiO2 system. (C) 2016 Elsevier B.V. All rights reserved.
C1 [Walkley, Brant; San Nicolas, Rackel; van Deventer, Jannie S. J.] Univ
Melbourne, Dept Chem & Biomol Engn, Melbourne, Vic 3010, Australia.
3010, Australia.
[Sani, Marc-Antoine; Gehman, John D.] Univ Melbourne, Sch Chem, Melbourne, Vic
3010, Australia.
[Sani, Marc-Antoine; Gehman, John D.] Univ Melbourne, Inst Bio21, Melbourne, Vic
3010, Australia.
[Gehman, John D.] GehmanLab, Woodend, Vic 3442, Australia.
[van Deventer, Jannie S. J.] Zeobond Pty Ltd, POB 23450, Docklands, Vic 8012,
Australia.
[Provis, John L.] Univ Sheffield, Dept Mat Sci & Engn, Sheffield S1 3JD, S
Yorkshire, England.
C3 University of Melbourne; University of Melbourne; University of
Melbourne; University of Melbourne; University of Sheffield
RI Provis, John L/A-7631-2008; Sani, Marc-Antoine/B-7707-2013; Provis,
John/AAR-3260-2020
OI Provis, John L/0000-0003-3372-8922; Sani,
Marc-Antoine/0000-0003-3284-2176; Provis, John/0000-0003-3372-8922;
Walkley, Brant/0000-0003-1069-1362
FU Australian Research Council (ARC) through the Particulate Fluids
Processing Centre, a Special Research Centre of the ARC; University of
Melbourne
(ARC), including support through the Particulate Fluids Processing
Centre, a Special Research Centre of the ARC. The University of
Melbourne also provided support through an Overseas Research Experience
Scholarship to support an extended visit by the first author to the
University of Sheffield. We also wish to thank and acknowledge Professor
Jon Woodhead, School of Earth Sciences, The University of Melbourne for
assistance obtaining the X-ray fluorescence data; Dr. Peng Zeng, Mercury
Centre, The University of Sheffield and Dr. Sergey Rubanov, Advanced
Microscopy Facility, The University of Melbourne for assistance with
transmission electron microscopy experiments; Mr. David Danaci,
Department of Chemical and Biomolecular Engineering, The University of
Melbourne for assistance with nitrogen gas adsorption experiments; and
Dr. Oday H. Hussein, University of Sheffield, for assistance with the
TG-MS experiments.
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NR 65
TC 34
Z9 37
U1 2
U2 50
PU ELSEVIER
PI AMSTERDAM
SN 0032-5910
EI 1873-328X
J9 POWDER TECHNOL
JI Powder Technol.
PD SEP
PY 2016
VL 297
BP 17
EP 33
DI 10.1016/j.powtec.2016.04.006
PG 17
SC Engineering
GA DQ1NZ
UT WOS:000378969000003
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Sun, J
Liu, WQ
Li, MK
Yang, XW
Wang, WY
Hu, YC
Chen, HQ
Li, X
Xu, MH
AF Sun, Jian
Liu, Wenqiang
Li, Mingkui
Yang, Xinwei
Wang, Wenyu
Hu, Yingchao
Chen, Hongqiang
Li, Xian
Xu, Minghou
TI Mechanical Modification of Naturally Occurring Limestone for
High-Temperature CO2 Capture
SO ENERGY & FUELS
LA English
DT Article
ID CAO-BASED SORBENT; CALCIUM LOOPING CYCLES; SELF-REACTIVATION;
FLUIDIZED-BED; CARBIDE SLAG; PERFORMANCE; ENHANCEMENT; CARBONATION;
COMBUSTION; ALUMINATE
AB The rapid decrease of CO2 capture capacity is one of the most challenging
problems hindering the use of naturally occurring limestone in the calcium looping
process. In this work, the mechanical modification method (dry planetary ball
milling) was used to improve the cyclic CO2 capture performance of naturally
occurring limestone. Low-cost Bayer aluminum hydroxide sourced from the industrial-
scale production of alumina from bauxite ore was used as the precursor of the inert
support to enhance the CO2 sorption stability of the ball-milled, sorbents. It was
found that the CO2 uptake of the Milled sorbents could be further improved by
increasing the ball-milling time because this generated more amounts of fine
particles. Moreover, the pellets produced from ball-milled limestone powder
possessed a relatively high. CO2 capture capacity of 0:252 g/g in the 25th cycle,
which is nearly 1.3 times the capture capacity of naturally occurring limestone
powder. This indicates that the combination of mechanical modification and
pelletization is an effective approach to produce highly efficient CO2 capture
pellets from naturally occurring limestone.
C1 [Sun, Jian; Liu, Wenqiang; Li, Mingkui; Yang, Xinwei; Wang, Wenyu; Hu, Yingchao;
Chen, Hongqiang; Li, Xian; Xu, Minghou] Huazhong Univ Sci & Technol, Sch Energy &
Power Engn, State Key Lab Coal Combust, 1037 Luoyu Rd, Wuhan 430074, Hubei, Peoples
R China.
C3 Huazhong University of Science & Technology
RP Liu, WQ; Xu, MH (corresponding author), Huazhong Univ Sci & Technol, Sch Energy
& Power Engn, State Key Lab Coal Combust, 1037 Luoyu Rd, Wuhan 430074, Hubei,
Peoples R China.
EM wenqiang.liu@hust.edu.cn; mhxu@hust.edu.cn
OI Hu, Yingchao/0000-0001-9118-1895
FX The research is supported by the National Natural Science Foundation of
China (51306063 and 21306059). The authors appreciate the Foundation of
State Key Laboratory of Coal Combustion (FSKLCCB1602) and the Analytical
and Testing Center at the Huazhong University of Science and Technology.
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NR 59
TC 34
Z9 34
U1 2
U2 55
PI WASHINGTON
SN 0887-0624
EI 1520-5029
J9 ENERG FUEL
JI Energy Fuels
PD AUG
PY 2016
VL 30
IS 8
BP 6597
EP 6605
DI 10.1021/acs.energyfuels.6b01131
PG 9
GA DT8XH
UT WOS:000381778500045
DA 2023-12-05
ER
PT J
AU Hou, D
Jiang, ZH
Dong, YW
Cao, Y
Cao, H
Gong, W
AF Hou, D.
Jiang, Z. H.
Dong, Y. W.
Cao, Y.
Cao, H.
Gong, W.
TI Thermodynamic design of electroslag remelting slag for high titanium and
low aluminium stainless steel based on IMCT
LA English
DT Article
DE Electroslag remelting; Ion and molecule coexistence theory of slag;
Slag; Titanium control; 1Cr21Ni5Ti
ID SILICON; ALLOYS; OXIDE; MODEL
AB The advantages of the electroslag remelting (ESR) process as to cleanness and
homogeneity of the ingot structure are well known. As to homogeneity of
composition, the control of titanium in stainless steel with high titanium and low
aluminium contents during the ESR process has not been resolved well so far. The
current work focuses on designing appropriate slag for controlling titanium content
during 1Cr21Ni5Ti remelting based on the interaction of the slag/metal interface.
Several kinds of slag containing different CaO contents combined with steel samples
of 1Cr21Ni5Ti were employed to investigate the effect of slag on titanium content
in an electrical resistance furnace, and metal samples were taken at different
times for investigating the change of titanium and aluminium contents in steel. The
results show that slag with low CaO content at low temperature has excellent
capacity for avoiding loss of titanium content caused by its reaction with the
alumina in slag, especially in case of remelting of stainless steel with high
titanium and low aluminium contents. The CaO in slag has great effect on the
activities of TiO2 and Al2O3, and thermodynamic analysis was applied to investigate
the CaO behaviour based on the ion and molecule coexistence theory of slag. The
thermodynamic analysis results show that the lg (a(TiO2)(3)/(a2)(Al2O3)) increases
as CaO content in slag decreases, which is better for preventing loss of titanium
caused by its reaction with the alumina in the ESR slag. The slag with low CaO
content at low temperature is suitable for ESR of 1Cr21Ni5Ti.
C1 [Hou, D.; Jiang, Z. H.; Dong, Y. W.; Cao, Y.; Cao, H.; Gong, W.] Northeastern
Univ, Sch Met & Mat, Shenyang 110819, Peoples R China.
RP Jiang, ZH; Dong, YW (corresponding author), Northeastern Univ, Sch Met & Mat,
Shenyang 110819, Peoples R China.
EM jiangzh@smm.neu.edu.cn; dongyw@smm.neu.edu.cn
OI Jiang, Zhouhua/0000-0001-8887-7250
FU National Nature Science Foundation of China [51274266]; Joint Research
Fund of National Nature Science Foundation of China; Baosteel Group
Corporation [U1360103]; Liaoning Excellent Talents in University
[LR2013009]
FX This project is supported by the National Nature Science Foundation of
China with the grant No. 51274266 and supported by Joint Research Fund
of National Nature Science Foundation of China and Baosteel Group
Corporation with the grant No. U1360103. In addition, this project
supported by Liaoning Excellent Talents in University with the grant No.
LR2013009.
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Bandyopadhyay T.R., 2012, METALL MIN IND, V4, P6
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NR 27
TC 34
Z9 36
U1 2
U2 29
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PY 2016
VL 43
IS 7
BP 517
EP 525
DI 10.1080/03019233.2015.1110920
PG 9
GA DU5OC
UT WOS:000382260100006
DA 2023-12-05
ER
PT J
AU Valcke, SLA
Pipilikaki, P
Fischer, HR
Verkuijlen, MHW
van Eck, ERH
AF Valcke, Siska L. A.
Pipilikaki, Panagiota
Fischer, Hartmut R.
Verkuijlen, Margriet H. W.
van Eck, Ernst R. H.
TI FT-IR and 29Si-NMR for evaluating aluminium-silicate
precursors for geopolymers
LA English
DT Article
DE FT-IR; Solid state Si-29-NMR; Geopolymer; Secondary resources; Fly ash;
Blast furnace slag; Sustainable concrete
ID FLY-ASH; REACTIVITY; KINETICS; ACTIVATION
AB Geopolymers are systems of inorganic binders that can be used for sustainable,
cementless concrete and are formed by alkali activation of an aluminium-silicate
precursor (often secondary resources like fly ash or slag). The type of aluminium-
silicate precursor and its potential variations within one batch may influence
geopolymer performance. Therefore, if geopolymers are to be applied for sustainable
concrete with reproducible quality, a characterization tool for quality control of
precursors and optimizing mix design is needed, which links the (variable)
secondary resource characteristics to the performance of geopolymers. This paper
shows the potential of using FT-IR and solid state Si-29-NMR for a
(semi-)quantitative evaluation of secondary resources suitable for geopolymers.
More specifically, the aim is to investigate whether the presence of particular
aluminium-silicate phases may have a dominant influence on the strength of a simple
geopolymer system. Based on deconvolution of FT-IR and NMR spectra of 9 source
materials (fly ash and slag) and their geopolymers, relative amounts of different
(aluminium-silicate) phases were estimated and trends with strength were evaluated.
A clear trend is observed for both NMR and FT-IR results: the precursors containing
a higher amount of 'active bonds', predominantly from silicates with a medium
amount of aluminium and alkalis incorporated in their framework, result in higher
paste strengths. As such, due to its relatively quick and easy measurements, FT-IR
for estimating relative amounts of these aluminium-silicate phases, can be a useful
tool for evaluating geopolymer precursors.
C1 [Valcke, Siska L. A.; Pipilikaki, Panagiota; Fischer, Hartmut R.] Netherlands
Org Appl Sci Res TNO, Delft, Netherlands.
[Verkuijlen, Margriet H. W.; van Eck, Ernst R. H.] Radboud Univ Nijmegen, Inst
Mol & Mat, NL-6525 ED Nijmegen, Netherlands.
C3 Netherlands Organization Applied Science Research; Radboud University
Nijmegen
RP Valcke, SLA (corresponding author), Netherlands Org Appl Sci Res TNO, Delft,
Netherlands.
EM siska.valcke@tno.nl
RI van Eck, Ernst RH/HKW-3617-2023; van Eck, Ernst RH/F-9704-2015
OI van Eck, Ernst RH/0000-0002-2365-9583;
FU European Union [285463]; Carbon Trust [0911-0252]
FX The research leading to the results in this paper has received funding
from the European Union FP7/2007-2013 programme (GA no285463). Support
of NWO for the 'Solid state NMR facility for advanced materials science'
in Nijmegen is acknowledged. Vliegasunie BV, RockTron International
Limited, West Burton Power Station, Ecocem Materials Limited, Hanson UK,
Queen's University Belfast and the National Technical University of
Athens are acknowledged for providing the samples. The UK samples were
selected based on the work described in Barnett et al. [2], carried out
at Liverpool University in the Carbon Trust funded project 0911-0252.
CR Barbosa VFF, 2000, INT J INORG MATER, V2, P309, DOI 10.1016/S1466-6049(00)00041-
6
Barnett S, 2011, P 31 CEM CONCR C IMP
2916.2009.02948.x
10.1016/j.micromeso.2007.02.055
10.1016/j.micromeso.2005.11.015
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3
Rahier H, 2007, J MATER SCI, V42, P2982, DOI 10.1007/s10853-006-0568-8
Saraber AJ, 2006, INVOLVED POEDERKOOLV
10.1016/j.conbuildmat.2009.09.002
Valcke SLA, 2013, FUEL, V106, P490, DOI 10.1016/j.fuel.2012.12.070
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NR 25
TC 34
Z9 35
U1 3
U2 60
PU SPRINGER
PI DORDRECHT
SN 1359-5997
EI 1871-6873
J9 MATER STRUCT
JI Mater. Struct.
PD MAR
PY 2015
VL 48
IS 3
SI SI
BP 557
EP 569
DI 10.1617/s11527-014-0432-2
PG 13
GA CB2FY
UT WOS:000349443600005
DA 2023-12-05
ER
PT J
AU Risha, GA
Connell, TL
Yetter, RA
Sundaram, DS
Yang, V
AF Risha, Grant A.
Connell, Terrence L., Jr.
Yetter, Richard A.
Sundaram, Dilip S.
Yang, Vigor
TI Combustion of Frozen Nanoaluminum and Water Mixtures
SO JOURNAL OF PROPULSION AND POWER
LA English
DT Article
ID ALUMINUM PARTICLE DUST; HYDROGEN; METAL; SIZE
AB Steady-state strand burner and laboratory-scale static fire motor experiments
were used to determine the relative performance and viability of an environmentally
friendly solid propellant composed of only nanoaluminum and frozen water. The
nominal size of the nanoaluminum particles was 80nm. The particles were
homogeneously mixed with water to form pastes or colloids and then frozen. The
measured parameters include burning rates, slag accumulation, thrust, and pressure.
A system scaling study was performed to examine the effect of the size of the
small-scale motors. The equivalence ratio was fixed at 0.71 for the strand burner
and the laboratory-scale motor experiments. The effect of pressure on the linear
burning rate was also examined. For an equivalence ratio of 0.71, the mixture
exhibited a linear burning rate of 4.8cm/s at a pressure of 10.7MPa and a pressure
exponent of 0.79. Three motors of internal diameters in the range of 1.91-7.62cm
were studied. Grain configuration, nozzle throat diameter, and igniter strength
were varied. The propellants were successfully ignited and combusted in each
laboratory-scale motor, generating thrust levels above 992N in the 7.62-cm-diam
motor with a center-perforated grain configuration (7.62cm length) and an expansion
ratio of 10. For the 7.62cm motor, combustion efficiency was 69%, whereas the
specific impulse efficiency was 64%. Increased combustion efficiency and improved
ease of ignition were observed at higher chamber pressures (greater than 8MPa).
C1 [Risha, Grant A.] Penn State Univ, Div Business & Engn, University Pk, PA 16801
USA.
[Connell, Terrence L., Jr.; Yetter, Richard A.] Penn State Univ, Dept Mech &
Nucl Engn, University Pk, PA 16801 USA.
[Sundaram, Dilip S.; Yang, Vigor] Georgia Inst Technol, Sch Aerosp Engn,
Atlanta, GA 30332 USA.
C3 Pennsylvania Commonwealth System of Higher Education (PCSHE);
University Park; Pennsylvania Commonwealth System of Higher Education
(PCSHE); Pennsylvania State University; Pennsylvania State University -
University Park; University System of Georgia; Georgia Institute of
Technology
RP Risha, GA (corresponding author), Penn State Univ, Div Business & Engn,
University Pk, PA 16801 USA.
OI SUNDARAM, DILIP/0000-0003-3798-5504
FU U.S. Air Force Office of Scientific Research; NASA [FA9550-07-1-0582]
FX The authors would like to thank the U.S. Air Force Office of Scientific
Research and NASA for their sponsorship of this program under contract
no. FA9550-07-1-0582. The authors would also like to thank Timothee L.
Pourpoint, Steven F. Son, Tyler D. Wood, and Mark A. Pfeil from Purdue
University for their contributions. Special thanks go to Rob Uhlig,
Bryan Sones, and Lynn Witherite of the Applied Research Laboratory (ARL)
at Pennsylvania State University for their assistance and usage of the
Pennsylvania State University ARL test cell facilities. The efforts of
Steven Dean for conducting the thermogravimetric analysis and
differential scanning calorimetry experiments, Matthew Loomis for
performing the energy dispersive spectroscopy tests, and Jeff Gesner for
performing Brunauer Emmett Teller and transmission electron microscopy
analyses are greatly appreciated.
CR [Anonymous], 2007, PROG PROPUL PHYS, DOI DOI 10.1051/EUCASS/200901031
[Anonymous], THESIS PURDUE U W LA
Connell T.L., 2011, THESIS PENNSYLVANIA
Connell TL, 2012, INT J ENERG MATER CH, V11, P259, DOI
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Ingenito A, 2004, J PROPUL POWER, V20, P1056, DOI 10.2514/1.5132
Ivanov VG, 2000, COMBUST EXPLO SHOCK+, V36, P213, DOI 10.1007/BF02699363
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MALCHI JY, 2007, THESIS PENNSYLVANIA
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Puri P, 2009, J NANOPART RES, V11, P1117, DOI 10.1007/s11051-008-9505-x
Risha GA, 2007, P COMBUST INST, V31, P2029, DOI 10.1016/j.proci.2006.08.056
Risha GA, 2008, COMBUST SCI TECHNOL, V180, P2127, DOI 10.1080/00102200802414873
Sabourin JL, 2008, COMBUST FLAME, V154, P587, DOI
10.1016/j.combustflame.2008.05.015
Sundaram DS, 2013, P COMBUST INST, V34, P2221, DOI 10.1016/j.proci.2012.06.129
Sutton G. P., 1992, ROCKET PROPULSION EL, P447
Yetter RA, 2009, P COMBUST INST, V32, P1819, DOI 10.1016/j.proci.2008.08.013
NR 24
TC 34
Z9 38
U1 0
U2 30
PU AMER INST AERONAUTICS ASTRONAUTICS
PI RESTON
PA 1801 ALEXANDER BELL DRIVE, STE 500, RESTON, VA 22091-4344 USA
SN 0748-4658
EI 1533-3876
J9 J PROPUL POWER
JI J. Propul. Power
PD JAN-FEB
PY 2014
VL 30
IS 1
BP 133
EP 142
DI 10.2514/1.B34783
PG 10
WC Engineering, Aerospace
SC Engineering
GA AD9SK
UT WOS:000333604600017
DA 2023-12-05
ER
PT J
AU Yang, J
Wang, XH
Jiang, M
Wang, WJ
AF Yang Jun
Wang Xin-hua
Jiang Min
Wang Wan-jun
TI Effect of Calcium Treatment on Non-Metallic Inclusions in Ultra-Low
Oxygen Steel Refined by High Basicity High Al2O3
Slag
LA English
DT Article
DE ultra-low oxygen; top slag; deoxidization; aluminium; oxide inclusion;
calcium treatment
ID COMPLEX DEOXIDATION; CLEANLINESS; ALUMINUM; IRON; AL
AB The influence of calcium treatment on non-metallic inclusions had been studied
when control technology of refining top slag in ladle furnace was used in ultra-low
oxygen steelmaking. A sufficient amount aluminium was added to experimental heats
for final deoxidizing during BOF tapping, and the refining top slag with strong
reducibility, high basicity and high Al2O3 in ladle furnace was used to produce
ultra-low oxygen steel and the transformation of non-metallic inclusions in molten
steel was compared by calcium treatment and no calcium treatment. The results show
that the transformation of Al2O3 -> MgO center dot Al2O3 spinel -> CaO-MgO-Al2O3
complex inclusions has been completed for aluminum deoxidation products and calcium
treatment to molten steel is unnecessary when using the control technology of ladle
furnace refining top slag to produce ultra-low oxygen steel, and the complex
inclusions are liquid at the temperature of steelmaking and easily removable to
obtain very high cleanliness steel by flotation. Furthermore, the problems of
nozzle clogging in casting operations do not happen and the remaining oxide
inclusions in steel are the relatively lower melting point complex inclusions.
C1 [Yang Jun; Wang Xin-hua; Jiang Min; Wang Wan-jun] Univ Sci & Technol Beijing,
RP Yang, J (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol Engn,
EM yangjun20010406@yahoo.com.cn
RI Wang, Xin/AAN-8435-2021; Wang, Xin/JCE-2009-2023
OI Wang, Xin/0000-0002-4457-7376; Wang, Xin/0000-0002-4457-7376
FU National Basic Research Program of China [2010CB630806]
FX Foundation Item: Item Sponsored by National Basic Research Program of
China (2010CB630806)
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NR 14
TC 34
Z9 44
U1 0
U2 16
PI BEIJING
SN 1006-706X
PD JUL
PY 2011
VL 18
IS 7
BP 8
EP 14
PG 7
GA 820VP
UT WOS:000294934500002
DA 2023-12-05
ER
PT J
AU Wu, FH
Chen, BJ
Qu, GF
Liu, S
Zhao, CY
Ren, YC
Liu, XX
AF Wu, Fenghui
Chen, Bangjin
Qu, Guangfei
Liu, Shan
Zhao, Chenyang
Ren, Yuanchaun
Liu, Xinxin
TI Harmless treatment technology of phosphogypsum: Directional
stabilization of toxic and harmful substances
LA English
DT Article
DE Phosphogypsum; Carbide slag; Solidification; Harmless treatment; High
targeting
ID GYPSUM
AB Phosphogypsum is one of the typical by-products of phosphorus chemical industry.
As a strategic industry related to the national livelihood of China, phosphorus
chemical industry has accumulated and produced a significant amount of
phosphogypsum. In general, phosphogypsum contains approximately 80%-95% calcium
sulfate dihydrate, and less than 5% toxic and harmful elements. In this paper,
toxic and hazardous components in phosphogypsum were efficiently solidified and
stabilized by highly targeted solidification and stabilization technology. Calcium
carbide slag or lime was used as an alkali-base neutralizer of phosphogypsum, and
poly-meric ferric sulfate or polymeric aluminum chloride as a directional
solidification stabilizer to analyze the leaching toxicity of the mixed powder in
1, 3, 5 and 15 days. The experimental results demonstrate excellent solidification
and stabilization effect with the leaching pH of 6-9, the leaching concentration of
P, F and heavy metals of less than 0.5 mg/L, 10 mg/L and 0.1 mg/L, respectively,
which meets the requirements of relevant international standards. Mechanistic
analysis indicates that the solidification and stabilization of toxic and hazardous
substances in phosphogypsum is perfectly achieved owing to the generation,
adsorption and encap-sulation of insoluble substances. This technology can reduce
the costs and difficulty in the phosphogypsum treatment, and has extensive
application potentials.
C1 [Wu, Fenghui; Chen, Bangjin; Qu, Guangfei; Liu, Shan; Zhao, Chenyang; Ren,
Yuanchaun; Liu, Xinxin] Kunming Univ Sci & Technol, Fac Environm Sci & Engn,
Kunming 650500, Yunnan, Peoples R China.
[Wu, Fenghui; Chen, Bangjin; Qu, Guangfei; Liu, Shan; Zhao, Chenyang; Ren,
Yuanchaun; Liu, Xinxin] Natl Reg Engn Res Ctr NCW, Kunming 650500, Yunnan, Peoples
R China.
C3 Kunming University of Science & Technology
RP Qu, GF (corresponding author), Kunming Univ Sci & Technol, Fac Environm Sci &
Engn, Kunming 650500, Yunnan, Peoples R China.
EM qgflab@sina.com
FU National Key Research and Development Plan-Ecological Link Technology
[2018YFC1900203]; National Natural Science Foundation of China-Migration
and transformation of heavy metals in lead and zinc tailings and the
stabilization [51968033]
FX & nbsp;This work is supported by The National Key Research and
Develop-ment Plan-Ecological Link Technology for Clean processing of
Typical by-products of Unconventional Wet/thermal Production
(2018YFC1900203) . The National Natural Science Foundation of
China-Migration and transformation of heavy metals in lead and zinc
tailings and the stabilization (51968033) .
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NR 41
TC 33
Z9 34
U1 37
U2 142
PI LONDON
SN 0301-4797
EI 1095-8630
J9 J ENVIRON MANAGE
PD JUN 1
PY 2022
VL 311
AR 114827
DI 10.1016/j.jenvman.2022.114827
EA MAR 2022
PG 12
GA 0W6YT
UT WOS:000789171300002
PM 35248928
DA 2023-12-05
ER
PT J
AU Perumal, P
Niu, H
Kiventer, J
Kinnunen, P
Illikainen, M
AF Perumal, Priyadharshini
Niu, He
Kiventer, Jenni
Kinnunen, Paivo
Illikainen, Mirja
TI Upcycling of mechanically treated silicate mine tailings as alkali
activated binders
LA English
DT Article
DE Mine tailings; Silicate tailings; Mechanical activation; Milling; Alkali
activation
ID WASTE-ROCK; HYDRATION; PRODUCTS; STRENGTH; KINETICS; SLAG
AB Mining activity is inevitable in human societies, and thus, disposal of mining
waste in a proper and effective way is crucial to preserving our environment. In
this context, studies on the reuse potential for mine tailings in the construction
sector are booming. However, utilizing tailings as binder material is complicated
due to the high variation in mineralogical composition and the low reactivity of
these materials. In this study, an attempt was made to understand the effect of
mechanical treatment on silicate mine tailings in order to improve their properties
for use as a sole precursor in alkali-activated binders. Two different silicate
tailings from Finland were studied: one rich in tremolite, which is high in
magnesium (HM tailings) and one rich in anorthite and epidote, which is high in
aluminum (HA tailings). Interestingly, grinding activity performed at different
durations affected the properties of the tailings with various intensities,
including their mineralogical and physical properties and characteristics and, thus
the reactivity of tailings. Tremolite does not respond to milling for longer
durations, and layered anorthite was easily distorted by the mechanical
disturbance. Irrespective of the type of tailings, the compressive strength of
alkali-activated milled tailings increased with an increase in grinding time from 1
to 16 min. However, the percentage of compressive strength increase varied with the
type of tailings and their mineralogy.
C1 [Perumal, Priyadharshini; Niu, He; Kiventer, Jenni; Kinnunen, Paivo; Illikainen,
Mirja] Univ Oulu, Fac Technol, Fibre & Particle Engn Res Unit, POB 4300, Oulu,
Finland.
RP Perumal, P (corresponding author), Univ Oulu, Fibre & Particle Engn Res Unit,
Inorgan Binders Grp, Pentti Kaiteran Katu 1, Oulu 90014, Finland.
EM priyadharshini.perumal@oulu.fi
RI P, Priyadharshini/P-7995-2018; Niu, He/GNH-3651-2022; Niu,
He/ABS-0624-2022
OI P, Priyadharshini/0000-0002-7731-2016; Niu, He/0000-0001-9424-1937; Niu,
He/0000-0001-9424-1937; Kinnunen, Paivo/0000-0001-8490-1890; Illikainen,
Mirja/0000-0001-7545-4574
FU Academy of Finland [319676, 292526]; European Union's EU Framework
Programme for Research and Innovation Horizon 2020 [812580]; Academy of
Finland (AKA) [319676, 319676, 292526, 292526] Funding Source: Academy
of Finland (AKA)
FX The authors gratefully acknowledge the financial support received from
the project GEOMINS [grant #319676: Steps towards the use of mine
tailings in geopolymer materials: reactivity, CO2 sequestration and
heavy metal stabilization], CERATAIL [grant #292526: Novel synthesis
methods for porous ceramic from mine tailings] funded by Academy of
Finland and European Union's EU Framework Programme for Research and
Innovation Horizon 2020 [Grant Agreement No 812580 ("SULTAN",
https://etn-sultan.eu)].
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NR 38
TC 33
Z9 34
U1 8
U2 34
PI OXFORD
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD NOV 1
PY 2020
VL 158
AR 106587
DI 10.1016/j.mineng.2020.106587
PG 10
GA NR7EH
UT WOS:000571723500001
OA hybrid
DA 2023-12-05
ER
PT J
AU Cui, FH
Mu, WN
Zhai, YC
Guo, XY
AF Cui, Fuhui
Mu, Wenning
Zhai, Yuchun
Guo, Xueyi
TI The selective chlorination of nickel and copper from low-grade
nickel-copper sulfide-oxide ore: Mechanism and kinetics
SO SEPARATION AND PURIFICATION TECHNOLOGY
LA English
DT Article
DE Low-grade nickel-copper ore; Chlorination; Extraction; Thermodynamic
analysis; Kinetics; Anhydrous aluminum chloride
ID OPTIMIZING UG2 FLOTATION; VALUABLE METALS; CONCENTRATE; RECOVERY; TALC;
EXTRACTIONS; PENTLANDITE; DEPRESSION; COBALT; SLAG
AB On account of the complex occurrence of valuable metals in a large amount of
low-grade nickel sulfide ore, obstacles have been caused by using the existing
metallurgical method. Therefore, we are reporting a new selective chlorination
roasting and water leaching process to treat complex nickel sulfide ore. Anhydrous
aluminum chloride was firstly used as the solid chlorination agent to sulfide ore.
The chlorination mechanism for metals in nickel-copper sulfide ore were determined
by thermodynamic calculation and experiment. The thermodynamic analysis showed that
the predominant matter contributing to the chlorination of talc, lizardite, and
magnetite were AlCl3 (both solid or gas) and the generated HCl, however, the
chlorination of metal sulfide (pentlandite, chalcopyrite, and pyrite) were mostly
contributed by the generated Cl-2. The effect of roasting temperature, the roasting
time, the mass ratio of AlCl3 to the ore, the content of O-2 in the roasting
atmosphere and the particle size of ore were investigated. The orthogonal
experiments results showed that the optimal conditions of the chlorination roasting
process were the roasting time of 3 h, the roasting temperature of 450 degrees C,
the mass ratio of AlCl3 to ore of 1.5:1, the content of O-2 of 20%, and particle
size of the ore of 96-80 mu m, under this condition, an extraction rate of nickel,
copper, iron, and magnesium of 91.6%, 88.5%, 28.4%, and 16.4% was obtained. The
chlorination mechanism is that, in the chlorination roasting process, nickel and
copper were transferred into their corresponding metal chlorides, while most of the
iron and magnesium were transferred into ferric oxide and magnesia-alumina
silicates, respectively. TAK (thermal analytic kinetics) were used to clarify the
chlorination kinetics, the results showed that the apparent activation energy
calculated from DSC data was 70.4 kJmol(-1), while calculated from TG data was 86.5
kJmol(-1) (average) by using the FWO method, one of the most probable mechanism
function of the chlorination process was G(alpha) = 0.8701[1 - (1 - alpha)(0.8701)]
(integral form) and f(alpha) = (1 - alpha)(1.8701) (differential form). The
chlorination selectivity for metals could give guidance to the extraction of metals
(especially for valuable metals) either in nickel sulfide ore or other minerals
with a complex metal occurrence.
C1 [Cui, Fuhui; Guo, Xueyi] Cent South Univ, Sch Met & Environm, Changsha 410083,
Peoples R China.
[Cui, Fuhui; Guo, Xueyi] Nonferrous Met Ind China, Cleaner Met Engn Res Ctr,
Changsha 410083, Peoples R China.
[Mu, Wenning; Zhai, Yuchun] Northeastern Univ Qinhuangdao, Sch Resources & Mat,
Qinhuangdao 066004, Hebei, Peoples R China.
C3 Central South University; Northeastern University - China
RP Cui, FH (corresponding author), Cent South Univ, Sch Met & Environm, Changsha
EM fuhuicui@csu.edu.cn
FU National Basic Research Program of China [2014CB643405]; National
FX This research was jointly supported by the National Basic Research
Program of China (Grant 2014CB643405) and National Natural Science
Foundation of China (Grant 51874371).
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NR 48
TC 33
Z9 36
U1 5
U2 73
PU ELSEVIER
PI AMSTERDAM
SN 1383-5866
EI 1873-3794
J9 SEP PURIF TECHNOL
JI Sep. Purif. Technol.
PD MAY 15
PY 2020
VL 239
AR 116577
DI 10.1016/j.seppur.2020.116577
PG 13
SC Engineering
GA KN3NQ
UT WOS:000514748000053
DA 2023-12-05
ER
PT J
AU Li, FH
Liu, QR
Li, M
Fang, YT
AF Li, Fenghai
Liu, Quanrun
Li, Meng
Fang, Yitian
TI Understanding fly-ash formation during fluidized-bed gasification of
high-silicon-aluminum coal based on its characteristics
SO ENERGY
LA English
DT Article
DE High-silicon-aluminum coal; Fluidized-bed gasification; Fly ashes;
Characteristics; Formation
ID LOW-RANK COAL; PULVERIZED COAL; FORMATION MECHANISM; COMBUSTION; SLAG;
BIOMASS; BEHAVIOR; AGGLOMERATION; TEMPERATURE; FUSIBILITY
AB Investigations on fly-ash formation in fluidized-bed gasification are important
in mitigating ash-related problems and exploiting its further usage. In this study,
the characteristics of ash fusion, size distribution, and the elemental composition
of fly ash from the fluidized-bed gasification of high-silicon aluminum coals were
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smaller than that from Lu'an bitumite, they both have a two-peak distribution. The
carbon content and elemental distribution in the two fly ashes vary obviously
because of the differences in maceral distribution and mineral composition of
original coal. For high-silicon-aluminum coal, fly-ash formation occurred through
the char gasification of a shrinking nucleus, the agglomeration of some fine
particles into large particles by sintering and collision, and the entry of char
particles into a cyclone separator that is entrained by syngas. (C) 2018 Elsevier
C1 [Li, Fenghai; Li, Meng] Heze Univ, Dept Chem & Chem Engn, Heze 274015, Shandong,
Peoples R China.
[Li, Fenghai; Liu, Quanrun; Li, Meng] Henan Polytech Univ, Coll Chem & Chem
Engn, Jiaozuo 454003, Henan, Peoples R China.
RP Li, FH (corresponding author), Heze Univ, Dept Chem & Chem Engn, Heze 274015,
Shandong, Peoples R China.; Li, FH; Liu, QR (corresponding author), Henan Polytech
Univ, Coll Chem & Chem Engn, Jiaozuo 454003, Henan, Peoples R China.
EM hzIfh@163.com; quanrunliu@126.com
RI LI, feng/HIR-1703-2022
FU Natural Science Foundation of Shandong Province, China [ZR2014BM014];
National Natural Science Foundation of China [21506242]; Youth Natural
Science Foundation of Shanxi Province, China [Y5SJ1A1121]
Shandong Province, China (ZR2014BM014), the National Natural Science
Foundation of China (21506242), the and Youth Natural Science Foundation
of Shanxi Province, China (Y5SJ1A1121). We are thankful to all workers
in the coal gasification pilot scale center, ICC, CAS.
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Zhao XL, 2010, ENERG FUEL, V24, P91, DOI 10.1021/ef9005065
Zhou CG, 2016, APPL ENERG, V172, P230, DOI 10.1016/j.apenergy.2016.03.106
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NR 52
TC 33
Z9 38
U1 4
U2 64
PI OXFORD
SN 0360-5442
EI 1873-6785
J9 ENERGY
JI Energy
PD MAY 1
PY 2018
VL 150
BP 142
EP 152
DI 10.1016/j.energy.2018.02.137
PG 11
GA GF2DL
UT WOS:000431748400013
DA 2023-12-05
ER
PT J
AU Wang, KT
Lemougna, PN
Tang, Q
Li, W
He, Y
Cui, XM
AF Wang, Kaituo
Lemougna, Patrick N.
Tang, Qing
Li, Wei
He, Yan
Cui, Xuemin
TI Low temperature depolymerization and polycondensation of a slag-based
inorganic polymer
LA English
DT Article
DE Powders: solid state reaction; Impedance; Strength; Silicate; Thermal
applications
ID ALKALI-ACTIVATED MATERIALS; BLAST-FURNACE SLAG; MECHANICAL-PROPERTIES;
AL-27 NMR; FLY-ASH; COMPRESSIVE STRENGTH; TRANSPORT-PROPERTIES;
THERMAL-PROPERTIES; AQUEOUS-SOLUTION; STEEL SLAG
AB In this paper, the depolymerization and polycondensation process, compressive
strength, gel content and conductance of an alkali-activated slag (AAS) (an
inorganic polymer or high-calcium geopolymer) paste cured at low temperature (-25
degrees C similar to 25 degrees C) were studied. The results showed that gel
content of the AAS inorganic polymer sample first increased and then decreased with
the decreasing of the curing temperature for 24 h, reaching a maximum value of 37.8
wt% in the samples cured at 0 degrees C. Chemical structural data are obtained by
nuclear magnetic resonance (NMR) spectroscopy for 6-coordinated (octahedral)
aluminum can be observed at low temperature (< 0 degrees C) and the gel contains
primarily Q(1),(1Al), Q(2)(Al-1) and Q(3) at 0 degrees C. The inductively coupled
plasma emission spectrometry (ICP) analysis of the products showed depolymerization
of a great amount of slag at low temperature. The impedance analysis indicated that
low temperature (< 0 degrees C) will inhibit the polycondensation process but
almost not affect the depolymerization process so as to make a distinction between
the depolymerization and polycondensation process in the AAS inorganic polymer
system.
C1 [Cui, Xuemin] Guangxi Univ, Sch Chem & Chem Engn, Nanning 530004, Peoples R
China.
Guangxi Univ, Guangxi Key Lab Petrochem Resource Proc & Proc In, Nanning 530004,
Peoples R China.
C3 Guangxi University; Guangxi University
RP Cui, XM (corresponding author), Guangxi Univ, Sch Chem & Chem Engn, Nanning
EM cui-xm@tsinghua.edu.cn
OI Lemougna Ninla, Patrick/0000-0003-2233-9745; cui,
xuemin/0000-0003-1818-8470
FU Chinese Natural Science Fund [51262002, 21566006, 51561135012]; Guangxi
Natural Science Fund [2016GXNSFGA380003, 2013GXNSFBA019229]
FX This work was supported by the Chinese Natural Science Fund (grant:
51262002, 21566006 and 51561135012), the Guangxi Natural Science Fund
(grant: 2016GXNSFGA380003 and 2013GXNSFBA019229).
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Wang KT, 2017, GONDWANA RES, V44, P1, DOI 10.1016/j.gr.2016.11.001
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Yan S, 2016, CERAM INT, V42, P7837, DOI 10.1016/j.ceramint.2016.01.197
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10.1016/j.cemconres.2007.11.001
Yue YL, 2014, MATER LETT, V136, P356, DOI 10.1016/j.matlet.2014.08.090
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10.1016/j.conbuildmat.2016.03.102
NR 51
TC 33
Z9 33
U1 2
U2 47
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD AUG 15
PY 2017
VL 43
IS 12
BP 9067
EP 9076
DI 10.1016/j.ceramint.2017.04.052
PG 10
GA EW5ZL
UT WOS:000402584900074
DA 2023-12-05
ER
PT J
AU Hou, D
Jiang, ZH
Dong, YW
Gong, W
Cao, YL
Cao, HB
AF Hou, Dong
Jiang, Zhou-Hua
Dong, Yan-Wu
Gong, Wei
Cao, Yu-Long
Cao, Hai-bo
TI Effect of Slag Composition on the Oxidation Kinetics of Alloying
Elements during Electroslag Remelting of Stainless Steel: Part-1
Mass-transfer Model
LA English
DT Article
DE electroslag remelting; kinetics; mass transfer; penetration theory; ion
and molecule coexistence theory
ID THERMODYNAMIC MODEL; MATHEMATICAL-MODEL; DEOXIDATION; TITANIUM; OXIDE
AB A new mathematical model for the computation of concentration changes occurring
in electroslag remelting is proposed in order to study the oxidation behavior of
titanium, aluminum, silicon in stainless steel. The solutions of the mass transfer
are simultaneously calculated by penetration theory and film theory. In order to
make the each system of Al+Al2O3, Si+SiO2, Ti+TiO2 and Fe+FeO reach the
thermodynamic equilibrium at the slag-metal interface in the model, the molarity of
FeO at the interface C-(FeO)* is employed, and then calculated by mass transfer
balance for oxygen element. The ion and molecule coexistence theory is employed to
investigate the effect of slag composition on the change of each alloying element.
At the process of liquid metal film formation, metal droplet passing though the
molten slag and metal pool, the fluxion of molten slag was considered into the mass
transfer coefficient. Finally, the model was established using the software of
Matlab. In theory, this model is suitable for all the chemical reaction of each
element during the ESR process, and determines the change of concentration of each
component both in metal and slag.
C1 [Hou, Dong; Jiang, Zhou-Hua; Dong, Yan-Wu; Gong, Wei; Cao, Yu-Long; Cao, Hai-bo]
Northeastern Univ, Sch Met, Shenyang 110819, Liaoning, Peoples R China.
RP Jiang, ZH (corresponding author), Northeastern Univ, Sch Met, Shenyang 110819,
OI Jiang, Zhouhua/0000-0001-8887-7250
FU National Nature Science Foundation of China [U1560203, 51274266];
Baosteel Group Corporation [U1560203]
FX This project is supported by Joint Research Fund of National Nature
Science Foundation of China and Baosteel Group Corporation with the
grant No. U1560203, and it is also supported by the National Nature
Science Foundation of China with the grant No. 51274266.
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147
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NR 29
TC 33
Z9 35
U1 1
U2 14
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 8
BP 1400
EP 1409
PG 10
GA FE7RF
UT WOS:000408403900014
OA gold
DA 2023-12-05
ER
PT J
AU Ji, CX
Cui, Y
Zeng, Z
Tian, ZH
Zhao, CL
Zhu, GS
AF Ji, Chen-xi
Cui, Yang
Zeng, Zhi
Tian, Zhi-hong
Zhao, Chang-liang
Zhu, Guo-sen
TI Continuous Casting of High-Al Steel in Shougang Jingtang Steel Works
LA English
DT Article
DE high aluminum steel; continuous casting; mold powder; slag-metal
reaction
AB Reaction between mold flux and liquid high aluminum steel is considerably
strong:It changes the physical property of the mold powder greatly and leads to a
larger fluctuation of heat flux in the mold. Transverse depression and longitudinal
cracks were often found on the slab surface. Three casting trials were carried out
to investigate the effects of mold powder and slab width on castability and surface
quality of high aluminum steels. The result shows that the SiO2 content of liquid
mold powder decreases while Al2O3 content increases during the casting process. It
was found that the degree of slag-metal reaction, addition and consumption of mold
powder determined the final equilibrium content of SiO2 and Al2O3. Under the same
process condition, it takes more time for the mold powder content to reach
equilibrium when casting wide slabs than narrow ones. Considering the sticking and
slab surface quality, mold powder A with high melting point and high viscosity is
suitable for casting 1 200 mm-width slab and mold powder B with low melting point
and low viscosity is suitable for casting 1 900 mm-width one.
C1 [Ji, Chen-xi; Cui, Yang; Zeng, Zhi; Tian, Zhi-hong] Shougang Res Inst Technol,
[Zhao, Chang-liang; Zhu, Guo-sen] Shougang Jingtang United Iron & Steel Co Ltd,
Tangshan 063200, Hebei, Peoples R China.
C3 Shougang Group; Shougang Group
RP Ji, CX (corresponding author), Shougang Res Inst Technol, Beijing 100043,
Peoples R China.
EM jichenxi@gmail.com
CR Becker J. J., 2005, P AISTECH 2005, P99
Gui-rong L., 2007, J CHONGQING U, V14, P25
Hiromoto T., 1979, 62 STEELM C P DETR P, P40
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[王欢 WANG Huan], 2011, [北京科技大学学报, Journal of University Science and
Wang Q., 2012, BASIC APPL RES NEW A
Wang Q., 2012, STEELMAKING, V28, P74
Wang Q., 2004, SPECIAL STEEL, V25, P1
Wang Q., 1991, STEELMAKING, P22
8620.2013.01.013, DOI 10.3969/J.ISSN.1003-8620.2013.01.013]
Yang Bo, 2011, Chinese Journal of Nonferrous Metals, V21, P913
Yu X., 2011, BASIC STUDY MOULD PO
NR 14
TC 33
Z9 34
U1 2
U2 14
PU SPRINGER
PI NEW YORK
SN 1006-706X
EI 2210-3988
PD NOV
PY 2015
VL 22
SU 1
BP 53
EP 56
DI 10.1016/S1006-706X(15)30138-2
PG 4
GA CZ2QJ
UT WOS:000366949400009
DA 2023-12-05
ER
PT J
AU Andersson, MAT
Jönsson, PG
Hallberg, M
AF Andersson, MAT
Jönsson, PG
Hallberg, M
TI Optimisation of ladle slag composition by application of sulphide
capacity model
LA English
DT Article
ID BEARING-STEEL PRODUCTION; SULFIDE CAPACITIES
AB The sulphur distribution ratio for ladle slags at Ovako Steel AB has been
determined by calculating the sulphide capacity using the Royal Institute of
Technology (KTH) model and the alumina activity via an empirical expression
suggested by Ohta and Suite, and by using the well established theories for sulphur
refining. A parameter study was carried out based on plant data from a previous
study on desulphurisation, The effect of carbon and aluminium in the steel, the
temperature of the steel, and alumina and lime in the slag on the sulphur
distribution ratio was investigated, it was shown that the Al2O3/CaO ratio had the
largest influence on the conditions studied, and that when it increased the sulphur
distribution ratio decreased. Based on these results, new plant trials were carried
out, in which the alumina content in the slag was changed. The calculated sulphur
distribution ratios for these trials were found to be in good agreement with
experimentally determined sulphur distribution ratios. It is concluded that the
present approach can be used to optimise multicomponent ladle slags with respect to
sulphur refining. I&S/1493.
C1 Royal Inst Technol, Dept Met, S-10044 Stockholm, Sweden.
Ovako Steel AB, S-81382 Hofors, Sweden.
RP Andersson, MAT (corresponding author), Royal Inst Technol, Dept Met, S-10044
Stockholm, Sweden.
ENGH TA, 1992, PRINCIPLES METAL REF, P62
GORNERUP M, 1997, 53 TRITA TPM DEP MET
Hayes P, 1993, PROCESS PRINCIPLES M, P633
Huet L, 1997, STEEL INT, V21, P47
JONSSON PG, 1997, P C CLEAN STEEL 5 BA, P218
LUND TB, 1996, P 5 INT S BEAR STEEL, P124
NILSSON R, 1995, P SCAN 7 MEF LUL SWE, P149
Reinholdsson F, 1997, ISIJ INT, V37, P637, DOI 10.2355/isijinternational.37.637
RICHARDSON FD, 1974, PHYSICAL CHEM MELTS, P291
Sjodin P, 1997, SCAND J METALL, V26, P41
TEMKIN M, 1945, ACTA PHYSICOCHIM URS, V20, P411
NR 17
TC 33
Z9 36
U1 1
U2 9
PU I O M COMMUNICATIONS LTD INST MATERIALS
PI LONDON
PA 1 CARLTON HOUSE TERRACE, LONDON SW1Y 5DB, ENGLAND
SN 0301-9233
J9 IRONMAK STEELMAK
PY 2000
VL 27
IS 4
BP 286
EP 293
DI 10.1179/030192300677570
PG 8
GA 392RA
UT WOS:000166424400003
DA 2023-12-05
ER
PT J
AU THEISEN, J
MAULSHAGEN, A
FUCHS, J
AF THEISEN, J
MAULSHAGEN, A
FUCHS, J
TI ORGANIC AND INORGANIC SUBSTANCES IN THE COPPER SLAG KIESELROT
SO CHEMOSPHERE
LA English
DT Article
DE KIESELROT; DIOXIN; HOMOLOG DISTRIBUTION; CONGENER DISTRIBUTION;
SCREENING METHOD; BACKGROUND CONCENTRATIONS IN SOIL; PCDF/D MASS
FRAGMENTOGRAMS; TE-CORRELATIONS
AB In the slag ''Kieselrot'' highly chlorinated, aromatic compounds have been
detected as main organic components. Thus pure ''Kieselrot'' contains
1,2,3,4,6,7,8-hepta- and octachlorodibenzofuran, 2,2',3,3',4,4',5,5',6-nona- and
decachlorobiphenyl, penta- and hexachlorobenzene, pentachlorophenol as well as
hexa- and heptachloronaphthalene in low ppm concentrations. Additionally
concentrations of higher than 100 ppm for aluminum, lead, copper and manganese are
usually found in this material.
The concentrations of polychlorinated dibenzofurans and polychlorinated
dibenzodioxins found in pure ''Kieselrot'' are much higher than the limit values
specified in the German ''Gefahrstoffverordnung'' (Regulations for Dangerous
Substances) and ''Gefahrgutverordnung'' (Regulations for Road Transport of
Dangerous Goods). The concentrations of arsenic found in this material exceeds
value II of the decree ''Metalle auf Kinderspielplatzen'' (Metals in Childrens'
Playgrounds) of Northrhine-Westphalia (NRW). For areas covered with ''Kieselrot'',
all TE (Toxicity Equivalent)-values which are currently recommended by the German
Federal Health Office/Federal Environment Office (BGA/UBA) are exceeded.
The identification of ''Kieselrot'' is possible on the basis of certain
parameters from so-called ''screening methods''. The best correlation with the TE-
value of relatively pure ''Kieselrot'' was found for decachlorobiphenyl, which is
used as test parameter in the NRW-screening test. From the concentration of
octachlorodibenzofuran determined at the same time by this method, the PCDF/D
homologues and congener concentrations can be calculated relatively accurately,
based on the fact, that about the same profile is observed for the PCDF/D in the
slag ''Kieselrot''.
RP THEISEN, J (corresponding author), GESELL ARBEITSPLATZ & UMWELTANALYT MBH,OTTO
HAHN STR 22,W-4400 MUNSTER,GERMANY.
CR GERSCHLER LJ, 1991, EMPFEHLUNG SCHNELTES
1991, BUNDESGESETZBLATT, V1, pS1218
1990, 69 RD ERL D NRW MIN
1990, BUNDESGESETZBLATT, V1, pS1326
1991, MEITEILUNG NRW MINIS
NR 5
TC 33
Z9 33
U1 0
U2 2
PI OXFORD
SN 0045-6535
J9 CHEMOSPHERE
JI Chemosphere
PD MAR
PY 1993
VL 26
IS 5
BP 881
EP 896
DI 10.1016/0045-6535(93)90363-A
PG 16
GA KT488
UT WOS:A1993KT48800006
DA 2023-12-05
ER
PT J
AU Wang, HJ
Feng, YL
Li, HL
Li, HR
Wu, H
AF Wang, Hongjun
Feng, Yali
Li, Hailong
Li, Haoran
Wu, Hao
TI Recovery of vanadium from acid leaching solutions of spent oil
hydrotreating catalyst using solvent extraction with D2EHPA (P204)
SO HYDROMETALLURGY
LA English
DT Article
DE Solvent extraction; Di (2-ethylhexyl) phosphoric acid (P204); Vanadium;
Spent oil hydrotreating catalyst; Thermodynamics
ID SEPARATION; MOLYBDENUM; MEDIA; THERMODYNAMICS; TITANIUM; MIXTURE;
METALS; NICKEL; WASTE; SLAG
AB In this paper, a process of selective extraction and separation of vanadium (IV)
from acid leaching solution of spent oil hydrotreating catalyst by a solvent
extraction method with P204 as an extractant was proposed. Because the leaching
solution contained a large amount of elements such as nickel, aluminium and iron,
the effects of various conditions on the separation of vanadium from nickel,
aluminium and iron were investigated and the optimum conditions were determined. At
the same time, the thermodynamic discussion on the extraction process of vanadium
in the system was carried out. Using kerosene as a diluent and 20% (v/v) P204 as an
extractant, the single-stage maximum extraction ratio of 93.47% for vanadium was
obtained under the optimum extraction conditions of O/A ratio of 2, oscillation
time of 8 min, extraction temperature of 298 k(25 degrees C) and pH value of
initial aqueous phase of 2. After three stages of countercurrent extraction
experiments, the concentration of vanadium, iron, nickel and aluminium in the
loaded organic phase were 0.377, 0.001, 0.005 and 0.02 g/L, respectively, and their
extraction ratios were determined to be 99.21%, 1.02%, 2.857% and 1.942%,
respectively, realizing the selective extraction and separation of vanadium. With 2
mol/L of sulfuric acid as a stripping reagent, the complete removal of vanadium
from the loaded organic phase could be achieved at O/A ratio of 2 by three stages
of countercurrent experiments of vanadium removal. The thermodynamic calculation
showed that the enthalpy change of the vanadium extraction in the system was -20.37
kJ.mol(-1). This demonstrated that the extraction of vanadium from acid leaching
solution of spent oil hydrotreating catalyst with P204 as the extractant was an
exothermic reaction.
C1 [Wang, Hongjun; Feng, Yali; Li, Hailong; Wu, Hao] Univ Sci & Technol Beijing,
Civil & Resource Engn Sch, Beijing 100083, Peoples R China.
[Li, Haoran] Chinese Acad Sci, Inst Proc Engn, State Key Lab Biochem Engn,
C3 University of Science & Technology Beijing; Chinese Academy of Sciences;
Institute of Process Engineering, CAS
RP Wang, HJ; Feng, YL (corresponding author), Univ Sci & Technol Beijing, Civil &
Resource Engn Sch, Beijing 100083, Peoples R China.
EM hongjunwang0707@163.com; ylfeng126@126.com
RI Li, Hao/GPS-9834-2022; li, chunyuan/IQW-1618-2023; Li, Li/IAQ-0885-2023;
Wu, Hao/AAS-9969-2021; Wang, Xin/HZL-4695-2023; Wang,
Xinhua/ISR-8520-2023; wei, li/ISB-3361-2023; wei, li/GSD-3630-2022
OI Wu, Hao/0000-0001-7273-3578;
FU China Ocean Mineral Resource RD Association [DY135-B2-15]; Major science
and technology program for water pollution control and treatment
[2015ZX07205-003]; National Natural Science Foundation of China
[21176242, 21176026]
FX This research was supported by China Ocean Mineral Resource R&D
Association under Grant No. DY135-B2-15, Major science and technology
program for water pollution control and treatment under Grant No.
2015ZX07205-003, the National Natural Science Foundation of China under
Grant No. 21176242 and No. 21176026.
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NR 36
TC 32
Z9 35
U1 10
U2 58
PU ELSEVIER
PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD AUG
PY 2020
VL 195
AR 105404
DI 10.1016/j.hydromet.2020.105404
PG 7
GA MK9YS
UT WOS:000549135400038
DA 2023-12-05
ER
PT J
AU Liu, TZ
Li, FL
Jin, ZS
Yang, YG
AF Liu, Taoze
Li, Feili
Jin, Zhisheng
Yang, Yuangen
TI Acidic leaching of potentially toxic metals cadmium, cobalt, chromium,
copper, nickel, lead, and zinc from two Zn smelting slag materials
incubated in an acidic soil
SO ENVIRONMENTAL POLLUTION
LA English
DT Article
DE Soil amendment; Simulated acid deposition; Leaching index; Chemical
species; Mineral saturation
ID SEQUENTIAL EXTRACTION PROCEDURE; HEAVY-METAL; CONTAMINATED SOIL;
ORGANIC-MATTER; TRACE-ELEMENTS; CU; PB; BIOAVAILABILITY; ADSORPTION;
MOBILITY
AB A column leaching study, coupled with acid deposition simulation, was conducted
to investigate the leaching of potentially toxic metals (PTM) from zinc smelting
slag materials (SSM) after being incubated in an acid Alfisol for 120 days at room
temperature. Two SSMs (SSM-A: acidic, 10 yrs exposure with moderate high PTM
concentrations versus SSM-B: alkaline, 2 yrs exposure with extremely high PTM
concentrations), were used for the incubation at 0.5, 1, 2.5, 5 wt% amendment
ratios in triplicate. Five leaching events were conducted at day 1, 3, 7,14, and
28, and the leaching of PTMs mainly occurred in the first three leaching events,
with the highest PTM concentrations in leachate measured from 5 wt% SSM amendments.
After leaching, 2.5, 12, 5.5, 14, 11, and 9 wt% of M3 extractable Pb, Zn, Cd, Co,
Cr, and Ni could be released from 5 wt% SSM-A amended soils, being respectively 25,
12, 4, 2, 2, and 2 times more than those from 5 wt% SSM-B amended soils. In the
leachates, the concentrations of PTMs were mostly affected by leachant pH and were
closely correlated to the concentrations of Fe, Al, Ca, Mg and P with Cd, Pb, and
Zn showing the most environmental concern. Visual MINTEQ 3.1 modeling suggested
metallic ions and sulfate forms as the common chemical species of PTMs in the
leachates; whereas, organic bound species showed importance for Cd, Pb, Cu, and Ni,
and CdCl+ was observed for Cd. Aluminum hydroxy, phosphate, and sulfate minerals
prevailed as the saturated minerals, followed by chloropyromorphite (Pb-5(PO4)
(3)Cl) and plumbogummite (PbAl3(PO4)(2)(OH)(5)center dot H2O) in the leachates.
This study suggested that incubation of SSMs in acidic soil for a long term can
enhance the release of PTMs as the forms of metallic ions and sulfate when
subjected to acid deposition leaching. (C) 2018 Elsevier Ltd. All rights reserved.
C1 [Liu, Taoze; Jin, Zhisheng] Chinese Acad Sci, Inst Geochem, 99 West Lincheng Rd,
Guiyang 550002, Guizhou, Peoples R China.
[Li, Feili] Zhejiang Univ Technol, Coll Environm, 18 Chaowang Rd, Hangzhou
310032, Zhejiang, Peoples R China.
[Yang, Yuangen] Univ Georgia, AESL, 2300 Coll Stn Rd, Athens, GA 30602 USA.
C3 Chinese Academy of Sciences; Guiyang Institute of Geochemistry, CAS;
Zhejiang University of Technology; University System of Georgia;
University of Georgia
RP Yang, YG (corresponding author), Univ Georgia, AESL, 2300 Coll Stn Rd, Athens,
GA 30602 USA.
EM yangyuangen@hotmail.com
RI fei-li, Li/A-1550-2012
OI fei-li, Li/0000-0003-0903-9481
FU National Science Foundation of China [40473049, 41273129]; Open Fund of
the State Key Laboratory of Environmental Geochemistry [SKLEG2017901]
FX Funding support from National Science Foundation of China (Grant Nos.
40473049 and 41273129) and Open Fund of the State Key Laboratory of
Environmental Geochemistry (SKLEG2017901) is acknowledged.
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NR 64
TC 32
Z9 33
U1 4
U2 116
PU ELSEVIER SCI LTD
PI OXFORD
SN 0269-7491
EI 1873-6424
J9 ENVIRON POLLUT
JI Environ. Pollut.
PD JUL
PY 2018
VL 238
BP 359
EP 368
DI 10.1016/j.envpol.2018.03.022
PG 10
GA GI8EM
UT WOS:000434754600038
PM 29574360
OA Bronze
DA 2023-12-05
ER
PT J
AU Saravanakumar, R
Ramachandran, K
Laly, LG
Ananthapadmanabhan, PV
Yugeswaran, S
AF Saravanakumar, R.
Ramachandran, K.
Laly, Lintu G.
Ananthapadmanabhan, P. V.
Yugeswaran, S.
TI Plasma assisted synthesis of γ-alumina from waste aluminium dross
SO WASTE MANAGEMENT
LA English
DT Article
DE Aluminium dross; Ultrafine alumina powder; Transferred arc plasma;
Plasma waste treatment; gamma-alumina
ID THERMAL PLASMA; RECOVERING ALUMINUM; ACID DISSOLUTION; HAZARDOUS-WASTE;
ROTARY FURNACE; HOLLOW-CATHODE; ARC; HYDROLYSIS; EXTRACTION; MANAGEMENT
AB Aluminium dross, a waste generated from aluminium melting process, contains
aluminium metal, aluminium oxide, aluminium oxy-nitride and impurities such as
sodium chloride and potassium chloride. Since aluminium dross is land filled
without treatment, it is hazardous to the environment. Conventional methods for the
metal recovery from the recycling of aluminium dross involve chemicals and are time
consuming. In this study, an attempt was made to treat aluminium dross using plasma
arc melting process. The aluminium dross was melted and evaporated by the plasma
arc established between a crucible anode and a rod type hollow cathode made of
graphite. Raw dross and products of plasma treated dross such as slag and fine
powder were characterized. The generation of ultrafine alumina powder and slag are
explained using simulation of the plasma arc inside the crucible and free energy
minimization calculations. High temperature and air entrainment into the plasma
inside the crucible converted the dross into alumina slag and fine powder. The
amount of fine alumina powder produced increased substantially with plasma power
initially as seen from the results of alumina obtained at 5 kW and 10 kW. However,
further increase in plasma power resulted only in marginal increase in the
conversion of Al dross to alumina. Results of this study indicate that arc plasma
technology can be effectively applied to convert Al dross into value added fine
alumina powder. (C) 2018 Elsevier Ltd. All rights reserved.
C1 [Saravanakumar, R.; Ramachandran, K.; Laly, Lintu G.] Bharathiar Univ, Dept
Phys, Coimbatore, TN, India.
[Ananthapadmanabhan, P. V.] PSN Coll Engn & Technol, Tirunelveli, TN, India.
[Yugeswaran, S.] Univ Toronto, Ctr Adv Coating Technol, Toronto, ON M5S 3G8,
Canada.
C3 Bharathiar University; University of Toronto
RP Ramachandran, K (corresponding author), Bharathiar Univ, Dept Phys, Coimbatore,
TN, India.
EM ramspsg@yahoo.com
RI Ramachandran, Kandasamy/AAE-3982-2020
OI Ramachandran, Kandasamy/0000-0001-7844-7353; /0000-0002-5165-8094
FU UGC; DST, Government of India
FX Financial supports from UGC and DST, Government of India are greatly
acknowledged.
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TC 32
Z9 34
U1 4
U2 48
PI OXFORD
SN 0956-053X
J9 WASTE MANAGE
JI Waste Manage.
PD JUL
PY 2018
VL 77
BP 565
EP 575
DI 10.1016/j.wasman.2018.05.005
PG 11
GA GO8YR
UT WOS:000440389600058
PM 29778404
DA 2023-12-05
ER
PT J
AU Galindo, R
López-Delgado, A
Padilla, I
Yates, M
AF Galindo, R.
Lopez-Delgado, A.
Padilla, I.
Yates, M.
TI Hydrotalcite-like compounds: A way to recover a hazardous waste in the
aluminium tertiary industry
LA English
DT Article
DE Hydrotalcite; Layered double hydroxide (LDH); Non-conventional aluminium
source; Hazardous waste
ID LAYERED DOUBLE HYDROXIDE; THERMAL-DECOMPOSITION; NANOPARTICLES;
MECHANISM; CATALYST; RESIDUE; POWDER
AB Magnesium-aluminium hydrotalcite-like compounds at ratios of 2:1, 3:1 and 4:1
were prepared using a non-conventional aluminium source, the hazardous wastes from
the aluminium tertiary industry. The method consisted in a conventional
coprecipitation at constant pH 10 with magnesium chloride hexahydrate and stable
solutions of Al3+ from dispersions of the fine powder from the sleeve filter
suction system in the aluminium slag milling process. The characterisation of the
resulting materials indicated that hydrotalcites were strongly dependent on the
presence of iron in the layers, as well as the carbonate and chloride content in
the interlayer which affected the final properties. XRD and SAED indicated low
crystallinity for these materials. Furthermore, as can be seen by SEM, the
formation of disordered tiny nuclei was significant causing small spherical
agglomerates. The infrared spectra showed a change of symmetry in the interlayer
for the different ratios and the textural data suggested the "ink-bottle shaped"
mesopores and type IIb isotherms, similar to the results obtained for pillared
clays, and the transition to H2 type in the hysteresis loops as a function of the
higher ratio. (C) 2014 Elsevier B.V. All rights reserved.
C1 [Galindo, R.; Lopez-Delgado, A.; Padilla, I.] CSIC, Natl Ctr Met Res, Madrid
28040, Spain.
[Yates, M.] CSIC, Inst Catalysis & Petrochem, E-28049 Madrid, Spain.
C3 Consejo Superior de Investigaciones Cientificas (CSIC); Consejo Superior
de Investigaciones Cientificas (CSIC); CSIC - Instituto de Catalisis y
Petroleoquimica (ICP)
RP López-Delgado, A (corresponding author), CSIC, Natl Ctr Met Res, Avda Gregorio
del Amo 8, Madrid 28040, Spain.
EM alopezdelgado@cenim.csic.es
RI Lopez-Delgado, Aurora/D-3785-2012; Padilla, Isabel/AAI-8479-2021;
Padilla, Isabel/I-2712-2015; Yates, Malcolm/H-5152-2015; GALINDO
LLORACH, ROBERTO/M-4224-2015
OI Lopez-Delgado, Aurora/0000-0002-0121-9501; Padilla,
Isabel/0000-0001-7684-200X; Yates, Malcolm/0000-0001-5128-1218; GALINDO
LLORACH, ROBERTO/0000-0002-4242-0981
FU CSIC [P.I.E. 201260E115]
FX Authors thank the company Metalquex, S.L. (Zaragoza, Spain) for
supplying wastes, and the CSIC for the financial support (P.I.E.
201260E115). We also gratefully acknowledge the assistance provided by
Dr. Blanca Casal and Dr. Juan Carlos Galvan.
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NR 32
TC 32
Z9 35
U1 1
U2 42
PI AMSTERDAM
SN 0169-1317
EI 1872-9053
J9 APPL CLAY SCI
JI Appl. Clay Sci.
PD JUN
PY 2014
VL 95
BP 41
EP 49
DI 10.1016/j.clay.2014.03.022
PG 9
GA AK7MK
UT WOS:000338612200007
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Mukhopadhyay, S
Dutta, S
Ansar, SA
Das, S
Misra, S
AF Mukhopadhyay, Sunanda
Dutta, Sarbasree
Ansar, Sheikh A.
Das, Sumita
Misra, Susmita
TI Spinel-Coated Graphite for Carbon Containing Refractory Castables
LA English
DT Article
ID OXIDATION RESISTANCE; MGAL2O4 SPINEL; WATER-WETTABILITY; ALUMINUM;
POWDER; IMPROVEMENT
AB Oxidation resistance and water wettability of graphite flakes have been improved
by a thin sol-gel film of magnesium aluminate spinel (MgAl2O4) over its surface.
The hydrosol has been synthesized by less expensive precursors and the spinel
formation has been studied by scanning electron microscopy (SEM), supplemented with
energy dispersive spectral analysis. After an easy-to-use mixing procedure, drying
(110 degrees C), and subsequent calcination (550 degrees C), coated graphites were
sieved to below 75 mu m. The coating over the powder contained 1.5 wt% MgAl2O4,
which enormously increased the oxidation resistance (performed at 600 degrees, 900
degrees, and 1200 degrees C) and water wettability, as revealed by hydrophilic
functional groups from infrared spectra. Defective, intermediate spinel structure
of fine, lamellar Mg-doped gamma-Al2O3 has been considered to be significant for
this improvement. An approximate (1:2) stoichiometry of (Mg:Al) in the coating
composition was confirmed by an X-ray photoelectron spectroscopy test. Castables
prepared by this graphite remarkably improved their bulk density and apparent
porosity compared with those prepared by the as-received graphite. Casting water
was reduced along with the amount of antioxidants. This also enhanced the
resistance toward the basic slag by retaining the graphite in the refractory.
C1 [Mukhopadhyay, Sunanda; Dutta, Sarbasree; Ansar, Sheikh A.; Das, Sumita; Misra,
Susmita] Univ Calcutta, Dept Chem Technol, Kolkata 700009, W Bengal, India.
C3 University of Calcutta
RP Mukhopadhyay, S (corresponding author), Univ Calcutta, Dept Chem Technol,
Kolkata 700009, W Bengal, India.
EM msunanda_cct@yahoo.co.in
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NR 38
TC 32
Z9 34
U1 1
U2 24
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD AUG
PY 2009
VL 92
IS 8
BP 1895
EP 1900
DI 10.1111/j.1551-2916.2009.03133.x
PG 6
GA 480AS
UT WOS:000268704600045
DA 2023-12-05
ER
PT J
AU SINKKONEN, S
VATTULAINEN, A
AITTOLA, JP
PAASIVIRTA, J
TARHANEN, J
LAHTIPERA, M
AF SINKKONEN, S
VATTULAINEN, A
AITTOLA, JP
PAASIVIRTA, J
TARHANEN, J
LAHTIPERA, M
TI METAL RECLAMATION PRODUCES SULFUR ANALOGS OF TOXIC DIOXINS AND FURANS
SO CHEMOSPHERE
LA English
DT Article
ID MASS-SPECTROMETRY; SUBSTITUTED DIBENZOTHIOPHENES; STRUCTURE ELUCIDATION;
H-1-NMR SPECTROSCOPY; SULFUR ANALOGS; CHROMATOGRAPHY;
POLYCHLORODIBENZOTHIOPHENES; COMBUSTION; SAMPLES; PLANT
AB Polychlorinated dibenzothiophenes (PCDBTs), polychlorinated thianthrenes (PCTAs)
and polychlorinated diphenylsulphides (PCDPSs) which are sulphur analogues for
polychlorinated dibenzofurans (PCDFs), polychlorinated dibenzo-p-dioxins (PCDDs)
and polychlorinated diphenyl ethers (PCDEs), were analyzed by HRGC/HRMS in
different samples from a metal reclamation plant. The samples were gas phase
samples from an aluminium smelter and a car shredder and ash and slag from
processes where different temperatures (300-850-degrees-C) were used. Tri-, tetra-
and pentaCDBTs were most abundant sulphur chloroaromatics at amounts comparable to
PCDDs and PCDFs in emissions and wastes. Small amounts of tri- and tetraCTAs were
identified in car shredder samples. Occurence of PCDPSs remained uncertain due to
interferences even in GC/HRMS analyses.
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NR 19
TC 32
Z9 33
U1 0
U2 19
PI OXFORD
SN 0045-6535
J9 CHEMOSPHERE
JI Chemosphere
PD APR
PY 1994
VL 28
IS 7
BP 1279
EP 1288
DI 10.1016/0045-6535(94)90072-8
PG 10
GA NP179
UT WOS:A1994NP17900003
DA 2023-12-05
ER
PT J
AU Aydin, S
Baradan, B
AF Aydin, Serdar
Baradan, Bulent
TI Sulfate resistance of alkali-activated slag and Portland cement based
reactive powder concrete
LA English
DT Article
DE Reactive powder concrete; Alkali-activated cement; Sulfate attack;
Toughness; Microstructure
ID HIGH-STRENGTH CONCRETE; SILICA FUME; ATTACK; DURABILITY
AB This paper investigates the sulfate resistance of conventional Portland cement-
based and alkali-activated slagbased reactive powder concretes (CRPC and ARPC).
CRPC and ARPC mixtures were subjected to 10% sodium sulfate and magnesium sulfate
solutions for 6 months. The influence of sulfate exposure was assessed by
monitoring the expansions, mechanical and microstructural properties of RPC
mixtures during the exposure time. Both RPC mixtures showed superior sodium sulfate
resistance with very low mechanical strength losses and expansions. Magnesium
sulfate was found more detrimental for both mixtures as compared to sodium sulfate.
ARPC performed better than CRPC in magnesium sulfate solution in terms of strength
and toughness losses, and visual deterioration. The superior performance of ARPC
against sulfate attacks may be attributed to the absence of Ca(OH)(2) and the
substitution of aluminum to C-S-H structure.
C1 [Aydin, Serdar; Baradan, Bulent] Dokuz Eylul Univ, Dept Civil Engn, TR-35390
Izmir, Turkey.
C3 Dokuz Eylul University
RP Aydin, S (corresponding author), Dokuz Eylul Univ, Dept Civil Engn, TR-35390
Izmir, Turkey.
EM serdar.aydin@deu.edu.tr
RI aydın, serdar/AAA-2821-2022
FU Scientific Research Council of Dokuz Eylul University [2009.KB.FEN009]
FX The project presented in this article is supported by the Scientific
Research Council of Dokuz Eylul University (2009.KB.FEN009) . The
authors gratefully acknowledge for the financial support.
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NR 45
TC 31
Z9 31
U1 9
U2 29
PU ELSEVIER
PI AMSTERDAM
EI 2352-7102
J9 J BUILD ENG
JI J. Build. Eng.
PD NOV
PY 2021
VL 43
AR 103205
DI 10.1016/j.jobe.2021.103205
EA SEP 2021
PG 10
GA UW3AT
UT WOS:000700033900006
DA 2023-12-05
ER
PT J
AU Kumar, SS
Kumar, A
Singh, S
Malyan, SK
Baram, S
Sharma, J
Singh, R
Pugazhendhi, A
AF Kumar, Smita S.
Kumar, Amit
Singh, Swati
Malyan, Sandeep K.
Baram, Shahar
Sharma, Jyoti
Singh, Rajesh
Pugazhendhi, Arivalagan
TI Industrial wastes: Fly ash, steel slag and phosphogypsum- potential
candidates to mitigate greenhouse gas emissions from paddy fields
SO CHEMOSPHERE
LA English
DT Review
DE Rice; Methane; Nitrous oxide; Steel slag; Phosphogypsum; Fly ash
ID SOIL MICROBIAL COMMUNITIES; METHANE EMISSION; RICE; IRON; AMENDMENT;
IMPACT; CARBON; YIELD; WATER; CO2
AB Waste management and global warming are the two challenging issues of the
present global scenario. Increased human population has set the platform for rapid
industrialization and modern agriculture. The industries such as energy, steel, and
fertilizers play a significant role in improving the social, and economic status of
human beings. The industrial production of energy (that involves combustion of
coal), production of steel items and diammonium ammonium fertilizer generate a huge
amount of wastes such as fly ash (FA), steel slag (SS) and phosphogypsum (PG),
respectively. Inappropriate dumping of any kind of waste poses a threat to the
environment, therefore, scientific management of waste is required to reduce
associated environmental risks. These wastes i.e. SS, FA, and PG being rich sources
of oxides of calcium (CaO), silicon (SiO2), iron (FeO), and aluminum (Al2O3), etc.
may affect the release of greenhouse gases from the soil. The information
associated with the application of FA, SS, and PG onto the paddy fields and their
impacts on methane and nitrous oxide emissions are highly fragmented and scarce.
The present review extensively and critically explores the available information
with respect to the effective utilization of FA, SS, and PG in paddy cultivation,
their potential to mitigate greenhouse gases emission and their associated
mechanisms. The fine grid assessment of these waste management provides new insight
into the next level research and future policy options for industries and farmers.
C1 [Kumar, Smita S.; Sharma, Jyoti] Indian Inst Technol Delhi, Ctr Rural Dev &
Technol, New Delhi 110016, India.
[Kumar, Amit] Dayalbagh Educ Inst Deemed Univ, Dayalbagh Educ Inst, Dept Bot,
Agra 282005, Uttar Pradesh, India.
[Singh, Swati] Chaudhary Charan Singh Univ, Dept Environm Sci, Meerut 250001,
Uttar Pradesh, India.
[Malyan, Sandeep K.; Baram, Shahar] Agr Res Org, Volcani Ctr, Inst Soil Water &
Environm Sci, IL-7505101 Rishon Leziyyon, Israel.
[Singh, Rajesh] Natl Inst Hydrol, Environm Hydrol Div, Roorkee 247667,
Uttarakhand, India.
[Pugazhendhi, Arivalagan] Ton Duc Thang Univ, Fac Environm & Labour Safety,
Innovat Green Prod Synth & Renewable Environm Dev, Ho Chi Minh City, Vietnam.
Technology (IIT) - Delhi; Dayalbagh Educational Institute (DEI);
Chaudhary Charan Singh University; VOLCANI INSTITUTE OF AGRICULTURAL
RESEARCH; Ton Duc Thang University
RP Pugazhendhi, A (corresponding author), Ton Duc Thang Univ, Fac Environm & Labour
Safety, Innovat Green Prod Synth & Renewable Environm Dev, Ho Chi Minh City,
Vietnam.
EM arivalagan.pugazhendhi@tdtu.edu.vn
RI Kumar, Smita S/O-4532-2019; Sharma, Jyoti/GQA-5895-2022; Malyan, Sandeep
K/AAJ-6514-2020; Pugazhendhi, Arivalagan/F-5411-2018; Kumar,
Amit/ABC-8065-2020
OI Kumar, Smita S/0000-0002-9294-7634; Malyan, Sandeep
K/0000-0003-1759-8902; Pugazhendhi, Arivalagan/0000-0002-9529-3306;
Kumar, Amit/0000-0003-1956-0174; Singh, Rajesh/0000-0002-0631-1593
FU Science & Engineering Research Board (SERB) [PDF/2017/002783]
FX We are thankful to the Science & Engineering Research Board (SERB) for
awarding National Post-doctoral Fellowship (NPDF) to Dr. Smita vide
letter no PDF/2017/002783. The authors would like to thank IGPRED
(www.igpred.com) for providing insight and expertise on the research
topic and for the assistance that greatly improved the manuscript.
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[No title captured]
NR 71
TC 31
Z9 35
U1 7
U2 122
PI OXFORD
SN 0045-6535
EI 1879-1298
J9 CHEMOSPHERE
JI Chemosphere
PD FEB
PY 2020
VL 241
AR 124824
DI 10.1016/j.chemosphere.2019.124824
PG 9
GA KG2RX
UT WOS:000509791600076
PM 31590026
DA 2023-12-05
ER
PT J
AU Gu, FQ
Peng, ZW
Zhang, YB
Tang, HM
Ye, L
Tian, WG
Liang, GS
Rao, MJ
Li, GH
Jiang, T
AF Gu, Foquan
Peng, Zhiwei
Zhang, Yuanbo
Tang, Huimin
Ye, Lei
Tian, Weiguang
Liang, Guoshen
Rao, Mingjun
Li, Guanghui
Jiang, Tao
TI Facile Route for Preparing Refractory Materials from Ferronickel Slag
with Addition of Magnesia
SO ACS SUSTAINABLE CHEMISTRY & ENGINEERING
LA English
DT Article
DE Ferronickel slag; Refractory material; Sintering; Magnesia; Resources
utilization
ID COMPRESSIVE STRENGTH; FINE AGGREGATE; SELECTIVE RECOVERY; CONVERTER
SLAG; NICKEL; CEMENT; REPLACEMENT; CONCRETE; METALS; WASTES
AB The feasibility of a facile technological route to preparation of refractory
materials from a ferronickel slag with the addition of sintered magnesia was
verified in this study based on the thermodynamics analysis and the experimental
exploration of the effect of the sintered magnesia addition on the phase
transformation of ferronickel slag during the sintering process. For the first
time, the results of thermodynamics calculation, X-ray diffraction (XRD), and
scanning electron microscopy-energy dispersive X-ray spectroscopy (SEM-EDS)
analyses revealed that the original phase of the slag can be transformed to high
melting point phases by addition of MgO during the sintering process at high
temperatures (e.g., 1350 degrees C). Specifically, the olivine in ferronickel slag
decomposed initially, generating a low-iron olivine phase and an enstatite phase.
With increasing addition of sintered magnesia, the enstatite phase changed to
forsterite, and the iron, aluminum, and chromium components in the ferronickel slag
converted to high melting point spinel phases, including magnesium aluminate spinel
and magnesium chromate spinel via a low-magnesium transient phase. The experimental
results showed that a good refractory material with refractoriness of 1660 degrees
C, bulk density of 2.92 g/cm(3), apparent porosity of 1.82%, and compressive
strength of 100.61 MPa could be obtained when the slag was sintered with addition
of 20 wt % sintered magnesia at 1350 degrees C for 3 h. Due to the low production
cost and property superiority of the prepared refractory material over commercial
counterparts, the method proposed in this study is expected to have widespread
applications in recycling of ferronickel slag.
C1 [Gu, Foquan; Peng, Zhiwei; Zhang, Yuanbo; Tang, Huimin; Ye, Lei; Rao, Mingjun;
Li, Guanghui; Jiang, Tao] Cent S Univ, Sch Minerals Proc & Bioengn, Changsha
[Tian, Weiguang; Liang, Guoshen] Guangdong Guangqing Met Technol Co Ltd,
Yangjiang 529500, Guangdong, Peoples R China.
RP Peng, ZW (corresponding author), Cent S Univ, Sch Minerals Proc & Bioengn,
Changsha 410083, Hunan, Peoples R China.
EM zwpeng@csu.edu.cn
RI jiang, tao/GWC-7108-2022; Rao, Mingjun/GSD-5794-2022; Jiang,
Tao/IWM-7503-2023; li, guanghui/JNS-0836-2023
OI Rao, Mingjun/0000-0001-6032-9340; Gu, Foquan/0000-0002-0257-8530
Natural Science Foundation of Hunan Province, China [2017JJ3383]; Key
Laboratory for Solid Waste Management and Environment Safety (Tsinghua
University) Open Fund [SWMES2017-04]; Hunan Provincial Co-Innovation
Center for Clean and Efficient Utilization of Strategic Metal Mineral
Resources [2014-405]; Guangdong Guangqing Metal Technology Co. Ltd.
[738010210]; Innovation-Driven Program of Central South University
[2016CXS021]; Shenghua Lieying Program of Central South University
[502035001]
FX This work was partially supported by the National Natural Science
Foundation of China under Grants 51774337 and 51504297, the Natural
Science Foundation of Hunan Province, China, under Grant 2017JJ3383, the
Key Laboratory for Solid Waste Management and Environment Safety
(Tsinghua University) Open Fund under Grant SWMES2017-04, the Hunan
Provincial Co-Innovation Center for Clean and Efficient Utilization of
Strategic Metal Mineral Resources under Grant 2014-405, the Guangdong
Guangqing Metal Technology Co. Ltd. under Grant 738010210, the
Innovation-Driven Program of Central South University under Grant
2016CXS021, and the Shenghua Lieying Program of Central South University
under Grant 502035001.
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NR 47
TC 31
Z9 32
U1 4
U2 90
PI WASHINGTON
SN 2168-0485
J9 ACS SUSTAIN CHEM ENG
JI ACS Sustain. Chem. Eng.
PD APR
PY 2018
VL 6
IS 4
BP 4880
EP 4889
DI 10.1021/acssuschemeng.7b04336
PG 19
WC Chemistry, Multidisciplinary; Green & Sustainable Science & Technology;
SC Chemistry; Science & Technology - Other Topics; Engineering
GA GB7WM
UT WOS:000429285800050
DA 2023-12-05
ER
PT J
AU Shi, RY
Li, JY
Jiang, J
Kamran, MA
Xu, RK
Qian, W
AF Shi, Ren-yong
Li, Jiu-yu
Jiang, Jun
Kamran, Muhammad Aqeel
Xu, Ren-kou
Qian, Wei
TI Incorporation of corn straw biochar inhibited the re-acidification of
four acidic soils derived from different parent materials
LA English
DT Article
DE Corn straw biochar; Acidic soil; pH buffering capacity; Soil
re-acidification; Potential reactiveAl pool
ID PH BUFFERING CAPACITY; VARIABLE-CHARGE SOILS; NITROGEN DEPOSITION;
ADIRONDACK REGION; SOUTHERN CHINA; POTENTIAL ROLE; ALKALINE SLAG;
ALUMINUM; ULTISOL; ADSORPTION
AB The effect of corn straw biochar on inhibiting the re-acidification of acid
soils derived from different parent materials due to increased soil pH buffering
capacity (pHBC) was investigated using indoor incubation and simulated
acidification experiments. The incorporation of the biochar increased the pHBC of
all four soils due to the increase in soil cation exchange capacity (CEC). When 5%
biochar was incorporated, the pHBC was increased by 62, 27, 32, and 24% for the
Ultisols derived from Tertiary red sandstone, Quaternary red earth, granite, and
the Oxisol derived from basalt, respectively. Ca(OH)(2) and the biochar were added
to adjust the soil pH to the same values, and then HNO3 was added to acidify these
amended soils. The results of this simulated acidification indicated that the
decrease in soil pH induced by HNO3 was lower for the treatments with the biochar
added than that of the treatments with Ca(OH)(2) added. Consequently, the biochar
could inhibit the re-acidification of the amended acid soils due to the increased
resistance of the soils to acidification when the pH of amended soil was higher
than 5.5. The inhibiting effectiveness of the biochar on soil re-acidification was
greater in the Ultisol derived from Tertiary red sandstone due to its lower clay
and organic matter contents and CEC than the other three soils. The incorporation
of the biochar also decreased the potentially reactive Al, i.e., exchangeable Al,
organically bound Al, and sorbed hydroxyl Al, compared with the treatments amended
with Ca(OH)(2). Therefore, the incorporation of corn straw biochar not only
inhibited the re-acidification of amended acid soils through increasing their
resistance to acidification but also decreased the potential of Al toxicity
generated during re-acidification.
C1 [Shi, Ren-yong; Li, Jiu-yu; Jiang, Jun; Kamran, Muhammad Aqeel; Xu, Ren-kou;
Qian, Wei] Chinese Acad Sci, Inst Soil Sci, State Key Lab Soil & Sustainable Agr,
POB 821, Nanjing, Jiangsu, Peoples R China.
[Shi, Ren-yong; Kamran, Muhammad Aqeel] Univ Chinese Acad Sci, Beijing 100049,
Peoples R China.
Soil & Sustainable Agr, POB 821, Nanjing, Jiangsu, Peoples R China.
EM rkxu@issas.ac.cn
RI Qian, Wei/B-8231-2013; Jiang, Jun/G-9125-2011
OI Jiang, Jun/0000-0001-8686-9476; /0000-0002-9727-8169
FU National Key Basic Research Program of China [2014CB441003]; National
Key Research and Development of China [2016YFD0200302]
FX This study was supported by the National Key Basic Research Program of
China (Grant Number 2014CB441003) and the National Key Research and
Development of China (Grant Number 2016YFD0200302).
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NR 53
TC 31
Z9 39
U1 21
U2 160
PI HEIDELBERG
SN 0944-1344
EI 1614-7499
PD APR
PY 2018
VL 25
IS 10
SI SI
BP 9662
EP 9672
DI 10.1007/s11356-018-1289-7
PG 11
GA GC1SK
UT WOS:000429561900044
PM 29363035
DA 2023-12-05
ER
PT J
AU Li, S
Huang, X
Muhammad, F
Yu, L
Xia, M
Zhao, J
Jiao, BQ
Shiau, Y
Li, DW
AF Li, Shan
Huang, Xiao
Muhammad, Faheem
Yu, Lin
Xia, Ming
Zhao, Jian
Jiao, Binquan
Shiau, YanChyuan
Li, Dongwei
TI Waste solidification/stabilization of lead-zinc slag by utilizing fly
ash based geopolymers
SO RSC ADVANCES
LA English
DT Article
ID PART I; CONDENSATION-REACTIONS; DISSOLUTION PROCESSES; ALKALI
ACTIVATION; SIO2/NA2O RATIO; HEAVY-METALS; IMMOBILIZATION; STRENGTH;
MICROSTRUCTURE; TEMPERATURE
AB Solidification/stabilization (S/S) is recognized as an effective technology for
solid waste treatment. In S/S, the application of geopolymers synthesized by
industrial waste (rich in active silicon and aluminum) to immobilize hazardous
waste is a research focus. In this article, a fly ash based geopolymer was used to
immobilize lead-zinc slag containing Pb, Ni, Zn and Mn. A fly ash based geopolymer
with good mechanical strength was obtained through single factor experiments and
the compressive strength of the geopolymer reached 29.72 MPa. The effects of
immobilizing lead-zinc slag in the fly ash based geopolymer were discussed by means
of compressive strength, leaching test and speciation analysis. The
solidification/stabilization mechanism was further investigated using XRD, FTIR and
SEM. The mechanical properties of the fly ash based geopolymer were negatively
affected by addition of lead-zinc slag, and compressive strength decreased to 8.67
MPa when 60% lead-zinc slag was added. The geopolymer has the ability to reduce
toxicity of lead-zinc slag by immobilizing heavy metals (Pb, Ni, Zn and Mn), but
the ability was not unlimited. The migration of heavy metals to residual form
indicates that heavy metals may either be bonded into the geopolymer matrix via the
T-O bond (T = Si, Al) or captured in framework cavities to maintain the charge
balance. The NASH (Na2O-Al2O3-SiO2-H2O) gel structure observed by XRD, FTIR and SEM
can physically encapsulate the contaminants during geopolymerization. It is finally
concluded that heavy metals were immobilized in the fly ash based geopolymer
through a combination of chemical bonding and physical encapsulation.
C1 [Li, Shan; Jiao, Binquan; Li, Dongwei] Chongqing Univ, State Key Lab Coal Mine
Disaster Dynam & Control, Chongqing 400044, Peoples R China.
[Li, Shan; Huang, Xiao; Muhammad, Faheem; Yu, Lin; Xia, Ming; Zhao, Jian; Jiao,
Binquan; Li, Dongwei] Chongqing Univ, Coll Resource & Environm Sci, Chongqing
[Yu, Lin; Jiao, Binquan] Chongqing Univ, City Coll Sci & Technol, Chongqing
[Shiau, YanChyuan] Chung Hua Univ, Dept Construct Management, 707 Wufu Rd,Sec 2,
Hsinchu 30012, Taiwan.
C3 Chongqing University; Chongqing University; Chongqing University; Chung
Hua University
RP Jiao, BQ; Li, DW (corresponding author), Chongqing Univ, State Key Lab Coal Mine
Disaster Dynam & Control, Chongqing 400044, Peoples R China.; Jiao, BQ; Li, DW
(corresponding author), Chongqing Univ, Coll Resource & Environm Sci, Chongqing
400044, Peoples R China.; Jiao, BQ (corresponding author), Chongqing Univ, City
Coll Sci & Technol, Chongqing 400044, Peoples R China.; Shiau, Y (corresponding
author), Chung Hua Univ, Dept Construct Management, 707 Wufu Rd,Sec 2, Hsinchu
30012, Taiwan.
EM j.binquan@cqu.edu.cn; ycshiau@chu.edu.tw; litonwei@cqu.edu.cn
RI Li, Dongwei/F-4215-2011; Xia, Ming/AAC-7896-2019; Shiau,
Yan-Chyuan/R-1816-2016; LI, DONGWEI/JJE-8110-2023; Faheem,
Muhammad/CAA-0924-2022
OI Xia, Ming/0000-0001-5614-4677; Shiau, Yan-Chyuan/0000-0001-5287-6643;
Faheem, Muhammad/0000-0002-9795-370X
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NR 34
TC 31
Z9 34
U1 9
U2 52
PI CAMBRIDGE
ENGLAND
SN 2046-2069
J9 RSC ADV
JI RSC Adv.
PY 2018
VL 8
IS 57
BP 32956
EP 32965
DI 10.1039/c8ra06634e
PG 10
SC Chemistry
GA GY2DE
UT WOS:000448348200060
PM 35547705
DA 2023-12-05
ER
PT J
AU Abisheva, ZS
Karshigina, ZB
Bochevskaya, YG
Akcil, A
Sargelova, EA
Kvyatkovskaya, MN
Silachyov, IY
AF Abisheva, Zinesh Sadyrovna
Karshigina, Zaure Baytasovna
Bochevskaya, Yelena Gennadyevna
Akcil, Ata
Sargelova, Elmira Abdikhalikovna
Kvyatkovskaya, Marina Nikolayevna
Silachyov, Igor Yurievich
TI Recovery of rare earth metals as critical raw materials from phosphorus
slag of long-term storage
SO HYDROMETALLURGY
LA English
DT Article
DE Rare-earth metals; Phosphorus slag; Leaching; Nitric acid; Lanthanides
ID WASTE; ELEMENTS; CONCRETE; POWDER
AB The present research is directed towards processing of slag originating during
the yellow phosphorus production. The slag was investigated using physical and
chemical treatment methods. The following group of rare earth elements were
identified in phosphorus slag such as: Sc, Y, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Ho,
Tm, Yb, Lu. Thermodynamic calculation for reactions probability of phosphorous slag
components with nitric acid was made. Nitric-acid leaching of slag generated during
phosphorus production was investigated for extraction of rare earth metals (REMs).
Silicon containing cake obtained after leaching was suitable for precipitated
silicon dioxide production. Behaviour of associated components such as calcium,
aluminium and iron was studied during the leaching process. The following optimum
parameters were selected for leaching studies: nitric acid concentration was 7.5
mol/dm(3); solid-to-liquid ratio was 1:2.6-3; temperature was 50-80 degrees C;
process duration was 1 h; pulp stirring rate was 500 rpm and the recovery of rare-
earth metals, calcium, aluminum and iron into the solution were seen to be 85%,
98%, 80.7%, and 11.8%, respectively. Cake produced as a result of leaching
contained similar to 80-85% of amorphous SiO2. The solution obtained after
phosphorus slag leaching was processed through solvent extraction methods to
concentrate and separate it from basic macroimpurities. After precipitation of REMs
oxalates from strip liquor and calcination of the precipitate a concentrate was
obtained, which contained similar to 17% of EREMs oxides.
C1 [Abisheva, Zinesh Sadyrovna; Karshigina, Zaure Baytasovna; Bochevskaya, Yelena
Gennadyevna; Sargelova, Elmira Abdikhalikovna; Kvyatkovskaya, Marina Nikolayevna]
Inst Met & Ore Beneficat, Shevchenko St 29-133, Alma Ata 050010, Kazakhstan.
[Akcil, Ata] Suleyman Demirel Univ, Dept Min Engn, Mineral Proc Div, Mineral Met
Recovery & Recycling MMR&R Res Grp, TR-32260 Isparta, Turkey.
[Silachyov, Igor Yurievich] Inst Nucl Phys, Ibragimova St 1, Alma Ata 050032,
Kazakhstan.
C3 Institute of Metallurgy & Ore Beneficiation; Suleyman Demirel
University; Institute of Nuclear Physics - Kazakhstan
RP Akcil, A (corresponding author), Suleyman Demirel Univ, Dept Min Engn, Mineral
Proc Div, Mineral Met Recovery & Recycling MMR&R Res Grp, TR-32260 Isparta, Turkey.
EM ataakcil@sdu.edu.tr
RI Bochevskaya, Yelena/O-4998-2017; Karshyga, Zaure Baitaskyzy/O-5905-2017;
Akcil, Ata/J-1280-2017; Elmira, Sargelova/AAW-7908-2020; Abisheva,
Zinesh/O-8453-2017
OI Bochevskaya, Yelena/0000-0001-5413-6446; Karshyga, Zaure
Baitaskyzy/0000-0002-3025-7363; Akcil, Ata/0000-0002-9991-0543; Elmira,
Sargelova/0000-0002-3239-6594; Abisheva, Zinesh/0000-0002-4506-0694
FU Ministry of Education and Science of the Republic of Kazakhstan [1220
GF/4]
FX The study has been completed by means of the grant no. 1220 GF/4
received from the Ministry of Education and Science of the Republic of
Kazakhstan. This collaborative research was based on the results of
bilateral contacts of the Centre of Earth Sciences, Metallurgy and Ore
Beneficiation, Almaty, Kazakhstan and the Mineral-Metal Recovery and
Recycling Research Group, Mineral Processing Division, Department of
Mining Engineering, Suleyman Demirel University, Isparta, Turkey. The
authors are thankful to Dr. Srabani Mishra for her kind help during
language editing.
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NR 49
TC 31
Z9 33
U1 3
U2 69
PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD NOV
PY 2017
VL 173
BP 271
EP 282
DI 10.1016/j.hydromet.2017.08.022
PG 12
GA FJ8ZG
UT WOS:000413056600032
DA 2023-12-05
ER
PT J
AU Cho, JW
Yoo, S
Park, MS
Park, JK
Moon, KH
AF Cho, Jung-Wook
Yoo, Shin
Park, Min-Seok
Park, Joong-Kil
Moon, Ki-Hyeon
TI Improvement of Castability and Surface Quality of Continuously Cast TWIP
Slabs by Molten Mold Flux Feeding Technology
LA English
DT Article
ID RADIATIVE HEAT-TRANSFER; CRYSTALLIZATION BEHAVIOR; INITIAL
SOLIDIFICATION; STEEL; FILM; THICKNESS; VISCOSITY; PREDICTION; OXIDES;
POWDER
AB An innovative continuous casting process named POCAST (POSCO's advanced CASting
Technology) was developed based on molten mold flux feeding technology to improve
both the productivity and the surface quality of cast slabs. In this process,
molten mold flux is fed into the casting mold to enhance the thermal insulation of
the meniscus and, hence, the lubrication between the solidifying steel shell and
the copper mold. Enhancement of both the castability and the surface quality of
high-aluminum advanced high-strength steel (AHSS) slabs is one of the most
important advantages when the new process has been applied into the commercial
continuous casting process. A trial cast of TWIP steel has been carried out using a
10-ton scale pilot caster and 100-ton scale and 250-ton scale commercial casters.
The amount of mold flux consumption was more than 0.2 kg/m(2) in the new process,
which is much larger than that in the conventional powder casting. Trial TWIP
castings at both the pilot and the plant caster showed stable mold performances
such as mold heat transfer. Also, cast slabs showed periodic/sound oscillation
marks and little defects. The successful casting of TWIP steel has been attributed
to the following characteristics of POCAST: dilution of the reactant by increasing
the slag pool depth, enlargement of channel for slag film infiltration at meniscus
by elimination of the slag bear, and decrease of apparent viscosity of the mold
slag at meniscus by increasing the slag temperature.
C1 [Cho, Jung-Wook; Yoo, Shin; Park, Min-Seok; Park, Joong-Kil; Moon, Ki-Hyeon]
Tech Res Labs POSCO, Pohang 37895, South Korea.
C3 Pohang University of Science & Technology (POSTECH)
RP Cho, JW; Park, JK (corresponding author), Tech Res Labs POSCO, Pohang 37895,
South Korea.; Cho, JW (corresponding author), Pohang Univ Sci & Technol POSTECH,
Grad Inst Ferrous Technol, Pohang 37673, South Korea.
EM jungwook@postech.ac.kr; jk_park@posco.com
RI Cho, Jung-Wook/A-8142-2013
OI Cho, Jung-Wook/0000-0003-2364-1938
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NR 34
TC 31
Z9 34
U1 3
U2 45
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD FEB
PY 2017
VL 48
IS 1
BP 187
EP 196
DI 10.1007/s11663-016-0818-3
PG 10
Engineering
GA EI2CZ
UT WOS:000392295500020
DA 2023-12-05
ER
PT J
AU Behera, S
Sarkar, R
AF Behera, Satyananda
Sarkar, Ritwik
TI Effect of different metal powder anti-oxidants on N220 nano carbon
containing low carbon MgO-C refractory: An in-depth investigation
LA English
DT Article
DE MgO-C refractory; Metal powder anti-oxidants; Properties; In situ
ceramic phases
ID MECHANICAL-PROPERTIES; NANOCARBON; MICROSTRUCTURES; CORROSION; BEHAVIOR;
OXIDE
AB Effect of three different metal powder antioxidants, namely, Al, Si, and Mg was
studied on the development of N220 nano carbon containing low carbon MgO-C
refractory. The study was also extended to conventional MgO-C refractory
compositions with 16% graphite content. All the refractory compositions were
processed as per conventional MgO-C refractory manufacturing techniques and were
evaluated for physical, mechanical, thermo-mechanical properties, oxidation
resistance and static corrosion resistance against steel converter slag.
Microstructural developments and in-situ ceramic phase formation in the
compositions were also studied. The results show that nano carbon containing low
carbon MgO-C refractory compositions have better properties than conventional
composition and among the three antioxidants, the aluminum metal powder has shown
the improved properties. (C) 2016 Elsevier Ltd and Techna Group S.r.l. All rights
reserved.
C1 [Behera, Satyananda; Sarkar, Ritwik] Natl Inst Technol, Dept Ceram Engn,
Rourkela, India.
Technology Rourkela
RP Behera, S (corresponding author), Natl Inst Technol, Dept Ceram Engn, Rourkela,
India.
EM satyananda.1990@gmail.com
RI Behera, Satyananda/N-2974-2018
OI Behera, Satyananda/0000-0002-7513-3313; SARKAR,
RITWIK/0000-0002-4017-5599
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NR 23
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U1 0
U2 28
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
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JI Ceram. Int.
PD DEC
PY 2016
VL 42
IS 16
BP 18484
EP 18494
DI 10.1016/j.ceramint.2016.08.185
PG 11
GA ED0OV
UT WOS:000388542700070
DA 2023-12-05
ER
PT J
AU Lou, WT
Zhu, MY
AF Lou, Wentao
Zhu, Miaoyong
TI Numerical Simulation of Slag-metal Reactions and Desulfurization
Efficiency in Gas-stirred Ladles with Different Thermodynamics and
Kinetics
LA English
DT Article
DE slag-metal reactions; desulfurization; CFD-SRM coupled model; ladle;
numerical simulation
ID SULFUR PARTITION; SULFIDE CAPACITY; BATH SURFACES; HOT METAL; MODEL;
SILICON; DYNAMICS; FURNACE; SPOUTS; STEEL
AB A computational fluid dynamics-simultaneous reaction model (CFD-SRM) coupled
model has been proposed to investigate the effects of different contents of
aluminum, manganese and silicon in slag and liquid steel, the arrangement of bottom
blowing tuyeres and the height ratio of slag and metal on the slag-metal reactions
and desulfurization efficiency in gas-stirred ladles. The results show that as the
aluminum is added into liquid steel, both the desilication rate and demanganization
rate decrease, and the desulfurization rate increases rapidly. Meanwhile as the
initial aluminum content [%YAl](t=0) exceeds 0.01 mass%, the desulfurization
efficiency increases slowly. With the increase of initial silicon content [%Y-Si]
(t=0), the demanganization rate decreases, while the desulfurization rate
increases. When the [%Y-Si](t=0) exceeds 0.5 mass%, the effect of [%Y-Si](t=0)
becomes weak. As well, the variations of manganese content in liquid steel has
little effect on the desulfurization efficiency. For the initial content (%Y-i)
(t=0), in slag, with the decreasing of (%Y-Al2O3)(t=0), the desulfurization rate
increases rapidly, but as the (%Y-Al2O3)(t=0) is less than 23.0 mass%, the
desulfurization efficiency increases slightly. With the increasing of the (%Y-MnO)
(t=0), the desulfurization efficiency decreases rapidly. Furthermore, the dual
blowing gives higher desulfurization efficiency in comparison with the center
blowing or eccentric blowing with one tuyere. With the increasing of height ratio
of slag and metal (h/H), the desulfurization efficiency increases, but when the h/H
exceeds 0.4, the desulfurization efficiency changes weakly.
C1 [Lou, Wentao; Zhu, Miaoyong] Northeastern Univ, Sch Mat & Met, Shenyang 110819,
Peoples R China.
RP Zhu, MY (corresponding author), Northeastern Univ, Sch Mat & Met, 3-11 Wenhua
Rd, Shenyang 110819, Peoples R China.
EM myzhu@mail.neu.edu.cn
FU National Natural Science Foundation of China [51134009]; Specialized
[20110042110010]
FX The authors wish to express thanks to the National Natural Science
Foundation of China (51134009) and the Specialized Research Fund for the
Doctoral Program of Higher Education of China (20110042110010) for
supporting this work.
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PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2015
VL 55
IS 5
BP 961
EP 969
PG 9
GA CI8YV
UT WOS:000355058500008
OA gold
DA 2023-12-05
ER
PT J
AU Schmukat, A
Duester, L
Ecker, D
Schmid, H
Heil, C
Heininger, P
Ternes, TA
AF Schmukat, A.
Duester, L.
Ecker, D.
Schmid, H.
Heil, C.
Heininger, P.
Ternes, T. A.
TI Leaching of metal(loid)s from a construction material: Influence of the
particle size, specific surface area and ionic strength
LA English
DT Article
DE Specific surface area; Metal(loid) release; Copper slag; Iron silicate;
Salinity
ID COPPER SLAGS; RELEASE
AB Construction materials are tested worldwide for a potential release of dangerous
substances to prevent adverse effects on humans and biota. It is crucial to
identify and understand the processes which are decisive for the release of
hazardous substances. The current study compares the results of different test
methods. Taking copper slag as model material, the influence of material particle
size, eluant composition and ionic strength was tested. Ionic strength and salinity
significantly influenced the release of metal(loid)s in the water phase.
Furthermore, it was elucidated that colloids can cause methodological artefacts.
The available specific surface area exhibited a positive correlation with the
release of hazardous substances. The specific surface areas of materials were
determined by the Brunauer, Emmett and Teller model (BET) and four other methods.
The aluminium foil method showed the best results with regard to the statistical
uncertainty, compared to a 3D laser scanning method. With help of the roughness
factor A. it is possible to compare the results from surface area measurements with
different material particle sizes (0-250 mm). This comparability offers the
potential to match the release of metal(loid)s from laboratory studies with field
applications and catchment area calculations/modelling, based on the release per
m(2). (C) 2012 Elsevier B.V. All rights reserved.
C1 [Schmukat, A.; Duester, L.; Ecker, D.; Schmid, H.; Heil, C.; Heininger, P.;
Ternes, T. A.] Fed Inst Hydrol, Dept Aquat Chem, D-56068 Koblenz, Germany.
RP Duester, L (corresponding author), Fed Inst Hydrol, Dept Aquat Chem, Mainzer Tor
1, D-56068 Koblenz, Germany.
EM duester@bafg.de
RI Duester, Lars/I-3478-2014
OI Duester, Lars/0000-0001-7025-3810
FU KLIWAS
FX This study was financed by KLIWAS. We would like to thank RPBL for the
provision of the basanite.
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Z9 32
U1 0
U2 35
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD AUG 15
PY 2012
VL 227
BP 257
EP 264
DI 10.1016/j.jhazmat.2012.05.045
PG 8
GA 976ZX
UT WOS:000306627000033
PM 22683212
DA 2023-12-05
ER
PT J
AU Shi, CB
Chen, XC
Guo, HJ
AF Shi, Cheng-bin
Chen, Xi-chun
Guo, Han-jie
TI Characteristics of inclusions in high-Al steel during electroslag
remelting process
LA English
DT Article
DE electroslag remelting; aluminum nitride; inclusions; thermodynamics
ID ALUMINUM NITRIDE; FE-CR; DEOXIDATION; SOLIDIFICATION; SLAGS; OXIDE;
IRON; NI
AB The characteristics of inclusions in high-Al steel refined by electroslag
remelting (ESR) were investigated by image analysis, scanning electron microscopy
(SEM), and energy-dispersive spectrometry (EDS). The results show that the size of
almost all the inclusions observed in ESR ingots is less than 5 mu m. Inclusions
smaller than 3 mu m take nearly 75% of the total inclusions observed in each ingot.
Inclusions observed in ESR ingots are pure AlN as dominating precipitates and some
fine spherical Al2O3 inclusions with a size of 1 mu m or less. It is also found
that protective gas operation and slag deoxidation treatment during ESR process
have significant effects on the number of inclusions smaller than 2 mu m but little
effects on that of inclusions larger than 2 mu m. Thermodynamic calculations show
that AlN inclusions are unable to precipitate in the liquid metal pool under the
present experimental conditions, while the precipitation of AlN inclusions could
take place at the solidifying front due to the microsegregation of Al and N in
liquid steel during solidification.
C1 [Shi, Cheng-bin; Guo, Han-jie] Univ Sci & Technol Beijing, State Key Lab Adv
[Shi, Cheng-bin; Guo, Han-jie] Univ Sci & Technol Beijing, Sch Met & Ecol Engn,
[Chen, Xi-chun] Cent Iron & Steel Res Inst, Res Inst High Temp Mat, Beijing
C3 University of Science & Technology Beijing; University of Science &
Technology Beijing; Central Iron & Steel Research Institute
RP Guo, HJ (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
EM guohanjie@ustb.edu.cn
RI Shi, Chengbin/J-1262-2016
OI Shi, Chengbin/0000-0001-8127-3382; Guo, Han-jie/0000-0002-6493-8853
FU International Science and Technology Cooperation and Exchange of Special
Projects [2010DFR50590]
FX This work was financially supported by the International Science and
Technology Cooperation and Exchange of Special Projects (No.
2010DFR50590).
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PD APR
PY 2012
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IS 4
BP 295
EP 302
DI 10.1007/s12613-012-0554-x
PG 8
Mineral Processing
GA 917TI
UT WOS:000302201100004
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ER
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Nakashima, K
Mori, K
AF Nakasuga, T
Nakashima, K
Mori, K
TI Recovery rate of chromium from stainless slag by iron melts
LA English
DT Article
DE ironmaking; steelmaking; recycle; stainless slag; Cr2O3; reduction;
slag-metal reaction; kinetics; modeling
ID SMELTING REDUCTION; CARBON; OXIDE; DEPHOSPHORIZATION; CR2O3; STEEL;
STATE; METAL; ORE
AB The kinetic behavior of Cr2O3 reduction by iron melts containing carbon,
aluminum and silicon were investigated at various conditions in order to understand
effective slag treatment for recovery of chromium from stainless slag. It was found
that the recovery rate of chromium was fairly slow, but it was considerably
accelerated by the addition of some fluxes, such as Al2O2 and SiO2 to the slag,
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C1 Kobe Steel Ltd, Kakogawa Works, Ctr Res & Dev, Kakogawa 6750023, Japan.
Kyushu Univ, Grad Sch Engn, Dept Mat Sci & Engn, Higashi Ku, Fukuoka 8128581,
Japan.
Kyushu Univ, Fukuoka 812, Japan.
C3 Kobe Steel; Kyushu University; Kyushu University
RP Nakasuga, T (corresponding author), Kobe Steel Ltd, Kakogawa Works, Ctr Res &
Dev, Kakogawa 6750023, Japan.
EM nakasima@zaiko.kyushu-u.ac.jp
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BP 665
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ER
PT J
AU Pedarnig, JD
Trautner, S
Grünberger, S
Giannakaris, N
Eschlböck-Fuchs, S
Hofstadler, J
AF Pedarnig, Johannes D.
Trautner, Stefan
Gruenberger, Stefan
Giannakaris, Nikolaos
Eschlboeck-Fuchs, Simon
Hofstadler, Josef
TI Review of Element Analysis of Industrial Materials by In-Line
Laser-Induced Breakdown Spectroscopy (LIBS)
SO APPLIED SCIENCES-BASEL
LA English
DT Review
DE laser-induced breakdown spectroscopy (LIBS); multi-element detection;
industrial materials; technology materials; in-line chemical analysis;
process control in industrial production
ID LOW-ALLOY STEELS; QUANTITATIVE-ANALYSIS; DOUBLE-PULSE; INDUCED PLASMA;
ALUMINUM-ALLOYS; RAPID ANALYSIS; SLAG ANALYSIS; HEAVY-METALS;
SINGLE-PULSE; MULTIVARIATE-ANALYSIS
AB Laser-induced breakdown spectroscopy (LIBS) is a rapidly developing technique
for chemical materials analysis. LIBS is applied for fundamental investigations,
e.g., the laser plasma matter interaction, for element, molecule, and isotope
analysis, and for various technical applications, e.g., minimal destructive
materials inspection, the monitoring of production processes, and remote analysis
of materials in hostile environment. In this review, we focus on the element
analysis of industrial materials and the in-line chemical sensing in industrial
production. After a brief introduction we discuss the optical emission of chemical
elements in laser-induced plasma and the capability of LIBS for multi-element
detection. An overview of the various classes of industrial materials analyzed by
LIBS is given. This includes so-called Technology materials that are essential for
the functionality of modern high-tech devices (smartphones, computers, cars, etc.).
The LIBS technique enables unique applications for rapid element analysis under
harsh conditions where other techniques are not available. We present several
examples of LIBS-based sensors that are applied in-line and at-line of industrial
production processes.
C1 [Pedarnig, Johannes D.; Trautner, Stefan; Gruenberger, Stefan; Giannakaris,
Nikolaos] Johannes Kepler Univ Linz, Inst Appl Phys, A-4040 Linz, Austria.
[Eschlboeck-Fuchs, Simon; Hofstadler, Josef] Voestalpine Stahl GmbH, A-4020
Linz, Austria.
RP Pedarnig, JD (corresponding author), Johannes Kepler Univ Linz, Inst Appl Phys,
A-4040 Linz, Austria.
EM johannes.pedarnig@jku.at; stefan.trautner@tgw-group.com;
stefan.gruenberger@jku.at; nikolaos.giannakaris@jku.at;
simon.eschlboeck-fuchs@voestalpine.com; Josef.Hofstadler@voestalpine.com
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OI Pedarnig, Johannes D/0000-0002-7842-3922; Giannakaris,
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NR 475
TC 30
Z9 31
U1 25
U2 107
PU MDPI
PI BASEL
EI 2076-3417
J9 APPL SCI-BASEL
JI Appl. Sci.-Basel
PD OCT
PY 2021
VL 11
IS 19
AR 9274
DI 10.3390/app11199274
PG 46
WC Chemistry, Multidisciplinary; Engineering, Multidisciplinary; Materials
Science, Multidisciplinary; Physics, Applied
SC Chemistry; Engineering; Materials Science; Physics
GA YY5VE
UT WOS:000754855900001
OA gold, Green Published
DA 2023-12-05
ER
PT J
AU Sotiriadis, K
Mácová, P
Mazur, AS
Viani, A
Tolstoy, PM
Tsivilis, S
AF Sotiriadis, Konstantinos
Macova, Petra
Mazur, Anton S.
Viani, Alberto
Tolstoy, Peter M.
Tsivilis, Sotirios
TI Long-term thaumasite sulfate attack on Portland-limestone cement
concrete: A multi-technique analytical approach for assessing phase
assemblage
LA English
DT Article
DE Portland-limestone cement; Supplementary cementitious materials;
Thaumasite sulfate attack; Solid state NMR spectroscopy
ID C-S-H; SI-29 MAS NMR; SOLID-SOLUTIONS; HYDRATION KINETICS; CALCIUM;
AL-27; ETTRINGITE; MAGNESIUM; ALUMINUM; SPECTROSCOPY
AB Multiple techniques were applied to the investigation of the phase composition
of the deteriorated surface of Portland-limestone cement concrete specimens exposed
for 10 years to conditions promoting thaumasite sulfate attack. The results were
interpreted in terms of the limestone content of cement and the incorporation of
supplementary cementitious materials (SCMs) (natural pozzolana, blastfurnace slag,
metakaolin). Thaumasite, detected in high amounts in concrete specimens made
without SCMs, was associated with Al to some extent. Considerable degradation of
calcium silicate hydrate occurred in all specimens, resulting in the formation of
Al-associated cross-linked silicate chains, magnesium silicate hydrate and silica
gel, a process most effectively prevented by metakaolin. For the highest limestone
content in cement or use of natural pozzolana, thaumasite underwent extensive
decomposition. Al incorporation into cross-linked silicate chains increased with
increasing limestone content in cement. Longer aluminosilicate chains with larger
Al fractions were observed in concrete specimens incorporating SCMs.
C1 [Sotiriadis, Konstantinos; Macova, Petra; Viani, Alberto] Czech Acad Sci, Inst
Theoret & Appl Mech, Prosecka 809-76, CZ-19000 Prague, Czech Republic.
[Mazur, Anton S.; Tolstoy, Peter M.] St Petersburg State Univ, Ctr Magnet
Resonance, Univ Sky Pr 26, RU-198504 St Petersburg, Russia.
[Tsivilis, Sotirios] Natl Tech Univ Athens, Sch Chem Engn, Heroon Polytechniou
9, GR-15773 Athens, Greece.
C3 Institute of Theoretical & Applied Mechanics of the Czech Academy of
Sciences; Czech Academy of Sciences; Saint Petersburg State University;
National Technical University of Athens
RP Sotiriadis, K (corresponding author), Czech Acad Sci, Inst Theoret & Appl Mech,
Prosecka 809-76, CZ-19000 Prague, Czech Republic.
EM sotiriadis@itam.cas.cz
RI Tolstoy, Peter M/J-2966-2013; Viani, Alberto/H-2153-2014; Macova,
Petra/H-2138-2014; Sotiriadis, Konstantinos/C-7130-2017
OI Tolstoy, Peter M/0000-0002-8426-3988; Viani,
Alberto/0000-0002-6019-1094; Sotiriadis,
Konstantinos/0000-0002-9848-4028; Macova, Petra/0000-0002-8277-133X
FU Czech Science Foundation (GACR) [18-26056Y]
FX This study was accomplished in the frame of the project "Experimental
quantification and modelling of deterioration in Portland-limestone
cement pastes affected by thaumasite sulfate attack" (grant number
18-26056Y), financed by the Czech Science Foundation (GACR). NMR
measurements were performed within the framework of the cooperation
agreement between the St. Petersburg State University and the Institute
of Theoretical and Applied Mechanics of the Czech Academy of Sciences.
The authors thank Mgr. Dita Frankeova for the assistance during the
evaluation of thermogravimetric analysis results.
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NR 102
TC 30
Z9 31
U1 4
U2 29
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD APR
PY 2020
VL 130
AR 105995
DI 10.1016/j.cemconres.2020.105995
PG 12
GA LG2BU
UT WOS:000527913700012
DA 2023-12-05
ER
PT J
AU Sayehi, M
Tounsi, H
Garbarino, G
Riani, P
Busca, G
AF Sayehi, Mouna
Tounsi, Hassib
Garbarino, Gabriella
Riani, Paola
Busca, Guido
TI Reutilization of silicon- and aluminum- containing wastes in the
perspective of the preparation of
SiO2-Al2O3 based porous materials for
adsorbents and catalysts
SO WASTE MANAGEMENT
LA English
DT Article
DE Valorization; Wastes; Porous materials; Alumina; Silica; Zeolites
ID COAL FLY-ASH; HYDROTHERMAL SYNTHESIS; GAMMA-ALUMINA; NA-A; CHEMICAL
CHARACTERISTICS; ZEOLITE SYNTHESIS; COPPER SLAG; X ZEOLITES; REMOVAL;
RECOVERY
AB The waste materials available as sources of silicon and aluminum for producing
porous materials like amorphous silicas, aluminas, amorphous silica-aluminas, and
zeolites, to be used as catalyst and adsorbents, are briefly summarized. The
procedures for preparing these materials from wastes are also taken into account.
The limits of this approach in terms of economy and environmental protection are
also briefly considered. It is concluded that mesoporous materials can be prepared
from wastes, but care to product quality and to overall process efficiency is
needed. (c) 2019 Elsevier Ltd. All rights reserved.
C1 [Sayehi, Mouna; Tounsi, Hassib] Univ Sfax, Lab Mat Avances, Ecole Natl
Ingenieurs Sfax, Sfax, Tunisia.
[Garbarino, Gabriella; Busca, Guido] Univ Genoa, Dipartimento Ingn Civile Chim &
Ambientale DICCA, Via Opera Pia 15, I-16145 Genoa, Italy.
[Garbarino, Gabriella; Riani, Paola; Busca, Guido] UdR Genova, Consorzio INSTM,
Via Dodecaneso 31, I-16146 Genoa, Italy.
[Riani, Paola] Univ Genoa, Dipartimento Farm DIFAR, Viale Cembrano 4, I-16148
Genoa, Italy.
C3 Universite de Sfax; Ecole Nationale dIngenieurs de Sfax (ENIS);
University of Genoa; University of Genoa
RP Busca, G (corresponding author), Univ Genoa, Dipartimento Ingn Civile Chim &
Ambientale DICCA, Via Opera Pia 15, I-16145 Genoa, Italy.
EM Guido.Busca@unige.it
RI Busca, Guido/A-1095-2008; Garbarino, Gabriella/B-7976-2015
OI Busca, Guido/0000-0002-5682-2682; Garbarino,
Gabriella/0000-0002-5590-6155; Tounsi, Hassib/0000-0002-6889-7585
FU University of Sfax
FX Mouna Sayehi acknowledges the University of Sfax for a grant (bourse d'
alternance 2018 program).
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Z9 31
U1 7
U2 67
PI OXFORD
SN 0956-053X
EI 1879-2456
J9 WASTE MANAGE
JI Waste Manage.
PD FEB 15
PY 2020
VL 103
BP 146
EP 158
DI 10.1016/j.wasman.2019.12.013
PG 13
GA MI4GI
UT WOS:000547367900016
PM 31877498
DA 2023-12-05
ER
PT J
AU Shao, HQ
Gao, EZ
Wang, WL
Zhang, L
AF Shao, Hanqing
Gao, Erzhuo
Wang, Wanlin
Zhang, Lei
TI Effect of fluorine and CaO/Al2O3 mass ratio on the
viscosity and structure of CaO-Al2O3-based mold
fluxes
LA English
DT Article
DE CaO; Al2O3; fluorine; mold flux; spectroscopy; structure; viscosity
ID CRYSTALLIZATION BEHAVIOR; CALCIUM ALUMINOSILICATE; IONOMER GLASSES;
ALUMINUM; RAMAN; NMR; SPECIATION; STEEL; SLAG; PERALKALINE
AB The effect of CaO/Al2O3 mass ratio (C/A) and fluorine content on the viscosity
and structure of CaO-Al2O3-based mold fluxes has been researched in this paper. The
viscosity results indicated that increasing fluorine only slightly decreases the
viscosity of the slag melt, and higher C/A is also observed to decrease the
viscosity of molten slag when the C/A changes from 1.3 to 1.7. Structural analysis
of the as-quenched fluxes using the Raman spectroscopy showed that the amounts of
Al-O-0 and Si-O-Al structural units all decrease with higher fluorine content and
C/A, indicating that a depolymerization of the molten structure is occurring. The
results of Al-27 and F-19 magic angle spinning nuclear magnetic resonance showed
that fluorine tends to participate in the network structure and coordinate with
Al3+ ions to form complex ionic clusters. The results suggested that the role of
fluorine in the CaO-Al2O3-based slag system is different from the traditional slag
system in which fluorine only acts as a diluent, thus reducing the effect of
fluorine on lowering the viscosity. In addition, the coordination environment of
Al3+ ions can be simplified by higher C/A through promoting the generation of
[AlO4](-) tetrahedral structures. Besides, the free O2- ions provided by excess CaO
would break the Al-O-0 bonds and further depolymerize the network structure,
thereby decrease the viscosity.
C1 [Shao, Hanqing; Gao, Erzhuo; Wang, Wanlin; Zhang, Lei] Cent S Univ, Sch Met &
Environm, Changsha, Hunan, Peoples R China.
[Shao, Hanqing; Gao, Erzhuo; Wang, Wanlin; Zhang, Lei] Natl Ctr Int Cooperat
Clean Met, Changsha, Hunan, Peoples R China.
RP Wang, WL (corresponding author), Cent S Univ, Sch Met & Environm, Changsha,
RI Zhang, Lei/ABA-4375-2021
OI Zhang, Lei/0000-0002-1758-5733
FU National Science Foundation of China [51661130154, U1760202]; Newton
Advanced Fellowship [NA150320]
FX National Science Foundation of China, Grant/Award Number: 51661130154,
U1760202; Newton Advanced Fellowship, Grant/Award Number: NA150320
CR [Anonymous], GLASSES THEIR APPL
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5
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NR 39
TC 30
Z9 31
U1 1
U2 55
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD AUG
PY 2019
VL 102
IS 8
BP 4440
EP 4449
DI 10.1111/jace.16322
PG 10
GA IB1HT
UT WOS:000470016900009
DA 2023-12-05
ER
PT J
AU Walkley, B
Kashani, A
Sani, MA
Ngo, TD
Mendis, P
AF Walkley, Brant
Kashani, Alireza
Sani, Marc-Antoine
Ngo, Tuan D.
Mendis, Priyan
TI Examination of alkali-activated material nanostructure during thermal
treatment
LA English
DT Article
ID CALCIUM SILICATE HYDRATE; MAS-NMR-SPECTROSCOPY; BLAST-FURNACE SLAG;
FLY-ASH; PHASE EVOLUTION; ELEVATED-TEMPERATURE; THERMODYNAMIC MODEL;
RANGE ORDER; SI-29; GEOPOLYMERS
AB The key nanostructural changes occurring in a series of alkali-activated
materials (AAM) based on blends of slag and fly ash precursors during exposure to
temperatures up to 1000 A degrees C are investigated. The main reaction product in
each AAM is a crosslinked sodium- and aluminium-substituted calcium silicate
hydrate (C-(N)-A-S-H)-type gel. Increased alkali content promotes the formation of
an additional sodium aluminosilicate hydrate (N-A-S-(H)) gel reaction product due
to the structural limitations on Al substitution within the C-(N)-A-S-H gel.
Heating each AAM to 1000 A degrees C results in the crystallisation of the
disordered gels and formation of sodalite, nepheline and wollastonite. Increased
formation of N-A-S-(H) reduces binder structural water content after thermal
treatment and correlates closely with previous observations of improved strength
retention and reduced microcracking in these AAM after heating to 1000 A degrees C.
This provides new insight into thermally induced changes to gel atomic structure
and thermal durability of C-(N)-A-S-H/N-A-S-H gel blends which are fundamental for
the development of new fire-resistant construction materials.
C1 [Walkley, Brant] Univ Sheffield, Dept Mat Sci & Engn, Sheffield S1 3JD, S
Yorkshire, England.
[Kashani, Alireza; Ngo, Tuan D.; Mendis, Priyan] Univ Melbourne, Dept
Infrastruct Engn, Parkville, Vic 3010, Australia.
[Sani, Marc-Antoine] Univ Melbourne, Sch Chem, Parkville, Vic 3010, Australia.
[Sani, Marc-Antoine] Univ Melbourne, Inst Bio21, Parkville, Vic 3010, Australia.
RP Walkley, B (corresponding author), Univ Sheffield, Dept Mat Sci & Engn,
EM b.walkley@sheffield.ac.uk
RI Sani, Marc-Antoine/B-7707-2013; Ngo, Tuan/P-8184-2014
OI Sani, Marc-Antoine/0000-0003-3284-2176; Ngo, Tuan/0000-0002-9831-8580;
Walkley, Brant/0000-0003-1069-1362; Mendis, Priyan/0000-0003-4068-8201
FU Australian Research Council (ARC); ARC [LP140100504]; ARC Centre for
Advanced Manufacturing of Prefabricated Housing
FX This project was funded by the Australian Research Council (ARC),
including support through an ARC Linkage Project (Grant number:
LP140100504) and through the ARC Centre for Advanced Manufacturing of
Prefabricated Housing. XRD data were acquired at the Materials
Characterisation and Fabrication Platform (MCFP), The University of
Melbourne, and the Victorian Node of the Australian National Fabrication
Facility (ANFF). The authors thank Professor John L. Provis, The
University of Sheffield, for very insightful discussions regarding this
work.
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NR 81
TC 30
Z9 32
U1 2
U2 56
PU SPRINGER
PI NEW YORK
SN 0022-2461
EI 1573-4803
J9 J MATER SCI
JI J. Mater. Sci.
PD JUL
PY 2018
VL 53
IS 13
BP 9486
EP 9503
DI 10.1007/s10853-018-2270-z
PG 18
GA GD0EB
UT WOS:000430171400010
OA hybrid
DA 2023-12-05
ER
PT C
AU Burduhos-Nergis, DD
Abdullah, MMAB
Vizureanu, P
Tahir, MFM
AF Burduhos-Nergis, D. D.
Abdullah, M. M. A. B.
Vizureanu, P.
Tahir, M. F. M.
BE Sandu, AV
Abdullah, MMAB
Vizureanu, P
Ghazali, CMR
Sandu, I
TI Geopolymers and Their Uses: Review
SO EUROINVENT ICIR 2018
SE IOP Conference Series-Materials Science and Engineering
LA English
DT Proceedings Paper
CT EUROINVENT International Conference on Innovative Research (ICIR)
CY MAY 17-18, 2018
CL Iasi, ROMANIA
ID BLAST-FURNACE SLAG; FLY-ASH; COMPRESSIVE STRENGTH; BOTTOM ASH; ALUMINUM
POWDER; WASTE GLASS; RED MUD; CONCRETE; MICROSTRUCTURE; METAKAOLIN
AB Outlining the past-present history of the study of alumino-silicate materials,
it is well known that geopolymers are inorganic polymers obtained from chemical
reaction, also known as geopolymerisation, between an alkaline solution and a solid
reach in aluminium and silicone. There is still some controversy surrounding the
alkaline activators used to create geopolymer concrete, because homogeneous mixture
composed of two (NaOH and Na2SO3) or more chemical in varying proportions are
usually highly corrosive and hard to handle. In order to overcome Portland cement
many wastes have been used in recent studies to create "friendly" cements by
geopolymerisation. In this short review we present basic information's about how to
create and use geopolymers, alkaline activators and raw materials that can be used
and conclusions. One question that needs to be asked: Can those materials replace
on large scale Portland cement?
C1 [Burduhos-Nergis, D. D.; Vizureanu, P.] Tech Univ Gheorghe Asachi Iasi Romania,
Dept Technol & Equipments Mat Proc, Blvd Mangeron 51, Iasi 700050, Romania.
[Abdullah, M. M. A. B.; Tahir, M. F. M.] Univ Malaysia Perlis, Sch Mat Engn, Ctr
Excellent Geopolymer & Green Technol, POB 77, Perlis 01000, Malaysia.
C3 GH Asachi Technical University
RP Vizureanu, P (corresponding author), Tech Univ Gheorghe Asachi Iasi Romania,
Dept Technol & Equipments Mat Proc, Blvd Mangeron 51, Iasi 700050, Romania.
EM peviz2002@yahoo.com
RI Abdullah, Mohd Mustafa Al Bakri/C-9844-2012; Tahir, Muhammad Faheem
Mohd/AAT-9691-2021; BURDUHOS-NERGIS, DUMITRU DORU/O-7206-2019; NERGIS,
DUMITRU DORU BURDUHOS/Z-3888-2019; VIZUREANU, Petrica/E-5108-2010
OI Abdullah, Mohd Mustafa Al Bakri/0000-0002-9779-8586; BURDUHOS-NERGIS,
DUMITRU DORU/0000-0002-2716-1328; NERGIS, DUMITRU DORU
BURDUHOS/0000-0002-2716-1328; VIZUREANU, Petrica/0000-0002-3593-9400
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NR 68
TC 30
Z9 32
U1 2
U2 12
PU IOP PUBLISHING LTD
PI BRISTOL
PA DIRAC HOUSE, TEMPLE BACK, BRISTOL BS1 6BE, ENGLAND
SN 1757-8981
J9 IOP CONF SER-MAT SCI
PY 2018
VL 374
AR 012019
DI 10.1088/1757-899X/374/1/012019
PG 10
WC Materials Science, Multidisciplinary; Materials Science,
Characterization & Testing
WE Conference Proceedings Citation Index - Science (CPCI-S)
GA BL0UX
UT WOS:000446775900019
OA gold
DA 2023-12-05
ER
PT J
AU Zhang, L
Chen, B
AF Zhang, Lei
Chen, Bing
TI Hydration and Properties of Slag Cement Activated by Alkali and Sulfate
LA English
DT Article
DE Slag cement; Alkali and sulfate; Setting time; Strength; Microstructure
ID BLAST-FURNACE SLAG; MINERAL ADMIXTURE; PORE STRUCTURE; CONCRETE; PASTES;
SI-29; TEMPERATURE; DURABILITY; STRENGTH; PHASES
AB In this paper, the results of a study on the influence of sodium hydroxide,
calcium hydroxide, aluminum hydroxide, sodium sulfate, calcium sulfate, and calcium
sulfate dihydrate as activators on the setting time and mechanical properties of
slag-cement mixtures are presented. The results obtained show that the sulfate is
more effective in activating the activity of the slag cement than the other
chemical activators. Specimens prepared from calcium sulfate, blast-furnace slag,
and ordinary portland cement exhibit better mechanical performance compared to
admixtures prepared from other mix ratios. The sulfate ions from sulfates would
react with Ca2+ from slag cement and form the reaction product ettringite. However,
the addition of sodium hydroxide seems ineffective in activating the slag cement.
Successive addition of sodium hydroxide deteriorates the mechanical strength of the
slag cement. The reaction kinetics are also studied by examining the hydration
products of slag-blended cement paste through the technologies of X-ray diffraction
(XRD), scanning electron microscopy (SEM), and nuclear magnetic resonance
spectroscopy (NMR). Those experimental results provide detailed insights into the
understanding of how the activators influence the hydration products of slag-
blended cement and structural models of calcium silicate hydrates (C-S-H). (C) 2017
American Society of Civil Engineers.
C1 [Zhang, Lei] Tianjin Chenjian Univ, Sch Mat Sci & Engn, Jinjing Rd 26, Tianjin
[Chen, Bing] Shanghai Jiao Tong Univ, Dept Civil Engn, Dongchuan Rd 800,
C3 Tianjin Chengjian University; Shanghai Jiao Tong University
RP Chen, B (corresponding author), Shanghai Jiao Tong Univ, Dept Civil Engn,
Dongchuan Rd 800, Shanghai 200240, Peoples R China.
EM hntchen@sjtu.edu.cn
RI Chen, Bing/AAJ-5203-2020
FX This research work was financially supported by the National Natural
Science Foundation of China, Grant No. 51378309.
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NR 34
TC 30
Z9 32
U1 5
U2 74
PI RESTON
SN 0899-1561
EI 1943-5533
PD SEP
PY 2017
VL 29
IS 9
AR 04017091
DI 10.1061/(ASCE)MT.1943-5533.0001879
PG 8
GA EZ3HD
UT WOS:000404601100002
DA 2023-12-05
ER
PT J
AU Xue, NN
Zhang, YM
Liu, T
Huang, J
Zheng, QS
AF Xue, Nan-nan
Zhang, Yi-min
Liu, Tao
Huang, Jing
Zheng, Qiu-shi
TI Effects of hydration and hardening of calcium sulfate on muscovite
dissolution during pressure acid leaching of black shale
LA English
DT Article
DE Black shale; Muscovite dissolution; Hydration and hardening; CaSO4
ID STONE COAL; EXTRACTING VANADIUM; MECHANISM; DECOMPOSITION; NUCLEATION;
SYNGENITE; SYSTEM; GYPSUM; RATES; SLAG
AB In the conventional process of oxygen pressure acid leaching of black shale,
vanadium extraction depends on acid attack to muscovite, resulting in high acid
consumption and a long leaching time. The two problems significantly reduce
equipment life, increase production costs, and decrease production efficiency. To
solve these problems, hydration and hardening of calcium sulfate were introduced to
promote muscovite cracking, increasing the exchange reaction rate of hydrogen ion
to aluminum ion. This paper investigated the effect of hydration and hardening of
calcium sulfate on calcium sulfate growth and muscovite dissolution, exploring
interactions between calcium sulfate and muscovite. Results indicate that in
stress-damaged muscovite structure, propagation of ductile cracks in muscovite
particles increases their specific surface area and weakens muscovite structural
strength. These effects allow muscovite to dissolve much more easily during the
pressure acid leaching process. The hydration and hardening of calcium sulfate
crystals can thus facilitate muscovite dissolution. (C) 2017 Elsevier Ltd. All
rights reserved.
C1 [Xue, Nan-nan; Zhang, Yi-min; Liu, Tao; Huang, Jing; Zheng, Qiu-shi] Wuhan Univ
Sci & Technol, Sch Resource & Environm Engn, Wuhan 430081, Peoples R China.
[Xue, Nan-nan; Zhang, Yi-min; Liu, Tao; Huang, Jing] Hubei Prov Engn Technol Res
Ctr High Efficient Cl, Wuhan 430081, Peoples R China.
[Zhang, Yi-min; Liu, Tao; Huang, Jing; Zheng, Qiu-shi] Hubei Collaborat Innovat
Ctr High Efficient Utili, Wuhan 430081, Peoples R China.
C3 Wuhan University of Science & Technology
RP Zhang, YM (corresponding author), Wuhan Univ Sci & Technol, Sch Resource &
Environm Engn, Wuhan 430081, Peoples R China.
EM zym126135@126.com
Project in the National Science & Technology Pillar Program of China
[2015BAB18B01]
FX This research was funded by the National Natural Science Foundation of
China (No. 51404174 and No. 51474162) and the Project in the National
Science & Technology Pillar Program of China (No. 2015BAB18B01).
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TC 30
Z9 30
U1 1
U2 36
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD APR 15
PY 2017
VL 149
BP 989
EP 998
DI 10.1016/j.jclepro.2017.02.152
PG 10
& Ecology
GA EX6CO
UT WOS:000403330200087
DA 2023-12-05
ER
PT J
AU He, SP
Chen, GJ
Guo, YT
Shen, BY
Wang, Q
AF He, Shengping
Chen, Gujun
Guo, Yintao
Shen, Boyi
Wang, Qian
TI Morphology Control for Al2O3 Inclusion Without Ca
Treatment in High-Aluminum Steel
LA English
DT Article
ID LIQUID-IRON; DEOXIDATION EQUILIBRIUM; NONMETALLIC INCLUSIONS;
CAO-SIO2-AL2O3 SLAGS; KILLED STEEL; CALCIUM; DISSOLUTION; IMPROVEMENT;
MELTS
AB Nozzle blockage is a major problem during continuous casting of Al-containing
steel. Herein, we analyzed the thermodynamic equilibrium behavior between aluminum
and oxygen in steel at 1873 K (1600 degrees C) and demonstrated that, the dissolved
[O] initially decreases with increasing the dissolved [Al] until approximately 0.1
wt pct [Al], and after that, the dissolved [O] increases with dissolved [Al]. Thus,
for high-aluminum steel with 1.0 wt pct dissolved [Al], the precipitation of Al2O3
inclusion can be avoided during cooling from deoxidation temperature to the
liquidus temperature, if the actual dissolved [O] can be kept from increasing when
the dissolved [Al] further increases from 0.1 to 1.0 wt pct. Hence, a method of
inclusion control for high-aluminum steel without traditional Ca treatment
technology was proposed based on the thermodynamic analysis. Industrial tests
confirmed that low-melting point Ca-aluminate inclusions were observed typically
through a slag washing with SiO2-minimized high-basicity slag during tapping,
accompanied by two-step Al-adding process for production of high-aluminum steel.
Moreover, there was no nozzle clogging occurred for five heats of continuous
casting. (C) The Minerals, Metals & Materials Society and ASM International 2014
C1 [He, Shengping; Chen, Gujun; Guo, Yintao; Shen, Boyi; Wang, Qian] Chongqing
Univ, Coll Mat Sci & Engn, Chongqing 400044, Peoples R China.
RP He, SP (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
EM heshp@cqu.edu.cn
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NR 55
TC 30
Z9 34
U1 7
U2 37
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD APR
PY 2015
VL 46
IS 2
BP 585
EP 594
DI 10.1007/s11663-014-0264-z
PG 10
Engineering
GA CE5GW
UT WOS:000351860300009
OA Bronze
DA 2023-12-05
ER
PT J
AU Zhang, GH
Chou, KC
AF Zhang, Guo-Hua
Chou, Kuo-Chih
TI Influence of Al2O3/SiO2 Ratio on
Viscosities of CaO-Al2O3-SiO2 Melt
LA English
DT Article
DE CaO-Al2O3-SiO2; viscosity; degree of polymerization; Arrhenius law;
model
ID ALUMINOSILICATE MELTS; SLAGS; ALUMINUM; ALKALI; SYSTEM; OXIDES; MODEL
AB The influence of Al2O3/SiO2 ratio on viscosity of CaO-Al2O3/SiO2 melt was
investigated by the rotating cylinder method in this study. Three groups of
compositions with different CaO contents of 0.35, 0.4 and 0.45 were studied. From
the experimental results, it was concluded that viscosity always first increases
and then decreases as gradually increasing Al2O3/SiO2 ratio. The appearance of
viscosity maximum may be resulted from the opposite variation tendencies of mean
bond strength and the degree of polymerization of melt with Al2O3/SiO2 ratio. When
substituting SiO2 by Al2O3, the mean bond strength decreases because of the weak
Al-O bond relative to Si-O bond, which decreases viscosity; while the degree of
polymerization is enhanced by the charge compensation effect of Al3+ ion, which
increases viscosity. Our new proposed viscosity model can well describe the
viscosity variation of CaO-Al2O3-SiO2 melt.
C1 [Zhang, Guo-Hua; Chou, Kuo-Chih] Univ Sci & Technol Beijing, State Key Lab Adv
Met, Beijing, Peoples R China.
[Zhang, Guo-Hua; Chou, Kuo-Chih] Univ Sci & Technol Beijing, Sch Met & Ecol
Engn, Beijing, Peoples R China.
Technology Beijing
RP Zhang, GH (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
Met, Beijing, Peoples R China.
EM ghzhang_ustb@163.com
RI Zhang, Guo-Hua/AAM-7264-2021; Zhang, He/GXN-0028-2022
FU China Postdoctoral Science Foundation [2012M510318]; Chinese Natural
Science Foundation [51174022, 51234001]
FX The authors wish to express their gratitude to Professor Fumitaka
Tsukihashi (University of Tokyo) for his valuable comments. Thanks are
also given to the Financial supports from China Postdoctoral Science
Foundation (2012M510318) and the Chinese Natural Science Foundation
(51174022 and 51234001).
CR BILLS PM, 1963, J IRON STEEL I, V201, P133
Johannsen F., 1959, Z ERZBERG METALLHUT, V12, P272
KITA Y, 2001, J HIGH TEMP SOC, V27, P144
0090-y
10.1051/metal/196057020149
2916.1948.tb14290.x
Mysen B. O., 1988, STRUCTURE PROPERTIES, P85
SCARFE CM, 1986, AM MINERAL, V71, P767
Susa M, 2005, GLASS TECHNOL, V46, P55
Yasukouchi T, 1999, TETSU TO HAGANE, V85, P571
Zhang GH, 2012, J MIN METALL B, V48, P1, DOI 10.3901/JME.2012.08.001
Zhang G. H., 2012, J MIN MET B IN PRESS
Zhang GH, 2012, METALL MATER TRANS B, V43, P841, DOI 10.1007/s11663-012-9668-9
Zhang GH, 2012, METALL MATER TRANS B, V43, P849, DOI 10.1007/s11663-012-9674-y
Zhang GH, 2012, METALL MATER TRANS B, V43, P64, DOI 10.1007/s11663-011-9589-z
NR 19
TC 30
Z9 32
U1 5
U2 37
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2013
VL 53
IS 1
BP 177
EP 180
PG 4
GA 102HC
UT WOS:000315834700026
OA gold
DA 2023-12-05
ER
PT J
AU Fruehan, RJ
Li, Y
Carkin, G
AF Fruehan, RJ
Li, Y
Carkin, G
TI Mechanism and rate of reaction of Al2O, Al, and CO vapors
with carbon
LA English
DT Article
AB During the production of aluminum by carbothermic reduction, large quantities of
Al2O and Al vapor are generated. For the process to be economical, the aluminum and
energy associated with these species must be captured and used in the process. This
is accomplished by reacting them with carbon to form Al4C3. The mechanism and rate
of the reactions of gas containing Al and Al2O with various forms of carbon was
studied. The Al2O-Al-CO gas was generated by reacting an Al4C3-Al2O3 melt with
carbon at high temperatures (2000 degreesC to 2050 degreesC). The gas then reacted
with carbon at lower temperatures (1900 degreesC to 1950 degreesC). The only form
of carbon that reacted extensively, forming Al4C3, was wood charcoal; with other
forms of carbon, such as metallurgical coke and petroleum coke, primarily only
Al2O3 condensed on the surface formed. The rate of formation of Al4C3 on wood
charcoal was found to be controlled by the diffusion of Al2O and Al through the
Al4C3 product layer, and their effective diffusivities were estimated to be 0.82
and 1.31 cm(2)/s, respectively. Over 90 pct of the carbide is formed by Al2O and
only 10 pct by Al vapor. When an Al4C3-Al2O3 dense slag was formed on the charcoal
at lower temperatures (1920 degreesC to 1930 degreesC) and then reacted at a higher
temperature, it appears that the slag and carbon reacted to form Al4C3 relatively
fast. The volume of Al4C3 formed is much greater than that of the original carbon.
It is believed that this is the reason the other forms of carbon with lower
porosity (25 pct vs 60 pct) did not react significantly. Any amount of Al4C3 formed
would quickly fill the pores of the more dense carbon, stopping any further
reaction.
US Steel Res Ctr, Monroeville, PA 15146 USA.
RP Fruehan, RJ (corresponding author), Carnegie Mellon Univ, Dept Mat Sci & Engn,
EM fruehan@cmu.edu
CR BRUNO M, LIGHT METALS 2003, P395
Motzfeldt K., 1979, LIGHT METALS 1979, P411
PELTON AD, FACTSAGE
QUI C, 1998, J ALLOY COMPD, V213, P55
NR 4
TC 30
Z9 36
U1 1
U2 9
PU MINERALS METALS MATERIALS SOC
PI WARRENDALE
PA 184 THORN HILL RD, WARRENDALE, PA 15086 USA
SN 1073-5615
PD AUG
PY 2004
VL 35
IS 4
BP 617
EP 623
DI 10.1007/s11663-004-0002-z
PG 7
Engineering
GA 841OH
UT WOS:000222939500002
DA 2023-12-05
ER
PT J
AU Mymrin, VA
Vázquez-Vaamonde, AJ
AF Mymrin, VA
Vázquez-Vaamonde, AJ
TI Red mud of aluminium production waste as basic component of new
construction materials
SO WASTE MANAGEMENT & RESEARCH
LA English
DT Article
DE red mud; solid industrial wastes; dump ferrous slag; activator;
properties; construction materials
AB The work presented here shows the possibility of using the red mud waste from
the Bayer process used for aluminium production as the main component of new
construction materials. It describes some recent experiments lasting 180 days as
well as some I year old samples. The best part of materials used are industrial
wastes, but some of them contain small (no more, the 2%) additions of CaO or
Portland Cement (PC) to increase the strengthening rate of the samples. The high
strength values of these materials allow their use as new materials for road and
airfields bases, levee core, dumps, foundations, etc. They can also be used to make
bricks, tiles, and similar items. In addition to the economic factors, these
materials are very easy to use and no new residues are generated.
The results of the heavy metal leaching tests, not included in this paper, show
very low levels of their leachability in acid solutions, far below the demands of
the Spanish environmental standards. This can be explained by the strong chemical
binding of heavy metals in practically insoluble chemical compositions.
C1 CSIC, CENIM, Madrid 28040, Spain.
CIENTEC, Porto Alegre, RS, Brazil.
C3 Consejo Superior de Investigaciones Cientificas (CSIC); Centro Nacional
de Investigaciones Metalurgicas (CENIM)
RP Vázquez-Vaamonde, AJ (corresponding author), CSIC, CENIM, Av Gregorio del Amo 8,
Madrid 28040, Spain.
CR FERNANDEZ C, 1996, P LIGHT MET C ANN CA, P99
KANEV R, 1990, P 6 YUG INT S AL BAU, P18
KIRKPATRICK DB, 1996, P LIGHT MET C AN CAL, P75
Mymrin V., 1998, REV METAL MADRID, P441
MYMRIN VA, 1978, STRATTO GEOLOGIA APP, V13, P293
MYMRIN VA, 1998, Patent No. 9802248
MYMRIN VA, 1981, 7 KRAIOW K MECH GRUN, P498
MYMRIN VA, 1994, P 3 INT C OPF CHEM N, P108
Sujana M. G., 1996, P LIGHT METL C AN CA, P93
NR 9
TC 30
Z9 33
U1 0
U2 30
PU I W M BUSINESS SERVICES LTD
PI NORTHAMPTON
PA 9 SAXONS COURT, ST PETER'S GARDEN, NORTHAMPTON NN1 1SX, ENGLAND
SN 0734-242X
J9 WASTE MANAGE RES
JI Waste Manage. Res.
PD OCT
PY 2001
VL 19
IS 5
BP 465
EP 469
DI 10.1177/0734242X0101900512
PG 5
GA 508YU
UT WOS:000173118000011
PM 11954733
DA 2023-12-05
ER
PT J
AU Wang, F
Long, GC
Bai, M
Wang, JL
Zhou, JL
Zhou, X
AF Wang, Fan
Long, Guangcheng
Bai, Min
Wang, Jilin
Zhou, John L.
Zhou, Xiang
TI Application of electrolytic manganese residues in cement products
through pozzolanic activity motivation and calcination
LA English
DT Article
DE Calcination; Electrolytic manganese residue; Pozzolanic activity;
Hazard-free treatment; Mortar stabilization
ID SOLIDIFICATION/STABILIZATION; STRENGTH; AMMONIA; SLAG; MUD
AB Degradation in grade of manganese ore aggravates the complexity of electrolytic
manganese residue (EMR). Calcination is one of the most practical pretreatment
methods to improve EMR activity and dispose the hazardous elements. In this paper,
the evolution of mineral phase, pozzolanic activity, pore structure and harmful
components induced by calcining EMR was investigated. The results show that EMR
calcined at 800 degrees C has the strength activity index (SAI) of 84.79 at 28 d,
which is attributed to the decomposition of dihydrate gypsum and the formation of
activated calcium, silicon and aluminum oxide. The formation of beta-type
hemihydrate gypsum increases the pozzolan activity, while the latter is limited by
the formation of stable Mn-spinel (Mn3O4) and Mnhercynite (MnFe2O4). In the EMR-
doped mortar matrix, the production of a large amount of ettringite due to the
existence of gypsum, as well as common C-S-H, portlandite and AFm, which strongly
verify the pozzolanic activity of EMR. Leaching results show that Mn2+ and NH4+-N
could not be eliminated completely at low temperature (<600 <degrees>C), but could
be completely stabilized in the alkaline environment provided by the cement. The
Mn2+ and NH4+-N levels in mortar are fully below the regulatory standards when
calcinated above 800 degrees C. All heavy metals are fixed in the cement and
calcination process, ensuring the cleaner utilization of EMR in building materials.
C1 [Wang, Fan; Long, Guangcheng; Bai, Min; Wang, Jilin; Zhou, John L.; Zhou, Xiang]
Cent South Univ, Sch Civil Engn, 68 South Shaoshan Rd, Changsha 410075, Hunan,
Peoples R China.
[Zhou, John L.] Univ Technol Sydney, Ctr Green Technol, Sch Civil & Environm
Engn, Sydney, NSW 2007, Australia.
C3 Central South University; University of Technology Sydney
RP Long, GC (corresponding author), Cent South Univ, Sch Civil Engn, 68 South
Shaoshan Rd, Changsha 410075, Hunan, Peoples R China.
EM wn2020@csu.edu.cn; longguangcheng@csu.edu.cn; minbai2021@163.com;
193571717@qq.com; junliang.zhou@uts.edu.au; junliang.zhou@uts.edu.au
RI wang, fan/HNS-6617-2023; Zhou, John L./E-7610-2011; bai,
min/GRJ-6447-2022
OI wang, fan/0000-0002-6417-155X; Zhou, John L./0000-0003-1393-1608; Wang,
Jilin/0000-0002-6093-0272
FU Hunan Province Key Field RD Program [2020wk2005]; Postgraduate
Scholarship, Central South University, Changsha, China
FX The authors appreciate the financial support from Hunan Province Key
Field R&D Program (Grant No.2020wk2005) , and the Postgraduate
Scholarship, Central South University, Changsha, China.
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10.1016/j.conbuildmat.2019.06.009
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Zhou YX, 2021, CONSTR BUILD MATER, V294, DOI 10.1016/j.conbuildmat.2021.123533
NR 58
TC 29
Z9 30
U1 9
U2 69
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAR 1
PY 2022
VL 338
AR 130629
DI 10.1016/j.jclepro.2022.130629
EA JAN 2022
PG 15
& Ecology
GA ZZ0XH
UT WOS:000772999300005
DA 2023-12-05
ER
PT J
AU Valeev, D
Zinoveev, D
Kondratiev, A
Lubyanoi, D
Pankratov, D
AF Valeev, Dmitry
Zinoveev, Dmitry
Kondratiev, Alex
Lubyanoi, Dmitry
Pankratov, Denis
TI Reductive Smelting of Neutralized Red Mud for Iron Recovery and Produced
Pig Iron for Heat-Resistant Castings
SO METALS
LA English
DT Article
DE red mud; Mossbauer spectroscopy; reductive smelting; thermodynamic
modeling; slag; pig iron
ID BAUXITE RESIDUE; MAGNETIC-PROPERTIES; SOLVENT-EXTRACTION; MINING WASTE;
MOSSBAUER; NANOPARTICLES; ALUMINA; ALKALI; ACID; COMPOSITE
AB The chemical and mineral composition of the red mud from the Ural Aluminum Plant
were studied by XRF, XRD, and Mossbauer spectroscopy. Experiments on reductive
smelting of red mud were carried out in a range of temperatures (1650-1750 degrees
C) to recover iron from the aluminum production waste with maximum efficiency. It
was found that it is possible to obtain pig iron with a high content of titanium,
phosphorus, and vanadium, and low sulfur content. The efficiency of iron recovery
at 1750 degrees C was found to be around 98%. Thermodynamic calculations were
carried out to assist in finding the optimal conditions for the process (e.g.,
carbon content, furnace temperature, slag liquidus temperature). It was also found
that the pig iron phase obtained at 1650 to 1700 degrees C is not separated from
the slag phase into ingot compared with the sample obtained at 1750 degrees C. Pig
iron obtained at 1750 degrees C can be used to produce molds for the steel-casting
equipment.
C1 [Valeev, Dmitry] Russian Acad Sci, AA Baikov Inst Met & Mat Sci, IP Bardin Lab
Problems Met Complex Ores, 49 Leninsky Prospect, Moscow 119334, Russia.
[Valeev, Dmitry; Kondratiev, Alex] Natl Univ Sci & Technol MISIS, Sci Res Ctr
Thermochem Mat, 4 Leninsky Prospect, Moscow 119049, Russia.
[Zinoveev, Dmitry] Russian Acad Sci, AA Baikov Inst Met & Mat Sci, Lab Phys Chem
& Iron Ore Proc Technol, 49 Leninsky Prospect, Moscow 119334, Russia.
[Lubyanoi, Dmitry] Kuzbass State Tech Univ, 19a Nogradskaya St, Prokopyevsk
653033, Russia.
[Pankratov, Denis] Lomonosov Moscow State Univ, Dept Chem, 1 Leninsky Gory,
Moscow 119991, Russia.
Science (IMET RAS); National University of Science & Technology (MISIS);
Russian Academy of Sciences; Baikov Institute of Metallurgy & Materials
Science (IMET RAS); Kuzbass State Technical University; Lomonosov Moscow
State University
RP Valeev, D (corresponding author), Russian Acad Sci, AA Baikov Inst Met & Mat
Sci, IP Bardin Lab Problems Met Complex Ores, 49 Leninsky Prospect, Moscow 119334,
Russia.; Valeev, D (corresponding author), Natl Univ Sci & Technol MISIS, Sci Res
Ctr Thermochem Mat, 4 Leninsky Prospect, Moscow 119049, Russia.
EM dvaleev@imet.ac.ru; dzinoveev@imet.ac.ru; al.v.kondratiev@gmail.com;
lubjanoy@yandex.ru; pankratov@radio.chem.msu.ru
RI Zinoveev, Dmitry/I-2795-2017; Kondratiev, Alex/G-9598-2015; Valeev,
Dmitry/A-9683-2016; Pankratov, Denis/J-3613-2012; Kondratiev,
Alex/ABH-5376-2020
OI Zinoveev, Dmitry/0000-0003-4520-4659; Kondratiev,
Alex/0000-0001-6658-0421; Valeev, Dmitry/0000-0002-8820-7502; Pankratov,
Denis/0000-0001-6557-2753; Kondratiev, Alex/0000-0001-6658-0421
FU Program of Basic research of the Presidium of Russian Academy of Science
[39, AAA-A18-118031690039-9]; Ministry of Education and Science of the
Russian Federation [11.7971.2017/6.7]
FX The present study was funded by Program of Basic research of the
Presidium of Russian Academy of Science No 39 "Fundamentals and
energy-efficient, resource-saving, innovative technologies of mineral
processing, utilization of industrial and household waste" (Grant No.
AAA-A18-118031690039-9). Alex Kondratiev is financially supported by the
Ministry of Education and Science of the Russian Federation in the
framework of the basic part of the state program 'Organisation of the
Research Work' for higher educational institutions in 2017-2019 no.
11.7971.2017/6.7.
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NR 62
TC 29
Z9 30
U1 1
U2 24
PU MDPI
PI BASEL
EI 2075-4701
J9 METALS-BASEL
JI Metals
PD JAN
PY 2020
VL 10
IS 1
AR 32
DI 10.3390/met10010032
PG 20
Engineering
GA KQ3LK
UT WOS:000516827800032
OA gold
DA 2023-12-05
ER
PT J
AU Liu, WH
Li, H
Zhu, HM
Xu, PJ
AF Liu, Wenhuan
Li, Hui
Zhu, Huimei
Xu, Pinjing
TI Properties of a Steel Slag-Permeable Asphalt Mixture and the Reaction of
the Steel Slag-Asphalt Interface
SO MATERIALS
LA English
DT Article
DE FTIR; asphalt; steel slag; chemical reaction; asphalt-steel slag
interface
ID PERFORMANCE; MECHANISM; REMOVAL; SO2; XRD
AB Steel slag is an industrial solid waste with the largest output in the world. It
has the characteristics of wear resistance, good particle shape, large porosity,
etc. At the same time, it has good adhesion characteristics with asphalt. If steel
slag is used in asphalt pavement, it not only solves the problem of insufficient
quality aggregates in asphalt concrete, but can also give full play to the high
hardness and high wear resistance of steel slag to improve the performance of
asphalt pavement. In this study, a steel slag aggregate was mixed with road
petroleum asphalt to prepare a permeable steel slag-asphalt mixture, which was then
compared with the permeable limestone-asphalt mixture. According to the Technical
Regulations for Permeable Asphalt Pavement (CJJT 190-2012), the permeability, water
stability, and Marshall stability of the prepared asphalt mixtures were tested and
analyzed. In addition, the high-temperature stability and expansibility were
analyzed according to the Experimental Regulations for Highway Engineering Asphalt
and Asphalt Mixture (JTG E20-2011). The chemical composition of the steel slag was
tested and analyzed by X-ray fluorescence spectrometer (XRF). The mineral
composition of the steel slag was tested and analyzed by X-ray diffractometer
(XRD). The asphalt was analyzed by Fourier transform infrared spectroscopy (FTIR).
The results show that the steel slag asphalt permeable mixture had good
permeability, water stability, and Marshall stability, as well as good high-
temperature stability and a low expansion rate. The main mineral composition was
ferroferric oxide, the RO phase (RO phase is a broad solid solution formed by
melting FeO, MgO, and other divalent metal oxides such as MnO), dicalcium silicate,
and tricalcium silicate. In the main chemical composition of steel slag, there was
no chemical reaction between aluminum oxide, calcium oxide, silicon dioxide, and
asphalt, while ferric oxide chemically reacted with asphalt and formed new
organosilicon compounds. The main mineral composition of the steel slag (i.e.,
triiron tetroxide, dicalcium silicate, and tricalcium silicate) reacted chemically
with the asphalt and produced new substances. There was no chemical reaction
between the RO phase and asphalt.
C1 [Liu, Wenhuan; Li, Hui; Zhu, Huimei; Xu, Pinjing] Xian Univ Architecture &
Technol, Coll Mat Sci & Engn, Xian 710055, Shaanxi, Peoples R China.
[Liu, Wenhuan] Shaanxi Key Lab Architectural Sci & Technol, Xian 710055,
Shaanxi, Peoples R China.
C3 Xi'an University of Architecture & Technology
RP Liu, WH; Li, H (corresponding author), Xian Univ Architecture & Technol, Coll
Mat Sci & Engn, Xian 710055, Shaanxi, Peoples R China.; Liu, WH (corresponding
author), Shaanxi Key Lab Architectural Sci & Technol, Xian 710055, Shaanxi, Peoples
R China.
EM liuwenhuan@xauat.edu.cn; sunshineli@vip.sina.com; zhuhuimeitj@163.com;
xpj6100@163.com
FU Key Laboratory Project of Shaanxi Education Department [15JS051];
National Key Research and Development Program [2018YFC1903804]; National
FX This work was supported by the Key Laboratory Project of Shaanxi
Education Department (No.15JS051), National Key Research and Development
Program (No. 2018YFC1903804), and the National Natural Science
Foundation of China (No. 50872105).
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NR 23
TC 29
Z9 29
U1 20
U2 79
PU MDPI
PI BASEL
EI 1996-1944
J9 MATERIALS
JI Materials
PD NOV
PY 2019
VL 12
IS 21
AR 3603
DI 10.3390/ma12213603
PG 10
Physics
GA JW1DK
UT WOS:000502798800144
PM 31684050
DA 2023-12-05
ER
PT J
AU Shi, CB
Wang, H
Li, J
AF Shi, Chengbin
Wang, Hui
Li, Jing
TI Effects of Reoxidation of Liquid Steel and Slag Composition on the
Chemistry Evolution of Inclusions During Electroslag Remelting
LA English
DT Article
ID MGO-CENTER-DOT-AL2O3 SPINEL INCLUSIONS; NONMETALLIC INCLUSIONS; TOOL
STEEL; SOLIDIFICATION STRUCTURE; MNS PRECIPITATION; CLEAN STEELS; DIE
STEEL; MO ALLOY; AL-TI; OXIDE
AB Electroslag remelting (ESR) is increasingly used to produce some varieties of
special steels and alloys, mainly because of its ability to provide extreme
cleanliness and an excellent solidification structure simultaneously. In the
present study, the combined effects of varying SiO2 contents in slag and
reoxidation of liquid steel on the chemistry evolution of inclusions and the
alloying element content in steel during ESR were investigated. The inclusions in
the steel before ESR refining were found to be oxysulfides of patch-type (Ca,Mn)S
adhering to a CaO-Al2O3-SiO2-MgO inclusion. The oxide inclusions in both the liquid
metal pool and remelted ingots are CaO-Al2O3-MgO and MgAl2O4 together with CaO-
Al2O3-SiO2-MgO inclusions (slightly less than 30 pct of the total inclusions),
which were confirmed to originate from the reduction of SiO2 from the original
oxide inclusions by dissolved Al in liquid steel during ESR. CaO-Al2O3-MgO and
MgAl2O4 are newly formed inclusions resulting from the reactions taking place
inside liquid steel in the liquid metal pool caused by reoxidation of liquid steel
during ESR. Increasing the SiO2 content in slag not only considerably reduced
aluminum pickup in parallel with silicon loss during ESR, but also suppressed the
decrease in SiO2 content in oxide inclusions. (Ca,Mn)S inclusions were fully
removed before liquid metal droplets collected in the liquid metal pool.
C1 [Shi, Chengbin; Li, Jing] USTB, State Key Lab Adv Met, Beijing 100083, Peoples R
China.
[Wang, Hui] Shougang Res Inst Technol, Beijing 100041, Peoples R China.
C3 University of Science & Technology Beijing; Shougang Group
RP Shi, CB (corresponding author), USTB, State Key Lab Adv Met, Beijing 100083,
Peoples R China.
EM chengbin.shi@ustb.edu.cn
RI Shi, Chengbin/J-1262-2016
OI Shi, Chengbin/0000-0001-8127-3382
National Key Research and Development Program of China [2016YFB0300604]
FX The financial support by the National Natural Science Foundation of
China (Grant Nos. 51504019 and 51774225) and the National Key Research
and Development Program of China (Grant No. 2016YFB0300604) is greatly
acknowledged.
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NR 50
TC 29
Z9 31
U1 2
U2 29
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2018
VL 49
IS 4
BP 1675
EP 1689
DI 10.1007/s11663-018-1296-6
PG 15
Engineering
GA GM8IO
UT WOS:000438469300014
DA 2023-12-05
ER
PT J
AU Kaussen, FM
Friedrich, B
AF Kaussen, F. M.
Friedrich, B.
TI Phase characterization and thermochemical simulation of (landfilled)
bauxite residue ("red mud") in different alkaline processes optimized
for aluminum recovery
SO HYDROMETALLURGY
LA English
DT Article
DE Aluminum recovery; Aluminum extraction; Bauxite residue; Red mud;
Bayer-process; Pedersen-process
ID CANCRINITE; TRANSFORMATION; DESILICATION; SODALITE; SILICA
AB In coherent studies three different processes of hydrometallurgical, alkaline
extraction of aluminum from bauxite residue (BR) are examined and benchmarked
regarding their efficiency on aluminum recovery. The employed processes include a
direct second caustic pressure leaching, a caustic pressure leaching of the slag
produced by reductive smelting of BR with simultaneous pig iron recovery (adapted
"Pedersen-process") and leaching of BR after a sintering stage with sodium
carbonate and further additives including lime and coke. In order to ensure a
direct comparability, all experiments are conducted using the same homogenized BR
from an old industrial landfill. After detailed characterization of the used BR
using XRF chemical analysis, XRD phase analysis, SEM optical analysis and Qemscan
(R) phase analysis/distribution, occurring phase formations during the employed
processes are also calculated and predicted by FactSage (R) simulation software.
The actual phase formation and leachability of the formed aluminum phases are
verified during experiments and a special focus is set on the dissolution of
silicon as major impurity in all processes. It can be shown that aluminum
extraction efficiencies of 90% are still possible but interlinked with massive
silicon dissolution due to the almost complete dissolution of aluminum silicates.
C1 [Kaussen, F. M.; Friedrich, B.] Rhein Westfal TH Aachen, IME Dept Proc Met & Met
Recycling, Intzestr 3, D-52056 Aachen, Germany.
C3 RWTH Aachen University
RP Kaussen, FM (corresponding author), Rhein Westfal TH Aachen, IME Dept Proc Met &
Met Recycling, Intzestr 3, D-52056 Aachen, Germany.
EM fkaussen@ime-aachen.de; bfriedrich@ime-aachen.de
RI Friedrich, Bernd/AAM-7005-2021; Friedrich, Bernd/AAM-7029-2021
OI Friedrich, Bernd/0000-0002-2934-2034
FU German Federal Ministry of Education and Research (BMBF) [033R085A]
FX The project upon which this publication is based is funded by the German
Federal Ministry of Education and Research (BMBF) under project number
033R085A from 2012 to 2016. This publication reflects the views of the
authors only. Special thanks to all project partners, the analytical
laboratory of the School of Geosciences Energy & Mineral Resources,
Department of Mineralogy & Economic Geology for Qemscan analysis, the
Institute of Inorganic Chemistry for XRD analyses, both RWTH Aachen
School of Mining and Metallurgical Engineering, University and National
Technical University of Athens in person of Prof. D. Panias and E.
Balomenos for scientific input and fruitful discussions.
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PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD MAR
PY 2018
VL 176
BP 49
EP 61
DI 10.1016/j.hydromet.2018.01.006
PG 13
GA GA3KK
UT WOS:000428227300007
DA 2023-12-05
ER
PT J
AU Mallapur, VP
Oubagaranadin, JUK
AF Mallapur, Veeresh P.
Oubagaranadin, John U. Kennedy
TI A Brief Review on the Synthesis of Zeolites from Hazardous Wastes
SO TRANSACTIONS OF THE INDIAN CERAMIC SOCIETY
LA English
DT Article
DE Zeolite; Catalyst; Porcelain; Fly ash
ID COAL FLY-ASH; RICE HUSK ASH; NA-A ZEOLITE; ALKALINE HYDROTHERMAL
CONVERSION; PAPER SLUDGE ASH; ZSM-5 ZEOLITE; SOLID-WASTE; REMOVAL;
SILICA; WATER
AB Zeolite is a versatile and environmentally important micro-porous material which
can be synthesized using inorganic wastes like fly ash, porcelain wastes, natural
clays, rice husk ash and also from its chemical precursors. Silica and alumina are
the source materials for the synthesis of zeolites. Various industries produce
hazardous inorganic wastes that are rich in silica and alumina, and its production
rate worldwide is enormous. Majority of these wastes are dumped in landfills and
only a very small percentage is reutilized. The cost of synthesis of zeolite from
inorganic waste materials is very less when compared to synthesis from its chemical
precursors. Zeolite synthesis from such hazardous material has shown promising and
versatile industrial applications. This paper gives an overview of zeolite
synthesis from hazardous inorganic wastes such as fly ash, municipal solid wastes,
waste metallic residues, lithium slag, agro wastes, porcelain wastes, waste LCD
panel glass, waste kaolin from industry, windshield waste, cupola slag with
aluminium sludge and waste stone cake.
C1 [Mallapur, Veeresh P.; Oubagaranadin, John U. Kennedy] PDA Coll Engn, Dept Ceram
& Cement Technol, Gulbarga 585102, Karnataka, India.
C3 Poojya Dodappa Appa College of Engineering
RP Oubagaranadin, JUK (corresponding author), PDA Coll Engn, Dept Ceram & Cement
Technol, Gulbarga 585102, Karnataka, India.
EM ju_kennedy@yahoo.co.in
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NR 95
TC 29
Z9 32
U1 4
U2 83
PU INDIAN CERAMIC SOC
PI KOLKATA
PA CENTRAL GLASS & CERAMIC RES INST, KOLKATA, 700 032, INDIA
SN 0371-750X
EI 2165-5456
J9 T INDIAN CERAM SOC
JI Trans. Indian Ceram. Soc.
PY 2017
VL 76
IS 1
BP 1
EP 13
DI 10.1080/0371750X.2016.1231086
PG 13
GA ES5IG
UT WOS:000399571000001
DA 2023-12-05
ER
PT J
AU Wu, T
He, SP
Zhu, LL
Wang, Q
AF Wu, Ting
He, Shengping
Zhu, Lilong
Wang, Qian
TI Study on Reaction Performances and Applications of Mold Flux for
High-Aluminum Steel
SO MATERIALS TRANSACTIONS
LA English
DT Article
DE mold fluxes; high-aluminum steel; reaction performance; industry
application
AB During the continuous ecasting of high-aluminum steel, important components of
the mold flux can be easily reduced by the aluminum in the molten steel.
Consequently, the mold flux performance is deteriorated, impeding the smooth
running of the continuous casting and affecting the quality of the cast slab. To
solve this problem, thermodynamic calculations and laboratorial crucible
experiments were performed to investigate the reduction of different mold fluxes by
the aluminum in molten steel. Plant trials based on the laboratory studies were
performed. It was found that SiO2, MnO, Na2O and B2O3 reacted with the aluminum in
molten steel, while CaO, CaF2, MgO, Li2O and BaO did not. Since the composition
contents of in CaO-Al2O3-based mold flux were changed only slightly after
steel/slag interfacial reactions, a stable CaO-Al(2)O(3-)based mold flux was tested
in industry production. The application effect of this stable mold flux was very
good.
C1 [Wu, Ting; He, Shengping; Zhu, Lilong; Wang, Qian] Chongqing Univ, Coll Mat Sci
& Engn, Chongqing 400044, Peoples R China.
RP He, SP (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
EM heshp@cqu.edu.cn
FU Chongqing Research Program of Foundation and Advanced Technology
[cstc2013jcyjA50003]; Fundamental Research Funds for the Central
Universities in China [CDJZR11130004]
FX The authors would like to deeply appreciate the fund from Chongqing
Research Program of Foundation and Advanced Technology (Project No.
cstc2013jcyjA50003) and the Fundamental Research Funds for the Central
Universities in China (Project No. CDJZR11130004).
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NR 16
TC 29
Z9 32
U1 2
U2 13
PU JAPAN INST METALS & MATERIALS
PI SENDAI
PA 1-14-32, ICHIBANCHO, AOBA-KU, SENDAI, 980-8544, JAPAN
SN 1345-9678
EI 1347-5320
J9 MATER TRANS
JI Mater. Trans.
PD JAN
PY 2016
VL 57
IS 1
BP 58
EP 63
DI 10.2320/matertrans.M2015311
PG 6
Engineering
GA DF6CU
UT WOS:000371444200012
OA Bronze
DA 2023-12-05
ER
PT J
AU Yan, W
Chen, W
Yang, Y
Lippold, C
McLean, A
AF Yan, W.
Chen, W.
Yang, Y.
Lippold, C.
McLean, A.
TI Effect of CaO/Al2O3 ratio on viscosity and
crystallisation behaviour of mould flux for high Al non-magnetic steel
LA English
DT Article
DE High aluminium; Non-magnetic steel; Mould flux; CaO/Al2O3; Viscosity;
Crystallisation
ID HEAT-TRANSFER; SLAG; B2O3
AB In order to facilitate the development of CaO-Al2O3 based mould flux for casting
high aluminium, non-magnetic steel, the effect of CaO/Al2O3 ratios from 0.6 to 3.2
on viscosity and crystallisation characteristics were investigated with the aid of
a rotational viscometer, Fourier transform infrared spectroscopy, a single hot
thermocouple technique and X-ray diffraction analysis. The results showed that, at
temperatures above 1543 K (1270 degrees C), the viscosity first decreased and then
became stable with increase in the CaO/Al2O3 ratio. At temperatures below 1543 K
(1270 degrees C), the viscosity again first decreased but then increased, with the
CaO/Al2O3 ratio. This viscosity behaviour can be attributed to changes in the
network structure characteristics and the precipitation of solid particles within
the liquid flux. Increase in the CaO/Al2O3 ratio also first inhibited and then
enhanced crystallisation as demonstrated by the changes in initial crystallisation
temperatures and incubation times. The X-ray diffraction results confirmed that, at
both low and high CaO/Al2O3 ratios, the dominant precipitates were compounds with
high melting points. On the other hand, with CaO/Al2O3 ratios in the midrange, the
dominant precipitates were compounds with relatively low melting temperatures. It
is concluded that mould flux with a CaO/Al2O3 ratio in the range 1.1-1.6 is the
most appropriate for casting high aluminium, non-magnetic steels.
C1 [Yan, W.; Chen, W.] Univ Sci & Technol Beijing, State Key Lab Adv Met, Beijing
[Yan, W.; Yang, Y.; McLean, A.] Univ Toronto, Dept Mat Sci & Engn, Toronto, ON
M5S 3E4, Canada.
[Lippold, C.] Qingdao Stollberg & Samil Co Ltd, Qingdao 266300, Peoples R China.
EM yanweimetal@gmial.com
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TC 29
Z9 31
U1 1
U2 20
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD OCT
PY 2015
VL 42
IS 9
BP 698
EP 704
DI 10.1179/1743281215Y.0000000024
PG 7
GA CZ3VD
UT WOS:000367031200008
DA 2023-12-05
ER
PT J
AU Schafföner, S
Aneziris, CG
Berek, H
Hubálková, J
Rotmann, B
Friedrich, B
AF Schaffoener, Stefan
Aneziris, Christos G.
Berek, Harry
Hubalkova, Jana
Rotmann, Bjoern
Friedrich, Bernd
TI Corrosion behavior of calcium zirconate refractories in contact with
titanium aluminide melts
LA English
DT Article
DE Refractories; Calcium zirconate; Titanium aluminides; Vacuum induction
melting; Electron backscatter diffraction
ID ELECTRON BACKSCATTER DIFFRACTION; HIGH-TEMPERATURE; ALLOYS; OXIDE;
STABILITY; EBSD
AB This contribution investigated the corrosion mechanisms of calcium zirconate
crucibles during vacuum induction melting of titanium aluminides. The crucibles
withstood several melts and exhibited no cracking due to thermal shock. However, a
significant amount of zirconium dissolved in the melt, whereas the oxygen content
of the melt increased on a much lower level. In contrast to melting Ti6A14V in the
same crucibles an increased calcium zirconate content of the crucibles did not
reduce the melt contamination of the titanium aluminide melts. The investigation of
the corrosion front of the crucibles revealed the formation of calcium aluminates,
whereas titanium was almost absent. The melting of titanium aluminides with
subsequent refining by electro slag remelting could be a viable production route to
produce titanium zirconium aluminum alloys. Furthermore, the relation between the
corrosion of calcium zirconate refractories in contact with titanium based alloys
depending on their composition should be further evaluated. (C) 2014 Elsevier Ltd.
C1 [Schaffoener, Stefan; Aneziris, Christos G.; Berek, Harry; Hubalkova, Jana] Tech
Univ Bergakad Freiberg, Inst Ceram Glass & Construct Mat, D-09599 Freiberg,
Germany.
[Rotmann, Bjoern; Friedrich, Bernd] Rhein Westfal TH Aachen, IME Inst Proc Met &
Met Recycling, D-52056 Aachen, Germany.
C3 Technical University Freiberg; RWTH Aachen University
RP Schafföner, S (corresponding author), Tech Univ Bergakad Freiberg, Inst Ceram
Glass & Construct Mat, Agricolastr 17, D-09599 Freiberg, Germany.
EM stefan.schaffoener@ikgb.tu-freiberg.de
RI Schafföner, Stefan/AAA-5648-2020; Friedrich, Bernd/AAM-7005-2021;
Friedrich, Bernd/AAM-7029-2021
OI Friedrich, Bernd/0000-0002-2934-2034; Schaffoner,
Stefan/0000-0002-6526-2496; Hubalkova, Jana/0000-0003-3624-8940
FU German Research Foundation (DFG) within the Research Unit 1372 [AN
322/25-1, FR 1713/19-1]
FX The authors would like to thank the German Research Foundation (DFG) for
supporting this work within the Research Unit 1372 (Grant No. AN
322/25-1 and FR 1713/19-1).
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NR 40
TC 29
Z9 32
U1 1
U2 40
PU ELSEVIER SCI LTD
PI OXFORD
SN 0955-2219
EI 1873-619X
J9 J EUR CERAM SOC
PD MAR
PY 2015
VL 35
IS 3
BP 1097
EP 1106
PG 10
GA AY6GF
UT WOS:000347664500025
DA 2023-12-05
ER
PT J
AU Liu, Q
Wen, G
Li, J
Fu, X
Tang, P
Li, W
AF Liu, Q.
Wen, G.
Li, J.
Fu, X.
Tang, P.
Li, W.
TI Development of mould fluxes based on lime-alumina slag system for
casting high aluminium TRIP steel
LA English
DT Article
DE Continuous casting; Mould fluxes; Lime-alumina based fluxes; TRIP Steel;
Surface quality
ID TRANSFORMATION-INDUCED-PLASTICITY; CRYSTALLIZATION BEHAVIOR; AL
AB With excellent strength and ductility properties, transformation induced
plasticity (TRIP) steels are superior to ordinary commercial steels and have great
application potential in the automobile industry. However, the continuous casting
of TRIP steels is associated with challenges owing to its high aluminium content,
approximately 0.5-1.8%. The reaction of aluminium near the steel/slag interface
continuously changes the basicity of conventional lime-silica based mould fluxes
causing variation in the flux physical properties between the solidifying shell and
mould wall. Therefore, the heat transfer process is unstable and the surface
quality of the as-cast slab is not guaranteed.
To reduce the reactivity of aluminium in TRIP steel during casting, it is
suggested to replace the lime-silica based fluxes with a lime-alumina based mould
flux, based on laboratory measurements and industrial trials.
The trials showed great improvement in the slab surface quality and no
depression defect was noticed so far.
C1 [Liu, Q.; Wen, G.; Fu, X.; Tang, P.] Chongqing Univ, Coll Mat Sci & Engn,
Chongqing 400044, Peoples R China.
[Li, J.; Li, W.] Wuhan Iron & Steel Co Ltd, Wuhan 430080, Peoples R China.
C3 Chongqing University; China Baowu Steel Group
RP Wen, G (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
EM wengh@cqu.edu.cn
FU National Natural Science Foundation of China [51274260]; Wuhan Iron and
Steel Company Limited
National Natural Science Foundation of China (Grant No. 51274260).
Thanks are also given to Wuhan Iron and Steel Company Limited for the
support provided for this work.
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Huang X. H., 2002, FUNDAMENTALS STEEL M, P242
Liu L. L., 2003, LIGHT METAL, V3, P19
Sugimoto K, 2005, ISIJ INT, V45, P1194, DOI 10.2355/isijinternational.45.1194
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[于雄 Yu Xiong], 2011, [重庆大学学报, Journal of Chongqing University], V34, P66
NR 19
TC 29
Z9 29
U1 0
U2 18
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD MAY
PY 2014
VL 41
IS 4
BP 292
EP 297
DI 10.1179/1743281213Y.0000000131
PG 6
GA AI7JK
UT WOS:000337064600010
DA 2023-12-05
ER
PT J
AU Yang, DX
Liu, YG
Fang, MH
Huang, ZH
Ye, DY
AF Yang, De-Xin
Liu, Yan-Gai
Fang, Ming-Hao
Huang, Zhao-Hui
Ye, Ding-Yun
TI Study on the slag corrosion resistance of unfired
Al2O3-SiC/β-Sialon/Ti(C, N)-C refractories
LA English
DT Article
DE Unfired refractories; Ti(C, N)/beta-Sialon powders; Slag resistance;
Fractal theory
ID OXIDATION
AB Al2O3-SiC-C refractories are widely used in the steelmaking process due to their
outstanding properties, and in order to improve their slag corrosion resistance,
the erosion resistant materials have often been used. beta-Sialon and Ti(C, N) are
point out as novel additives that present suitable properties to increase the
corrosion resistance of refractories. In this study, unfired Al2O3-SiC/beta-
Sialon/Ti(C, N)-C refractories were prepared using Ti(C, N)/beta-Sialon powders,
brown alumina, SIC, micro alpha-Al2O3 powder, silica fume, ball pitch, calcium
aluminate cement, aluminum and silicon as the starting materials. The effect of the
Ti(C, N)beta-Sialon powders and SiC on the slag penetration and corrosion
resistance of the refractories was investigated, and the slag resistance mechanisms
of the Al2O3-SiC/beta-Sialon/Ti(C, N)-C refractories were also discussed. Fractal
theory, scanning electron microscopy (SEM) and energy dispersive spectroscope (EDS)
were carried out in order to better understand the slag resistance effects and
reaction mechanisms. The results showed that all samples made with Ti(C, N)/beta-
Sialon powders had excellent slag corrosion resistance. The slag corrosion
resistance of the samples was based on their low apparent porosity and high volume
density. The beta-Sialon and SiC powders contributed to the improved slag corrosion
resistance performance of the composite refractories. (C) 2013 Elsevier Ltd and
C1 [Yang, De-Xin; Liu, Yan-Gai; Fang, Ming-Hao; Huang, Zhao-Hui; Ye, Ding-Yun]
China Univ Geosci, Sch Mat Sci & Technol, Beijing 100083, Peoples R China.
C3 China University of Geosciences
RP Liu, YG (corresponding author), China Univ Geosci, Sch Mat Sci & Technol,
EM liuyang@cugb.edu.cn
RI liu, yan/HCI-5542-2022; Fang, Minghao/M-9048-2013
OI Fang, Minghao/0000-0003-4646-9915
Research Funds for the Central Universities [2652012071, 2652013040];
Key Projects in the National Science & Technology Pillar Program
[2011BAB03B08]; Program for New Century Excellent Talents in University
of Ministry of Education of China [NCET-12-0951]; Key Laboratory on Deep
GeoDrilling Technology, Ministry of Land and Resources [NLSD201216]
China (Grant no. 51032007), the Fundamental Research Funds for the
Central Universities (Grant nos. 2652012071 and 2652013040), the Key
Projects in the National Science & Technology Pillar Program (Grant no.
2011BAB03B08), the Program for New Century Excellent Talents in
University of Ministry of Education of China (Grant no. NCET-12-0951)
and the Key Laboratory on Deep GeoDrilling Technology, Ministry of Land
and Resources (Grant no. NLSD201216).
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NR 26
TC 29
Z9 35
U1 3
U2 39
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD JAN
PY 2014
VL 40
IS 1
BP 1593
EP 1598
DI 10.1016/j.ceramint.2013.07.047
PN B
PG 6
GA AA0XL
UT WOS:000330820600040
DA 2023-12-05
ER
PT J
AU Praher, B
Rössler, R
Arenholz, E
Heitz, J
Pedarnig, JD
AF Praher, B.
Roessler, R.
Arenholz, E.
Heitz, J.
Pedarnig, J. D.
TI Quantitative determination of element concentrations in industrial oxide
materials by laser-induced breakdown spectroscopy
SO ANALYTICAL AND BIOANALYTICAL CHEMISTRY
LA English
DT Article
DE Calibration-free laser-induced breakdown spectroscopy (CF-LIBS);
Multi-element analysis; Slag; Industrial oxides
ID DOUBLE-PULSE; SLAG ANALYSIS; PLASMA; ABLATION; SAMPLES; LIBS;
EQUILIBRIUM
AB Calibration-free laser-induced breakdown spectroscopy (CF-LIBS) method is
employed for quantitative determination of oxide concentrations in multi-component
materials. Industrial oxide materials from steel industry are laser ablated in air,
and the optical plasma emission is collected by spectrometers and gated detectors.
The temperature and electron number density of laser-induced plasma are determined
from measured LIBS spectra. Emission lines of aluminium (Al), calcium (Ca), iron
(Fe), manganese (Mn), magnesium (Mg), silicon (Si), titanium (Ti), and chromium
(Cr) of low self-absorption are selected, and the concentration of oxides CaO,
Al2O3, MgO, SiO2, FeO, MnO, TiO2, and Cr2O3 is calculated by CF-LIBS analysis. For
all sample materials investigated, we find good match of calculated concentration
values (C-CF) with nominal concentration values (CN). The relative error in oxide
concentration, e(r)=vertical bar C-CF-C-N vertical bar/C-N, decreases with
increasing concentration and it is e(r)<= 100% for concentration C-N >= 1 wt.%. The
CF-LIBS results are stable against fluctuations of experimental parameters. The
variation of laser pulse energy over a large range changes the error by less than
10% for major oxides (C-N >= 10 wt.%). The results indicate that CF-LIBS method can
be employed for fast and stable quantitative compositional analysis of
multicomponent materials.
C1 [Praher, B.; Heitz, J.; Pedarnig, J. D.] Johannes Kepler Univ Linz, Inst Appl
Phys, Christian Doppler Lab Laser Assisted Diagnost, A-4040 Linz, Austria.
[Roessler, R.; Arenholz, E.] Voestalpine Stahl GmbH, A-4031 Linz, Austria.
RP Pedarnig, JD (corresponding author), Johannes Kepler Univ Linz, Inst Appl Phys,
Christian Doppler Lab Laser Assisted Diagnost, A-4040 Linz, Austria.
EM johannes.pedarnig@jku.at
RI Heitz, Johannes/O-8637-2015; Pedarnig, Johannes D/A-8500-2016
OI Heitz, Johannes/0000-0002-5608-5133; Pedarnig, Johannes
D/0000-0002-7842-3922
FU Austrian Federal Ministry of Economy, Family and Youth; National
Foundation for Research, Technology and Development
FX We want to thank the Austrian Federal Ministry of Economy, Family and
Youth and the National Foundation for Research, Technology and
Development for financial support (Christian Doppler Laboratory LAD).
CR Aguilera JA, 2009, SPECTROCHIM ACTA B, V64, P685, DOI 10.1016/j.sab.2009.06.002
[Anonymous], 2006, Handbook of Laser-Induced Breakdown Spectroscopy
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8547(01)00191-4
APPLICATIONS, pXV
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KURUCZ ATOMIC SPECTR
NR 44
TC 29
Z9 30
U1 0
U2 70
PI HEIDELBERG
SN 1618-2642
EI 1618-2650
J9 ANAL BIOANAL CHEM
JI Anal. Bioanal. Chem.
PD JUL
PY 2011
VL 400
IS 10
BP 3367
EP 3375
DI 10.1007/s00216-011-5000-9
PG 9
WC Biochemical Research Methods; Chemistry, Analytical
SC Biochemistry & Molecular Biology; Chemistry
GA 789IE
UT WOS:000292508200019
PM 21523330
DA 2023-12-05
ER
PT J
AU Cui, LH
Zhu, XZ
Ma, M
Ouyang, Y
Dong, M
Zhu, WL
Luo, SM
AF Cui, Lihua
Zhu, Xizhen
Ma, Mei
Ouyang, Ying
Dong, Mei
Zhu, Wenling
Luo, Shiming
TI Phosphorus sorption capacities and physicochemical properties of nine
substrate materials for constructed wetland
SO ARCHIVES OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY
LA English
DT Article
ID WASTE-WATER; REMOVAL; MEDIA; SOILS; LANGMUIR; SANDS
AB Constructed wetland (CW) is a promising technique for removal of pollutants from
wastewater and agricultural runoff. The performance of a CW to remove pollutants,
however, hinges on the use of suitable substrate materials. This study examined the
physicochemical properties and phosphorus (P) sorption capacities of nine different
CW substrate materials using both batch experiments and the Freundlich as well as
the Langmuir isotherm. The nine substrate materials used in this study were turf,
topsoil, gravel, midsized sand (MSS), blast furnace slag (BFS), coal burn slag
(CBS), blast furnace artificial slag (BFAS), coal burn artificial slag (CBAS), and
midsized artificial sand (MSAS). Experimental data showed that sorption of P
increased with initial solution P concentrations for all nine substrate materials.
The maximum P sorption capacity of the substrate materials estimated by Langmuir
isotherm was in the following order: turf (4243 mg/kg substrate) > BFAS (2116 mg/kg
substrate) > BFS (1598 mg/kg substrate) > CBS (1449 mg/kg substrate) > top soil
(1396 mg/kg substrate) > CBAS (1194 mg/kg substrate) > MSAS (519 mg/kg substrate) >
gravel (494 mg/kg substrate) > MSS (403 mg/kg substrate). The specific gravity of
eight substrate materials (except gravel) had very significant negative
correlations with the P sorption, whereas the particle diameter of D-60 and
uniformity coefficient (K-60) had positive correlations with the P sorption. The
cation exchange capacity, organic matter, available ferrous, and exchangeable
aluminum of the eight substrate materials also had very significant positive
correlations with the P sorption, while the pH of the substrate materials showed a
very significant negative correlation with the P sorption. Our study further
suggests that turf and CBAS are the two relatively ideal substrate materials
suitable for removal of P from a CW system.
C1 [Cui, Lihua; Zhu, Xizhen; Dong, Mei; Zhu, Wenling; Luo, Shiming] S China Agr
Univ, Coll Nat Resource & Environm Sci, Guangzhou 510642, Guangdong, Peoples R
China.
[Ouyang, Ying] Dept Water Resources, Palatka, FL 32177 USA.
C3 South China Agricultural University
RP Cui, LH (corresponding author), S China Agr Univ, Coll Nat Resource & Environm
Sci, Guangzhou 510642, Guangdong, Peoples R China.
EM lihcui@scau.edu.cn
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2002, Patent No. 012358797
NR 30
TC 29
Z9 44
U1 1
U2 60
PU SPRINGER
PI NEW YORK
SN 0090-4341
EI 1432-0703
J9 ARCH ENVIRON CON TOX
JI Arch. Environ. Contam. Toxicol.
PD AUG
PY 2008
VL 55
IS 2
BP 210
EP 217
DI 10.1007/s00244-007-9109-y
PG 8
WC Environmental Sciences; Toxicology
SC Environmental Sciences & Ecology; Toxicology
GA 316CQ
UT WOS:000256926900006
PM 18175159
DA 2023-12-05
ER
PT J
AU Reddy, RG
AF Reddy, RG
TI Emerging technologies in extraction and processing of metals
LA English
DT Article
ID HIGH PARTIAL PRESSURES; MINOR ELEMENTS DISTRIBUTION; SULFIDE CAPACITIES;
PHASE-EQUILIBRIUM; 1573 K; IONIC LIQUIDS; MATTE; SLAG; ALUMINUM
C1 Univ Alabama, Ctr Green Mfg, Tuscaloosa, AL 35487 USA.
C3 University of Alabama System; University of Alabama Tuscaloosa
RP Reddy, RG (corresponding author), Univ Alabama, Ctr Green Mfg, Tuscaloosa, AL
35487 USA.
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NR 52
TC 29
Z9 36
U1 0
U2 5
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD APR
PY 2003
VL 34
IS 2
BP 137
EP 152
DI 10.1007/s11663-003-0001-5
PG 16
Engineering
GA 662KU
UT WOS:000181946500001
DA 2023-12-05
ER
PT J
AU Abdel-latif, MA
AF Abdel-latif, MA
TI Recovery of vanadium and nickel from petroleum flyash
LA English
CT Conference on Pyrometallurgy (Pyromet 02)
CY MAR, 2002
CL CAPE TOWN, SOUTH AFRICA
DE environmental; recycling; reduction; extractive metallurgy; mass
balancing
AB Flyash is a powdery residue generated by the power stations that use heavy oil
as the source of fuel. The ash poses a threat to the environment due to the
presence of certain heavy elements such as chromium. At the same time, it contains
valuable metals, including vanadium and nickel, that are extractable if an
economical and environmentally acceptable process can be developed. To this end,
Mintek, in co-operation with Oxbow Carbon and Minerals, undertook a major research
program over a two-year period in an attempt to find the most suitable technology
to deal with this ash. After considering various alternatives, a process flowsheet
was developed and used as a basis to identify the testwork required for the major
processing units. The flowsheet consisted of a drying stage at moderate
temperatures of about 150degreesC, a de-carburization and de-sulphurization (pre-
treatment) stage, and finally a smelting step in a DC arc furnace.
Testwork carried out at the 40 kW scale, using pre-treated flyash, indicated the
feasibility of producing a ferrovanadium alloy containing more than 15% vanadium
and 6% nickel, with vanadium recovery of more than 89%, and a disposable slag based
on USA EPA safe disposal criteria. Several parameters were studied in order to
optimise the smelting stage including operating temperature, aluminium addition,
the use of ferrosilicon as the reducing agent and lime (flux) addition. The results
of the investigation are presented in this paper. (C) 2002 Elsevier Science Ltd.
C1 MINTEK, ZA-2125 Randburg, South Africa.
RP Abdel-latif, MA (corresponding author), MINTEK, 200 Hans Striidom Dr, ZA-2125
Randburg, South Africa.
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PI OXFORD
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD NOV
PY 2002
VL 15
IS 11
SU S
BP 953
EP 961
AR PII S0892-6875(02)00134-6
DI 10.1016/S0892-6875(02)00134-6
PG 9
GA 629TY
UT WOS:000180066000007
DA 2023-12-05
ER
PT J
AU Klose, S
Koch, J
Bäucker, E
Makeschin, F
AF Klose, S
Koch, J
Bäucker, E
Makeschin, F
TI Indicative properties of fly-ash affected forest soils in Northeastern
Germany
SO JOURNAL OF PLANT NUTRITION AND SOIL SCIENCE
LA English
DT Article
DE fly ash depositions; forest soils; humic horizon; ferromagnetic
susceptibility; scanning electron microscopy (SEM); energy dispersive
X-ray microanalysis (EDX)
ID MAGNETIC-SUSCEPTIBILITY; ORGANIC-MATTER; MINE SOILS; LIGNITE
AB Many forest ecosystems in Germany are strongly influenced by emissions of
pollutants like SO2 and alkaline dusts. To quantify and evaluate the consequences
of long-term fly ash deposition on forest soils, a study was conducted in pine
stands (Pinus sylvestris) in the Dubener Heide in Northeastern Germany. This forest
area has been influenced mainly by emissions from coal-fired power plants and the
chemical industry of the industrial region Bitterfeld-Wolfen-Zschornewitz since the
early 1900. The study sites are located along a fly ash deposition gradient of 8,
16, 14, 18, and 25 km away from the main emission source in Bitterfeld (sites 1, 2,
3, 4, and 5, respectively). Samples of the organic horizons (Oi, Oe, and Oa) and
mineral topsoil (0-10 cm) were taken in fall 1998 and analyzed for their
ferromagnetic susceptibility and total ash content. Scanning electron microscopy
(SEM) and energy dispersive X-ray microanalysis (EDX) were performed on selected
samples to differentiate between the pedogenic and atmospheric origin of the
mineral components in the organic horizons. As a result of the long-term
deposition. ferromagnetic fly ash components are mainly accumulated in the Oe and
Oa horizons of the forest soils studied. Ferromagnetic susceptibility was
significantly higher (p less than or equal to 0.05) in the Oe horizon of sites 1
and 2 compared to sites 3, 4, and 5. Unusually high total ash contents for organic
horizons of > 74 % were determined in the Oa at all sites. SEM revealed 3 distinct
features of persistent fly ash deposits from coal-fired power plants within the
organic horizons that can be defined as "stable glasses" with magnetic properties,
aluminum-silicate-minerals, and slag fragments. SEM and EDX indicated that a great
portion of the mineral particles found in the organic horizons of forests soils
influenced by fly ash are from atmospheric sources. For detection of atmospheric
lignite-derived deposition into forest soils, the Oe and Oa horizons have to be
considered as specific diagnostic horizons because they show indicative properties
for such soils.
C1 Tech Univ Dresden, Fac Forestry Geo & Hydro Sci, Inst Soil Sci, D-01735
Tharandt, Germany.
Tech Univ Dresden, Fac Forestry Geo & Hydro Sci, Inst Forest Utilizat & Forest
Technol, D-01735 Tharandt, Germany.
C3 Technische Universitat Dresden; Technische Universitat Dresden
RP Klose, S (corresponding author), Tech Univ Dresden, Fac Forestry Geo & Hydro
Sci, Inst Soil Sci, PO 1117, D-01735 Tharandt, Germany.
EM sklose@forst.tu-dresden.de
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NR 34
TC 29
Z9 30
U1 0
U2 9
PI WEINHEIM
SN 1436-8730
EI 1522-2624
J9 J PLANT NUTR SOIL SC
JI J. Plant Nutr. Soil Sci.
PD OCT
PY 2001
VL 164
IS 5
BP 561
EP 568
DI 10.1002/1522-2624(200110)164:5<561::AID-JPLN561>3.0.CO;2-9
PG 8
WC Agronomy; Plant Sciences; Soil Science
SC Agriculture; Plant Sciences
GA 487PQ
UT WOS:000171884800014
DA 2023-12-05
ER
PT J
AU Baligidad, RG
Prakash, U
Radhakrishna, A
AF Baligidad, RG
Prakash, U
Radhakrishna, A
TI Processing of high carbon Fe3Al based intermetallic alloy
SO INTERMETALLICS
LA English
CT Kyoto Workshop on High Temperature Intermetallic Compounds
CY MAY 10-13, 1998
CL KYOTO, JAPAN
DE iron aluminides; based on Fe3Al; mechanical properties at ambient
temperature; casting; melting; microstructure
ID MECHANICAL-PROPERTIES; EMBRITTLEMENT
AB A melting procedure for air induction melting (AIM) of an Fe3Al based
intermetallic alloy Fe-15.38wt%Al-1.1wt%C is described. Use of an appropriate slag
cover during AIM results in elimination of hydrogen gas porosity in cast AIM
ingots. Criteria for slag selection and slag to metal ratio are discussed. Refining
by slag-metal reactions results in significant reduction in impurity levels (S, O,
N) during AIM. Consequently, low cost raw materials such as mild steel scrap and
commercial aluminium were used for melting the alloy. The AIM ingot exhibited
excellent tensile properties. The ductility and hot workability of the ingot may be
further improved by subsequent processing through electroslag remelting. It is also
argued that the presence of carbon may be necessary to get AIM castings with
desirable mechanical properties. (C) 1998 Elsevier Science Limited. All rights
reserved.
C1 Def Met Res Lab, Hyderabad 500058, Andhra Pradesh, India.
C3 Defence Research & Development Organisation (DRDO); Defence
Metallurgical Research Laboratory (DMRL)
RP Baligidad, RG (corresponding author), Def Met Res Lab, Hyderabad 500058, Andhra
Pradesh, India.
RI Nath, S Shashi/B-5115-2009
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NR 15
TC 29
Z9 30
U1 0
U2 3
PU ELSEVIER SCI LTD
PI OXFORD
SN 0966-9795
J9 INTERMETALLICS
JI Intermetallics
PD NOV-DEC
PY 1998
VL 6
IS 7-8
BP 765
EP 769
DI 10.1016/S0966-9795(98)00050-8
PG 5
GA 139HH
UT WOS:000077022100036
DA 2023-12-05
ER
PT J
AU Tayeb, AM
AF Tayeb, AM
TI Use of some industrial wastes as energy storage media
SO ENERGY CONVERSION AND MANAGEMENT
LA English
DT Article
DE energy storage; solid storage materials (SSM); mixed systems; phase
change material (PCM); heat transfer fluid (HTF)
AB Solar energy is stored using different solid storage materials, both chemical
and metallic industrial wastes. The materials tested in the present study are
paraffin wax, copper slag, aluminium slag, iron slag, cast iron slag and copper
chips. Solar energy is stored in these materials, and the energy is then recovered
with a water stream at different how rates, and the storage capacity and period for
different materials were compared. The same set of experiments is run on solid
metallic materials mixed with wax. The results indicated that iron slag has the
highest storage capacity followed by cast iron slag then aluminium slag and copper
chips and copper slag. It is also noted that the addition of paraffin wax to the
solid metallic material greatly improves its storage capacity and duration. The
storage efficiency of different units is calculated and compared.
RP Tayeb, AM (corresponding author), MENIA UNIV,FAC ENGN,MENIA,EGYPT.
NR 0
TC 29
Z9 30
U1 1
U2 7
PI OXFORD
SN 0196-8904
J9 ENERG CONVERS MANAGE
JI Energy Conv. Manag.
PD FEB
PY 1996
VL 37
IS 2
BP 127
EP 133
DI 10.1016/0196-8904(95)00171-9
PG 7
WC Thermodynamics; Energy & Fuels; Mechanics
SC Thermodynamics; Energy & Fuels; Mechanics
GA TJ139
UT WOS:A1996TJ13900001
DA 2023-12-05
ER
PT J
AU Chen, HC
Lin, HR
Zhang, PP
Yu, L
Chen, LJ
Huang, X
Jiao, BQ
Li, DW
AF Chen, Hongcai
Lin, Huirong
Zhang, Pengpeng
Yu, Lin
Chen, Liangjun
Huang, Xiao
Jiao, Binquan
Li, Dongwei
TI Immobilisation of heavy metals in hazardous waste incineration residue
using
SiO2-Al2O3-Fe2O3-
CaO glass-ceramic
LA English
DT Article
DE Hazardous waste incineration residue; SiO2-Al2O3-Fe2O3-CaO
glass-ceramics; Heavy metals; Immobilisation mechanism
ID ORE PROCESSING RESIDUE; FLY-ASH; BOTTOM ASH; SLAG; CRYSTALLIZATION;
VITRIFICATION; DURABILITY; STRENGTH; BEHAVIOR; SODIUM
AB Hazardous waste incineration residue (HWIR) is categorised as hazardous waste
due to the presence of heavy metals such as Zn, Cu, and Cr. Based on the abundant
components of silica, aluminium oxide, iron oxide, and calcium oxide in a HWIR from
an environmental protection corporation in China, a 100% HWIR was used to prepare
SiO2-Al2O3-Fe2O3-CaO glass-ceramic samples. The results showed that Zn, Cu, and Cr
present in the glass-ceramic samples were effectively immobilised through the
melting-sintering process. Among the four parameters of heat treatment,
crystallisation temperature played the most significant role. The glass-ceramic
that was formed under optimal conditions contained haematite, pseudobrookite, and
anorthite, and exhibited a superior compressive strength, volume density, and water
absorption of 204.84 MPa, 2.80 g/cm(3), and 1.20%, respectively. Compared with the
raw HWIR sample, the leaching concentrations of Zn, Cu, and Cr from the prepared
glass-ceramic samples decreased significantly, and their immobilisation
efficiencies exceeded 99%. Physical encapsulation in the glass-ceramic samples
along with ion exchange in the amorphous glassy matrix and iron-rich crystalline
phases were the main immobilisation mechanisms of Zn, Cu, and Cr.
C1 [Chen, Hongcai; Zhang, Pengpeng; Huang, Xiao; Jiao, Binquan; Li, Dongwei]
Chongqing Univ, State Key Lab Coal Mine Disaster Dynam & Control, Chongqing 400044,
Peoples R China.
[Chen, Hongcai; Lin, Huirong; Zhang, Pengpeng; Yu, Lin; Huang, Xiao; Jiao,
Binquan; Li, Dongwei] Chongqing Univ, Sch Resources & Safety Engn, Chongqing
[Lin, Huirong; Li, Dongwei] Natl & Local Joint Engn Res Ctr Hazardous Waste I,
[Chen, Liangjun] Anhui Univ Technol, Sch Met Engn, Hefei 243002, Anhui, Peoples
R China.
C3 Chongqing University; Chongqing University; Anhui University of
Technology
RP Huang, X; Jiao, BQ; Li, DW (corresponding author), Chongqing Univ, State Key Lab
Coal Mine Disaster Dynam & Control, Chongqing 400044, Peoples R China.
EM shawwong@126.com; j.binquan@cqu.edu.cn; litonwei@cqu.edu.cn
RI lin, hui/HJI-4472-2023; LI, DONGWEI/JJE-8110-2023; Li,
Dongwei/F-4215-2011
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NR 55
TC 28
Z9 30
U1 3
U2 66
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD MAR 15
PY 2021
VL 47
IS 6
BP 8468
EP 8477
DI 10.1016/j.ceramint.2020.11.213
EA FEB 2021
PG 10
GA QM0XT
UT WOS:000621504700001
DA 2023-12-05
ER
PT J
AU Casanova, S
Silva, RV
de Brito, J
Pereira, MFC
AF Casanova, S.
Silva, R. V.
de Brito, J.
Pereira, M. F. C.
TI Mortars with alkali-activated municipal solid waste incinerator bottom
ash and fine recycled aggregates
LA English
DT Article
DE Municipal solid waste; Incinerator bottom ash; Alkali-activated
materials; Recycled aggregates; Curing conditions
ID FLY-ASH; GEOPOLYMER MORTAR; STRENGTH; SLAG; CARBONATION
AB Milled municipal solid waste incinerator bottom ash was used as a precursor in
the production of alkaliactivated mortars with recycled concrete aggregates as a
sand substitute. Fly ash was used as control precursor and sodium hydroxide as an
alkaline activator. Different thermal curing regimens were used: 24 h in ambient
conditions; 24 h/70 degrees C; 48 h/70 degrees C; and 24 h/90 degrees C. Mechanical
and durability-related performances were evaluated (i.e. flexural and compressive
strength, modulus of elasticity, ultrasonic pulse velocity, carbonation, capillary
water absorption, and shrinkage). The reaction between metallic aluminium from
municipal solid waste incinerator bottom ash and OH- ions produced hydrogen gas,
causing expansion, porosity increase and thus decline in performance. Low stability
in high relative humidity settings due to leaching of highly soluble compounds was
also observed. A further decline in performance was observed in mixes containing
recycled aggregates. Alkali activated municipal solid waste incinerator bottom ash
presented fast carbonation but also a considerable strength enhancement. (C) 2021
C1 [Casanova, S.] Univ Lisbon, Inst Super Tecn, Ave Rovisco Pais, P-1049001 Lisbon,
Portugal.
[Silva, R. V.; de Brito, J.] Univ Lisbon, Inst Super Tecn, CERIS, Ave Rovisco
Pais, P-1049001 Lisbon, Portugal.
[Pereira, M. F. C.] Univ Lisbon, Inst Super Tecn, CERENA, Ave Rovisco Pais, P-
1049001 Lisbon, Portugal.
C3 Universidade de Lisboa; Instituto Superior Tecnico; Universidade de
Lisboa; Instituto Superior Tecnico; Universidade de Lisboa; Instituto
Superior Tecnico
RP Silva, RV (corresponding author), Univ Lisbon, Inst Super Tecn, CERIS, Ave
Rovisco Pais, P-1049001 Lisbon, Portugal.; Silva, RV (corresponding author), Univ
Lisbon, Inst Super Tecn, CERENA, Ave Rovisco Pais, P-1049001 Lisbon, Portugal.
EM sofia3casanova@gmail.com; rui.v.silva@tecnico.ulisboa.pt;
jb@civil.ist.utl.pt; mfcp@ist.utl.pt
RI Silva, Ana/JGM-6679-2023; de Brito, Jorge/A-4299-2008; Silva, Rui
Vasco/D-5814-2013; Pereira, Manuel Francisco Costa/AAX-5262-2020
OI de Brito, Jorge/0000-0001-6766-2736; Silva, Rui
Vasco/0000-0002-2276-9721; Pereira, Manuel Francisco
Costa/0000-0002-7932-8062
FU CERIS Research Institute, IST, University of Lisbon; FCT - Foundation
for Science and Technology [PTDC/ECI-CON/29196/2017]; CERENA Strategic
Project [UID/ECI/04028/2013]; Fundação para a Ciência e a Tecnologia
[PTDC/ECI-CON/29196/2017] Funding Source: FCT
FX The authors gratefully acknowledge the support of the CERIS Research
Institute, IST, University of Lisbon and FCT - Foundation for Science
and Technology, through the research project PTDC/ECI-CON/29196/2017
"Recycled Inorganic Polymer Concrete: Towards a fully recycled and
cement-free concrete" (RInoPolyCrete) and CERENA Strategic Project
UID/ECI/04028/2013. The authors would also like to acknowledge the
support of Valorsul, EDP, SIKA and Secil for part of the materials
provided for this experimental campaign.
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U1 6
U2 68
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PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAR 20
PY 2021
VL 289
AR 125707
DI 10.1016/j.jclepro.2020.125707
EA JAN 2021
PG 12
& Ecology
GA QK3HV
UT WOS:000620272500001
DA 2023-12-05
ER
PT J
AU Jun, YB
Kim, T
Kim, JH
AF Jun, Yubin
Kim, Taewan
Kim, Jae Hong
TI Chloride-bearing characteristics of alkali-activated slag mixed with
seawater: Effect of different salinity levels
LA English
DT Article
DE Hydrotalcite; Hydrocalumite; Seawater; Alternative cement
ID THERMAL-DECOMPOSITION; CRYSTAL-STRUCTURE; HYDRATION; HYDROTALCITE;
CONCRETE
AB This paper presents the microstructural properties of KOH-activated slag pastes
produced with natural seawater under different salinity levels. The seawater-mixed
samples exhibit higher 91-day strength compared to the control sample produced with
deionized water. Their reduced total porosity and decrease in average pore size are
closely related to the strength improvement. The dense microstructure is composed
of reaction products resulting from the inclusion of seawater; these include Cl-
hydrocalumite, Cl-hydrotalcite, AlClO, K2SO4, CaCO3, calcium aluminum iron oxide
carbonate hydroxide hydrate, and aluminum chloride hydrate. In addition, CO32- in
the CO3-hydrotalcite and CO3-hydrocalumite is replaced by chloride ions, and then a
Cl-bearing phase is formed, leading to a higher bound chloride content. Lastly, in
the single ocean current investigated in this study, the strength of seawater-mixed
samples is weakly vulnerable to salinity variation.
C1 [Jun, Yubin; Kim, Jae Hong] Korea Adv Inst Sci & Technol, Dept Civil & Environm
Engn, Daejeon 34141, South Korea.
[Kim, Taewan] Pusan Natl Univ, Dept Civil Engn, Busan 46241, South Korea.
C3 Korea Advanced Institute of Science & Technology (KAIST); Pusan National
University
RP Kim, JH (corresponding author), Korea Adv Inst Sci & Technol, Dept Civil &
Environm Engn, Daejeon 34141, South Korea.
EM jae.kim@kaist.ac.kr
RI Kim, Jae Hong/F-7775-2011
OI Kim, Jae Hong/0000-0002-6253-6877; Kim, Taewan/0000-0002-9367-8747
FU Basic Science Research Program through the National Research Foundation
of Korea (NRF) - Ministry of Education [NRF-2017R1D1A1B03034700];
National Research Foundation of Korea [4199990614407] Funding Source:
FX This research was supported by the Basic Science Research Program
through the National Research Foundation of Korea (NRF) funded by the
Ministry of Education (NRF-2017R1D1A1B03034700).
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TC 28
Z9 28
U1 0
U2 35
PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
PD SEP
PY 2020
VL 112
AR 103680
DI 10.1016/j.cemconcomp.2020.103680
PG 10
GA MW1SQ
UT WOS:000556826200029
DA 2023-12-05
ER
PT J
AU Yoon, HN
Seo, J
Kim, S
Lee, HK
Park, S
AF Yoon, H. N.
Seo, Joonho
Kim, Seonhyeok
Lee, H. K.
Park, Solmoi
TI Characterization of blast furnace slag-blended Portland cement for
immobilization of Co
LA English
DT Article
DE Cobalt; Cementation; Blast furnace slag; Solidification; Immobilization
ID LAYERED DOUBLE HYDROXIDES; AL-27; HYDRATION; SPECIATION; ALUMINUM;
KINETICS; BEHAVIOR
AB The leaching behavior of Co2+ from blast furnace slag-blended cement is
investigated. Semi-dynamic leaching test results show that the performance of the
cement with regard to the retention of Co2+ is increased by replacing Portland
cement with slag (similar to 70 wt%). The changes in the formation and structure of
calcium-silicate-hydrate gels in the blended cement as a function of the slag
content are insignificant after 28 days of curing, while slag in the binder leads
to the formation of more layered double-hydroxide (LDH) structured phases,
including AFm and Co-Al LDH phases. The enhanced Co uptake by the LDH phases
together with the refined pore structure of the slag-blended cement significantly
improves the performance for retention of Co2+ in the cement matrix.
C1 [Yoon, H. N.; Seo, Joonho; Kim, Seonhyeok; Lee, H. K.; Park, Solmoi] Korea Adv
Inst Sci & Technol, Dept Civil & Environm Engn, 291 Daehak Ro, Daejeon 34141, South
Korea.
[Park, Solmoi] Pukyong Natl Univ, Dept Civil Engn, 45 Yongso Ro, Busan 48513,
South Korea.
C3 Korea Advanced Institute of Science & Technology (KAIST); Pukyong
National University
RP Park, S (corresponding author), Pukyong Natl Univ, Dept Civil Engn, 45 Yongso
Ro, Busan 48513, South Korea.
EM solmoi.park@pknu.ac.kr
RI Park, Solmoi/AHE-4311-2022; Park, Solmoi/AAA-5658-2022; Park,
Solmoi/AAD-5326-2019
OI Park, Solmoi/0000-0003-0746-3940; Seo, Joonho/0000-0002-8027-492X
FU National Research Foundation of South Korea [2018R1D1A1B07047233,
2018R1A2A1A05076894]; Korean government; National Research Foundation of
Korea [2018R1D1A1B07047233] Funding Source: Korea Institute of Science &
Technology Information (KISTI), National Science & Technology
Information Service (NTIS)
FX This study was supported by National Research Foundation of South Korea
(Grant No. 2018R1D1A1B07047233, and 2018R1A2A1A05076894) funded by the
Korean government. We would like to thank Dr. Seen-Ae Chae at Korea
Basic Science Institute (Western Seoul Center) for assistance with
solid-state NMR spectroscopy.
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NR 42
TC 28
Z9 28
U1 2
U2 35
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD AUG
PY 2020
VL 134
AR 106089
DI 10.1016/j.cemconres.2020.106089
PG 9
GA LW0VH
UT WOS:000538864100003
DA 2023-12-05
ER
PT J
AU Zhang, BY
He, PP
Poon, CS
AF Zhang, Binyu
He, Pingping
Poon, Chi Sun
TI Optimizing the use of recycled glass materials in alkali activated
cement (AAC) based mortars
LA English
DT Article
DE Recycled glass aggregate; Recycled glass powder; Alkali activated cement
(AAC); Alkali silica reaction (ASR); Elevated temperature exposure;
Optimization
ID FLY-ASH; MECHANICAL-PROPERTIES; WASTE GLASS; POWDER; DURABILITY;
COMPOSITES
AB The management of waste glass generated mainly from waste glass beverage bottles
has become a pressuring waste management problem. This study presents a novel way
to incorporate recycled glass materials into alkali-activated cement (AAC) based
pastes/mortars. Waste glass cullet (GC) was used to replace natural aggregates and
waste glass powder (GP) was used to partially replace conventional precursors such
as ground blast furnace slag (GGBS). Optimization was conducted innovatively aiming
at maximizing the total waste glass content in the AAC materials while maintaining
adequate mechanical, durability and functional properties of the final products
that contained more than 70% of recycled glass materials by mass. Using the
developed technology, recycled glass incorporated alkali activated cement based
mortars (AAMs) with a 28-day compressive strength of about 40 MPa can be produced.
Furthermore, the excellent high temperature resistance of the optimized AAC mortar
mixture allowed the retention of over 50% of the original strength after 2 h of
exposure at 800 degrees C. The experimental results also showed that the
detrimental expansion caused by the alkali silica reaction (ASR) between the alkali
and the waste GC in the AAC mortars could be controlled successfully by using
additional aluminium sources such as calcium aluminate cement (CAC). Further
reduction in ASR expansion was possible via adjusting the GC to binder ratio. Also,
the drying shrinkage level could be controlled to less than 1000tte which is a
significant improvement to conventional AAC materials prepared by using GGBS. The
findings presented in this paper are pivotal for maximizing the recycling and
reusing of waste glass in AAC. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Zhang, Binyu; He, Pingping; Poon, Chi Sun] Hong Kong Polytech Univ, Dept Civil
& Environm Engn, Hung Hom, Hong Kong, Peoples R China.
Engn, Hung Hom, Hong Kong, Peoples R China.
RI Poon, Chi Sun/H-4152-2015; Poon, Chi Sun/JQI-2195-2023
OI Poon, Chi Sun/0000-0003-4912-3936; He, pingping/0000-0002-9120-8864
FU Environment and Conservation Fund (ECF); Hong Kong Polytechnic
University
FX The authors wish to thank the Environment and Conservation Fund (ECF)
and The Hong Kong Polytechnic University for funding support.
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PI OXFORD
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EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAY 10
PY 2020
VL 255
AR 120228
DI 10.1016/j.jclepro.2020.120228
PG 11
& Ecology
GA KW1TG
UT WOS:000520953200084
DA 2023-12-05
ER
PT J
AU Kim, T
Kim, IT
Seo, KY
Park, HJ
AF Kim, Taewan
Kim, In-Tae
Seo, Ki-Young
Park, Hyun-Jae
TI Strength and pore characteristics of OPC-slag cement paste mixed with
polyaluminum chloride
LA English
DT Article
DE Polyaluminum chloride; Compressive strength; Pore structure; Friedel's
salt; C-A-S-H gel
ID C-S-H; AL-27 MAS NMR; COMPRESSIVE STRENGTH; FRIEDELS SALT; ALUMINUM
INCORPORATION; COAGULATION BEHAVIOR; HYDRATED CEMENT; CALCIUM; ALKALI;
BINDING
AB An experimental study of ordinary Portland cement mixed with ground granulated
blast-furnace slag (OPC-slag) showed varying rates of slag (60%, 40%, and 20%
replacement rate to OPC) and polyaluminum chloride (PAC) (0%, 2%, 4%, 6%, 8%, and
10% added to the mixing water) were mixed into the cement to assess the strength
and pore structure properties of the cement. X-ray diffractometer, mercury
introsion porosimetry, scanning electron microscopy and thermal analysis were
performed to observe the pore structures and hydration reactants. As the amount of
PAC increased, the compressive strength increased, the total porosity decreased,
and the pore volume less than 50 nm diameter increased. PAC promotes hydration of
slag particles. The aluminum contained in the PAC also changes the C-S-H gel to a
more dense C-A-S-H gel and contributes to the formation of Friedel's salt. And the
chloride ion in the PAC forms a Friedel's salt to fill the pores. In this process,
portlandite was consumed. 10% PAC showed the highest compressive strength at all
slag replacement rates. 20% slag showed 134.6% at 28 days, 151.9% at 7 days for 40%
slag, and 159.0% at 1 day for 60% slag. 10% PAC decreased total porosity and
increased pores smaller than 50 nm compared to without-PAC sample. In particular,
the OPC-slag sample with 20% slag substitution showed the largest pore structure
change due to the large and clear reduction effect of pore diameter and volume by
PAC. It was confirmed that mixing of PAC with OPC-slag cement paste formed a dense
matrix and affected the improvement of compressive strength and the change of pore
structure. (C) 2019 Elsevier Ltd. All rights reserved.
C1 [Kim, Taewan; Kim, In-Tae] Pusan Natl Univ, Dept Civil Engn, Busan 46241, South
Korea.
[Seo, Ki-Young; Park, Hyun-Jae] HK Engn & Consultants, Busan 46220, South Korea.
C3 Pusan National University
RP Kim, T (corresponding author), Pusan Natl Univ, Dept Civil Engn, Busan 46241,
South Korea.
EM ring2014@naver.com
OI Kim, Taewan/0000-0002-9367-8747
FU National Research Foundation of Korea (NRF) - Korean Government (MOE)
[NRF-2015R1D1A3A01019583]
FX This work was supported by the National Research Foundation of Korea
(NRF) grant funded by the Korean Government (MOE)
(NRF-2015R1D1A3A01019583).
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10.1016/j.conbuildmat.2012.07.079
NR 68
TC 28
Z9 28
U1 3
U2 35
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 30
PY 2019
VL 223
BP 616
EP 628
DI 10.1016/j.conbuildmat.2019.07.009
PG 13
GA JA1HW
UT WOS:000487569100054
DA 2023-12-05
ER
PT J
AU Chi, CY
Li, YJ
Zhang, W
Wang, ZY
AF Chi, Changyun
Li, Yingjie
Zhang, Wan
Wang, Zeyan
TI Synthesis of a hollow microtubular Ca/Al sorbent with high CO2
uptake by hard templating
SO APPLIED ENERGY
LA English
DT Article
DE Absorbent cotton; Hard templating synthesis; Hollow microtubular
structure; Calcium looping; CO2 capture
ID CO2 CAPTURE PERFORMANCE; THERMOCHEMICAL ENERGY-STORAGE; CAO-BASED
SORBENTS; CARBIDE SLAG; TECHNOECONOMIC EVALUATION; COMBINED-CYCLE;
TEMPERATURE; BEHAVIOR; CARBONATION; EFFICIENT
AB A novel hollow microtubular Ca/Al CO2 sorbent was synthesized through a hard
templating pathway using absorbent cotton as a template, limestone as a CaO
precursor and aluminum nitrate as an Al2O3 precursor. The synthetic Ca/Al sorbent
consists of hollow porous microtubes with diameters ranging from 0.5 to 5 mu m and
replicates the biomorph of the absorbent cotton template well. When the mass ratio
of CaO/Al2O3 is 90:10, the hollow microtubular Ca/Al sorbent exhibits the highest
CO2 capture capacities during the cycles. The CO2 capture capacities of the novel
Ca/Al sorbent after 50 cycles under a mild calcination condition (850 degrees C in
pure N-2 ) and a severe calcination condition (920 degrees C in 70% CO2/30% N-2)
are respectively 0.55 and 0.38 g/g, which are 7.91 and 8.93 times greater than
those of limestone. The main compositions of the walls of the microtubes in the
novel Ca/Al sorbent are CaO and Ca12Al14O33. Ca12Al14O33, as a good supporter,
maintains the structural stability of the microtubes during the CO2 capture cycles.
CO2 diffuses into the porous wall of the microtube in both directions
(simultaneously into the outer and inner surfaces), so the CO2 diffusion resistance
in the microtubes is low. The calcium looping system using the novel Ca/Al sorbent
shows much lower energy consumption of the calciner and lower cost, compared with
using limestone. Thus, Ca-Al-T appears promising in the calcium looping.
C1 [Chi, Changyun; Li, Yingjie; Zhang, Wan] Shandong Univ, Sch Energy & Power Engn,
Jinan 250061, Shandong, Peoples R China.
[Wang, Zeyan] Shandong Univ, State Key Lab Crystal Mat, Jinan 250100, Shandong,
Peoples R China.
C3 Shandong University; Shandong University
EM liyj@sdu.edu.cn
Research Funds of Shandong University [2018JC039]
FX Financial supports from the National Natural Science Foundation of China
(51876105) and the Fundamental Research Funds of Shandong University
(2018JC039) are gratefully appreciated.
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NR 60
TC 28
Z9 28
U1 2
U2 53
PU ELSEVIER SCI LTD
PI OXFORD
SN 0306-2619
EI 1872-9118
J9 APPL ENERG
JI Appl. Energy
PD OCT 1
PY 2019
VL 251
AR 113382
DI 10.1016/j.apenergy.2019.113382
PG 14
GA JP0MM
UT WOS:000497966300090
DA 2023-12-05
ER
PT J
AU Fernández-Pereira, C
Luna-Galiano, Y
Pérez-Clemente, M
Leiva, C
Arroyo, F
Villegas, R
Vilches, LF
AF Fernandez-Pereira, C.
Luna-Galiano, Y.
Perez-Clemente, M.
Leiva, C.
Arroyo, F.
Villegas, R.
Vilches, L. F.
TI Immobilization of heavy metals (Cd, Ni or Pb) using aluminate
geopolymers
LA English
DT Article
DE Slag; Geopolymer; Fly ash; Aluminum waste; Hazardous metals;
Immobilization
ID ASH-BASED GEOPOLYMERS; FLY-ASH; SODIUM ALUMINATE; WASTE; LEAD
AB In the present study, a waste aluminate solution from the anodizing industry was
used to synthesize coal fly ash-and blast furnace slag-based geopolymers as metal-
immobilizing matrixes. Different alkali-activating agents such as NaOH and sodium
silicate have also been used in order to achieve defined Si/Al or Na/Al ratios in
the mixtures. Mixtures of simulated waste containing hazardous metals such as Pb,
Cd, or Ni with the geopolymer materials have been processed to study the potential
of geopolymers as waste immobilizing agents. The effects of composition on the
compressive strength and metals leachability were assessed. Of the two aluminate
geopolymers studied, those containing slag exhibited better mechanical performance.
Concentrations of the metals leached from the stabilized products were strongly pH
dependent, showing that the leachate pH was an important variable for the
immobilization of metals. (C) 2018 Elsevier B.V. All rights reserved.
C1 [Fernandez-Pereira, C.; Luna-Galiano, Y.; Perez-Clemente, M.; Leiva, C.; Arroyo,
F.; Villegas, R.; Vilches, L. F.] Univ Seville, Chem & Environm Engn Dept, Camino
Descubrimientos S-N, Seville 41092, Spain.
C3 University of Sevilla
RP Fernández-Pereira, C (corresponding author), Univ Seville, Chem & Environm Engn
Dept, Camino Descubrimientos S-N, Seville 41092, Spain.
EM pereira@us.es
RI Torralvo, Fátima Arroyo/I-5975-2012; leiva, carlos/AAJ-3229-2020;
Vilches, L. F./AAC-8740-2020; Luna-Galiano, Y./V-8972-2018; Fernandez
Pereira, Constantino/F-4845-2016
OI Torralvo, Fátima Arroyo/0000-0002-1705-8335; leiva,
carlos/0000-0001-7967-8102; Vilches, L. F./0000-0002-2786-8059;
Luna-Galiano, Y./0000-0002-0117-8316; Fernandez Pereira,
Constantino/0000-0003-4173-7677
CR [Anonymous], 2006, 1961 EN
Background Information for the Leaching Environmental Assessment (LEAF), 2010,
EPA600R10170
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NR 14
TC 28
Z9 29
U1 4
U2 56
PI AMSTERDAM
SN 0167-577X
EI 1873-4979
J9 MATER LETT
JI Mater. Lett.
PD SEP 15
PY 2018
VL 227
BP 184
EP 186
DI 10.1016/j.matlet.2018.05.027
PG 3
GA GK7VQ
UT WOS:000436420200048
DA 2023-12-05
ER
PT J
AU Yang, J
Hou, DS
Ding, QJ
AF Yang, Jun
Hou, Dongshuai
Ding, Qingjun
TI Structure, Dynamics, and Mechanical Properties of Cross-Linked Calcium
Aluminosilicate Hydrate: A Molecular Dynamics Study
LA English
DT Article
DE Low carbon footprint; Reactive molecular dynamics; Aluminosilicate
chains polymerization; Reactivity; Uniaxial tension; Hydrolytic reaction
ID C-S-H; REACTIVE FORCE-FIELD; SUPPLEMENTARY CEMENTITIOUS MATERIALS; ROMAN
SEAWATER CONCRETE; ALKALI-ACTIVATED SLAG; ALUMINUM INCORPORATION;
FLY-ASH; TRICALCIUM SILICATE; ELASTIC PROPERTIES; PORTLAND-CEMENT
AB C-A-S-H is the main hydration product of environmental friendly concrete with
cement material partially substituted by the industrial waste. The molecular
structure of C-A-S-H gel determines the durability of the material. In this study,
the cross-linking C-A-S-H models with Al/Si ratios of 0, 0.05, 0.10, 0.15, and 0.2
are constructed, and the structure, reactivity, and mechanical properties of the C-
A-S-H gel are investigated by the reactive force field molecular dynamics. The
incorporation of aluminate species in the C-A-S-H gel modifies the silicate-
aluminate skeleton and interlayer water molecules. On the one hand, the bridging
silicate tetrahedron is substituted by the aluminate species that polymerize with
defective silicate chains, improve the crystalline order, enhance the Qspecies
connectivity, and transform the layered C-S-H structure to cross-linked branch of
C-A-S-H gel. On the other hand, the Al-Si substitution enhances the reactivity of
the bridging oxygen sites in Si-O-Al, which contributes to more interlayer water
molecules dissociation into the hydroxyl groups at high Al/Si ratio. The
incorporated Al atoms, associating with silicate oxygen atoms, interlayer waters,
and hydroxyl groups form the tetra/penta/octahedron local structures. Al-O-Si
cross-links can not only exert geometry restriction on the interlayer water
molecules but also increases the substrate affinity toward water molecules, which
stabilizes the interlayer H-bond connection and significantly reduce the mobility
of water molecules. Furthermore, uniaxial tensile test is utilized to study the
mechanical behavior and deformation mechanism of the cross-linking C-A-S-H gel.
Both the interlayer cohesive strength and stiffness of the C-A-S-H gel is
significantly enhanced with the increasing of the aluminate branch structures that
resist the tensile loading and strengthen the soft interlayer zone. Besides, during
the tensile failure process, the mechanical response of the C-A-S-H gel is coupled
with depolymerization of silicate-aluminate chains and the hydrolytic reaction of
interlayer water molecules.
C1 [Yang, Jun; Ding, Qingjun] Wuhan Univ Technol, Sch Mat Sci & Engn, 122 Luoshi
Rd, Wuhan 430070, Hubei, Peoples R China.
[Hou, Dongshuai] Qingdao Technol Univ, Dept Civil Engn, 11 Fushun Rd, Qingdao
C3 Wuhan University of Technology; Qingdao University of Technology
RP Hou, DS (corresponding author), Qingdao Technol Univ, Dept Civil Engn, 11 Fushun
Rd, Qingdao 266033, Peoples R China.
EM dshou@outlook.com
RI Yang, jun/GRY-0158-2022
OI Hou, Dongshuai/0000-0002-1252-2987
FU China Ministry of Science and Technology [2015CB655101]; National
FX Financial support from the China Ministry of Science and Technology
(under Grant 2015CB655101) and the National Natural Science Foundation
of China (under Grant 51778513) are gratefully acknowledged.
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NR 68
TC 28
Z9 31
U1 4
U2 81
PI WASHINGTON
SN 2168-0485
PD JUL
PY 2018
VL 6
IS 7
BP 9403
EP 9417
PG 29
GA GU0FK
UT WOS:000444924500145
DA 2023-12-05
ER
PT J
AU Isert, S
Lane, CD
Gunduz, IE
Son, SF
AF Isert, Sarah
Lane, Colin D.
Gunduz, I. Emre
Son, Steven F.
TI Tailoring burning rates using reactive wires in composite solid rocket
propellants
SO PROCEEDINGS OF THE COMBUSTION INSTITUTE
LA English
DT Article
DE Embedded wires; Ammonium perchlorate composite propellant; Enhanced
burning rate; Mechanically-activated powder; Self-alloying materials
ID METAL WIRES; COMBUSTION; AGGLOMERATION; ALUMINUM
AB Tailoring solid propellant burning rates is a perpetual goal of solid propellant
designers. Many methods have been used to alter the burning rate including changing
the propellant formulation, adding burning rate modifiers, and changing the
propellant core shape. Alternatively, metallic fibers such as copper and silver
have been added to propellants to increase the burning rate by providing fast heat
diffusion paths. However, these metallic wires do not significantly add further to
the energetics and have a limited tailoring range. In this paper we describe the
effect of embedding mechanically-activated aluminum/polytetrafluoroethylene
(Al/PTFE) reactive foils, nickel/aluminum nanofoils and Pyrofuze (R) self-alloying
wirein an AP/HTPB composite propellant. We quantify the resulting burning rate and
compare the burning rate to propellants with embedded copper wires. We find that
the nickel/aluminum nanofoils and Pyrofuze (R) wire provide a constant increase in
local burning rate regardless of pressure, while the local burning rates of
propellants with Al/PTFE foils change as a function of pressure. The Al/PTFE foil
is consumed, releasing significant gas, unlike the other materials investigated.
The Al/PTFE foil combustion products contribute to the energy and gas production of
the propellant, resulting in a propellant efficiency larger than typical wired
propellants. While the other materials increase propellant burning rate by causing
an increase in surface area and therefore mass burning rate, the aluminum and
carbon liberated by the Al/PTFE wire reaction can oxidize with the propellant
products and increase the temperature of the combustion gases. Additionally,
Al/PTFE or similar reactive wires could result in a decrease in slag production
compared to inert and self-alloying wires (i.e., copper, nickel/aluminum nanofoils
and Pyrofuze (R)) and may be better suited to use in propellants due to the high
burning rate tailorability and the participation in propellant combustion. (C) 2016
by The Combustion Institute. Published by Elsevier Inc.
C1 [Isert, Sarah; Gunduz, I. Emre; Son, Steven F.] Purdue Univ, Maurice J Zucrow
Labs, 500 Allison, W Lafayette, IN 47905 USA.
[Lane, Colin D.] United States Air Force Acad, Dept Engn Mech, Colorado Springs,
CO 80840 USA.
C3 Purdue University System; Purdue University; Purdue University West
Lafayette Campus
RP Isert, S (corresponding author), Purdue Univ, Maurice J Zucrow Labs, 500
Allison, W Lafayette, IN 47905 USA.
EM sarah.isert@gmail.com
FU NSF GRFP Grant [1147384]; AFOSR MURI contract [FA9550-13-1-0004]; Direct
For Education and Human Resources; Division Of Graduate Education
[1147384] Funding Source: National Science Foundation
FX Thanks to Dr. B. Tappan of Los Alamos National Laboratories and Dr. B.
Terry of Purdue University, for providing the Pyrofuze and Al/PTFE, and
Andrew McBain for experimental assistance. This research was conducted
with funding through NSF GRFP Grant no. 1147384 and AFOSR MURI contract
#FA9550-13-1-0004 with Mitat Birkan as Program Manager.
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WINCH PC, 1988, J PROPUL POWER, V4, P104, DOI 10.2514/3.23037
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Zaseck CR, 2013, COMBUST FLAME, V160, P184, DOI
10.1016/j.combustflame.2012.10.001
NR 27
TC 28
Z9 35
U1 3
U2 31
PI NEW YORK
PA 360 PARK AVE SOUTH, NEW YORK, NY 10010-1710 USA
SN 1540-7489
EI 1873-2704
J9 P COMBUST INST
JI Proc. Combust. Inst.
PY 2017
VL 36
IS 2
BP 2283
EP 2290
DI 10.1016/j.proci.2016.06.141
PG 8
WC Thermodynamics; Energy & Fuels; Engineering, Chemical; Engineering,
Mechanical
GA EP5ZY
UT WOS:000397458900072
OA hybrid
DA 2023-12-05
ER
PT J
AU Chen, CT
Nguyen, HA
Chang, TP
Yang, TR
Nguyen, TD
AF Chen, Chun-Tao
Hoang-Anh Nguyen
Chang, Ta-Peng
Yang, Tzong-Ruey
Tien-Dung Nguyen
TI Performance and microstructural examination on composition of hardened
paste with no-cement SFC binder
LA English
DT Article
DE CFBC fly ash; Fly ash; Slag; Compressive strength; No-cement
ID C-S-H; FLUIDIZED-BED COMBUSTION; BLAST-FURNACE SLAG; FLY-ASH; HYDRATION;
PRODUCTS; STRENGTH; COAL
AB This research aims to present the engineering performance and microstructural
examination on compositions of hardened paste with a no-cement SFC binder, which is
fabricated with mixture of ground granulated blast furnace slag (GGBFS) (S), Type F
fly ash (FA) (F) and circulating fluidized bed combustion (CFBC) fly ash (C).
Specimens with four FA/GGBFS weight ratios (0, 1/9, 3/7 and 1) are prepared to
estimate the effects of FA on the engineering performance. CFBC fly ash, around 10-
25 wt.% of the mixture, is used as the main activator. The results show that the
optimum mixtures are obtained by 15-20 wt.% CFBC fly ash and 10-30 wt.% FA. They
have higher compressive strengths than those without FA The early hydration of CFBC
fly ash and GGBFS provides sufficient alkalis and releases heat, both play a
crucial role in the pozzolanic reaction of FA particles. The main hydration
products of the hardened paste are ettringite (AFt) and calcium aluminum silicate
hydrate (C-A-S-H) gel, as examined by scanning electron microscopy (SEM) and X-ray
diffraction (XRD). (C) 2014 Elsevier Ltd. All rights reserved.
C1 [Chen, Chun-Tao; Hoang-Anh Nguyen; Chang, Ta-Peng; Yang, Tzong-Ruey; Tien-Dung
Nguyen] Natl Taiwan Univ Sci & Technol NTUST Taiwan Tech, Dept Civil & Construct
Engn, Taipei 106, Taiwan.
[Hoang-Anh Nguyen] Cantho Univ, Coll Engn Technol, Dept Civil Engn, Cantho City,
Vietnam.
C3 Can Tho University
RP Chang, TP (corresponding author), Natl Taiwan Univ Sci & Technol NTUST Taiwan
Tech, Dept Civil & Construct Engn, Taipei 106, Taiwan.
RI Nguyen, Tien-Dung/AAD-9608-2021
OI Nguyen, Dung T./0000-0001-9102-4072; Chen, Chun-Tao/0000-0003-2038-2205
Tech)
FX The authors would like to acknowledge the financial aid from National
Taiwan University of Science and Technology (NTUST) (Taiwan Tech) for
this investigation.
10.1016/j.cemconres.2003.10.009
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10.1016/j.resconrec.2007.04.002
NR 28
TC 28
Z9 28
U1 1
U2 11
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD FEB 1
PY 2015
VL 76
BP 264
EP 272
DI 10.1016/j.conbuildmat.2014.11.032
PG 9
GA CA4MX
UT WOS:000348879600026
DA 2023-12-05
ER
PT J
AU Karsch, T
Bomas, H
Zoch, HW
Mändl, S
AF Karsch, T.
Bomas, H.
Zoch, H. -W.
Maendl, S.
TI Influence of hydrogen content and microstructure on the fatigue
behaviour of steel SAE 52100 in the VHCF regime
SO INTERNATIONAL JOURNAL OF FATIGUE
LA English
DT Article
DE Very high cycle fatigue (VHCF); SAE 52100; Hydrogen; Optically bright
zone (OBZ); Fine grain area (FGA)
ID CHROMIUM-BEARING STEEL; HIGH-STRENGTH STEELS; SUBSURFACE CRACK
INITIATION; LONG-LIFE FATIGUE; MECHANISM; LIMIT; IRON; CLASSIFICATION;
EMBRITTLEMENT; PROPAGATION
AB The fatigue life of the bearing steel 52100 (100Cr6) in bainite and martensite
conditions was investigated up to 2 x 10(9) cycles. The tests were performed under
cycling tension (R = 0.1) and tension-compression (R = -1) on a piezo-electric
ultrasonic testing equipment. The specimens are designed with a cylindrical part in
the highly stressed centre. Due to grinding, compressive residual stresses are
found at the surface, hence crack initiation solely occurs subsurface. Prior
testing half of the specimens was charged with hydrogen. The hydrogen content
varies from 0.6 as initial condition to 3 ppm after charging. The increased
hydrogen content decreased the endurance limit to nearly half of the value of
uncharged conditions and crack initiation changed: Conditions with low hydrogen
content failed from chromium carbides, titanium nitrides or slag agglomerations.
Conditions with 3 ppm hydrogen failed from slag agglomerations, often in
combination with aluminium magnesium oxides, and manganese sulphides. Next to the
inclusions a fine granular area (FGA) could be observed in some cases, and nearly
all fractured surfaces showed a fisheye surrounded by an Optically Bright Zone
(OBZ) with the crack initiating inclusion in its centre. Furthermore, selected
specimens where analysed using secondary ion mass spectroscopy in a time of flight
setup (ToF-SIMS) to ascertain the local hydrogen content. From the results it is
assumed that hydrogen accumulates in the cavity at inclusions or bonds to the
inclusion if it contains silicon. (C) 2013 Elsevier Ltd. All rights reserved.
C1 [Karsch, T.; Bomas, H.; Zoch, H. -W.] Stiftung Inst Werkstofftech, IWT, D-28359
Bremen, Germany.
[Maendl, S.] Leibniz Inst Oberflachenmodifizierung, D-04318 Leipzig, Germany.
C3 Leibniz Institut fur Oberflachenmodifizierung (IOM)
RP Karsch, T (corresponding author), Stiftung Inst Werkstofftech, IWT, D-28359
Bremen, Germany.
EM karsch@iwt-bremen.de
OI Zoch, Hans-Werner/0000-0002-4347-4746
FU Deutsche Forschungsgemeinschaft (DFG, German Research Foundation) [INST
144/268-1, ZO 140/7]; Hans L. Merkle-Stiftung [T 113/16843/07]
FX The authors gratefully acknowledge financial support by Deutsche
Forschungsgemeinschaft (DFG, German Research Foundation) under Contract
Number INST 144/268-1 FUGG for buying one of the testing systems. The
scientific work was subsidised by the "Hans L. Merkle-Stiftung" under
contract number T 113/16843/07 and by Deutsche Forschungsgemeinschaft
(DFG, German Research Foundation) under Contract Number ZO 140/7.
CR [Anonymous], KORROSION KORROSIONS
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NR 38
TC 28
Z9 31
U1 1
U2 51
PU ELSEVIER SCI LTD
PI OXFORD
SN 0142-1123
EI 1879-3452
J9 INT J FATIGUE
JI Int. J. Fatigue
PD MAR
PY 2014
VL 60
BP 74
EP 89
DI 10.1016/j.ijfatigue.2013.09.006
PG 16
WC Engineering, Mechanical; Materials Science, Multidisciplinary
GA AA5TF
UT WOS:000331161800011
DA 2023-12-05
ER
PT J
AU Jung, SM
Fruehan, RJ
AF Jung, SM
Fruehan, RJ
TI Thermodynamics of titanium oxide in ladle slags
LA English
DT Article
DE ladle slags; titanium oxide; activity; silicon-added stainless steel;
aluminum-killed steel
ID NITROGEN
AB It is necessary to have information on the thermodynamic behavior of titanium
oxide in ladle type stags in order to control the titanium content in several
grades of steel. In the present study, the thermodynamics was determined from the
equilibrium between Fe-C-sat-Ti and CaO-SiO2-30%Al2O3-MgO-TiOx stags in equilibrium
with CO and from the equilibrium between Fe-C-sat-(16 similar to 18)%Cr-Si-Ti and
CaO-SiO2- 20%Al2O3-MgO-TiOx stags in equilibrium with CO. From the experiment with
Fe-C-sat-Ti alloy, the activity coefficients of TiO1 5 and TiO2 vary with basicity
from 0.3 to 1.5 and from 0.5 to 2.3, respectively. And from the experiment with Fe-
C-sat-(16 similar to 18)%Cr-Si-Ti alloy, the activity coefficients of TiO1.5 and
TiO2 vary with basicity from 0.4 to 1.4 and from 0.6 to 3.5, respectively. The
results obtained from the equilibrium between Fe-C-sat-(16 similar to 18)%Cr-Si-Ti
and CaO-SiO2-20%Al2O3-MgO-TiOx stags were used to estimate the titanium content of
silicon-added stainless steel. Experiments were also conducted using Fe-Al-Ti melts
in equilibrium with CaO-SiO2-Al2O3-TiOx stags saturated with MgO. In this case most
of the titanium in the slag is present as TiO2(Ti4+). The present results were used
to predict the titanium content of aluminum-killed steel in equilibrium with ladle
stags containing titanium oxide and the predictions agreed with plant data.
RP Jung, SM (corresponding author), Pohang Univ Sci & Technol, Grad Sch Iron &
Steel Technol, Pohang 790784, South Korea.
CR BENESCH R, 1989, THERMOCHIM ACTA, V152, P433, DOI 10.1016/0040-6031(89)85411-5
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NR 14
TC 28
Z9 33
U1 0
U2 10
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2001
VL 41
IS 12
BP 1447
EP 1453
PG 7
GA 504FJ
UT WOS:000172846400005
OA gold
DA 2023-12-05
ER
PT J
AU CHO, SW
SUITO, H
AF CHO, SW
SUITO, H
TI ALUMINUM DEOXIDATION EQUILIBRIUM IN LIQUID NI-FE ALLOYS EQUILIBRATED
WITH CAO-AL2O3 SLAGS
SO STEEL RESEARCH
LA English
DT Article
ID OXYGEN; NICKEL; MELTS
AB The deoxidation equilibrium for Al in Ni-Fe alloys was studied in the
equilibrium experiments between CaO-Al2O3 slags and Fe-30, 50 and 70 % Ni alloys at
1873 K. By using the values for the first and second order interaction parameters
between oxygen and nickel in liquid iron and those between oxygen and iron in
liquid nickel, the effect of Ni on the activity coefficient of Al in liquid iron
and that of Fe on the activity coefficient of Al in liquid nickel were determined
in the whole composition range of Ni-Fe alloys. The oxygen contents in Ni-Fe alloys
calculated by the iterative method based on pure iron were in good agreement with
those based on pure nickel in the range of [% Al] < 0.03. From this fact, it was
found that the Wagner's approximation relating to the multi-component solution was
applicable to the deoxidation equilibrium in the whole composition range of Ni-Fe
alloys in the restricted concentration of a deoxidizer.
RP CHO, SW (corresponding author), TOHOKU UNIV,INST ADV MAT PROC,SENDAI,MIYAGI
980,JAPAN.
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NR 26
TC 28
Z9 29
U1 0
U2 1
PI DUSSELDORF
SN 0177-4832
J9 STEEL RES
JI Steel Res.
PD JUN
PY 1995
VL 66
IS 6
BP 237
EP 243
DI 10.1002/srin.199501118
PG 7
GA RF456
UT WOS:A1995RF45600002
DA 2023-12-05
ER
PT J
AU INOUE, R
SUITO, H
AF INOUE, R
SUITO, H
TI CALCIUM DESULFURIZATION EQUILIBRIUM IN LIQUID-IRON
SO STEEL RESEARCH
LA English
DT Article
ID CAO-AL2O3 MELTS; OXYGEN; SULFUR; STEEL; SLAGS; SOLUBILITY; NITROGEN
AB Sulfur distribution ratios between CaO-Al2O3 slags and liquid iron were measured
at 1873 K as a function of aluminum content using an alumina or a lime crucible.
Activity coefficients of CaS relative to a solid standard state were obtained as
52+/-2.6 and 23+/-1.7 for the CaO-Al2O3 slags saturated with an Al2O3 and a CaO
crucible, respectively, in the concentration range up to the CaS solubility limit.
From these results, logarithm of the equilibrium constant, log K(CaS), for the
calcium desulfurization reaction CaS(s) = Ca + S and the first-order interaction
parameter e(S)Ca (e(S)Ca) were estimated to be -8.72+/-0.27 and -269+/-28 (-336+/-
35), respectively.
RP INOUE, R (corresponding author), TOHOKU UNIV,INST ADV MAT PROC,SENDAI,MIYAGI
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NR 26
TC 28
Z9 30
U1 0
U2 3
PI DUSSELDORF
SN 0177-4832
J9 STEEL RES
JI Steel Res.
PD OCT
PY 1994
VL 65
IS 10
BP 403
EP 409
DI 10.1002/srin.199401184
PG 7
GA PR358
UT WOS:A1994PR35800001
DA 2023-12-05
ER
PT J
AU Maniraj, S
Thanigaivelan, R
AF Maniraj, S.
Thanigaivelan, R.
TI Effect of electrode heating on performance of electrochemical
micromachining
SO MATERIALS AND MANUFACTURING PROCESSES
LA English
DT Article
DE Electrochemical; micromachining; overcut; aluminum; composites;
material; removal; rate; conicity; factor; heated; electrode
AB This paper investigates the effect of process parameters on aluminum metal
matrix composites using electrochemical micromachining (EMM). In EMM, the
electrolyte temperature plays a vital role in enhancing the reaction rate. Hence,
in this research, an innovative method of electrolyte heating is proposed for
improving the performance of the EMM. The experiments are conducted with a heated
electrode (HE) in which the temperature of the electrode is controlled with closed-
loop control system. The input parameters such as applied voltage (V), duty cycle
(%), electrolytic concentration (g/l) along with the temperature of the tool
electrode (degrees C) are varied on output performance like material removal rate,
conicity factor (CF) and radial overcut (ROC). The workpiece is made up of aluminum
6061 with 12% composition of ground granulated blast furnace slag reinforcement and
sodium nitrate (NaNO3) is used as an electrolyte. Based on the conducted
experiments, HE improves the machining rate by 88.37%, reduces the ROC by 37.03%
and reduces the CF by 33.33% at 8 V, 90% duty cycle, 35 g/l electrolyte
concentration and 60celcius electrode temperature.
C1 [Maniraj, S.] Paavai Engn Coll Autonomous, Mech Engn, Pachal 637018, India.
[Thanigaivelan, R.] Muthayammal Engn Coll Autonomous, Mech Engn, Rasipuram,
India.
C3 Muthayammal Engineering College
RP Maniraj, S (corresponding author), Paavai Engn Coll Autonomous, Mech Engn,
Pachal 637018, India.
EM maniraj4016@gmail.com
RI R, Thanigaivelan/AAB-9435-2022; SEKAR, MANIRAJ/IYJ-7139-2023
OI Rajasekaran, Thanigaivelan/0000-0001-9514-9120; S,
Maniraj/0000-0003-0911-6651
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NR 26
TC 27
Z9 27
U1 1
U2 15
PI PHILADELPHIA
SN 1042-6914
EI 1532-2475
J9 MATER MANUF PROCESS
JI Mater. Manuf. Process.
PD OCT 3
PY 2019
VL 34
IS 13
BP 1494
EP 1501
DI 10.1080/10426914.2019.1655153
EA AUG 2019
PG 8
WC Engineering, Manufacturing; Materials Science, Multidisciplinary
GA JA4MX
UT WOS:000482890600001
DA 2023-12-05
ER
PT J
AU Sankar, K
Sutrisno, A
Kriven, WM
AF Sankar, Kaushik
Sutrisno, Andre
Kriven, Waltraud M.
TI Slag-fly ash and slag-metakaolin binders: Part IIProperties of
precursors and NMR study of poorly ordered phases
LA English
DT Article
ID C-S-H; CALCIUM SILICATE HYDRATE; ALKALINE ACTIVATION; MICROSTRUCTURAL
DEVELOPMENT; SELECTIVE DISSOLUTION; TRICALCIUM SILICATE; GEL;
ALUMINOSILICATE; CEMENT; AL-27
AB Sodium silicate-activated slag-fly ash binders (SFB) and slag-metakaolin binders
(SMKB) are room-temperature hardening binders that have excellent mechanical
properties and a significantly lower carbon footprint than ordinary Portland cement
(OPC). The aim of this study was to use nuclear magnetic resonance (NMR)
spectroscopy to study the nanostructure of poorly ordered phases in SFB by varying
slag/fly ash ratio, curing time, and curing temperature. Fly ash was completely
substituted with metakaolin and the effect of this substitution on the poorly
ordered phases was studied. It was observed that the proportion of geopolymer was
generally higher in SMKB when compared to SFB. Although C-N-A-S-H and geopolymer
coexisted in SFB and SMKB, C-N-A-S-H was the major product phase formed. The mean
chain length (MCL) and the structure of C-N-A-S-H gel were estimated as a function
of time, temperature, and slag/fly ash ratio. The MCL was found to have a negative
correlation with slag/fly ash ratio and Ca/(Si+Al) ratio, but positive correlation
with curing temperature. The average Si/Al atom ratios for geopolymers were also
estimated. Lastly, the increased proportion of five-coordinated aluminum (Al(V)) in
metakaolin resulted in the decreased unreacted metakaolin in the hardened binder
but did not increase the geopolymer content.
C1 [Sankar, Kaushik; Kriven, Waltraud M.] Univ Illinois, Dept Mat Sci & Engn,
Urbana, IL 61820 USA.
[Sutrisno, Andre] Univ Illinois, NMR EPR Lab, Sch Chem Sci, Urbana, IL USA.
University of Illinois System; University of Illinois Urbana-Champaign
RP Kriven, WM (corresponding author), Univ Illinois, Dept Mat Sci & Engn, Urbana,
IL 61820 USA.
EM kriven@illinois.edu
RI Sankar, Kaushik/Y-2152-2019; Sutrisno, Andre/N-9908-2015
OI Sankar, Kaushik/0000-0001-8837-7854; Kriven,
Waltraud/0000-0002-2983-5760; Sutrisno, Andre/0000-0003-2308-5708
FU US Army Corps of Engineers through the Construction Engineering Research
laboratory (CERL), Champaign
FX US Army Corps of Engineers through the Construction Engineering Research
laboratory (CERL), Champaign though Dr. Ghassan Al-Chaar
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NR 80
TC 27
Z9 29
U1 8
U2 39
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD JUN
PY 2019
VL 102
IS 6
BP 3204
EP 3227
DI 10.1111/jace.16224
PG 24
GA HU5VK
UT WOS:000465347700019
DA 2023-12-05
ER
PT J
AU Zhang, Y
Guo, ZH
Han, ZY
Xiao, XY
Peng, C
AF Zhang, Yong
Guo, Zhao-hui
Han, Zi-yu
Xiao, Xi-yuan
Peng, Chi
TI Feasibility of aluminum recovery and MgAl2O4
spinel synthesis from secondary aluminum dross
LA English
DT Article
DE secondary aluminum dross; reuse; extraction; sintering; magnesium
aluminate spinel
ID DISORDER TRANSITION; BAUXITE RESIDUE; TEMPERATURE; FABRICATION;
KINETICS; WASTE
AB The feasibility of aluminum recovery from secondary aluminum dross by extraction
with NaOH solution and the subsequent synthesis of MgAl2O4 spinel by sintering the
extracted slag were studied. The extraction percentage of soluble aluminum from the
dross reached 80% at a temperature of 353 K, liquid-to-solid ratio of 12 mLg( -1),
stirring speed of 300 rmin( -1), and an extraction time of 15 min; the hydrolysis
percentage of AlN reached 40% with an extraction time of 30 min. The activation
energies of the soluble aluminum and AlN extracted from the dross were 7.15 and
8.98 kJmol( -1), respectively, indicating that their kinetics were controlled by
outer diffusion without a product layer. The extracted slag was sintered in the
temperature range 1373-1773 K; MgAl2O4 spinel with a compressive strength as high
as 69.4 MPa was produced in the sample sintered at 1673 K for 3 h. This value
exceeds the threshold (40 MPa) prescribed by the National Standard for the Magnesia
and Magnesia-alumina Refractory Bricks of China (GB/T 2275-2007). These results
establish the effectiveness of aluminum recovery from secondary aluminum dross and
subsequent MgAl2O4 spinel synthesis.
C1 [Zhang, Yong; Guo, Zhao-hui; Han, Zi-yu; Xiao, Xi-yuan; Peng, Chi] Cent S Univ,
Sch Met & Environm, Changsha 410083, Hunan, Peoples R China.
RP Guo, ZH (corresponding author), Cent S Univ, Sch Met & Environm, Changsha
EM zhguo@csu.edu.cn
RI Xiao, Xiao/IAN-3011-2023; Peng, Chi/A-8110-2012; Xiao,
Xiao/GQP-7793-2022; Peng, Chi/AAV-3780-2021; xiao, xiang/GWU-6035-2022
OI Peng, Chi/0000-0003-3332-184X; Peng, Chi/0000-0003-3332-184X;
FU National Natural Science Foundation of China [21577176]; Environment
Protection Scientific Research Project of Hunan Province, China
[[2016]59-3]
Foundation of China (No. 21577176) and the Environment Protection
Scientific Research Project of Hunan Province, China (No. [2016]59-3).
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NR 35
TC 27
Z9 28
U1 5
U2 95
PU SPRINGER
PI NEW YORK
SN 1674-4799
EI 1869-103X
PD MAR
PY 2019
VL 26
IS 3
BP 309
EP 318
DI 10.1007/s12613-019-1739-3
PG 10
Mineral Processing
GA HO3TE
UT WOS:000460845000006
DA 2023-12-05
ER
PT J
AU Cai, LX
Li, XG
Ma, BG
Lv, Y
AF Cai, Lixiong
Li, Xiangguo
Ma, Baoguo
Lv, Yang
TI Effect of binding materials on carbide slag based high utilization
solid-wastes autoclaved aerated concrete (HUS-AAC): Slurry,
physic-mechanical property and hydration products
LA English
DT Article
DE High utilization solid-wastes; Autoclaved aerated concrete; Binding
materials; Slurry property; Physic-mechanical property; Hydration
products
ID RHEOLOGICAL PROPERTIES; IRON-TAILINGS; CO2 CAPTURE; CEMENT;
MICROSTRUCTURE; PASTES; QUARTZ; SI-29
AB With the objective of adjusting rough-body foaming and thickening stability of
carbide slag based high utilization solid-wastes autoclaved aerated concrete (HUS-
AAC) during pre-curing process, the effect of binding material composition and
admixture on slurry, physic-mechanical property and hydration products were
investigated to put forward an appropriate slurry performance adjustment scheme.
Slurry properties include slump flow, time-dependent theological, and gas foaming
properties. Slump flow was conducted to estimate the initial fluidity of primary
slurry with different ordinary portland cement 42.5 (OPC42.5) content and sulphate
aluminium cement (SAC) substitution ratio. The slurry time dependent shear stress,
apparent viscosity and gas foaming property were measured to evaluate the rough-
body stability during the coupling of foaming and thickening process. Physic-
mechanical properties were carried out to evaluating the influence of binding
materials on applicability. The mineral composition (XRD), thermal characteristics
(TG-DSC) and crystal characteristics (Si-29-NMR) of carbide slag based HUS-AAC
hydration products were analyzed to making a thorough inquiry in the influence
mechanism of binding materials on the mechanical properties. The results indicated
that increasing OPC42.5 content can modify slurry properties in a small range,
which was unable to meet the slurry adjustment target. Introducing of SAC can
improve rough-body stability and shorten pre-curing time of HUS-MC effectively. On
the other hand, increasing proportion of OPC42.5 and SAC both has indistinctive
effect on bulk density and positive effect on compressive strength of NUS-MC.
Furthermore, increment of OPC42.5 content resulted in increscent crystallinity and
quantity of tobermorite, however, addition of SAC led to the opposite effect. The
enhancement effect of SAC on HUS-MC may attribute to the strengthen of pore
partition material caused by substituting microcelluiar structure filling particles
from soft white to tough quartz, which is equivalent to increase the strength of
aggregate in pore partition material. In conclusion, from the angle of rough-body
pre-curing stability and efficiency, and mechanical properties, the conventional
OPC42.5 can be substituted by SAC completely. (C) 2018 Elsevier Ltd. All rights
reserved.
C1 [Cai, Lixiong] Huazhong Univ Sci & Technol, Sch Civil Engn & Mech, Wuhan, Hubei,
Peoples R China.
[Li, Xiangguo; Ma, Baoguo; Lv, Yang] Wuhan Univ Technol, State Key Lab Silicate
Mat Architectures, Wuhan, Hubei, Peoples R China.
[Cai, Lixiong] Hubei Engn Res Ctr Virtual Safe & Automated Const, Wuhan, Hubei,
Peoples R China.
C3 Huazhong University of Science & Technology; Wuhan University of
Technology
RP Cai, LX (corresponding author), Huazhong Univ Sci & Technol, Sch Civil Engn &
Mech, Wuhan, Hubei, Peoples R China.
EM cailixiong@hust.edu.cn
OI Cai, Lixiong/0000-0003-3177-8897
FU State Key Laboratory of Silicate Materials for Architectures (Wuhan
University of Technology) [SYSJJ2018-17]
FX This work was supported by State Key Laboratory of Silicate Materials
for Architectures (Wuhan University of Technology) (SYSJJ2018-17).
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NR 39
TC 27
Z9 28
U1 1
U2 61
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD NOV 10
PY 2018
VL 188
BP 221
EP 236
DI 10.1016/j.conbuildmat.2018.08.115
PG 16
GA GX2WA
UT WOS:000447579600020
DA 2023-12-05
ER
PT J
AU Sima, TV
Letshwenyo, MW
Lebogang, L
AF Sima, Thandie Veronicah
Letshwenyo, Moatlhodi Wise
Lebogang, Lesedi
TI Efficiency of waste clinker ash and iron oxide tailings for phosphorus
removal from tertiary wastewater: Batch studies
SO ENVIRONMENTAL TECHNOLOGY & INNOVATION
LA English
DT Article
DE Adsorption; Phosphorus removal; Clinker ash; Iron oxide tailings
ID AQUEOUS-SOLUTION; ADSORPTION; PHOSPHATE; EQUILIBRIUM; SLAG; KINETICS;
CARBON; MEDIA; BLUE
AB Phosphorus removal from wastewater using waste materials as novel adsorbents has
been gaining attention. This work exploits and compares phosphorus adsorption
capacities of iron oxide tailings and clinker ash waste from the copper-nickel mine
(BCL LTD) in Botswana. The surface heterogeneity of the media was investigated
using scanning electron microscope, which revealed a highly porous structure of
clinker ash as compared to iron oxide tailings. The chemical and mineralogical
composition was determined using the X-ray Fluorescence and X-ray Diffractometer
respectively. The adsorption kinetics, equilibrium isotherms and regeneration
potential of the media were investigated through batch experiments at room
temperature using real wastewater. XRF results revealed 25.1% of iron oxide in
tailings and 5.3% for clinker ash. The concentrations of aluminium oxide were 5.4%
and 11.7% for tailings and clinker ash respectively. Small amounts of phosphorus
were present in both media before the experiment and there was an increase of
phosphorus in used tailings whereas in clinker ash there was a reduction of
phosphorus suggesting retention of phosphorus by tailings and desorption by clinker
ash. Pseudo second order model best described the kinetics of adsorption onto both
media with R2 values of 0.99 for both media compared to pseudo first values of 0.98
and 0.96 for tailings and clinker ash respectively, suggesting that chemisorption
was the dominant force. Intra-particle diffusion model revealed that intra-particle
diffusion was not the solely rate controlling mechanism but other mechanisms such
as mass transfer were involved as well. The equilibrium data for both iron oxide
tailings and clinker ash were best described by Langmuir model, which suggested a
monolayer adsorption process with homogeneous distribution of energies. The batch
results (Langmuir) indicate that iron oxide tailings have a higher phosphorus
removal capacity (1.29 mg P g_1 media) than clinker ash (0.29 mg P g_1 media). The
iron oxide tailings demonstrated high regeneration potential with 87%, 81% and 56%
phosphorus removed during first, second and third cycle compared to 24%, 5% and
0.6% shown by clinker ash. This study demonstrated that these two mine wastes have
capabilities to remove phosphorus, with iron oxide tailings having more potential
than clinker ash. Iron oxide tailings is a better phosphorus adsorbent, thus it
could be utilised in improving the quality of wastewaters as well as providing a
waste disposal option for the mine. (C) 2018 Elsevier B.V. All rights reserved.
C1 [Sima, Thandie Veronicah; Letshwenyo, Moatlhodi Wise; Lebogang, Lesedi] Botswana
Int Univ Sci & Technol, Fac Engn & Technol, Palapye, Botswana.
[Sima, Thandie Veronicah; Letshwenyo, Moatlhodi Wise] Dept Civil & Environm
Engn, Palapye, Botswana.
[Lebogang, Lesedi] Dept Biol Sci & Biotechnol, Fac Sci, Private Bag 16, Palapye,
Botswana.
RP Letshwenyo, MW (corresponding author), Botswana Int Univ Sci & Technol, Fac Engn
& Technol, Palapye, Botswana.
EM thandie.sima@studentmail.biust.ac.bw; letshwenyom@biust.ac.bw;
lebogangl@biust.ac.bw
RI Letshwenyo, Moatlhodi/V-7177-2019
OI Marata, Thandie Veronicah/0000-0002-3262-9765
FU Botswana International University of Science and Technology
FX This study was conducted through Thandie Sima's postgraduate studies
sponsored by Botswana International University of Science and
Technology.
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Xiong JB, 2010, DESALINATION, V259, P59, DOI 10.1016/j.desal.2010.04.035
Zhang XL, 2016, WATER RES, V96, P280, DOI 10.1016/j.watres.2016.03.063
Zheng XL, 2014, PROCESS BIOCHEM, V49, P2207, DOI 10.1016/j.procbio.2014.10.008
NR 36
TC 27
Z9 28
U1 3
U2 46
PU ELSEVIER
PI AMSTERDAM
SN 2352-1864
J9 ENVIRON TECHNOL INNO
JI Environ. Technol. Innov.
PD AUG
PY 2018
VL 11
BP 49
EP 63
DI 10.1016/j.eti.2018.04.008
PG 15
WC Biotechnology & Applied Microbiology; Engineering, Environmental;
SC Biotechnology & Applied Microbiology; Engineering; Environmental
Sciences & Ecology
GA GP1ZX
UT WOS:000440618800005
DA 2023-12-05
ER
PT J
AU Wang, JX
Lyu, XJ
Wang, LY
Cao, XQ
Zang, HY
Liu, Q
AF Wang, Junxiang
Lyu, XianJun
Wang, Lingyun
Cao, Xiaoqiang
Zang, Haoyu
Liu, Qing
TI Effect of Anhydrite on the Hydration of Calcium Oxide-Activated Ground
Granulated Blast Furnace Slag Binders
SO SCIENCE OF ADVANCED MATERIALS
LA English
DT Article
DE Calcium Oxide-Activated Slag; Anhydrite; Mechanisms; Hydration
Properties; Products
ID SODIUM-CARBONATE; PHOTOCATALYTIC ACTIVITY; ELEVATED-TEMPERATURES;
STRENGTH DEVELOPMENT; ROOM-TEMPERATURE; CEMENT; CONCRETE; MORTARS;
COMPOSITES; ETTRINGITE
AB To explore the potential use of anhydrite in calcium oxide-activated ground
granulated blast furnace slag binders, this paper investigated the influence of
anhydrite on the compressive strength, the pH of the pore solution and the non-
evaporable water content for up to 28 days. The hydration products were studied by
X-ray diffraction, thermogravimetric analysis, nuclear magnetic resonance
spectroscopy and scanning electron microscopy combined with energy-dispersive X-ray
spectroscopy. Mechanical tests showed that the optimal anhydrite content was 5 wt.%
of the total binder regardless of the curing time. The increase in compressive
strength was mainly due to the formation of ettringite, which had a beneficial
reinforcing effect in the matrix. Although a higher anhydrite content (over 5 wt.%)
resulted in a remarkable increase in the non-evaporable water content, it did not
make any contribution to the compressive strength due to the decrease in the
calcium silicate hydrate gels content. Additionally, the presence of anhydrite
inhibited the formation of hydrotalcite-like phases because most aluminum ions were
incorporated into ettringite. It was also found that the addition of anhydrite
reduced the mean chain length and aluminum proportion of the calcium aluminum
silicate hydrate gels.
C1 [Wang, Junxiang; Lyu, XianJun; Cao, Xiaoqiang; Zang, Haoyu; Liu, Qing] Shandong
Univ Sci & Technol, Coll Chem & Environm Engn, Qingdao 266590, Peoples R China.
[Wang, Lingyun] Shandong Univ Sci & Technol, Coll Mat Sci & Engn, Qingdao
C3 Shandong University of Science & Technology; Shandong University of
Science & Technology
RP Lyu, XJ (corresponding author), Shandong Univ Sci & Technol, Coll Chem &
Environm Engn, Qingdao 266590, Peoples R China.
EM lvyxianjun@163.com
FU National Natural Science Foundation of China [51674161]; Key Research
and Development Program of Shandong Province [2016GSF116013]; Research
Fund for the Doctoral Program of Higher Education of China
[20133718110005]
China (51674161), the Key Research and Development Program of Shandong
Province (2016GSF116013) and the Research Fund for the Doctoral Program
of Higher Education of China (20133718110005). The authors also express
their gratitude to American Journal Experts for language editing.
CR Abdalqader AF, 2016, J CLEAN PROD, V113, P66, DOI 10.1016/j.jclepro.2015.12.010
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Deng F, 2016, SCI ADV MATER, V8, P1737, DOI 10.1166/sam.2016.2768
8846(03)00208-4
10.1016/j.cemconcomp.2014.09.001
10.1016/j.cemconres.2008.03.004
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10.1016/j.conbuildmat.2013.08.013
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10.1016/j.cemconres.2015.02.014
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10.1016/j.conbuildmat.2015.01.022
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Yan K, 2016, SCI ADV MATER, V8, P1454, DOI 10.1166/sam.2016.2758
10.1016/j.conbuildmat.2011.10.063
10.1016/j.conbuildmat.2009.09.001
Yang KC, 2016, SCI ADV MATER, V8, P2253, DOI 10.1166/sam.2016.2885
Yang L, 2015, SCI ADV MATER, V7, P1858, DOI 10.1166/sam.2015.2419
Yang WQ, 2018, POLYM ENG SCI, V58, P1127, DOI 10.1002/pen.24675
Yao Y, 2016, SCI ADV MATER, V8, P2133, DOI 10.1166/sam.2016.2840
Yuan B, 2017, CERAM INT, V43, P6039, DOI 10.1016/j.ceramint.2017.01.144
Yuan XH, 2014, CONSTR BUILD MATER, V66, P422, DOI
10.1016/j.conbuildmat.2014.05.085
Zhang L, 2017, J ELECTROCHEM SOC, V164, pH651, DOI 10.1149/2.1531709jes
NR 60
TC 27
Z9 27
U1 2
U2 48
PU AMER SCIENTIFIC PUBLISHERS
PI VALENCIA
PA 26650 THE OLD RD, STE 208, VALENCIA, CA 91381-0751 USA
SN 1947-2935
EI 1947-2943
J9 SCI ADV MATER
JI Sci. Adv. Mater.
PD DEC
PY 2017
VL 9
IS 12
BP 2214
EP 2222
DI 10.1166/sam.2017.3248
PG 9
WC Nanoscience & Nanotechnology; Materials Science, Multidisciplinary;
Physics, Applied
SC Science & Technology - Other Topics; Materials Science; Physics
GA FS4IX
UT WOS:000419755000024
DA 2023-12-05
ER
PT J
AU Javali, S
Chandrashekar, AR
Naganna, SR
Manu, DS
Hiremath, P
Preethi, HG
Kumar, NV
AF Javali, Shriraksha
Chandrashekar, A. R.
Naganna, Sujay Raghavendra
Manu, D. S.
Hiremath, Parameshwar
Preethi, H. G.
Kumar, N. Vinod
TI Eco-concrete for sustainability: utilizing aluminium dross and iron slag
as partial replacement materials
SO CLEAN TECHNOLOGIES AND ENVIRONMENTAL POLICY
LA English
DT Article
DE Eco-concrete; Aluminium dross; Iron slag; Sustainability; Toxicity
analysis
ID RAW-MATERIAL; WASTE; STRENGTH; INDUSTRY; RESIDUE; ASH
AB Emphasis on utilizing the industrial waste/discarded materials can be brought
about by discovering innovative methods of disposal. One such a way of waste
disposal can be through utilizing them in concrete production as a filler material
or pozzolana. In this regard, the present study proposes to use the aluminium dross
and granular iron slag as partial replacement materials for cement and natural
sand, respectively, to develop eco-concrete. Nine mixes were produced with
different proportions of cement, aluminium dross, sand and granular iron slag
content. The aluminium dross was replaced at 5, 10, 15 and 20% of the weight of the
cement. Initially, the optimal substitution percentage of aluminium dross was found
without the substitution of iron slag based on the strength results. Later, by
adopting the optimal aluminium dross percentage with cement, the granular iron slag
was partially substituted at 10, 20, 30 and 40% of natural sand to find the overall
optimal blend. The strength and durability properties of the M40 grade concrete
employing these two admixture combinations were analysed. It was noticed that the
strength and durability properties of the eco-concrete produced by incorporating
aluminium dross -5% and iron slag -20% were comparable to that of conventional
concrete. Furthermore, from the toxicity analysis, it was seen that the leaching of
heavy and trace elements from the eco-concrete was negligibly small and within the
limits. In near future, the cost-effective, eco-friendly materials and technologies
can be opted as a perpetual strategy to overcome severe material shortages for
resource conservation and economy.
C1 [Javali, Shriraksha; Preethi, H. G.] REVA Inst Technol & Management, Dept Civil
Engn, Bangalore 560064, Karnataka, India.
[Chandrashekar, A. R.] Vijaya Vittala Inst Technol, Dept Civil Engn, Bangalore
560077, Karnataka, India.
[Naganna, Sujay Raghavendra] Natl Inst Technol Karnataka, Dept Appl Mech &
Hydraul, Mangalore 575025, India.
[Manu, D. S.; Hiremath, Parameshwar] Natl Inst Technol Karnataka, Dept Civil
Engn, Mangalore 575025, India.
[Kumar, N. Vinod] Acharya Inst Technol, Dept Civil Engn, Bangalore 560107,
Karnataka, India.
C3 REVA University; National Institute of Technology (NIT System); National
Institute of Technology Karnataka; National Institute of Technology (NIT
System); National Institute of Technology Karnataka
RP Naganna, SR (corresponding author), Natl Inst Technol Karnataka, Dept Appl Mech
& Hydraul, Mangalore 575025, India.
EM sujay.am14f03@nitk.edu.in
RI Hiremath, Parameshwar N/AAS-6051-2020; Naganna, Sujay
Raghavendra/D-2871-2014
OI Hiremath, Parameshwar N/0000-0001-9997-7329; Naganna, Sujay
Raghavendra/0000-0002-0482-1936; D S, MANU/0000-0003-4870-8342
FU Chemical Engineering Department, National Institute of Technology
Karnataka; FIST fund of Department of Science and Technology, Government
of India
FX The authors would like to thank the Assistant Executive Engineer of
Quality Assurance Laboratory, Public Works, Port and Internal Water
Transport Department, Dharwad, for allowing access to the experimental
facilities and the laboratory staff for their help and assistance during
experimentation. We are deeply indebted to Nikita Metallurgicals Pvt.
Limited, Raipur, for providing us sufficient quantity of aluminium dross
used in the research. The authors would like to acknowledge the support
from Chemical Engineering Department, National Institute of Technology
Karnataka, for letting us to conduct tests using Inductively Coupled
Plasma Optical Emission Spectroscopy (ICP-OES) equipment procured from
the FIST fund of Department of Science and Technology, Government of
India.
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construction
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NR 38
TC 27
Z9 27
U1 3
U2 20
PU SPRINGER
PI NEW YORK
SN 1618-954X
EI 1618-9558
J9 CLEAN TECHNOL ENVIR
JI Clean Technol. Environ. Policy
PD NOV
PY 2017
VL 19
IS 9
BP 2291
EP 2304
DI 10.1007/s10098-017-1419-9
PG 14
& Ecology
GA FK6NB
UT WOS:000413619300010
DA 2023-12-05
ER
PT J
AU Miganei, L
Gock, E
Achimovicová, M
Koch, L
Zobel, H
Kähler, J
AF Miganei, Leila
Gock, Eberhard
Achimovicova, Marcela
Koch, Lutz
Zobel, Horst
Kaehler, Joerg
TI New residue-free processing of copper slag from smelter
LA English
DT Article
DE Copper slag; Leaching kinetics; Residue-free processing; Mass balance;
Products characterization
ID CEMENT
AB Deposited copper slag originated from a region Mansfeld (Saxony-Anhalt, Germany)
was characterized from mineralogical, chemical and structural point of view for
purpose of its sustained processing and removal. Subsequently hydrometallurgical
processing of copper slag was investigated because of extraction of metals as Zn,
Cu, Ni, Co, Mo, Cr, V and Fe in total content about 5%. Although the slags with
their mineralogical composition of calcium, magnesium, aluminum, and iron silicates
are perfectly suitable as building materials, their cumulative heavy metal content
prevents this. Novel residue-free recycling process for copper smelter slag was
developed which consists of sorting, roasting, leaching with HCl, carbonate
precipitation, precipitate complexation and solvent extraction of metals steps.
This process solves the problem with calcium silicate matrix which enclosed
dissolved metals. By setting pH of leaching process to 2.5, 80-90% of Cu can be
extracted and dissolution of silicate matrix can be prevented. Mass balance of
process strategy indicates the proceeds from four marketable products: blasting
agent, cement additive, metal salts solution, and fertilizer, which make the
process more economical with sustainable benefits. Economic evaluation of new
process is also done and confirmed its utility and favourable balance. (C) 2017
C1 [Miganei, Leila; Gock, Eberhard; Achimovicova, Marcela; Kaehler, Joerg] Tech
Univ Clausthal, Inst Mineral & Waste Proc Waste Disposal & Geomec, Walther Nernst
Str 9, D-38678 Clausthal Zellerfeld, Germany.
[Koch, Lutz; Zobel, Horst] Projektservice GbR Eisleben, Wolferoder Weg 14, D-
06295 Lutherstadt Eisleben, Germany.
[Achimovicova, Marcela] Slovak Acad Sci, Inst Geotech, Watsonova 45, Kosice
04001, Slovakia.
C3 TU Clausthal; Slovak Academy of Sciences; Institute of Geotechnics, SAS
RP Achimovicová, M (corresponding author), Tech Univ Clausthal, Inst Mineral &
Waste Proc Waste Disposal & Geomec, Walther Nernst Str 9, D-38678 Clausthal
Zellerfeld, Germany.
EM marcela.achimovicova@tu-clausthal.de
RI Achimovicova, Marcela/ABE-8585-2020
OI Achimovicova, Marcela/0000-0002-0533-8866
FU German Federal Ministry for Education and Research (BMBF) [FKZ033RK017B]
FX We would like to thank the German Federal Ministry for Education and
Research (BMBF) FKZ033RK017B for financial support.
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10.1016/j.conbuildmat.2015.08.021
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Organization U.N.I.D. Center I.F.D., 1979, FERT MAN
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Zobel H., 2016, FICZ033RK017B BMBF
NR 22
TC 27
Z9 27
U1 2
U2 43
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD OCT 15
PY 2017
VL 164
BP 534
EP 542
DI 10.1016/j.jclepro.2017.06.209
PG 9
& Ecology
GA FF8TM
UT WOS:000409290700050
DA 2023-12-05
ER
PT J
AU Li, SJ
Cheng, GG
Miao, ZQ
Chen, L
Li, CW
Jiang, XY
AF Li, Shi-jian
Cheng, Guo-guang
Miao, Zhi-qi
Chen, Lie
Li, Cheng-wei
Jiang, Xin-yan
TI Kinetic Analysis of Aluminum and Oxygen Variation of G20CrNi2Mo Bearing
Steel during Industrial Electroslag Remelting Process
LA English
DT Article
DE bearing steel; ESR; slag-metal reaction; kinetic analysis; oxygen
variation
AB Kinetics of slag-metal reactions was investigated in order to elucidate the
mechanism of AI-oxidation and oxygen increase during industrial electroslag
remelting (ESR) process. G20CrNi2Mo bearing steel was utilized as the consumable
electrode and remelted using a 2 400-kg industrial ESR furnace. It was found that
with the content of FeO in the slag increasing from 0.20 wt% to 0.45 wt%, the
content of oxygen increased from 12 ppm in electrode to 16 ppm, 21 ppm in the ingot
while Al decreased from 0.040 wt% in the electrode to 0.031 wt%, 0.019 wt% in the
ingot. Based on penetration and film theories, a kinetic model has been developed.
The model indicates that Al in the electrode is mainly oxidized by FeO at the metal
film. Increase of soluble oxygen mainly occurs during the time of droplet formation
and falling. The content of soluble oxygen occupies about fifty percent of the
total oxygen. The rate-determining step of Al-oxidation is the mass transfer of Al
at metal side, whereas oxygen increase lies in the mass transfer of FeO at slag
side. With the content of FeO increasing from 0.20 wt% to 0.45 wt%, the mass
transfer resistance of FeO decreases obviously, thus would result in an increase of
Al-oxidation and total oxygen. In order to improve the cleanliness of refined
ingot, it is more effective to decrease the oxygen potential of slag pool to a
minimum level, or decrease the time of droplet formation and the temperature of
slag pool to some extent, rather than improve the Al content in the electrode.
C1 [Li, Shi-jian; Cheng, Guo-guang; Miao, Zhi-qi] Univ Sci & Technol Beijing, State
Key Lab Adv Met, Beijing 100083, Peoples R China.
[Chen, Lie; Li, Cheng-wei; Jiang, Xin-yan] Xining Special Steel Grp Co Ltd,
Xining 810005, Qinghai, Peoples R China.
RP Cheng, GG (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
EM chengguoguang@metall.ustb.edu.cn
RI Li, Chengwei/ISB-3373-2023
FU National Natural Science Foundation of China [51674024]; Xining Special
Steel Plant
FX The authors gratefully wish to express their thanks to Xining Special
Steel Plant and National Natural Science Foundation of China (Grant Nos.
51674024) for their financial support for this study.
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NR 18
TC 27
Z9 28
U1 0
U2 12
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 12
BP 2148
EP 2156
PG 9
GA FR3UR
UT WOS:000418992600009
DA 2023-12-05
ER
PT J
AU Ren, Y
Zhang, LF
AF Ren, Ying
Zhang, Lifeng
TI Thermodynamic Model for Prediction of Slag-Steel-Inclusion Reactions of
304 Stainless Steels
LA English
DT Article
DE thermodynamic model; slag; inclusions; 304 stainless steels
ID OF-THE-ART; DEOXIDATION EQUILIBRIA; NONMETALLIC INCLUSIONS; REOXIDATION
BEHAVIOR; MOLTEN STEEL; LIQUID-IRON; CALCIUM; ALUMINUM;
304-STAINLESS-STEEL; DESULFURIZATION
AB A thermodynamic model was developed to predict slag steel inclusion reactions of
304 stainless steels. The dissolved aluminum in the steel, the sulfur distribution
ratio and the composition of inclusions equilibrated with varying slags were
predicted using the current model. The model can also be widely used to predict the
liquid fraction of inclusions. For Al-killed 304 stainless steels, the optimized
composition of CaO Al2O3 SiO2 MgO slags is proposed to modify solid Al2O3
inclusions to liquid CaO Al2O3 MgO at 1 873 K. For Si-Mn-killed 304 stainless
steels, the optimized composition of CaO-SiO2-MgO-Al2O3-20%CaF2 slags is suggested
to suppress the formation of Al2O3 MgO in SiO2 CaO MnO MgO Al2O3 inclusions and
lower their melting temperatures.
C1 [Ren, Ying; Zhang, Lifeng] Univ Sci & Technol Beijing, Sch Met & Ecol Engn, 30
Xueyuan Rd, Beijing 100083, Peoples R China.
Engn, 30 Xueyuan Rd, Beijing 100083, Peoples R China.
FU National Science Foundation China [51274034, 51334002, 51404019];
Beijing Key Laboratory of Green Recycling and Extraction of Metals
(GREM); Laboratory of Green Process Metallurgy and Modeling (GPM2); High
Quality steel Consortium (HQSC) at the School of Metallurgical and
Ecological Engineering at University of Science and Technology Beijing
(USTB), China
FX The authors are grateful for support from the National Science
Foundation China (Grant No. 51274034, No. 51334002, and No. 51404019),
Beijing Key Laboratory of Green Recycling and Extraction of Metals
(GREM), the Laboratory of Green Process Metallurgy and Modeling
(GPM2) and the High Quality steel Consortium (HQSC) at the
School of Metallurgical and Ecological Engineering at University of
Science and Technology Beijing (USTB), China.
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NR 49
TC 27
Z9 30
U1 4
U2 39
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 1
BP 68
EP 75
PG 8
GA EJ0FU
UT WOS:000392884800010
OA gold
DA 2023-12-05
ER
PT J
AU Seco, A
Miqueleiz, L
Prieto, E
Marcelino, S
García, B
Urmeneta, P
AF Seco, A.
Miqueleiz, L.
Prieto, E.
Marcelino, S.
Garcia, B.
Urmeneta, P.
TI Sulfate soils stabilization with magnesium-based binders
LA English
DT Article
DE Sulfate soil; Soil stabilization; Valorization; Construction material;
Ettringite
ID DELAYED ETTRINGITE FORMATION; HEAT-CURED MORTARS; C FLY-ASH;
GEOTECHNICAL PROPERTIES; SWELLING CLAYS; MARLY SOILS; SLAG GGBS; LIME;
CEMENT; THAUMASITE
AB Sulfate soils' stabilization is a very interesting subject with technical,
economic and environmental implications. The difficulty of their stabilization is
due to the fact that the usual stabilizer additives are based on calcium. In these
soils, sulfate combines with the calcium from the additive and the aluminum from
the clay, resulting in a highly hydrated expansive mineral named ettringite. This
provokes the swelling of the treated material and even its destruction. This study
analyzes the result of the substitution of the calcium based additives by one
alternative additive based on magnesium, an industrial byproduct named PC-8, in the
stabilization of five different sulfate soils. From a mechanical point of view
soils treated with PC-8 reached similar resistance values to the lime treated ones,
of about 2-3 MPa for 4% dosage and 2-5 MPa for 8% dosage, being usually better with
the PC-8 results than with the lime ones. When PC-8 was combined with GGBS the
resistance values increased up to 11-13 MPa and the lime-GGBS reached the 6-7 MPa.
The natural swelling of the soils treated with PC-8 decreased substantially and
maintained constant even for immersion at long-term. In the case of the soils
treated with lime, long-term swelling increased up to very high values even in the
case of soils without natural swelling. XRD analysis of these samples demonstrated
the existence of ettringite in 4 of the 5 soils when they were treated with lime
and there was not expansive minerals in the PC-8 treated soils, agreeing with the
swelling observed behavior of the soils when treated with both additives. (C) 2016
C1 [Seco, A.; Miqueleiz, L.; Prieto, E.; Marcelino, S.] Univ Publ Navarra, Dept
Projects & Rural Engn, Pamplona 31006, Spain.
[Garcia, B.] Univ Basque Country, Ingn Cartog Geodes & Fotogrametria, Vitoria
01006, Spain.
[Urmeneta, P.] Magnesitas Navarras SA, Zubiri 31630, Spain.
C3 Universidad Publica de Navarra; University of Basque Country
RP Seco, A (corresponding author), Univ Publ Navarra, Dept Projects & Rural Engn,
Pamplona 31006, Spain.
EM andres.seco@unavarra.es; Imiqueleiz@gmail.com; epc@unavarra.es;
sara.marcelino@unavarra.es; benat.garcia@ehu.eus;
p.urmeneta@magnesitasnavarras.es
RI García, Beñat/AAE-3278-2020; Seco, Andres/K-6694-2017; Prieto,
Eduardo/I-2873-2016; Marcelino, Sara/M-5178-2017
OI García, Beñat/0000-0002-8925-4677; Seco, Andres/0000-0003-3156-6624;
Prieto, Eduardo/0000-0001-5039-3517; Marcelino,
Sara/0000-0001-8824-9676; Mikeleiz Elarre, Itziar/0000-0002-8139-400X
FU Magnesitas de Navarra S.A. Company [OTRI 2011021091]
FX This research has been supported by research project OTRI 2011021091
with Magnesitas de Navarra S.A. Company.
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NR 37
TC 27
Z9 28
U1 3
U2 36
PI AMSTERDAM
SN 0169-1317
EI 1872-9053
J9 APPL CLAY SCI
JI Appl. Clay Sci.
PD JAN
PY 2017
VL 135
BP 457
EP 464
DI 10.1016/j.clay.2016.10.033
PG 8
GA EF8ZZ
UT WOS:000390621800050
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Lin, G
Zhuang, Q
Cui, Q
Wang, HY
Yao, HQ
AF Lin, Guo
Zhuang, Qiang
Cui, Qun
Wang, Haiyan
Yao, Huqing
TI Synthesis and adsorption property of zeolite FAU/LTA from lithium slag
with utilization of mother liquid
LA English
DT Article
DE Lithium slag; FAU/LTA; Co-crystalline zeolite; Mother liquid; Detergent
builder
ID GREEN
AB Co-crystalline zeolite FAU/LTA-0 was synthesized by hydrothermal method from
lithium slag. To make the most of excess silicon and alkali sources in mother
liquid derived from FAU/LTA-0, zeolite FAU/LTA-1b was synthesized in the same
method with the use of mother liquid by adding a certain amount of aluminum source.
Influences of different adding ways of aluminum source and recycling dosages of
mother liquid on synthesis of zeolites FAU/LTA with mother liquid were
investigated. The phase, microstructure and thermostability of FAU/LTA-0 and
FAU/LTA-1b were characterized by XRD, SEM and TG-DTA. The calcium and magnesium
cation exchange capacities (CECs) of the zeolites were determined. The results have
shown that co-crystalline zeolite can be synthesized with the use of mother liquid
by adding aluminum source after 2 h of reaction. Compared with FAU/LTA-0, the
crystal twinning structure of FAU/LTA-1b became weaker, the grain size was smaller,
and the thermostability was better. With a lower dosage of mother liquid, the
content of P-type impurity in product decreased significantly, and the content of
LTA phase increased. The reuse rate of mother liquid can reach 48%. The CECs of
FAU/LTA-1b-150 can reach 343 mg CaCO3.g(-1) and 180 mg MgCO3.g(-1), showing more
excellent adsorption capacities than FAU/LTA-0 and commercial zeolite 4A. The full
recycling use of mother liquid to synthesize zeolite FAU/LTA which can be applied
for detergent not only improves resource utilization but also reduces production
cost. (C) 2015 The Chemical Industry and Engineering Society of China, and Chemical
Industry Press. All rights reserved.
C1 [Lin, Guo; Zhuang, Qiang; Cui, Qun; Wang, Haiyan; Yao, Huqing] Nanjing Tech
Univ, Coll Chem Engn, Nanjing 210009, Peoples R China.
C3 Nanjing Tech University
RP Cui, Q (corresponding author), Nanjing Tech Univ, Coll Chem Engn, Nanjing
EM cuiqun@njtech.edu.cn
FX Supported by the National Natural Science Foundation of China
(51476074).
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NR 20
TC 27
Z9 30
U1 5
U2 94
PU CHEMICAL INDUSTRY PRESS CO LTD
PI BEIJING
PA NO 13, QINGNIANHU SOUTH ST, DONGCHENG DIST, BEIJING 100011, PEOPLES R
CHINA
SN 1004-9541
EI 2210-321X
PD NOV
PY 2015
VL 23
IS 11
BP 1768
EP 1773
DI 10.1016/j.cjche.2015.10.001
PG 6
SC Engineering
GA CZ7HZ
UT WOS:000367271800005
DA 2023-12-05
ER
PT J
AU Sun, Y
Zheng, HY
Dong, Y
Jiang, X
Shen, YS
Shen, FM
AF Sun, Yu
Zheng, Haiyan
Dong, Yue
Jiang, Xin
Shen, Yansong
Shen, Fengman
TI Melting and separation behavior of slag and metal phases in metallized
pellets obtained from the direct-reduction process of vanadium-bearing
titanomagnetite
SO INTERNATIONAL JOURNAL OF MINERAL PROCESSING
LA English
CT 2nd Australia-China Joint Symposium of Minerals and Metallurgy
CY JUL 23-25, 2014
CL Sydney, AUSTRALIA
DE Vanadium-bearing titanomagnetite; Metallized pellet; Melting and
separation
AB With increasing attention to environment and energy issues, it is important to
utilize vanadium-bearing titanomagnetite resource effectively in ironmaking
industry. In this paper, melting and separation behavior of metallization pellets
produced in a direct-reduction process of vanadium-bearing titanomagnetite was
studied. The results showed that the effective separation of slag and metal phases
could be obtained in which over 95% Fe was transferred into metal phase and over
90% Ti was remained in slag under the conditions of reducing atmosphere and
complete carburizing; there were some inclusions of residual carbon and sulfur in
the metal phase; the main components in the slag are geikielite, titanium oxide,
aluminum silicate, magnesium silicate, and a small amount of iron and its oxides;
the complete separation of slag and metal phases was achieved at the condition of
1500 degrees C, holding time of 50 min, reducing atmosphere, and limited
carburization; it was considered that the melting and separation process of
metallization pellet could be divided into three stages of which slag and metal
respectively and sequentially melted and gathered, the molten slag leaked while
metallized pellet shrank, and then the slag and metal phases separated from each
other completely. (C) 2015 Elsevier B.V. All rights reserved.
C1 [Sun, Yu; Zheng, Haiyan; Dong, Yue; Jiang, Xin; Shen, Fengman] Northeastern
Univ, Sch Mat & Met, Shenyang 110819, Peoples R China.
[Shen, Yansong] Monash Univ, Dept Chem Engn, Clayton, Vic 3800, Australia.
C3 Northeastern University - China; Monash University
RP Zheng, HY (corresponding author), Northeastern Univ, Sch Mat & Met, Shenyang
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OI Shen, Yansong/0000-0001-8472-8805
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NR 47
TC 27
Z9 28
U1 2
U2 23
PI AMSTERDAM
SN 0301-7516
EI 1879-3525
J9 INT J MINER PROCESS
JI Int. J. Miner. Process.
PD SEP 10
PY 2015
VL 142
SI SI
BP 119
EP 124
DI 10.1016/j.minpro.2015.04.002
PG 6
GA CR8CS
UT WOS:000361579300018
DA 2023-12-05
ER
PT J
AU Gil, A
Albeniz, S
Korili, SA
AF Gil, A.
Albeniz, S.
Korili, S. A.
TI Valorization of the saline slags generated during secondary aluminium
melting processes as adsorbents for the removal of heavy metal ions from
aqueous solutions
LA English
DT Article
DE Saline slags; Secondary aluminium; Industrial wastes; Heavy metal
cations; Adsorption
ID ACTIVATED RED MUD; INDUSTRY WASTE; SURFACE-AREA; SALT CAKE; MANAGEMENT;
ADSORPTION; SORPTION; DYE
AB This work describes the surface properties of saline slags generated during
secondary aluminium melting processes and the application of these materials as
adsorbents for the removal of Cd(II), Cu(II), Pb(II) and Zn(II) from aqueous
solutions. Saline slags were chemically treated with aqueous solutions of HNO3,
H2SO4 and NaOH of varying concentrations (0, 0.5, 1, 1.5 and 2 mol/dm(3)) for 0.5,
4 and 24 h. Nitrogen adsorption at -196 degrees C was used to study the textural
properties of the solids. The specific surface area and pore volume decrease as the
chemical reagent concentrations and duration of the treatments increase. Solids
with a surface area of up to 109 m(2)/g are obtained. The adsorption of heavy metal
ions has been studied in terms of pseudo-first-order and pseudo-second-order
kinetics, and several isotherm models have also been applied to the equilibrium
adsorption data at various values. The adsorption capacity of the saline slags was
maintained after several cycles of reuse. (C) 2014 Elsevier B.V. All rights
reserved.
C1 [Gil, A.; Albeniz, S.; Korili, S. A.] Univ Publ Navarra, Dept Appl Chem, E-31006
Pamplona, Spain.
RP Gil, A (corresponding author), Univ Publ Navarra, Dept Appl Chem, Bldg Los
Acebos,Campus Arrosadia, E-31006 Pamplona, Spain.
FU Spanish Ministry of Environment [A554/2007/3-11.1]
FX This work was supported by the Spanish Ministry of Environment
(A554/2007/3-11.1). The authors thank Iberica de Aleaciones Ligeras,
Ltd., IDALSA, for the provided information.
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NR 24
TC 27
Z9 27
U1 1
U2 42
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD SEP 1
PY 2014
VL 251
BP 43
EP 50
DI 10.1016/j.cej.2014.04.056
PG 8
SC Engineering
GA AL0FJ
UT WOS:000338802500006
DA 2023-12-05
ER
PT J
AU Fagerström, J
Näzelius, IL
Gilbe, C
Boström, D
Öhman, M
Boman, C
AF Fagerstrom, Jonathan
Nazelius, Ida-Linn
Gilbe, Carl
Bostrom, Dan
Ohman, Marcus
Boman, Christoffer
TI Influence of Peat Ash Composition on Particle Emissions and Slag
Formation in Biomass Grate Co-combustion
SO ENERGY & FUELS
LA English
DT Article
ID HIGH-TEMPERATURE CORROSION; BED AGGLOMERATION; STRAW COMBUSTION;
RELEASE; TRANSFORMATION; DEPOSITION; MECHANISMS; OPERATION; ADDITIVES;
MIXTURES
AB Co-combustion by fuel blending of peat and biomass has shown positive effects on
operational problems. However, peat ash compositions vary considerably, and this
has been shown to affect the potential for operational problems in different fuel-
blending situations. The present work used three different peat types with the
objective to elucidate how the variation in peat ash composition influences both
particle emissions and slag formation during co-combustion with three different
biomasses in a small-scale pellet boiler. Estimations of potassium release and slag
formation were performed and discussed in relation to fuel composition in the (K2O
+ Na2O) (CaO + MgO) (SiO2) system. All tested peat types reduced the fine particle
emissions by capturing potassium into the bottom ash as one or several of the
following forms: slag, sulfates, chlorides, and alumina silicates. However, there
were considerable differences between the peat types, presumably depending upon
both their content and mineral composition of silicon, calcium, aluminum, and
sulfur. Some general important and beneficial properties of peat type in co-
combustion situations with biomass are defined here, but the specific blending
proportion of peat should be decided on an individual basis for each scenario based
on the relative contents in the fuel mixture of the most relevant ash-forming
elements.
C1 [Fagerstrom, Jonathan; Bostrom, Dan; Boman, Christoffer] Umea Univ, Dept Appl
Phys & Elect, Thermochem Energy Convers Lab, SE-90187 Umea, Sweden.
[Nazelius, Ida-Linn; Gilbe, Carl; Ohman, Marcus] Lulea Univ Technol, Div Energy
Sci, SE-97187 Lulea, Sweden.
C3 Umea University; Lulea University of Technology
RP Fagerström, J (corresponding author), Umea Univ, Dept Appl Phys & Elect,
Thermochem Energy Convers Lab, SE-90187 Umea, Sweden.
EM jonathan.fagerstrom@umu.se
FU Varmeforsk (Swedish Thermal Engineering Research Institute); Swedish
Energy Agency; Bio4Energy
FX The Biofuel Technology Centre (BTC) at the Swedish Agricultural
University in Lima is acknowledged for the help with pelletizing the
fuels. Varmeforsk (Swedish Thermal Engineering Research Institute),
Swedish Energy Agency, and Bio4Energy are acknowledged for the financial
support.
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NR 37
TC 27
Z9 27
U1 0
U2 59
PI WASHINGTON
SN 0887-0624
EI 1520-5029
J9 ENERG FUEL
JI Energy Fuels
PD MAY
PY 2014
VL 28
IS 5
BP 3403
EP 3411
DI 10.1021/ef4023543
PG 9
GA AH5VN
UT WOS:000336199300063
DA 2023-12-05
ER
PT J
AU Engström, F
Larsson, ML
Samuelsson, C
Sandström, Å
Robinson, R
Björkman, B
AF Engstrom, Fredrik
Larsson, Margareta Lidstrom
Samuelsson, Caisa
Sandstrom, Ake
Robinson, Ryan
Bjorkman, Bo
TI Leaching Behavior of Aged Steel Slags
LA English
DT Article
DE steel slag; leaching; slag ageing; slag properties; carbonation
ID CO2 SEQUESTRATION; CARBONATION; POROSITY; PRODUCTS
AB Large amounts of slag are generated by the Swedish Steel Industry each year. The
Electric Arc Furnace process generates about 200000ton of slag per annum, from
which approximately 40% is deposited. An alternative to deposit is to use slag as
road construction material. However, leaching of metals from the slag can be a
reason to limit slag use in road construction. The aim of this work was to
investigate how stable these materials are when aged, in an environment open to
seasonable weather conditions, with respect to leaching and mineralogy. Three
different EAF-slags from domestic steel plants were used in this study. The
materials were characterized after 0, 6, 12, 18, and 24 months to evaluate the
ageing process. The analytical techniques that were used to evaluate the effect of
ageing are scanning electron microscopy (SEM), X-ray powder diffraction (XRD) and a
standard test for leaching. The changes in ageing behavior differ between the three
materials. The conductivity and the pH decreases with time for all samples. The
leaching of calcium, chromium as well as aluminum decreases with time while the
leaching of magnesium increases. CaCO3 was formed on slag surfaces as CaO reacts
with moisture and CO2 from the air.
C1 [Engstrom, Fredrik; Larsson, Margareta Lidstrom; Samuelsson, Caisa; Sandstrom,
Ake; Robinson, Ryan; Bjorkman, Bo] Lulea Univ Technol, Div Sustainable Proc Engn,
Minerals & Met Res Lab, SE-97187 Lulea, Sweden.
C3 Lulea University of Technology
RP Engström, F (corresponding author), Lulea Univ Technol, Div Sustainable Proc
Engn, Minerals & Met Res Lab, SE-97187 Lulea, Sweden.
EM fredrik.i.engstrom@ltu.se
FU MiMeR (Minerals and Metals Research Laboratory); CAMM (Centre of
Advanced Mining and Metallurgy); VINNOVA; Swedish Steel producers'
Association via MISTRA
FX We wish to thank MiMeR (Minerals and Metals Research Laboratory), CAMM
(Centre of Advanced Mining and Metallurgy), VINNOVA and the Swedish
Steel producers' Association via MISTRA, for invaluable financial
support and commitment as well as colleagues and company members for
their support and assistance.
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NR 18
TC 27
Z9 28
U1 2
U2 30
PI WEINHEIM
SN 1611-3683
EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD APR
PY 2014
VL 85
IS 4
BP 607
EP 615
DI 10.1002/srin.201300119
PG 9
GA AE3WS
UT WOS:000333909700012
DA 2023-12-05
ER
PT J
AU Cwirzen, A
Punkki, J
Engblom, R
Habermehl-Cwirzen, K
AF Cwirzen, Andrzej
Punkki, Jouni
Engblom, Ronny
Habermehl-Cwirzen, Karin
TI Effects of curing: comparison of optimised alkali-activated PC-FA-BFS
and PC concretes
SO MAGAZINE OF CONCRETE RESEARCH
LA English
DT Article
ID FLY-ASH; CEMENT PASTES; MICROSTRUCTURE; METAKAOLIN; HYDRATION
AB The effects of curing on the mechanical properties, chemical composition,
microstructure and shrinkage of optimised alkali-activated concretes (AACs) based
on ternary mixtures of fly ash (FA), blast-furnace slag (BFS) and Portland cement
(PC) were compared. Heat treatment was found to accelerate the early-age strength
development of both the PC concrete and the AAC. The long-term strength of AAC was
not adversely affected by the heat treatment after 90 d of dry curing. Water curing
slightly enhanced the ultimate long-term strength of non-heat-treated AAC specimens
but had barely any effect on the heat-treated specimens. Conversely, the dry-cured
PC specimens showed a significant decrease in long-term compressive strength. The
ultimate drying shrinkage of the PC concrete was lower compared with the AAC,
independent of the type of applied curing. In the case of AAC, the drying shrinkage
was significantly decreased by the application of heat treatment while water curing
did not have any measurable effect. Conversely, the drying shrinkage of AAC cured
at ambient temperatures was decreased with the application of water curing.
Compared with the PC concrete, the microstructure of the AAC samples was denser and
more homogeneous without visible microcracking of the binder matrix. The dominant
phases were geopolymer and calcium silicate hydrate (C-S-H) gels intermixed with
probably sodium and aluminium ions and crystalline inclusions of zeolitic
hydroxysodalite. A large amount of unreacted FA and BFS was observed in the
hardened binder matrix of the AAC specimens. At the same time, no anhydrous PC was
observed, thus indicating its extensive dissolution and contribution to the
formation of the modified C-S-H gel.
C1 [Cwirzen, Andrzej; Engblom, Ronny; Habermehl-Cwirzen, Karin] Aalto Univ, Sch
Engn, Dept Civil & Struct Engn, Espoo, Finland.
[Punkki, Jouni] Consolis Technol Oy, Vantaa, Finland.
C3 Aalto University
RP Cwirzen, A (corresponding author), Aalto Univ, Sch Engn, Dept Civil & Struct
Engn, Espoo, Finland.
RI cwirzen, andrzej/AAV-1299-2021; Habermehl-Cwirzen, Karin/AAM-9658-2020
OI Cwirzen, Andrzej/0000-0001-6287-2240
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10.1016/j.conbuildmat.2012.07.041
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[Anonymous], 2009, Testing hardened concrete part 3: Compressive strength of
test specimens
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4
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NR 38
TC 27
Z9 27
U1 0
U2 30
PU ICE PUBLISHING
PI WESTMINISTER
SN 0024-9831
EI 1751-763X
J9 MAG CONCRETE RES
JI Mag. Concr. Res.
PY 2014
VL 66
IS 6
BP 315
EP 323
DI 10.1680/macr.13.00231
PG 9
GA AD4VH
UT WOS:000333248900005
DA 2023-12-05
ER
PT J
AU Kinoshita, H
Swift, P
Utton, C
Carro-Mateo, B
Marchand, G
Collier, N
Milestone, N
AF Kinoshita, Hajime
Swift, Paul
Utton, Claire
Carro-Mateo, Beatriz
Marchand, Geraldine
Collier, Nick
Milestone, Neil
TI Corrosion of aluminium metal in OPC- and CAC-based cement matrices
LA English
DT Article
DE Radioactive waste; Corrosion; Blended cement; Calcium aluminate cement
ID CONTAINING REFRACTORY CASTABLES; COMPOSITE CEMENTS; PORTLAND-CEMENT;
NUCLEAR-WASTES; CALCIUM; SULFATE; SYSTEM
AB Corrosion of aluminium metal in ordinary Portland cement (OPC) based pastes
produces hydrogen gas and expansive reaction products causing problems for the
encapsulation of aluminium containing nuclear wastes. Although corrosion of
aluminium in cements has been long known, the extent of aluminium corrosion in the
cement matrices and effects of such reaction on the cement phases are not well
established. The present study investigates the corrosion reaction of aluminium in
OPC, OPC-blast furnace slag (BFS) and calcium aluminate cement (CAC) based systems.
The total amount of aluminium able to corrode in an OPC and 4:1 BFS:OPC system was
determined, and the correlation between the amount of calcium hydroxide in the
system and the reaction of aluminium obtained. It was also shown that a CAC-based
system could offer a potential matrix to incorporate aluminium metal with a further
reduction of pH by introduction of phosphate, producing a calcium phosphate cement.
Crown Copyright (c) 2013 Published by Elsevier Ltd. All rights reserved.
C1 [Kinoshita, Hajime; Swift, Paul; Utton, Claire] Univ Sheffield, Dept Mat Sci &
[Carro-Mateo, Beatriz] Univ Publ Navarra, Pamplona 31007, Spain.
[Marchand, Geraldine] Natl Inst Appl Sci INSA Lyon, F-69621 Villeurbanne,
France.
[Collier, Nick] Natl Nucl Lab, Warrington WA3 6AE, Cheshire, England.
[Milestone, Neil] Ind Res Ltd, Lower Hutt 5040, New Zealand.
C3 University of Sheffield; Universidad Publica de Navarra; Institut
National des Sciences Appliquees de Lyon - INSA Lyon; Callaghan
Innovation
RP Kinoshita, H (corresponding author), Univ Sheffield, Dept Mat Sci & Engn, Mappin
St, Sheffield S1 3JD, S Yorkshire, England.
EM h.kinoshita@sheffield.ac.uk
OI Collier, Nicholas/0000-0003-2491-829X; Kinoshita,
Hajime/0000-0001-8805-1774
FU CASE award from the National Nuclear Laboratory (NNL); EPSRC
FX Part of this work was supported by CASE award from the National Nuclear
Laboratory (NNL) and EPSRC. The authors wish to thank Hanson Heidelberg
cements for supplying BE and OPC materials.
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NR 25
TC 27
Z9 27
U1 2
U2 47
PI OXFORD
SN 0008-8846
JI Cem. Concr. Res.
PD AUG
PY 2013
VL 50
BP 11
EP 18
DI 10.1016/j.cemconres.2013.03.016
PG 8
GA 163QP
UT WOS:000320352300002
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Frías, M
Rodríguez Largo, O
García Jiménez, R
Vegas, I
AF Frias, Moises
Rodriguez Largo, Olga
Garcia Jimenez, Rosario
Vegas, Inigo
TI Influence of Activation Temperature on Reaction Kinetics in Recycled
Clay Waste-Calcium Hydroxide Systems
LA English
DT Article
ID PAPER SLUDGE; PORTLAND CEMENTS; METAKAOLIN; HYDRATION; MANUFACTURE;
PERFORMANCE; KAOLINITE; CONCRETE; SLAG
AB Obtaining pozzolanic materials from recycling of industrial waste and byproducts
is a priority action of environmental policy all over the world. This paper
describes the effect of activation conditions on the reaction kinetics in calcined
clay waste (CCW)/calcium hydroxide systems. The CCW used in this work shows
excellent qualities for use as supplementary cementing material in the manufacture
of commercial blended cements. This research work presents an exhaustive study
about the kinetics of a pozzolanic reaction in this cementing system. The results
obtained by different techniques (DTA/TG, X-ray diffraction, and SEM/EDAX) confirm
that the activation conditions (in the range 700 degrees-800 degrees C and 2-5 h of
retention) have a direct effect on the formation and evolution of hydrated phases.
Low activation temperatures favor the CSH gels' formation, while at higher
temperatures aluminates (C(4)AH(13)) and aluminum silicate hydrates (C(4)ASH(8),
hydrotalcites) are predominant.
C1 [Frias, Moises; Rodriguez Largo, Olga] CSIC, Eduardo Torroja Inst, Madrid 28033,
Spain.
[Garcia Jimenez, Rosario] Univ Autonoma Madrid, Madrid 28049, Spain.
[Vegas, Inigo] LABEIN Tecnalia, Derio Biscay 48160, Spain.
de Ciencias de la Construccion Eduardo Torroja (IETCC); Autonomous
University of Madrid
RP Frías, M (corresponding author), CSIC, Eduardo Torroja Inst, Madrid 28033,
Spain.
EM mfrias@ietcc.csic.es
RI Largo, Olga Rodriguez/F-4005-2014; Rodriguez, Olga/N-2514-2019;
Rodriguez, Olga/C-8736-2012; Frias, Moises/H-3331-2015
OI Rodriguez, Olga/0000-0003-0511-5176; Rodriguez,
Olga/0000-0003-0511-5176; Frias, Moises/0000-0001-6621-7227; Vegas, PhD
Inigo J./0000-0003-3422-6270
FU Spanish Ministry of Education and Science [MAT2003-06479-CO3,
CTM2006-12551-CO3]
FX This work was financially supported by the Spanish Ministry of Education
and Science (Project ref: MAT2003-06479-CO3, CTM2006-12551-CO3).
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NR 31
TC 27
Z9 27
U1 0
U2 11
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD DEC
PY 2008
VL 91
IS 12
BP 4044
EP 4051
DI 10.1111/j.1551-2916.2008.02807.x
PG 8
GA 384AC
UT WOS:000261714700034
DA 2023-12-05
ER
PT J
AU Molian, R
Neumann, C
Shrotriya, P
Molian, P
AF Molian, Raathai
Neumann, Clayton
Shrotriya, Pranav
Molian, Pal
TI Novel laser/water-jet hybrid manufacturing process for cutting ceramics
SO JOURNAL OF MANUFACTURING SCIENCE AND ENGINEERING-TRANSACTIONS OF THE
ASME
LA English
DT Article
DE laser cutting; water-jet; ceramics; thermal stresses; precision
machining
ID OXIDATION BEHAVIOR; ALUMINUM NITRIDE; KINETICS
AB Laser and water-jet manufacturing processes are independently used to cut
monolithic and composite ceramics. While these processes offer many advantages over
diamond sawing and other abrasive processes, the energy efficiency, precision,
cutting speed, and environmental threats remain as barriers to their continued
success. This is partly attributed to the material removal mechanisms, which are
melting, and subsequent evaporation (laser) and energy-intensive erosive wear
(water jet). In this paper, we describe a novel laser and water-jet (LWJ) hybrid
manufacturing process that enables the synergistic effects of CO2 laser and
pressurized pure water jet, facilitating precise material removal by thermal shock-
induced fracture and overcoming the deficiencies listed above. Experiments of the
LWJ effects on the cutting of aluminum nitride, an electronic ceramic substrate,
are presented. The most exciting results are very narrow kerf dictated by the crack
width; the absence of thermally affected zone, slag formation, chemical
decomposition; and controlled thermal cracking, implying that the LWJ process is
far superior to conventional laser cutting of ceramics. The LWJ process also
improved the surface finish while reducing energy losses in the process. The
practical realization of the LWJ manufacturing process could be a potential
alternative to diamond saw, high-power laser, and high-pressure abrasive water-jet
methods for machining hard and brittle ceramics.
C1 [Molian, Raathai; Neumann, Clayton; Shrotriya, Pranav; Molian, Pal] Iowa State
Univ, Lab Lasers MEMS & Nanotechnol, Dept Mech Engn, Ames, IA 50011 USA.
C3 Iowa State University
RP Molian, P (corresponding author), Iowa State Univ, Lab Lasers MEMS &
Nanotechnol, Dept Mech Engn, Ames, IA 50011 USA.
EM molian@iastate.edu
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NR 19
TC 27
Z9 27
U1 2
U2 30
PU ASME
PI NEW YORK
PA TWO PARK AVE, NEW YORK, NY 10016-5990 USA
SN 1087-1357
EI 1528-8935
J9 J MANUF SCI E-T ASME
JI J. Manuf. Sci. Eng.-Trans. ASME
PD JUN
PY 2008
VL 130
IS 3
AR 031008
DI 10.1115/1.2844592
PG 10
WC Engineering, Manufacturing; Engineering, Mechanical
SC Engineering
GA 324RK
UT WOS:000257535500008
DA 2023-12-05
ER
PT J
AU O'Connor, GA
Brinton, S
Silveira, ML
AF O'Connor, GA
Brinton, S
Silveira, ML
TI Evaluation and selection of soil amendments for field testing to reduce
P losses
SO SOIL AND CROP SCIENCE SOCIETY OF FLORIDA PROCEEDINGS
LA English
CT 64th Annual Meeting of the Soil-and-Crop-Science-Society-of-Florida
CY MAY 19-21, 2004
CL Tallahassee, FL
ID WATER-TREATMENT RESIDUALS; COMBUSTION BY-PRODUCTS; PHOSPHORUS
SOLUBILITY; BIOAVAILABLE PHOSPHORUS; CHEMICAL AMENDMENTS; POULTRY
LITTER; ALUMINUM; RUNOFF; RETENTION; BIOSOLIDS
AB The effectiveness of chemical amendments in reducing P losses from manure
impacted Florida soil was evaluated using a variety of protocols, including total
elemental analysis, short-term laboratory equilibrations, column leaching
experiments, and simulated rainfall studies. Amendments used included: two Fe-
humates [a Fe-water treatment residual (WTR) and a titanium-mine waste], two Al-
WTRs, one Ca-WTR, a coal combustion slag, a Si-rich material (Pro-Sil), a
Leonardite material (dinoSoil), and two agricultural materials (lime and gypsum).
In equilibration studies, Al-WTRs were the most effective at sorbing P, while Fe-
humate sorbed the least P of all treatments. Other amendments effectively reduced
soluble P, but increased suspension pH and electrical conductivity (EC) to an
extent expected to adversely affect plant growth. Gypsum was the most effective
amendment in reducing P leaching in small column studies. DinoSoil treatment
significantly altered the soil hydraulic properties, yielding the greatest runoff
volumes in a simulated rainfall study. Total P loss (runoff + leachate) was largely
determined by the leaching component, and was essentially all soluble reactive
phosphorus (SRP) for both bare and grassed soil surfaces. AD treatments reduced
runoff SRP compared to the control. Amendment effects in the grassed rainfall study
(dominated by leaching) were inconsistent with results from the small column
leaching study, possibly due to the different hydraulic conditions and kinetic
factors involved in the two studies. The Al-WTRs amendments were recommended for
field evaluation.
C1 Univ Florida, Dept Soil & Water Sci, Gainesville, FL 32611 USA.
C3 State University System of Florida; University of Florida
RP O'Connor, GA (corresponding author), Univ Florida, Dept Soil & Water Sci,
Gainesville, FL 32611 USA.
EM gao@ufl.edu
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NR 42
TC 27
Z9 27
U1 0
U2 17
PU SOIL CROP SCIENCE SOC FLORIDA
PI GAINESVILLE
PA C/O UNIV FLORIDA, PO BOX 110290, GAINESVILLE, FL 32611-0290 USA
SN 0096-4522
J9 SOIL CROP SCI SOC FL
JI Soil Crop Sci. Soc. Fla. Proc.
PY 2005
VL 64
BP 22
EP 34
PG 13
WC Agronomy; Soil Science
SC Agriculture
GA 984VS
UT WOS:000233334100004
DA 2023-12-05
ER
PT J
AU Chung, YS
Cramb, AW
AF Chung, YS
Cramb, AW
TI Direct observation of spontaneous emulsification and associated
interfacial phenomena at the slag-steel interface
SO PHILOSOPHICAL TRANSACTIONS OF THE ROYAL SOCIETY A-MATHEMATICAL PHYSICAL
AND ENGINEERING SCIENCES
LA English
CT Meeting on Marangoni and Interfacial Phenomena in Materials Processing
CY JUN 04-05, 1997
CL LONDON, ENGLAND
DE X-ray photography; spontaneous emulsification; interfacial tension;
steel-slag interface; casting
ID IRON
AB Interfacial tension decreases drastically when an intense chemical reaction
occurs at a steel-slag interface. This phenomenon results in spontaneous droplet
spreading during the initial period of reaction and droplet recovery as the rate of
reaction decreases. In the present work, spreading tendency was found to be
associated with spontaneous emulsification of both steel in slag and slag in steel.
Spontaneous emulsification was observed at 1550 degrees C when a liquid Fe3.28%Al
alloy droplet was placed in contact with liquid CaO-SiO2-Al2O3 (40:40:20 by weight)
slag.
Surface turbulence induced metal emulsification and droplet spreading was
observed by X-ray photography. Spontaneous droplet spreading was noted at alloy
aluminium contents as low as 0.25%. Spontaneous emulsification was steel into slag
was documented at aluminium contents greater than 3%. From the observation of
quenched Fe-3.28%Al alloy droplets by optical and scanning electron microscopy,
slag entrapment and metal emulsification were documented and the metal-slag
interface was shown to be extremely perturbed during the reaction of aluminium with
silica.
RP Chung, YS (corresponding author), Carnegie Mellon Univ, Dept Mat Sci & Engn,
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TC 27
Z9 29
U1 1
U2 13
PU ROYAL SOC
PI LONDON
PA 6-9 CARLTON HOUSE TERRACE, LONDON SW1Y 5AG, ENGLAND
SN 1364-503X
J9 PHILOS T R SOC A
JI Philos. Trans. R. Soc. A-Math. Phys. Eng. Sci.
PD APR 15
PY 1998
VL 356
IS 1739
BP 981
EP 993
DI 10.1098/rsta.1998.0202
PG 13
WC Multidisciplinary Sciences
SC Science & Technology - Other Topics
GA ZM298
UT WOS:000073524500023
DA 2023-12-05
ER
PT J
AU Li, SW
Pan, J
Zhu, DQ
Guo, ZQ
Shi, Y
Dong, T
Lu, SH
Tian, HY
AF Li, Siwei
Pan, Jian
Zhu, Deqing
Guo, Zhengqi
Shi, Yue
Dong, Tao
Lu, Shenghu
Tian, Hongyu
TI A new route for separation and recovery of Fe, Al and Ti from red mud
LA English
DT Article
DE Red mud; Pre-reducing-smelting; Alkaline leaching; Acid leaching;
Stepwise extraction
ID REDUCTION-MAGNETIC SEPARATION; BAUXITE RESIDUE; COPPER SLAG; IRON;
WASTE; NEUTRALIZATION; ALUMINUM; ELEMENTS; WATER
AB Red mud is one kind of by-products rejected from industrial production of
alumina plant and characterized by high content of alkaline and containing many
valuable metals such as iron, aluminum, titanium, etc. It is urgent to effectively
utilize red mud for the sustainable development of aluminum metallurgy industry. In
this paper, a new route was proposed to fully recover Fe, Al2O3 and TiO2 from the
red mud, which includes three procedures, i.e. pre-reducing-smelting, alkaline
leaching and acid leaching. The pre-reducing-smelting step was employed to recover
iron from the mud, producing pig iron at an iron recovery of some 98.15% and slag
containing 43.17% Al2O3 and 15.71%TiO2, respectively. Then, based on the thermal
dynamic calculations, a modification of the slag-alkaline leaching and hydrochloric
acid leaching process were conducted to obtain the stepwise recovery of Al2O3 and
TiO2, respectively, from the smelting slag. Aluminum and titanium were recovered in
the form of sodium aluminum solution and perovskite at a recovery of 85.85% and
95.53%, respectively. The innovative route is probably a potential way to achieve
comprehensive and clean utilization of red mud.
C1 [Li, Siwei; Pan, Jian; Zhu, Deqing; Guo, Zhengqi; Shi, Yue; Dong, Tao; Lu,
Shenghu; Tian, Hongyu] Cent South Univ, Sch Minerals Proc & Bioengn, Room 322 Biol
Bldg, Changsha 410083, Hunan, Peoples R China.
RP Pan, J; Zhu, DQ (corresponding author), Cent South Univ, Sch Minerals Proc &
Bioengn, Room 322 Biol Bldg, Changsha 410083, Hunan, Peoples R China.
EM swli@csu.edu.cn; pjcsu@csu.edu.cn; dqzhu@csu.edu.cn
FU Co-Innovation Center for Clean and Efficient Utilization of Strategic
Metal Mineral Resources of Hunan Province; National Natural Science
Foundation of China [51474161]; Innovation-driven Project of Guangxi
Zhuang Autonomous Region [AA18242003, AA148242003]
FX The authors wish to express thanks to Co-Innovation Center for Clean and
Efficient Utilization of Strategic Metal Mineral Resources of Hunan
Province and National Natural Science Foundation of China (No. 51474161)
and Innovation-driven Project of Guangxi Zhuang Autonomous Region (Nos.
AA18242003, AA148242003). Which supplied us the facilities and funds to
fulfill the experiments.
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NR 35
TC 26
Z9 28
U1 15
U2 94
PU ELSEVIER
PI AMSTERDAM
SN 0921-3449
EI 1879-0658
PD MAY
PY 2021
VL 168
AR 105314
DI 10.1016/j.resconrec.2020.105314
EA MAR 2021
PG 10
GA SM0FP
UT WOS:000657289000051
DA 2023-12-05
ER
PT J
AU Santamaría, L
Devred, F
Gaigneaux, EM
Vicente, MA
Korili, SA
Gil, A
AF Santamaria, L.
Devred, F.
Gaigneaux, E. M.
Vicente, M. A.
Korili, S. A.
Gil, A.
TI Effect of the surface properties of Me2+/Al layered double
hydroxides synthesized from aluminum saline slag wastes on the
adsorption removal of drugs
SO MICROPOROUS AND MESOPOROUS MATERIALS
LA English
DT Article
DE Aluminum Industrial wastes; Adsorption removal of diclofenac;
Hydrotalcite from saline slags; Layered double hydroxides; Adsorption
removal of salicylic acid; Butanol conversion; Acidity and basicity
characterization
ID MG-AL HYDROTALCITES; EMERGING CONTAMINANTS; AQUEOUS-SOLUTION; DICLOFENAC
SODIUM; TRANSITION-METAL; BASIC PROPERTIES; CATALYSTS; ACID;
PHARMACEUTICALS; WASTEWATERS
AB This work presents the synthesis of Me2+ (Co, Mg, Ni and Zn)/Al layered double
hydroxides (LDH) with a 3:1 M ratio by the co-precipitation method. Structural
characterization and comparison of the series has been achieved using powder X-ray
diffraction (PXRD), scanning electron microscopy (SEM), nitrogen physisorption at
77 K, thermogravimetry measurements (TGA), temperature-programmed reduction (TPR),
X-ray photoelectron spectroscopy (XPS), ammonia temperature-programmed desorption
(NH3-TPD) and point of zero charge (pHpzc). Batch experiments were performed to
analyze the adsorption capacity of the different LDH on diclofenac and salicylic
acid, as example of emergent pollutants. The pH, mass of adsorbent, contact time
and concentration of pollutant were the parameters used to compare the adsorption
performance of the synthesized materials. Samples showed different behavior and the
equilibrium was reached at different times, Mg6Al2 and Zn6Al2 showed lower
equilibrium times but had higher adsorption capacity. Various adsorption and
isotherm equation models were employed to study both the kinetic and equilibrium
results and, in general, the removal of diclofenac was greater than that of
salicylic acid. 1-Butanol conversion was also used as a means of acidity and
basicity characterization and the results were compared with the adsorption
performance of the samples in order to explain the results found. A relationship
between the amount of pollutants adsorbed and the butenes formed in the
dehydrogenation reaction of 1-butanol was found.
C1 [Santamaria, L.; Korili, S. A.; Gil, A.] Univ Publ Navarra, Dept Ciencias,
INAMAT 2, Edificio Acebos,Campus Arrosadia, E-31006 Pamplona, Spain.
[Devred, F.; Gaigneaux, E. M.] UCLouvain, Inst Condensed Matter & Nanosci IMCN,
Pl Louis Pasteur 1,Box L4-01-09, B-1348 Louvain La Neuve, Belgium.
[Vicente, M. A.] Univ Salamanca, Fac Ciencias Quim, Dept Quim Inorgan, GIR
QUESCAT, Plaza Merced S-N, E-37008 Salamanca, Spain.
C3 Universidad Publica de Navarra; Universite Catholique Louvain;
University of Salamanca
RP Gil, A (corresponding author), Univ Publ Navarra, Dept Ciencias, INAMAT 2,
Edificio Acebos,Campus Arrosadia, E-31006 Pamplona, Spain.
RI Santamaría, Leticia/K-2587-2018; Santamaría, Leticia/ABD-2455-2020;
Leticia/0000-0003-1248-341X; Gil, Antonio/0000-0001-9323-5981; Vicente,
Miguel Angel/0000-0002-6714-0249
Government of Navarra [PI017-PI039]; Universidad Publica de Navarra;
Santander Bank
through projects PI017-PI039 CORRAL. LS thanks Universidad Publica de
Navarra for a pre-doctoral grant. AG also thanks Santander Bank for
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NR 58
TC 26
Z9 26
U1 0
U2 64
PU ELSEVIER
PI AMSTERDAM
SN 1387-1811
EI 1873-3093
J9 MICROPOR MESOPOR MAT
JI Microporous Mesoporous Mat.
PD DEC 15
PY 2020
VL 309
AR 110560
DI 10.1016/j.micromeso.2020.110560
PG 13
WC Chemistry, Applied; Chemistry, Physical; Nanoscience & Nanotechnology;
Materials Science, Multidisciplinary
GA NZ7WM
UT WOS:000577314100006
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Yliniemi, J
Walkley, B
Provis, JL
Kinnunen, P
Illikainen, M
AF Yliniemi, J.
Walkley, B.
Provis, J. L.
Kinnunen, P.
Illikainen, M.
TI Nanostructural evolution of alkali-activated mineral wools
LA English
DT Article
DE Alkali-activated material; Mineral wool; Waste valorisation; X-ray
diffraction; Electron microscopy; Nuclear magnetic resonance
ID BLAST-FURNACE SLAG; PHASE EVOLUTION; WASTE GLASS; ROCK WOOL; S-H;
MICROSTRUCTURE; CEMENTS; MICROANALYSIS; MICROSCOPY; STRENGTH
AB Mineral wools are the most widely used building insulation material worldwide.
Annually, 2.5 million tonnes of mineral wool waste are generated in the EU alone,
and this is a largely unutilised material that is landfilled or incinerated.
However, mineral wool wastes are promising precursors for production of alkali-
activated cementitious binders due to their favourable chemical and mineralogical
composition and high surface area. Alkali-activation is therefore a valuable route
for valorisation of large quantities of mineral wool waste. This study resolves the
phase assemblage and nanostructure of reaction products formed upon alkali
activation of stone wool and glass wool by sodium hydroxide and sodium silicate
solutions with X-ray diffraction, electron microscopy and solid state nuclear
magnetic resonance spectroscopy experiments probing Al-27 and Si-29. The stone
wool-based alkali-activated binder comprises an amorphous sodium- and aluminium-
substituted calcium silicate hydrate (C-(N-)A-S-H) gel, an amorphous sodium
aluminosilicate hydrate (N-A-S-H) gel and small amounts of the layered double
hydroxide phase quintinite and zeolite F. The glass wool-based alkali-activated
binder comprises an amorphous Ca- and Al-substituted sodium silicate (N-(C-)(A-)S-
H) gel. Gel chemical composition and reaction kinetics of alkali-activated mineral
wools are shown to be dependent on the activating solution chemistry, with reaction
rate and extent promoted by inclusion of a source of soluble Si in the reaction
mixture. This work provides the most advanced description of the chemistry and
structure of alkali-activated mineral wools to date, yielding new insight that is
essential in developing valorisation pathways for mineral wools by alkali
activation and providing significant impetus for development of sustainable
construction materials.
C1 [Yliniemi, J.; Kinnunen, P.; Illikainen, M.] Univ Oulu, Fibre & Particle Engn
Res Unit, POB 4300, Oulu 90014, Finland.
[Walkley, B.; Provis, J. L.] Univ Sheffield, Dept Mat Sci & Engn, Sir Robert
Hadfield Bldg,Mappin St, Sheffield S1 3JD, S Yorkshire, England.
[Walkley, B.] Univ Sheffield, Dept Chem & Biol Engn, Sir Robert Hadfield
Bldg,Mappin St, Sheffield S1 3JD, S Yorkshire, England.
C3 University of Oulu; University of Sheffield; University of Sheffield
RP Yliniemi, J (corresponding author), Univ Oulu, Fibre & Particle Engn Res Unit,
POB 4300, Oulu 90014, Finland.
EM juho.yliniemi@oulu.fi
RI Kinnunen, Paivo/I-3430-2012; Provis, John/AAR-3260-2020; Provis, John
L/A-7631-2008
OI Kinnunen, Paivo/0000-0001-8490-1890; Provis, John/0000-0003-3372-8922;
Provis, John L/0000-0003-3372-8922; Yliniemi, Juho/0000-0003-0013-8598;
Walkley, Brant/0000-0003-1069-1362; Illikainen,
Mirja/0000-0001-7545-4574
FU Geodesign-project - Business Finland [1215/31/2015]; Boliden Harjavalta
Oy; Destamatic Oy; Fortum Power and Heat Oy; Paroc Group Oy;
Saint-Gobain Finland Oy; Suomen Erityisjate Oy
FX The research was performed under the auspices of Geodesign-project
funded by the Business Finland (grant ID 1215/31/2015) and various
companies (Boliden Harjavalta Oy, Destamatic Oy, Fortum Power and Heat
Oy, Paroc Group Oy, Saint-Gobain Finland Oy, and Suomen Erityisjate Oy).
The experimental work was performed at the University of Sheffield, UK
and at the University of Oulu, Finland. Dan Geddes, Dr Oday Hussein,
Jarno Karvonen and Elisa Wirkkala are acknowledged for their assistance
with some of the laboratory work. Dr Dale Prentice is acknowledged for
assistance with SEM-EDX data processing and Dr Sandra van Meurs is
acknowledged for her assistance acquiring NMR data. The authors thank
the PQ Corporation for generously supplying the sodium silicate solution
used in this investigation.
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TC 26
Z9 26
U1 4
U2 35
PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
PD FEB
PY 2020
VL 106
AR 103472
DI 10.1016/j.cemconcomp.2019.103472
PG 12
GA KJ7DY
UT WOS:000512219700019
DA 2023-12-05
ER
PT J
AU Rashad, AM
AF Rashad, Alaa M.
TI Effect of nanoparticles on the properties of geopolymer materials
LA English
DT Article
DE compressive strength; durability-related properties; workability
ID ALKALI-ACTIVATED SLAG; NANO-SILICA; CEMENTITIOUS MATERIALS; SHORT GUIDE;
COMPRESSIVE STRENGTH; METAKAOLIN; NANO-SIO2; MICROSTRUCTURE; DURABILITY;
RESISTANCE
AB Geopolymer is an innovative material and a real alternative to traditional
Portland cement for use in the construction industry. Incorporation of the use of
geopolymers in civil engineering is one of the most-promising options for reducing
environmental impact and the huge energy consumption of Portland cement
manufacture. Since geopolymers were discovered, further development has produced
more modified, strong, durable and sustainable binders. One option to develop and
modify some properties of this system is to add other prospective materials such as
nanoparticles. In general, the applications and advances of nanotechnology in
geopolymer materials remain limited in comparison with those of traditional
cementitious materials. However, in the last few years, the effect of nanoparticles
on the properties of geopolymers has been given increased attention. This article
presents an overview of earlier studies focused on adding different types of
nanoparticles, such as nano-silicone dioxide (SiO2), nano-titanium dioxide (TiO2),
nano-aluminium oxide (Al2O3), nano-clay and geothermal nanosilica waste, into
different geopolymer matrices. Fresh and hardened properties have been reviewed and
briefed. The current review can be used as a guide to know what has already been
covered in the research and what should be covered in future studies.
C1 [Rashad, Alaa M.] Housing & Bldg Natl Res Ctr HBRC, Bldg Mat Res & Qual Control
Inst, Cairo, Egypt.
[Rashad, Alaa M.] Shaqra Univ, Coll Engn, Dept Civil Engn, Shaqraa, Saudi
Arabia.
C3 Egyptian Knowledge Bank (EKB); Housing & Building National Research
Center (HBRC); Shaqra University
RP Rashad, AM (corresponding author), Housing & Bldg Natl Res Ctr HBRC, Bldg Mat
Res & Qual Control Inst, Cairo, Egypt.; Rashad, AM (corresponding author), Shaqra
Univ, Coll Engn, Dept Civil Engn, Shaqraa, Saudi Arabia.
EM alaarashad@yahoo.com
RI Rashad, Alaa M./AAG-2286-2019
OI Rashad, Alaa M./0000-0002-5138-5452
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NR 56
TC 26
Z9 26
U1 1
U2 43
PU ICE PUBLISHING
PI WESTMINISTER
SN 0024-9831
EI 1751-763X
J9 MAG CONCRETE RES
JI Mag. Concr. Res.
PD DEC
PY 2019
VL 71
IS 24
BP 1283
EP 1301
DI 10.1680/jmacr.18.00289
PG 19
GA JN3FS
UT WOS:000496785200002
DA 2023-12-05
ER
PT J
AU Li, FH
Li, Y
Fan, HL
Wang, T
Guo, MX
Fang, YT
AF Li, Fenghai
Li, Yang
Fan, Hongli
Wang, Tao
Guo, Mingxi
Fang, Yitian
TI Investigation on fusion characteristics of deposition from biomass
vibrating grate furnace combustion and its modification
SO ENERGY
LA English
DT Article
DE Biomass combustion; Deposition; Fusion characteristics; Additives;
Variation mechanism
ID FLUIDIZED-BED GASIFICATION; ASH-FUSION; SINTERING CHARACTERISTICS;
TEMPERATURE COAL; ALUMINUM COAL; SEWAGE-SLUDGE; BEHAVIORS; SLAG; STRAW;
AGGLOMERATION
AB To mitigate increasing environmental pressures, biomass is becoming a crucial
alternative energy source worldwide. Ash fusion characteristics of biomass has
closely related to ash-related problems during its conversion. The fusion
characteristics of cotton stalk (CS), the deposition from CS vibrating grate
furnace combustion (D-CS), and their modification mechanisms were investigated. The
results indicate the sintering temperature (T-s) and ash fusion temperature (AFT)
of D-CS are lower than that of CS. Kaolinite causes obvious increases in the T-s
and flow temperature, while the additions of calcite and Ca-sludge waste (Ca-W)
make Dcs deformation temperature increase more obviously than that of flow
temperature. That an increase in kalsilite content and leucite formation make the
mixture T-s and AFT increase with increasing kaolinite proportion; the replacement
of K+ in the silicates by Ca2+ causes the formations of high melting point Ca2+
silicates (e.g., rankinite and wollastonite) with increasing calcite or Ca-W, which
makes their T-s and AFT increase. It is found that the deformation temperature
corresponds to the temperature at which its liquid phase content at 15% or so based
on FactSage calculation. (C) 2019 Elsevier Ltd. All rights reserved.
C1 [Li, Fenghai; Fan, Hongli; Wang, Tao; Guo, Mingxi] Heze Univ, Sch Chem & Chem
Engn, Heze 274015, Shandong, Peoples R China.
[Li, Fenghai; Li, Yang] Henan Polytech Univ, Sch Chem & Chem Engn, Jiaozuo
454003, Henan, Peoples R China.
RP Li, FH (corresponding author), Heze Univ, Sch Chem & Chem Engn, Heze 274015,
Shandong, Peoples R China.
EM hzlfh@163.com
RI guo, mingxi/ABB-3916-2020; LI, feng/HIR-1703-2022
FU Natural Science Foundation of China [21875059]; Strategic Priority
Research Program of the Chinese Academy of Sciences [XDA07050103];
Natural Science Foundations of Shandong Province, China [ZR2018MB037,
ZR2017BB063, ZR2014BM014]
China (21875059), Strategic Priority Research Program of the Chinese
Academy of Sciences (XDA07050103), and the Natural Science Foundations
of Shandong Province, China (ZR2018MB037, ZR2017BB063, ZR2014BM014).
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U2 37
PI OXFORD
SN 0360-5442
EI 1873-6785
J9 ENERGY
JI Energy
PD MAY 1
PY 2019
VL 174
BP 724
EP 734
DI 10.1016/j.energy.2019.02.154
PG 11
GA IA1HF
UT WOS:000469309200063
DA 2023-12-05
ER
PT J
AU Cristelo, N
Castro, F
Fernandes, L
Tavares, P
AF Cristelo, Nuno
Fernandez-Jimenez, Ana
Castro, Fernando
Fernandes, Lisete
Tavares, Pedro
TI Sustainable alkaline activation of fly ash, aluminium anodising sludge
and glass powder blends with a recycled alkaline cleaning solution
LA English
DT Article
DE Alkaline activation; Glass powder; Aluminium anodizing sludge; Fly ash;
Mechanical behaviour
ID WASTE-GLASS; GEOPOLYMERISATION; PRODUCTS; STRENGTH; INDUSTRY; CEMENT;
BELITE
AB Introduction of new residues and wastes in the development of alkaline activated
materials is a major concern regarding the spreading and dissemination of this
technique. Such increase in the spectrum of available raw materials will decrease
the need for long-distance transportation of the more traditional precursors that
have been tirelessly used in the past two decades (e.g. fly ash, blast furnace
slag). Additionally, the use of commercial activators severely hinders its
environmental and financial performance, promoting the need to develop waste-based
activators. In this paper, wastes from the aluminium anodising and extrusion
processes and from the production of optical lenses were combined with low-calcium
fly ash, to produce binders exclusively made from wastes and residues. The
performance was assessed through uniaxial compression strength tests, which were
accompanied by the monitorisation of several physical properties, including
temperature, pH and weight; and by a thorough microscopic analysis, including
scanning electron microscopy, coupled with energy dispersive spectroscopy, and x-
ray diffraction, for mineralogy characterisation. Results show that the addition of
glass powder and aluminium anodising sludge to class-F fly ash optimised the final
precursor, which was then successfully activated with a disposed solution,
originally used to clean the aluminium extrusion steel dies. The inclusion of
soluble silicon and aluminium in the precursor raised the compression strength
after short-term curing, compared with pastes prepared only with fly ash. (C) 2019
C1 [Cristelo, Nuno] Univ Tras Os Montes & Alto Douro, CQVR, Dept Engn, P-5000801
[Fernandez-Jimenez, Ana] CSIC, Eduardo Torroja Inst Construct Sci IETcc, E-28033
Madrid, Spain.
[Castro, Fernando] Univ Minho, W2V, Dept Mech Engn, Campus Azurem, P-4800058
Guimaraes, Portugal.
[Fernandes, Lisete] Univ Tras Os Montes & Alto Douro, CQVR, Elect Microscopy
Unit, P-5000801 Vila Real, Portugal.
[Tavares, Pedro] Univ Tras Os Montes & Alto Douro, CQVR, Dept Chem, P-5000801
C3 University of Tras-os-Montes & Alto Douro; Consejo Superior de
Investigaciones Cientificas (CSIC); CSIC - Instituto de Ciencias de la
Construccion Eduardo Torroja (IETCC); Universidade do Minho; University
of Tras-os-Montes & Alto Douro; University of Tras-os-Montes & Alto
Douro
RP Cristelo, N (corresponding author), Univ Tras Os Montes & Alto Douro, CQVR, Dept
Engn, P-5000801 Vila Real, Portugal.
EM ncristel@utad.pt; anafj@ietcc.csic.es; fcastro@dem.uminho.pt;
ume@utad.pt; ptavares@utad.pt
RI Fernández, ANA Maria/G-2597-2016; Fernandes, Lisete Sofia
Gomes/GZK-4443-2022; Tavares, Pedro B/B-8253-2013; Cristelo, Nuno
Miguel/B-3636-2010; Castro, Fernando A.P./H-6642-2015
OI Fernández, ANA Maria/0000-0002-5721-2923; Fernandes, Lisete Sofia
Gomes/0000-0002-2986-7818; Tavares, Pedro B/0000-0001-7589-1299;
Cristelo, Nuno Miguel/0000-0002-3600-1094; Castro, Fernando
A.P./0000-0002-6674-3988
FU R&D Project JUSTREST-Development of Alkali Binders for Geotechnical
Applications Made Exclusively from Industrial Waste - Foundation for
Science and Technology - FCT/MCTES (PIDDAC) [PTDC/ECM-GEO/0637/2014];
GEO-DESIGN project [17501]; European Regional Development Fund (ERDF)
through NORTE 2020 (North Regional Operational Program 2014/2020);
Fundação para a Ciência e a Tecnologia [PTDC/ECM-GEO/0637/2014] Funding
Source: FCT
FX This work was funded by the R&D Project JUSTREST-Development of Alkali
Binders for Geotechnical Applications Made Exclusively from Industrial
Waste, with reference PTDC/ECM-GEO/0637/2014, financed by the Foundation
for Science and Technology - FCT/MCTES (PIDDAC).; The research was
supported by the GEO-DESIGN project, no 17501, co-financed by the
European Regional Development Fund (ERDF) through NORTE 2020 (North
Regional Operational Program 2014/2020).
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10.1016/j.conbuildmat.2013.05.047
10.1016/j.jclepro.2014.11.074
10.1016/j.bsecv.2015.03.004
10.1016/j.conbuildmat.2018.10.203
10.1016/j.cemconres.2004.10.042
NR 41
TC 26
Z9 28
U1 2
U2 20
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD APR 20
PY 2019
VL 204
BP 609
EP 620
DI 10.1016/j.conbuildmat.2019.01.226
PG 12
GA HS8AO
UT WOS:000464090600056
OA hybrid, Green Submitted
DA 2023-12-05
ER
PT J
AU El-Didamony, H
Amer, AA
Mohammed, MS
Abd El-Hakim, M
AF El-Didamony, Hamdy
Amer, Ahmed A.
Mohammed, Mona S.
Abd El-Hakim, Mahmmoud
TI Fabrication and properties of autoclaved aerated concrete containing
agriculture and industrial solid wastes
LA English
DT Article
DE Autoclaved aerated concrete; GBFS; Meta-kaolin; RHA; Silica-fume;
Mechanical properties
ID FLY-ASH; SLAG; REPLACEMENT; HYDRATION; TAILINGS
AB Autoclaved aerated concrete (AAC) has been used as a lightweight, porous and
thermally insulating material. AAC is mainly fabricated by autoclaving composite
containing sand, cement, lime, calcium sulfate, and a small amount of aluminum
powder content (foaming agent). In the present work the possibility of recycling
different industrial and agriculture wastes in AAC-production was studied. The
impact of granulated blast furnace slag (GBFS) and meta-kaolin (MK) as cement
replacement on the performance of AAC was individually evaluated. In contrast,
active silica sources such as silica fume (SF) and rice husk ash (RHA) were used as
partial replacement of sand for inactive silica. The physical and mechanical
properties were evaluated by measuring bulk density and compressive strength. The
hydration products were identified by mean of XRD and DSC techniques. The results
proved that, the AAC containing GBFS (GS-AAC) showed the higher mechanical
properties compared to that having MK (MK-AAC) at all replacement levels. Samples
incorporated with 2.5 wt% RHA and 7.5 wt% SF exhibited the highest mechanical
properties compared to that containing silica sand.
C1 [El-Didamony, Hamdy; Amer, Ahmed A.; Abd El-Hakim, Mahmmoud] Zagazig Univ, Fac
Sci, Chem Dept, Zagazig, Egypt.
[Mohammed, Mona S.] Natl Res Ctr, Dept Chem Engn & Pilot Plant, Cairo, Egypt.
C3 Egyptian Knowledge Bank (EKB); Zagazig University; Egyptian Knowledge
Bank (EKB); National Research Centre (NRC)
RP Mohammed, MS (corresponding author), Natl Res Ctr, Dept Chem Engn & Pilot Plant,
Cairo, Egypt.
EM monsmohmmed015@gmail.com
RI Amer, Ahmed/AAU-5206-2020
OI Abd El-Hakim, Mahmoud/0000-0003-4092-4462
Baspinar MS, 2014, KSCE J CIV ENG, V18, P47, DOI 10.1007/s12205-014-0392-7
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10.1016/j.conbuildmat.2017.07.116
El-Didamony H, 2015, J THERM ANAL CALORIM, V122, P81, DOI 10.1007/s10973-015-
4691-0
El-Didamony H, 2014, ADV CEM RES, V26, P248, DOI 10.1680/adcr.13.00049
Ferretti D, 2015, CONSTR BUILD MATER, V98, P353, DOI
10.1016/j.conbuildmat.2015.08.121
Hafez AI., 2017, ARPN J ENG APPL SCI, V12, P2854
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5
10.1016/j.conbuildmat.2011.08.034
10.1016/j.cemconcomp.2009.10.002
10.1016/j.cemconcomp.2014.07.021
10.1016/j.jmatprotec.2008.02.044
Mohammed M. S., 2008, THESIS
Mohammed MA, 2000, THESIS
Mohammed MS, 2014, POLYM COMPOSITE, V35, P174, DOI 10.1002/pc.22647
10.1016/j.cemconres.2004.10.011
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Walczak P, 2015, PROCEDIA ENGINEER, V122, P302, DOI 10.1016/j.proeng.2015.10.040
10.1016/j.conbuildmat.2012.03.006
NR 23
TC 26
Z9 26
U1 0
U2 33
PI AMSTERDAM
SN 2352-7102
J9 J BUILD ENG
JI J. Build. Eng.
PD MAR
PY 2019
VL 22
BP 528
EP 538
DI 10.1016/j.jobe.2019.01.023
PG 11
GA HK1BO
UT WOS:000457639900046
DA 2023-12-05
ER
PT J
AU Nguyen, THY
Tsuchiya, K
Atarashi, D
AF Thi Hai Yen Nguyen
Tsuchiya, Koichi
Atarashi, Daiki
TI Microstructure and composition of fly ash and ground granulated blast
furnace slag cement pastes in 42-month cured samples
LA English
DT Article
DE C-A-S-H; Outer products; Inner products; Fly ash; Ground granulated
blast furnace slags; Portland cement; SEM-EDS; Si-29 MAS NMR; Al-27 MAS
NMR
ID C-S-H; PORTLAND-CEMENT; CALCIUM; SILICATE; NMR; HYDRATION; ALUMINUM;
TEMPERATURE; AL-27; NANOSTRUCTURE
AB Microstructure and composition of 42-month cured pastes using Portland cement
(OPC), fly-ash cement (FAC), and ground-granulated-blast-furnace-slag cement
(GGBFSC) were investigated. The granular structure of C-A-S-H in outer products of
GGBFSC and FAC pastes was finer than in OPC paste. Fly ash offered higher capacity
in increasing the Si/Ca ratio of C-A-S-H than slag in the pastes. However, their
effects on the chain length were opposite. The incorporation of aluminum into
silicate anions in GGBFSC paste was greater compared to others. AlO45- played an
essential role in bridging the shorter silicate anions together, forming a longer
chain of aluminosilicate anions in the pastes. Mg-Al layered-double hydroxide (LDH)
was abundant in the inner products of slag particles with the interbedding of TAH,
leading to a low ratio of Mg/Al ratio on hydrotalcite-like phase. (C) 2018 Elsevier
C1 [Thi Hai Yen Nguyen; Tsuchiya, Koichi] Natl Inst Mat Sci, Res Ctr Struct Mat, 1-
2-1 Sengen, Tsukuba, Ibaraki 3050047, Japan.
[Atarashi, Daiki] Shimane Univ, Interdisciplinary Grad Sch Sci & Engn, 1060
Nishikawatsu Cho, Matsue, Shimane 6908504, Japan.
C3 National Institute for Materials Science; Shimane University
RP Nguyen, THY (corresponding author), Natl Inst Mat Sci, Res Ctr Struct Mat, 1-2-1
Sengen, Tsukuba, Ibaraki 3050047, Japan.
EM NGUYEN.ThiHaiYen@nims.go.jp
RI Tsuchiya, Koichi/E-7191-2011
OI Tsuchiya, Koichi/0000-0003-0267-2727; NGUYEN, Thi Hai
Yen/0000-0002-6988-4778
FU Council for Science, Technology and Innovation(CSTI), Cross-ministerial
Strategic Innovation Promotion Program (SIP), Infrastructure
maintenance, renovation and management (Funding agency: JST)
FX The authors would like to appreciate Dr. Kenjiro Hashi and Mr. Kenzo
Deguchi for their help on NMR measurement. We gratefully thank Professor
Hiroshi Yokota at Hokkaido University for sending us the paste samples.
This work was supported by Council for Science, Technology and
Innovation(CSTI), Cross-ministerial Strategic Innovation Promotion
Program (SIP), Infrastructure maintenance, renovation and management
(Funding agency: JST).
10.1016/j.cemconres.2003.10.009
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NR 40
TC 26
Z9 28
U1 1
U2 41
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD DEC 10
PY 2018
VL 191
BP 114
EP 124
DI 10.1016/j.conbuildmat.2018.09.206
PG 11
GA HB5MO
UT WOS:000451105100011
OA hybrid
DA 2023-12-05
ER
PT J
AU Duan, SC
Shi, X
Mao, MT
Yang, WS
Han, SW
Guo, HJ
Guo, J
AF Duan, Shengchao
Shi, Xiao
Mao, Mingtao
Yang, Wensheng
Han, Shaowei
Guo, Hanjie
Guo, Jing
TI Investigation of the Oxidation Behaviour of Ti and Al in Inconel 718
Superalloy During Electroslag Remelting
SO SCIENTIFIC REPORTS
LA English
DT Article
ID THERMODYNAMIC PROPERTIES; ALLOYING ELEMENTS; TITANIUM; STEEL; SLAG;
ALUMINUM; SILICON; ESR; DEOXIDATION; INCLUSION
AB In the current study, the thermodynamics of the slag-metal equilibrium reaction
between Inconel 718 Ni-based alloy and CaF2-CaO-Al2O3-MgO-TiO2 electroslag
remelting (ESR)-type slags were systematically investigated in the temperature
range from 1773 to 1973 K (1500 to 1700 degrees C). The equilibrium Al content
increased with increasing temperature, whereas the equilibrium Ti content decreased
with increasing temperature at a fixed slag composition. The important factors for
controlling the oxidation of Al and Ti in the Inconel 718 superalloy were TiO2 >
Al2O3 > CaO > CaF2 > MgO in ESR-type slag and Al > Ti in a consumable electrode.
The conventional method of sampling by means of a quartz tube could result in
contamination of the molten metal and changes in the size of the "special reaction
interface". Therefore, a novel method was used in the present study to investigate
the slag-metal reaction kinetics to accurately obtain the kinetic parameters. The
mass transfer coefficient was determined by coupling with the kinetic model derived
from the assumption that the reaction rate ([Al] + (TiO2) = [Ti] + (Al2O3)) was
controlled by the mass transfer of [Ti], [Al], (TiO2) and (Al2O3) in the boundary
layer, respectively.
C1 [Duan, Shengchao; Shi, Xiao; Mao, Mingtao; Yang, Wensheng; Han, Shaowei; Guo,
Hanjie; Guo, Jing] Univ Sci & Technol Beijing, Sch Met & Ecol Engn, Beijing 100083,
Peoples R China.
[Duan, Shengchao; Shi, Xiao; Yang, Wensheng; Han, Shaowei; Guo, Hanjie; Guo,
Jing] Beijing Key Lab Special Melting & Preparat High E, Beijing 100083, Peoples R
China.
[Mao, Mingtao] CISRI, Res Inst High Temp Mat, Beijing 100081, Peoples R China.
C3 University of Science & Technology Beijing; Central Iron & Steel
Research Institute
RP Guo, HJ (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol Engn,
Beijing 100083, Peoples R China.; Guo, HJ (corresponding author), Beijing Key Lab
Special Melting & Preparat High E, Beijing 100083, Peoples R China.
RI Duan, Sheng-chao/J-3331-2019
OI Duan, Sheng-chao/0000-0001-5007-3601; Guo, Han-jie/0000-0002-6493-8853
FU National Natural Science Foundation of China [U1560203, 51274031]
FX The author (Shengchao Duan) would like to express their sincere thanks
to Dr. Fei Wang of Research Institute of High Temperature Materials,
Central Iron and Steel Research Institute (CISRI) helped to design the
experimental apparatus. Ph.D. Bin Li, Shao-ying Li and Xue-liang Zhang
of School of Metallurgical and Ecological Engineering, and Professor
Cheng-bin Shi as well as Ph.D. Ding-li Zheng of State Key Laboratory of
Advanced Metallurgy (SKL) at University of Science and Technology
Beijing (USTB) contributed to the discussion of the results. The authors
are also thankful to the financial support from the National Natural
Science Foundation of China (Nos U1560203 and 51274031).
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NR 35
TC 26
Z9 29
U1 0
U2 51
PU NATURE PUBLISHING GROUP
PI LONDON
PA MACMILLAN BUILDING, 4 CRINAN ST, LONDON N1 9XW, ENGLAND
SN 2045-2322
J9 SCI REP-UK
JI Sci Rep
PD MAR 27
PY 2018
VL 8
AR 5232
DI 10.1038/s41598-018-23556-3
PG 14
WC Multidisciplinary Sciences
SC Science & Technology - Other Topics
GA GA5IK
UT WOS:000428366700012
PM 29588460
DA 2023-12-05
ER
PT J
AU Shin, JH
Park, JH
AF Shin, Jae Hong
Park, Joo Hyun
TI Effect of CaO/Al2O3 Ratio of Ladle Slag on
Formation Behavior of Inclusions in Mn and V Alloyed Steel
LA English
DT Article
DE Mn-V-alloyed steel; non-metallic inclusions; secondary refining; ladle
slag; refractory-slag-metal-inclusion (ReSMI) multiphase reactions
simulation; MgAl2O4 spinel
ID STAINLESS-STEEL; NONMETALLIC INCLUSIONS; FORMATION MECHANISM; SPINEL
INCLUSIONS; CALCIUM TREATMENT; DEOXIDATION; EQUILIBRIA; EVOLUTION;
ALUMINUM; SULFUR
AB The effect of CaO/Al2O3 (=C/A) ratio of the ladle slag on the formation behavior
of non-metallic inclusions in the Mn-V-alloyed steel was investigated using both
the experimental method and refractory-slag metal-inclusion (ReSMI) multiphase
reactions simulation. The formation behavior of inclusion was strongly affected by
the activity of MgO in the initial slag at the early stage of the reaction.
However, since the MgO activity converged to unity due to MgO dissolution from
refractory to slag during the reaction, the formation behavior of inclusion was
affected by the activity of CaO and Al2O3 in the slag rather than that of MgO at
the final stage of the reaction. From the experimental results and ReSMI multiphase
reaction model, the formation behavior of inclusions could be divided into three
cases according to the C/A ratio of the slag as follows; 1) C/A < 1.5; Alumina ->
Spinel -> Spinel + Liquid oxide, 2) 1.5 < C/A < 2.5; Alumina -> Spinel -> Liquid
oxide, 3) C/A > 3.0; Alumina -> Spinel -> Liquid oxide Magnesia. Therefore, it was
concluded that the C/A ratio of the ladle slag should be controlled from about 1.5
to 2.5 in order to suppress the harmful solid inclusions such as spinel during
secondary refining processes.
C1 [Shin, Jae Hong; Park, Joo Hyun] Hanyang Univ, Dept Mat Engn, Ansan 426791,
South Korea.
South Korea.
OI Shin, JaeHong/0000-0001-7737-4375
FU Korea Evaluation Institute of Industrial Technology (KEIT) [10063056]
Funding Source: Korea Institute of Science & Technology Information
(KISTI), National Science & Technology Information Service (NTIS);
National Research Foundation of Korea [22A20130012792] Funding Source:
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0136(95)02002-4
NR 36
TC 26
Z9 27
U1 4
U2 17
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2018
VL 58
IS 1
BP 88
EP 97
PG 10
GA FT8RH
UT WOS:000423420400011
DA 2023-12-05
ER
PT J
AU Kruger, D
Garbers-Craig, A
AF Kruger, Dirk
Garbers-Craig, Andrie
TI Characteristics and Modification of Non-metallic Inclusions in
Titanium-Stabilized AISI 409 Ferritic Stainless Steel
LA English
DT Article
ID MGO-CENTER-DOT-AL2O3 SPINEL INCLUSIONS; THERMODYNAMICS; EVOLUTION; SLAG
AB This study describes an investigation into the improvement of castability, final
surface quality and formability of titanium-stabilized AISI 409 ferritic stainless
steel on an industrial scale. Non-metallic inclusions found in this industrially
produced stainless steel were first characterized using SEM-EDS analyses through
the INCA-Steel software platform. Inclusions were found to consist of a MgO center
dot Al2O3 spinel core, which acted as heterogeneous nucleation site for titanium
solubility products. Plant-scale experiments were conducted to either prevent the
formation of spinel, or to modify it by calcium treatment. Modification to
spherical dual-phase spinel-liquid matrix inclusions was achieved with calcium
addition, which eliminated submerged entry nozzle clogging for this grade. Complete
modification to homogeneous liquid calcium aluminates was achieved at high levels
of dissolved aluminum. A mechanism was suggested to explain the extent of
modification achieved.
C1 [Garbers-Craig, Andrie] Univ Pretoria, Dept Mat Sci & Met Engn, Ctr
Pyrometallurgy, ZA-0002 Pretoria, South Africa.
[Kruger, Dirk] Columbus Stainless, Old Hendrina Rd, S-1055 Middelburg,
Mpumalanga, South Korea.
C3 University of Pretoria
RP Garbers-Craig, A (corresponding author), Univ Pretoria, Dept Mat Sci & Met Engn,
Ctr Pyrometallurgy, ZA-0002 Pretoria, South Africa.
EM Andrie.Garbers-Craig@up.ac.za
CR Ehara Y, 2007, TETSU TO HAGANE, V93, P1
GAO Y, 1993, ISIJ INT, V33, P291, DOI 10.2355/isijinternational.33.291
Harkness B., 1994, CONT CAST C P, P70
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Yin X, 2017, IRONMAK STEELMAK, V44, P152, DOI 10.1080/03019233.2016.1185285
Zheng H, 2004, AISTECH P, V1, P937
NR 31
TC 26
Z9 27
U1 0
U2 14
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD JUN
PY 2017
VL 48
IS 3
BP 1514
EP 1532
DI 10.1007/s11663-017-0945-5
PG 19
Engineering
GA ET6FF
UT WOS:000400385900011
DA 2023-12-05
ER
PT J
AU Hou, D
Jiang, ZH
Dong, YW
Gong, W
Cao, YL
Cao, HB
AF Hou, Dong
Jiang, Zhou-Hua
Dong, Yan-Wu
Gong, Wei
Cao, Yu-Long
Cao, Hai-bo
TI Effect of Slag Composition on the Oxidation Kinetics of Alloying
Elements during Electroslag Remelting of Stainless Steel: Part-2 Control
of Titanium and Aluminum Content
LA English
DT Article
DE electroslag remelting; kinetics; mass transfer; titanium control; ion
and molecule coexistence theory
ID SILICON
AB Kinetics of slag/metal reaction were investigated experimentally using 50 kg
electroslag remelting (ESR) furnace in order to clarify the effect of slag
containing different CaO and TiO2 content on titanium, aluminum and silicon content
during the ESR process with 1Cr21Ni5Ti stainless steel. The results obtained show
that the more CaO content in slag is, the more aluminum content in ingots
increases. The Ig([Al](4)/[Ti](3)) increases with the increase of slag temperature
in the first 13 minutes during the ESR process, and after the slag temperature
tends to be stable, the Ig([Al](4)/[Ti](3)) decreases with the increase of TiO2
content in the rest process. The penetration and film theories were employed to
analyze the rate determining step of slag/metal reaction, and it was found that the
rate determining step of the reaction was the mass transfer of aluminum through the
molten steel, silica through the slag and titanium on both of the metal and slag
sides. The slag containing low CaO content combined with extra titania constantly
added into molten slag in the first temperature-rising period is suitable for
electroslag remelting of 1Cr21Ni5Ti stainless steel with high titanium and low
aluminum content.
C1 [Hou, Dong; Jiang, Zhou-Hua; Dong, Yan-Wu; Gong, Wei; Cao, Yu-Long; Cao, Hai-bo]
Northeastern Univ, Sch Met, Shenyang 110819, Liaoning, Peoples R China.
RP Jiang, ZH (corresponding author), Northeastern Univ, Sch Met, Shenyang 110819,
OI Jiang, Zhouhua/0000-0001-8887-7250
FU National Nature Science Foundation of China [U1560203, 51274266];
Baosteel Group Corporation [U1560203]
FX This project is supported by Joint Research Fund of National Nature
Science Foundation of China and Baosteel Group Corporation with the
grant No. U1560203, and it is also supported by the National Nature
Science Foundation of China with the grant No. 51274266.
Blazenko K., 1978, HUETTENMAENN MONATSH, V123, P17
Hou D, 2016, IRONMAK STEELMAK, V43, P517, DOI 10.1080/03019233.2015.1110920
Hou D., 2017, ISIJ INT, V57, P1399
Jiang Z. H., 2000, PHYS CHEM TRANSMISSI, V154
Li Z. B., 2010, ELECTROSLAG METALLUR, V141
NR 13
TC 26
Z9 27
U1 3
U2 10
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 8
BP 1410
EP 1419
PG 10
GA FE7RF
UT WOS:000408403900015
DA 2023-12-05
ER
PT J
AU Zhang, TS
Liu, CJ
Qiu, JY
Li, XB
Jiang, MF
AF Zhang, Tongsheng
Liu, Chengjun
Qiu, Jiyu
Li, Xiaobing
Jiang, Maofa
TI Effect of Ti Content on the Characteristics of Inclusions in Al-Ti-Ca
Complex Deoxidized Steel
LA English
DT Article
DE calcium; titanium; inclusion; deoxidation; thermodynamic
ID LIQUID-IRON; DEOXIDATION EQUILIBRIUM; NONMETALLIC INCLUSION; OXYGEN
EQUILIBRIUM; OXIDE INCLUSIONS; KILLED STEEL; MG ADDITION; EVOLUTION;
THERMODYNAMICS; ALUMINUM
AB Experiments with different titanium addition were carried out in alumina
crucible without slag at 1 873 K to investigate the variation of inclusion
composition, size and morphology in Al-Ti-Ca complex deoxidized steel. The samples
exacted from the experimental steels were analyzed by field emission scanning
electron microscopy (FE-SEM) and energy dispersive spectroscopy (EDS). Titanium
influence significantly on the morphology, size distribution and composition of
oxide inclusions in Al-Ca deoxidized steels, and the inclusions characteristics
vary with titanium content. Liquid oxide inclusions are promptly modified by
titanium. On the other hand, titanium can also change solid calcium aluminate
inclusions into spherical ones in the melts similarly, but there are a number of
inhomogeneous inclusions in molten steel at the initial stage. Therefore, to modify
inclusions better, the content of titanium and calcium in molten steel should be
controlled simultaneously during the production process.
C1 [Zhang, Tongsheng; Qiu, Jiyu; Jiang, Maofa] Northeastern Univ, Sch Met & Mat,
POB 313, 3-11,Wenhua Rd,Heping Dist, Shenyang 110819, Peoples R China.
[Liu, Chengjun] Northeast Univ, Sch Met & Mat, Inst Ferrous Met, POB 313,3-
11,Wenhua Rd,Heping Dist, Shenyang 110819, Peoples R China.
[Li, Xiaobing] Northeastern Univ, Sch Met & Mat, Lab Ecol Met Multimetall Min
Minist Educ, POB 313, 3-11,Wenhua Rd,Heping Dist, Shenyang 110819, Peoples R China.
C3 Northeastern University - China; Northeastern University - China;
Northeastern University - China
RP Li, XB (corresponding author), Northeastern Univ, Sch Met & Mat, Lab Ecol Met
Multimetall Min Minist Educ, POB 313, 3-11,Wenhua Rd,Heping Dist, Shenyang 110819,
Peoples R China.
EM lixb_neu@sina.com
RI li, xiao/GSN-6181-2022; li, xiaofeng/GXF-9442-2022; liu,
xinyu/IWD-6630-2023
Fundamental Research Funds for the Central Universities of China
[N120602005]
FX The authors wish to thank the National Natural Science Foundation of
China (No. 51374059 and No. 51374060) and the Fundamental Research Funds
for the Central Universities of China (No. N120602005) for their
financial support for the current study.
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NR 64
TC 26
Z9 28
U1 4
U2 26
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 2
BP 314
EP 321
PG 8
GA EO4CO
UT WOS:000396642300014
OA gold
DA 2023-12-05
ER
PT J
AU Xie, X
Li, YJ
Liu, CT
Wang, WJ
AF Xie, Xin
Li, Ying-Jie
Liu, Chang-Tian
Wang, Wen-Jing
TI HCl absorption by CaO/Ca3Al2O6 sorbent
from CO2 capture cycles using calcium looping
LA English
DT Article
DE HCl absorption; Carbide slag; CaO/Ca3Al2O6 sorbent; Calcium looping; CO2
capture
ID CA-BASED SORBENTS; HYDRATED LIME REACTION; HOT FLUE-GASES;
FLUIDIZED-BED; CARBIDE SLAG; TEMPERATURE; LIMESTONE; KINETICS;
ENHANCEMENT; PERFORMANCE
AB The synthetic CaO/Ca3Al2O6 (prepared from carbide slag, aluminum nitrate
enneahydrate, and glycerol water solution by combustion synthesis) as a CO2 sorbent
discharged from the CO2 capture cycles using the calcium looping was used to remove
HCl after a series of carbonation/calcination cycles. The effects of chlorination
temperature, HCl concentration, presence of CO2, and cycle number on the HCl
absorption by the CaO/Ca3Al2O6 sorbent after the repetitive carbonation/calcination
cycles for CO2 capture were discussed. In addition, the HCl absorption capacities
of the CaO/Ca3Al2O6 sorbent and the carbide slag were compared. The chlorination
products of the CaO/Ca3Al2O6 sorbent after 1 h HCl absorption are CaClOH, CaO, and
Ca3Al2O6 detected by XRD analysis. Among 600-800 degrees C, the CaO/Ca3Al2O6
sorbent from the carbonation/calcination cycles achieves the highest HCl absorption
capacity at 700 degrees C. The HCl absorption capacity of the cycled CaO/Ca3Al2O6
sorbent rises as HCl concentration increases. CO2 is adverse to the HCl absorption
by the cycled CaO/Ca3Al2O6 sorbent in the chlorination process. With the
carbonation/calcination cycle number increasing from 0 to 50, the CaO/Ca3Al2O6
sorbent after 5 cycles exhibits the highest HCl absorption capacity. HCl absorption
capacities of the cycled CaO/Ca3Al2O6 sorbent after 20 and 50 cycles were 0.18 and
0.13 g/g, which were 2.3 and 2.6 times as high as those of the cycled carbide slag
after the same cycles, respectively. (C) 2015 Elsevier B.V. All rights reserved.
C1 [Xie, Xin; Li, Ying-Jie; Liu, Chang-Tian; Wang, Wen-Jing] Shandong Univ, Sch
Energy & Power Engn, Jinan 250061, Peoples R China.
C3 Shandong University
EM liyj@sdu.edu.cn
OI Wang, Wenjing/0000-0003-1090-388X
FX Financial support from the National Natural Science Foundation of China
(51376003) is gratefully appreciated.
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TC 26
Z9 27
U1 2
U2 45
PI AMSTERDAM
SN 0378-3820
EI 1873-7188
PD OCT
PY 2015
VL 138
BP 500
EP 508
DI 10.1016/j.fuproc.2015.06.028
PG 9
GA CT6JV
UT WOS:000362920200058
DA 2023-12-05
ER
PT J
AU Liu, MQ
Niu, SL
Lu, CM
Cheng, SQ
AF Liu, Mengqi
Niu, Shengli
Lu, Chunmei
Cheng, Shiqing
TI An optimization study on transesterification catalyzed by the activated
carbide slag through the response surface methodology
SO ENERGY CONVERSION AND MANAGEMENT
LA English
DT Article
DE Biodiesel; Transesterification; Catalyst; Carbide slag; Response surface
methodology
ID SOLID BASE CATALYST; BIODIESEL PRODUCTION; SOYBEAN OIL; ASSISTED
TRANSESTERIFICATION; SUNFLOWER OIL; CALCIUM-OXIDE; METAL-OXIDES;
JATROPHA OIL; SEED; CAO
AB After activated at 850 degrees C under air condition, calcium hydroxide and
calcium carbonate in carbide slag are transformed into calcium oxide. The prepared
transesterification catalyst, labeled as CS-850, gains surface area of 8.00 m(2)
g(-1), functional groups of vanishing O-C-O and O-H bonds, surface morphology of
tenuous branch and porous structure and basic strength of 9.8 < H_ < 15.0. From
aspects of the molar ratio of methanol to oil (gamma), the catalyst added amount
(zeta) and the reaction temperature (T-r), transesterification catalyzed by CS-850
is optimized through the Box-Behnken design of the response surface methodology
(BBD-RSM). A quadratic polynomial model is preferred for transesterification
efficiency prediction with coefficient of determination (R-2) of 0.9815. The
optimal parameters are predicted to be gamma = 13.8, zeta = 6.7% and T-r = 60
degrees C with the efficiency of 94.70% and validated by experimental value of
93.83%. Meanwhile, gamma is demonstrated to be the most significant variable for
the minimum p-value. Besides, CS-850 performs acceptable reusability and for the
fifth time reusage, efficiency of 82.61% could still be supplied. Aluminium oxide
is proved to have the greatest effect on the catalytic activity of CS-850 among
other small quality oxides. Physicochemical properties of the purified biodiesel
meet American Society for Testing and Material (ASTM) standard. (C) 2014 Elsevier
C1 [Liu, Mengqi; Niu, Shengli; Lu, Chunmei; Cheng, Shiqing] Shandong Univ, Sch
Energy & Power Engn, Jinan 250061, Peoples R China.
RP Niu, SL (corresponding author), Shandong Univ, Sch Energy & Power Engn, 17923
Jingshi Rd, Jinan 250061, Peoples R China.
EM nsl@sdu.edu.cn
RI cheng, sq/GPT-4112-2022
FU Natural Science Foundation of China [51206098]; China Postdoctoral
Science Foundation [2013T60667]; Promotive Research Fund for Excellent
Young and Middle-aged Scientists of Shandong Province, China
[BS2012NJ005]
FX This work is supported by Natural Science Foundation of China
(51206098), China Postdoctoral Science Foundation Special Funding
(2013T60667) and Promotive Research Fund for Excellent Young and
Middle-aged Scientists of Shandong Province, China (BS2012NJ005).
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NR 41
TC 26
Z9 28
U1 1
U2 36
PI OXFORD
SN 0196-8904
EI 1879-2227
J9 ENERG CONVERS MANAGE
JI Energy Conv. Manag.
PD MAR 1
PY 2015
VL 92
BP 498
EP 506
DI 10.1016/j.enconman.2014.12.074
PG 9
WC Thermodynamics; Energy & Fuels; Mechanics
SC Thermodynamics; Energy & Fuels; Mechanics
GA CB6GF
UT WOS:000349724800046
DA 2023-12-05
ER
PT J
AU Ma, WJ
Bao, YP
Wang, M
Zhao, DW
AF Ma, W. -J.
Bao, Y. -P.
Wang, M.
Zhao, D. W.
TI Influence of slag composition on bearing steel cleanness
LA English
DT Article
DE Bearing steel; Cleanness; Slag; Inclusion
ID INCLUSIONS
AB Al2O3 and high Al2O3 content composite oxides are the main types of inclusions
in aluminium killed bearing steel, and these also have the most significant impact
on rolling contact fatigue (RCF) life. The calculation results in the phase diagram
by using the FactSage showed that the activity of Al2O3 reached the minimum with
the slag composition in a low melting point area at a MgO content less than 5%; a
basicity of 5 to 8 and a ratio of CaO/Al2O3 of 1.5 to 2.0 in slag. This slag was
most effective in improving the absorption ability of slag for inclusions in
bearing steel. By using the experimental slag, the total oxygen could be reduced to
7-10 ppm at Hangzhou Iron and Steel Group Company (HIRGC).
C1 [Ma, W. -J.; Bao, Y. -P.; Wang, M.; Zhao, D. W.] Univ Sci & Technol Beijing,
State Key Lab Adv Met, Beijing 100083, Peoples R China.
[Ma, W. -J.; Bao, Y. -P.; Wang, M.; Zhao, D. W.] Univ Sci & Technol Beijing, Sch
Met & Ecol Engn, Beijing 100083, Peoples R China.
Technology Beijing
RP Ma, WJ (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
EM mawenjun2929@163.com
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[Anonymous], 2003, CLEANNESS AND FATIGU
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NR 17
TC 26
Z9 28
U1 2
U2 19
PU MANEY PUBLISHING
PI LEEDS
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD JAN
PY 2014
VL 41
IS 1
BP 26
EP 30
DI 10.1179/1743281212Y.0000000096
PG 5
GA AE6OZ
UT WOS:000334114700005
DA 2023-12-05
ER
PT J
AU López-Delgado, A
Tayibi, H
AF Lopez-Delgado, Aurora
Tayibi, Hanan
TI Can hazardous waste become a raw material? The case study of an
aluminium residue: a review
LA English
DT Review
DE Aluminium hazardous waste; end-of-waste; glass/glass-ceramic; boehmite;
calcium aluminate
ID CHEMICAL-SYNTHESIS; BOEHMITE; GLASS; VITRIFICATION; CRYSTALLIZATION;
BEHAVIOR; INDUSTRY; CEMENT; ALOOH
AB The huge number of research studies carried out during recent decades focused on
finding an effective solution for the waste treatment, have allowed some of these
residues to become new raw materials for many industries. Achieving this ensures a
reduction in energy and natural resources consumption, diminishing of the negative
environmental impacts and creating secondary and tertiary industries. A good
example is provided by the metallurgical industry, in general, and the aluminium
industry in this particular case. The aluminium recycling industry is a beneficial
activity for the environment, since it recovers resources from primary industry,
manufacturing and post-consumer waste. Slag and scrap which were previously
considered as waste, are nowadays the raw material for some highly profitable
secondary and tertiary industries. The most recent European Directive on waste
establishes that if waste is used as a common product and fulfils the existing
legislation for this product, then this waste can be defined as 'end-of-waste'. The
review presented here, attempts to show several proposals for making added-value
materials using an aluminium residue which is still considered as a hazardous
waste, and accordingly, disposed of in secure storage. The present proposal
includes the use of this waste to manufacture glass, glass-ceramic, boehmite and
calcium aluminate. Thus the waste might effectively be recovered as a secondary
source material for various industries
C1 [Lopez-Delgado, Aurora; Tayibi, Hanan] CSIC, Natl Ctr Met Res, Madrid 28040,
Spain.
C3 Consejo Superior de Investigaciones Cientificas (CSIC)
RI Lopez-Delgado, Aurora/D-3785-2012
OI Lopez-Delgado, Aurora/0000-0002-0121-9501
FU CAM [07M/0136/2000]; MEC [CTM2005-01964]
FX The projects 07M/0136/2000 and CTM2005-01964 were financed by CAM and
MEC, respectively
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NR 67
TC 26
Z9 27
U1 6
U2 75
PU SAGE PUBLICATIONS LTD
PI LONDON
PA 1 OLIVERS YARD, 55 CITY ROAD, LONDON EC1Y 1SP, ENGLAND
SN 0734-242X
EI 1096-3669
J9 WASTE MANAGE RES
PD MAY
PY 2012
VL 30
IS 5
BP 474
EP 484
DI 10.1177/0734242X11422931
PG 11
GA 951KS
UT WOS:000304720000003
PM 22071175
DA 2023-12-05
ER
PT J
AU Hessien, MM
Kashiwaya, Y
Ishii, K
Nasr, MI
El-Geassy, AA
AF Hessien, M. M.
Kashiwaya, Y.
Ishii, K.
Nasr, M. I.
El-Geassy, A. A.
TI Sintering and heating reduction processes of alumina containing iron ore
samples
LA English
DT Article
DE iron ore sinter; alumina; structure; reduction; microanalysis; silico
calcium aluminium ferrite; haematite; magnetite; iron; slag
ID SLAG-GRAPHITE WETTABILITY; REACTION-KINETICS; MINERAL PHASES;
BLAST-FURNACE; BEHAVIOR; AL2O3
AB Alumina containing iron ore samples (0.7-5.5%Al2O3) were sintered in a down
draft sinter pot. The structures of the produced sinters were microscopically
examined and the different phases developed were identified. Electron probe micro
analyser (EPMA) was used for the quantitative analysis of Fe, Ca, Si, Mn and Al in
different phases. Silico ferrite of calcium and alumina (SFCA) phase sinter was
identified and its stability was Al2O3 content dependent. In sinter containing <=
1.5%Al2O3, SFCA was dissociated at higher temperatures to porous magnetite and
silicate melt. In samples containing >= 2.5% Al2O3, SFCA was stable and its
quantity increased with increasing alumina content. The non-isothermal reduction of
sinter samples was carried out using a heating reduction technique with the
facility of following up the high temperature phenomena during reduction process.
X-ray observations, reduction rate profile and the gasification rate were used for
the determination of high temperature properties of samples. In the gas-solid
reduction region, Al2O3 increased the reduction rate (RDR) at the initial stage up
to 1073 K and the RDR increases with increasing Al2O3 content up to 2.5%. At > 1073
K, the RDR was relatively slower due to the presence of primary low melt slag
containing alumina. For sinter containing.2.5% Al2O3, the lowering in RDR and total
reduction degree (TRD) starts to decrease with increasing Al2O3 content as a result
of the formation of SFCA phase which has a good reducibility and as a consequence
of the decrease in the quantity of the primary low melt slag containing alumina. No
more than >= 2.5% Al2O3 in the slag results in a harmful effect on the high
temperature properties while higher alumina content in sinter leads to the
formation of SFCA which improves the high temperature reduction properties.
C1 [Hessien, M. M.; Nasr, M. I.; El-Geassy, A. A.] CMRDI, Cairo, Egypt.
[Kashiwaya, Y.; Ishii, K.] Hokkaido Univ, Fac Engn, Sapporo, Hokkaido 060,
Japan.
Development Institute (CMRDI); Hokkaido University
RP Hessien, MM (corresponding author), CMRDI, POB 87 Helwan, Cairo, Egypt.
EM hessien@hotmail.com
RI Hessien, Mahmoud/CAJ-3142-2022; Hessien, Mahmoud M./AFW-2870-2022
OI Hessien, Mahmoud/0000-0003-2607-0050; Hessien, Mahmoud
M./0000-0003-2607-0050; El-Geassy, Abdel-Hady/0000-0002-2382-0568
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NR 24
TC 26
Z9 27
U1 2
U2 20
PU MANEY PUBLISHING
PI LEEDS
SN 0301-9233
J9 IRONMAK STEELMAK
PD APR
PY 2008
VL 35
IS 3
BP 191
EP 204
DI 10.1179/030192307X239551
PG 14
GA 301FK
UT WOS:000255881600006
DA 2023-12-05
ER
PT J
AU Li, HB
Jiang, ZH
Shen, MH
You, XM
AF Li Hua-bing
Jiang Zhou-hua
Shen Ming-hui
You Xiang-mi
TI High nitrogen austenitic stainless steels manufactured by nitrogen gas
alloying and adding nitrided ferroalloys
LA English
DT Article
DE nitrogen gas alloying; nitrided ferroalloy; high nitrogen austenitic
stainless steel; vacuum induction melting; electroslag remelting
AB A simple and feasible method for the production of high nitrogen austenitic
stainless steels involves nitrogen gas alloying and adding nitrided ferroalloys
under normal atmospheric conditions. Alloying by nitrogen gas bubbling in Fe-Cr-Mn-
Mo series alloys was carried out in MoSiz resistance furnace and air induction
furnace under normal atmospheric conditions. The results showed that nitrogen
alloying could be accelerated by increasing nitrogen gas flow rate, prolonging
residence time of bubbles, increasing gas/molten steel interfaces, and decreasing
the sulphur and oxygen contents in molten steel. Nitrogen content of 0.69% in
18Cr18Mn was obtained using air induction furnace by bubbling of nitrogen gas from
porous plug. In addition, the nickel-free, high nitrogen austenitic stainless
steels with sound and compact macrostructure had been produced in the laboratory
using vacuum induction furnace and electroslag remelting furnace under nitrogen
atmosphere by the addition of nitrided alloy with the maximum nitrogen content of
0.81%. Pores were observed in the ingots obtained by melting and casting in vacuum
induction furnace with the addition of nitrided ferroalloys and under nitrogen
atmosphere. After electroslag remelting of the cast ingots, they were all sound and
were free of pores. The yield of nitrogen increased with the decrease of melting
rate in the ESR process. Due to electroslag remelting under nitrogen atmosphere and
the consequential addition of aluminum as deoxidizer to the slag, the loss of
manganese decreased obviously. There existed mainly irregular Al2O3 inclusions and
MnS inclusions in ESR ingots, and the size of most of the inclusions was less than
5 mu m. After homogenization of the hot rolled plate at 1 150 degrees C X 1 h
followed by water quenching, the microstructure consisted of homogeneous austenite.
C1 Northeastern Univ, Sch Met & Mat, Shenyang 110004, Liaoning, Peoples R China.
RP Li, HB (corresponding author), Northeastern Univ, Sch Met & Mat, Shenyang
EM huabing_li@163.com
RI 李, 花兵/IQU-2254-2023
OI 李, 花兵/0000-0002-4182-9486
CR Jiang ZH, 2005, STEEL RES INT, V76, P740, DOI 10.1002/srin.200506090
Mudali U.K., 2004, HIGH NITROGEN STEELS
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NR 5
TC 26
Z9 27
U1 1
U2 16
PU SPRINGER
PI NEW YORK
SN 1006-706X
EI 2210-3988
PD MAY
PY 2007
VL 14
IS 3
BP 63
EP 68
PG 6
GA 183EE
UT WOS:000247554700012
DA 2023-12-05
ER
PT J
AU Murgier, S
Zanni, H
Gouvenot, D
AF Murgier, S
Zanni, H
Gouvenot, D
TI Blast furnace slag cement:: a 29Si and 27Al NMR
study
SO COMPTES RENDUS CHIMIE
LA English
CT 18th GERM Conference
CY MAY 18-23, 2003
CL Batz sur Mer, FRANCE
DE ground granulated blast-furnace slag; NMR
ID C-S-H; HYDRATION; ALUMINUM
AB Ground granulated blast-furnace slag (GGBS) is a secondary product of cast-iron
industry that can be used like a standard hydraulic binder. Nevertheless, it
requires a chemical activation to start the slag-hydration process. In this work,
four activators are studied. Solid-state NMR and mechanical compression tests are
used to determine the hydration products microstructure and performances. (C) 2004
Academie des sciences. Published by Elsevier SAS. All rights reserved.
C1 ESPCI, CNRS, UMR 7636, Phys & Mecan Milieux Heterogenes Lab, F-75231 Paris 05,
France.
Soletanche Bachy France, F-92000 Nanterre, France.
C3 Sorbonne Universite; Universite Paris Cite; Centre National de la
Recherche Scientifique (CNRS); CNRS - Institute for Engineering &
Systems Sciences (INSIS); Universite PSL; Ecole Superieure de Physique
et de Chimie Industrielles de la Ville de Paris (ESPCI)
RP Murgier, S (corresponding author), ESPCI, CNRS, UMR 7636, Phys & Mecan Milieux
Heterogenes Lab, 10,Rue Vauquelin, F-75231 Paris 05, France.
EM smurgier@pmmh.espci.fr
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TC 26
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U1 1
U2 28
PU ACAD SCIENCES
PI PARIS
PA 23 QUAI DE CONTI, PARIS, FRANCE
SN 1631-0748
EI 1878-1543
J9 CR CHIM
JI C. R. Chim.
PD MAR-APR
PY 2004
VL 7
IS 3-4
BP 389
EP 394
DI 10.1016/j.crci.2004.02.004
PG 6
SC Chemistry
GA 825WJ
UT WOS:000221789100026
OA Green Published
DA 2023-12-05
ER
PT J
AU Shen, HL
Liu, B
Shi, ZS
Zhao, SZ
Zhang, JJ
Zhang, SG
AF Shen, Hanlin
Liu, Bo
Shi, Zhisheng
Zhao, Shizhen
Zhang, Junjie
Zhang, Shengen
TI Reduction for heavy metals in pickling sludge with aluminum nitride in
secondary aluminum dross by pyrometallurgy, followed by glass ceramics
manufacture
LA English
DT Article
DE Secondary aluminum dross (SAD); Pickling sludge; Reduction by aluminum
nitride (AlN); Heavy metals; Glass ceramics
ID HYDROLYSIS
AB Secondary aluminum dross (SAD) from aluminum industry is classified as a
hazardous solid waste due to containing aluminum nitride (AlN). In this work, AlN
was first used to reduce heavy metals by pyrometallurgy. The reduction rates for
iron, chromium and nickel were up to 90%, 80% and 100%, respectively. However, the
reduction from AlN and oxygen oxidization of AlN occurred simultaneously. AlN which
formed solid solution with alumina could reduce heavy metals, while the rest was
oxidized by oxygen. In addition, the reduction rates for iron and chromium could be
increased with increasing CaF2 from 6.7 to 9.0 wt%. CaF2 could decreased viscosity
of molten slag, which favored the ion migration, and then increased the reduction
rates. After the reduction, glass ceramics were manufactured from the molten slags.
The bending strength, microhardness and alkali resistance of the glass ceramics
were up to 77 MPa, 1011 HV and 98.7%, respectively. According to XRD and SEM
results, glass ceramics with CaAl2SiO6 crystal phase, crosslinked network structure
grains and smaller pores exhibited better bending resistance. In addition, glass
ceramics with CaAl2SiO6 crystal phase possessed the highest microhardness and
alkali resistance. After this process, hazardous pickling sludge and SAD were
totally recycled.
C1 [Shen, Hanlin; Liu, Bo; Shi, Zhisheng; Zhao, Shizhen; Zhang, Junjie; Zhang,
Shengen] Univ Sci & Technol Beijing, Inst Adv Mat & Technol, Beijing 100083,
Peoples R China.
RP Zhang, SG (corresponding author), Univ Sci & Technol Beijing, Inst Adv Mat &
Technol, Beijing 100083, Peoples R China.
EM zhangshengen@mater.ustb.edu.cn
RI zhang, junjie/HIK-4860-2022; Shen, Hanlin/IVH-1336-2023
OI Zhang, Junjie/0000-0003-3425-2794
FU National Key RD Projects [2019YFC1907101, 2019YFC1907103,
2017YFB0702304]; Key R&D Project in Ningxia Hui Autonomous Region
[2020BCE01001]; National Natural Science Foundation of China [U2002212,
51672024]; Xijiang Inno-vation and Entrepreneurship Team [2017A0109004];
Fundamental Research Funds for the Central Universities [FRF-BD-20-24A,
FRF-TP-20-031A1, FRF-IC-19-017Z, FRF-GF-19-032B, 06500141]; State Key
Laboratory for Advanced Metals and Materials [2019Z-05]; Integration of
Green Key Process Systems MIIT
FX This work was sponsored by the National Key R&D Projects (Grants No.
2019YFC1907101, 2019YFC1907103, 2017YFB0702304) , Key R&D Project in
Ningxia Hui Autonomous Region (Grants No.2020BCE01001) , key and normal
projects National Natural Science Foundation of China (Grants No.
U2002212, 51672024) , Xijiang Inno-vation and Entrepreneurship Team
(Grants No. 2017A0109004) , the Fundamental Research Funds for the
Central Universities (Grants No. FRF-BD-20-24A, FRF-TP-20-031A1,
FRF-IC-19-017Z, FRF-GF-19-032B, 06500141) , Financial support from the
State Key Laboratory for Advanced Metals and Materials (Grants No.
2019Z-05) and Integration of Green Key Process Systems MIIT. The authors
would like to thank the editor for editing of the manuscript and the
anonymous reviewers for their detailed and helpful comments.
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NR 34
TC 25
Z9 25
U1 13
U2 69
PU ELSEVIER
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD SEP 15
PY 2021
VL 418
AR 126331
DI 10.1016/j.jhazmat.2021.126331
EA JUN 2021
PG 10
GA UL3YE
UT WOS:000692589800001
PM 34329004
DA 2023-12-05
ER
PT J
AU Zhou, SK
Wang, M
Tan, HZ
Wang, XB
Yang, WJ
Xiong, XH
Yang, FX
AF Zhou, Shangkun
Wang, Meng
Tan, Houzhang
Wang, Xuebin
Yang, Wenjun
Xiong, Xiaohe
Yang, Fuxin
TI Evaluation of aluminum ash in alleviating the ash deposition of
high-sodium and high-iron coal
SO FUEL
LA English
DT Article
DE High-sodium coal; High-iron coal; Aluminum ash; Ash fusion temperatures;
Ash deposition; Sodium capture
ID ZHUNDONG COAL; MELTING BEHAVIOR; HIGH-TEMPERATURE; COMBUSTION; CALCIUM;
VERMICULITE; FE2O3
AB The high sodium and high iron contents induce severe ash deposition in
pulverized coal boiler. Additive injection technology is deemed as an effective
solution to solve these problems. This work is to evaluate the effect of aluminum
ash on alleviating the ash deposition of high-sodium and high-iron coal. Results
show that sodium vapor volatilizes, condenses and forms a viscous bottom layer,
then the co-melting behavior of sodium-containing mineral and calcium
aluminosilicate causes the ash deposition of high-sodium coal, and the co-melting
behavior of Fe2O3 and calcium aluminosilicate causes the ash deposition of high-
iron coal. When the addition ratio of aluminum ash reaches 4%, ST (softening
temperature) and FT (flowing temperature) of mixed ash sample are close to and
exceed 1773 K, meanwhile, slag types of ash deposit are transformed from molten
slag and viscous slag to attached ash. Al2O3 and MgAl2O4 in aluminum ash can
inhibit the interaction between sodium, iron and calcium aluminosilicate, making
the particles less sticky. The optimum temperature of aluminum ash for sodium
capture is 823 K. Aluminum ash has a better sodium capture ability for high-sodium
coal than high-iron coal. Based on the above analysis, this work also provides the
blending strategies of additives due to the different ash deposition mechanisms of
coal.
C1 [Zhou, Shangkun; Wang, Meng; Tan, Houzhang; Wang, Xuebin; Yang, Wenjun; Xiong,
Xiaohe; Yang, Fuxin] Xi An Jiao Tong Univ, MOE Key Lab Thermofluid Sci & Engn, Xian
C3 Xi'an Jiaotong University
RP Tan, HZ (corresponding author), Xi An Jiao Tong Univ, MOE Key Lab Thermofluid
Sci & Engn, Xian 710049, Peoples R China.
EM hzt@mail.xjtu.edu.cn
RI Zhou, Shangkun/HLH-1640-2023; Wang, Xuebin/C-7203-2015
OI Wang, Xuebin/0000-0003-4270-7330
FU National Key Research and Development Program of China [2016YFB0600605]
FX This study was supported by the National Key Research and Development
Program of China (2016YFB0600605). Thanks to the advanced instruments
provided by instrumental analysis center of Xi'an Jiaotong University
and the patient tests provided by Zijun Ren.
CR [Anonymous], 2018, BP STAT REV
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NR 27
TC 25
Z9 28
U1 4
U2 65
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD AUG 1
PY 2020
VL 273
AR 117701
DI 10.1016/j.fuel.2020.117701
PG 9
GA LG6DI
UT WOS:000528188600026
DA 2023-12-05
ER
PT J
AU Wu, RD
Dai, SB
Jian, SW
Huang, J
Lv, Y
Li, BD
Azizbek, N
AF Wu, RenDi
Dai, ShaoBin
Jian, ShouWei
Huang, Jun
Lv, Yang
Li, BaoDong
Azizbek, Nurmirzayev
TI Utilization of the circulating fluidized bed combustion ash in
autoclaved aerated concrete: Effect of superplasticizer
LA English
DT Article
DE Circulating fluidized bed combustion ash; Autoclaved aerated concrete;
Polycarboxylate superplasticizers; Slurry property; Physic-mechanical
property; Pore distribution
ID CO-FIRING COAL; FLY-ASH; CFBC ASH; CEMENTITIOUS PROPERTIES;
IRON-TAILINGS; HYDRATION; MECHANISM; TECHNOLOGIES; ADSORPTION; SLAG
AB This paper aims to solve the problem of high water absorption in the use of
circulating fluidized bed combustion ash. Meanwhile, the feasibility of using the
circulating fluidized bed combustion ash to prepare autoclaved aerated concrete was
studied. The circulating fluidized bed combustion ash autoclaved aerated concrete
samples with different water consumption and different dosages of water reducing
agent were prepared. The rheological properties and gas-foaming results of the
slurry, the compressive strength, the dry density, specific strength, pore
structure and hydration products of the products were analyzed. The results show
that the incorporation of polycarboxylate superplasticizers has a positive effect
on the rheological properties of the slurry, the gas generation, and the physical
properties of the sample. Its water reducing effect not only can improve the
rheological properties of the slurry to match the gas generation rate of the
aluminum powder, but also optimize the pore structure to reduce the number of
harmful pores (less than 50 nm) and improve the strength of the product. Because a
large number of uneven macropores are introduced, the high water consumption is
unfavorable to the compressive strength of the product to a certain extent.
However, too low water consumption would hinder cement hydration to produce C-S-H
gel and reduce the formation of tobermorite. It is noticed that the reasonable
combination of water consumption and water reducing agent can improve the strength
of aerated concrete products without significantly changing the bulk density of the
sample. This paper provides a theoretical basis for use of other high-water-demand
solid wastes similar to circulating fluidized bed fly ash in the preparation of
autoclaved aerated concrete. (C) 2019 Elsevier Ltd. All rights reserved.
C1 [Wu, RenDi; Dai, ShaoBin; Huang, Jun] Wuhan Univ Technol, Sch Civil Engn &
Architecture, Wuhan 430070, Peoples R China.
[Wu, RenDi; Jian, ShouWei; Lv, Yang; Li, BaoDong] Wuhan Univ Technol, State Key
Lab Silicate Mat Architectures, Wuhan 430070, Peoples R China.
[Jian, ShouWei; Lv, Yang; Li, BaoDong; Azizbek, Nurmirzayev] Wuhan Univ Technol,
Sch Mat Sci & Engn, Wuhan 430070, Peoples R China.
C3 Wuhan University of Technology; Wuhan University of Technology; Wuhan
RP Jian, SW (corresponding author), Wuhan Univ Technol, State Key Lab Silicate Mat
Architectures, Wuhan 430070, Peoples R China.; Jian, SW (corresponding author),
Wuhan Univ Technol, Sch Mat Sci & Engn, Wuhan 430070, Peoples R China.
EM jianshouweiwhut@163.com
OI li, baodong/0000-0002-4886-0240
State Key Laboratory of Silicate Materials for Architectures (Wuhan
University of Technology, China) [SYSJJ2018-17]
FX The work is supported by The National Key Research and Development
Program of China (2017YFC0703202) and State Key Laboratory of Silicate
Materials for Architectures (Wuhan University of Technology, China) (NO.
SYSJJ2018-17). The author is grateful for the helpful discussions and
comments by Dr Liu Min.
CR [Anonymous], 2007, 1752007 GT
[Anonymous], WASTE MAT USED CONCR
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NR 54
TC 25
Z9 27
U1 7
U2 58
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD MAR 20
PY 2020
VL 237
AR 117644
DI 10.1016/j.conbuildmat.2019.117644
PG 12
GA LF3KT
UT WOS:000527320400053
DA 2023-12-05
ER
PT J
AU Zhao, WR
Li, JY
Jiang, J
Lu, HL
Hong, ZN
Qian, W
Xu, RK
Deng, KY
Guan, P
AF Zhao, Wen-rui
Li, Jiu-yu
Jiang, Jun
Lu, Hai-long
Hong, Zhi-neng
Qian, Wei
Xu, Ren-kou
Deng, Kai-Ying
Guan, Peng
TI The mechanisms underlying the reduction in aluminum toxicity and
improvements in the yield of sweet potato (Ipomoea batatas L.)
After organic and inorganic amendment of an acidic ultisol
SO AGRICULTURE ECOSYSTEMS & ENVIRONMENT
LA English
DT Article
DE Organic materials; Alkaline slag; Soluble Al species; Al toxicity;
Acidic soil
ID INDUSTRIAL BY-PRODUCTS; SOIL-PH CHANGES; CROP RESIDUES;
BIOLOGICAL-ACTIVITY; ALKALINE SLAG; PLANT-CELLS; AL TOXICITY;
ACIDIFICATION; NITROGEN; FRACTIONATION
AB Soil acidification limits crop and pasture production and leads to the
degradation of agroecosystems. The dissolution of aluminum (Al) in acidic soils can
lead to Al toxicity towards plants depending on the species of Al present, and can
decrease crop yield. Different organic materials have been suggested to alleviate
Al toxicity and increase the yields of important crops such as sweet potato
(Ipomoea batatas L.). Therefore, soil solution was collected from different
treatments in a field experiment to investigate how sweet potato yield responds to
different Al toxicity levels. The Al species in the soil solution were
characterized and the nutrient contents were determined to evaluate the efficacy of
alleviating Al toxicity by making a single application of canola straw (CS), peanut
straw (PS), commercial organic fertilizer (OF), lime, or alkaline slag (AS); and a
combined application of AS with one of the three organic materials in an acidic
Ultisol. The aims were to alleviate Al toxicity and increase sweet potato yields.
The results showed that all the amendments significantly decreased (P < 0.05) the
total Al, monomeric Al, monomeric inorganic Al, and Al3+ concentrations in the soil
solution. The AS and lime applications were more effective at decreasing the
concentrations of phytotoxic Al species in the soil solution than applications of
the three organic materials alone, and the Al3+ concentration decreased to as low
as 7 mu M, which was similar to lime. The AS, in combination with PS or OF, was
more effective than their respective sole applications in decreasing phytotoxic Al
species. The combined applications increased nutrient contents, and enhanced
nutrient uptake by sweet potato. The mitigation of soil Al toxicity and the
increase in nutrient contents after fertilization improve crop growth and crop
yields in acidic soils. The AS + PS and AS + OF treatments were the best amendments
for acidic Ultisols.
C1 [Zhao, Wen-rui; Li, Jiu-yu; Jiang, Jun; Lu, Hai-long; Hong, Zhi-neng; Qian, Wei;
Xu, Ren-kou; Deng, Kai-Ying; Guan, Peng] Chinese Acad Sci, Inst Soil Sci, State Key
Lab Soil & Sustainable Agr, POB 821, Nanjing, Jiangsu, Peoples R China.
[Zhao, Wen-rui; Lu, Hai-long; Xu, Ren-kou; Guan, Peng] Univ Chinese Acad Sci,
Coll Resources & Environm, Beijing 100049, Peoples R China.
EM rkxu@issas.ac.cn
RI Guan, Peng/AAH-9051-2019; Hong, Zhineng/G-4635-2013; Lu,
Hailong/HPD-8087-2023; Jiang, Jun/G-9125-2011
OI Guan, Peng/0000-0002-4207-0053; Hong, Zhineng/0000-0002-9549-7368;
Jiang, Jun/0000-0001-8686-9476
FU National Natural Science Foundation of China [41877036]; National Key
Research and Development of China [2016YFD0200302]
FX This study was supported by National Natural Science Foundation of China
(grant number 41877036) and the National Key Research and Development of
China (grant number 2016YFD0200302).
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NR 69
TC 25
Z9 29
U1 12
U2 103
PU ELSEVIER
PI AMSTERDAM
SN 0167-8809
EI 1873-2305
J9 AGR ECOSYST ENVIRON
JI Agric. Ecosyst. Environ.
PD FEB 1
PY 2020
VL 288
AR 106716
DI 10.1016/j.agee.2019.106716
PG 10
WC Agriculture, Multidisciplinary; Ecology; Environmental Sciences
SC Agriculture; Environmental Sciences & Ecology
GA JS3OF
UT WOS:000500217500008
DA 2023-12-05
ER
PT J
AU Maniraj, S
Thanigaivelan, R
AF Maniraj, S.
Thanigaivelan, R.
TI Optimization of Electrochemical Micromachining Process Parameters for
Machining of AMCs with Different % Compositions of GGBS Using Taguchi
and TOPSIS Methods
SO TRANSACTIONS OF THE INDIAN INSTITUTE OF METALS
LA English
DT Article
DE Electrochemical micromachining (EMM); Material removal rate; Radial
overcut; Aluminum composites; TOPSIS
ID GREY RELATIONAL ANALYSIS
AB In recent years, the application of aluminum metal matrix composites is
expanding to various fields like aerospace, automobile and other industrial
machineries. This paper presents the machinability of ground-granulated blast
furnace slag (GGBS)-reinforced aluminum 6061 metal matrix composites using
electrochemical micromachining for material removal rate (MRR) and radial overcut
(ROC). Input voltage, duty cycle, electrolyte concentration and % of composition
are selected as the input process parameters. Experiments have been investigated
using the L-18 mixed-level orthogonal array, and process parameters are optimized
using Taguchi technique. The model equation for MRR and ROC is developed using
regression analysis. Analysis of variance is performed, and the most significant
factor is found to be percentage (%) composition of GGBS. Additionally, the multi-
criteria decision-making technique has been used to find optimal machining
parameters for higher MRR and lower ROC. The optimal combination for higher MRR and
lower ROC is 10 V, 50%, 35 g/l and 12% of GGBS composition. The confirmation test
has been carried out to validate the results, and the obtained optimal parameter
levels are very close to an ideal solution.
C1 [Maniraj, S.] Paavai Engn Coll Autonomous, Mech Engn, Pachal 637018, India.
[Thanigaivelan, R.] Muthayammal Engn Coll Autonomous, Mech Engn, Rasipuram
637408, India.
C3 Muthayammal Engineering College
RP Maniraj, S (corresponding author), Paavai Engn Coll Autonomous, Mech Engn,
Pachal 637018, India.
EM maniraj4016@gmail.com
RI R, Thanigaivelan/AAB-9435-2022; SEKAR, MANIRAJ/IYJ-7139-2023
OI S, Maniraj/0000-0003-0911-6651; Rajasekaran,
Thanigaivelan/0000-0001-9514-9120
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NR 16
TC 25
Z9 25
U1 0
U2 8
PU SPRINGER INDIA
PI NEW DELHI
PA 7TH FLOOR, VIJAYA BUILDING, 17, BARAKHAMBA ROAD, NEW DELHI, 110 001,
INDIA
SN 0972-2815
EI 0975-1645
J9 T INDIAN I METALS
JI Trans. Indian Inst. Met.
PD DEC
PY 2019
VL 72
IS 12
BP 3057
EP 3066
DI 10.1007/s12666-019-01772-3
PG 10
GA JP5CS
UT WOS:000498283200008
DA 2023-12-05
ER
PT J
AU Wang, P
Sun, J
Guo, YF
Zhao, CW
Li, WL
Wang, GD
Lei, S
Lu, P
AF Wang, Peng
Sun, Jian
Guo, Yafei
Zhao, Chuanwen
Li, Weiling
Wang, Guodong
Lei, Su
Lu, Ping
TI Structurally improved, urea-templated, K2CO3-based
sorbent pellets for CO2 capture
LA English
DT Article
DE Pelletization; K2CO3-based sorbents; CO2 capture;
Extrusion-spheronization; Pore-forming
ID CAO-BASED PELLETS; POTASSIUM-BASED SORBENT; CARBIDE SLAG PELLETS;
FLUE-GAS; PERFORMANCE; BEHAVIOR; K2CO3/AL2O3; CARBONATION; BED;
ENHANCEMENT
AB The development of K2CO3-based sorbents with desirable CO2 capture capacity and
mechanical property is highly necessary for its large-scale application. In this
work, a range of extruded-spheronized K2CO3-based pellets containing different
K2CO3 loading (30-70 wt%) and Al2O3-based supports (i.e., activated alumina, Bayer
aluminum hydroxide, kaolinite clay and calcium aluminate cement) were prepared for
CO2 capture. It is found that the distinct textural properties of different
supports result in the obvious diversities in CO2 uptake and mechanical property of
K2CO3-based pellets. The activated alumina-supported sorbent pellets loaded with 50
wt % of K2CO3 possess the highest CO2 adsorption capacity of 2.29 mmol/g. It is
mainly attributed to the moderate amounts of active component contributing to good
textural properties and abundant CO2-philic sites, whereas excessive K2CO3 loading
will cause the destruction of porous structure, consequently the inferior CO2
uptake. Moreover, the addition of 15 wt% of urea can furher enhace CO2 uptake of
the activated alumina-supported sorbent pellets loaded with 50 wt% of K2CO3,
similar to 3.10 mmol CO2/g. The improved CO2 uptake is due to the significantly
enhanced porosity of sorbent pellets as a result of urea decomposition. In
addition, the urea-templated sorbent pellets still maintain the high compressive
strength (18.96 MPa) and good attrition resistance (a weight loss of 0.59% after
4000 rotations).
C1 [Wang, Peng; Sun, Jian; Guo, Yafei; Zhao, Chuanwen; Li, Weiling; Wang, Guodong;
Lei, Su; Lu, Ping] Nanjing Normal Univ, Sch Energy & Mech Engn, Engn Lab Energy
Syst Proc Convers & Emiss Control, Nanjing 210042, Jiangsu, Peoples R China.
C3 Nanjing Normal University
RP Zhao, CW (corresponding author), Nanjing Normal Univ, Sch Energy & Mech Engn,
Engn Lab Energy Syst Proc Convers & Emiss Control, Nanjing 210042, Jiangsu, Peoples
R China.
EM cwzhao@njnu.edu.cn
OI wang, peng/0009-0005-1949-2054; Sun, Jian/0000-0003-4514-4916
FU National Science Foundation of China [51806108, 51806109, 51706108];
Natural Science Foundation of Jiangsu Higher Education Institutions of
China [18KJB470018, 18KJB470019]
FX The authors wish to acknowledge the National Science Foundation of China
(51806108, 51806109 and 51706108) and the Natural Science Foundation of
Jiangsu Higher Education Institutions of China (18KJB470018 and
18KJB470019) for financial support.
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Sun J, 2018, FUEL, V222, P334, DOI 10.1016/j.fuel.2018.02.162
Sun J, 2017, P COMBUST INST, V36, P3977, DOI 10.1016/j.proci.2016.09.001
Wang P, 2017, APPL ENERG, V201, P34, DOI 10.1016/j.apenergy.2017.05.096
Wu Y, 2015, CHEM ENG J, V262, P1192, DOI 10.1016/j.cej.2014.10.027
Xu YQ, 2018, CHEM ENG J, V334, P2520, DOI 10.1016/j.cej.2017.11.160
Yang XW, 2016, CHEMSUSCHEM, V9, P1607, DOI 10.1002/cssc.201501699
Yang YD, 2018, CHEM ENG J, V353, P92, DOI 10.1016/j.cej.2018.07.044
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Zhao CW, 2012, ENERG FUEL, V26, P1395, DOI 10.1021/ef200324u
Zhao CW, 2010, ENERG FUEL, V24, P1009, DOI 10.1021/ef901018f
NR 50
TC 25
Z9 27
U1 10
U2 134
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD OCT 15
PY 2019
VL 374
BP 20
EP 28
DI 10.1016/j.cej.2019.05.091
PG 9
SC Engineering
GA IM0CP
UT WOS:000477652900003
DA 2023-12-05
ER
PT J
AU Liu, WZ
Yin, S
Luo, DM
Zhang, GQ
Yue, HR
Liang, B
Wang, LM
Li, C
AF Liu, Weizao
Yin, Shu
Luo, Dongmei
Zhang, Guoquan
Yue, Hairong
Liang, Bin
Wang, Liming
Li, Chun
TI Optimising the recovery of high-value-added ammonium alum during mineral
carbonation of blast furnace slag
LA English
DT Article
DE Blast furnace slag; Ammonium sulfate; Mineralisation; Ammonium alum;
Solubility
ID CO2; SYSTEM
AB A route for the indirect mineral carbonation of blast furnace slag (BFS) with
(NH4)(2)SO4 as a recyclable reagent has been proposed recently. To improve the
economy of the process, an improved recovery route was put forward herein, guided
by thermodynamic studies and phase diagrams. A purer, and thus higher-value-added
byproduct, ammonium alum, can be obtained during the mineral carbonation of BFS.
The effects of parameters such as roasting temperature and time, mass ratio of
liquid to solid during leaching, and crystallisation temperature were investigated
systematically. The results showed that the extraction reaction of BFS with
ammonium sulfate occurred not only in the roasting stage but also in the leaching
stage. The purity and recovery of aluminium as NH4Al(SO4)(2)center dot 12H(2)O can
reach 99.6% and 73%, respectively, at the optimal conditions. A preliminary
economic evaluation predicted that this route can achieve 2.5 times the profit of
the original process. (C) 2018 Elsevier B.V. All rights reserved.
C1 [Liu, Weizao; Yin, Shu; Luo, Dongmei; Zhang, Guoquan; Yue, Hairong; Liang, Bin;
Li, Chun] Sichuan Univ, Sch Chem Engn, Chengdu 610065, Sichuan, Peoples R China.
[Wang, Liming] Sichuan Univ, Hitech Grp Co Ltd, Chengdu 610065, Sichuan, Peoples
R China.
C3 Sichuan University; Sichuan University
RP Li, C (corresponding author), Sichuan Univ, Sch Chem Engn, Chengdu 610065,
EM lic@scu.edu.cn
RI Liu, Weizao/K-5038-2019; Liang, Bin/JHU-0581-2023; Wang,
Liming/N-9512-2015; yue, Hairong/D-1874-2013
OI Liu, Weizao/0000-0003-0976-2864; Wang, Liming/0000-0002-9470-2112;
[2016YFB0600904]; Science and Technology Support Project of Sichuan
Province [2016KJT0079]; Fundamental Research Funds for the Central
FX The authors are grateful for financial support from the National Key
(2016YFB0600904), the Science and Technology Support Project of Sichuan
Province (2016KJT0079), and the Fundamental Research Funds for the
Central Universities (2012017yjsy112).
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0008
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Liu WZ, 2018, FLUID PHASE EQUILIBR, V473, P226, DOI 10.1016/j.fluid.2018.06.021
Ober JA., 2018, Miner Commod Summ, DOI DOI 10.3133/70194932
10.1016/j.conbuildmat.2015.12.153
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10.1016/j.jnoncrysol.2010.05.063
Zhao Y, 2012, CERAM INT, V38, P2495, DOI 10.1016/j.ceramint.2011.11.018
NR 19
TC 25
Z9 29
U1 3
U2 55
PI LAUSANNE
SN 0925-8388
EI 1873-4669
J9 J ALLOY COMPD
JI J. Alloy. Compd.
PD FEB 5
PY 2019
VL 774
BP 1151
EP 1159
DI 10.1016/j.jallcom.2018.09.392
PG 9
GA GZ8LS
UT WOS:000449743600131
DA 2023-12-05
ER
PT J
AU Xu, H
Dal Magro, F
Sadiki, N
Mancaux, JM
Py, X
Romagnoli, A
AF Xu, Haoxin
Dal Magro, Fabio
Sadiki, Najim
Mancaux, Jean-Marie
Py, Xavier
Romagnoli, Alessandro
TI Compatibility study between aluminium alloys and alternative recycled
ceramics for thermal energy storage applications
SO APPLIED ENERGY
LA English
CT 9th International Conference on Applied Energy (ICAE)
CY AUG 21-24, 2017
CL Cardiff, WALES
DE Latent heat thermal energy storage; Aluminium alloys; Recycled ceramics;
Compatibility; Waste heat recovery; Waste-to-energy
ID PHASE-CHANGE MATERIALS; WASTE HEAT-RECOVERY; SYSTEM; CONSUMPTION;
SELECTION; AL
AB Recycled ceramics from industrial wastes, compared with traditional high-purity
ceramics, present high market potential as refractory materials due to their low
cost production process with very low environmental impacts. However, there still
exists a research gap of how recycled ceramics behave while in contact with liquid
metal. In order to study the feasibility of using recycled ceramics as the
encapsulation material in the application of high temperature Latent Heat Thermal
Energy Storage system, this paper investigates the compatibility of recycled
ceramics with three kinds of aluminium-based alloys at high temperature, with a
comparison to the corrosion resistant behaviour of alumina. The recycled ceramics
explored include Cofalit from asbestos containing waste, blast furnace slags from
steel production, and coal fly ashes sintered ceramics from incineration plants.
The study consists of a steady state thermal treatment of ceramic samples in
contact with the three different alloys at 1000 degrees C for 100 h, and a post
instrumental characterization of ceramic samples by Environmental Scanning Electron
Microscopy, Energy Dispersive Spectrometry and X-ray diffractometer, to understand
the chemical and structural transformation of the ceramics. Results demonstrate
that Cofalit shows chemical stability with Al99% but instability with A1Si5% and
AlSi12%. Blast furnace slag presents quite good thermochemical stability towards
molten AlSi5% and AlSi12%. Coal fly ashes sintered ceramics are highly interactive
towards all three aluminium alloys. In conclusion, besides alumina, Cofalit is
recommended as alternative encapsulation material for molten A199%, while blast
furnace slag being recommended for molten AlSi5% and AlSi12%.
C1 [Xu, Haoxin; Dal Magro, Fabio; Romagnoli, Alessandro] Nanyang Technol Univ, 50
Nanyang Ave, Singapore 639798, Singapore.
[Sadiki, Najim; Mancaux, Jean-Marie; Py, Xavier] Univ Perpignan, Lab UPR 8521,
PROMES CNRS, Via Domitia, F-66100 Perpignan, France.
C3 Nanyang Technological University & National Institute of Education (NIE)
Singapore; Nanyang Technological University; Universite Perpignan Via
Domitia; Centre National de la Recherche Scientifique (CNRS); CNRS -
Institute for Engineering & Systems Sciences (INSIS)
RP Romagnoli, A (corresponding author), Nanyang Technol Univ, 50 Nanyang Ave,
EM a.romagnoli@ntu.edu.sg
RI Dal Magro, Fabio/ABD-8223-2020; Romagnoli, Alessandro/N-1975-2014
OI Dal Magro, Fabio/0000-0002-8866-5618; Romagnoli,
Alessandro/0000-0003-1271-5479
FU National Research Foundation, Prime Minister's Office, Singapore;
National Environment Agency, Ministry of the Environment and Water
Resources, Singapore [WTE CRP 1501 104]
FX This work was made possible with the research findings from the project
"Application of Phase Change Materials for Improved Energy Efficiency in
Waste to Energy Plants", which is supported by the National Research
Foundation, Prime Minister's Office, Singapore, and the National
Environment Agency, Ministry of the Environment and Water Resources,
Singapore, under the Waste-to-Energy Competitive Research Programme (WTE
CRP 1501 104).
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NR 34
TC 25
Z9 25
U1 1
U2 37
PU ELSEVIER SCI LTD
PI OXFORD
SN 0306-2619
EI 1872-9118
J9 APPL ENERG
JI Appl. Energy
PD JUN 15
PY 2018
VL 220
BP 94
EP 105
DI 10.1016/j.apenergy.2018.03.021
PG 12
GA GG7NH
UT WOS:000432884500009
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Wang, JY
Huang, XW
Cui, DL
Wang, LS
Feng, ZY
Hu, B
Long, ZQ
Zhao, N
AF Wang, Jinyu
Huang, Xiaowei
Cui, Dali
Wang, Liangshi
Feng, Zongyu
Hu, Bin
Long, Zhiqi
Zhao, Na
TI Recovery of rare earths and aluminum from FCC waste slag by acid
leaching and selective precipitation
SO JOURNAL OF RARE EARTHS
LA English
DT Article
DE Rare earth; Aluminum; Recovery; FCC catalyst; Waste slag
ID CRACKING CATALYSTS; ELEMENTS; ZEOLITES; KINETICS
AB This paper investigated the recovery of rare earth elements (REEs) and aluminum
(Al) from the waste slag discharged by FCC catalyst factory (FCC waste slag) via
acid leaching and selective precipitation. Analysis methods such as ICP-AES, XRF
and XRD were applied to obtain experiment data. The maximum leaching efficiency of
REEs and Al was achieved at pH value of 1 and with liquid to solid ratio of 4:1.
Under such conditions, 91.01%, 92.24% and 94.77% of La, Ce and Al were extracted at
20 degrees C for 2 h from the FCC waste slag, respectively. The SiO2 content in the
leaching residue was 88.3%, which can be used as an available silicon resource. The
REEs can be precipitated in the form of REEs and sodium double sulfate (NaRE(SO4)
(2)center dot xH(2)O) by adding Na2SO4 to the leaching solution, while Al remained
in the solution. Afterwards, the pH value of the filtrate was adjusted to 4.5, and
Al was precipitated as Al(OH)(3). Finally, NaRE(SO4)(2)center dot xH(2)O and Al(OH)
(3) were converted into RECl3 and Al-2(SO4)(3) solution, respectively, which were
recycled to manufacture zeolite. This process recovered REEs and Al from the FCC
waste slag and reduced the emissions of waste slag simultaneously, which has an
important economic and environment significance. (C) 2017 Chinese Society of Rare
Earths. Published by Elsevier B.V. All rights reserved.
C1 [Wang, Jinyu; Huang, Xiaowei; Cui, Dali; Wang, Liangshi; Feng, Zongyu; Hu, Bin;
Long, Zhiqi; Zhao, Na] Natl Engn Res Ctr Rare Earth Mat, Gen Res Inst Nonferrous
[Wang, Jinyu; Huang, Xiaowei; Cui, Dali; Wang, Liangshi; Feng, Zongyu; Hu, Bin;
Long, Zhiqi; Zhao, Na] Grirem Adv Mat Co Ltd, Beijing 100088, Peoples R China.
RP Huang, XW; Wang, LS (corresponding author), Natl Engn Res Ctr Rare Earth Mat,
Gen Res Inst Nonferrous Met, Beijing 100088, Peoples R China.; Huang, XW; Wang, LS
(corresponding author), Grirem Adv Mat Co Ltd, Beijing 100088, Peoples R China.
EM hxw0129@188.com; 13810047587@163.com
OI Wang, Liangshi/0000-0003-4432-0842
FU Rare-earth Adjustment Upgrade Projects of Ministry of Industry and
Information Technology of China; Beijing Nova Program [Z161100004916108]
FX Project supported by the Rare-earth Adjustment Upgrade Projects of
Nova Program (Z161100004916108).
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NR 29
TC 25
Z9 28
U1 3
U2 59
PI AMSTERDAM
SN 1002-0721
J9 J RARE EARTH
JI J. Rare Earths
PD NOV
PY 2017
VL 35
IS 11
BP 1141
EP 1148
DI 10.1016/j.jre.2017.05.011
PG 8
WC Chemistry, Applied
SC Chemistry
GA FO8NM
UT WOS:000417144000011
DA 2023-12-05
ER
PT J
AU Kong, LZ
Deng, ZY
Zhu, MY
AF Kong, Lingzhong
Deng, Zhiyin
Zhu, Miaoyong
TI Formation and Evolution of Non-metallic Inclusions in Medium Mn Steel
during Secondary Refining Process
LA English
DT Article
DE non-metallic inclusions; MgO center dot Al2O3 spinel; MnO center dot
Al2O3 spinel; medium Mn steel; secondary refining
ID FERRITIC STAINLESS-STEEL; SPINEL SOLID-SOLUTION; FORMATION MECHANISM;
MOLTEN STEEL; ALLOY-STEEL; LIQUID-IRON; THERMODYNAMICS; SLAG; ALUMINUM;
304-STAINLESS-STEEL
AB Industrial and laboratory experiments were carried out to understand the
formation and evolution mechanism of non-metallic inclusions in medium Mn steel
during secondary steelmaking process. In industrial experiments, with the
generation of dissolved Mg and Ca in liquid steel, the inclusions in liquid steel
would transform along with the route of Al2O3 inclusions + MgO-Al2O3 spinel
inclusions -> (Mn, MgO center dot Al2O3 spinel inclusions -> MgO MnO center dot
Al2O3 system calcium aluminate inclusions -> (Mn, Mg) O center dot Al2O3 spinel
with a high MnO content was found as a different type of inclusions compared with
conventional Al-killed steel grades, and finally, the MnO content in calcium
aluminate inclusions became very low. Laboratory experiments were employed to
explain the generation of (Mn, Mg)O center dot Al2O3 spinel inclusions. It is found
that the crystal structure of MgO center dot Al2O3 spinel phase would help the
formation of (Mn, Mg)O center dot Al2O3 spinel inclusions, while Al2O3 inclusions
can not react with dissolved Mn in steel to form (Mn, Mg)O center dot Al2O3 spinel
inclusions, even the Mn content was around 5 mass% in steel. Consequently, (Mn, Mg)
O center dot Al2O3 spinel inclusions formed after the formation of MgO center dot
Al2O3 spinel inclusions in industrial practice.
C1 [Kong, Lingzhong; Deng, Zhiyin; Zhu, Miaoyong] Northeastern Univ, Sch Met,
RP Deng, ZY (corresponding author), Northeastern Univ, Sch Met, Shenyang 110819,
EM dengzy@smm.neu.edu.cn
RI Deng, Zhiyin/K-8739-2017
OI Deng, Zhiyin/0000-0002-0338-5896
FU National High Technology Research and Development Program of China
[2015AA03A501]; National Natural Science Foundation of China [U1660204];
Fundamental Research Funds for the Central Universities [N162504002]
FX The authors are grateful for the support of the National High Technology
Research and Development Program of China (Grant No. 2015AA03A501), the
National Natural Science Foundation of China (Grant No. U1660204) and
the Fundamental Research Funds for the Central Universities (Grant No.
N162504002).
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NR 46
TC 25
Z9 28
U1 9
U2 28
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 9
BP 1537
EP 1545
PG 9
GA FI4DE
UT WOS:000411919100007
DA 2023-12-05
ER
PT J
AU Li, C
Gao, JT
Wang, Z
Ren, HR
Guo, ZC
AF Li, Chong
Gao, Jintao
Wang, Zhe
Ren, Hongru
Guo, Zhancheng
TI Separation of Fe-bearing and P-bearing Phase from the Steelmaking Slag
by Super Gravity
LA English
DT Article
DE steelmaking slag; super gravity; P-bearing phase; centrifugal separation
ID PEROVSKITE PHASE; CAO-TIO2-SIO2-AL2O3-MGO MELT; PHOSPHORUS; ENRICHMENT;
RECOVERY; P2O5
AB The Fe-bearing phase and P-bearing phase were successfully separated from a
steelmaking slag by the super gravity and the separated efficiency was improved
with increasing the separated time. The P-bearing phase precipitating at 1 663 K
was intercepted by the filter, while most residual melt went through the filter
into the lower crucible to form calcium iron and aluminum and solid solution of
iron, magnesium and manganese (RO phase) after centrifugal separation. Under the
condition of gravity coefficient G=600 g, T=1 663 K and t= 15 minutes, the mass
fraction of P2O5 in the P-bearing slag increased from 2.49 wt% before separation to
3.56 wt% and that of FetO in the Fe-bearing slag from 23.99 wt% to 38.67 wt%. The
recovery ratio of P2O5 and FetO accounted for 82.2% and 68.5%, respectively.
C1 [Li, Chong; Gao, Jintao; Wang, Zhe; Ren, Hongru; Guo, Zhancheng] Univ Sci &
Technol Beijing, State Key Lab Adv Met, Beijing 100083, Peoples R China.
RP Gao, JT (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
EM jintaogao@ustb.edu.cn
RI Guo, Z. C./AAS-1733-2021
FU National Natural Science Foundations of China [51234001, 51404025];
Fundamental Research Funds for the Central Universities
[FRF-TP-15-009A2]
FX This work is supported by the National Natural Science Foundations of
China (No. 51234001 and No. 51404025) and the Fundamental Research Funds
for the Central Universities (FRF-TP-15-009A2), which is acknowledged
with gratitude.
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NR 14
TC 25
Z9 26
U1 0
U2 5
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 4
BP 767
EP 769
PG 3
GA ET5JG
UT WOS:000400319400025
DA 2023-12-05
ER
PT J
AU Shi, H
Feng, KQ
Wang, HB
Chen, CH
Zhou, HL
AF Shi, Huan
Feng, Ke-qin
Wang, Hai-bo
Chen, Chang-hong
Zhou, Hong-ling
TI Influence of aluminium nitride as a foaming agent on the preparation of
foam glass-ceramics from high-titanium blast furnace slag
LA English
DT Article
DE blast furnace slag; aluminium nitride; powder sintering; foam;
glass-ceramics; crystallization
ID CRYSTALLIZATION BEHAVIOR; WASTE GLASS; TIO2; MICROSTRUCTURE; RECOVERY;
RATIO; ASH
AB To effectively reuse high-titanium blast furnace slag (TS), foam glass-ceramics
were successfully prepared by powder sintering at 1000A degrees C. TS and waste
glass were used as the main raw materials, aluminium nitride (AlN) as the foaming
agent, and borax as the fluxing agent. The influence of the amount of AlN added
(1wt%-5wt%) on the crystalline phases, microstructure, and properties of the
produced foam glass-ceramics was studied. The results showed that the main crystal
phases were perovskite, diopside, and augite. With increasing AlN content, a
transformation from diopside to augite occurred and the crystallinity of the
pyroxene phases slightly decreased. Initially, the average pore size and porosity
of the foam glass-ceramics increased and subsequently decreased; similarly, their
bulk density and compressive strength decreased and subsequently increased. The
optimal properties were obtained when the foam glass-ceramics were prepared by
adding 4wt% AlN.
C1 [Shi, Huan; Feng, Ke-qin; Wang, Hai-bo; Chen, Chang-hong; Zhou, Hong-ling]
Sichuan Univ, Sch Mfg Sci & Engn, Chengdu 610065, Peoples R China.
[Wang, Hai-bo] Panzhihua Coll, Sch Mat Engn, Panzhihua 617000, Peoples R China.
RP Feng, KQ (corresponding author), Sichuan Univ, Sch Mfg Sci & Engn, Chengdu
EM kqfeng@scu.edu.cn
FU Science and Technology Support Projects of Sichuan Province
[2014GZ0011]; Industry Promotion Projects of Panzhihua in China
[2013CY-C-2]
FX The authors gratefully acknowledge the Science and Technology Support
Projects of Sichuan Province (No. 2014GZ0011) and the Industry Promotion
Projects of Panzhihua in China (No. 2013CY-C-2) for their financial
support.
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NR 25
TC 25
Z9 29
U1 2
U2 45
PU SPRINGER
PI NEW YORK
SN 1674-4799
EI 1869-103X
PD MAY
PY 2016
VL 23
IS 5
BP 595
EP 600
DI 10.1007/s12613-016-1271-7
PG 6
Mineral Processing
GA DM3ZE
UT WOS:000376284500012
DA 2023-12-05
ER
PT J
AU Larsson, MA
D'Amato, M
Cubadda, F
Raggi, A
Öborn, I
Kleja, DB
Gustafsson, JP
AF Larsson, Maja A.
D'Amato, Marilena
Cubadda, Francesco
Raggi, Andrea
Oborn, Ingrid
Kleja, Dan Berggren
Gustafsson, Jon Petter
TI Long-term fate and transformations of vanadium in a pine forest soil
with added converter lime
SO GEODERMA
LA English
DT Article
DE Vanadium; Soil; Converter lime; Speciation; XANES spectroscopy;
HPLC-ICP-MS
ID PLASMA-MASS SPECTROMETRY; K-EDGE XANES; ENVIRONMENTAL-SAMPLES;
OXIDATION-STATE; STEEL SLAG; SPECIATION; SPECTROSCOPY; ADSORPTION;
WATER; BIOAVAILABILITY
AB A field-trial with different application rates of converter lime (0.2, 0.7 and
1.0 kg m(-2)) was set up in a pine forest stand in southern Sweden in 1984. The
lime contained 14.6 g kg(-1) vanadium. The aim with this study was to evaluate the
vanadium concentration and speciation in the soil 26 years after application.
Samples of the organic mar layer and the mineral soil were analyzed separately. The
vanadium concentration decreased with soil depth, from 680 to 8 mg kg(-1) soil.
Analysis by vanadium K-edge}CANES spectroscopy showed that vanadium(IV) was the
predominant species in the mar layer. Further, iron and/or aluminum (hydr)oxides
were important sorbents for vanadium(V) in the mineral soil. The spedation of
dissolved vanadium, as determined by HPLC-ICP-MS, was dominated by vanadium(V),
which is considered the most toxic vanadium species. However, the vanadium sorption
capacity of the soil was sufficient to reduce the total bioavailable vanadium below
phytotoxic levels. By combining two different vanadium spedation methods, this
study was able to conclude that vanadium speciation in soils is governed by soil
properties such as pH, organic matter content and the content of metal
(hydr)oxides, but not by the vanadium species added to the soil. (C) 2015 Elsevier
C1 [Larsson, Maja A.; Kleja, Dan Berggren; Gustafsson, Jon Petter] Swedish Univ Agr
Sci, Dept Soil & Environm, SE-75007 Uppsala, Sweden.
[D'Amato, Marilena; Cubadda, Francesco; Raggi, Andrea] Ist Super Sanita, Dept
Food Safety & Vet Publ Hlth, Italian Natl Hlth Inst, I-00161 Rome, Italy.
[Oborn, Ingrid] Swedish Univ Agr Sci, Dept Crop Prod Ecol, S-75007 Uppsala,
Sweden.
[Oborn, Ingrid] World Agroforestry Ctr ICRAF, Nairobi 00100, Kenya.
[Kleja, Dan Berggren] Swedish Geotech Inst, Dept Environm Engn, S-11127
Stockholm, Sweden.
[Gustafsson, Jon Petter] Royal Inst Technol, Div Land & Water Resources Engn, S-
10044 Stockholm, Sweden.
C3 Swedish University of Agricultural Sciences; Istituto Superiore di
Sanita (ISS); Swedish University of Agricultural Sciences; CGIAR; World
Agroforestry (ICRAF); Royal Institute of Technology
RP Larsson, MA (corresponding author), Swedish Univ Agr Sci, Dept Soil & Environm,
Box 7014, SE-75007 Uppsala, Sweden.
EM maja.larsson@slu.se; marilena.damato@iss.it; francesco.cubadda@iss.it;
andrea.raggi@iss.se; i.oborn@cgiar.org; dan.berggren@slu.se;
jon-petter.gustafsson@slu.se
RI Gustafsson, Jon Petter/B-1655-2010; Cubadda, Francesco/O-4291-2014;
D'AMATO, MARILENA/C-6068-2015
OI Gustafsson, Jon Petter/0000-0001-8771-7941; Cubadda,
Francesco/0000-0003-3454-7947;
FU LKAB; Merox; Ruukki; U.S. Department of Energy, Office of Science,
Office of Basic Energy Sciences [DE-AC02-76SF00515]; DOE Office of
Biological and Environmental Research; National Institutes of Health,
National Institute of General Medical Sciences [P41GM103393]
FX LKAB, Merox and Ruukki are acknowledged for financial support. Use of
the Stanford Synchrotron Radiation Lightsource, SLAC National
Accelerator Laboratory, is supported by the U.S. Department of Energy,
Office of Science, Office of Basic Energy Sciences under Contract No.
DE-AC02-76SF00515. The SSRL Structural Molecular Biology Program is
supported by the DOE Office of Biological and Environmental Research,
and by the National Institutes of Health, National Institute of General
Medical Sciences (including P41GM103393). The contents of this
publication are solely the responsibility of the authors and do not
necessarily represent the official views of NIGMS or NIH. Professor
Bengt Nihlgard and Anders Jonshagen are acknowledged for helping with
background information and soil sampling.
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NR 46
TC 25
Z9 26
U1 3
U2 61
PI AMSTERDAM
SN 0016-7061
EI 1872-6259
J9 GEODERMA
JI Geoderma
PD DEC
PY 2015
VL 259
BP 271
EP 278
DI 10.1016/j.geoderma.2015.06.012
PG 8
WC Soil Science
SC Agriculture
GA CQ8OM
UT WOS:000360867800028
OA Green Submitted, Green Published, hybrid, Green Accepted
DA 2023-12-05
ER
PT J
AU Kumar, EM
Ramamurthy, K
AF Kumar, E. Muthu
Ramamurthy, K.
TI Effect of fineness and dosage of aluminium powder on the properties of
moist-cured aerated concrete
LA English
DT Article
DE Aluminium powder; Aerated concrete; Fineness; Workability; Compressive
strength; Water absorption
ID BOTTOM ASH; WASTE; SLAG
AB The influence of fineness of aluminium powder through an evaluation of variation
in the workability of the mix, rate of aeration and fresh density with time, dry
density, compressive strength and water absorption of aerated cement paste and
mortar were studied. Flow table test clearly distinguishes variation in initial
workability of the mixes for the variations in water-cement ratio, whereas the
Marsh cone test is suitable for reflecting the reduction in workability of the mix
with time caused by aeration. The dosage of aluminium powder required to achieve a
desired density reduces with an increase in its fineness. Inconsistent with the
dosage of aluminium powder required, for a given dry density or compressive
strength of aerated cement paste or mortar, the water absorption increases with
fineness of aluminium powder. For a given fineness of aluminium powder, appropriate
dosage and water-cement ratio required has to be identified based on the desired
density and strength, or strength to density ratio. (C) 2015 Elsevier Ltd. All
rights reserved.
C1 [Kumar, E. Muthu; Ramamurthy, K.] Indian Inst Technol, Dept Civil Engn, Bldg
Technol & Construct Management Div, Madras 600036, Tamil Nadu, India.
Technology (IIT) - Madras
RP Ramamurthy, K (corresponding author), Indian Inst Technol, Dept Civil Engn, Bldg
Technol & Construct Management Div, Madras 600036, Tamil Nadu, India.
EM vivek@iitm.ac.in
RI K, Ramamurthy/D-1414-2009; Kumar, Muthu/B-5384-2011; /AAH-9013-2020
OI K, Ramamurthy/0000-0001-6177-6230; Kumar, Muthu/0000-0002-2865-5696;
/0000-0001-6177-6230
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NR 22
TC 25
Z9 28
U1 2
U2 27
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 1
PY 2015
VL 95
BP 486
EP 496
DI 10.1016/j.conbuildmat.2015.07.122
PG 11
GA CQ2GC
UT WOS:000360417000049
DA 2023-12-05
ER
PT J
AU Grace, MA
Healy, MG
Clifford, E
AF Grace, Maebh A.
Healy, Mark G.
Clifford, Eoghan
TI Use of industrial by-products and natural media to adsorb nutrients,
metals and organic carbon from drinking water
LA English
DT Article
DE Adsorption isotherms; Nutrients; Metals; Organic pollutants;
Environmental quality
ID RED MUD; AQUEOUS-SOLUTION; ACTIVATED CARBON; FLY-ASH; REMOVAL;
ADSORPTION; WASTE; EQUILIBRIUM; TECHNOLOGY; ENERGY
AB Filtration technology iswell established in the water sector but is limited by
inability to remove targeted contaminants, found in surface and groundwater, which
can be damaging to human health. This study optimises the design of filters by
examining the efficacy of seven media (fly ash, bottom ash, Bayer residue, granular
blast furnace slag (GBS), pyritic fill, granular activated carbon (GAC) and
zeolite), to adsorb nitrate, ammonium, total organic carbon (TOC), aluminium,
copper (Cu) and phosphorus. Each medium and contaminant was modelled to a Langmuir,
Freundlich or Temkin adsorption isotherm, and the impact of pH and temperature
(ranging from 10 degrees C to 29 degrees C) on their performance was quantified. As
retention time within water filters is important in contaminant removal, kinetic
studieswere carried out to observe the adsorption behaviour over a 24 h period. Fly
ash and Bayer residue had good TOC, nutrient and Cu adsorption capacity. Granular
blast furnace slag and pyritic fill, previously un-investigated inwater treatment,
showed adsorption potential for all contaminants. In general, pH or temperature
adjustment was not necessary to achieve effective adsorption. Kinetic studies
showed that at least 60% of adsorption had occurred after 8 h for all media. These
media show potential for use in a multifunctional water treatment unit for the
targeted treatment of specific contaminants. (C) 2015 Elsevier B.V. All rights
reserved.
C1 [Grace, Maebh A.; Healy, Mark G.; Clifford, Eoghan] Natl Univ Ireland Univ Coll
Galway, Coll Engn & Informat, Civil Engn, Galway, Ireland.
C3 Ollscoil na Gaillimhe-University of Galway
RP Healy, MG (corresponding author), Natl Univ Ireland Univ Coll Galway, Coll Engn
& Informat, Civil Engn, Galway, Ireland.
EM mark.healy@nuigalway.ie
RI Healy, Mark G/C-1400-2009; Clifford, Eoghan/D-1985-2010
OI Healy, Mark G/0000-0003-0869-5225; Clifford, Eoghan/0000-0001-6283-1246
FU Environmental Protection Agency (EPA) [2012-W-PhD-5]; Environmental
Protection Agency Ireland (EPA) [2012-W-PhD-5] Funding Source:
Environmental Protection Agency Ireland (EPA)
FX The authors would like to acknowledge the financial support of the
Environmental Protection Agency (EPA) (Grant no: 2012-W-PhD-5).
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NR 42
TC 25
Z9 29
U1 2
U2 70
PI AMSTERDAM
SN 0048-9697
EI 1879-1026
PD JUN 15
PY 2015
VL 518
BP 491
EP 497
DI 10.1016/j.scitotenv.2015.02.075
PG 7
GA CG4BL
UT WOS:000353225700050
PM 25777954
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Karshigina, Z
Abisheva, Z
Bochevskaya, Y
Akcil, A
Sargelova, E
AF Karshigina, Zaure
Abisheva, Zinesh
Bochevskaya, Yelena
Akcil, Ata
Sargelova, Elmira
TI Recovery of rare earth metals and precipitated silicon dioxide from
phosphorus slag
LA English
DT Article
DE Phosphorus slags; Rare earth metals; Leaching; Precipitation; Silicon
dioxide
ID WASTE
AB This article presents the results of a study conducted to investigate the
recovery of rare earth metals and precipitated silicon dioxide from phosphorus
slag. To determine the possibility and completeness of the studied processes,
thermodynamic data was obtained through the determination of the Gibbs energy and
equilibrium constant of the reactions of calcium metasilicate with different
reagents, namely sodium hydroxide and carbonate as well as nitric, hydrochloric,
and sulphuric acids. This article also presents the results of studies on the
treatment of phosphorus slags via hydrometallurgical methods using alkaline agents
(sodium hydroxide and sodium carbonate) and nitric acid. The recovery of silicon in
solution by the autoclave leaching of phosphorus slag using solutions of sodium
hydroxide and sodium carbonate resulted in recovery efficiencies of 1.1% and 16.6%,
respectively. The nitric acid treatment of phosphorus slag was studied, and the
recovery efficiencies of various elements were the following: rare earth metals,
98.3-98.6%; aluminium, 96.5-98.6%; iron, 94.9-96.5%; and calcium, 99.1-99.5%.
Nitric acid (46.5%) was selected as the phosphorus slag recovery agent. The cake
produced after the nitric acid treatment of phosphorus slag was leached using two
processes based on the use of a sodium hydroxide solution: (1) in a temperature-
controlled cell under normal conditions and (2) in an autoclave. The process of
leaching under normal conditions was determined to be the most effective process,
resulting in an efficiency of silicon recovery into solution of 97.7%. (C) 2015
C1 [Karshigina, Zaure; Abisheva, Zinesh; Bochevskaya, Yelena; Sargelova, Elmira]
Ctr Earth Sci Met & Ore Beneficiat, Alma Ata 050010, Kazakhstan.
[Akcil, Ata] Suleyman Demirel Univ, Mineral Met Recovery & Recycling MMR&R Res
Grp, Mineral Proc Div, Dept Min Engn, TR-32260 Isparta, Turkey.
C3 Institute of Metallurgy & Ore Beneficiation; Suleyman Demirel University
RP Akcil, A (corresponding author), Suleyman Demirel Univ, Mineral Met Recovery &
Recycling MMR&R Res Grp, Mineral Proc Div, Dept Min Engn, TR-32260 Isparta, Turkey.
EM ataakcil@sdu.edu.tr
RI Akcil, Ata/J-1280-2017; Karshyga, Zaure Baitaskyzy/O-5905-2017; Elmira,
Sargelova/AAW-7908-2020; Abisheva, Zinesh/O-8453-2017; Bochevskaya,
Yelena/O-4998-2017
OI Akcil, Ata/0000-0002-9991-0543; Karshyga, Zaure
Baitaskyzy/0000-0002-3025-7363; Elmira, Sargelova/0000-0002-3239-6594;
Abisheva, Zinesh/0000-0002-4506-0694; Bochevskaya,
Yelena/0000-0001-5413-6446
10.1134/S0040579513040027
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NR 30
TC 25
Z9 26
U1 5
U2 40
PI OXFORD
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD JUN
PY 2015
VL 77
BP 159
EP 166
DI 10.1016/j.mineng.2015.03.013
PG 8
GA CJ7WW
UT WOS:000355712100020
DA 2023-12-05
ER
PT J
AU Li, JY
Liu, ZD
Zhao, WZ
Masud, MM
Xu, RK
AF Li, Jiu-yu
Liu, Zhao-dong
Zhao, Wen-zhi
Masud, M. M.
Xu, Ren-kou
TI Alkaline slag is more effective than phosphogypsum in the amelioration
of subsoil acidity in an Ultisol profile
SO SOIL & TILLAGE RESEARCH
LA English
DT Article
DE Alkaline slag; Phosphogypsum; Amelioration of subsoil acidity; Soil pH;
Exchangeable acidity
ID INDUSTRIAL BY-PRODUCTS; SURFACE INCORPORATED LIME; SUBSURFACE SOIL
ACIDITY; VARIABLE-CHARGE SOILS; MINERALOGICAL IMPLICATIONS;
CHEMICAL-PROPERTIES; GYPSUM; TOXICITY; ALUMINUM; GROWTH
AB Subsoil acidity seriously inhibits the development of agriculture and forestry
in southern China. However, there are few effective methods for amelioration of
subsoil acidity. In order to develop low cost and efficient methods for
amelioration of subsoil acidity through surface application of amendments, a column
leaching experiment and an in situ field experiment were conducted to investigate
the amelioration effects of surface application of alkaline slag (AS) and
phosphogypsum (PG) on the soil properties in an Ultisol profile. AS increased soil
pH and base saturation, and decreased exchangeable acidity of the different
segments in the soil profile to different degrees. Since AS contains a high content
of soluble chloride, the quick leaching of chloride ions promoted the migration of
base cations in the amendments through the soil profile, the exchange of base
cations with exchangeable aluminum (Al) and manganese (Mn), and the leaching of
soluble Al and Mn out of the profile. Although PG could increase the soil
exchangeable calcium (Ca), PG significantly increased the soluble Al and Mn in the
Ultisol profile. Compared with PG, AS was more effective in decreasing soil acidity
and soluble Al and Mn, and increasing exchangeable Ca and magnesium (Mg) in the
Ultisol profile. Therefore, AS was superior to PG in ameliorating soil acidity in
the surface soil and subsoil of this Ultisol. (C) 2014 Elsevier B.V. All rights
reserved.
C1 [Li, Jiu-yu; Liu, Zhao-dong; Masud, M. M.; Xu, Ren-kou] Chinese Acad Sci, Inst
Soil Sci, State Key Lab Soil & Sustainable Agr, Nanjing, Jiangsu, Peoples R China.
[Zhao, Wen-zhi] Yunnan Agr Univ, Coll Resources & Environm, Kunming 650201,
Peoples R China.
C3 Chinese Academy of Sciences; Institute of Soil Science, CAS; Yunnan
Agricultural University
EM rkxu@issas.ac.cn
OI Masud, Mohammad Masuduzzaman/0000-0002-9891-6230
FU National Key Basic Research Program of China [2014CB441003]; National
Natural Science Foundation of China [41271010, 41230855]
China (2014CB441003) and the National Natural Science Foundation of
China (41271010, 41230855).
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NR 34
TC 25
Z9 32
U1 1
U2 63
PI AMSTERDAM
SN 0167-1987
EI 1879-3444
J9 SOIL TILL RES
JI Soil Tillage Res.
PD JUN
PY 2015
VL 149
BP 21
EP 32
DI 10.1016/j.still.2014.12.017
PG 12
WC Soil Science
SC Agriculture
GA CC1GA
UT WOS:000350088000003
DA 2023-12-05
ER
PT J
AU Santos, RM
Chiang, YW
Elsen, J
Van Gerven, T
AF Santos, Rafael M.
Chiang, Yi Wai
Elsen, Jan
Van Gerven, Tom
TI Distinguishing between carbonate and non-carbonate precipitates from the
carbonation of calcium-containing organic acid leachates
SO HYDROMETALLURGY
LA English
DT Article
DE Mineral carbonation; Precipitated calcium carbonate; Organic acids;
Blast furnace slag; Calcium succinate
ID AQUEOUS MINERAL CARBONATION; STEEL SLAGS; CO2; SEQUESTRATION;
VALORIZATION; DISSOLUTION
AB Two organic acids were trialed for the extraction of calcium from steelmaking
blast furnace slag for the purpose of precipitated calcium carbonate (PCC)
production: succinic and acetic acids. While the leaching performance of succinic
acid was superior, carbonation of its leachate did not result in the production of
PCC, but rather the precipitation of calcium succinate, and only after the use of
pH buffering agents (sodium hydroxide or bicarbonate). In contrast, carbonation of
the acetic acid leachate resulted in the production of PCC, also with the aid of
buffering agents. This discrepancy highlights the need for a combination of
chemical, mineralogical and morphological analytical techniques for the accurate
characterization of carbonation precipitates for future publications in this field.
Additional effects observed in this study were the low atom-efficiency of the acids
for calcium leaching, at similar to 20-30% of the stoichiometric value, the low
extraction selectivity but high carbonation selectivity between calcium and
magnesium, and the contamination of the formed PCCs with small amounts of co-
leached aluminium and silicon. Further work is warranted on the purification of
this PCC synthesis route. (C) 2014 Elsevier B.V. All rights reserved.
C1 [Santos, Rafael M.; Van Gerven, Tom] Katholieke Univ Leuven, Dept Chem Engn, B-
3001 Louvain, Belgium.
[Chiang, Yi Wai] Katholieke Univ Leuven, Dept Microbial & Mol Syst, B-3001
Louvain, Belgium.
[Chiang, Yi Wai] Univ Guelph, Sch Engn, Guelph, ON N1G 2W1, Canada.
[Elsen, Jan] Katholieke Univ Leuven, Dept Earth & Environm Sci, B-3001 Louvain,
Belgium.
C3 KU Leuven; KU Leuven; University of Guelph; KU Leuven
RP Santos, RM (corresponding author), Katholieke Univ Leuven, Dept Chem Engn,
Willem Croylaan 46, B-3001 Louvain, Belgium.
EM rafael.santos@alumni.utoronto.ca
RI Van Gerven, Tom/B-5806-2015; elsen, jan/AAE-2352-2021; Chiang, Yi
Wai/K-5452-2012; Santos, Rafael M./G-1657-2011; elsen, jan/AAB-9873-2021
OI Van Gerven, Tom/0000-0003-2051-5696; Santos, Rafael
M./0000-0002-8368-8618; Chiang, Yi Wai/0000-0002-7798-9166; elsen,
jan/0000-0002-4370-3852
FU KU Leuven Industrial Research Fund (IOF); Natural Sciences and
Engineering Research Council of Canada (NSERC) [PGSD3-388899-2010]
FX This work was supported by the KU Leuven Industrial Research Fund (IOF),
through the Knowledge Platform on Sustainable Materialization of
Residues from Thermal Processes into Products (SMaRT-Pro2 -
www.smartpro2.eu). Rafael Santos is grateful for PGS-D
financial support from the Natural Sciences and Engineering Research
Council of Canada (NSERC) (PGSD3-388899-2010). The KU Leuven Department
of Metallurgy and Materials Engineering is acknowledged for the use of
XRF and SEM equipment. Koen de Crom is thanked for identifying the
discrepancies in literature reported values of the add dissociation
constant of carbonic add.
CR [Anonymous], 2004, ANAL CHEM
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NR 19
TC 25
Z9 25
U1 1
U2 23
PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD AUG
PY 2014
VL 147
BP 90
EP 94
DI 10.1016/j.hydromet.2014.05.001
PG 5
GA AN1HK
UT WOS:000340333100013
OA Green Published
DA 2023-12-05
ER
PT J
AU Wang, RC
Zhai, YC
Ning, ZQ
Ma, PH
AF Wang, Ruo-chao
Zhai, Yu-chun
Ning, Zhi-qiang
Ma, Pei-hua
TI Kinetics of SiO2 leaching from Al2O3
extracted slag of fly ash with sodium hydroxide solution
LA English
DT Article
DE fly ash; leaching; kinetics; SiO2
ID COAL; ALUMINUM
AB Kinetics of SiO2 leaching from Al2O3 extracted slag of fly ash with sodium
hydroxide solution was studied. The effect of leaching temperature, mass ratio of
NaOH to SiO2 and stirring speed on SiO2 leaching rate was investigated. The results
show that increasing leaching temperature, mass ratio of NaOH to SiO2 and stirring
speed increases SiO2 leaching rate. The SiO2 leaching rate is 95.66% under the
optimized conditions. There are two stages for the SiO2 leaching process, and the
leaching reaction is very rapid in the first stage but quite slow in the second
stage. The whole leaching process follows the shrinking core model, and the outer
diffusion of no product layer is the rate-controlling step. The activation energies
of the first and second stages are calculated to be 8.492 kJ/mol and 8.668 kJ/mol,
respectively. The kinetic equations of the first and the second stages were
obtained, respectively.
C1 [Wang, Ruo-chao; Zhai, Yu-chun; Ning, Zhi-qiang; Ma, Pei-hua] Northeastern Univ,
Sch Met & Mat, Shenyang 110819, Peoples R China.
RP Zhai, YC (corresponding author), Northeastern Univ, Sch Met & Mat, Shenyang
EM 370347814@163.com
RI Ma, Peihua/ABD-5627-2021
OI Ma, Peihua/0000-0002-5041-0361
FU National Basic Research Program of China [2007CB613603]; Postdoctoral
Science Foundation of China [2013M530934]
FX Project (2007CB613603) supported by the National Basic Research Program
of China; Project (2013M530934) supported by the Postdoctoral Science
Foundation of China
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[Anonymous], 2004, INTRO KINETICS METAL
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NR 18
TC 25
Z9 32
U1 3
U2 47
PI AMSTERDAM
SN 1003-6326
EI 2210-3384
PD JUN
PY 2014
VL 24
IS 6
BP 1928
EP 1936
DI 10.1016/S1003-6326(14)63273-8
PG 9
GA AL6XZ
UT WOS:000339278400039
DA 2023-12-05
ER
PT J
AU Roy, D
Pistorius, PC
Fruehan, RJ
AF Roy, Debdutta
Fruehan, Richard J.
TI Effect of Silicon on the Desulfurization of Al-Killed Steels: Part II.
Experimental Results and Plant Trials
LA English
DT Article
ID SLAGS
AB Recent observations suggest that increased silicon levels improve ladle
desulfurization of aluminum-killed steel. A kinetic model was developed and
presented in part I of this paper, demonstrating that increased silicon levels in
steel suppress the consumption of aluminum by parasitic reactions like silica
reduction and FeO/MnO reduction, thus making more aluminum available at the
interface for desulfurization. The results are increases in the rate and the extent
of desulfurization. Predictions were compared with laboratory induction furnace
melts using 1 kg of steel and 0.1 kg slag. The experimental results demonstrate the
beneficial effect of silicon on the desulfurization reaction and that alumina can
be reduced out of the slag and aluminum picked up by the steel, if the silicon
content in the steel is high enough. The experimental results are in close
agreement with the model predictions. Plant trials also show that with increased
silicon content, both the rate and extent of desulfurization increase;
incorporating silicon early into the ladle desulfurization process leads to
considerable savings in aluminum consumption. (C) The Minerals, Metals & Materials
Society and ASM International 2013
C1 [Roy, Debdutta; Pistorius, Petrus Christiaan; Fruehan, Richard J.] Carnegie
Mellon Univ, Dept Mat Sci & Engn, Ctr Iron & Steelmaking Res, Pittsburgh, PA 15213
USA.
Ctr Iron & Steelmaking Res, 5000 Forbes Ave, Pittsburgh, PA 15213 USA.
RI Pistorius, Petrus Christiaan/A-8247-2011
OI Pistorius, Petrus Christiaan/0000-0002-2966-1879
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NR 7
TC 25
Z9 28
U1 2
U2 22
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD OCT
PY 2013
VL 44
IS 5
BP 1095
EP 1104
DI 10.1007/s11663-013-9888-7
PG 10
Engineering
GA 231QI
UT WOS:000325431900008
OA Bronze
DA 2023-12-05
ER
PT C
AU Bruno, MJ
AF Bruno, MJ
BE Crepeau, PN
TI Aluminum carbothermic technology comparison to Hall-Heroult process
SO LIGHT METALS 2003
SE LIGHT METALS
LA English
CT Light Metals Symposium held at the 132nd TMS Annual Meeting
CY MAR 02-06, 2003
CL SAN DIEGO, CA
AB Production of aluminum by carbothermic reduction has been investigated by every
major aluminum company over the past forty seven years. As an alternative to the
Hall-Heroult Process, carbothermic offers potential energy, cost and environmental
advantages if solutions to critical technical hurdles identified by previous
research could be developed. These include efficient delivery of energy to attain
2000-2200degreesC, while minimizing loss of volatile aluminum-containing species;
capture and recycle of those volatiles that do evolve to recover mass and energy
values; effective decarbonization of the Al-C metal phase; and recovery of energy
values in the by-product CO to reduce net energy consumption.
To address these hurdles, Alcoa and Elkem, with support from DOE, initiated
joint development of a new Advanced Reactor Process. The incentives for renewed
interest in researching carbothermic were Alcoa's understanding of the Al-O-C
system and Elkem's expertise in high intensity slag resistance smelting technology.
If successful, the Advanced Reactor Process will provide significant benefits
including reductions in electrical energy up to 38%, in capital costs up to 60% or
more, and in CO2 emissions from the combined power generation-smelter complex up to
37% for a fossil fuel power plant.
C1 Alcoa Inc, Alcoa Tech Ctr, Alcoa Ctr, PA 15069 USA.
C3 Alcoa
RP Bruno, MJ (corresponding author), Alcoa Inc, Alcoa Tech Ctr, 100 Tech Dr, Alcoa
Ctr, PA 15069 USA.
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NR 15
TC 25
Z9 27
U1 0
U2 4
PU MINERALS, METALS & MATERIALS SOC
PI WARRENDALE
PA 184 THORN HILL RD, WARRENDALE, PA 15086-7514 USA
SN 0147-0809
BN 0-87339-531-X
J9 LIGHT MET
PY 2003
BP 395
EP 400
PG 6
Engineering
GA BW64R
UT WOS:000182684700058
DA 2023-12-05
ER
PT J
AU Yu, Y
Ruan, YZ
Huang, QM
Zhou, M
Du, YH
Wu, RP
AF Yu, Y
Ruan, YZ
Huang, QM
Zhou, M
Du, YH
Wu, RP
TI Polycrystalline structure of waste slag in aluminum factory at different
calcining temperature
SO CHINESE JOURNAL OF STRUCTURAL CHEMISTRY
LA Chinese
DT Article
DE waste slag of aluminum factory; gamma-AlOOH; gamma-Al2O3; gamma-Al2O3;
polycrystalline structure
AB The waste slag of aluminum factory composed of crystalline gamma-AlOOH and
amorphous solid was calcined at 450, 600, 800, 1000, 1100, 1200 and 1300 degreesC,
respectively, and the changes of crystalline phase at different temperature can
provide us suitable data for its comprehensive applications. Their polycrystalline
structures and microstructures were characterized by XRD and SEM techniques. The
crystalline phases of the waste slag were changed as the increasing of calcining
temperature:
[GRAPHICS]
It is different from our process. Both gamma-Al2O3 and amorphous solid were
formed in the samples at 600, 800 and 1000 degreesC. The contents of gamma-Al2O3
and amorphous solid decrease with the rise of calcining temperature, and they are
completely transformed into alpha-Al2O3 when the temperature increased up to 1200
degreesC. gamma-Al2O3 was metastable phase with high-activity while alpha-Al2O3 was
stable phase with low-activity.
C1 Fuzhou Univ, Mat Sci & Technol Coll, Fuzhou 350002, Peoples R China.
C3 Fuzhou University
RP Yu, Y (corresponding author), Fuzhou Univ, Mat Sci & Technol Coll, Fuzhou
RI Huang, Qingming/F-2579-2011
OI Huang, Qingming/0000-0002-9247-2763
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NR 3
TC 25
Z9 52
U1 0
U2 6
PU CHINESE JOURNAL STRUCTURAL CHEMISTRY
PI FUJIAN
PA FUIJAN INST RES STRUCT MATTER, CHINESE ACAD SCIENCES, FUZHOU, FUJIAN,
PRC
SN 0254-5861
J9 CHINESE J STRUC CHEM
JI Chin. J. Struct. Chem.
PY 2003
VL 22
IS 5
BP 607
EP 612
PG 6
WC Chemistry, Inorganic & Nuclear; Crystallography
SC Chemistry; Crystallography
GA 730PW
UT WOS:000185840000023
DA 2023-12-05
ER
PT J
AU Cai, Q
Ma, B
Jiang, J
Wang, JQ
Shao, ZY
Hu, YY
Qian, BB
Wang, LM
AF Cai, Qiang
Ma, Bing
Jiang, Jun
Wang, Jiaqing
Shao, Zhiyuan
Hu, Yueyang
Qian, Binbin
Wang, Luming
TI Utilization of waste red gypsum in autoclaved aerated concrete
preparation
LA English
DT Article
DE Red gypsum; Autoclaved aerated concrete; Gas foaming; Mechanical
characteristics
ID CO2 SEQUESTRATION; CARBONATION; MICROSTRUCTURE; TAILINGS; ALUMINUM; SLAG
AB In this study, the utilization feasibility of red gypsum (RG) as a substitute
for fly ash to prepare the autoclaved aerated concrete (AAC) was examined.
Influences of RG replacement ratio on the gas foaming, mineral components,
morphology and mechanical properties were investigated. In addition, analyses of
microstructure evolutions, phase compositions and thermal changes were carried out
to explore the mechanism of strength improvement for AAC blocks. Results show that
the replacement of fly ash by RG reduced the gas-foaming rate, which was resolved
by Na2CO3 addition and it's optimum dosage is 0.75%. The main phases in AAC are C-
S-H gel, katoite, tobermorite and anhydrite. A proper amount of RG replacement (5%-
20%) promoted the increase of relative strength of AAC samples. The synergistic
enhancement of the anhydrite system and tobermorite system ensured an increase in
relative strength. The optimum RG replacement ratio in AAC is 20%. With this
substitution ratio, density can be obtained around 617 kg/m(3) and compressive
strength can reach about 4.2 MPa, which satisfies the requirements of B06, A3.5
grade in Chinese national standard GB 11968-2019. (C) 2021 Elsevier Ltd. All rights
reserved.
C1 [Cai, Qiang; Jiang, Jun; Shao, Zhiyuan; Hu, Yueyang; Wang, Luming] Yancheng Inst
Technol, Coll Mat Sci & Engn, Yancheng 224000, Peoples R China.
[Ma, Bing] Minist Ecol & Environm Peoples Republ China, Nanjing Inst Environm
Sci, Nanjing 210042, Peoples R China.
[Wang, Jiaqing] Nanjing Forestry Univ, Coll Civil Engn, Nanjing 210037, Peoples
R China.
[Qian, Binbin] Monash Univ, Dept Chem Engn, Wellington Rd, Clayton, Vic 3800,
Australia.
[Wang, Luming] Yancheng Inst Technol, Jiangsu Proving Straw Ecol Bldg Mat Engn
Ctr, Yancheng 224000, Peoples R China.
C3 Yancheng Institute of Technology; Nanjing Forestry University; Monash
University; Yancheng Institute of Technology
RP Qian, BB (corresponding author), Monash Univ, Dept Chem Engn, Wellington Rd,
Clayton, Vic 3800, Australia.; Hu, YY; Wang, LM (corresponding author), Yancheng
Inst Technol, Coll Mat Sci & Engn, 211 Jianjun Rd, Tinghu Dist, Yancheng, Peoples R
China.
EM huyueyang1989@163.com; binbin.qian@monash.edu; wlm@ycit.cn
RI Wang, Jiaqing/AAW-2541-2020
OI Wang, Jiaqing/0000-0002-0477-3516
National Natural Science Foundation of China [51672237]; Jiangsu
Agricultural Science and Technology Innovation Fund [CX(19)2041];
Jiangsu Provincial Key Research and Development Project [BE2020630];
China Scholarship Council (CSC) [201708610139]; basic business of the
central public welfare research institute of China [GYZX180102,
GYZX170304]
Research and Development Program of China (2019YFC1907103), the National
Natural Science Foundation of China (51672237), the Jiangsu Agricultural
Science and Technology Innovation Fund (CX(19)2041) and the Jiangsu
Provincial Key Research and Development Project (No. BE2020630). Dr.
Binbin Qian acknowledges the China Scholarship Council (CSC NO.
201708610139) for financial support. The basic business of the central
public welfare research institute of China (No. GYZX180102, GYZX170304)
is also acknowledged.
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NR 35
TC 24
Z9 25
U1 4
U2 40
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUL 12
PY 2021
VL 291
AR 123376
DI 10.1016/j.conbuildmat.2021.123376
EA APR 2021
PG 11
GA SQ3WV
UT WOS:000660287600010
DA 2023-12-05
ER
PT J
AU Yang, SZ
Yao, XL
Li, JW
Wang, XJ
Zhang, C
Wu, S
Wang, K
Wang, WL
AF Yang, Shizhao
Yao, Xingliang
Li, Jingwei
Wang, Xujiang
Zhang, Chao
Wu, Shuang
Wang, Kun
Wang, Wenlong
TI Preparation and properties of ready-to-use low-density foamed concrete
derived from industrial solid wastes
LA English
DT Article
DE Low-density foamed concrete; Industrial solid wastes; Sulfoaluminate
high-activity material; Mechanical properties; Air-void structure
ID CEMENTITIOUS MATERIALS; MECHANICAL-PROPERTIES; STRENGTH; WATER
AB Foamed concrete is widely used as a highly energy-efficient building material.
However, low-density foamed concrete requires increased amounts of Portland cement
or steam curing to meet engineering requirements. This is due to inadequate
compressive strength and long setting time of Portland cement. In this study, we
investigate a method for preparing green, high strength, low-density foamed
concrete, which is ready to use without the application of heat or pressure. First,
a sulfoaluminate high-activity material (SHAM) was prepared using red mud, aluminum
dust, flue gas desulfurization-gypsum, and carbide slag. The SHAM was used to
produce ready-to-use low-density foamed concrete (RLFC). RLFC with a dry density of
615 kg/m(3) had a compressive strength of 4.11 MPa and a thermal conductivity of
0.1638 W/m.K. Addition of 0.2 wt% hydroxypropyl methylcellulose (HPMC) as foam
stabilizer, increased the compressive strength by 27.22% to 5.22 MPa, which was
3.48 times the compressive strength specified by the relevant Chinese standard (1.5
MPa). To further enhance the practicality, other solid wastes (limestone tailings
and gold tailings) were blended with SHAM to prepare the RLFC. RLFC prepared from
SHAM, limestone tailings, gold tailings, and HPMC in the match ratio of
54:6:40:0.11 (wt%) delivered dry density, compressive strength and thermal
conductivity values of 612 kg/m(3), 2.37 MPa and 0.1556 W/m.K, respectively. This
study provides a low-cost and highly promising method for preparing low-density
foamed concrete, which not only consumes a large amount of industrial solid waste
but also avoids depletion of resources and generates profits. (C) 2021 Elsevier
C1 [Yang, Shizhao; Yao, Xingliang; Li, Jingwei; Wang, Xujiang; Zhang, Chao; Wu,
Shuang; Wang, Kun; Wang, Wenlong] Shandong Univ, Engn Res Ctr Environm Thermal
Technol, Sch Energy & Power Engn,Minist Educ, Natl Engn Lab Reducing Emiss Coal
Combust,Shandon, Jinan 250061, Shandong, Peoples R China.
RP Wang, WL (corresponding author), Shandong Univ, Engn Res Ctr Environm Thermal
Technol, Sch Energy & Power Engn,Minist Educ, Natl Engn Lab Reducing Emiss Coal
Combust,Shandon, Jinan 250061, Shandong, Peoples R China.
EM wwenlong@sdu.edu.cn
RI wang, wenlong/L-2239-2013; YI, J/JJE-7713-2023; Yao,
Xingliang/AAG-2215-2021
OI Yao, Xingliang/0000-0001-5355-905X; Wu, Shuang/0000-0001-9125-8741
FU Shandong Provincial Major Scientific and Technological Innovation
Project [2019JZZY020306, 2020CXGC011403]
FX The authors acknowledge the support of Shandong Provincial Major
Scientific and Technological Innovation Project (No. 2019JZZY020306 and
No.2020CXGC011403).
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TC 24
Z9 26
U1 14
U2 95
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUN 14
PY 2021
VL 287
AR 122946
DI 10.1016/j.conbuildmat.2021.122946
EA MAR 2021
PG 12
GA RX9VC
UT WOS:000647563200007
DA 2023-12-05
ER
PT J
AU He, PP
Zhang, BY
Lu, JX
Poon, CS
AF He, Pingping
Zhang, Binyu
Lu, Jian-Xin
Poon, Chi Sun
TI ASR expansion of alkali-activated cement glass aggregate mortars
LA English
DT Article
DE Waste glass; Alkali activated cement; Calcium aluminate cement;
Alkali-aggregate reaction; Pore solution
ID CALCIUM ALUMINATE CEMENT; SILICA REACTION; WASTE-GLASS; SLAG MORTARS;
AL-27 NMR; FLY-ASH; DISSOLUTION; STRENGTH; POWDER; STABILITY
AB Previous studies showed using calcium aluminate cement (CAC) can effectively
mitigate the alkali-silica reaction (ASR) expansion of alkali-activated cement
(AAC) mortars incorporating glass cullet (GC) as fine aggregates but the mechanism
was not clear. This study presents a systematic study on exploring the underlying
mechanism to fill in the knowledge gap and to ascertain the safe use of GC in AAC
to maximize the possibility of recycling of waste glass in construction materials.
The results showed that the ASR expansion of alkali-activated glass mortars was
more than 1000 mu epsilon after 1 day of alkaline immersion when using glass cullet
as fine aggregates. The incorporation of CAC could decrease the expansion to less
than 1000 mu epsilon even after 14 days of alkaline immersion. The ASR expansion
decreased with the increase of CAC content up to 20%. That was due to several
reasons. Firstly, aluminum (Al) in CAC was incorporated in the AAC matrix with
tetrahedral and octahedral units. The tetrahedral unit increased with the increase
of CAC content, which required more Na ions to balance the excessive charge.
Therefore, the alkalinity of the pore solution decreased and the ASR expansion
decreased consequently. Besides, more AAC gel was formed due to the CAC
incorporation, which decreased the alkalinity of the pore solution as well. But
further increase the CAC content (25%) increased the ASR expansion, which might be
due to the formation of zeolite that decreased the strength of AAC mortars. (C)
C1 [He, Pingping; Zhang, Binyu; Lu, Jian-Xin; Poon, Chi Sun] Hong Kong Polytech
Univ, Dept Civil & Environm Engn, Kowloon, Hong Kong, Peoples R China.
Engn, Kowloon, Hong Kong, Peoples R China.
RI Poon, Chi Sun/H-4152-2015; Poon, Chi Sun/JQI-2195-2023
OI Poon, Chi Sun/0000-0003-4912-3936; He, pingping/0000-0002-9120-8864
FU Environment and Conservation Fund of the Hong Kong Government; Hong Kong
Polytechnic University; Department of Civil and Environmental
Engineering
FX The authors wish to acknowledge the financial support of the Environment
and Conservation Fund of the Hong Kong Government and The Hong Kong
Polytechnic University. Mr. Lu would like to thank the scholarship
sponsored by the Department of Civil and Environmental Engineering.
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Environmental Protection Department, MON SOL WAST HONG KO
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NR 42
TC 24
Z9 24
U1 5
U2 15
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD NOV 20
PY 2020
VL 261
AR 119925
DI 10.1016/j.conbuildmat.2020.119925
PG 11
GA OH4GR
UT WOS:000582529400029
DA 2023-12-05
ER
PT J
AU Huang, GD
Yang, K
Chen, L
Lu, ZY
Sun, YH
Zhang, XY
Feng, YQ
Ji, YS
Xu, ZS
AF Huang, Guodong
Yang, Ke
Chen, Lei
Lu, Zeyang
Sun, Yuhua
Zhang, Xingyu
Feng, Yongqi
Ji, Yongsheng
Xu, Zhishan
TI Use of pretreatment to prevent expansion and foaming in high-performance
MSWI bottom ash alkali-activated mortars
LA English
DT Article
DE Municipal solid waste incineration; Bottom ash; Compressive strength;
Alkali defoaming; Calcination-melting; Alkali-activated
ID FLY-ASH; STRENGTH DEVELOPMENT; GEOPOLYMER CONCRETE; PORTLAND-CEMENT;
BLENDED CEMENT; PORE SOLUTION; SLAG; CALCIUM; CARBONATION; METAKAOLIN
AB This study has investigated the impact of foaming and expansion of municipal
solid waste incinerator (MSWI) bottom ash (BA) during alkali reaction. Furthermore,
the activity enhancement of the BA has been investigated. Based on the
microanalytic appearance and compressive strength of the samples, the results show
that the reaction between the metallic aluminium in the BA and alkali in the
activator, which produced large quantities of hydrogen, is the primary cause for
both foaming and expansion. The residual organic matter and unburnt substances in
the BA are the main factors that affect the activity. However, the alkali defoaming
and calcination-melting pretreatments completely prevented the expansion and
calcining further improved the BA activity. The alkali activated materials prepared
with the BA calcined at 700 degrees C, granulated blast furnace slag, and slaked
lime followed by alkali defoaming pretreatment produced the best mechanical
properties. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Huang, Guodong; Yang, Ke; Lu, Zeyang; Sun, Yuhua; Zhang, Xingyu; Feng, Yongqi]
Anhui Univ Sci & Technol, Sch Civil Engn & Construct, 168 Taifeng Rd, Huainan
[Huang, Guodong; Yang, Ke; Chen, Lei] Anhui Univ Sci & Technol, Sch Energy &
Safety, 168 Taifeng Rd, Huainan 232001, Anhui, Peoples R China.
[Huang, Guodong; Ji, Yongsheng; Xu, Zhishan] China Univ Min & Technol, Sch Mech
& Civil Engn, 1 Daxue Rd, Xuzhou 221116, Jiangsu, Peoples R China.
[Huang, Guodong] JiangSu Collaborat Innovat Ctr Bldg Energy Saving, 26 Xuanyuan
Rd, Xuzhou 221116, Jiangsu, Peoples R China.
C3 Anhui University of Science & Technology; Anhui University of Science &
Technology; China University of Mining & Technology
RP Yang, K (corresponding author), Anhui Univ Sci & Technol, Sch Civil Engn &
Construct, 168 Taifeng Rd, Huainan 232001, Anhui, Peoples R China.; Yang, K
(corresponding author), Anhui Univ Sci & Technol, Sch Energy & Safety, 168 Taifeng
Rd, Huainan 232001, Anhui, Peoples R China.
EM keyang@aust.edu.cn
OI Ji, Yongsheng/0000-0002-7414-9719
FU JiangSu Collaborative Innovation Center for Building Energy Saving and
Construction Technology
FX This study was supported by the funding through JiangSu Collaborative
Innovation Center for Building Energy Saving and Construction Technology
(No.SJXTQ1615).
CR [Anonymous], 2010, GB50010-2010
10.1016/j.conbuildmat.2007.10.011
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10.1016/j.cemconcomp.2017.09.005
NR 53
TC 24
Z9 24
U1 10
U2 54
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUN 10
PY 2020
VL 245
AR 118471
DI 10.1016/j.conbuildmat.2020.118471
PG 10
GA LF4TN
UT WOS:000527412100052
DA 2023-12-05
ER
PT J
AU Lin, YH
Xu, DQ
Zhao, XH
AF Lin, Yonghui
Xu, Dongqiang
Zhao, Xianhui
TI Effect of Soda Residue Addition and Its Chemical Composition on Physical
Properties and Hydration Products of Soda Residue-Activated Slag
Cementitious Materials
SO MATERIALS
LA English
DT Article
DE alkaline activation; soda residue; ground granulated blast furnace slag;
physical properties; hydration products; microstructure
ID MECHANICAL-PROPERTIES; CHLORIDE BINDING; FLY-ASH; STRENGTH; MORTARS;
BINDERS; WASTE
AB Soda residue (SR), the solid waste of Na2CO3 produced by ammonia soda process,
pollutes water and soil, increasing environmental pressure. SR has high alkalinity,
and its main components are Ca(OH)(2), NaCl, CaCl2, CaSO4, and CaCO3, which accords
with the requirements of being an alkali activator. The aim of this research is to
investigate the best proportion of SR addition and the contribution of individual
chemical components in SR to SR- activated ground granulated blast furnace slag
(GGBS) cementitious materials. In this paper, GGBS pastes activated by SR, Ca(OH)
(2), Ca(OH)(2) + NaCl, Ca(OH)(2) + CaCl2, Ca(OH)(2) + CaSO4, and Ca(OH)(2) + CaCO3
were studied regarding setting time, compressive strength (1 d, 3 d, 7 d, 14 d, 28
d), hydration products, and microstructure. The results demonstrate that SR (24%)-
activated GGBS pastes possess acceptable setting time and compressive strength
(29.6 MPa, 28 d), and its hydration products are calcium silicate hydrate (CSH)
gel, calcium aluminum silicate hydrates (CASH) gel and Friedel's salt. CaCl2 in SR
plays a main role in hydration products generation and high compressive strength of
SR- activated GGBS pastes.
C1 [Lin, Yonghui; Xu, Dongqiang; Zhao, Xianhui] Hebei Univ Technol, Sch Civil &
Transportat Engn, Tianjin 300401, Peoples R China.
[Lin, Yonghui] Hebei Normal Univ Nationalities, Dept Econ & Management, Chengde
C3 Hebei University of Technology; Hebei Normal University for
Nationalities
RP Lin, YH (corresponding author), Hebei Univ Technol, Sch Civil & Transportat
Engn, Tianjin 300401, Peoples R China.; Lin, YH (corresponding author), Hebei
Normal Univ Nationalities, Dept Econ & Management, Chengde 067000, Peoples R China.
EM 201611601012@stu.hebut.edu.cn; 2002021@hebut.edu.cn;
201411601006@stu.hebut.edu.cn
RI lin, yonghui/GYU-9632-2022
OI Zhao, Xianhui/0000-0001-6983-5290
FU Science and Technology Project Foundation of Hebei Province, China
[16273809]
FX This research was funded by the Science and Technology Project
Foundation of Hebei Province, China, grant number 16273809.
CR [Anonymous], 1999, 176711999 GB GEN ADM
[Anonymous], 2007, 1752007 GB GEN ADM Q
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10.1016/j.cemconcomp.2019.02.009
NR 48
TC 24
Z9 24
U1 1
U2 28
PU MDPI
PI BASEL
EI 1996-1944
J9 MATERIALS
JI Materials
PD APR
PY 2020
VL 13
IS 7
AR 1789
DI 10.3390/ma13071789
PG 13
Physics
GA LJ0PF
UT WOS:000529875600307
PM 32290192
DA 2023-12-05
ER
PT J
AU Sasaki, K
Kurumisawa, K
Ibayashi, K
AF Sasaki, Kenta
Kurumisawa, Kiyofumi
Ibayashi, Kouhei
TI Effect of retarders on flow and strength development of alkali-activated
fly ash/blast furnace slag composite
LA English
DT Article
DE Geopolymer; Fly ash; Blast furnace slag; Compressive strength; Setting
time; Retarder; Chelator
ID CEMENT PASTES; WORKABILITY
AB Geopolymer concrete presents a major problem regarding its practical
application, in that the geopolymer paste has very short setting time. Previous
studies have shown that the addition of blast furnace slag to geopolymer paste
considerably shortens the setting time. Based on these findings, in the present
study, setting retarders were used to lengthen the setting time of the geopolymer
paste. The objective of the present study was to identify the effect of a setting
retarder on the fluidity and compressive strength of alkali-activated fly ash/blast
furnace slag-based materials. It was shown that, by adding a chelator as a
retarder, the setting time can be prolonged. However, the setting time was found to
be dependent on the type of chelator. Similarly, the compressive strength
development of the geopolymer was also found to be dependent on the type of
chelator. It was clarified that the concentration of calcium and aluminum in
solution during hardening changes with the addition of a chelator, and it was shown
that there is a correlation between the concentrations of calcium and aluminum and
the setting time. (C) 2019 Elsevier Ltd. All rights reserved.
C1 [Sasaki, Kenta] Hokkaido Univ, Cooperat Program Resources Engn, Grad Sch Engn,
[Kurumisawa, Kiyofumi] Hokkaido Univ, Div Sustainable Resources Engn, Fac Engn,
[Ibayashi, Kouhei] Hokkaido Univ, Course Sustainable Resources Engn, Sch Engn,
C3 Hokkaido University; Hokkaido University; Hokkaido University
RP Kurumisawa, K (corresponding author), Hokkaido Univ, Div Sustainable Resources
Engn, Fac Engn, Sapporo, Hokkaido, Japan.
EM kurumi@eng.hokudai.ac.jp
OI Kurumisawa, Kiyofumi/0000-0002-8093-1942
FU [16K06563]
FX Part of this research was supported by a Grant-in-Aid for Scientific
Research (Kakenhi) [grant number 16K06563].
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10.1016/j.cemconcomp.2006.11.002
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10.1016/j.jhazmat.2009.01.120
NR 22
TC 24
Z9 25
U1 10
U2 63
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD AUG 20
PY 2019
VL 216
BP 337
EP 346
DI 10.1016/j.conbuildmat.2019.05.022
PG 10
GA IE9LZ
UT WOS:000472697200028
OA Green Published
DA 2023-12-05
ER
PT J
AU Reddy, PN
Naqash, JA
AF Reddy, P. Narasimha
Naqash, J. Ahmed
TI Experimental Study on TGA, XRD and SEM Analysis of Concrete with
Ultra-fine Slag
SO INTERNATIONAL JOURNAL OF ENGINEERING
LA English
DT Article
DE Alccofine; Thermogravimetric Analysis; X-ray diffraction; Scanning
Electron Microscope
ID SELF-COMPACTING CONCRETE; FLY-ASH; BLENDED CEMENTS; PERMEABILITY; FIBER
AB The performances of cementitious materials as well as the efficiency of
construction are adversely affected at high temperatures. Previous studies have
already demonstrated that ultra-fine (alccofine) material accelerates the hydration
of cement particles and subsequently improves the mechanical and durability
properties of the concrete at normal temperature. Moreover, at higher temperatures
the performance of the concrete with the addition of alccofine is still unknown.
This paper presents the effect of analytical properties of concrete with alccofine
(25%) as a replacement of cement for various W/B ratios (i.e. 0.38, 0.4 and 0.45).
The effect of addition of alccofine dosage on the thermogravimetric analysis was
carried out in which not only mass loss and decomposition of hydration products
from concrete with respect to temperature was found but also bound water (%) and
calcium hydroxide (%) present in the concrete were determined. From X-ray
diffraction it was observed that alccofine improved the formation of calcium
silicate hydrate and calcium silicate aluminum hydrate in concrete and scanning
electron microscope (SEM) analysis showed the formation of ettringite needles and
calcium silicate hydrate in voids which made concrete denser. Therefore, it was
concluded from this study that alccofine can be used as a viable substitute to
cement in normal concrete considering its positive effects on property enhancement
and an eco-friendly product.
C1 [Reddy, P. Narasimha; Naqash, J. Ahmed] Natl Inst Technol, Srinagar, Jammu &
Kashmir, India.
Technology Srinagar
RP Reddy, PN (corresponding author), Natl Inst Technol, Srinagar, Jammu & Kashmir,
India.
EM narasimha_07phd16@nitsri.ac.in
RI Reddy, Dr. Panga Narasimha/G-3685-2019; Naqash, Javed
Ahmed/ABB-3455-2020
OI Reddy, Dr. Panga Narasimha/0000-0001-8856-9741;
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NR 24
TC 24
Z9 24
U1 0
U2 9
PU MATERIALS & ENERGY RESEARCH CENTER-MERC
PI TEHRAN
PA 16, AHURAMAZDA ST, ALVAND AVE, TEHRAN, 15169, IRAN
SN 1025-2495
EI 1735-9244
J9 INT J ENG-IRAN
JI Int. J. Eng.
PD MAY
PY 2019
VL 32
IS 5
BP 679
EP 684
DI 10.5829/ije.2019.32.05b.09
PG 6
WC Engineering, Multidisciplinary
WE Emerging Sources Citation Index (ESCI)
SC Engineering
GA IJ3ZE
UT WOS:000475842800009
OA Bronze
DA 2023-12-05
ER
PT J
AU Al-Ameen, Y
Ianakiev, A
Evans, R
AF Al-Ameen, Yasameen
Ianakiev, Anton
Evans, Robert
TI Recycling construction and industrial landfill waste material for
backfill in horizontal ground heat exchanger systems
SO ENERGY
LA English
CT 3rd International Conference on Smart Energy Systems and 4th Generation
District Heating (SES4DH)
CY SEP 12-13, 2017
CL Copenhagen, DENMARK
DE Energy; Horizontal ground heat exchanger; Waste materials; Temperature
distribution; Space heating
ID THERMAL PERFORMANCE EVALUATION; PUMP SYSTEM; OPERATING PARAMETERS;
TAGUCHI METHOD; CLOSED-LOOP; GREENHOUSE; BUILDINGS; DESIGN;
OPTIMIZATION; METHODOLOGY
AB This research experimentally and numerically investigates the possibility of
recycling some low cost construction and industrial waste landfills materials as
potential backfills in horizontal ground heat exchangers (HGHE). The aim of this
study was to compare the temperature distribution development in different backfill
materials with respect to time. The tested materials include sand, crushed basalt,
broken brick, crushed concrete, and metallic by-products including copper slag,
aluminium slag, mill scale and iron ores (fine and pellets). Initial thermal
testing on these materials in an environmental climatic chamber indicated concrete
and crushed brick had similar performance to sand, whereas metallic materials had
better performance by up to 77% improvement compared to sand. Various percentages
of the backfill material (20, 40, 60, 80 and 100%) blended with the remaining
percentage of sand showed that the higher the percentage addition of the waste
material, the better the heat storage of the enhanced sand. Particle size
distribution was also a significant parameter in backfill selection, where medium
sized particle sizes (1.18-2 mm) performed 92% better compared to course and fine
gradations of the same material. An experimental set-up of a HGHE system was then
constructed and filled with the best performing backfill materials to determine the
heat storage and release processes on the thermal performance of the system. The
paper also reports results from a transient three-dimensional finite volume model
developed in ANSYS Fluent 17.2 computational fluid dynamic (CFD) software of a thin
section of a HGHE. The experimental and numerical model were used to predict and
analyze the temperature distribution developing within the surrounding backfill
material with respect to charging (heating) and discharging (extracting heat) modes
of the HGHE. Results obtained from both experimental and numerical studies show the
temperature range and duration of hot water produced from the system were in line
with low temperature space heating guidelines and that mill-scale, copper slag and
aluminium slag were the best backfill materials, where the thermal capacity of the
HGHE system can be doubled using these materials, compared to the use of sand
alone. Congruence between the numerical simulations and experimental data was
found. Crown Copyright (C) 2018 Published by Elsevier Ltd. All rights reserved.
C1 [Al-Ameen, Yasameen; Ianakiev, Anton; Evans, Robert] Nottingham Trent Univ, Sch
Architecture Design & Built Environm, Nottingham, England.
C3 Nottingham Trent University
RP Al-Ameen, Y (corresponding author), Nottingham Trent Univ, Sch Architecture
Design & Built Environm, Nottingham, England.
EM yasameen.alameen@ntu.ac.uk
OI Ianakiev, Anton/0000-0002-1413-8110
FU REMOURBAN project - EU Horizon research and innovation programme
[646511]
FX The authors gratefully acknowledge the financial support from the
REMOURBAN project supported by the EU Horizon 2020 research and
innovation programme under grant agreement No 646511. The sponsor had no
involvement in the design or delivery of this paper.
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NR 59
TC 24
Z9 25
U1 2
U2 23
PI OXFORD
SN 0360-5442
EI 1873-6785
J9 ENERGY
JI Energy
PD MAY 15
PY 2018
VL 151
BP 556
EP 568
DI 10.1016/j.energy.2018.03.095
PG 13
GA GG2GU
UT WOS:000432509000048
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Masindi, V
Osman, MS
Mbhele, RN
Rikhotso, R
AF Masindi, Vhahangwele
Osman, Muhammad S.
Mbhele, Ryneth N.
Rikhotso, Rirhandzu
TI Fate of pollutants post treatment of acid mine drainage with basic
oxygen furnace slag: Validation of experimental results with a
geochemical model
LA English
DT Article
DE Acid mine drainage (AMD); Basic oxygen furnace (BOF) slag; Inorganic
contaminants; Neutralization; Geochemical modelling; Recovery of
minerals
ID INORGANIC CONTAMINANTS; FLY-ASH; NEUTRALIZATION; REMOVAL; REMEDIATION;
METALS; IRON
AB Basic Oxygen Furnace (BOF) slag has been widely used for Acid Mine Drainage
(AMD) treatment with its reaction chemistry and contaminants attenuation mechanisms
barely reported. This pioneer study was therefore designed with the aim of
evaluating the partitioning of inorganic contaminants post the interactions of acid
mine drainage and BOF slag and explore the chemistry thereof. This will aid in
situation where metal recovery and waste classifications need to be pursued. To
fulfil the goals of the study, laboratory experiments were conducted at 60 min of
shaking and 100 g: 1 L solids to liquids ratios (S/L). To validate the results,
experimental results were complemented by pH Redox Equilibrium (in C language)
(PHREEQC) geochemical model. The water chemistry and mineral phase changes during
the interaction of BOF and Acid mine drainage (AMD) were evaluated. Reaction of BOF
slag and AMD led to an increase in pH (approximate to 10) and a drastic reduction
in metal species (>= 99%) and sulphate (>= 75%). PHREEQC indicated that the removal
of chemical species from AMD was dependent on pH. Furthermore, it indicated that Fe
was mainly removed as Fe(OH)(3), goethite, and jarosite whereas Al was removed as
basa-luminite, boehmite and jurbanite, Al(OH)(3), gibbsite and diaspore. Al and Fe
precipitated as iron (oxy)-hydroxides and aluminium (oxy)-hydroxides. Mn
precipitated as rhodochrosite and manganite. Ca and sulphate were removed as
gypsum. Mg was removed as brucite and dolomite. The results from experimental runs
and geochemical modelling were in agreements hence proving that the obtained
results are valid. As such, it can be concluded that BOF slag effectively
neutralized AMD and significantly lowered the levels of inorganic contaminants to
meet prescribed standards as stipulated by the water quality guideline. Gypsum and
magnetite were also recovered from mine water treatment process using BOF slag
hence depicting that there is commercial value from the treatment process. (C) 2017
C1 [Masindi, Vhahangwele; Osman, Muhammad S.; Mbhele, Ryneth N.] CSIR, Built
Environm, Hydraul Infrastruct Engn, POB 395, ZA-0001 Pretoria, South Africa.
[Masindi, Vhahangwele] Univ South Africa UNISA, Sch Agr & Environm Sci, Dept
Environm Sci, POB 392, ZA-1710 Florida, South Africa.
[Rikhotso, Rirhandzu] CSIR, DST CSIR Natl Ctr Nanostruct Mat, POB 395, ZA-0001
Pretoria, South Africa.
C3 Council for Scientific & Industrial Research (CSIR) - South Africa;
University of South Africa; Council for Scientific & Industrial Research
(CSIR) - South Africa
RP Masindi, V (corresponding author), CSIR, Built Environm, Hydraul Infrastruct
Engn, POB 395, ZA-0001 Pretoria, South Africa.
EM VMasindi@csir.co.za
RI Masindi, Vhahangwele/ABE-3363-2020
OI Masindi, Vhahangwele/0000-0002-5440-8373
FU Council for Scientific and Industrial research (CSIR) and City of
Johannesburg
FX The authors wish to express their sincere gratitude to the Council for
Scientific and Industrial research (CSIR) and City of Johannesburg for
providing financial support to this project. Furthermore, the authors
would like to thanks Corlien Cloete from CGS for XRF analysis, Charity
Maepa for HR-SEM analysis, Tshwane University of Technology for
providing lab space to execute this research work. The authors would
also like to thank Khathutshelo Muedi for the helpful and insightful
discussions.
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NR 42
TC 24
Z9 24
U1 6
U2 41
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD JAN 20
PY 2018
VL 172
BP 2899
EP 2909
DI 10.1016/j.jclepro.2017.11.124
PG 11
& Ecology
GA FT2UT
UT WOS:000423002200141
DA 2023-12-05
ER
PT J
AU Wang, Y
Tang, HY
Wu, T
Wu, GH
Li, JS
AF Wang, Yong
Tang, Haiyan
Wu, Tuo
Wu, Guanghui
Li, Jingshe
TI Effect of Acid-Soluble Aluminum on the Evolution of Non-metallic
Inclusions in Spring Steel
LA English
DT Article
ID DEOXIDATION EQUILIBRIUM; SLAG COMPOSITION; KILLED STEEL; FATIGUE LIFE;
MOLTEN STEEL; 1873 K; AL; THERMODYNAMICS; ALLOY; IRON
AB The content of acidic soluble aluminum in molten steel ([Al](s)) is of
significance to the control of total oxygen (TO), the formation of non-metallic
inclusions, and the improvement of the surface quality of billets. Industrial
trials and thermodynamic calculations were performed to study the effects of [Al]
(s) content on the TO and the evolution of non-metallic inclusions in 60Si2Mn-Cr
spring steel that was deoxidized by Si-Mn ((low aluminum process (LAP)) and Si-Mn-
Al (high aluminum process (HAP)). The results show that the [Al](s) contents in
billets are within 0.0060 to 0.0069 mass pct in the LAP and 0.016 to 0.055 mass pct
in the HAP. The TO content at each station of the LAP is higher than that in the
HAP; the inclusions of billets were mainly of the CaO-Al2O3-SiO2 type in the
former, and of the CaO-Al2O3-MgO and CaS-Al2O3-MgO types in the latter. A tendency
is found that the higher the [Al](s), the easier it is to deviate from the low
melting point region of the inclusion distribution and the larger the size of the
inclusions. The relationships between [Al](s) and the melting point of the oxide
inclusions and the Al2O3 content in the oxide inclusions are also discussed in
terms of experiment and calculation.
C1 [Wang, Yong; Tang, Haiyan; Wu, Tuo; Wu, Guanghui; Li, Jingshe] Univ Sci &
Technol Beijing, Sch Met & Ecol Engn, Room 412,Yejin Bldg,30 Xueyuan Rd, Beijing
RP Tang, HY (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol
Engn, Room 412,Yejin Bldg,30 Xueyuan Rd, Beijing 400044, Peoples R China.
EM tanghaiyan@metall.ustb.edu.cn
OI Wang, Yong/0000-0001-7585-4674
Research Funds for the Central Universities of China [FRF-UM-15-048]
FX The authors are grateful for the help of Dr. Shufeng Yang in the
industrial sampling. Thank for the financial support from the National
Natural Science Foundation of China (No. 51374021) and the Fundamental
Research Funds for the Central Universities of China (No.
FRF-UM-15-048).
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NR 25
TC 24
Z9 24
U1 0
U2 33
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD APR
PY 2017
VL 48
IS 2
BP 943
EP 955
DI 10.1007/s11663-017-0922-z
PG 13
Engineering
GA EN5EO
UT WOS:000396028600019
DA 2023-12-05
ER
PT J
AU Xu, L
Chen, M
Yin, XL
Wang, N
Liu, L
AF Xu, Lei
Chen, Min
Yin, Xue-Liang
Wang, Nan
Liu, Lei
TI Effect of TiO2 addition on the sintering densification and
mechanical properties of
MgAl2O4-CaAl4O7-CaAl12O19 composite
LA English
DT Article
DE TiO2; Al2O3-MgO-CaO; Sintering; Morphology; Mechanical properties
ID CONTAINING REFRACTORY CASTABLES; ALUMINA/ALUMINIUM TITANATE; ALUMINA;
SPINEL; BEHAVIOR; TEMPERATURE; MICROSTRUCTURE; HIBONITE; SLAG;
RESISTANCE
AB Materials designed in the high-alumina region of Al2O3-MgO-CaO system have been
widely used in many technological fields. However, their further applications are
limited by the high sintering temperatures necessary to achieve densification due
to the poor sintering ability of calcium hexaluminate (CaAl12O19) and spinel
(MgAl2O4). Considering this aspect, the present work investigated the effect of
TiO2 addition on the sintering densification and mechanical properties of MgAl2O4-
CaAl4O7-CaAl12O19 composite by solid state reaction sintering. The results showed
that the CA(6) grains presented a more equiaxed morphology instead of platelet
structure by incorporating Ti4+ into its structure, which greatly improved the
densification after heating at 1600 degrees C. The flexural strength was greatly
enhanced with increasing addition of TiO2 due to the significant decrease in
porosity and improvement in uniformity of grain size as well as the absence of
microcracks in the presence of Al2TiO5. The increased content of TiO2 also played
an active role in toughening this composite attributed to the increase in
resistance to crack initiation and propagation. (C) 2016 Elsevier Ltd and Techna
C1 [Xu, Lei; Chen, Min; Yin, Xue-Liang; Wang, Nan; Liu, Lei] Northeastern Univ, Sch
Met, 3-11 Wen Hua Rd, Shenyang 110819, Peoples R China.
RP Chen, M (corresponding author), Northeastern Univ, Sch Met, 3-11 Wen Hua Rd,
Shenyang 110819, Peoples R China.
EM chenm@smm.neu.edu.cn
RI Wang, Nan/GRY-3150-2022; Wang, Nan/HLV-7836-2023
OI Xu, Lei/0000-0002-3598-1502; Liu, Lei/0000-0001-5972-5629
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NR 47
TC 24
Z9 24
U1 1
U2 40
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD JUN
PY 2016
VL 42
IS 8
BP 9844
EP 9850
DI 10.1016/j.ceramint.2016.03.082
PG 7
GA DK3IZ
UT WOS:000374811600069
DA 2023-12-05
ER
PT J
AU Suraneni, P
Palacios, M
Flatt, RJ
AF Suraneni, Prannoy
Palacios, Marta
Flatt, Robert J.
TI New insights into the hydration of slag in alkaline media using a
micro-reactor approach
LA English
DT Article
DE Hydration (A); SEM (B); Alkalis (D); Granulated Blast-Furnace Slag (D);
Dissolution
ID BLAST-FURNACE SLAG; A-S-H; CALCIUM HYDROXIDE; FLY ASHES; DISSOLUTION;
SUPERPLASTICIZER; ACTIVATION; CEMENT; REACTIVITY; ADMIXTURES
AB A micro-reactor approach, developed previously, is used to study the reactions
of slag in alkaline media. Micronsized gaps are milled in slag grains using a
focused ion beam (FIB) and subsequently filled with alkaline solutions, leading to
dissolution and hydration of the slag. After the hydration is stopped, a scanning
electron microscope (SEM) is used to image the gaps. We present the effect of pH
and nature of the alkaline solution on the slag dissolution and the hydrate
morphology. The results obtained in this study confirm that the presence of
aluminum and calcium in solution has a strong retarding effect on the slag
dissolution. A major implication of these results is that in blended cements, the
reactivity of slag probably suffers from the ions released by cement into solution.
We show that strongly adsorbing superplasticizers inhibit the dissolution of slag,
but only at lower alkali concentrations and C-S-H seeds may also inhibit the
dissolution of slag under certain experimental conditions. The obtained results are
compared and contrasted with results obtained for alite and tricalcium silicate
previously reported in the literature. (C) 2015 Elsevier Ltd. All rights reserved.
C1 [Suraneni, Prannoy; Palacios, Marta; Flatt, Robert J.] ETH, Dept Civil Environm
& Geomat Engn, CH-8093 Zurich, Switzerland.
C3 Swiss Federal Institutes of Technology Domain; ETH Zurich
RP Flatt, RJ (corresponding author), ETH, Dept Civil Environm & Geomat Engn, CH-
8093 Zurich, Switzerland.
EM flattr@ethz.ch
RI Flatt, Robert J/D-3295-2013; Palacios, Marta/K-3699-2016
OI Flatt, Robert J/0000-0002-5609-8487; Palacios,
Marta/0000-0001-5004-128X; Suraneni, Prannoy/0000-0002-0899-2601
FU Scientific Center for Optical and Electron Microscopy (ScopeM) at ETH
Zurich
FX The authors acknowledge the support of the Scientific Center for Optical
and Electron Microscopy (ScopeM) at ETH Zurich, and specifically of Dr.
Anne Greet Bittermann at ScopeM for aid with the electron microscopy
work reported here. Thomas Matschei from Holcim Technology Ltd. and
Prof. Donald Macphee from the University of Aberdeen are thanked for
their useful comments and criticisms of the manuscript and for
insightful discussions. Thomas Matschei is also thanked for providing
the slag. Delphine Marchon from ETH Zurich and Sika AG are thanked for
providing the superplasticizers. Lydia Zehnder from the Institute for
Geochemistry and Petrology at ETH Zurich is thanked for the XRF analysis
of the slag. Giulia Gelardi from ETH Zurich is thanked for her helpful
suggestions and for running the SEC measurements.
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NR 55
TC 24
Z9 26
U1 3
U2 41
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD JAN
PY 2016
VL 79
BP 209
EP 216
DI 10.1016/j.cemconres.2015.09.015
PG 8
GA DA0JI
UT WOS:000367483000018
DA 2023-12-05
ER
PT J
AU Wei, KX
Zheng, DM
Ma, WH
Yang, B
Dai, YNA
AF Wei, Kuixian
Zheng, Damin
Ma, Wenhui
Yang, Bin
Dai, Yongnian
TI Study on Al Removal from MG-Si by Vacuum Refining
SO SILICON
LA English
DT Article
DE Vacuum refining; Metallurgical-grade silicon; Aluminum removal
ID METALLURGICAL GRADE-SILICON; ALUMINUM; IMPURITIES; CALCIUM
AB Aluminum is one of the main impurity elements in metallurgical-grade silicon
(MG-Si). The methods of aluminum removal from MG-Si are slag refining, directional
solidification, acid leaching and vacuum evaporation refining, respectively. Based
on the theoretical calculation, the vacuum evaporation refining experiments for
aluminum removal were carried out in this paper. The effects of refining time and
temperature on the removal efficiency of aluminum were investigated. The results
show that the vacuum evaporation is an efficient refining technique for removing
impurity aluminum from MG-Si. The content of aluminum in MG-Si can be reduced from
1120 x 10(-6) to 427 x 10(-6), and its removal efficiency is 61.9 %. Meanwhile, the
removal efficiency of aluminum is improved with the increasing refining time and
temperature during vacuum evaporation.
C1 [Wei, Kuixian; Zheng, Damin; Ma, Wenhui; Yang, Bin; Dai, Yongnian] Kunming Univ
Sci & Technol, Natl Engn Lab Vacuum Met, Kunming, Peoples R China.
[Wei, Kuixian; Zheng, Damin; Ma, Wenhui; Yang, Bin; Dai, Yongnian] Key Lab
Vacuum Met Nonferrous Met Yunnan Prov, Kunming, Peoples R China.
[Wei, Kuixian; Zheng, Damin; Ma, Wenhui; Yang, Bin; Dai, Yongnian] Silicon Met &
Mat Engn Res Ctr Univ Yunnan Prov, Kunming, Peoples R China.
RP Ma, WH (corresponding author), Kunming Univ Sci & Technol, Natl Engn Lab Vacuum
Met, 253 Xuefu Rd, Kunming, Peoples R China.
EM mwhsilicon@163.com
RI ma, wenhui/GQZ-0052-2022
FU National Key Technology RD Program [2011BAE03B01]; National Natural
Science Foundation of China [U1137601]; Natural Science Foundation of
Yunnan of China [KKSY201252078]; Program for Innovative Research Team in
University of Ministry of Education of China [IRT1250]
FX This work was supported by the National Key Technology R&D Program
(2011BAE03B01), the National Natural Science Foundation of China
(U1137601), the Natural Science Foundation of Yunnan of China
(KKSY201252078), and the Program for Innovative Research Team in
University of Ministry of Education of China (Grant No. IRT1250).
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NR 19
TC 24
Z9 25
U1 1
U2 29
PU SPRINGER
PI DORDRECHT
SN 1876-990X
EI 1876-9918
J9 SILICON-NETH
JI Silicon
PD JUL
PY 2015
VL 7
IS 3
SI SI
BP 269
EP 274
DI 10.1007/s12633-014-9228-9
PG 6
WC Chemistry, Physical; Materials Science, Multidisciplinary
GA CJ2WT
UT WOS:000355346100006
DA 2023-12-05
ER
PT J
AU Hussain, SI
Blowes, DW
Ptacek, CJ
Olding, D
AF Hussain, Syed I.
Blowes, David W.
Ptacek, Carol J.
Olding, Daniel
TI Phosphorus Removal from Lake Water Using Basic Oxygen Furnace Slag:
System Performance and Characterization of Reaction Products
SO ENVIRONMENTAL ENGINEERING SCIENCE
LA English
DT Article
DE precipitation; zero valent iron; adsorption; lake water; XANES; basic
oxygen furnace slag; phosphorus treatment
ID BLAST-FURNACE; PHOSPHATE ADSORPTION; TRICALCIUM PHOSPHATE;
PHASE-TRANSITIONS; XANES SPECIATION; STEEL SLAG; HYDROXYAPATITE;
SPECTROSCOPY; CARBONATE; CALCITE
AB Effectiveness of basic oxygen furnace slag (BOFS) for removing dissolved
phosphorus (P) was evaluated in a hypolimnetic withdrawal system. Lake water
collected from the hypolimnion, with phosphate (PO4-P) concentrations of 0.25 to
0.49 mg/L, was passed through a pilot-scale (pore volume, similar to 0.87 m(3))
treatment system over two successive summers. In year 1, the hydraulic retention
time (HRT) varied from 0.58 to 1.64 days and 96.1-98.1% PO4-P was removed. The HRT
in year 2 was 0.31 to 0.48 days and PO4-P removal was 97.4-99.9%. Effluent pH was
11.37 +/- 0.17 and 11.96 +/- 0.17 in years 1 and 2, respectively, with the increase
attributed to dissolution of CaO and Ca(OH)(2) from the BOFS. The effluent was
neutralized by addition of CO2(g) before the water was discharged. Vanadium and
aluminum were released from the BOFS, and were subsequently removed through
addition of a filter containing 5 wt.% granular zero valent iron with a balance of
silica sand and by neutralizing pH. Solid phase analyses conducted on the spent
media, including FESEM-EDX, XPS, FTIR, and XANES spectroscopy, confirmed the
presence of calcium carbonate and calcium phosphate minerals. Diminished hydraulic
performance was observed in year 1, which was attributed to CaCO3 accumulation on
the spent BOFS media. Restricting ingress of atmospheric CO2 into the system in
year 2 minimized the extent of CaCO3 accumulation on the treatment media and led to
improved hydraulic characteristics. Results show potential for long-term removal of
phosphorus.
C1 [Hussain, Syed I.; Blowes, David W.; Ptacek, Carol J.] Univ Waterloo, Dept Earth
& Environm Sci, Waterloo, ON N2L 3G1, Canada.
[Olding, Daniel] Town Richmond Hill, Richmond Hill, ON, Canada.
C3 University of Waterloo
RP Blowes, DW (corresponding author), Univ Waterloo, Dept Earth & Environm Sci, 200
Univ Ave W, Waterloo, ON N2L 3G1, Canada.
EM blowes@uwaterloo.ca
FU Idea to Innovation (I2I) program of the Natural Sciences and Engineering
Research Council (NSERC) of Canada; Government of Canada; NSERC; NRC;
CIHR; University of Saskatchewan [06B1-1, 16-4419]
FX This research was supported by the Idea to Innovation (I2I) program of
the Natural Sciences and Engineering Research Council (NSERC) of Canada,
the Green Municipal Fund financed by the Government of Canada and
administered by the Federation of Canadian Municipalities, and the Town
of Richmond Hill, Ontario, Canada. The XANES experiments were performed
at the Canadian Light Source, which is supported by NSERC, NRC, CIHR,
and the University of Saskatchewan on the 06B1-1 (SXRMB) beamline as
part of proposal # 16-4419. We thank Y. Hu for assistance with
synchrotron spectroscopy. We also thank J. Jamieson-Hanes, B. Gibson, K.
T. Leung, N. Heinig, J. Fisher, H. Siu, M. Biesinger, J. Bain, L. Groza,
J. Hu, D. Smyth, M. Lindsay, G. Binsted, and A. Campbell for their
assistance.
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NR 59
TC 24
Z9 26
U1 1
U2 46
PU MARY ANN LIEBERT, INC
PI NEW ROCHELLE
PA 140 HUGUENOT STREET, 3RD FL, NEW ROCHELLE, NY 10801 USA
SN 1092-8758
EI 1557-9018
J9 ENVIRON ENG SCI
JI Environ. Eng. Sci.
PD NOV 1
PY 2014
VL 31
IS 11
BP 631
EP 642
DI 10.1089/ees.2014.0074
PG 12
GA AR9MF
UT WOS:000343898200006
DA 2023-12-05
ER
PT J
AU Hiraki, T
Miki, T
Nakajima, K
Matsubae, K
Nakamura, S
Nagasaka, T
AF Hiraki, Takehito
Miki, Takahiro
Nakajima, Kenichi
Matsubae, Kazuyo
Nagasaka, Tetsuya
TI Thermodynamic Analysis for the Refining Ability of Salt Flux for
Aluminum Recycling
SO MATERIALS
LA English
DT Article
DE recycling of aluminum; thermodynamic analysis; impurity removal; salt
flux; refining ability
ID ALLOYING ELEMENTS; OPTIMIZATION; SEPARATION; SCRAP; FLOW
AB The removability of impurities during the aluminum remelting process by
oxidation was previously investigated by our research group. In the present work,
alternative impurity removal with chlorination has been evaluated by thermodynamic
analysis. For 43 different elements, equilibrium distribution ratios among metal,
chloride flux and oxide slag phases in the aluminum remelting process were
calculated by assuming the binary systems of aluminum and an impurity element. It
was found that the removability of impurities isn't significantly affected by
process parameters such as chloride partial pressure, temperature and flux
composition. It was shown that Ho, Dy, Li, La, Mg, Gd, Ce, Yb, Ca and Sr can be
potentially eliminated into flux by chlorination from the remelted aluminum.
Chlorination and oxidation are not effective to remove other impurities from the
melting aluminum, due to the limited parameters which can be controlled during the
remelting process. It follows that a proper management of aluminum scrap such as
sorting based on the composition of the products is important for sustainable
aluminum recycling.
C1 [Hiraki, Takehito; Miki, Takahiro; Matsubae, Kazuyo; Nagasaka, Tetsuya] Tohoku
Univ, Grad Sch Engn, Sendai, Miyagi 9808578, Japan.
[Nakajima, Kenichi] Natl Inst Environm Studies, Ctr Mat Cycles & Waste
Management Res, Tsukuba, Ibaraki 3058506, Japan.
[Nakamura, Shinichiro] Waseda Univ, Grad Sch Econ, Tokyo 1698050, Japan.
C3 Tohoku University; National Institute for Environmental Studies - Japan;
Waseda University
RP Hiraki, T (corresponding author), Tohoku Univ, Grad Sch Engn, Sendai, Miyagi
9808578, Japan.
EM hiraki@material.tohoku.ac.jp; miki@material.tohoku.ac.jp;
nakajima.kenichi@nies.go.jp; matsubae@m.tohoku.ac.jp;
nakashin@waseda.jp; t-nagasaka@m.tohoku.ac.jp
RI Nakajima, Kenichi/AAQ-3768-2021; Matsubae, Kazuyo/J-8842-2015
OI Nakajima, Kenichi/0000-0002-7241-7695; Matsubae,
Kazuyo/0000-0002-3816-3898
FU Japan Society for the Promotion of Science (JSPS) [B-22360387,
B-22360218]
FX This study was supported by a Grant-in-Aid for Scientific Research
(Grant No. B-22360387 and B-22360218) from the Japan Society for the
Promotion of Science (JSPS). Useful comments and encouragement given by
Takako Yamashita (JFE Steel Corporation) are gratefully acknowledged.
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NR 23
TC 24
Z9 26
U1 5
U2 37
PU MDPI
PI BASEL
SN 1996-1944
J9 MATERIALS
JI Materials
PD AUG
PY 2014
VL 7
IS 8
BP 5543
EP 5553
DI 10.3390/ma7085543
PG 11
Physics
GA AO3EC
UT WOS:000341210400009
PM 28788144
OA Green Submitted, gold, Green Published
DA 2023-12-05
ER
PT J
AU Huang, QY
Lv, XW
Huang, R
Song, JJ
AF Huang, Q. Y.
Lv, X. W.
Huang, R.
Song, J. J.
TI Preparation of Ti-Si-Al alloy by aluminothermic reduction of
TiO2 bearing blast furnace slag
SO CANADIAN METALLURGICAL QUARTERLY
LA English
DT Article
DE Blast furnace slag bearing TiO2; Aluminium; Reduction
ID KINETICS
AB The aluminothermic reduction of Ti containing BF slag was carried out to prepare
Ti-Si-Al alloy in this study in order to improve the recovery rate of the Ti from
the vanadium-titanium magnetite ore and solve the deposit problem of huge amount of
BF slag bearing 20-25% TiO2. It was found that the mass of alloy increased with
increasing Al addition. The mass of the slag obtained was more than that calculated
by FACTSage by 2-4%, meaning some unreduced oxide still remained in the slag,
and/or that equilibrium was not obtained. The Perovskite and Pyroxene minerals
disappeared, and the CaAl2O4 and MgAl2O3 were the dominant phases with increasing
the Al2O3 in the slag. The Ti5Si3, AlTi3 and TiSi2 were the main phase in the
solidified alloy. The LFe, LSi, and LTi, which represents the distribution ratio of
the elements like Fe, Si and Ti between the metal and the slag, decreased with
increasing temperature, and increased with increasing the Al addition. The measured
LFe departed greatly from the equilibrium, while the measured LSi almost reached
the equilibrium. The LTi reached the equilibrium when the Al addition was less than
18%, LTi departed from the equilibrium condition when the Al addition was more than
18%. The recovery of both Ti and Si increased with increasing the Al addition. For
Ti, it reached 80% when the Al addition was above 20%. For Si, the recovery is
always lower than that of Ti, it reached 70% when the Al addition was above 24%.
C1 [Huang, Q. Y.] Chongqing Unviers Sci & Technolgy, Sch Met & Mat Engn, Chongqing,
Peoples R China.
[Lv, X. W.; Huang, R.] Chongqing Univ, Sch Mat Sci & Engn, Chongqing 400044,
Peoples R China.
[Song, J. J.] Ctr Mat Chongqing Metrol Inst Qual Inspect, Chongqing 400038,
Peoples R China.
RP Lv, XW (corresponding author), Chongqing Univ, Sch Mat Sci & Engn, Chongqing
EM lvxuewei@163.com
FU Fund of Integrated Utilization on Panzhihua High Titanium-bearing BF
Slag [2010CY-G-1-1]; Fundamental Research Funds for the Central
Universities [0211005202025]
FX The authors are especially grateful to the Fund of Integrated
Utilization on Panzhihua High Titanium-bearing BF Slag (grant no.
2010CY-G-1-1), and Fundamental Research Funds for the Central
Universities (grant no. 0211005202025).
CR Du H, 1996, THEORY SMELTING V TI, P144
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TC 24
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U2 47
PI ABINGDON
SN 0008-4433
EI 1879-1395
J9 CAN METALL QUART
JI Can. Metall. Q.
PD OCT
PY 2013
VL 52
IS 4
BP 413
EP 421
DI 10.1179/1879139513Y.0000000087
PG 9
GA 269RM
UT WOS:000328259600011
DA 2023-12-05
ER
PT J
AU Mantry, S
Behera, D
Mishra, SK
Debasish, D
Jha, BB
Mishra, BK
AF Mantry, Sisir
Behera, Debadhyan
Mishra, Srimant K.
Debasish, Debidutta
Jha, Bharat B.
Mishra, Barada K.
TI Erosive Wear Analysis of Plasma-Sprayed Cu Slag-Al Composite Coatings
SO TRIBOLOGY TRANSACTIONS
LA English
DT Article
DE Erosion Wear; Plasma Spray Coating; Copper Slag; Taguchi Experimental
Design
ID PERFORMANCE
AB This article depicts the solid particle erosion response of plasma-sprayed
composite coatings using an industrial waste product (i.e., copper slag) and
aluminum. The influence of five operating parametersthat is, impact velocity,
erodent size, erodent temperature, impingement angle, and aluminum content of
feedstock with four different levels eachon performance output (i.e., erosion rate)
are studied using Taguchi's L16 orthogonal array design. Out of the five
parameters, impact velocity has been found to be most influential factor on the
erosion wear rate of coated samples. Maximum erosion takes place at an impingement
angle of 60 degrees, showing the semiductile response of the coating to solid
particle erosion. In addition, a multilinear mathematical equation is proposed in
order to predict the wear rate. The percentage of error between experimental data
and predicted data was small, with a very high correlation coefficient (r2) of
0.997 showing the correctness of the mathematical equation used.
C1 [Mantry, Sisir; Mishra, Srimant K.; Debasish, Debidutta; Jha, Bharat B.] CSIR
Inst Minerals & Mat Technol, Dept Surface Engn, Bhubaneswar 751013, Orissa, India.
[Behera, Debadhyan] CSIR Inst Minerals & Mat Technol, Dept Adv Mat Technol,
Bhubaneswar 751013, Orissa, India.
[Mishra, Barada K.] CSIR Inst Minerals & Mat Technol, Dept Hydro & Elect Met,
Bhubaneswar 751013, Orissa, India.
Institute of Minerals & Materials Technology (IMMT); Council of
Scientific & Industrial Research (CSIR) - India; CSIR - Institute of
Minerals & Materials Technology (IMMT); Council of Scientific &
Industrial Research (CSIR) - India; CSIR - Institute of Minerals &
Materials Technology (IMMT)
RP Mantry, S (corresponding author), CSIR Inst Minerals & Mat Technol, Dept Surface
Engn, Bhubaneswar 751013, Orissa, India.
RI Mishra, Srimant Kumar/AAS-7355-2020
OI Mishra, Srimant Kumar/0000-0001-7513-0078
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NR 27
TC 24
Z9 24
U1 0
U2 13
PI PHILADELPHIA
SN 1040-2004
EI 1547-397X
J9 TRIBOL T
JI Tribol. Trans.
PD MAR 1
PY 2013
VL 56
IS 2
BP 196
EP 202
DI 10.1080/10402004.2012.737503
PG 7
WC Engineering, Mechanical
SC Engineering
GA 100GX
UT WOS:000315686900006
DA 2023-12-05
ER
PT J
AU Fu, Y
Zhang, JC
Wang, YZ
Yu, YZ
AF Fu Ying
Zhang Jichao
Wang Yanzheng
Yu Yanzhen
TI Resource preparation of poly-Al-Zn-Fe (PAZF) coagulant from galvanized
aluminum slag: Characteristics, simultaneous removal efficiency and
mechanism of nitrogen and organic matters
LA English
DT Article
DE Galvanized aluminum slag; Coagulant; Zinc; Nitrogen; Organic matters;
Mechanism
ID BIOLOGICAL DENITRIFICATION; WASTE; WATER; FLOCCULANT; SLUDGE;
PHOSPHORUS; NITRATE; SI
AB A poly-Al-Zn-Fe (PAZF) coagulant was prepared using a galvanized aluminum slag
as main raw material, and was characterized by Scanning Electron Microscopy (SEM),
Infrared Spectroscopy (IR) and X-ray Diffraction (XRD). Simultaneous removal
efficiency and mechanism of nitrogen (as NH3-N) and organic matters (as CODCr)
during coagulation process in treating simulated fountain water by PAZF were
investigated compared to those by poly-aluminum-chloride (PAC). The results
indicated that PAZF has better coagulation performance than PAC: PAZF gave the
greatest NH3-N and CODCr removal of 82% and 89% over the whole dosage range,
respectively, in comparison with 17% and 57% by PAC. PAZF has stronger adsorption
than PAC: PAZF has a large surface area which consisted of series of cauliflower
head structure having some pleated ditches with different width and depth, in
comparison with an irregular mountain appearance of convex-concave structure of PAC
having a small surface area. PAZF has greater capability of
neutralization/destabilization for pollutants than PAC: the amount of positive
charge carried by the hydrolysis products of PAZF was more than that of PAC because
PAZF was composed of more crystalline and amorphous substances and was a co-polymer
of three metals of Al, Zn and Fe. PAZF gave higher nitrogen removal than PAC: PAZF
was a coagulant containing much zinc (w(Zn) = 30.25%), so one of its hydrolysis
products of "zinc of hydroxide system" can react with NH4+ and NH3 to give "zinc-
ammonia ion complexing system" positively charged. Nitrogen removal mechanism by
PAZF was a comprehensive action of coagulation and chemical reaction. (C) 2012
C1 [Fu Ying; Zhang Jichao; Wang Yanzheng; Yu Yanzhen] Univ Jinan, Sch Civil Engn &
Architecture, Jinan 250022, Shandong, Peoples R China.
C3 University of Jinan
RP Fu, Y (corresponding author), Univ Jinan, Sch Civil Engn & Architecture, Jinan
EM cea_fuy@ujn.edu.cn
FU Shandong Outstanding Young Scientist Award Foundation Funded Project;
International Cooperation Program for Excellent Lectures by Shandong
Provincial Education Department; [SBS1112]
FX This research was supported by a financial from Shandong Outstanding
Young Scientist Award Foundation Funded Project and (SBS1112) and
Financial Foundation funded from International Cooperation Program for
Excellent Lectures by Shandong Provincial Education Department (2009).
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NR 37
TC 24
Z9 29
U1 4
U2 72
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD SEP 1
PY 2012
VL 203
BP 301
EP 308
DI 10.1016/j.cej.2012.07.045
PG 8
SC Engineering
GA 017ZS
UT WOS:000309630300036
DA 2023-12-05
ER
PT J
AU Gerogiorgis, DI
Ydstie, BE
AF Gerogiorgis, DI
Ydstie, BE
TI Multiphysics CFD modelling for design and simulation of a multiphase
chemical reactor
SO CHEMICAL ENGINEERING RESEARCH & DESIGN
LA English
CT 7th World Congress of Chemical Engineering
CY JUL 10-14, 2005
CL Glasgow, SCOTLAND
DE computational fluid dynamics (CFD); modelling; design; simulation;
carbothermic reduction; aluminium
AB The present simulation study elaborates on a finite element (FE) computational
fluid dynamics (CFD) model (Gerogiorgis and Ydstie, 2003a) developed for a
candidate carbothermic aluminium reactor (Johansen and Aune, 2002), aimed at
industrial implementation of carbothermic Al production. Carbothermic reduction is
an alternative to the conventional Hall-Heroult electrolysis process and is
characterized by cost and environmental advantages as well as by a challenging
complexity. Process technology encompasses a wide spectrum of phenomena
(convection, diffusion, reaction, evapouration, electric field) that occur
simultaneously in a multiphase configuration, the geometry of which is an open
design problem and remains to be determined without prior experience or even
abundance of experimental data. The strong interaction among Joule heating,
endothermic reaction, natural Boussinesq convection and turbulent flow phenomena is
of paramount importance for understanding reactor performance; conducting CFD
simulations is an efficient way to advance with the latter goal, since reliable
high-temperature measurements of state variables are remarkably laborious,
uncertain and expensive. The quadruple partial differential equation (PDE) problem
(electric charge, heat, momentum and gas volume balances) for the slag flow in the
ARP reactor is solved via a commercial CFD software suite (FEMLAB (R) v. 2.3) to
obtain potential, temperature, velocity and gas volume fraction distributions in a
two-dimensional domain, representing in detail the complete second stage of the
proposed carbothermic reactor. The new challenge is the present paper is to
accurately calculate the volume fraction of the gas generated within the molten
slag and understand how the proposed geometry affects production, via the
instantaneous thermodynamic equilibrium assumption. The main objective of this CFD
study is to extract conclusions regarding the reactive slag flow, the extent of
space utilization and the existence of dead volumes, and to provide design
guidelines. A steady state sensitivity analysis of state variable distributions
(namely, potential, temperature, velocity and gas volume fraction) with respect to
a key design variable (the imposed voltage profile) reveals the reactor heating
potential, the geometry of the Al region and the nontrivial operation, design and
optimization problems.
C1 Carnegie Mellon Univ, Dept Chem Engn, Pittsburgh, PA 15213 USA.
RP Gerogiorgis, DI (corresponding author), Univ London Imperial Coll Sci Technol &
Med, CPSE, Prince Consort Rd,S Kensington Campus, London SW7 2AZ, England.
EM d.gerogiorgis@imperial.ac.uk
RI Gerogiorgis, Dimitrios Ι./E-3594-2014
OI Gerogiorgis, Dimitrios Ι./0000-0002-2210-6784
CR Bruno MJ, 2003, LIGHT MET, P395
Chung T.J., 2010, Computational fluid dynamics
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Gerogiorgis DI, 2003, LIGHT MET, P407
Gerogiorgis DI, 2003, ALUMINUM 2003, P289
Gerogiorgis DI, 2001, COMPUTATIONAL MODELING OF MATERIALS, MINERALS AND METALS
PROCESSING, P273
GEROGIORGIS DI, 2004, THESIS CARNEGIE MELL
GEROGIORGIS DI, 2003, P 3 INT C CFD MIN PR, P607
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Wetind R., 2001, THESIS ROYAL I TECHN
NR 15
TC 24
Z9 29
U1 0
U2 28
PU INST CHEMICAL ENGINEERS
PI RUGBY
PA 165-189 RAILWAY TERRACE, DAVIS BLDG, RUGBY CV21 3HQ, ENGLAND
SN 0263-8762
EI 1744-3563
J9 CHEM ENG RES DES
JI Chem. Eng. Res. Des.
PD JUN
PY 2005
VL 83
IS A6
BP 603
EP 610
DI 10.1205/cherd.04364
PG 8
SC Engineering
GA 947AL
UT WOS:000230614300006
DA 2023-12-05
ER
PT J
AU Rabah, MA
AF Rabah, MA
TI Recovery of aluminium, nickel-copper alloys and salts from spent
fluorescent lamps
SO WASTE MANAGEMENT
LA English
CT Conference on Sustainable Wastes Management
CY OCT, 2003
CL SARDINIA, ITALY
DE waste management; recycling; nickel-copper alloy; florescent lamps;
industrial waste
ID EXTRACTION
AB This study explores a combined pyro-hydrometallurgical method to recover pure
aluminium, nickel-copper alloy(s), and some valuable salts from spent fluorescent
lamps (SFLs). It also examines the safe recycling of clean glass tubes for the
fluorescent lamp industry. Spent lamps were decapped under water containing 35%
acetone to achieve safe capture of mercury vapour. Cleaned glass tubes, if broken,
were cut using a rotating diamond disc to a standard shorter length. Aluminium and
copper-nickel alloys in the separated metallic parts were recovered using suitable
flux to decrease metal losses going to slag. Operation variables affecting the
quality of the products, and the extent of recovery with the suggested method were
investigated. Results revealed that total loss in the glass tube recycling
operation was 2% of the SFLs. Pure aluminium meeting standard specification DIN
1712 was recovered by melting at 800 degreesC under sodium chloride/carbon flux for
20 min. Standard nickel-copper alloys with less than 0.1% tin were prepared by
melting at 1250 degreesC using a sodium borate/carbon flux. De-tinning of the
molten nickel-copper alloy was carried out using oxygen gas. Tin in the slag as
oxide was recovered by reduction using carbon or hydrogen gas at 650-700 degreesC.
Different valuable chloride salts were also obtained in good quality. Further
research is recommended on the thermodynamics of nickel-copper recovery, yttrium
and europium recovery, and process economics. (C) 2003 Elsevier Ltd. All rights
reserved.
C1 CMRDI, Ind Wastes Lab, Cairo 11421, Egypt.
RP Rabah, MA (corresponding author), CMRDI, Ind Wastes Lab, POB 87 Helwan, Cairo
11421, Egypt.
EM rucmrdi@rusys.eg.net
RI rabah, mahmoud/ABA-0085-2022
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NR 23
TC 24
Z9 27
U1 0
U2 34
PI OXFORD
SN 0956-053X
J9 WASTE MANAGE
JI Waste Manage.
PY 2004
VL 24
IS 2
BP 119
EP 126
DI 10.1016/j.wasman.2003.07.001
PG 8
GA 773GK
UT WOS:000188889400002
PM 14761750
DA 2023-12-05
ER
PT J
AU LOPEZ, FA
BALCAZAR, N
FORMOSO, A
PINTO, M
RODRIGUEZ, M
AF LOPEZ, FA
BALCAZAR, N
FORMOSO, A
PINTO, M
RODRIGUEZ, M
TI THE RECYCLING OF LINZ-DONAWITZ (LD) CONVERTER SLAG BY USE AS A LIMING
AGENT ON PASTURE LAND
LA English
DT Article
DE LINZ-DONAWITZ (LD) CONVERTER SLAG; RECYCLING; NUTRIENT CONTENT; ACIDIC
SOILS; DACTYLIS GLOMERATA; TRIFOLIUM REPENS AND LOLIUM PERENNE
AB Slag is a major by-product of the basic oxygen steelmaking converter process
(BOS). Methods are being developed to make use of this by-product and large
quantities are now employed in agriculture and in the production of aggregates in
several European Community (EC) countries. However, a great deal of slag is still
either simply discarded or discharged in landfills. This paper reports the effects
over a 3-year period on both soil and crops, of the application of Linz-Donawitz
(LD) converter slag on pasture land. Comparative studies were performed using
different quantities of low phosphorus LD converter slag and fertilizer on land
sown with Dactylis glomerata, Trifolium repens and Lolium perenne. The results
showed an increase in soil pH and in the availability of Ca and Mg in the soil
exchange complex. Aluminium content was reduced. When LD converter slag and
fertilizer were applied together, plants were seen to contain the greatest
concentrations of nutrients and greater yields were obtained. (C) 1995 ISWA
RP LOPEZ, FA (corresponding author), CSIC,NATL CTR MET RES,DEPT MAT RECYCLING,AVE
GREGORIO AMO 8,E-28040 MADRID,SPAIN.
RI López, Félix A./F-6016-2010
OI López, Félix A./0000-0001-9023-2996; Pinto, Miriam/0000-0002-7398-3306
NR 0
TC 24
Z9 25
U1 0
U2 8
PU ACADEMIC PRESS (LONDON) LTD
PI LONDON
PA 24-28 OVAL RD, LONDON, ENGLAND NW1 7DX
SN 0734-242X
J9 WASTE MANAGE RES
PD DEC
PY 1995
VL 13
IS 6
BP 555
EP 568
DI 10.1016/S0734-242X(05)80034-5
PG 14
GA TH554
UT WOS:A1995TH55400005
DA 2023-12-05
ER
PT J
AU HOWARD, RL
RICHARDS, SR
WELCH, BJ
MOORE, JJ
AF HOWARD, RL
RICHARDS, SR
WELCH, BJ
MOORE, JJ
TI VANADIUM DISTRIBUTION IN MELTS INTERMEDIATE TO FERROALLOY PRODUCTION
FROM VANADIFEROUS SLAG
LA English
DT Article
AB Processing of vanadiferous slags through the pyrometallurgical process route
appears to offer advantages both in terms of ferroalloy production and in the
potential for efficient vanadium recovery from hot metal. In order to investigate
the effect of slag composition on the phase distribution of vanadium, a series of
laboratory smelting experiments was carried out. The effect of basicity adjustments
on the slag/metal distribution of iron, vanadium, and manganese was investigated
using carbon and FeSi as a reductant. A simulation of the final stage of slag
reduction was also carried out to determine the efficiency of vanadium recovery
during metallothermic smelting using aluminum and FeSi.
C1 IND RES LTD, WELLINGTON, NEW ZEALAND.
COLORADO SCH MINES, DEPT MET & MAT ENGN, GOLDEN, CO 80401 USA.
UNIV AUCKLAND, DEPT CHEM & MAT ENGN, AUCKLAND, NEW ZEALAND.
C3 Callaghan Innovation; Colorado School of Mines; University of Auckland
RP HOWARD, RL (corresponding author), AFRICAN MINING & TRUST CO, JOHANNESBURG,
SOUTH AFRICA.
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NR 15
TC 24
Z9 25
U1 0
U2 5
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD FEB
PY 1994
VL 25
IS 1
BP 27
EP 32
DI 10.1007/BF02663175
PG 6
Engineering
GA MU427
UT WOS:A1994MU42700003
DA 2023-12-05
ER
PT J
AU Das, P
Upadhyay, S
Dubey, S
Singh, KK
AF Das, Pallabi
Upadhyay, Sidhidatri
Dubey, Sudarshan
Singh, Krishnakant K.
TI Waste to wealth: Recovery of value-added products from steel slag
SO JOURNAL OF ENVIRONMENTAL CHEMICAL ENGINEERING
LA English
DT Article
DE Resource recovery; Steel slag; Value-added product; Waste valorization;
Waste to wealth
ID BLAST-FURNACE SLAG; RARE-EARTH-ELEMENTS; UPGRADE PHOSPHORUS REMOVAL;
CALCIUM SILICATE HYDRATE; CONVERTER SLAG; MAGNETIC SEPARATION; SELECTIVE
RECOVERY; STEELMAKING SLAG; METAL RECOVERY; PHYSICAL-PROPERTIES
AB Steel slag, a by-product generated during steel production poses a solid waste
disposal challenge. The same slag contains valuables such as titanium, nickel,
vanadium, iron, aluminum, silica among others. The extracted components can cause
productive value addition in diverse realms like wastewater treatment to
semiconductor devices. A paradigm shift is required towards waste valorization for
developing profitable extraction methods for these constituent elements. In this
review, an attempt was made to assimilate such technologies into one concrete and
concise compendium. The pros and cons of each method were weighed comparatively
with respect to applicability and innovation. An effort was attempted for assessing
key design aspects and scale-up potential vis 'a-vis the economic analysis for the
valorization techniques. It was seen that the leaching technique was the most
widely used in the resource recovery domain followed by other techniques like
fusion, hydrothermal treatment. Techniques that dominate the exploration of some of
the metals from their lean ores or respective mineral slags might also be explored
for their recovery from steel slag. Some technologies like slag filter development
for phosphate removal has already been tested in real-life conditions while others
are in the nascent stages of development. Special focus can be directed towards the
simultaneous extraction of multiple components or direct in-situ product formation
and its subsequent separation. This paper reviews various technologies for steel
slag valorization to guide researchers working in the field of slag resource
recovery and sustainable waste utilization.
C1 [Das, Pallabi; Upadhyay, Sidhidatri; Singh, Krishnakant K.] CSIR Cent Inst Min &
Fuel Res, Barwa Rd, Dhanbad 826015, Jharkhand, India.
[Dubey, Sudarshan] Birla Inst Technol & Sci, Pilani Hyderabad Campus, Hyderabad,
India.
Central Institute of Mining & Fuel Research (CIMFR); Birla Institute of
Technology & Science Pilani (BITS Pilani)
RP Das, P (corresponding author), CSIR Cent Inst Min & Fuel Res, Barwa Rd, Dhanbad
826015, Jharkhand, India.
EM pallabidas@cimfr.nic.in
OI Das, Pallabi/0000-0003-4831-8360
FU Ministry of Steel, GOI; Ministry of Steel, Government of India
FX Ms. Pallabi Das is recipient of Grant-in-Aid research funding from
Ministry of Steel, GOI The authors are grateful to Ministry of Steel,
Government of India for Grant-in-Aid funding. The Authous are also
grateful to Director, CSIR-CIMFR for his continued support and
encouragement
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TC 23
Z9 24
U1 11
U2 63
PU ELSEVIER SCI LTD
PI OXFORD
SN 2213-2929
EI 2213-3437
J9 J ENVIRON CHEM ENG
JI J. Environ. Chem. Eng.
PD AUG
PY 2021
VL 9
IS 4
AR 105640
DI 10.1016/j.jece.2021.105640
EA MAY 2021
PG 21
SC Engineering
GA TF0HT
UT WOS:000670389100003
DA 2023-12-05
ER
PT J
AU Xu, CY
Wang, C
Xu, RZ
Zhang, JL
Jiao, KX
AF Xu, Chen-yang
Wang, Cui
Xu, Ren-ze
Zhang, Jian-liang
Jiao, Ke-xin
TI Effect of Al2O3 on the viscosity of
CaO-SiO2-Al2O3-MgO-Cr2O
3 slags
LA English
DT Article
DE slag; viscosity; high aluminium oxide; apparent activation energy;
structure; viscosity prediction
ID MODEL; BEHAVIOR; ALUMINOSILICATE; PROPERTY; ALUMINA; MELTS; CAF2
AB We investigated the effect of Al2O3 content on the viscosity of CaO-SiO2-Al2O3-
8wt%MgO-1wt%Cr2O3 (mass ratio of CaO/SiO2 is 1.0, and Al2O3 content is 17wt%-29wt%)
slags. The results show that the viscosity of the slag increases gradually with
increases in the Al2O3 content in the range of 17wt% to 29wt% due to the role of
Al2O3 as a network former in the polymerization of the aluminosilicate structure of
the slag. With increases in the Al2O3 content from 17wt% to 29wt%, the apparent
activation energy of the slags also increases from 180.85 to 210.23 kJ/mol, which
is consistent with the variation in the critical temperature. The Fourier-transform
infrared spectra indicate that the degree of polymerization of this slag is
increased by the addition of Al2O3. The application of Iida's model for predicting
the slag viscosity in the presence of Cr2O3 indicates that the calculated viscosity
values fit well with the measured values when both the temperature and Al2O3
content are at relatively low levels, i.e., the temperature range of 1673 to 1803 K
and the Al2O3 content range of 17wt%-29wt% in CaO-SiO2-Al2O3-8wt%MgO-1wt%Cr2O3
slag.
C1 [Xu, Chen-yang; Xu, Ren-ze; Zhang, Jian-liang; Jiao, Ke-xin] Univ Sci & Technol
[Wang, Cui; Zhang, Jian-liang] Univ Sci & Technol Beijing, State Key Lab Adv
Technology Beijing
RP Xu, RZ; Zhang, JL (corresponding author), Univ Sci & Technol Beijing, Sch Met &
Ecol Engn, Beijing 100083, Peoples R China.; Zhang, JL (corresponding author), Univ
Sci & Technol Beijing, State Key Lab Adv Met, Beijing 100083, Peoples R China.
EM zurenze2010@163.com; zhang.jianliang@hotmail.com
RI jin, li/IWU-4648-2023; zhan, y/ISA-2807-2023; zhang, jian/HPD-1712-2023
CR [Anonymous], 2017, STEEL RES INT, V88
[Anonymous], 2018, STEEL RES INT, V89
[杜长坤 Du Changkun], 2013, [钢铁研究学报, Journal of Iron and Steel Research],
V25, P19
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2916.1952.tb13057.x
2916.1945.tb14500.x
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120
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NR 34
TC 23
Z9 23
U1 2
U2 33
PU SPRINGER
PI NEW YORK
SN 1674-4799
EI 1869-103X
PD MAY
PY 2021
VL 28
IS 5
BP 797
EP 803
DI 10.1007/s12613-020-2187-9
PG 7
Mineral Processing
GA RY2KH
UT WOS:000647745700006
DA 2023-12-05
ER
PT J
AU Zhao, HL
Liu, FQ
Xie, MZ
Liu, W
Sohn, HY
AF Zhao, Hongliang
Liu, Fengqin
Xie, Mingzhuang
Liu, Wei
Sohn, Hong Yong
TI Recycling and utilization of spent potlining by different high
temperature treatments
LA English
DT Article
DE Spent potlining; Classification; High temperature treatment; Recycling;
Utilization
ID RECOVERY; COMPONENT; CARBON
AB Spent potlining (SPL) is generated at the end of the service life of aluminum
reduction cells and is a hazardous solid waste that negatively impacts the
environment and ecology. Based on the differences in the hazardous and valuable
components of SPL, a classified recycling and utilization path is proposed in this
work. Three different high-temperature processes of oxygen-controlled treatment,
vacuum treatment, and co-processing in a cement kiln were adopted for spent cathode
carbon block (SCCB), spent silicon carbide block (SSCB) and spent barrier and
insulating refractory materials (SBIM), respectively. After the classified
treatments, all the cyanides in SCCB were decomposed, almost all the Si3N4 was
decomposed and Na2SiO3 was removed from SSCB, and over 99% of the fluorides was
separated from SCCB and SSCB to obtain high graphitization carbon and silicon
carbide. The fluorides in SBIM were converted into a mineralizer that lowered the
burning temperature of the cement clinker. The performances of prepared cement met
the requirements of Portland slag, Portland pozzolana and Portland flash ash
cements. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Zhao, Hongliang; Liu, Fengqin; Xie, Mingzhuang; Liu, Wei] Univ Sci & Technol
Beijing, State Key Lab Adv Met, Beijing 100083, Peoples R China.
[Zhao, Hongliang; Liu, Fengqin; Xie, Mingzhuang; Liu, Wei] Univ Sci & Technol
[Zhao, Hongliang; Sohn, Hong Yong] Univ Utah, Dept Mat Sci & Engn, Salt Lake
City, UT 84112 USA.
Technology Beijing; Utah System of Higher Education; University of Utah
RP Liu, FQ (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
EM liufq@ustb.edu.cn
OI Sohn, Hong Yong/0000-0002-6710-9508
Key Research and Development Program of Ningxia Hui Autonomous Region
[2018BDE02050]; China Scholarship Council
Program of China (2019YFC1908403), and the Key Research and Development
Program of Ningxia Hui Autonomous Region (2018BDE02050). The authors
also thank the China Scholarship Council for providing Chinese
Government Scholarship to Hongliang Zhao to study as a Visiting Scholar
in Professor Hong Yong Sohn's laboratory at the University of Utah.
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NR 53
TC 23
Z9 23
U1 8
U2 58
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAR 20
PY 2021
VL 289
AR 125704
DI 10.1016/j.jclepro.2020.125704
EA JAN 2021
PG 9
& Ecology
GA QK3IP
UT WOS:000620274500023
DA 2023-12-05
ER
PT J
AU Yoldi, M
Korili, SA
Gil, A
AF Yoldi, M.
Korili, S. A.
Gil, A.
TI Zeolite synthesis from aluminum saline slag waste
LA English
DT Article
DE Industrial waste valorization; High-value-added products; Aluminum
alkaline extraction; Wastes valorization; Zeolite synthesis
AB This work describes the synthetic procedures developed to obtain zeolite X
(NaX), zeolite A (LTA) and sodalite (SOD) using aluminum saline slag waste (AISSW)
as aluminum source in a two-step hydrothermal method involving alkaline extraction
of Al, with separation of the residual waste, and hydrothermal treatment at low
temperatures and long reaction times. Use of the mother liquor obtained after
filtration and separation of the zeolite is also analyzed in the alkaline
extraction of AI. The synthetic parameters that determine the type of zeolite,
purity, crystallinity, specific surface area, pore size and pore volume include the
Si/AI molar ratio, pH, nucleation temperature and time, and crystallization
temperature and time. These critical parameters were studied and determined to
synthesize NaX. LTA and SOD as individual phases. The materials obtained were
characterized by X-ray diffraction, scanning electron microscopy and N-2
adsorption/desorption measurements at -196 degrees C. The characteristics of the
best zeolites obtained are similar to those of IZA references and the specific
surface areas are in the range of commercial ones: NaX ranges from 450 to 500
m(2)/g and LTA from 250 to 300 m(2)/g. The results show that it is possible to
synthesize zeolites from AISSW, thus allowing these materials to be applied as
promising adsorbents and catalysts. (C) 2020 Elsevier B.V. All rights reserved.
OI Gil, Antonio/0000-0001-9323-5981
European Regional Development Fund (ERDF); Government of Navarra
[MAT2016-78863-C2-1-R, PI017-PI039 CORRAL]; Banco Santander
Regional Development Fund (ERDF) and the Government of Navarra through
projects MAT2016-78863-C2-1-R and PI017-PI039 CORRAL. AG, EGFO and MY
also thank Banco Santander for funding via the Research Intensification
Program.
CR Ahmadi B, 2010, CEMENT CONCRETE COMP, V32, P134, DOI
10.1016/j.cemconcomp.2009.10.006
Auerbach S.M., 2003, HDB ZEOLITE
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10.1016/j.micromeso.2018.04.038
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9465(99)00010-4
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10.1016/j.conbuildmat.2012.04.038
10.1016/j.micromeso.2016.01.037
Yoldi M, 2019, MINER ENG, V140, DOI 10.1016/j.mineng.2019.105884
10.1016/j.micromeso.2019.06.009
NR 15
TC 23
Z9 23
U1 3
U2 41
PU ELSEVIER
PI AMSTERDAM
SN 0032-5910
EI 1873-328X
J9 POWDER TECHNOL
JI Powder Technol.
PD APR 15
PY 2020
VL 366
BP 175
EP 184
DI 10.1016/j.powtec.2020.02.069
PG 10
SC Engineering
GA LH0NV
UT WOS:000528488000019
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Ni, PY
Tanaka, T
Suzuki, M
Nakamoto, M
Jönsson, PG
AF Ni, Peiyuan
Tanaka, Toshihiro
Suzuki, Masanori
Nakamoto, Masashi
Jonsson, Par Goren
TI A Kinetic Model of Mass Transfer and Chemical Reactions at a Steel/Slag
Interface under Effect of Interfacial Tensions
LA English
DT Article
DE steel-slag interfacial tension; mass transfer; thermodynamics and
kinetics; interfacial reactions; dynamic modeling
ID MOLTEN IRON; SLAG; METAL; EQUILIBRIUM; INCLUSIONS; ALLOY
AB A new kinetic model was developed to predict the dynamic change of the
interfacial oxygen content and the steel/slag interfacial tension. This model
mainly describes the following interfacial physicochemical phenomena: i) Silica
decomposition and oxygen adsorption at the interface, ii) Oxygen and aluminum
reactions at the interface, iii) Oxygen desorption from the interface, iv) Silica
mass transfer from the slag to the interface, v) Dissolution of the formed alumina
into the slag and its transfer in slag and vi) Blockage on the silica mass
transfer, to come in contact with the steel, by the accumulation of the formed
alumina at the interface. With this model, the dynamic changes of the interfacial
oxygen contents under different aluminum contents in steel and different slag
viscosities were predicted. Overall, the interfacial oxygen content was found to
increase with a decreased aluminum content and a decreased slag viscosity.
Furthermore, the aluminum reaction rate can significantly influence the interfacial
oxygen content as well as the interfacial tension. In addition, the model captured
the fast increase of the interfacial tension after passing the minimum value point
for the system of a high -Al content steel and a low viscous slag, which is in
agreement with the experimental observations. Furthermore, a parameter study was
carried out to show the influence of various parameters on the dynamic interfacial
phenomena.
C1 [Ni, Peiyuan; Tanaka, Toshihiro; Suzuki, Masanori; Nakamoto, Masashi] Osaka
Univ, Div Mat & Mfg Sci, Grad Sch Engn, 2-1 Yamadaoka, Suita, Osaka 5650871, Japan.
[Jonsson, Par Goren] KTH Royal Inst Technol, Dept Mat Sci & Engn, S-10044
Stockholm, Sweden.
C3 Osaka University; Royal Institute of Technology
RP Tanaka, T (corresponding author), Osaka Univ, Div Mat & Mfg Sci, Grad Sch Engn,
2-1 Yamadaoka, Suita, Osaka 5650871, Japan.
EM tanaka@mat.eng.osaka-u.ac.jp
OI Nakamoto, Masashi/0000-0003-4684-0200
FU Japan Society for the Promotion of Science [JP17F17766]; Swedish
Foundation for Strategic Research
FX This work was supported by a Grant-in-Aid for JSPS (Japan Society for
the Promotion of Science) International Research Fellow (Grant No.
JP17F17766). Peiyuan NI wants to thank the support by JSPS for his stay
at Osaka University as a JSPS International Postdoctoral Research
Fellow, and also thanks the support by Swedish Foundation for Strategic
Research.
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303
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654
NR 18
TC 23
Z9 23
U1 0
U2 14
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2019
VL 59
IS 5
BP 737
EP 748
PG 12
GA IA2QT
UT WOS:000469406900001
DA 2023-12-05
ER
PT J
AU Font, A
Borrachero, MV
Soriano, L
Monzó, J
Mellado, A
Payá, J
AF Font, Alba
Victoria Borrachero, Maria
Soriano, Lourdes
Monzo, Jose
Mellado, Ana
Paya, Jordi
TI New eco-cellular concretes: sustainable and energy-efficient materials
SO GREEN CHEMISTRY
LA English
DT Article
ID ALKALI-ACTIVATED BINDERS; CATALYST RESIDUE FCC; CANE STRAW ASH; FOAM
CONCRETE; WASTE GLASS; FLY-ASH; GEOPOLYMER; MORTAR; CONSTRUCTION;
STRENGTH
AB Chemistry is an essential science for understanding and developing construction
materials. Specifically, the application of the green chemistry concept to the
cement sector may allow the fabrication of new environmentally friendly materials
with good sustainability and energy efficiency. Cellular concretes are an excellent
alternative to conventional concrete in terms of thermal insulation and material
economy. In this paper, the development of waste-based cellular concrete is
presented; due to its good performance and low environmental impact, this focus is
warranted. Three different cellular concrete systems were investigated: (i)
traditional cellular concrete based on ordinary Portland cement and commercial
aluminium powder; (ii) geopolymer cellular concrete applying alkali-activated
chemical technology with a comparison of the use of two precursors, fluid catalytic
cracking catalyst residue (FCC) and blast furnace slag (BFS), and recycled
aluminium foil as an aerating agent; (iii) eco-cellular concrete, where commercial
waterglass was replaced by an agro-industrial by-product, rice husk ash (RHA), in
the activating solution. The development of geopolymer cellular concretes with
different precursors and activating solutions has proven that the production of
this type of concrete using different types of precursors is possible, depending on
the availability of by-products and wastes. The densities, compressive strengths,
and thermal properties of the three cellular concrete systems are assessed and a
complete study on the carbon footprints of the developed concretes is presented.
The results show that the alternative concretes have densities from 474 to 813 kg
m(-3), with compressive strengths from 2.6 to 4.6 MPa and thermal conductivities
from 0.083 to 0.281 W m(-1) K-1. In the case of the cellular concrete prepared
using RHA in the activating reagent, the heat released from the dissolution of NaOH
pellets in water dissolved the soluble silica present in the ash. This production
method resulted in a reduction of its carbon footprint by 78%.
C1 [Font, Alba; Victoria Borrachero, Maria; Soriano, Lourdes; Monzo, Jose; Mellado,
Ana; Paya, Jordi] Univ Politecn Valencia, Grp Invest Quim Mat GIQUIMA, ICITECH Inst
Ciencia & Tecnol Hormigon, Valencia, Spain.
C3 Universitat Politecnica de Valencia
RP Payá, J (corresponding author), Univ Politecn Valencia, Grp Invest Quim Mat
GIQUIMA, ICITECH Inst Ciencia & Tecnol Hormigon, Valencia, Spain.
EM jjpaya@cst.upv.es
RI Balbuena, José María Monzó/L-7253-2014; Soriano, Lourdes/F-7471-2014;
PAYA, JORDI/K-6377-2014; Mellado Romero, Ana Maria/K-5880-2014
OI Balbuena, José María Monzó/0000-0002-3657-3076; Soriano,
Lourdes/0000-0002-5749-4609; Borrachero/0000-0002-7873-0658; PAYA,
JORDI/0000-0001-7425-5311; Mellado Romero, Ana Maria/0000-0002-2105-154X
FU Universitat Politecnica de Valencia (UPV)
FX The authors acknowledge financial support from the Universitat
Politecnica de Valencia (UPV) through the internal project GEOCELPLUS.
The authors would also like to express special gratitude to Dr Mrs
Josefa L. Rosello Caselles for the recycled aluminium foil and to the
Electronic Microscopy Service of the UPV. Thanks are given to DACSA,
Cementval and BPOil for supplying samples.
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NR 40
TC 23
Z9 23
U1 4
U2 87
PI CAMBRIDGE
ENGLAND
SN 1463-9262
EI 1463-9270
J9 GREEN CHEM
JI Green Chem.
PD OCT 21
PY 2018
VL 20
IS 20
BP 4684
EP 4694
DI 10.1039/c8gc02066c
PG 11
GA GY2AK
UT WOS:000448339400014
OA Green Published
DA 2023-12-05
ER
PT J
AU Cai, BY
Watanabe, T
Kamijo, C
Susa, M
Hayashi, M
AF Cai, Boyuan
Watanabe, Takashi
Kamijo, Chikashi
Susa, Masahiro
Hayashi, Miyuki
TI Comparison between Reducibilities of Columnar Silico-ferrite of Calcium
and Aluminum (SFCA) Covered with Slag and Acicular SFCA with Fine Pores
LA English
DT Article
DE acicular SFCA; columnar SFCA; calcio-wustite; high temperature X-ray
diffraction; reduction; microstructure; hydrogen addition
ID CONSTITUENT MINERALS; CRYSTAL-STRUCTURE; SINTER; REDUCTION; TEMPERATURE;
STAGE
AB Reducibilities of silico-ferrite of calcium and aluminum (SFCA) have been
examined using high temperature X-ray diffraction (XRD) analysis including the
effect of hydrogen. Two types of sample were prepared: columnar SFCA covered with
slag and acicular SFCA with fine pores, denoted by 'Columnar SFCA and Acicular
SFCA, respectively. These samples were synthesized using chemical reagents and iron
ore powders. XRD analysis was applied to the samples heated in a condition
simulating a blast furnace. Oxygen partial pressure was controlled by gas mixtures
of CO-CO2-He, and there were some cases where 3.9 vol% of hydrogen gas was added to
the mixture. The microstructures of the samples before and after heating were
observed by electron probe microanalysis (EPMA). XRD profiles indicated: (i) both
SFCA samples were reduced to Fe via calcio-wustite (CW), (ii) the reduction from
'Acicular SFCA to CW took place at lower temperatures than that of 'Columnar SFCA
during the heating cycle up to 1 000 degrees C, and (iii) CW produced from
'Acicular SFCA' was reduced to Fe earlier than CW from 'Columnar SFCA at 1 000
degrees C. These results suggest that SFCA and CW phases in 'Acicular SFCA have
higher reducibility than those in 'Columnar SFCA. This would be because 'Acicular
SFCA consists of smaller SFCA particles with fine pores. BSE images have revealed
that such microstructures still remained even after the reduction to CW. Additions
of hydrogen promoted reduction of 'Columnar SFCA more effectively, and this effect
was observed more remarkably in the reduction from CW to Fe than from SFCA to CW.
C1 [Cai, Boyuan] Tokyo Inst Technol, Dept Met & Ceram Sci, Meguro Ku, 2-12-1
Ookayama, Tokyo 1528552, Japan.
[Watanabe, Takashi; Susa, Masahiro; Hayashi, Miyuki] Tokyo Inst Technol, Dept
Mat Sci & Engn, Meguro Ku, 2-12-1 Ookayama, Tokyo 1528552, Japan.
[Kamijo, Chikashi] Nippon Steel & Sumitomo Met Corp, R&D Labs, 20-1 Shintomi,
Futtsu, Chiba 2938511, Japan.
C3 Tokyo Institute of Technology; Tokyo Institute of Technology; Nippon
Steel & Sumitomo Metal Corporation
RP Cai, BY (corresponding author), Tokyo Inst Technol, Dept Met & Ceram Sci, Meguro
Ku, 2-12-1 Ookayama, Tokyo 1528552, Japan.
EM cai.b.aa@m.titech.ac.jp
RI Hayashi, Miyuki/AAW-9891-2020
FU New Energy and Industrial Technology Development Organization (NEDO);
Japan Iron and Steel Federation (JISF)
FX The present work was carried out as a part of COURSE50 project. The
authors are thankful to the New Energy and Industrial Technology
Development Organization (NEDO) and the Japan Iron and Steel Federation
(JISF) for their financial support.
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NR 19
TC 23
Z9 23
U1 4
U2 23
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2018
VL 58
IS 4
BP 642
EP 651
PG 10
GA GE0LV
UT WOS:000430906200009
OA gold
DA 2023-12-05
ER
PT J
AU Wegner, CE
Liesack, W
AF Wegner, Carl-Eric
Liesack, Werner
TI Unexpected Dominance of Elusive Acidobacteria in Early Industrial Soft
Coal Slags
SO FRONTIERS IN MICROBIOLOGY
LA English
DT Article
DE Soft coal; slags; mineral leaching; acid mine drainage; microbiome;
acidobacteria; metagenomics; microbial dark matter
ID PROTEIN FAMILIES DATABASE; MICROBIAL COMMUNITIES; SP-NOV.;
ORGANIC-MATTER; COMPARATIVE GENOMICS; SOIL BACTERIA; HUMIC ACIDS; GEN.
NOV.; DIVERSITY; SEQUENCES
AB Acid mine drainage (AMD) and mine tailing environments are well-characterized
ecosystems known to be dominated by organisms involved in iron- and sulfur-cycling.
Here we examined the microbiology of industrial soft coal slags that originate from
alum leaching, an ecosystem distantly related to AMD environments. Our study
involved geochemical analyses, bacterial community profiling, and shotgun
metagenomics. The slags still contained high amounts of alum constituents
(aluminum, sulfur), which mediated direct and indirect effects on bacterial
community structure. Bacterial groups typically found in AMD systems and mine
tailings were not present. Instead, the soft coal slags were dominated by
uncharacterized groups of Acidobacteria (DA052 [subdivision 2], KF-JG30-18
[subdivision 13]), Actinobacteria (TM214), Alphaproteobacteria (DA111), and
Chloroflexi (JG37-AG-4), which have previously been detected primarily in peatlands
and uranium waste piles. Shotgun metagenomics allowed us to reconstruct 13 high-
quality Acidobacteria draft genomes, of which two genomes could be directly linked
to dominating groups (DA052, KF-JG30-18) by recovered 16S rRNA gene sequences.
Comparative genomics revealed broad carbon utilization capabilities for these two
groups of elusive Acidobacteria, including polysaccharide breakdown (cellulose,
xylan) and the competence to metabolize C1 compounds (ribulose monophosphate
pathway) and lignin derivatives (dye-decolorizing peroxidases). Equipped with a
broad range of efflux systems for metal cations and xenobiotics, DA052 and KF-JG30-
18 may have a competitive advantage over other bacterial groups in this unique
habitat.
C1 [Wegner, Carl-Eric; Liesack, Werner] Max Planck Inst Terr Microbiol, Dept
Biogeochem, Marburg, Germany.
[Wegner, Carl-Eric] Friedrich Schiller Univ, Aquat Geomicrobiol, Inst Ecol,
Jena, Germany.
C3 Max Planck Society; Friedrich Schiller University of Jena
RP Liesack, W (corresponding author), Max Planck Inst Terr Microbiol, Dept
Biogeochem, Marburg, Germany.
EM liesack@mpi-marburg.mpg.de
RI Wegner, Carl-Eric/U-9401-2019
OI Wegner, Carl-Eric/0000-0002-4339-6602; Liesack,
Werner/0000-0002-9533-1552
FU German Research Foundation (DFG) [SFB 987]
FX Funding was provided by the German Research Foundation (DFG SFB 987,
Microbial Diversity in Environmental Signal Response, Project A05 to
WL).
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NR 104
TC 23
Z9 24
U1 2
U2 48
PI LAUSANNE
EI 1664-302X
J9 FRONT MICROBIOL
JI Front. Microbiol.
PD JUN 8
PY 2017
VL 8
AR 1023
DI 10.3389/fmicb.2017.01023
PG 13
WC Microbiology
SC Microbiology
GA EW9RD
UT WOS:000402856000002
PM 28642744
DA 2023-12-05
ER
PT J
AU Yasipourtehrani, S
Strezov, V
Bliznyukov, S
Evans, T
AF Yasipourtehrani, Sara
Strezov, Vladimir
Bliznyukov, Sergey
Evans, Tim
TI Investigation of thermal properties of blast furnace slag to improve
process energy efficiency
LA English
DT Article
DE Blast furnace slag; Slag viscosity; Slag heat exchange; Pig iron
heating; Slag thermal behaviours; End use product value; High
temperature hot stage SEM; In-situ SEM heating
ID IRON; VISCOSITY; BEHAVIOR
AB Blast furnace slag (BFS) is the main by-product of iron making and is produced
in large amounts worldwide. To improve energy use, it is necessary to understand
the thermal behaviour of slags under differing compositions at varying
temperatures. This study determines the thermal properties and behaviour of
selected slag samples using several experimental techniques, including high
temperature Hot Stage Scanning Electron Microscopy (HS-SEM), and Computer Aided
Thermal Analysis (CATA). Further methods, such as Energy Dispersive Spectroscopy
(EDS) and Fourier Transfer Infrared Spectroscopy (FTIR) were applied to determine
the chemical content and nature of the studied BFS samples. Comparing the chemical
composition of the slags and their thermal behaviour, the effect of magnesium oxide
and aluminium oxide was evident on the crystallisation and fluidity of the molten
slag. Additionally, the content of silicon dioxide had an effect on the
crystallisation temperature and network strength. (C) 2017 Elsevier Ltd. All rights
reserved.
C1 [Yasipourtehrani, Sara; Strezov, Vladimir; Bliznyukov, Sergey; Evans, Tim]
Macquarie Univ, Fac Sci & Engn, Dept Environm Sci, N Ryde, NSW 2109, Australia.
C3 Macquarie University
RP Strezov, V (corresponding author), Macquarie Univ, Fac Sci & Engn, Dept Environm
Sci, N Ryde, NSW 2109, Australia.
EM vladimir.strezov@mq.edu.au
RI Strezov, Vladimir/J-4827-2019
OI Strezov, Vladimir/0000-0002-9129-9284
FU Australian Research Council's Linkage Projects funding scheme
[LP140100182]; Australian Research Council [LP140100182] Funding Source:
Australian Research Council
FX This research was supported under Australian Research Council's Linkage
Projects funding scheme (project number LP140100182).
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Z9 25
U1 1
U2 17
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD APR 15
PY 2017
VL 149
BP 137
EP 145
DI 10.1016/j.jclepro.2017.02.052
PG 9
& Ecology
GA EX6CO
UT WOS:000403330200012
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Zhang, GQ
Zhang, TA
Zhang, Y
Lv, GZ
Liu, Y
Liu, ZL
AF Zhang, Guo-Quan
Zhang, Ting-An
Zhang, Ying
Lv, Guo-Zhi
Liu, Yan
Liu, Zhuo-Lin
TI Pressure leaching of converter vanadium slag with waste titanium dioxide
SO RARE METALS
LA English
DT Article
DE Vanadium; Waste titanium dioxide; Pressure leaching; Resource
utilization
ID EXTRACTION
AB The process of pressure leaching the converter vanadium slag with waste titanium
dioxide without roasting was studied. Mineralogy analysis indicates that the
converter vanadium slag contains mainly three mineral phases: magnetite, titanium
magnetite, and silicate phase. Vanadium is in combination with iron, titanium,
manganese, aluminum, and silicon. The impacts of leaching temperature, leaching
time, stirring speed, liquid-to-solid ratio, and initial leaching agent
concentration were investigated on the waste titanium dioxide leaching process. The
results indicate that under the optimal conditions, the vanadium and the iron
leaching rates are 96.85 % and 93.50 %, respectively, and the content of titanium
is 12.6 % in the residue. The main mineral phases for the residues under the
optimal operation conditions are quartz, ilmenite, anatase, and silicate phase, and
the residues can be reused as the extraction of titanium raw materials for titanium
dioxide production technology by the sulfate method.
C1 [Zhang, Guo-Quan; Zhang, Ting-An; Zhang, Ying; Lv, Guo-Zhi; Liu, Yan; Liu, Zhuo-
Lin] Northeastern Univ, Sch Mat & Met, Minist Educ, Key Lab Ecol Utilizat Multimet
Intergrown Ores, Shenyang 110819, Peoples R China.
RP Zhang, TA (corresponding author), Northeastern Univ, Sch Mat & Met, Minist Educ,
Key Lab Ecol Utilizat Multimet Intergrown Ores, Shenyang 110819, Peoples R China.
EM zta2000@163.net
RI zhang, ting/IYT-0642-2023
FU Chinese National Programs for High Technology Research and Development
[2010AA03A405, 2012AA062303]; National Natural Science Foundation of
China [U1202274, 51004033, 51204040, 50974035]; National Science and
Technology Support Program [2012BAE01B02]; Fundamental Research Funds
for the Central Universities [N100302005]; Doctoral Fund Project
[20120042110011]
FX This work was financially supported by the Chinese National Programs for
High Technology Research and Development (Nos. 2010AA03A405 and
2012AA062303), the National Natural Science Foundation of China (Nos.
U1202274, 51004033, 51204040, and 50974035), the National Science and
Technology Support Program (No. 2012BAE01B02), the Fundamental Research
Funds for the Central Universities (No. N100302005), and the Doctoral
Fund Project (No. 20120042110011).
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NR 17
TC 23
Z9 23
U1 5
U2 58
PU NONFERROUS METALS SOC CHINA
PI BEIJING
PA 12B FUXIN RD, BEIJING 100814, PEOPLES R CHINA
SN 1001-0521
EI 1867-7185
J9 RARE METALS
JI Rare Metals
PD JUL
PY 2016
VL 35
IS 7
BP 576
EP 580
DI 10.1007/s12598-014-0225-3
PG 5
Engineering
GA DP2DF
UT WOS:000378297600012
DA 2023-12-05
ER
PT J
AU Yan, W
Chen, W
Yang, Y
Lippold, C
McLean, A
AF Yan, W.
Chen, W.
Yang, Y.
Lippold, C.
McLean, A.
TI Evaluation of B2O3 as replacement for
CaF2 in CaO-Al2O3 based mould flux
LA English
DT Article
DE High aluminium steel; Fluoride free CaO-Al2O3 based mould flux; Heat
transfer; Crystallisation
ID HEAT-TRANSFER BEHAVIOR; CRYSTALLIZATION BEHAVIOR; THERMAL-CONDUCTIVITY;
FLUORIDE-FREE; NA2O; SLAG; SOLIDIFICATION; PERFORMANCE; VISCOSITY;
SYSTEM
AB In order to develop low fluoride or fluoride free CaO-Al2O3 based mould flux for
casting high aluminium steel, an investigation was carried out to study the effect
of substituting CaF2 with B2O3 on heat transfer and crystallisation behaviour of
CaO-Al2O3 based mould flux by employing a heat transfer simulator of mould flux and
a single hot thermocouple technique. The results showed that addition of CaF2
promoted heat transfer of CaO-Al2O3 based mould flux, which was opposite to the
effect of CaF2 on heat transfer in conventional CaO-SiO2 based mould flux. Addition
of CaF2 inhibited crystallisation of CaO-Al2O3 based mould flux by lowering the
start crystallisation temperature and prolonging the incubation time of
crystallisation. B2O3 showed similar effects to CaF2 on heat transfer and
crystallisation of CaO-Al2O3 based mould flux, but its ability to promote heat
transfer and suppress crystallisation was stronger than CaF2. Ca3B2O6 (melting
temperature 1480 degrees C) was found as the primary crystalline phase in fluoride
free CaO-Al2O3 based mould flux compared with the primary crystalline phase
Ca2Al3O6F (melting temperature 1507 degrees C) in fluoride bearing (20% CaF2) CaO-
Al2O3 based mould flux.
C1 [Yan, W.; Chen, W.] Univ Sci & Technol Beijing, State Key Lab Adv Met, Beijing
[Yan, W.; Yang, Y.; McLean, A.] Univ Toronto, Dept Mat Sci & Engn, Toronto, ON
M5S 3E4, Canada.
[Lippold, C.] Qingdao Stollberg & Samil Co Ltd, Qingdao 266300, Peoples R China.
Met, Beijing 100083, Peoples R China.; Yan, W (corresponding author), Univ Toronto,
Dept Mat Sci & Engn, Toronto, ON M5S 3E4, Canada.
Bui AH, 2006, MET MATER INT, V12, P435, DOI 10.1007/BF03027711
Chen LY, 2015, IRONMAK STEELMAK, V42, P105, DOI 10.1179/1743281214Y.0000000216
Choi SY, 2004, J NON-CRYST SOLIDS, V345, P157, DOI
10.1016/j.jnoncrysol.2004.08.015
Cramb AW, 2014, ISIJ INT, V54, P2665, DOI 10.2355/isijinternational.54.2665
He SP, 2009, INT J MIN MET MATER, V16, P261, DOI 10.1016/S1674-4799(09)60047-9
Kim Y, 2014, ISIJ INT, V54, P2077, DOI 10.2355/isijinternational.54.2077
Qi X, 2008, J NON-CRYST SOLIDS, V354, P5444, DOI
10.1016/j.jnoncrysol.2008.09.012
Scheller P, 2009, P 8 INT C MOLT SLAG, P1101
Shen Y. S., 2006, BASIC PRINCIPLE META
VDEh, 1995, SLAG ATLAS
Wei J, 2014, METALL MATER TRANS B, V45, P643, DOI 10.1007/s11663-013-9957-y
8620.2013.01.013, DOI 10.3969/J.ISSN.1003-8620.2013.01.013]
Yan W., 2015, IRONMAKING STEELMAKI
Yan W, 2013, METALL MATER TRANS B, V44, P1466, DOI 10.1007/s11663-013-9918-5
Zhou LJ, 2015, ISIJ INT, V55, P821, DOI 10.2355/isijinternational.55.821
NR 33
TC 23
Z9 26
U1 6
U2 31
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PY 2016
VL 43
IS 4
BP 316
EP 323
DI 10.1179/1743281215Y.0000000062
PG 8
GA DO8SF
UT WOS:000378053200007
DA 2023-12-05
ER
PT J
AU Mobasher, N
Bernal, SA
Kinoshita, H
Sharrad, CA
Provis, JL
AF Mobasher, Neda
Bernal, Susan A.
Kinoshita, Hajime
Sharrad, Clint A.
Provis, John L.
TI Gamma irradiation resistance of an early age slag-blended cement matrix
for nuclear waste encapsulation
SO JOURNAL OF MATERIALS RESEARCH
LA English
DT Article
ID HYDRATED PORTLAND CEMENTS; MAS NMR-SPECTROSCOPY; C-S-H; TEMPERATURE;
CARBONATION; RADIATION; CONCRETE; AL-27; STRENGTH; ALUMINUM
AB Irradiation is one of the characteristic conditions that nuclear wasteforms must
withstand to assure integrity during their service life. This study investigates
gamma irradiation resistance of an early age slag cement-based grout, which is of
interest for the nuclear industry as it is internationally used for encapsulation
of low and intermediate level radioactive wastes. The slag cement-based grout
withstands a gamma irradiation dose of 4.77 MGy over 256 h without reduction in its
compressive strength; however, some cracking of irradiated samples was identified.
The high strength retention is associated with the fact that the main hydration
product forming in this binder, a calcium aluminum silicate hydrate (C-A-S-H) type
gel, remains unmodified upon irradiation. Comparison with a heat-treated sample was
carried out to identify potential effects of the temperature rise during
irradiation exposure. The results suggested that formation of cracks is a combined
effect of radiolysis and heating upon irradiation exposure.
C1 [Mobasher, Neda; Bernal, Susan A.; Kinoshita, Hajime; Provis, John L.] Univ
Sheffield, Dept Mat Sci & Engn, Immobilisat Sci Lab, Sheffield S1 3JD, S Yorkshire,
England.
[Sharrad, Clint A.] Univ Manchester, Res Ctr Radwaste & Decommissioning, Dalton
Nucl Inst, Manchester M13 9PL, Lancs, England.
C3 University of Sheffield; University of Manchester
Immobilisat Sci Lab, Sheffield S1 3JD, S Yorkshire, England.
RI Provis, John/AAR-3260-2020; Sharrad, Clint/E-2499-2017; Provis, John
L/A-7631-2008; Bernal, Susan A/E-8938-2011
OI Provis, John/0000-0003-3372-8922; Sharrad, Clint/0000-0001-7372-8666;
Provis, John L/0000-0003-3372-8922; Kinoshita,
Hajime/0000-0001-8805-1774; Bernal, Susan A/0000-0002-9647-3106
FU EPSRC through the University of Sheffield/University of Manchester
Doctoral Training Centre 'Nuclear FiRST'
FX This study has been sponsored by EPSRC through the University of
Sheffield/University of Manchester Doctoral Training Centre 'Nuclear
FiRST'. The NMR spectra were collected using the EPSRC UK National
Solid-state NMR Service at Durham University, and the assistance of Dr
David Apperley is gratefully acknowledged. Special thanks are due to Dr
Ruth Edge and Dalton Cumbrian Facility for their great assistance in the
irradiation experiments.
10.1016/j.cemconres.2004.06.015
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10.1016/j.cemconres.2010.02.012
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10.1016/j.cemconres.2007.04.015
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10.1016/j.cemconres.2004.10.016
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NR 29
TC 23
Z9 24
U1 0
U2 29
PU CAMBRIDGE UNIV PRESS
PI NEW YORK
PA 32 AVENUE OF THE AMERICAS, NEW YORK, NY 10013-2473 USA
SN 0884-2914
EI 2044-5326
J9 J MATER RES
JI J. Mater. Res.
PD MAY 14
PY 2015
VL 30
IS 9
BP 1563
EP 1571
DI 10.1557/jmr.2014.404
PG 9
GA CJ1ZK
UT WOS:000355283500033
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Tsakiridis, PE
Oustadakis, P
Agatzini-Leonardou, S
AF Tsakiridis, P. E.
Oustadakis, P.
Agatzini-Leonardou, S.
TI Black Dross Leached Residue: An Alternative Raw Material for Portland
Cement Clinker
SO WASTE AND BIOMASS VALORIZATION
LA English
DT Article
DE Black dross leached residue; Raw meal; Clinker; Cement; Hydration
ID CHEMICAL-COMPOSITION; GRINDABILITY; BAUXITE; WASTES; SLAG
AB The possibility of adding an aluminium black dross leached residue (BDLR),
mainly consisted of spinel (Al2MgO4) and corundum (Al2O3), in the raw meal for the
production of Portland cement clinker was investigated. This leached residue was
obtained during the hydrothermal treatment of an aluminium black dross, formed
during aluminium scrap melting. The process consisted of crushing and grinding of
the as received dross, sieving it to recover the Al metal value, water leaching at
high temperature to dissolve the salts and, finally, aluminium recovery by alkaline
pressure leaching. Three samples of raw meals were prepared, one with ordinary raw
materials, as a reference sample ((PC) Ref), and two others with different content
(2 and 4 wt%) of BDLR ((PC) BD-2% and (PC) BD-42%). All raw meals were sintered at
1,450 degrees C and the produced clinkers were characterised by chemical analysis,
X-ray diffraction (XRD), thermogravimetric/differential thermal analysis (TG/DTA)
as well as scanning electron microscopy. The produced cements were tested by
determining their grindability, setting time, compressive strength and
expansibility. The hydration products were examined by XRD analysis at 2, 7 and 28
days. The results of the physico-mechanical tests showed that BDLR could be
utilized as a raw material in the cement clinker production, presenting a promising
alternative to disposal in landfills.
C1 [Tsakiridis, P. E.; Oustadakis, P.; Agatzini-Leonardou, S.] Natl Tech Univ
Athens, Met Lab, Dept Min & Met Engn, Athens 15780, Greece.
RP Tsakiridis, PE (corresponding author), Natl Tech Univ Athens, Met Lab, Dept Min
& Met Engn, 9 Iroon Polytech St, Athens 15780, Greece.
EM ptsakiri@central.ntua.gr
RI Tsakiridis, Petros/AAH-6232-2019; Oustadakis, Paschalis/JAZ-9883-2023
OI Tsakiridis, Petros/0000-0002-2180-2454; Oustadakis,
Paschalis/0000-0003-2693-1965
CR Al-Dhamri H, 2010, J HAZARD MATER, V179, P852, DOI 10.1016/j.jhazmat.2010.03.083
[Anonymous], CEMENT DATA BOOK
*ASTM, 2000, C20400 ASTM
British Standards Institution, 2005, 1961 EN BRIT STAND I
British Standards Institution, 2005, 1963 EN BRIT STAND I
FRIGIONE G, 1983, CEMENT CONCRETE RES, V13, P483, DOI 10.1016/0008-
8846(83)90006-6
GOUDA GR, 1979, CEMENT CONCRETE RES, V9, P209, DOI 10.1016/0008-8846(79)90027-9
Lorber K.E., 2010, 2 INT C HAZ IND WAST
8846(00)00272-6
10.1016/j.resconrec.2013.01.005
Tokyay M, 1999, CEMENT CONCRETE RES, V29, P531, DOI 10.1016/S0008-8846(98)00219-
1
NR 20
TC 23
Z9 24
U1 3
U2 54
PU SPRINGER
PI DORDRECHT
SN 1877-2641
EI 1877-265X
J9 WASTE BIOMASS VALORI
JI Waste Biomass Valorization
PD DEC
PY 2014
VL 5
IS 6
BP 973
EP 983
DI 10.1007/s12649-014-9313-8
PG 11
GA AY7DQ
UT WOS:000347722000007
DA 2023-12-05
ER
PT J
AU Collier, NC
Milestone, NB
Gordon, LE
Ko, SC
AF Collier, N. C.
Milestone, N. B.
Gordon, L. E.
Ko, S-C
TI The suitability of a supersulfated cement for nuclear waste
immobilisation
SO JOURNAL OF NUCLEAR MATERIALS
LA English
DT Article
ID PORTLAND-CEMENT; COMPOSITE; ENCAPSULATION; CORROSION; MATRICES;
ALUMINUM; PHASES; FLOC
AB Composite cements based on ordinary Portland cement are used in the UK as
immobilisation matrices for low and intermediate level nuclear wastes. However, the
high pore solution pH causes corrosion of some metallic wastes and undesirable
expansive reactions, which has led to alternative cementing systems being examined.
We have investigated the physical, chemical and microstructural properties of a
supersulfated cement in order to determine its applicability for use in nuclear
waste encapsulation. The hardened supersulfated cement paste appeared to have
properties desirable for use in producing encapsulation matrices, but the high
powder specific surface resulted in a matrix with high porosity. Ettringite and
calcium silicate hydrate were the main phases formed in the hardened cement paste
and anhydrite was present in excess. The maximum rate of heat output during
hydration of the supersulfated cement paste was slightly higher than that of a 9:1
blastfurnace slag: ordinary Portland cement paste commonly used by the UK nuclear
waste processing industry, although the total heat output of the supersulfated
cement paste was lower. The pH was also significantly lower in the supersulfated
cement paste. Aluminium hydroxide was formed on the surface of aluminium metal
encapsulated in the cement paste and ettringite was detected between the aluminium
hydroxide and the hardened cement paste. (C) 2014 Elsevier B. V. All rights
reserved.
C1 [Collier, N. C.; Milestone, N. B.; Gordon, L. E.] Univ Sheffield, Dept Mat Sci &
Engn, Immobilisat Sci Lab, Sheffield S1 3JD, S Yorkshire, England.
[Milestone, N. B.] Callaghan Innovat, Lower Hutt 5040, New Zealand.
[Gordon, L. E.] Univ Melbourne, Geopolymer & Minerals Proc Grp, Dept Chem &
Biomol Engn, Parkville, Vic 3010, Australia.
[Ko, S-C] Holcim Technol Ltd, CH-8050 Zurich, Switzerland.
C3 University of Sheffield; Callaghan Innovation; University of Melbourne
RP Collier, NC (corresponding author), Univ Sheffield, Dept Mat Sci & Engn,
Immobilisat Sci Lab, Mappin St, Sheffield S1 3JD, S Yorkshire, England.
EM nick.collier@sheffield.ac.uk
OI Collier, Nicholas/0000-0003-2491-829X
CR Angus M.J., 2010, WM2010 C PHOEN US MA
Bai Y, 2006, MATER RES SOC SYMP P, V932, P759
Borges P. R., 2007, THESIS U SHEFFIELD S
*BRIT STAND I, 2004, 4248 BS
Civil and Marine, 2007, PROD US GGBS
10.1016/j.cemconres.2008.02.012
Collier NC, 2010, ADV APPL CERAM, V109, P269, DOI
10.1179/174367509X12447975734276
Collier NC, 2006, WASTE MANAGE, V26, P769, DOI 10.1016/j.wasman.2006.01.031
Collier NC, 2009, MATER RES SOC SYMP P, V1124, P345
Glasser FP, 1997, J HAZARD MATER, V52, P151, DOI 10.1016/S0304-3894(96)01805-5
Glasser FP, 2001, MINERAL MAG, V65, P621, DOI 10.1180/002646101317018442
8846(92)90058-4
Gordon LE, 2008, MATER RES SOC SYMP P, V1107, P135, DOI 10.1557/PROC-1107-135
Green KM, 1999, REV SCI INSTRUM, V70, P3397, DOI 10.1063/1.1149926
10.1016/j.cemconres.2008.03.004
Hayes M., 2014, COMMUNICATION
HUTSON GV, 1996, NUCL FUEL CYCLE ORE, P161
10.1016/j.cemconres.2010.11.012
Milestone NB, 2006, MATER RES SOC SYMP P, V932, P673
Richardson I. G., 1993, CEMENT CONCRETE RES, V23, P131
Setiadi A, 2006, ADV APPL CERAM, V105, P191, DOI 10.1179/174367606X120142
Utton C.A., 2006, THESIS U SHEFFIELD S
WILDING CR, 1992, CEMENT CONCRETE RES, V22, P299, DOI 10.1016/0008-
8846(92)90069-8
10.1016/j.cemconres.2009.08.014
NR 34
TC 23
Z9 25
U1 1
U2 37
PU ELSEVIER
PI AMSTERDAM
SN 0022-3115
EI 1873-4820
J9 J NUCL MATER
JI J. Nucl. Mater.
PD SEP
PY 2014
VL 452
IS 1-3
BP 457
EP 464
DI 10.1016/j.jnucmat.2014.05.078
PG 8
WC Materials Science, Multidisciplinary; Nuclear Science & Technology
SC Materials Science; Nuclear Science & Technology
GA AM2CU
UT WOS:000339657200066
DA 2023-12-05
ER
PT J
AU Adamczyk, B
Brenneis, R
Adam, C
Mudersbach, D
AF Adamczyk, B.
Brenneis, R.
Adam, C.
Mudersbach, D.
TI Recovery of Chromium from AOD-Converter Slags
LA English
DT Article
DE arc furnace; by-product; chromium recovery; high-alloyed steel;
reductive melting; slag treatment; slag; thermochemical treatment
ID OXIDE REDUCTION; SILICON; CARBON; IRON
AB Slags from the production of high-alloyed steel contain both chemically bound
chromium (mainly as Cr(2)O(3)) in the mineral fraction and elemental chromium in
the metallic remainders. Thermochemical post treatment of the slag in an electric
arc furnace under reducing conditions enables the nearly complete recovery of the
total amount of chromium in form of a metallic alloy. The best results were
achieved by resistance melting (submerged electrodes) with addition of a reducing
agent into the melt. The efficiencies of the reducing agents carbon, aluminium,
silicon (as ferrosilicon) and silicon carbide were investigated and compared. As
aluminium is the strongest reducing agent, it is less selective and reduces much
more SiO(2) than Cr(2)O(3). While SiC shows only low reactivity because of its high
thermal resistance, carbon and silicon had the highest reducing potentials: More
than 97% of the chemically bound chromium can be recovered by application of these
reducing agents. Due to the high temperature required for the reduction of the
chromium compounds, the reduction of SiO(2) as an undesired side reaction cannot be
avoided. However, compared with mechanical procedures that are limited to the
recovery of the metallic remainders, the total chromium recovery can be
significantly increased by the described reductive melting procedure.
C1 [Adamczyk, B.; Brenneis, R.; Adam, C.] BAM Fed Inst Mat Res & Testing, D-12489
Berlin, Germany.
[Mudersbach, D.] FEhS Bldg Mat Inst, D-47229 Duisburg, Germany.
C3 Federal Institute for Materials Research & Testing
RP Adamczyk, B (corresponding author), BAM Fed Inst Mat Res & Testing, Richard
Willstatter Str 11, D-12489 Berlin, Germany.
EM burkart.adamczyk@bam.de
RI Adam, Christian/A-8655-2011
OI Adam, Christian/0000-0002-3356-4617
FU European Union [LIFE03ENV/D/043-RecArc]
FX We gratefully thank the European Union for the financial support within
the LIFE-environment program (LIFE03ENV/D/043-RecArc).
CR ADAMCZYK B, 2004, TMS INASMET, V3, P2245
Adamczyk B, 2009, CHEM-ING-TECH, V81, P479, DOI 10.1002/cite.200800187
*DIN, 38414 DIN
*EN, 1744 EN
FAULSTICH M, 1992, RUCKSTANDE MULLVERBR, P703
GEISLER J, 1984, SCHLACKEN BEI HERSTE, P221
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Hino M, 1998, METALL MATER TRANS B, V29, P351, DOI 10.1007/s11663-998-0112-0
KLEY G, 1994, MULL ABFALL S, V31, P146
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Mashanyare HP, 1997, MINER ENG, V10, P1253, DOI 10.1016/S0892-6875(97)00111-8
Mori T, 2007, ISIJ INT, V47, P1387, DOI 10.2355/isijinternational.47.1387
MUDERSBACH D, 2009, REPORTS FEHS I, V16, P13
*OUT RES OY, HSC CHEM 5 11
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10.1016/j.minpro.2004.08.013
VERSTEYL LA, 2005, SCHRIFTENREIHE FEHS
NR 20
TC 23
Z9 24
U1 0
U2 25
PU WILEY-BLACKWELL PUBLISHING, INC
PI MALDEN
SN 1611-3683
J9 STEEL RES INT
JI Steel Res. Int.
PD DEC
PY 2010
VL 81
IS 12
BP 1078
EP 1083
DI 10.1002/srin.201000193
PG 6
GA 702LK
UT WOS:000285896000006
DA 2023-12-05
ER
PT C
AU Biswas, S
Satapathy, A
Patnaik, A
AF Biswas, Sandhyarani
Satapathy, Alok
Patnaik, Amar
BA Lee, JH
BF Lee, JH
TI Effect of Ceramic Fillers on Mechanical Properties of Bamboo Fiber
Reinforced Epoxy Composites: A Comparative Study
SO MULTI-FUNCTIONAL MATERIALS AND STRUCTURES III, PTS 1 AND 2
SE Advanced Materials Research
LA English
CT 3rd International Conference on Multi-Functional Materials and
Structures
CY SEP 14-18, 2010
CL Chonbuk Natl Univ, Jeollabuk do, Jeonju, SOUTH KOREA
HO Chonbuk Natl Univ, Jeollabuk do
DE Ceramic filler; Epoxy resin; Bamboo fiber; Glass fiber; Mechanical
properties
AB In order to obtain the favoured material properties for a particular
application, it is important to know how the material performance changes with the
filler content under given loading conditions. In this study, a series of bamboo
fiber reinforced epoxy composites are fabricated using conventional filler
(aluminium oxide (Al2O3) and silicon carbide (SiC) and industrial wastes (red mud
and copper slag) particles as filler materials. By incorporating the chosen
particulate fillers into the bamboo-fiber reinforced epoxy, synergistic effects, as
expected are achieved in the form of modified mechanical properties. Inclusion of
fiber in neat epoxy improved the load bearing capacity (tensile strength) and the
ability to withstand bending (flexural strength) of the composites. But with the
incorporation of particulate fillers, the tensile strengths of the composites are
found to be decreasing in most of the cases. Among the particulate filled bamboo-
epoxy composites, least value of void content are recorded for composites with
silicon carbide filling and for the composites with glass fiber reinforcement
minimum void fraction is noted for red mud filling. The effects of these four
different ceramics on the mechanical properties of bamboo-epoxy composites are
investigated and the conclusions drawn from the above investigation are discussed.
C1 [Biswas, Sandhyarani; Satapathy, Alok] Natl Inst Technol, Dept Mech Engn,
Rourkela 769008, India.
[Patnaik, Amar] Natl Inst Technol, Dept Mech Engn, Hamirpur 177005, India.
Technology Rourkela; National Institute of Technology (NIT System);
National Institute of Technology Hamirpur
RP Biswas, S (corresponding author), Natl Inst Technol, Dept Mech Engn, Rourkela
769008, India.
EM sandhya_biswas@yahoo.co.in; satapathy.alok@gmail.com; amar_mech@sify.com
RI Patnaik, Amar/GZM-0065-2022; Satapathy, Alok/N-4297-2017
OI Patnaik, Amar/0000-0001-9506-782X; Biswas,
Sandhyarani/0000-0003-4562-248X
CR Jiang L, 1999, ANGEW MAKROMOL CHEM, V268, P18
Kahraman R., 2005, INT J POLYM MATER, V54, P483
Takagi H, 2004, JSME INT J A-SOLID M, V47, P551, DOI 10.1299/jsmea.47.551
Takagi H., 2005, P 3 INT C EC STOCKH, V14, P1
Torres FG, 2005, POLYM TEST, V24, P694, DOI 10.1016/j.polymertesting.2005.05.004
NR 5
TC 23
Z9 23
U1 0
U2 9
PU TRANS TECH PUBLICATIONS LTD
PI DURNTEN-ZURICH
PA KREUZSTRASSE 10, 8635 DURNTEN-ZURICH, SWITZERLAND
SN 1022-6680
BN 978-0-87849-246-6
J9 ADV MATER RES-SWITZ
PY 2010
VL 123-125
BP 1031
EP +
DI 10.4028/www.scientific.net/AMR.123-125.1031
PG 2
GA BUH15
UT WOS:000289269600252
DA 2023-12-05
ER
PT J
AU Nakahira, A
Naganuma, H
Kubo, T
Yamasaki, Y
AF Nakahira, Atsushi
Naganuma, Hirokazu
Kubo, Takashi
Yamasaki, Yuki
TI Synthesis of monolithic tobermorite from blast furnace slag and
evaluation of its Pb removal ability
SO JOURNAL OF THE CERAMIC SOCIETY OF JAPAN
LA English
DT Article
DE blast furnace slag; aluminum substituted tobermorite; Pb removal;
recycle
AB Synthesis of aluminum substituted tobermorite from blast furnace slag was
attempted. Mixture of blast furnace slag and quartz controlled Ca/ (Al + Si) ratio
for 0.8 to 1.0 was treated by a rotary hydrothermal treatment for 24 h at 453 K.
Obtained samples were characterized by X-ray diffraction (XRD) and scanning
electron microscope (SEM) observation. Monolithic tobermorite was successfully
synthesized with 0.8 of Ca/ (Al + Si) ratio by this rotary hydrothermal treatment,
whereas monolithic tobermorite could not be synthesized by the conventional static
hydrothermal treatments, leading to the mixture of tobermorite and other calcium
silicate containing unreacted SiO2. Pb removal ability was investigated for this
monolithic tobermorite obtained by this rotary hydrothermal method from blast
furnace slag. It was found that monolithic tobermorite had a good Pb removal
ability. This result shows that the synthesis of tobermorite is useful as a recycle
of blast furnace slag. (c) 2008 The Ceramic Society of Japan. All rights reserved.
C1 [Yamasaki, Yuki] Hosei Univ, Fac Econ, Machida, Tokyo 1940298, Japan.
[Nakahira, Atsushi; Naganuma, Hirokazu; Kubo, Takashi] Osaka Prefecture Univ,
Dept Mat Sci, Sakai, Osaka 5998531, Japan.
C3 Hosei University; Osaka Metropolitan University
RP Yamasaki, Y (corresponding author), Hosei Univ, Fac Econ, 4342 Aihara Cho,
Machida, Tokyo 1940298, Japan.
CR Coleman NJ, 2006, WASTE MANAGE, V26, P260, DOI 10.1016/j.wasman.2005.01.019
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2
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8846(98)00111-2
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KORNARNENI S, 1989, J AM CERAM SOC, V72, P1668
OKADA Y, 1994, NIPPON SERAM KYO GAK, V102, P1148
YASUE T, 1993, J CERAM SOC JPN, V101, P1255
YASUE T, 1998, INORGANIC MAT, V5
NR 10
TC 23
Z9 23
U1 3
U2 21
PU CERAMIC SOC JAPAN-NIPPON SERAMIKKUSU KYOKAI
PI TOKYO
PA 22-17, HYAKUNIN-CHO 2-CHOME, SHINJUKU-KU, TOKYO, 169-0073, JAPAN
SN 1882-0743
EI 1348-6535
J9 J CERAM SOC JPN
JI J. Ceram. Soc. Jpn.
PD MAR
PY 2008
VL 116
IS 1351
BP 500
EP 504
DI 10.2109/jcersj2.116.500
PG 5
GA 277KT
UT WOS:000254212100030
OA Bronze
DA 2023-12-05
ER
PT C
AU Choate, W
Green, J
AF Choate, William
Green, John
BE Galloway, TJ
TI Technoeconomic assessment of the carbothermic reduction process for
aluminum production
SO LIGHT METALS 2006, VOL 2: ALUMINUM REDUCTION TECHNOLOGY
SE Light Metals
LA English
CT Technical Session on Light Metals 2006 held at the 135th TMS Annual
Meeting
CY MAR 12-16, 2006
CL San Antonio, TX
DE carbothermic; Hall-Heroult; mini-mill; wetted cathode; inert anode
AB In pursuit of the aluminum industry Vision and Roadmap goals, the Department of
Energy has partially supported a consortium of Alcoa and Elkem in the development
of the Aluminum Carbothermic Technology - Advanced Reduction Process (ACT-ARP),
which promises significant energy and emission reductions. This report explores the
progress of the ACT-ARP as a potential replacement for the Hall-Heroult process in
the context of several evolving Hall-Heroult development scenarios. Considerable
progress has been made and demonstrated, including new furnace wall designs
integral to successful operation of Stage I reactor, operational characteristics of
vapor recovery reactor and aluminum decarbonization reactor, as well as significant
modeling and simulation. Despite these considerable accomplishments, there are
still formidable technical and economic challenges to overcome before the ACT-ARP
can replace the conventional Hall-Heroult process, such as slag and scale
formation, metal and carbon quality issues, mini-mill operation, etc. All these and
other issues will be discussed.
C1 [Choate, William] BCS Inc, 5550 Sterrett Pl,Suite 306, Columbia, MD 21044 USA.
[Green, John] JASG Consulting, Ellicott City, MD 21042 USA.
RP Choate, W (corresponding author), BCS Inc, 5550 Sterrett Pl,Suite 306, Columbia,
MD 21044 USA.
FU Department of Energy, through its Oak Ridge National Laboratory
FX John Green acknowledges the financial support of the Department of
Energy, through its Oak Ridge National Laboratory, for this study. Both
authors also greatly appreciate the personal interest of Charles
Sorrell, Pete Angelini and Isaac Chan. Stimulating discussions with
several colleagues are gratefully acknowledged, especially Wayne Hayden.
The support of Rennie Friedman, Rajita Majumdar and Borys Marizza at
BCS, Inc., in assembling the final manuscript is also appreciated.
CR *AL ASS INC, AL STAT REV 2004
*AL ASS INC, AL IND TECHN ROADM
BROWN GD, 1998, QUEENST AL SMELT C 2
BRUNO M, 2004, 2004 ANN PROJ REV OC
CHAOTE WT, 2003, US ENERGY REQUIREMEN
CHOATE WT, 2005, WILL NEW TECHNOLOGIE
*DEP EN IND TECHN, 2005, DEFC36002D13900 DEP
GARCIAOSORIO V, DYNAMIC MODEL VAPOR
GREEN JAS, 2005, 4000031177 DEP EN IN
JOHANSEN K, CARBOTHERMIC ALUMINU
KJAR T, 2002, COMMUNICATION APR
LEEUWEN T, 2000, ALUMINUM REVOLU 0622
LIU FQ, 2005, COMMUNICATION FEB
NR 13
TC 23
Z9 25
U1 0
U2 5
PI WARRENDALE
SN 0147-0809
J9 LIGHT MET
PY 2006
BP 445
EP +
PG 2
WC Electrochemistry; Metallurgy & Metallurgical Engineering
SC Electrochemistry; Metallurgy & Metallurgical Engineering
GA BEQ58
UT WOS:000238943600046
DA 2023-12-05
ER
PT J
AU Kuo, YM
Lin, TC
Tsai, PJ
AF Kuo, YM
Lin, TC
Tsai, PJ
TI Effect of SiO2 on immobilization of metals and encapsulation
of a glass network in slag
SO JOURNAL OF THE AIR & WASTE MANAGEMENT ASSOCIATION
LA English
DT Article
ID FLY-ASH; WASTE; VITRIFICATION; CERAMICS; RESIDUES
AB The final disposal of ash from an incinerator is of special concern because of
the possibility of its releasing toxic substances. Melting/vitrification has been
regarded as a prospective technology of ash treatment. The object of this
investigation was to evaluate the effect of silica (SiO2) addition on the
immobilization of hazardous metals and the encapsulation of a glass network during
the vitrification process. Four specimens with SiO2/fly ash mixing ratios of 0,
0.1, 0.2, and 0.3, respectively, were tested. The mobility of metals in slag was
then estimated by a sequential extraction procedure. X-ray diffraction analysis
indicates that SiO2 leads to the polymerization of silicates. The encapsulation of
aluminum, calcium, and magnesium would not be observed unless adequate amount of
SiO2 was added. It was also found that SiO2 addition enhances the formation of a
compact and interconnected glass network structure and, thus, contributes to the
chemical stability of metals in slag. After vitrification, the mobility of cadmium,
copper, iron, chromium, nickel, lead, and zinc was significantly reduced. However,
there is no significant correlation between the immobilization of these metals and
the addition of SiO2.
C1 Natl Cheng Kung Univ, Dept Environm Engn, Tainan 70101, Taiwan.
Natl Cheng Kung Univ, Grad Inst Environm & Occupat Hlth, Coll Med, Tainan 70101,
Taiwan.
C3 National Cheng Kung University; National Cheng Kung University
RP Lin, TC (corresponding author), Natl Cheng Kung Univ, Dept Environm Engn, 1 Univ
Rd, Tainan 70101, Taiwan.
EM tachang@mail.ncku.edu.tw
CR Barbieri L, 2000, J EUR CERAM SOC, V20, P1637, DOI 10.1016/S0955-2219(00)00032-7
Barbieri L, 1999, FUEL, V78, P271, DOI 10.1016/S0016-2361(98)00134-3
Ecke H, 2001, ENVIRON SCI TECHNOL, V35, P1531, DOI 10.1021/es0001759
*EPA EX YUAN, 1974, EPA070020 EX YUAN
Haugsten KE, 2000, WASTE MANAGE, V20, P167, DOI 10.1016/S0956-053X(99)00325-6
Ito T, 1996, WASTE MANAGE, V16, P453, DOI 10.1016/S0956-053X(96)00090-6
Kersten M., 1995, P234
Kinto K, 1996, WASTE MANAGE, V16, P423, DOI 10.1016/S0956-053X(96)00088-8
Kuo YM, 2003, CHEMOSPHERE, V51, P313, DOI 10.1016/S0045-6535(02)00852-4
Li CT, 2003, IND ENG CHEM RES, V42, P2306, DOI 10.1021/ie0208164
Park YJ, 2002, J HAZARD MATER, V91, P83, DOI 10.1016/S0304-3894(01)00362-4
Sheng JW, 2001, FUEL, V80, P1365, DOI 10.1016/S0016-2361(01)00022-9
Spence RD, 1999, WASTE MANAGE, V19, P453, DOI 10.1016/S0956-053X(99)00237-8
VOGEL W, 1992, GLASS CHEM, P34
Wiles CC, 1996, J HAZARD MATER, V47, P325, DOI 10.1016/0304-3894(95)00120-4
Wunsch P, 1996, CHEMOSPHERE, V32, P2211, DOI 10.1016/0045-6535(96)00123-3
NR 18
TC 23
Z9 23
U1 1
U2 24
PI PHILADELPHIA
SN 1096-2247
EI 2162-2906
J9 J AIR WASTE MANAGE
JI J. Air Waste Manage. Assoc.
PD NOV
PY 2003
VL 53
IS 11
BP 1412
EP 1416
DI 10.1080/10473289.2003.10466307
PG 5
WC Engineering, Environmental; Environmental Sciences; Meteorology &
Atmospheric Sciences
SC Engineering; Environmental Sciences & Ecology; Meteorology & Atmospheric
Sciences
GA 738NK
UT WOS:000186294600016
PM 14649761
DA 2023-12-05
ER
PT J
AU Shibata, E
Egawa, S
Nakamura, T
AF Shibata, E
Egawa, S
Nakamura, T
TI Reduction behavior of chromium oxide in molten slag using aluminum,
ferrosilicon and graphite
LA English
DT Article
DE smelting reduction; chromium oxide; aluminum; ferrosilicon; graphite;
molten slag; X-ray observation
ID SMELTING REDUCTION; IRON-OXIDE; CARBON; ORE
AB To reduce chromium in stainless steel slag and simultaneously recover chromium
as a ferroalloy for the steel making industry, the direct smelting reduction of
chromium oxide in molten slag was investigated by small furnace experiments.
Thermodynamic equilibrium calculations were also carried out to suggest the limit
of reduction of CrOx, in the slags. Aluminum, ferrosilicon and graphite were used
as reductants under conditions of 1 723-1823 K and various slag compositions. In
the experiments, the formation of high Al2O3 solid phase in the upper and middle
parts of slag prevented uniform reduction when aluminum was added as a reductant,
although FeO and CrOx were reduced drastically to a low content compared with the
cases of ferrosilicon and graphite except for the lower part of slag melt. The low
content of CrOx by aluminum was about 0.01 mass% which was about one order higher
than calculated thermodynamic equilibrium one. The reductions of FeO and CrOx by
aluminum were promoted to the lower part of slag with the increase in temperature
and CaO/SiO2, ratio because of the increase in fluidity of slag. A liquid metal
containing chromium was formed and precipitated on the bottom of slag during the
reduction. The formation behavior of metal drop was observed directly by an X-ray
fluoroscopy technique.
C1 Tohoku Univ, Inst Multidisciplinary Res Adv Mat, Sendai, Miyagi 9808577, Japan.
RP Shibata, E (corresponding author), Tohoku Univ, Inst Multidisciplinary Res Adv
Mat, Sendai, Miyagi 9808577, Japan.
CR FURUKAWA T, 1999, B IRON STEEL I JPN, V4, P391
HARA S, 1990, TETSU TO HAGANE, V76, P360, DOI 10.2355/tetsutohagane1955.76.3_360
*JAP SOC PROM SCI, 1988, PHYS PROP HIGH TEMP, P131
KATAYAMA H, 1990, TETSU TO HAGANE, V76, P1855, DOI
10.2355/tetsutohagane1955.76.11_1855
MUKAI K, 1992, TETSU TO HAGANE, V78, P1682
Nakasuga T, 2000, TETSU TO HAGANE, V86, P499
Ogawa Y, 2001, TETSU TO HAGANE, V87, P14
SHIMOMURA Y, 1998, TEKKOHKAI, V11, P11
TAKAOKA T, 1990, TETSU TO HAGANE, V76, P1839, DOI
10.2355/tetsutohagane1955.76.11_1839
NR 11
TC 23
Z9 23
U1 0
U2 27
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2002
VL 42
IS 6
BP 609
EP 613
PG 5
GA 563RX
UT WOS:000176270300006
OA gold
DA 2023-12-05
ER
PT J
AU Chudek, JA
Hunter, G
Jones, MR
Scrimgeour, SN
Hewlett, PC
Kudryavtsev, AB
AF Chudek, JA
Hunter, G
Jones, MR
Scrimgeour, SN
Hewlett, PC
Kudryavtsev, AB
TI Aluminium-27 solid state NMR spectroscopic studies of chloride binding
in Portland cement and blends
LA English
DT Article
ID HIGH-RESOLUTION NMR; AL-27 NMR; CALCIUM ALUMINATE; QUADRUPOLAR NUCLEI;
CONCRETE; INGRESS; MAS; CORROSION; HYDRATION; SI-29
AB Alumina-rich pozzolanic and latent hydraulic binders such as pulverised fuel
ash, metakaolin, and ground granulated blast furnace slag, together with silica
fume, are frequently added to Portland cement concrete to improve performance and
to retard chloride ingress and thereby inhibit chloride-induced corrosion of the
carbon steel reinforcement. Al-27(H-1) MAS and CP/MAS NMR spectroscopies have been
used to follow both the hydration processes of the cement blends and the
interactions of chloride ion with the hydrated aluminium species. The spectra of
the hydrated aluminate phases were interpretable on the basis that the AFt
(Aluminate Ferrite tri-) phase ettringite, C(6)AS(3)H(32)(3CaO . Al2O3. 3CaSO(4).
32H(2)O, or C(3)A . 3CaSO(4). 32H(2)O), and the AFm (Aluminate Ferrite mono-)
phases calcium mono-sulphoaluminate, C(4)ASH(12) (3CaO . Al2O3. CaSO4. 12H(2)O, or
C(3)A . CaSO4. 12H(2)O), and the lamellar tetracalcium aluminate hydrate,
C(4)AH(13) (3CaO . Al2O3. Ca(OH)(2). 12H(2)O,or C(3)A . Ca(OH)(2). xH(2)O) were
present as the only hydrated species containing octahedrally-coordinated aluminium.
Inall cases, only the AFm phase Friedel's salt (3CaO . Al2O3. CaCl2. 10H(2)O, or
C(3)A . CaCl2.10H(2)O) could be identified as the major chloroaluminate phase
produced by the interactions of the cement pastes with chloride ion, (C)2000 Kluwer
Academic Publishers.
C1 Univ Dundee, Dept Chem, Dundee DD1 4HN, Scotland.
Univ Dundee, Dept Civil Engn, Dundee DD1 4HN, Scotland.
British Board Agrement, Watford WD2 7NG, Herts, England.
D Mendeleev Univ Chem Technol Russia, Analyt Ctr, Moscow 125190, Russia.
C3 University of Dundee; University of Dundee; Mendeleev University of
Chemical Technology of Russia
RP Hunter, G (corresponding author), Univ Dundee, Dept Chem, Dundee DD1 4HN,
Scotland.
OI Jones, Roderick/0000-0002-5844-2122
CR AMOUREUX JP, 1994, APPL NMR SPECTROSCOP, P481
[Anonymous], MAG CONCR RES, DOI [10.1680/macr.1962.14.42.143, DOI
10.1680/MACR.1962.14.42.143]
[Anonymous], LEAS CHEM CEMENT CON
BARRAS J, 1994, J CHEM SOC FARADAY T, V90, P3719, DOI 10.1039/ft9949003719
BARRIE PJ, 1993, CHEM PHYS LETT, V208, P486, DOI 10.1016/0009-2614(93)87177-5
BASTOW TJ, 1994, MATER LETT, V18, P197, DOI 10.1016/0167-577X(94)90230-5
*BRIT STAND I, 1995, 1971 DDENV BSI
CONSHOHOCKEN W, 1995, 595M ASTM
Daimdot D, 1993, CEMENT CONCRETE RES, V23, P221
2
9
DHIR RK, 1993, P I CIVIL ENG-STR B, V99, P167, DOI 10.1680/istbu.1993.23375
DHIR RK, 1997, P INT ASH S LEX KENT
FENZKE D, 1984, CHEM PHYS LETT, V111, P171, DOI 10.1016/0009-2614(84)80458-3
FREUDE D, 1985, CHEM PHYS LETT, V119, P365, DOI 10.1016/0009-2614(85)80434-6
FYFFE CA, 1983, SOLID STATE NMR CHEM
Glass GK, 1997, MAG CONCRETE RES, V49, P323, DOI 10.1680/macr.1997.49.181.323
GONI S, 1991, CEMENT CONCRETE RES, V21, P635, DOI 10.1016/0008-8846(91)90114-W
Hanneman RA, 1995, SOCIOL METHODOL, V25, P1, DOI 10.2307/271060
JACKSON PJ, 1998, LEAS CHEM CEMENT CON, P33
6
JONES MR, 1997, CEMENT CONCRETE RES, V27, P789
Kudryavtsev AB, 1997, CEMENT CONCRETE RES, V27, P501, DOI 10.1016/S0008-
8846(97)00044-6
KUDRYAVTSEV AB, 1990, CEMENT CONCRETE RES, V20, P407, DOI 10.1016/0008-
8846(90)90031-R
KUNDLA E, 1981, CHEM PHYS LETT, V83, P229, DOI 10.1016/0009-2614(81)85451-6
MAN PP, 1985, CHEM PHYS LETT, V119, P143
MASSAZZA F, 1998, LEAS CHEM CEMENT CON, P518
MASSIOT D, 1994, APPL NMR SPECTROSCOP, P157
MORANVILLEREGOU.M, 1998, LEAS CHEM CEMENT CON, P654
MORTUZA MG, 1993, APPL MAGN RESON, V4, P89, DOI 10.1007/BF03162557
MULLER D, 1994, APPL NMR SPECTROSCOP, P259
ODLER I, 1998, LEAS CHEM CEMENT CON, P260
2916.1993.tb07765.x
SAMOSON A, 1983, PHYS REV B, V28, P6567, DOI 10.1103/PhysRevB.28.6567
Sanjuan MA, 1997, J MATER SCI, V32, P6207, DOI 10.1023/A:1018624824702
Scrivener K.L., 1998, LEAS CHEM CEMENT CON, P723
8846(96)85009-5
Tang F.J., 1988, Adv. Cem. Res, V1, P67, DOI [10.1680/adcr.1988.1.2.67, DOI
10.1680/ADCR.1988.1.2.67]
TAYLOR H, 1997, CLAIM COUNTRYSIDE, pCH6
ZHANG MH, 1995, CEMENT CONCRETE RES, V25, P1713, DOI 10.1016/0008-8846(95)00167-
0
NR 45
TC 23
Z9 23
U1 0
U2 24
PI DORDRECHT
SN 0022-2461
J9 J MATER SCI
JI J. Mater. Sci.
PD SEP 1
PY 2000
VL 35
IS 17
BP 4275
EP 4288
DI 10.1023/A:1004824100029
PG 14
GA 364FU
UT WOS:000089882000008
DA 2023-12-05
ER
PT J
AU Nishi, T
Shinme, K
AF Nishi, T
Shinme, K
TI Variation of inclusion morphology in molten Fe-Ni alloys
LA Japanese
DT Article
DE inclusion; morphology control; Fe-Ni alloy; deoxidation; slag; spinel
ID DEOXIDATION EQUILIBRIUM; THERMODYNAMICS; DISSOLUTION; MAGNESIUM;
ALUMINUM; NICKEL; IRON
AB The morphology changes of the inclusions in molten Fe-42mass%Ni alloy were
investigated in the Si-Mn complex deoxidation experiments under CaO-SiO(2)-
Al(2)O(3)-MgO slags in order to clarify the mechanism of the morphology control of
the inclusions by means of the slag-metal-inclusions reactions,
An increase in the Al(2)O(3) content of SiO(2)-MnO inclusions was observed in
the process of the deoxidation with time. As the result, SiO(2)-MnO-Al(2)O(3)
ductile inclusions could be produced in Fe-Ni alloy. This was caused by the
decomposition of Al(2)O(3) in slag, and the reaction between aluminum in molten
alloy and the inclusions. An increasing amount of MgO in the inclusions was also
observed simultaneously in that process. That phenomenon caused the formation of
MgO-Al(2)O(3) spinel inclusion, It was presumed that transportation of Mg from
slags to inclusions would be occurred as the result of the chemical reaction in the
same manner as that of aluminum.
C1 Sumitomo Met Ind Ltd, Corp Res & Dev Labs, Hasaki, Ibaraki 31402, Japan.
C3 Nippon Steel & Sumitomo Metal Corporation
RP Nishi, T (corresponding author), Sumitomo Met Ind Ltd, Corp Res & Dev Labs, 16-1
Oaza Sunayama, Hasaki, Ibaraki 31402, Japan.
CR [Anonymous], 1979, METALLURGICAL THERMO
BELTON GR, 1967, J PHYS CHEM-US, V71, P1403, DOI 10.1021/j100864a034
Ishii FJ, 1996, ISIJ INT, V36, P25, DOI 10.2355/isijinternational.36.25
SAMUELSSON E, 1992, METALL TRANS B, V23, P805, DOI 10.1007/BF02656459
SCHWERDTFEGER K, 1965, T METALL SOC AIME, V233, P1327
STULL DR, 1971, JANAF THERMOCHEMICHA
NR 11
TC 23
Z9 23
U1 0
U2 2
PI TOKYO
JAPAN
SN 0021-1575
J9 TETSU TO HAGANE
PD FEB
PY 1998
VL 84
IS 2
BP 97
EP 102
PG 6
GA ZW937
UT WOS:000074463300003
DA 2023-12-05
ER
PT J
AU NOMURA, K
OZTURK, B
FRUEHAN, RJ
AF NOMURA, K
OZTURK, B
FRUEHAN, RJ
TI REMOVAL OF NITROGEN FROM STEEL USING NOVEL FLUXES
SO METALLURGICAL TRANSACTIONS B-PROCESS METALLURGY
LA English
DT Article
ID SLAGS
AB The solubility of nitrogen and the nitride capacity of CaO-Al2O3-TiO2 and CaO-
BaO-Al2O3-TiO2 slags were measured at 1873 K using a gas-slag-metal equilibration
technique with carbon-saturated iron and gas mixtures of CO and N2. The nitride
capacity increased with increasing the TiO2 and BaO content and is significantly
higher than the nitride capacity for normal ladle slags. The activity coefficient
of TiO2 in CaO-Al2O3-TiO2 and CaO-BaO-Al2O3-TiO2 systems were measured. This is
necessary to know in order to estimate the possible pickup of titanium in the metal
when an aluminum-killed steel is treated with these slags. Also, the activity
coefficient of Ti in carbon-saturated iron was measured. The kinetics of the
nitrogen reaction between slag and metal is influenced by the oxygen potential in
the metal and is primarily controlled by liquid-phase mass transfer of nitrogen in
the metal.
C1 CARNEGIE MELLON UNIV,DEPT MET ENGN & MAT SCI,PITTSBURGH,PA 15213.
RP NOMURA, K (corresponding author), DAIDO STEEL CO LTD,ACHI,JAPAN.
CR ITO K, 1988, METALL TRANS B, V19, P419, DOI 10.1007/BF02657739
MARTINEZ C, 1988, CURRENT ADV MATERIAL, V1
MIN DJ, 1990, METALL TRANS B, V21, P1025, DOI 10.1007/BF02670273
MULFINGER HO, 1966, J AM CERAM SOC, V49, P462, DOI 10.1111/j.1151-
2916.1966.tb13300.x
OZTURK B, 1988, IRONMAK STEELMAK, V15, P305
SASAGAWA M, 1990, T IRON STEEL SOC, P51
SCHWERDTFEGER K, 1974, ARCH EISENHUTTENWES, V54, P649
Shimoo T., 1972, J JAPAN I METALS, V36, P723, DOI 10.2320/jinstmet1952.36.8_723
SUITO H, 1987, TETSU TO HAGANE, V73, pS246
TURKDOGAN ET, 1980, PHYSICAL CHEM HIGH T
Wagner C., 1975, Metallurgical Transactions B (Process Metallurgy), V6B, P405,
DOI 10.1007/BF02913825
1972, PHYSICAL PROPERTIES, P109
NR 14
TC 23
Z9 23
U1 0
U2 7
PI WARRENDALE
PA 420 COMMONWEALTH DR, WARRENDALE, PA 15086
SN 0360-2141
J9 METALL TRANS B
PD DEC
PY 1991
VL 22
IS 6
BP 783
EP 790
DI 10.1007/BF02651155
PG 8
GA GU039
UT WOS:A1991GU03900005
DA 2023-12-05
ER
PT J
AU Peys, A
Isteri, V
Yliniemi, J
Yorkshire, AS
Lemougna, PN
Utton, C
Provis, JL
Snellings, R
Hanein, T
AF Peys, Arne
Isteri, Visa
Yliniemi, Juho
Yorkshire, Antonia S.
Lemougna, Patrick N.
Utton, Claire
Provis, John L.
Snellings, Ruben
Hanein, Theodore
TI Sustainable iron-rich cements: Raw material sources and binder types
LA English
DT Article
DE Cement; Iron; Ferrite; Residue valorisation; Low-carbon; Clinkers;
Supplementary cementitious materials; Alkali-activated materials
ID SUPPLEMENTARY CEMENTITIOUS MATERIALS; ALUNITE PRECIPITATE ADDITION;
BLAST-FURNACE SLAG; PORTLAND-CEMENT; INORGANIC POLYMERS; VOLCANIC ASH;
COPPER SLAG; LEACHING BEHAVIOR; STEEL SLAG; RED MUD
AB The bulk of the cement industry's environmental burden is from the calcareous
source. Calcium is mostly available naturally as limestone (CaCO3), where almost
half of the mass is eventually released as CO2 during clinker manufacture. Iron
(Fe) is the fourth most common element in the Earth's crust surpassed only by
oxygen, silicon, and aluminium; therefore, potential raw materials for alternative
cements can contain significant amounts of iron. This review paper discusses in
detail the most abundantly available Fe-rich natural resources and industrial by-
products and residues, establishing symbiotic supply chains from various sectors.
The discussion then focusses on the impact of high iron content in clinker and on
ferrite (thermo)chemistry, as well as the importance of iron speciation on its
involvement in the reactions as supplementary cementitious material or alkali-
activated materials, and the technical quality that can be achieved from
sustainable Fe-rich cements.
C1 [Peys, Arne; Snellings, Ruben] VITO, Sustainable Mat, Boeretang 200, B-2400 Mol,
Belgium.
[Isteri, Visa] Univ Oulu, Fac Technol, Proc Met, POB 4300, Oulu 90014, Finland.
[Yliniemi, Juho] Univ Oulu, Fac Technol, Fibre & Particle Engn, POB 4300, Oulu
90014, Finland.
[Yorkshire, Antonia S.; Utton, Claire; Provis, John L.; Hanein, Theodore] Univ
Sheffield, Dept Mat Sci & Engn, Sheffield S1 3JD, England.
[Lemougna, Patrick N.] Vrije Univ Brussel, Dept Mat & Chem, Pleinlaan 2, B-1050
Brussels, Belgium.
[Lemougna, Patrick N.] Univ Ngaoundere, Sch Chem Engn & Mineral Ind EGCIM, Dept
Minerals Engn, POB 454, Ngaoundere, Cameroon.
C3 VITO; University of Oulu; University of Oulu; University of Sheffield;
Vrije Universiteit Brussel
RP Hanein, T (corresponding author), Univ Sheffield, Dept Mat Sci & Engn, Sheffield
S1 3JD, England.
EM t.hanein@sheffield.ac.uk
RI Peys, Arne/JDD-6025-2023; Peys, Arne/AAS-6258-2020; Snellings,
Ruben/GXV-6750-2022
OI Peys, Arne/0000-0001-9999-5236; Snellings, Ruben/0000-0002-4354-4871;
Hanein, Theodore/0000-0002-3009-703X; Lemougna Ninla,
Patrick/0000-0003-2233-9745
FU UKRI Future Leaders Fellowship [MR/V023829/1]; EPSRC [EP/T013524/1];
UKRI through the ICEC-MCM centre [EP/V011820/1]; Business Finland
project: Towards Carbon Neutral Metals - TOCANEM [41700/31/2020]
FX T. Hanein was funded by UKRI Future Leaders Fellowship (MR/V023829/1) .
A. Yorkshire and J. L. Provis were funded by EPSRC (EP/T013524/1) . J.
L. Provis and T. Hanein were also funded by UKRI through the ICEC-MCM
centre (EP/V011820/1) . V. Isteri was funded by Business Finland
project: Towards Carbon Neutral Metals - TOCANEM (No. 41700/31/2020) .
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NR 298
TC 22
Z9 22
U1 22
U2 62
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD JUL
PY 2022
VL 157
AR 106834
DI 10.1016/j.cemconres.2022.106834
EA MAY 2022
PG 20
GA 1X9DC
UT WOS:000807748400002
DA 2023-12-05
ER
PT J
AU Shen, ZJ
Nikolic, H
Caudill, LS
Liu, KL
AF Shen, Zhongjie
Nikolic, Heather
Caudill, Landon S.
Liu, Kunlei
TI A deep insight on the coal ash-to-slag transformation behavior during
the entrained flow gasification process
SO FUEL
LA English
DT Article
DE Entrained flow gasification; Coal ash-to-slag transformation;
Temperature; Syngas composition; Residual carbon
ID PHASE-TRANSFORMATION; VISCOSITY; CRYSTALLIZATION; TEMPERATURE;
PARTICLES; SODIUM; TIME; SIMULATION; PREDICTION; PYROLYSIS
AB Recent research provided deep insight on the coal ash-to-slag transformation
characterization during the entrained flow gasification process, with
experimentation on a 40 kg/hr (dry basis) coal-fed opposed multi-burner (OMB)
entrained flow gasifier and simulation via FactSage (TM) software. A general
mechanism is presented to relate the gasifier design temperature, ash fluid
temperature, and operating temperature with the degree of the slag polymerization.
The change of the high temperature zone, the corresponding particle residence time
in the high temperature zone, and syngas composition have obvious effects on the
slag mineral transformation behavior. Mineral types formed on the wall of the
gasifier chamber were mainly anorthite (CaAl2Si2O8), aluminum oxide (Al2O3), and
calcium sulfide (CaS). These minerals transformed to anorthite and diopside
(CaMgSi2O6) at the slag hole zone, while the minerals at the lock hopper were
anorthite, orthoclase (KAlSi3O8), quartz (SiO2), gypsum (CaSO4), calcite (CaCO3),
and halite (NaCl). FactSage (TM) predicted minerals as anorthite, diopside,
orthoclase, and albite (NaAlSi3O8), etc., where the slag temperature was below the
ash fluid temperature and when the ratios of CO/CO2 and (CO + H-2)/CO2 were lower
than 1.0 and 2.0, respectively. By simulation, residual carbon was found to be the
dominant factor over syngas composition to cause mineral transformation, and this
was verified experimentally. The Ca-based crystals, typically anorthite, was
shifted to diopside, near the slag hole zone, and a linear relationship was found
between the content ratios of diopside/(anorthite + diopside), CaO/SiO2, and (CaO +
MgO)/SiO2. A dimensionless number, theta, was defined to characterize the changing
chemical composition and the degree of slag polymerization, with temperature
deviation from the design condition. Three zones of theta were identified and
related to the deviation between the actual gasification condition from the design
condition. A low slag polymerization degree corresponded with a higher temperature
deviation between the actual condition and design condition, and this proved that
increased residual carbon content and changing iron valence state increased the
mineral types when the slag temperature was below the ash fluid temperature.
C1 [Shen, Zhongjie; Nikolic, Heather; Caudill, Landon S.; Liu, Kunlei] Univ
Kentucky, Ctr Appl Energy Res, Lexington, KY 40511 USA.
[Liu, Kunlei] Univ Kentucky, Dept Mech Engn, Lexington, KY 40506 USA.
C3 University of Kentucky; University of Kentucky
RP Liu, KL (corresponding author), Univ Kentucky, Ctr Appl Energy Res, Lexington,
KY 40511 USA.
EM kunlei.liu@uky.edu
FU US Department of Energy (DOE) National Energy Technology Laboratory
(NETL) [DE-FE0031506]
FX This work is funded by US Department of Energy (DOE) National Energy
Technology Laboratory (NETL), DE-FE0031506.
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NR 48
TC 22
Z9 23
U1 9
U2 53
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD APR 1
PY 2021
VL 289
AR 119953
DI 10.1016/j.fuel.2020.119953
PG 13
GA PY5CD
UT WOS:000612061200006
OA hybrid
DA 2023-12-05
ER
PT J
AU Jiménez, A
Misol, A
Morato, A
Rives, V
Vicente, MA
Gil, A
AF Jimenez, Alejandro
Misol, Alexander
Morato, Alvaro
Rives, Vicente
Vicente, Miguel A.
Gil, Antonio
TI Synthesis of pollucite and analcime zeolites by recovering aluminum from
a saline slag
LA English
DT Article
DE Saline slag; Aluminum recovery; Zeolitic materials; Pollucite; Analcime
ID HYDROTALCITE-LIKE COMPOUNDS; HYDROTHERMAL SYNTHESIS; INDUSTRIAL-WASTES;
HAZARDOUS-WASTE; SALT CAKES; DROSS; IMMOBILIZATION; VALORIZATION;
MANAGEMENT
AB This work describes a valorization procedure for one of the most important
wastes generated during aluminum recycling, namely, saline slag. This procedure was
divided in two steps: a) recovery of aluminum or its compounds in various
fractions, and b) the use of one of those fractions in the synthesis of two
zeolites: analcime (NaAlSi2O6 center dot H2O) and pollucite (CsAlSi2O6 center dot
nH(2)O). Saline slag was ground, sieved (1 mm), washed and separated into two
fractions of different sizes, one larger and another smaller than 0.4 mm. The
fraction smaller than 0.4 mm was treated under reflux conditions with NaOH or CsOH
solutions. The extraction liquor contained aluminum and alkali metal cations; after
adding the necessary amount of Si, hydrothermal synthesis was carried out,
obtaining the zeolitic materials. Characterization of the solids obtained was
carried out by powder X-ray diffraction, thermal analysis, FT-IR spectroscopy,
element chemical analysis and electron microscopy. The valorization procedure
proposed in this work showed that a high percentage of Al (close to 45 wt%) can be
recovered from the fraction smaller than 0.4 mm and that the liquors extracted with
NaOH or CsOH can be used as a source for the hydrothermal synthesis (200 degrees C
for 24 h) of two zeolites of the analcime family, obtaining in both cases pure and
crystalline solids. (C) 2021 Elsevier Ltd. All rights reserved.
C1 [Jimenez, Alejandro; Misol, Alexander; Morato, Alvaro; Rives, Vicente; Vicente,
Miguel A.] Univ Salamanca, Fac Ciencias Quim, Dept Quim Inorgan, GIR QUESCAT, E-
37008 Salamanca, Spain.
[Gil, Antonio] Univ Publ Navarra, INAMAT2 Dept Ciencias, Edificio Acebos,Campus
Arrosadia, E-31006 Pamplona, Spain.
C3 University of Salamanca; Universidad Publica de Navarra
RP Rives, V (corresponding author), Univ Salamanca, Fac Ciencias Quim, Dept Quim
Inorgan, GIR QUESCAT, E-37008 Salamanca, Spain.
EM vrives@usal.es
RI Misol, Alexander/C-3594-2018; Jiménez, Alejandro/AAB-2390-2020; Vicente,
Miguel Angel/L-5298-2014; Rives, Vicente/A-8719-2008
OI Misol, Alexander/0000-0002-8529-1091; Jiménez,
Alejandro/0000-0003-4847-8495; Vicente, Miguel
Angel/0000-0002-6714-0249; Rives, Vicente/0000-0002-0518-8351; Gil,
Antonio/0000-0001-9323-5981
FU MINECO; ERDF [MAT 201678863-C2-R]; Sistema Nacional de Garantia Juvenil;
Junta de Castilla y Leon; ERDF; Santander Bank; Universidad de
Salamanca; Banco Santander
FX This work was supported by MINECO and ERDF (MAT 201678863-C2-R). A.
Jimenez thanks Junta de Castilla y Leon and Sistema Nacional de Garantia
Juvenil for a formation contract and Universidad de Salamanca and Banco
Santander for a predoctoral contract. A. Misol thanks Junta de Castilla
y Leon and ERDF for a predoctoral contract. AG also thanks Santander
Bank for funding through the Research Intensification Program.
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10.1016/j.micromeso.2019.06.009
NR 43
TC 22
Z9 22
U1 1
U2 23
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAY 15
PY 2021
VL 297
AR 126667
DI 10.1016/j.jclepro.2021.126667
EA MAR 2021
PG 8
& Ecology
GA SO6VS
UT WOS:000659113300030
OA hybrid, Green Published
DA 2023-12-05
ER
PT J
AU Miao, ZK
Chen, LQ
Chen, KN
Zhang, XX
Zhang, YX
Wu, JJ
AF Miao, Zekai
Chen, Liqing
Chen, Kening
Zhang, Xinxiao
Zhang, Yixin
Wu, Jianjun
TI Physical properties and microstructures of residual carbon and slag
particles present in fine slag from entrained-flow coal gasification
SO ADVANCED POWDER TECHNOLOGY
LA English
DT Article
DE Fine slag; Residual carbon; Slag particles; Microstructures
ID SILICATE-GLASSES; SURFACE; SI-29; ASH; DECONVOLUTION; REACTIVITY;
SPECTRA
AB Fine slag (FS) consists of residual carbon (RC) and slag particles (SP). This
paper studies the characteristics of SP and RC separately. SP contain a little of
pores and mainly consist of spherical particles most of which are solids. RC have a
higher pore surface, more continuous and complete pore structure. The chemical
structure of inorganic minerals in SP has the following characteristics: According
to nuclear magnetic resonance results, the amounts of network structure Q(4) and
Q(3) are more than that of chain structure Q(2) and Q(1). The 4-coordinated
aluminum consists of 74% and the octahedral coordination (Al(VI)) takes up only
11%. SP is a heterogeneous material which contain not only inorganic minerals but
also organic carbon. C atom associated in chemical way with the inorganic matter
within SP matrix. The predominant groups of organic carbon within SP matrix are C-C
and C-O. C-O groups organically bound with inorganic elements in SP forming C-O-M
(M: inorganic elements) bands. The predominant components in RC are C-C and C-O.
(C) 2020 Published by Elsevier B.V. on behalf of The Society of Powder Technology
Japan. All rights reserved.
C1 [Miao, Zekai; Chen, Liqing; Chen, Kening; Zhang, Xinxiao; Wu, Jianjun] China
Univ Min & Technol, Sch Chem Engn & Technol, Xuzhou 221116, Jiangsu, Peoples R
China.
[Zhang, Yixin] China Univ Min & Technol, Chinese Natl Engn Res Ctr Coal Preparat
& Purific, Xuzhou 221116, Jiangsu, Peoples R China.
C3 China University of Mining & Technology; China University of Mining &
Technology
RP Wu, JJ (corresponding author), China Univ Min & Technol, Sch Chem Engn &
Technol, Xuzhou 221116, Jiangsu, Peoples R China.
EM yixinzhang@cumt.edu.cn; wujj@cumt.edu.cn
RI Wu, Jian/AAU-5221-2020; Wu, Jian/AAU-5221-2020
OI Wu, Jian/0000-0001-9933-7364; Wu, Jian/0000-0002-3394-1507
FU National Key Research and Development Program China [2019YFC1904302];
National Nature Science Foundation of China [51704292, 51974311]
FX This work was financially supported by the National Key Research and
Development Program China (2019YFC1904302), the National Nature Science
Foundation of China (51704292 and 51974311).
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NR 37
TC 22
Z9 25
U1 6
U2 66
PU ELSEVIER
PI AMSTERDAM
SN 0921-8831
EI 1568-5527
J9 ADV POWDER TECHNOL
JI Adv. Powder Technol.
PD SEP
PY 2020
VL 31
IS 9
BP 3781
EP 3789
DI 10.1016/j.apt.2020.07.019
PG 9
SC Engineering
GA OD2YB
UT WOS:000579717400041
DA 2023-12-05
ER
PT J
AU Gu, YC
Li, JL
Peng, JK
Xing, F
Long, WJ
Khayat, KH
AF Gu, Yu-cun
Li, Jin-Lin
Peng, Jun-Kai
Xing, Feng
Long, Wu-Jian
Khayat, Kamal H.
TI Immobilization of hazardous ferronickel slag treated using ternary
limestone calcined clay cement
LA English
DT Article
DE Limestone calcined clay cement; Ferronickel slag; Environmental
assessment; Heavy metal leaching; Solidification/stabilization
ID CONTAMINATED SITE SOIL; MAGNESIUM NICKEL SLAG; LIFE-CYCLE ASSESSMENT;
PORTLAND-CEMENT; BLENDED CEMENTS; BOTTOM ASH;
SOLIDIFICATION/STABILIZATION; WASTE; HYDRATION; CONCRETE
AB This study aims to develop the limestone calcined clay (LC3) as a low-carbon
treatment to immobilize waste ferronickel slag (FNS) containing heavy metals. The
results indicate that the ordinary portland cement (OPC) and limestone calcined
clay cement (LC3) adequately immobilized the Chromium (Cr), with the leaching
results of 0.10-0.30 mg/L. The LC3 cement provided superior Mn immobilization
(lower than 5 mg/L) compared to OPC. Calcium aluminum silicate hydrate (C-A-S-H)
and ettringite (AFt) were the two main hydrated products of LC3 that ensure the
capacity to encapsulate metals. The LC3 specimens had the lower porosity between 50
and 10,000 nm compared to that of OPC. The Embodied Energy (EE) and Embodied Carbon
Emissions (ECO(2)e) of per m(3) LC3 remarkably decreased by 38.21% and 44.77%. (C)
C1 [Gu, Yu-cun; Li, Jin-Lin; Peng, Jun-Kai; Xing, Feng; Long, Wu-Jian] Shenzhen
Univ, Coll Civil & Transportat Engn, Shenzhen Durabil Ctr Civil & Transportat Engn,
Guangdong Prov Key Lab Durabil Marine Civil Engn, Shenzhen 518060, Guangdong,
Peoples R China.
[Gu, Yu-cun; Khayat, Kamal H.] Missouri Univ Sci & Technol, Dept Civil
Architectural & Environm Engn, Rolla, MO 65401 USA.
[Li, Jin-Lin; Peng, Jun-Kai] Shenzhen Univ, Sino Australia Joint Res Ctr BIM &
Smart Construc, Shenzhen 518060, Guangdong, Peoples R China.
C3 Shenzhen University; University of Missouri System; Missouri University
of Science & Technology; Shenzhen University
RP Long, WJ (corresponding author), Shenzhen Univ, Coll Civil & Transportat Engn,
Shenzhen Durabil Ctr Civil & Transportat Engn, Guangdong Prov Key Lab Durabil
Marine Civil Engn, Shenzhen 518060, Guangdong, Peoples R China.
EM longwj@szu.edu.cn
RI Gu, Yucun/GXG-2875-2022; Long, Wu-Jian/O-8102-2017; Khayat,
Kamal/D-4255-2016
OI Gu, Yucun/0000-0003-4421-9728; Long, Wu-Jian/0000-0002-4760-0009;
Khayat, Kamal/0000-0003-1431-0715
FU Science and Technology Project of Shenzhen, China
[JCYJ20180305124844894]; National Natural Science Foundation of China
[51778368]
FX The authors gratefully acknowledge the financial support provided by the
Science and Technology Project of Shenzhen, China (No.
JCYJ20180305124844894) and the National Natural Science Foundation of
China (No. 51778368).
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NR 58
TC 22
Z9 25
U1 9
U2 71
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUL 30
PY 2020
VL 250
AR 118837
DI 10.1016/j.conbuildmat.2020.118837
PG 12
GA LR7ZF
UT WOS:000535914900035
DA 2023-12-05
ER
PT J
AU Sun, X
Hao, H
Liu, ZW
Zhao, FQ
AF Sun, Xin
Hao, Han
Liu, Zongwei
Zhao, Fuquan
TI Insights into the global flow pattern of manganese
SO RESOURCES POLICY
LA English
DT Article
DE Manganese; Material flow analysis; International trade; Resource
management
ID LITHIUM-ION BATTERY; MECHANICAL SEPARATION; SILICOMANGANESE SLAG;
METALS; IRON; CRITICALITY; RECOVERY; ALUMINUM; DEMAND; COBALT
AB Manganese is a necessary and irreplaceable metal resource for the steelmaking
industry. The essentiality and non-substitutability make the vulnerability to
supply restriction of manganese nonnegligible. With this concern, this study was
conducted to present a global trade-linked material flow analysis (MFA) model of
manganese for the year of 2017 to provide deep insight into its flow pattern. Using
the MFA model, the global manganese flow in 305 categories of commodities within
249 countries was mapped. The results showed that 23.9 million tons (Mt) of
manganese were supplied and used in 2017. An estimated 27.9 Mt of manganese
contained in various commodities was traded between countries, 38% of which was
contributed by the top ten trade flows. China, South Africa, Australia, Brazil,
Gabon, the USA, India, Japan and Germany were the nine most important members of
the global manganese trade flow community. The lack of a system for the complete
recovery of Mn from end-of-life products and slag, and a trend towards increasing
geographic concentration of Mn ore supplies, were identified as two areas of
potential risk and concern. Corresponding policy recommendations are proposed to
resolve these concerns. A more integrated recovery system of manganese needs to be
considered, particularly for the developing lithium-ion battery applications.
Establishment of national reserve needs to be put on the agenda for the large
manganese consumers. High supply concentration of manganese refining and
manufacturing stage, which is dominated by China, may need to be changed when
prospective global manganese consumption structure changes.
C1 [Sun, Xin; Hao, Han; Liu, Zongwei; Zhao, Fuquan] Tsinghua Univ, State Key Lab
Automot Safety & Energy, Beijing 100084, Peoples R China.
[Hao, Han] Tsinghua Univ, China Automot Energy Res Ctr, Beijing 100084, Peoples
R China.
[Hao, Han; Liu, Zongwei; Zhao, Fuquan] Tsinghua Univ, Tsinghua Automot Strategy
Res Inst, Beijing 100084, Peoples R China.
C3 Tsinghua University; Tsinghua University; Tsinghua University
RP Hao, H (corresponding author), Tsinghua Univ, State Key Lab Automot Safety &
Energy, Beijing 100084, Peoples R China.
EM hao@tsinghua.edu.cn
RI Hao, Han/M-8363-2019
OI Hao, Han/0000-0001-7542-4746; Sun, Xin/0000-0003-1772-8623
71403142]; Young Elite Scientists Sponsorship Program by CAST
[YESS20160140]; State Key Laboratory of Automotive Safety and Energy
[ZZ2019-023]; Tsinghua-Rio Tinto Research Center for Resources Energy
and Sustainable Development
FX This study is sponsored by the National Natural Science Foundation of
China (71774100, 71690241, 71403142), Young Elite Scientists Sponsorship
Program by CAST (YESS20160140), State Key Laboratory of Automotive
Safety and Energy (ZZ2019-023), Tsinghua-Rio Tinto Research Center for
Resources Energy and Sustainable Development.
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Z9 22
U1 9
U2 52
PU ELSEVIER SCI LTD
PI OXFORD
SN 0301-4207
EI 1873-7641
J9 RESOUR POLICY
JI Resour. Policy
PD MAR
PY 2020
VL 65
AR 101578
DI 10.1016/j.resourpol.2019.101578
PG 8
WC Environmental Studies
WE Social Science Citation Index (SSCI)
GA LG1BL
UT WOS:000527845100041
DA 2023-12-05
ER
PT J
AU Ye, HL
Fu, CQ
Yang, GJ
AF Ye, Hailong
Fu, Chuanqing
Yang, Guojun
TI Alkali-activated slag substituted by metakaolin and dolomite at 20 and
50°C
LA English
DT Article
DE Alkali-activated slag; Metakaolin; Dolomite; Curing temperature;
Hydrotalcite
ID BLAST-FURNACE SLAG; CEMENT PASTES; MICROSTRUCTURAL DEVELOPMENT;
HYDRATION PRODUCTS; REACTION-KINETICS; CHLORIDE-BINDING; PHASE
ASSEMBLAGE; PORTLAND-CEMENT; HYDROTALCITE; PERFORMANCE
AB This work focuses on the reaction of dolomite fines (DM) in combination with
metakaolin (MK) in alkali-activated slag (AAS), towards a better understanding of
the hydrotalcite-type phase formation in this system. The strength, phase
assemblage, and microstructure of AAS pastes with 40% slag substituted by a
combination of MK and DM and cured at two temperature conditions (i.e., 20 degrees
C and 50 degrees C) are studied. The results show that the DM at a less than 20%
substitution ratio in AAS poses a filler effect that advances slag reaction;
however, its potential chemical roles on supplementing magnesium and thus enhancing
the hydrotalcite formation are highly limited. The incorporation of MK in AAS
supplements aluminum but does not promote the hydrotalcite precipitation. The
results suggest that the absence of portlandite in AAS restricts the dissolution
and reaction of DM despite high alkalinity. The continued elevated temperature
curing has a detrimental effect on the strength development of AAS with greater
than 20% MK, likely due to the promoted transformation of strength-giving amorphous
gel products into zeolitic crystals. The optimum percentage ratio between MK and DM
lies around 1: 1 at a 40% replacement level in AAS, in term of strength achievement
and stability. This study contributes to the materials selection and mixture design
of slag-based alkali-activated composites with potentially enhanced chemical
durability.
C1 [Ye, Hailong] Univ Hong Kong, Dept Civil Engn, Pokfulam, Hong Kong, Peoples R
China.
[Fu, Chuanqing; Yang, Guojun] Zhejiang Univ Technol, Coll Civil Engn &
Architecture, Hangzhou, Zhejiang, Peoples R China.
C3 University of Hong Kong; Zhejiang University of Technology
RP Ye, HL (corresponding author), Univ Hong Kong, Dept Civil Engn, Pokfulam, Hong
Kong, Peoples R China.; Fu, CQ (corresponding author), Zhejiang Univ Technol, Coll
Civil Engn & Architecture, Hangzhou, Zhejiang, Peoples R China.
EM hlye@hku.hk; chqfii@zju.edu.cn
RI Ye, Hailong/ABI-5001-2020
OI Ye, Hailong/0000-0003-2665-3942
FU Hong Kong Research Grants Council [27204818]; National Natural Science
Foundation of China [51808475]
FX The authors would like to thank the financial support from the Hong Kong
Research Grants Council (Project number: 27204818) and National Natural
Science Foundation of China (Project number: 51808475). Any opinions,
findings and conclusions or recommendations expressed in this material
are those of the authors and do not necessarily reflect the views of the
sponsors.
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PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
PD JAN
PY 2020
VL 105
AR 103442
DI 10.1016/j.cemconcomp.2019.103442
PG 10
GA JW2JE
UT WOS:000502883200015
DA 2023-12-05
ER
PT J
AU Sukhomlinov, D
Klemettinen, L
O'Brien, H
Taskinen, P
Jokilaakso, A
AF Sukhomlinov, Dmitry
Klemettinen, Lassi
O'Brien, Hugh
Taskinen, Pekka
Jokilaakso, Ari
TI Behavior of Ga, In, Sn, and Te in Copper Matte Smelting
LA English
DT Article
ID PHASE-EQUILIBRIA; PARTIAL PRESSURES; SILICATE MELTS; FEO SYSTEM; SLAG;
THERMODYNAMICS; TIN; SATURATION; TELLURIUM; SELENIUM
AB The distributions of Ga, In, Sn, and Te between copper-iron mattes and silica-
saturated iron silicate slags over a wide range of matte grades 55 to 75 pct Cu
were determined at 1300 degrees C using a gas-phase equilibration-quenching
technique and direct phase composition analysis by Electron Probe X-ray
Microanalysis and Laser Ablation-Inductively Coupled Plasma-Mass Spectrometry.
Alumina from aluminum, a typical minor element of electric and electronic copper
scrap, and lime were adopted as slag modifiers for increasing the trace element
recoveries. Gallium and tin were distributed predominantly in the slag, indium
preferred sulfide matte at low matte grades and slag at high, whereas tellurium
strongly favored the sulfide matte in particular in high matte grades. The slag
modifiers alumina and lime had a minor impact on the distribution coefficients of
gallium and tin, but for indium and tellurium the distribution coefficients were
more strongly affected by the basic oxides. The strong tendencies of tin and
tellurium to vaporize at the experimental temperature were confirmed. (C) The
Author(s) 2019
C1 [Sukhomlinov, Dmitry; Klemettinen, Lassi; Taskinen, Pekka; Jokilaakso, Ari]
Aalto Univ, Sch Chem Engn, POB 16100, Aalto 00076, Finland.
[Sukhomlinov, Dmitry] NTNU, Dept Mat Sci & Engn, N-7491 Trondheim, Norway.
[O'Brien, Hugh] Geol Survey Finland, Vuorimiehentie 2, FIN-02150 Espoo, Finland.
C3 Aalto University; Norwegian University of Science & Technology (NTNU);
Geological Survey of Finland (GTK)
RP Taskinen, P (corresponding author), Aalto Univ, Sch Chem Engn, POB 16100, Aalto
00076, Finland.
EM pekka.taskinen@aalto.fi
RI Klemettinen, Lassi/AAA-4936-2020; Taskinen, Pekka/K-4292-2015;
Jokilaakso, Ari/AAP-6978-2020
OI Klemettinen, Lassi/0000-0001-9633-7131; Taskinen,
Pekka/0000-0002-4054-952X; Sukhomlinov, Dmitry/0000-0002-8752-4776;
Jokilaakso, Ari/0000-0003-0582-7181
FU Aalto University; Outotec; CMEco program of Business Finland
FX Open access funding provided by Aalto University. The study was
financially supported by Outotec and CMEco program of Business Finland,
which is gratefully acknowledged. The EPMA measurements were carried out
by Mr Lassi Pakkanen of the Geological Survey of Finland. This study
utilized the Academy of Finland's RawMatTERS Finland Infrastructure
(RAMI) based at Aalto University, GTK and VTT.
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NR 44
TC 22
Z9 22
U1 1
U2 19
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD DEC
PY 2019
VL 50
IS 6
BP 2723
EP 2732
DI 10.1007/s11663-019-01693-y
PG 10
Engineering
GA JT4TA
UT WOS:000500982500022
DA 2023-12-05
ER
PT J
AU Huang, GD
Yuan, L
Ji, YS
Liu, BL
Xu, ZS
AF Huang, Guodong
Yuan, Liang
Ji, Yongsheng
Liu, Benlin
Xu, Zhishan
TI Cooperative action and compatibility between Portland cement and MSWI
bottom ash alkali-activated double gel system materials
LA English
DT Article
DE Alkali-activated slag; MSWI bottom ash; Portland cement;
Calcium-Silicate-Hydrate (C-S-H); Hydration products
ID FLY-ASH; MECHANICAL-PROPERTIES; STRENGTH DEVELOPMENT; GEOPOLYMER
CONCRETE; BLENDED CEMENT; MORTARS; CALCIUM; HYDRATION; TEMPERATURE;
CARBONATION
AB This study investigated the cooperative action and compatibility between
Portland cement and municipal solid waste incineration (MSWI) bottom ash alkali-
activated double gel system materials, focusing on the two different methods of
mixed casting and layered casting. The results show that alkali-activated materials
and Portland cement have a severe incompatibility problem when mixed casting is
used. However, layered casting completely solves this compatibility problem in
double gelled system materials. This is because liquid sodium silicate accelerates
the initial setting time in alkali-activated materials and thus eliminates the
influence between polymerization and hydration. Furthermore, alkali-activated
materials can compensate for the lack of calcium by absorbing the Ca(OH)(2)
generated by the hydration of Portland cement. In this case, Calcium-Silicate-
Hydrate (C-S-H) and Aluminium-Modified Calcium-Silicate Hydrate (C-A-S-H) gels are
formed, which strengthens the interface transition zone. (C) 2019 Elsevier Ltd. All
rights reserved.
C1 [Huang, Guodong; Yuan, Liang] Anhui Univ Sci & Technol, Sch Civil Engn &
Construct, Huainan 232001, Anhui, Peoples R China.
[Huang, Guodong; Ji, Yongsheng; Liu, Benlin; Xu, Zhishan] China Univ Min &
Technol, State Key Lab Geomech & Deep Underground Engn, Xuzhou 21116, Jiangsu,
Peoples R China.
[Huang, Guodong] Jiangsu Collaborat Innovat Ctr Bldg Energy Saving, Xuzhou
21116, Jiangsu, Peoples R China.
C3 Anhui University of Science & Technology; China University of Mining &
Technology
RP Huang, GD (corresponding author), Anhui Univ Sci & Technol, Sch Civil Engn &
Construct, Huainan 232001, Anhui, Peoples R China.; Huang, GD (corresponding
author), China Univ Min & Technol, State Key Lab Geomech & Deep Underground Engn,
Xuzhou 21116, Jiangsu, Peoples R China.; Huang, GD (corresponding author), Jiangsu
Collaborat Innovat Ctr Bldg Energy Saving, Xuzhou 21116, Jiangsu, Peoples R China.
EM hgd522500@163.com
OI Ji, Yongsheng/0000-0002-7414-9719
FU JiangSu Collaborative Innovation Center for Building Energy Saving and
Construction Technology [SJXTQ1615]
FX This study was supported by the funding through JiangSu Collaborative
Innovation Center for Building Energy Saving and Construction Technology
(No. SJXTQ1615).
CR [Anonymous], 2007, GB 175-2007
[Anonymous], 1999, GBT176711999 ISO
[Anonymous], 2009, JGJ702009
[Anonymous], 1999, 24192005 GBT
Bahafid S, 2017, CEMENT CONCRETE RES, V95, P270, DOI
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10.1016/j.conbuildmat.2017.07.027
NR 56
TC 22
Z9 22
U1 6
U2 59
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUN 10
PY 2019
VL 209
BP 445
EP 453
DI 10.1016/j.conbuildmat.2019.03.141
PG 9
GA HZ2XV
UT WOS:000468713000042
DA 2023-12-05
ER
PT J
AU Gil, A
Arrieta, E
Vicen, MA
Korili, SA
AF Gil, Antonio
Arrieta, Ekhine
Angel Vicen, Miguel
Korili, Sophia A.
TI Application of Industrial Wastes from Chemically Treated Aluminum Saline
Slags as Adsorbents
SO ACS OMEGA
LA English
DT Article
ID CARBON-DIOXIDE CAPTURE; BASIC-DYES; AQUEOUS-SOLUTIONS; ACTIVATED CARBON;
MULTICOMPONENT EQUILIBRIUM; COMPETITIVE ADSORPTION; SIMULTANEOUS
REMOVAL; ISOSTERIC HEAT; CO2 CAPTURE; ACID-DYES
AB In this study, industrial wastes, which remain after aluminum extraction from
saline slags, were used as adsorbents. The aluminum saline slags were treated under
reflux with 2 mol/dm(3) aqueous solutions of NaOH, H2SO4, and HCl for 2 h. After
separation by filtration, aqueous solutions containing the extracted aluminum and
residual wastes were obtained. The wastes were characterized by nitrogen adsorption
at -196 degrees C, X-ray diffraction, scanning electron microscopy, and ammonia
pulse chemisorption. The chemical treatment reduced the specific surface area, from
84 to 23 m(2)/g, and the pore volume, from 0.136 to 0.052 cm(3)/g, of the saline
slag and increased the ammonia-adsorption capacity from 2.84 to 5.22 cm(3)/g, in
the case of acid-treated solids. The materials were applied for the removal of Acid
Orange 7 and Acid Blue 80 from aqueous solutions, considering both single and
binary systems. The results showed interesting differences in the adsorption
capacity between the samples. The saline slag treated with HCl rapidly adsorbed all
of the dyes present in solution, whereas the other materials retained between 50
and 70% of the molecules present in solution. The amount of Acid Orange 7 removed
by the nontreated material and by the material treated with NaOH increased in the
presence of Acid Blue 80, which can be considered as a synergistic behavior. The
CO2 adsorption of the solids at several temperatures up to 200 degrees C was also
evaluated under dry conditions. The aluminum saline slag presented an adsorption
capacity higher than the rest of treated samples, a behavior that can be explained
by the specific sites of adsorption and the textural properties of the solids. The
isosteric heats of CO2 adsorption, determined from the Clausius-Clapeyron equation,
varied between 1.7 and 26.8 kJ/mol. The wastes should be used as adsorbents for the
selective removal of organic contaminants in wastewater treatment.
C1 [Gil, Antonio; Arrieta, Ekhine; Korili, Sophia A.] Univ Publ Navarra, INAMAT
Dept Ciencias, Edificio Acebos,Campus Arrosadia, E-31006 Pamplona, Spain.
[Angel Vicen, Miguel] Univ Salamanca, GIR QUESCAT, Dept Quim Inorgan, E-37008
Salamanca, Spain.
RP Gil, A (corresponding author), Univ Publ Navarra, INAMAT Dept Ciencias, Edificio
Acebos,Campus Arrosadia, E-31006 Pamplona, Spain.
RI Vicente, Miguel Angel/L-5298-2014
OI Vicente, Miguel Angel/0000-0002-6714-0249
FU Seventh Framework Programme through the project RecycAl; Spanish
Ministry of Economy, Industry, and Competitiveness (AEI/MINECO);
Santander Bank
FX The authors are grateful for the financial support from the Seventh
Framework Programme through the project RecycAl, the Spanish Ministry of
Economy, Industry, and Competitiveness (AEI/MINECO), and the European
Regional Development Fund (ERDF) through project MAT2016-78863-C2-R.
A.G. also thanks Santander Bank for funding through the Research
Intensification Program.
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TC 22
Z9 23
U1 3
U2 15
PI WASHINGTON
SN 2470-1343
J9 ACS OMEGA
JI ACS Omega
PD DEC
PY 2018
VL 3
IS 12
BP 18275
EP 18284
DI 10.1021/acsomega.8b02397
PG 10
SC Chemistry
GA HL1FG
UT WOS:000458439900008
PM 31458405
DA 2023-12-05
ER
PT J
AU Ghodrat, M
Rhamdhani, MA
Khaliq, A
Brooks, G
Samali, B
AF Ghodrat, Maryam
Rhamdhani, Muhammad Akbar
Khaliq, Abdul
Brooks, Geoffrey
Samali, Bijan
TI Thermodynamic analysis of metals recycling out of waste printed circuit
board through secondary copper smelting
SO JOURNAL OF MATERIAL CYCLES AND WASTE MANAGEMENT
LA English
DT Article
DE Thermodynamic analysis; Waste PCBs; Secondary copper smelting; Precious
metals
ID ELECTRONIC WASTE; FLUORESCENT LAMPS; RARE-EARTHS; CYCLE; RECOVERY;
CONSEQUENCES; PERSPECTIVE; TECHNOLOGY; LIBERATION; MANAGEMENT
AB In this paper, a detailed thermodynamic analysis of processing of electronic
waste (e-waste), particularly printed circuit boards (PCB), through secondary
copper recycling (black copper smelting), was carried out. The mass balance
flowsheets of two scenarios, i.e., the case of secondary copper recycling with
(SCE1) and without (SCE2) addition of PCBs, have been developed and compared. From
the perspective of recovery of copper (Cu), gold (Au), and silver (Ag); the
thermodynamic analysis predicted that the process conditions at temperature of 1300
degrees C and oxygen partial pressure (pO(2)) of 10-8 atm are suitable for PCB
processing through secondary copper smelting route. Under these conditions, no
solid phases were predicted to form when the PCB addition is below 50 wt%. High PCB
addition was predicted to produce high volume of slag in the process and more
pollutants in the gas phase (Br-based gaseous compounds). The chemistry of the slag
was also predicted to change that is shifting the liquidus temperature to a higher
value due to the presence of aluminium (Al), silica (SiO2), and titanium dioxide
(TiO2) in the feed coming from the PCB. The carbon content of the PCB potentially
supplies additional heat and reductant (CO) in the process hence can partially
replace coke in the feed material. The predicted recoveries of copper (Cu), gold
(Au), and silver (Ag) from e-waste were 83.3, 96.5, and 88.5 wt% respectively.
C1 [Ghodrat, Maryam; Samali, Bijan] Western Sydney Univ, Sch Comp Engn & Math, Ctr
Infrastruct Engn, Sydney, NSW, Australia.
[Rhamdhani, Muhammad Akbar; Khaliq, Abdul; Brooks, Geoffrey] Swinburne Univ
Technol, Dept Mech Engn & Prod Design Engn, Melbourne, Vic, Australia.
C3 Western Sydney University; Swinburne University of Technology
RP Ghodrat, M (corresponding author), Western Sydney Univ, Sch Comp Engn & Math,
Ctr Infrastruct Engn, Sydney, NSW, Australia.
EM M.ghodrat@westernsydney.edu.au; arhamdhani@swin.edu.au;
aks1445@gmail.com; gbrooks@swin.edu.au; B.Samali@westernsydney.edu.au
RI Rhamdhani, Muhammad Akbar/ACM-2274-2022; Khaliq, Abdul/AAR-5080-2020
OI Rhamdhani, Muhammad Akbar/0000-0002-9457-3808; Khaliq,
Abdul/0000-0002-8512-105X; Brooks, Geoffrey/0000-0002-8499-780X; Samali,
Bijan/0000-0002-3426-7745; Ghodrat, Maryam/0000-0003-4009-5262
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Yamasue E, 2009, MATER TRANS, V50, P1536, DOI 10.2320/matertrans.MBW200816
NR 50
TC 22
Z9 22
U1 2
U2 36
PU SPRINGER
PI NEW YORK
SN 1438-4957
EI 1611-8227
J9 J MATER CYCLES WASTE
JI J. Mater. Cycles Waste Manag.
PD JAN
PY 2018
VL 20
IS 1
BP 386
EP 401
DI 10.1007/s10163-017-0590-8
PG 16
GA FS6GS
UT WOS:000419896500038
DA 2023-12-05
ER
PT J
AU Yang, JG
Park, JH
AF Yang, Jun Gil
Park, Joo Hyun
TI Distribution Behavior of Aluminum and Titanium Between Nickel-Based
Alloys and Molten Slags in the Electro Slag Remelting (ESR) Process
LA English
DT Article
ID THERMODYNAMIC PROPERTIES; CAO-SIO2-MNO SLAG; EQUILIBRIUM; SYSTEM; OXIDE;
CAPACITY; SILICON; DIAGRAM; <XCAF2
AB The equilibrium reaction between Ni alloys and CaO-Al2O3-CaF2-TiO2 system
electroslag remelting (ESR) slags was investigated in the temperature range of 1773
K to 1873 K (1500 A degrees C to 1600 A degrees C) at p(O-2) = 10(-16) atm in order
to obtain the optimized composition of the slags for producing Ni alloys with
various Al and Ti ratios. In addition, the temperature dependence of the reaction
equilibria between the ESR slags and Ni alloys was also evaluated. The stable ionic
species of titanium in the ESR slag under the present experimental conditions was
experimentally confirmed to be mainly Ti4+ (i.e., TiO2) by X-ray photoelectron
spectroscopy analysis of the quenched samples. The activity-composition
relationship of TiO2 and Al2O3 in the ESR slag was determined as a function of the
Al/Ti ratio of the alloys and the CaF2 content of the slags in conjunction with the
activity ratio of Al to Ti in the alloys calculated from the FactSage(TM) 7.0
software. The temperature dependence of the activity-composition relationship of
TiO2 and Al2O3 in the slag showed good linear correlations, and the equilibrium
content ratio of TiO2 to Al2O3 at a fixed activity ratio increased with increasing
temperature, which was expected based on the standard enthalpy change of the
reaction. Thus, higher amounts of TiO2 should be added at higher operation
temperatures in the ESR process. A 120 kg scale pilot ESR test (2000 A and 16 V)
was performed to produce a commercial grade Ni-based superalloy based on the
activity-composition relationship of the slag components obtained in the present
study. Consequently, the contents of Al and Ti in the solidified ESR ingot were
nearly the same as that of the original electrode throughout the entire length (280
mm) after the ESR process. (C) The Minerals, Metals & Materials Society and ASM
International 2017
C1 [Yang, Jun Gil; Park, Joo Hyun] Hanyang Univ, Dept Mat Engn, Ansan 426791, South
Korea.
South Korea.
FU National Research Foundation of Korea [22A20130012792] Funding Source:
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NR 36
TC 22
Z9 23
U1 1
U2 41
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2017
VL 48
IS 4
BP 2147
EP 2156
DI 10.1007/s11663-017-0994-9
PG 10
Engineering
GA EZ2CC
UT WOS:000404516400023
DA 2023-12-05
ER
PT J
AU Herisson, J
Guéguen-Minerbe, M
van Hullebusch, ED
Chaussadent, T
AF Herisson, Jean
Gueguen-Minerbe, Marielle
van Hullebusch, Eric D.
Chaussadent, Thierry
TI Influence of the binder on the behaviour of mortars exposed to
H2S in sewer networks: a long-term durability study
LA English
DT Article
DE Biodeterioration; Hydrogen sulphide (H2S); In situ exposition; Sewer
networks; Calcium aluminate cement (CAC); Ordinary Portland cement
(OPC); Blast furnace slag (BFS)
ID WASTE-WATER; ANAEROBIC DIGESTER; OXIDIZING BACTERIA; SULFIDE OXIDATION;
HYDROGEN-SULFIDE; SULFURIC-ACID; CONCRETE; CORROSION; RESISTANCE; PH
AB The present study deals with the exposure of four different mortar formulations
in the headspace of two distinct sewer networks prone to biodeterioration
phenomenon due to the presence of hydrogen sulphide. Cylindrical specimens composed
of two cements, ordinary Portland cement ( OPC) and calcium aluminate cement
( CAC), with or without a substitution of 75 % of cement by blast furnace slag
( BFS) were prepared and exposed. During the exposure, the evolution of cement
materials was monitored. After 4 years exposure, OPC materials without BFS are
deeply deteriorated at high speed. Best performances have been observed with CAC
mortars correlated to their higher content in aluminium ion ( Al3+). The rank of
durability observed on site is OPC < OPC+BFS<CAC+BFS<CAC. Molecular biology
analysis revealed that microbial diversity is varying according to binder type as
well as during the exposure duration.
C1 [Herisson, Jean] Kerneos Res Ctr, 1 Rue Le Chatelier,ZAC Parc Technol, F-38090
Vaulx Milieu, France.
[Gueguen-Minerbe, Marielle; Chaussadent, Thierry] Univ Paris Est, MAST, CPDM,
IFSTTAR, F-77447 Marne La Vallee, France.
[van Hullebusch, Eric D.] Univ Paris Est, Lab Geomat & Environm, EA 4508, UPEM,
F-77454 Marne La Vallee, France.
C3 Universite Gustave-Eiffel; Universite Gustave-Eiffel
RP Herisson, J (corresponding author), Kerneos Res Ctr, 1 Rue Le Chatelier,ZAC Parc
Technol, F-38090 Vaulx Milieu, France.
EM jean.herisson@kerneos.com
RI chaussadent, thierry/AAF-8518-2020; van Hullebusch, Eric D./C-3086-2018
OI chaussadent, thierry/0000-0001-8901-6305; van Hullebusch, Eric
D./0000-0002-1519-1925
FU Kerneos
FX The authors gratefully thank Nadia Dominique and Issam Nour for their
involvement in the on-site experimental work. They also would like to
acknowledge Kerneos for providing cementitious materials and financial
support. Finally, they would like to thank Veolia Eau, SIBA, and
SAGEBA-ELOA for allowing access to sewer networks and for monitoring
environmental parameters.
CR AFNOR, 1995, 9931B40321 AFNOR EN
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NR 54
TC 22
Z9 22
U1 1
U2 74
PU SPRINGER
PI DORDRECHT
SN 1359-5997
EI 1871-6873
J9 MATER STRUCT
JI Mater. Struct.
PD FEB
PY 2017
VL 50
IS 1
AR 8
DI 10.1617/s11527-016-0919-0
PG 18
GA DY3VE
UT WOS:000385022400008
DA 2023-12-05
ER
PT J
AU Kaushik, P
Lowry, M
Yin, H
Pielet, H
AF Kaushik, P.
Lowry, M.
Yin, H.
Pielet, H.
TI Inclusion characterisation for clean steelmaking and quality control
LA English
DT Article
DE Inclusion control; Steel cleanliness; Automated SEM; Total oxygen;
Remelt buttons; AHSS steels; Ca treatment
ID CALCIUM
AB Improving steelmaking and casting processes to adapt to the requirements of
internal and external customers involves continuous monitoring and evaluation of
existing and development of new steel refining practices. Internal quality control
of semifinished products requires tools that can correlate product defects to
process anomalies. This article focuses on use of techniques such as measurement of
complete steel and slag chemistry, inclusion analysis, process analysis and
thermodynamics to assess the influence of process conditions on product properties.
Examples from both long and flat products, including low carbon aluminium killed
steels, medium carbon aluminium killed steels, advanced high strength steels and
free machining steels, are presented to explain the benefit of using these tools to
understand the process conditions necessary for clean steelmaking and thus improve
product quality.
C1 [Kaushik, P.; Lowry, M.; Yin, H.; Pielet, H.] ArcelorMittal Global Res & Dev,
Steelmaking & Refractories, E Chicago, IN 46312 USA.
C3 ArcelorMittal
RP Kaushik, P (corresponding author), ArcelorMittal Global Res & Dev, Steelmaking &
Refractories, 3001 E Columbus Dr, E Chicago, IN 46312 USA.
EM pallava.kaushik@arcelormittal.com
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Alavanja M., 1995, P 78 ISS STEELM C NA, P415
Automated Steel Cleanliness Assessment Tool (ASCAT), AUT STEEL CLEANL ASS
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EQUILIBRIUM CAL
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NR 25
TC 22
Z9 30
U1 0
U2 18
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD MAY
PY 2012
VL 39
IS 4
BP 284
EP 300
DI 10.1179/1743281211Y.0000000069
PG 17
GA 927OM
UT WOS:000302917400007
DA 2023-12-05
ER
PT J
AU Lin, KL
Wang, KS
Tzeng, BY
Lin, CY
AF Lin, KL
Wang, KS
Tzeng, BY
Lin, CY
TI The., hydration characteristics and utilization of slag obtained by the
vitrification of MSWI fly ash
SO WASTE MANAGEMENT
LA English
CT Conference on Sustainable Wastes Management
CY OCT, 2003
CL SARDINIA, ITALY
AB This study investigated the effects of slag composition on the hydration
characteristics of slag blended cement (SBC) pastes. Synthetic slag samples were
prepared by melting CaO-modified and Al2O3-modified municipal solid waste
incinerator (MSWI) fly ash. MSWI fly ash was mixed with 5% CaO and 5% Al2O3 (by
weight), respectively, resulting in two fly ash mixtures. These mixtures were then
melted at 1400 degreesC for 30 min to produce two types of slag with different
contents, designated at C-slag and A-slag. Both the C-slag and A-slag samples
exhibited a pozzolanic activity index higher than the unmodified slag sample. The
results show that the synthetic slags all met the Taiwan EPA's current regulatory
thresholds. These synthetic slags were then blended with ordinary Portland cement
(OPC) at various weight ratios ranging from 10 to 40%. The 28-day strength of the
C1 paste was higher than that developed by the OPC paste, suggesting that the C-
slag contributed to the earlier strength of the SBC pastes. At curing times beyond
28 days, the strength of the A1 paste samples approached that of the OPC paste
samples. It can be seen from this that increasing the amount of calcium and
aluminum oxide increases the early strength of SBC. The C-slag blended cement paste
samples showed an increase in the number of fine pores with the curing time,
showing that the C-slag enhanced the pozzolanic reactions, filling the pores. Also,
the incorporation of a 10% addition of C-slag also tended to enhance the degree of
hydration of the SBC pastes during the early ages (3-28 days). However, at later
ages, no significant difference in degree of hydration between the OPC pastes and
the SBC pastes was observed with the 10% C-slag addition. However, the
incorporation of A-slag did decreased the degree of hydration. A slag blend ratio
of 40% significantly decreased the hydration degree. (C) 2003 Elsevier Ltd. All
rights reserved.
C1 Natl Ilan Technol Coll, Dept Environm Engn, Ilan 260, Taiwan.
Natl Cent Univ, Grad Inst Environm Engn, Chungli 32054, Taiwan.
C3 National Central University
RP Lin, KL (corresponding author), Natl Ilan Technol Coll, Dept Environm Engn, Ilan
260, Taiwan.
EM kllin@mail.ev.ncu.edu.tw
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NR 14
TC 22
Z9 30
U1 0
U2 18
PI OXFORD
SN 0956-053X
EI 1879-2456
J9 WASTE MANAGE
JI Waste Manage.
PY 2004
VL 24
IS 2
BP 199
EP 205
DI 10.1016/S0956-053X(03)00131-4
PG 7
GA 773GK
UT WOS:000188889400011
PM 14761759
DA 2023-12-05
ER
PT J
AU Klose, S
Tölle, R
Bäucker, E
Makeschin, F
AF Klose, S
Tölle, R
Bäucker, E
Makeschin, F
TI Stratigraphic distribution of lignite-derived atmospheric deposits in
forest soils of the Upper Lusatian region, East Germany
SO WATER AIR AND SOIL POLLUTION
LA English
DT Article
DE ash content; energy dispersive X-ray microanalysis; ferromagnetic
susceptibility; fly ash depositions; forest soils; humic layer; scanning
electron microscopy
ID FLY-ASH; MAGNETIC-SUSCEPTIBILITY; TRACE-ELEMENTS; ORGANIC-MATTER; MINE
SOILS; COAL; RESIDUES
AB Atmospheric fly ash emissions from lignite-fired power plants in the Upper
Lusatian and Turowan mining districts strongly affected large forest areas along
the German-Polish border. A field study was conducted in old spruce stands (Picea
abies (L.) Karst.) to assess the., strati graphic distribution of fly ash in the
forest floor and mineral topsoil in the St. Marienthal forest area in the eastern
part of Saxony, Germany. This forest area is subjected to long-term atmospheric
depositions by two German and one Polish power plants since the early 1900s. The
three study sites are located along a fly ash deposition gradient of 3, 6 and 15 km
from the power plant in Turow (Sites Ia, II and III, respectively). An additional
site (Site Ib) at a distance of 3 km from Turow was chosen to study the influence
of vegetation type on fly ash deposition intensity in forest soils. Samples of the
humic layer (Oi (L), Oe (F) and Oa (H) horizons) and mineral soil (0-10 cm) were
taken in Spring and Fall 1999 and analysed for their ferromagnetic susceptibility
and total ash content. Particle size distribution, magnetic susceptibility of
individual size fractions, scanning electron microscopy (SEM), and energy
dispersive X-ray microanalysis (EDX) were performed on selected samples to evaluate
the origin of mineral particles found in the forest floor. High magnetic
susceptibility of the Oa and Oe horizons is a result of the long-term accumulation
of lignite-derived atmospheric deposits in the forest floors of the studied area.
Pure conifer stands (year-round filtration of airborne pollutants) resulted in
higher inputs of ferromagnetic fly ash particles in forest soils. Unusually high
total ash contents for humic horizons (up to 77%) were determined in the Oa and Oe
horizons at Sites la and IIb, indicating the need for a new classification systems
for the organic layer in forest soils near coal-fired power plants. SEM revealed 4
typical phases of persistent fly ash deposits formed by combustion of Lusatian
lignite: (1) iron-containing 'stable glasses', (2) aluminium-iron-silicate-
minerals, (3) slag fragments and (4) lignite-derived fossil carbon. Particle size
analysis, magnetic susceptibility measurements and SEM-EDX techniques indicated
that a great portion of the mineral particles found in the humic horizons of
forests soils are from atmospheric sources. Fly ash accumulation consisting of
ferromagnetic minerals contributes mainly to the 125-63 and <63 μm fractions in
soils. EDX analysis revealed that atmospheric input of lignite-derived fly ash
increases the contents of the following ecological relevant elements in soils:
carbon, iron, aluminium, calcium, potassium, sulphur, titanium and sodium.
C1 Dresden Univ Technol, Inst Soil Sci, Fac Forest Geo & Hydro Sci, Tharandt,
Germany.
Humboldt Univ, Inst Crop Sci, Fac Agr & Hort, Berlin, Germany.
Dresden Univ Technol, Inst Forest Utilizat & Forest Technol, Fac Forest Geo &
Hydro Sci, Tharandt, Germany.
C3 Technische Universitat Dresden; Humboldt University of Berlin;
Technische Universitat Dresden
RP Klose, S (corresponding author), Dresden Univ Technol, Inst Soil Sci, Fac Forest
Geo & Hydro Sci, Tharandt, Germany.
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NR 32
TC 22
Z9 25
U1 0
U2 14
PI DORDRECHT
SN 0049-6979
J9 WATER AIR SOIL POLL
JI Water Air Soil Pollut.
PY 2003
VL 142
IS 1-4
BP 3
EP 25
DI 10.1023/A:1022075130048
PG 23
WC Environmental Sciences; Meteorology & Atmospheric Sciences; Water
Resources
SC Environmental Sciences & Ecology; Meteorology & Atmospheric Sciences;
Water Resources
GA 651CZ
UT WOS:000181303900002
DA 2023-12-05
ER
PT J
AU Rabah, MA
AF Rabah, MA
TI Preparation of aluminium-magnesium alloys and some valuable salts from
used beverage cans
SO WASTE MANAGEMENT
LA English
DT Article
AB The purpose of this work is to recover standard aluminium-magnesium alloy(s) and
some valuable salts from used beverage cans (UBCs). The suggested method updated
the current recycling technology by augmenting removal of the coating paint,
decreasing magnesium loss during melting process and improving hydrochloric acid
leaching of the formed slag. Iron impurity present in the leaching solution, was
removed by oxidation using oxygen gas or hydrogen peroxide and filtered as
goethite. Results obtained revealed that a mixture of methyl ethyl ketone/dimethyl
formamide entirely removes the paint coating at room temperature. The process
compares favorably to the current methods involving firing or swell peeling. The
coating decomposes to titanium dioxide by heating at 750 degreesC for 30 min.
Standard compositions of Al-Mg alloys are formulated using secondary magnesium. The
extent of recovery (R) of these alloy(s) is a function of the melting time and
temperature and type of the flux. The maximum (R) value amounts to 94.4%. Sodium
borate/chloride mix decreases magnesium loss to a minimum. The extent of leaching
valuable salts from the slag increases with increasing the molarity, stoichiometric
ratio and leaching temperature of-the acid used. Removal of iron is a function of
the potential of the oxidation process. Stannous chloride has been recovered from
the recovered and dried salts by distillation at 700-750 degreesC. (C) 2003
C1 Cent Met R&D Inst, Ind Wastes Lab, Cairo 11421, Egypt.
RP Rabah, MA (corresponding author), Cent Met R&D Inst, Ind Wastes Lab, POB 87,
Cairo 11421, Egypt.
EM rucmrdi@rusys.eg.net
RI rabah, mahmoud/ABA-0085-2022
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NR 20
TC 22
Z9 22
U1 3
U2 18
PI OXFORD
SN 0956-053X
EI 1879-2456
J9 WASTE MANAGE
JI Waste Manage.
PY 2003
VL 23
IS 2
BP 173
EP 182
AR PII S0956-053X(02)00152-6
DI 10.1016/S0956-053X(02)00152-6
PG 10
GA 654WX
UT WOS:000181520900010
PM 12623092
DA 2023-12-05
ER
PT J
AU Jian, ZY
Jie, WQ
AF Jian, ZY
Jie, WQ
TI Criterion for judging the homogeneous and heterogeneous nucleation
SO METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND
MATERIALS SCIENCE
LA English
DT Article
AB A criterion for judging the nucleation form in highly undercooled liquid has,
respectively, been derived from the nucleation and structure of liquid. It is found
that the nucleation form of a highly undercooled liquid can be judged by
determining the S-nu in the liquid (where S-nu, is the surface area of the supposed
catalyst in a unit volume of the liquid). When the determined value of S-nu, is
equal to 10(10+/-1) m(-1), the liquid has nucleated homogeneously; it has nucleated
heterogeneously if the determined value of S-nu is less than 10(10+/-1) m(-1). By
calculating the values of S-nu in highly undercooled aluminum, copper, and silver,
it is found that only silver melted under a slag has been undercooled to its
undercooling of homogeneous nucleation.
C1 Northwestern Polytech Univ, State Key Lab Solidificat Proc, Xian 710072, Peoples
R China.
Xian Inst Technol, Dept Mat Sci & Engn, Xian 710032, Peoples R China.
C3 Northwestern Polytechnical University
RP Jian, ZY (corresponding author), Northwestern Polytech Univ, State Key Lab
Solidificat Proc, Xian 710072, Peoples R China.
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OI Jian, Zengyun/0000-0002-0775-9461
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NR 15
TC 22
Z9 28
U1 1
U2 13
PI WARRENDALE
SN 1073-5623
J9 METALL MATER TRANS A
JI Metall. Mater. Trans. A-Phys. Metall. Mater. Sci.
PD FEB
PY 2001
VL 32
IS 2
BP 391
EP 395
DI 10.1007/s11661-001-0270-z
PG 5
Engineering
GA 398VK
UT WOS:000166777000020
DA 2023-12-05
ER
PT J
AU PINTO, M
RODRIGUEZ, M
BESGA, G
BALCAZAR, N
LOPEZ, FA
AF PINTO, M
RODRIGUEZ, M
BESGA, G
BALCAZAR, N
LOPEZ, FA
TI EFFECTS OF LINZ-DONAWITZ (LD) SLAG ON SOIL PROPERTIES AND PASTURE
PRODUCTION IN THE BASQUE COUNTRY (NORTHERN SPAIN)
SO NEW ZEALAND JOURNAL OF AGRICULTURAL RESEARCH
LA English
DT Article
DE SLAG; FERTILIZER; LIMING; SPAIN; PASTURE PRODUCTION; SOIL ACIDITY; SOIL
PROPERTIES
ID NEW-ZEALAND SOILS; ALUMINUM TOXICITY; LIME; PHOSPHORUS; RESPONSES;
FIXATION; ACIDITY; GROWTH; ISLAND; YIELD
AB Linz-Donawitz (LD) slag, containing 29% calcium (Ca), 21% iron (Fe), and 5%
magnesium (Mg), is a by-product of the iron and steel-making industry. It is
produced in large quantities in Europe and poses a substantial disposal problem. A
field trial was conducted to study whether LD slag could be used as a dolomitic
liming agent for pastures. The effects of six LD slag rates (0, 1000, 1500, 3000,
5000, and 7500 kg LD slag/ha), with or without NPK fertiliser, on soil properties,
pasture yield, and botanical composition were investigated at two locations, Derio
and Abadiano (Bizkaia, northern Spain). Soil at Derio was a fine silty, mixed
(acid), mesic Typic Udorthent and at Abadiano a fine loamy, mixed (nonacid), mesic
Aquic Udifluvent. At Derio, the 3-year trial was laid out on a newly established
pasture of perennial ryegrass (Lolium perenne L.), cocksfoot (Dactylis glomerata
L.), and white clover (Trifolium repens L.), whereas at Abadiano the trial was on a
resident pasture dominated by yorkshire fog (Holcus lanatus L.) and browntop
(Agrostis tenuis Sibth.). Application of LD slag increased the soil pH linearly at
both sites. At Derio, the 7500 kg slag/ha rate increased the soil pH from 5.3 to
6.4, whereas at Abadiano the pH was raised from 5.7 to 6.5 and from 5.8 to 6.7 with
and without NPK fertilisation respectively. The increase in pH was accompanied by a
decrease to less than 5% in the percentage of Al saturation in the cation exchange
complex. At Derio, soil exchangeable Ca increased in comparison with the control,
by a factor of 1.8 and 2.3, with and without NPK fertilisation, respectively. At
Derio, pasture yield increased with slag application, the second year responses
being the largest (41% increase with 3000 kg slag/ha). At Abadiano, pasture yield
did not respond to slag, but the botanical composition changed, with the
contribution of browntop and yorkshire fog decreasing, and the contribution of red
fescue (Festuca rubra L.) and ribwort (Planrago lanceolata L.) increasing.
According to the results, LD slag appears to be a useful liming material for
correcting soil acidity on pasture soils. As a consequence, the agronomic use of LD
slags will contribute towards solving the environmental problem of their disposal.
C1 NATL CTR MET RES,E-28040 MADRID,SPAIN.
RP PINTO, M (corresponding author), SERV INVEST & MEJORA AGR,GOBIERNO VASCO B
ARTEAGA 26,E-48016 DERIO,SPAIN.
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NR 33
TC 22
Z9 22
U1 0
U2 9
PU SIR PUBLISHING
PI WELLINGTON
PA PO BOX 399, WELLINGTON, NEW ZEALAND
SN 0028-8233
J9 NEW ZEAL J AGR RES
JI N. Z. J. Agric. Res.
PD MAR
PY 1995
VL 38
IS 1
BP 143
EP 155
DI 10.1080/00288233.1995.9513113
PG 13
WC Agriculture, Multidisciplinary
SC Agriculture
GA RQ479
UT WOS:A1995RQ47900016
OA Bronze
DA 2023-12-05
ER
PT J
AU Zhang, QS
Cao, X
Sun, SC
Yang, WC
Fang, L
Ma, R
Lin, CH
Li, HW
AF Zhang, Qiushi
Cao, Xing
Sun, Shichang
Yang, Weichen
Fang, Lin
Ma, Rui
Lin, Chenghua
Li, Haowen
TI Lead zinc slag-based geopolymer: Demonstration of heavy metal
solidification mechanism from the new perspectives of electronegativity
and ion potential
SO ENVIRONMENTAL POLLUTION
LA English
DT Article
DE Heavy metals; Geopolymers; Solidification mechanism; Ion exchange;
Covalent bonding
ID FLY-ASH; IMMOBILIZATION; STABILIZATION/SOLIDIFICATION; PB2+
AB Lead-zinc slag (LZS) is a solid waste product that is rich in silicon and
aluminum and has enormous resource potential for functional environmental
functional geopolymer materials. Unfortunately, the solidification mechanism of
heavy metals in geopolymers is still unclear, which is detrimental to the heavy
metal solidification of LZS. In this study, we comprehensively studied and
demonstrated the solidification mechanisms of Pb and Zn in geopolymers, based on
the preparation of high-performance LZS-based geopolymers (compressive strength up
to 89.3 MPa, and Pb and Zn solidification efficiency up to 93.1% and 90.0%,
respectively). Thereafter, the solidification mechanism differences between Pb and
Zn were explained by electronegativity and ion potential. Due to the ionic
potential order of Zn2+> Pb2+> Na+, both Zn2+ and Pb2+ could exchange with Na+ in
the geopolymer. In addition, due to the electronegativity order of Pb > Si > Zn, Pb
could attack the [SiO4] structure and form covalent bonds in the Pb-O structure,
while Zn did not (shown by Raman spectroscopy). As a result, Pb simultaneously
solidified in the geopolymer through covalent bonding and ion exchange, while Zn
was solidified mainly by ion exchange. Thus, this work provides new perspectives
and ideas for the solidification mechanisms of heavy metals in geopolymers.
C1 [Zhang, Qiushi; Cao, Xing; Sun, Shichang; Yang, Weichen; Fang, Lin; Ma, Rui;
Lin, Chenghua] Shenzhen Univ, Coll Chem & Environm Engn, Shenzhen 518060, Peoples R
China.
[Sun, Shichang] Shenzhen Univ, Res Ctr Water Sci & Environm Engn, Shenzhen
[Li, Haowen] Micro Opt Instruments Shenzhen Inc, Shenzhen 518129, Peoples R
China.
[Li, Haowen] Guangdong Engn Res Ctr Intelligent Spect, Shenzhen 518118, Peoples
R China.
C3 Shenzhen University; Shenzhen University
RP Ma, R (corresponding author), 3688 Nanhai Rd, Shenzhen 518060, Peoples R China.
EM marui067@163.com
RI Sun, Shichang/AAE-6064-2022; ma, rui/JGE-4890-2023
FU National Natural Science Foundation of China [51878410]; Shenzhen
Science and Technology Program [KQTD20190929173954826]
China (No. 22076127) , the National Natural Science Foundation of China
(No. 51878410) , Shenzhen Science and Technology Program (No.
KQTD20190929173954826) . We thank LetPub ( www.letpub.com ) for its
linguistic assistance during the preparation of this manuscript.
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NR 48
TC 21
Z9 21
U1 20
U2 96
PU ELSEVIER SCI LTD
PI OXFORD
SN 0269-7491
EI 1873-6424
J9 ENVIRON POLLUT
JI Environ. Pollut.
PD JAN 15
PY 2022
VL 293
AR 118509
DI 10.1016/j.envpol.2021.118509
EA NOV 2021
PG 10
GA YJ0PR
UT WOS:000744241700007
PM 34793905
DA 2023-12-05
ER
PT J
AU Cardona, Y
Korili, SA
Gil, A
AF Cardona, Yaneth
Korili, Sophia A.
Gil, Antonio
TI A nonconventional aluminum source in the production of alumina-pillared
clays for the removal of organic pollutants by adsorption
LA English
DT Article
DE Pillared clay; Alumina-pillared montmorillonite; Saline slag;
Adsorption; Organic contaminant removal
ID LAYERED DOUBLE HYDROXIDES; SALINE SLAGS; MICROPOROUS ACCESSIBILITY;
POLYALUMINUM CHLORIDE; THERMAL-TREATMENT; KEGGIN AL-13; AL-30;
MONTMORILLONITE; DROSS; TEMPERATURE
AB This study is the first to propose the use of aluminum saline slag as aluminum
source in the synthesis of alumina pillared clays (Al-PILC). Aluminum was extracted
from this waste using both alkaline and acid solutions and both were compared for
preparation of the intercalation solutions used for the synthesis of Al-PILC.
Variations in parameters such as [OH-]/[Al3+], Al/clay (mmol/g), clay/volume
solution ratios and temperature were studied in the synthesis processes. The solids
obtained were characterized by X-ray diffraction (XRD), N-2 adsorption-desorption
at -196 degrees C, transmission electron microscopy (TEM), scanning electron
microscopy (SEM) and energy-dispersive X-ray spectrometry (EDX), which confirmed
that the pillaring process was successful. PILC obtained from both acid (Al-PILCAE)
and alkaline (Al-PILCBE) extracts were evaluated as adsorbents for three organic
pollutants, namely bisphenol A (BPA), 2,6-dichlorophenol (2,6DCP) and triclosan
(TCS), in batch mode. The resulting adsorption capacities were compared with
montmorillonite (Mt) and an Al-PILC prepared by the conventional method, namely,
dropwise addition of an NaOH solution into an aluminum chloride solution (Al-
PILCCM). In all cases, the effect of factors such as pH, initial concentration of
pollutant, adsorbent dosages and contact time was studied. The kinetic and
equilibrium results obtained were evaluated using both pseudo-first- and pseudo-
second-order kinetics, and Langmuir, Freundlich and Sips equation isotherms for the
equilibrium. The kinetic study showed that the time needed to reach equilibrium was
30, 900 and 510 min for BPA, 2,6DCP and TCS, respectively. Moreover, adsorption
data showed that the Al-PILCAE and Al-PILCBE synthesized have excellent potential
as adsorbents for 2,6DCP and TCS, removing 98.46% and 98.47% of these compounds,
respectively.
C1 [Cardona, Yaneth; Korili, Sophia A.; Gil, Antonio] Univ Publ Navarra, INAMAT2
Dept Ciencias, Edificio Acebos,Campus Arrosadia, Pamplona 31006, Spain.
RP Gil, A (corresponding author), Univ Publ Navarra, INAMAT2 Dept Ciencias,
Edificio Acebos,Campus Arrosadia, Pamplona 31006, Spain.
RI Cardona, Yaneth/AAE-1979-2022; Cardona, Yaneth/HMD-7638-2023
OI Cardona, Yaneth/0000-0003-3323-7242; Cardona, Yaneth/0000-0003-3323-7242
FU Universidad Publica de Navarra (IberusTalent, European Union's H2020
research and innovation program under Marie Sklodowska-Curie grant)
[801586]; Santander Bank
FX YC thanks the Universidad Publica de Navarra for a pre-doctoral grant
(IberusTalent, European Union's H2020 research and innovation program
under Marie Sklodowska-Curie grant agreement No. 801586). AG
also thanks Santander Bank for funding via the Research Intensification
Program.
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NR 80
TC 21
Z9 22
U1 1
U2 20
PI LAUSANNE
SN 1385-8947
EI 1873-3212
J9 CHEM ENG J
JI Chem. Eng. J.
PD DEC 1
PY 2021
VL 425
AR 130708
DI 10.1016/j.cej.2021.130708
EA JUN 2021
PG 21
SC Engineering
GA WG6SY
UT WOS:000707126000147
DA 2023-12-05
ER
PT J
AU Wang, T
Ishida, T
Gu, R
Luan, Y
AF Wang, Tiao
Ishida, Tetsuya
Gu, Rui
Luan, Yao
TI Experimental investigation of pozzolanic reaction and curing
temperature-dependence of low-calcium fly ash in cement system and
Ca-Si-Al element distribution of fly ash-blended cement paste
LA English
DT Article
DE Fly ash; Pozzolanic reaction degree; Modified tangential method;
C-(A)-S-H gel; SEM-EDS
ID BLAST-FURNACE SLAG; SEM-EDS; HYDRATION; PERFORMANCE; CONCRETE; MODEL;
RATIO; XRD
AB Supplementary cementitious materials (SCMs) significantly improve concrete
performance. However, the application of SCMs remains limited by their
heterogeneity and variability. This study investigated the pozzolanic reaction and
curing temperature-dependence of low-calcium fly ash in cement systems over 2
years. The experimental results show that fly ashes have different reactivities and
temperature dependencies even though they have similar material properties. A
modified tangential method was developed for thermogravimetric analysis of the
calcium hydroxide content and chemically bound water of fly ash-blended cement
paste. The chemical composition of an aluminium-modified calcium silicate hydrate
(C-(A)-S-H) gel of fly ash-blended cement paste was studied by scanning electron
microscopy-energydispersive X-ray spectroscopy (SEM-EDS) with image analysis. The
experimental results show that as the Ca/Si ratio decreased in fly ash-cement
paste, the Al/Si ratio increased. The Al/Si distribution of fly ash-blended cement
paste varies widely from 0.05 to 0.50 with no specific maximum. The typical Ca/Si
and Al/Si ratios of C-(A)-S-H gel in fly ash cement paste are approximately 1.40
and 0.25. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Wang, Tiao; Ishida, Tetsuya] Univ Tokyo, Sch Engn, Dept Civil Engn, Concrete
Lab,Bunkyo Ku, 7-3-1 Hongo, Tokyo 1138656, Japan.
[Gu, Rui] Southern Univ Sci & Technol, Core Res Facil, Shenzhen 518055, Peoples
R China.
[Luan, Yao] Saitama Univ, Dept Civil & Environm Engn, Saitama 3388570, Japan.
C3 University of Tokyo; Southern University of Science & Technology;
Saitama University
RP Wang, T (corresponding author), Univ Tokyo, Sch Engn, Dept Civil Engn, Concrete
Lab,Bunkyo Ku, 7-3-1 Hongo, Tokyo 1138656, Japan.
EM wang@concrete.t.u-tokyo.ac.jp; tetsuya.ishida@civil.t.u-tokyo.ac.jp;
gur@sustech.edu.cn; luanyao@mail.saitama-u.ac.jp
RI Ishida, Tetsuya/AAE-1600-2019
OI Ishida, Tetsuya/0000-0001-7875-1101
FU Japan Society for the Promotion of Science [17H01284, 19K15059];
Grants-in-Aid for Scientific Research [19K15059, 17H01284] Funding
Source: KAKEN
FX The authors acknowledge the Core Research Facilities of Southern
University of Science and Technology for its technical support on the
SEM-EDS tests. The authors are grateful for the financial support
received from Japan Society for the Promotion of Science (Project code:
17H01284 and 19K15059).
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NR 43
TC 21
Z9 23
U1 8
U2 34
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JAN 18
PY 2021
VL 267
AR 121012
DI 10.1016/j.conbuildmat.2020.121012
PG 14
GA PN6FP
UT WOS:000604573000076
DA 2023-12-05
ER
PT J
AU Li, XY
Yu, LW
Zhou, H
Huang, G
Yang, CH
Wu, F
Zhang, Y
AF Li, Xinyuan
Yu, Linwen
Zhou, Huan
Huang, Gang
Yang, Changhui
Wu, Fang
Zhang, Yi
TI An environment-friendly pretreatment process of municipal solid waste
incineration fl y ash to enhance the immobilization ef fi ciency by
alkali-activated slag cement
LA English
DT Article
DE Alkali-activated slag cement; Municipal solid waste incineration fly
ash; Volumetric stability; Pretreatment; Metallic aluminum; Water
immersion
AB Municipal solid waste incineration (MSWI) fly ash can cause serious early volume
expansion when stabilized and solidified by cementitious materials. Many
pretreatment processes have been reported, such as alkali solution, milling and
chelating etc. However, these processes may lead to second pollution or higher
costs. This study proposed an original pretreatment process of MSWI fly ash, and
investigated its effect on the immobilization efficiency by alkali-activated slag
(AAS) cement. The possible reasons for volume instability were assumed and analyzed
by gas chromatography, scanning electron microscopy, Xray diffraction, hydrostatic
testing and leaching tests. It was found that the 0.377 wt% of metallic aluminum is
the main expansive source of volume expansion in early stage (within 24 h). Due to
the amphoteric characteristic of Al, it is possible to eliminate it using either
acid or alkaline. Considering the fact that alkali-activated system and the fly ash
were both alkaline, this study chose water immersion to pre-treat the fly ash,
aiming to avoid the possible neutralization process of acid treatment and the
entrained extra alkali component of alkali treatment, which may greatly affect many
characteristics of alkali-activated slag. After pretreatment, the solidified
specimens showed lower water demand (with a water to cement ratio of merely 0.27)
and higher compressive strength due to the refined and smoothed particles. The
volume expansive rate was greatly reduced, giving the better volumetric stability
and encapsulation rate. Up to 90% MSWI fly ash-added solidified bodies feature a
volume expansive rate of less than 0.09%. The alkali-activated slag pastes can
effectively immobilize up to 70% treated fly ash with the leaching rate of
solidified particles lower than the limits recommended by Chinese standard,
Identification for extraction toxicity (CSEPA GB 5085.1, 2007). Therefore, the
pretreatment process is easy to operate and is a promising way to increase the
immobilization efficiency of alkali-activated slag cement.
C1 [Li, Xinyuan; Yu, Linwen; Zhou, Huan; Yang, Changhui; Wu, Fang] Chongqing Univ,
Coll Mat Sci & Engn, Chongqing 400045, Peoples R China.
[Yu, Linwen; Yang, Changhui] Chongqing Engn Res Ctr High Performance Concrete,
[Huang, Gang] Chongqing Construct Project Cost Management Bur, Chongqing 400022,
Peoples R China.
[Zhang, Yi] Chongqing Construct Residential Engn Co Ltd, Chongqing 400015,
Peoples R China.
RP Yu, LW; Yang, CH (corresponding author), Chongqing Univ, Coll Mat Sci & Engn,
EM linwen.yu@cqu.edu.cn; ychh@cqu.edu.cn
RI YU, Linwen/C-2322-2016; fang, li/JNS-8415-2023; ZHOU, YUE/IZE-6277-2023;
YU, Linwen/JCO-1535-2023
OI YU, Linwen/0000-0002-3360-2484; YU, Linwen/0000-0002-3360-2484
FU National Natural Science Foundation of China [51778089]; Natural Science
Foundation of Chongqing, China [cstc2019jcyj-bshX0015,
cstc2019jscx-msxmX0304]
Foundation of China (No. 51778089), Natural Science Foundation of
Chongqing, China (Grant No. cstc2019jcyj-bshX0015,
cstc2019jscx-msxmX0304).
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NR 50
TC 21
Z9 21
U1 9
U2 68
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAR 25
PY 2021
VL 290
AR 125728
DI 10.1016/j.jclepro.2020.125728
EA JAN 2021
PG 12
& Ecology
GA QK3IT
UT WOS:000620274900012
DA 2023-12-05
ER
PT J
AU Reddy, KC
Gudur, C
Subramaniam, KVL
AF Reddy, K. Chiranjeevi
Gudur, Chetana
Subramaniam, Kolluru V. L.
TI Study on the influences of silica and sodium in the alkali-activation of
ground granulated blast furnace slag
LA English
DT Article
DE Slag; Hydration; Nano-silica; C-(A)-S-H; Alkali-activated; Waterglass
ID FLY ASH BLENDS; REACTION-KINETICS; EARLY HYDRATION; PORE SOLUTION; PART
I; S-H; CALCIUM; CEMENT; STRENGTH; MORTARS
AB Slag is activated with alkali-silicate solutions made with nano-silica and
waterglass. The reaction kinetics and the reaction products formed are evaluated
for different silica and sodium contents. Isothermal calorimetric measurements with
in-situ mixing reveal increased early reactivity with added silica, while the main
hydration reaction is delayed. The presence of Na with dissolved silica in the
activating solution does not influence the initial dissolution and early reactivity
of slag. At the same time, it has an accelerating effect on the main hydration peak
of slag. Dissolution studies of slag in alkaline solution with added silica
indicate the immediate formation of calcium silicate hydrates after dissolution
contributes to the early reactivity. The enhanced early reaction product formation
in the presence of dissolved silica leads to the very rapid development of the
internal structure. Rheological measurements indicate an early loss of workability
due to increased early reactivity. The increase in time for the main hydration
reaction of slag in the presence of added silica, however, delays the setting
behavior. The primary reaction product in alkali-activated slag is calcium silicate
hydrate with aluminum uptake, C-(A)-S-H. The addition of silica in the activating
solution leads to its larger incorporation in the C-(A)-S-H and higher compressive
strength. The sodium content in the activating solution does not contribute to the
ultimate strength. The sodium in the alkali-activated slag is present in the form
of a water-soluble amorphous product. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Reddy, K. Chiranjeevi; Gudur, Chetana; Subramaniam, Kolluru V. L.] Indian Inst
Technol Hyderabad, Dept Civil Engn, Hyderabad 502285, TS, India.
Technology (IIT) - Hyderabad
RP Subramaniam, KVL (corresponding author), Indian Inst Technol Hyderabad, Dept
Civil Engn, Hyderabad 502285, TS, India.
EM KVLS@iith.ac.in
RI Kamasani, Chiranjeevi Reddy/HHN-1908-2022; Subramaniam,
Kolluru/AAQ-4467-2021
OI Kamasani, Chiranjeevi Reddy/0000-0003-0289-4872; Subramaniam,
Kolluru/0000-0002-5995-0911
FU Department of Science and Technology, Initiative to Promote Energy
Efficient Habitant (I-PHEE) Grant [TMD/CERI/BEE/2016/031]
FX The authors would like to acknowledge support from the Department of
Science and Technology, Initiative to Promote Energy Efficient Habitant
(I-PHEE) Grant No. TMD/CERI/BEE/2016/031.
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NR 64
TC 21
Z9 21
U1 6
U2 37
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 10
PY 2020
VL 257
AR 119514
DI 10.1016/j.conbuildmat.2020.119514
PG 12
GA MF8AJ
UT WOS:000545559400034
DA 2023-12-05
ER
PT J
AU Dueramae, S
Tangchirapat, W
Sukontasukkul, P
Chindaprasirt, P
Jaturapitakkul, C
AF Dueramae, Saofee
Tangchirapat, Weerachart
Sukontasukkul, Piti
Chindaprasirt, Prinya
Jaturapitakkul, Chai
TI Investigation of compressive strength and microstructures of activated
cement free binder from fly ash - calcium carbide residue mixture
LA English
DT Article
DE Fly ash; Calcium carbide residue; Compressive strength; Microstructural
properties
ID A-S-H; MECHANICAL-PROPERTIES; CURING TEMPERATURES; ALUMINUM; SLAG
AB This paper investigates compressive strength and microstructural properties of
activated cement free binder from fly ash (FA) - calcium carbide residue (CC).
Different activation methods to enhance the strength of the FA-CC mixture were used
including the following: 1) curing at elevated temperature of 60 degrees C, 2)
adding 1% NaOH by weight of binder and 3) combining both 1% NaOH by weight of
binder and curing at temperature of 60 degrees C. The compressive strengths of
mortars with different activation techniques were determined at 3, 7, 28, and 90
days. Microstructural properties of activated cement free binder from the FA-CC
mixture, that is, XRD patterns, SEM microscopy, EDS analysis, and degree of
reaction were examined. Results from this study revealed that the activated cement
free binder from FA-CC had components of Ca, Al, and Si and indicated CSH and CASH
likewise the end products of pozzolanic reaction. Use of activation techniques had
significantly affected on the microstructure in cementing system. The activated
cement free binder from FA-CC mixture with addition of 1% NaOH and curing at 60
degrees C increased binder strength and promoted the formation of CSH, CASH, and
some amount of NASH phase or hybrid C(N)ASH. (C) 2019 The Authors. Published by
Elsevier B.V.
C1 [Dueramae, Saofee] Rajamangala Univ Technol Krungthep, Fac Engn, Dept Civil
Engn, Bangkok 10120, Thailand.
[Tangchirapat, Weerachart; Jaturapitakkul, Chai] King Mongkuts Univ Technol
Thonburi, Fac Engn, Dept Civil Engn, Bangkok 10140, Thailand.
[Sukontasukkul, Piti] King Mongkuts Univ Technol North Bangkok, Fac Engn, Dept
Civil Engn, Construct & Bldg Mat Res Ctr, Bangkok 10800, Thailand.
[Chindaprasirt, Prinya] Khon Kaen Univ, Fac Engn, Sustainable Infrastruct Res &
Dev Ctr, Dept Civil Engn, Khon Kaen 40002, Thailand.
[Chindaprasirt, Prinya] Royal Soc Thailand, Acad Sci, Bangkok 10300, Thailand.
C3 Rajamangala University of Technology Krungthep; King Mongkuts University
of Technology Thonburi; King Mongkuts University of Technology North
Bangkok; Khon Kaen University
RP Tangchirapat, W (corresponding author), King Mongkuts Univ Technol Thonburi, Fac
Engn, Dept Civil Engn, Bangkok 10140, Thailand.
EM weerachart.tan@kmutt.ac.th
RI Sukontasukkul, Piti/V-2304-2017; Chindaprasirt, Prinya/F-6768-2010
OI Sukontasukkul, Piti/0000-0002-9580-7063; Chindaprasirt,
Prinya/0000-0003-1062-3626
FU Petchra Pra Jom Klao Ph.D. Scholarship, King Mongkut's University of
Technology Than bun; Thailand Research Fund (TRF) under the TRF Research
Career Development [RSA6280032]; TRF Distinguished Research Professor
Grant [DPG6180002]
FX This study was supported by the Petchra Pra Jom Klao Ph.D. Scholarship,
King Mongkut's University of Technology Than bun. The authors also
gratefully acknowledged the Thailand Research Fund (TRF) under the TRF
Research Career Development Grant No. RSA6280032 and the TRF
Distinguished Research Professor Grant No. DPG6180002.
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NR 32
TC 21
Z9 23
U1 3
U2 18
PU ELSEVIER
PI AMSTERDAM
SN 2238-7854
EI 2214-0697
PD SEP-OCT
PY 2019
VL 8
IS 5
BP 4757
EP 4765
DI 10.1016/j.jmrt.2019.08.022
PG 9
Engineering
GA IY8FP
UT WOS:000486630400106
OA gold
DA 2023-12-05
ER
PT J
AU Gomes, HI
Mayes, WM
Whitby, P
Rogerson, M
AF Gomes, Helena I.
Mayes, William M.
Whitby, Paul
Rogerson, Mike
TI Constructed wetlands for steel slag leachate management: Partitioning of
arsenic, chromium, and vanadium in waters, sediments, and plants
LA English
DT Article
DE Alkaline drainage; Reedbeds; Passive treatment; Sediments; Phragmites
australis
ID HEAVY-METALS; ALKALINE; RECOVERY; BIOACCUMULATION; REMOVAL; SLUDGE;
WASTE; NEUTRALIZATION; ACCUMULATION; BEHAVIOR
AB Constructed wetlands can treat highly alkaline leachate resulting from the
weathering of steel slag before reuse (e.g. as aggregate) or during disposal in
repositories and legacy sites. This study aimed to assess how metal(loid)s soluble
at high pH, such as arsenic (As), chromium (Cr), and vanadium (V) are removed in
constructed wetlands and how they accumulate in the sediments and the plants
(Phragmites australis, common reed). The results show that reedbeds were very
effective at removing calcium (98%), aluminium (81%), barium (98%), chromium (90%),
gallium (80%), nickel (98%), and zinc (98%), and lowering pH and alkalinity. No
statistical difference was found for As and V between leachate influent and wetland
samples, showing that these metal(loid)s were not efficiently removed. As, Cr, and
V were significantly higher in the reedbed sediments than in a reference site.
However, sediment concentrations are not at levels that would pose a concern
regarding reuse for agricultural purposes (average values of 39 +/- 26 mg kg(-1)
for As, 108 +/- 15 mg kg(-1) for Cr, and 231 +/- 34 mg kg(-1) for V). Also, there
is no significant uptake of metals by the aboveground portions of the reeds
compared to reference conditions. Results show statistically significant enrichment
in metal(loid)s in rhizomes and also a seasonal effect on the Cr concentrations.
The data suggest minimal risk of oxyanion-forming element uptake and cycling in
wetlands receiving alkaline steel slag.
C1 [Gomes, Helena I.; Mayes, William M.; Rogerson, Mike] Univ Hull, Dept Geog Geol
& Environm, Cottingham Rd, Kingston Upon Hull HU6 7RX, N Humberside, England.
[Gomes, Helena I.] Univ Nottingham, Food Water Waste Res Grp, Univ Pk,
Nottingham NG7 2RD, England.
[Gomes, Helena I.] Univ Nottingham, Fac Engn, Univ Pk, Nottingham NG7 2RD,
England.
[Whitby, Paul] British Steel, Brigg Rd, Scunthorpe DN16 1BP, England.
C3 University of Hull; University of Nottingham; University of Nottingham
RP Gomes, HI (corresponding author), Univ Hull, Dept Geog Geol & Environm,
Cottingham Rd, Kingston Upon Hull HU6 7RX, N Humberside, England.
EM helena.gomes@nottingham.ac.uk
RI Gomes, Helena I./H-7557-2019; Mayes, William/ABA-8647-2021
OI Gomes, Helena I./0000-0003-1131-7604; Mayes,
William/0000-0002-1864-9057; Rogerson, Mike/0000-0001-6016-0549
FU UK Natural Environment Research Council [NE/L014211/1]; UK Economic and
Social Research Council [NE/L014211/1]; UK Department for Environment,
Food and Rural Affairs under the Resource Recovery from Waste theme
[NE/L014211/1]; NERC [NE/L014211/1, NE/L01405X/1] Funding Source: UKRI
FX This project was funded by the UK Natural Environment Research Council,
Economic and Social Research Council and the Department for Environment,
Food and Rural Affairs under the Resource Recovery from Waste theme via
grant NE/L014211/1. Many thanks to Prof. Dan Parsons for the loan of the
auto-sampler ISCO 6712. Bob Knight and Mike Thompson performed the
microwave digestion of plants and sediments and the ICP analysis. Thanks
to Dr Timothy Prior for the XRD analysis. Thanks to Craig Wood, Matt
Wilson, Christopher Dixon, and Richard Borrill from British Steel
(Scunthorpe) for granting us access to the site and the results of the
Yarborough leachate analysis.
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NR 55
TC 21
Z9 21
U1 7
U2 47
PI LONDON
SN 0301-4797
EI 1095-8630
J9 J ENVIRON MANAGE
PD AUG 1
PY 2019
VL 243
BP 30
EP 38
DI 10.1016/j.jenvman.2019.04.127
PG 9
GA IC6NR
UT WOS:000471089300004
PM 31078927
OA hybrid, Green Published, Green Accepted
DA 2023-12-05
ER
PT J
AU Gong, K
Cheng, YQ
Daemen, LL
White, CE
AF Gong, Kai
Cheng, Yongqiang
Daemen, Luke L.
White, Claire E.
TI In situ quasi-elastic neutron scattering study on the water
dynamics and reaction mechanisms in alkali-activated slags
SO PHYSICAL CHEMISTRY CHEMICAL PHYSICS
LA English
DT Article
ID HYDRATING TRICALCIUM SILICATE; REACTION-KINETICS; CALCIUM-SILICATE;
ACCELERATED CARBONATION; STRUCTURAL-ANALYSIS; SELF-DIFFUSION; CEMENT
PASTES; FLY-ASH; EVOLUTION; METAKAOLIN
AB In this study, in situ quasi-elastic neutron scattering (QENS) has been employed
to probe the water dynamics and reaction mechanisms occurring during the formation
of NaOH- and Na2SiO3-activated slags, an important class of low-CO2 cements, in
conjunction with isothermal conduction calorimetry (ICC), Fourier transform
infrared spectroscopy (FTIR) analysis and N-2 sorption measurements. We show that
the single ICC reaction peak in the NaOH-activated slag is accompanied with a
transformation of free water to bound water (from QENS analysis), which directly
signals formation of a sodium-containing aluminum-substituted calcium-silicate-
hydrate (C-(N)-A-S-H) gel, as confirmed by FTIR. In contrast, the Na2SiO3-activated
slag sample exhibits two distinct reaction peaks in the ICC data, where the first
reaction peak is associated with conversion of constrained water to bound and free
water, and the second peak is accompanied by conversion of free water to bound and
constrained water (from QENS analysis). The second conversion is attributed to
formation of the main reaction product (i.e., C-(N)-A-S-H gel) as confirmed by FTIR
and N-2 sorption data. Analysis of the QENS, FTIR and N-2 sorption data together
with thermodynamic information from the literature explicitly shows that the first
reaction peak is associated with the formation of an initial gel (similar to C-(N)-
A-S-H gel) that is governed by the Na+ ions and silicate species in Na2SiO3
solution and the dissolved Ca/Al species from slag. Hence, this study exemplifies
the power of in situ QENS, when combined with laboratory-based characterization
techniques, in elucidating the water dynamics and associated chemical mechanisms
occurring in complex materials, and has provided important mechanistic insight on
the early-age reactions occurring during formation of two alkali-activated slags.
C1 [Gong, Kai; White, Claire E.] Princeton Univ, Dept Civil & Environm Engn,
Princeton, NJ 08544 USA.
[Gong, Kai; White, Claire E.] Princeton Univ, Andlinger Ctr Energy & Environm,
Princeton, NJ 08544 USA.
[Cheng, Yongqiang; Daemen, Luke L.] Oak Ridge Natl Lab, Chem & Engn Mat Div, Oak
Ridge, TN 37830 USA.
C3 Princeton University; Princeton University; United States Department of
Energy (DOE); Oak Ridge National Laboratory
RP White, CE (corresponding author), Princeton Univ, Dept Civil & Environm Engn,
Princeton, NJ 08544 USA.; White, CE (corresponding author), Princeton Univ,
Andlinger Ctr Energy & Environm, Princeton, NJ 08544 USA.
EM whitece@princeton.edu
RI Gong, Kai/HNT-0798-2023; GONG, kai/N-7843-2019; Cheng,
Yongqiang/F-6567-2010; White, Claire E/A-1722-2011
OI GONG, kai/0000-0002-5884-4607; White, Claire E/0000-0002-4800-7960;
Cheng, Yongqiang/0000-0002-3263-4812
FU National Science Foundation [1362039]; Princeton University; Div Of
Civil, Mechanical, & Manufact Inn; Directorate For Engineering [1362039]
Funding Source: National Science Foundation
FX This work was supported by the National Science Foundation under Grant
No. 1362039. KG's participation was enabled by a Charlotte Elizabeth
Procter Fellowship from Princeton University. The authors would like to
acknowledge the use of the VISION beamline at the Spallation Neutron
Source, a DOE Office of Science User Facility operated by the Oak Ridge
National Laboratory. The authors would like to thank Mr Eric R.
McCaslin, Dr Timmy Ramirez-Cuesta and Dr Eugene Mamontov for interesting
discussions and/or suggestions on data analysis.
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NR 92
TC 21
Z9 23
U1 2
U2 29
PI CAMBRIDGE
ENGLAND
SN 1463-9076
EI 1463-9084
J9 PHYS CHEM CHEM PHYS
JI Phys. Chem. Chem. Phys.
PD MAY 28
PY 2019
VL 21
IS 20
BP 10277
EP 10292
DI 10.1039/c9cp00889f
PG 16
WC Chemistry, Physical; Physics, Atomic, Molecular & Chemical
SC Chemistry; Physics
GA IK4MM
UT WOS:000476561000003
PM 31070223
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Zhang, L
Wang, WL
Shao, HQ
AF Zhang, Lei
Wang, Wan-lin
Shao, Han-qing
TI Review of non-reactive CaO-Al2O3-based mold fluxes
for casting high-aluminum steel
LA English
DT Review
DE High-Al steel; CaO-Al2O3-based mold flux; Thermophysical property;
Lubrication; Crystallization
ID HIGH-AL STEEL; CRYSTALLIZATION BEHAVIOR; HEAT-TRANSFER; VISCOUS
BEHAVIOR; TIO2 ADDITION; SLAG; VISCOSITY; LI2O; PERFORMANCE; SYSTEM
AB Advanced high-strength steels (AHSSs) have been gradually applied to modern auto
industry, as they have the advantages of improving the steel strength and
lightening the car weight, which not only ensures the safety but also saves the
energy. However, the high-aluminum (Al) content in AHSSs may react with SiO2 in
conventional CaO-SiO2-based mold flux during the process of continuous casting,
which leads to the deterioration of the mold flux properties and a poor slab
quality. Then, the non-reactive CaO-Al2O3-based mold flux was proposed and has been
developing for the casting process of high-Al steels, but there are some problems
of low consumption and insufficient lubrication that need to be solved. Thus,
previous researches on the effect of each component on the properties of CaO-Al2O3-
based mold flux were systematically summarized, and the situation of plant trials
on CaO-Al2O3-based mold flux was evaluated. The results indicated that the proposed
CaO-Al2O3-based mold fluxes could avoid the slag-metal reaction problems; however,
the problems of lubrication, crystallization and heat transfer issues still exist.
Therefore, tremendous works still need to be conducted for the development of new
generation of CaO-Al2O3-based mold flux system. The review was performed aiming to
provide a technical guidance for designing and optimizing CaO-Al2O3-based mold flux
system that meets the demand of the continuous casting process of high-Al steels.
C1 [Zhang, Lei; Wang, Wan-lin; Shao, Han-qing] Cent S Univ, Sch Met & Environm,
EM wanlin.wang@csu.edu.cn
RI Zhang, Lei/ABA-4375-2021
OI Zhang, Lei/0000-0002-1758-5733
FU National Natural Science Foundation of China [U1760202, 51661130154];
Newton Advanced fellowship [NA150320]
FX The financial support from National Natural Science Foundation of China
(U1760202, 51661130154) and the Newton Advanced fellowship (NA150320) is
greatly acknowledged.
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NR 47
TC 21
Z9 24
U1 5
U2 66
PU SPRINGER
PI NEW YORK
SN 1006-706X
EI 2210-3988
PD APR
PY 2019
VL 26
IS 4
SI SI
BP 336
EP 344
DI 10.1007/s42243-018-00226-2
PG 9
GA HX8DO
UT WOS:000467636400002
DA 2023-12-05
ER
PT J
AU Zhu, XF
Zheng, SL
Zhang, Y
Fang, ZGZ
Zhang, M
Sun, P
Li, Q
Zhang, Y
Li, P
Jin, W
AF Zhu, Xiaofang
Zheng, Shili
Zhang, Ying
Fang, Zhigang Zak
Zhang, Min
Sun, Pei
Li, Qing
Zhang, Yang
Li, Ping
Jin, Wei
TI Potentially More Ecofriendly Chemical Pathway for Production of
High-Purity TiO2 from Titanium Slag
LA English
DT Article
DE Titanium dioxide; Titania slag; Aluminothermic reduction; Mild acid
digestion; Controlled hydrolysis
ID SURFACE-TENSION; DIOXIDE; MG; REDUCTION; BROOKITE; ALUMINUM; KINETICS;
REMOVAL; ENERGY; SYSTEM
AB TiO2 is an important inorganic material which is commercially produced by either
the chloride or the sulfate process. In general, the latter has lower cost and a
lower entry barrier than the former. However, the environmental impact associated
with the sulfate process is more visible than the chloride process because the
sulfuric acid with a low concentration (similar to 20 wt %) cannot be cost-
effectively recycled; therefore, it has to be neutralized, generating a large
amount of wet and useless red gypsum (RG). In this research, a potentially more
ecofriendly chemical pathway for TiO2 production from concentrated titanium ore,
aka titania slag, is presented. The new method consists of three critical steps
including transformation of the titania slag to a lower-valence titanium suboxide
by aluminothermic reduction, digestion by using mild acid, and controlled
hydrolysis accompanied by acid recycling. As a result of the phase transformation,
the digestion of titanium from the titanium feedstock becomes easier such that it
is feasible to use relatively mild acid to replace concentrated acid, reducing the
environmental impact from the red gypsum because the need for neutralizing the
waste acid can be eliminated. High-purity hydrous TiO2 can be prepared after
hydrolysis, and the spent liquor can be effectively recycled back to the digestion
unit.
C1 [Zhu, Xiaofang; Zheng, Shili; Zhang, Ying; Li, Qing; Zhang, Yang; Li, Ping; Jin,
Wei] Chinese Acad Sci, Key Lab Green Proc & Engn, Natl Engn Lab Hydromet Cleaner
Prod Technol, Inst Proc Engn, 1,Bei Er Jie, Beijing 100190, Peoples R China.
[Zhu, Xiaofang] Univ Chinese Acad Sci, 19,Yuquan Rd, Beijing 100049, Peoples R
China.
[Fang, Zhigang Zak; Sun, Pei] Univ Utah, Dept Met Engn, Room 412,135 S 1460 E,
Salt Lake City, UT 84112 USA.
[Zhang, Min] Foshan Univ, Coll Mat Sci & Energy Engn, 18,Jiangwan 1 Rd, Foshan
528000, Guangdong, Peoples R China.
Chinese Academy of Sciences; University of Chinese Academy of Sciences,
CAS; Utah System of Higher Education; University of Utah; Foshan
University
RP Zhang, Y (corresponding author), Chinese Acad Sci, Key Lab Green Proc & Engn,
Natl Engn Lab Hydromet Cleaner Prod Technol, Inst Proc Engn, 1,Bei Er Jie, Beijing
EM zhangying@ipe.ac.cn
RI jin, wei/HPD-7106-2023; Jin, Wei/ABD-7771-2021; Sun, Pei/ABE-6221-2021;
Li, Ping/P-9504-2015
OI Jin, Wei/0000-0003-2671-1989; Li, Ping/0000-0002-5758-1075; Fang,
Zhigang/0000-0001-9555-6412
FU Natural Science Foundation of China [51771179]; Beijing Municipal
Natural Science Foundation [2192056]; CAS Interdisciplinary Innovation
Team; State Key Laboratory of Vanadium and Titanium Resources
Comprehensive Utilization; ARPA-E of the US DOE [DE-AR0000420]
China under Grant 51771179 and the Beijing Municipal Natural Science
Foundation under Grant 2192056. The financial support from the CAS
Interdisciplinary Innovation Team and the State Key Laboratory of
Vanadium and Titanium Resources Comprehensive Utilization were also
acknowledged. In addition, this work was supported in part by the ARPA-E
of the US DOE under Contract DE-AR0000420.
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NR 50
TC 21
Z9 21
U1 6
U2 51
PI WASHINGTON
SN 2168-0485
PD MAR 4
PY 2019
VL 7
IS 5
BP 4821
EP 4830
PG 19
GA HO0NN
UT WOS:000460600500028
DA 2023-12-05
ER
PT J
AU Mu, HY
Zhang, TS
Fruehan, RJ
Webler, BA
AF Mu, Haoyuan
Zhang, Tongsheng
Fruehan, Richard J.
Webler, Bryan A.
TI Reduction of CaO and MgO Slag Components by Al in Liquid Fe
LA English
DT Article
ID SECONDARY REFINING PROCESS; FERRITIC STAINLESS-STEEL; KINETIC-MODEL;
MOLTEN STEEL; DEOXIDATION EQUILIBRIA; NONMETALLIC INCLUSIONS; CALCIUM
TREATMENT; ALLOYED STEEL; EVOLUTION; ALUMINUM
AB This study documents laboratory-scale observations of reactions between Fe-Al
alloys (0.1 to 2 wt pct Al) with slags and refractories. Al in steels is known to
reduce oxide components in slag and refractory. With continued development of Al-
containing Advanced High-Strength Steel (AHSS) grade, the effects of higher Al must
be examined because reduction of components such as CaO and MgO could lead to
uncontrolled modification of non-metallic inclusions. This may lead to castability
or in-service performance problems. In this work, Fe-Al alloys and CaO-MgO-Al2O3
slags were melted in an MgO crucible and samples were taken at various times up to
60 minutes. Inclusions from these samples were characterized using an automated
scanning electron microscope equipped with energy dispersive x-ray analysis
(SEM/EDS). Initially Al2O3 inclusions were modified to MgAl2O4, then MgO, then MgO
+ CaO-Al2O3-MgO liquid inclusions. Modification of the inclusions was faster at
higher Al levels. Very little Ca modification was observed except at 2 wt pct Al
level. The thermodynamic feasibility of inclusion modification and some of the mass
transfer considerations that may have led to the differences in the Mg and Ca
modification behavior were discussed.
C1 [Mu, Haoyuan] Adv Refractories Div Vesuvius, Bettsville, OH 44815 USA.
[Zhang, Tongsheng; Fruehan, Richard J.; Webler, Bryan A.] Carnegie Mellon Univ,
Ctr Iron & Steelmaking Res, Pittsburgh, PA 15213 USA.
[Zhang, Tongsheng] Cent S Univ, Sch Met & Environm, Changsha, Hunan, Peoples R
China.
[Zhang, Tongsheng] Cent S Univ, Natl Ctr Int Res Clean Met, Changsha, Hunan,
Peoples R China.
[Webler, Bryan A.] Carnegie Mellon Univ, Mat Sci & Engn Dept, Pittsburgh, PA
15213 USA.
C3 Carnegie Mellon University; Central South University; Central South
University; Carnegie Mellon University
RP Webler, BA (corresponding author), Carnegie Mellon Univ, Ctr Iron & Steelmaking
Res, Pittsburgh, PA 15213 USA.
EM webler@cmu.edu
OI Webler, Bryan/0000-0003-1032-8678; Mu, Haoyuan/0000-0001-5976-1849
FU [MCF-677785]
FX We gratefully acknowledge support from the industrial members of the
Center for Iron and Steelmaking Research as well as helpful discussions
with Prof. Chris Pistorius. We also acknowledge the use of the Materials
Characterization Facility at Carnegie Mellon University supported by
Grant MCF-677785.
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NR 39
TC 21
Z9 23
U1 0
U2 23
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2018
VL 49
IS 4
BP 1665
EP 1674
DI 10.1007/s11663-018-1294-8
PG 10
Engineering
GA GM8IO
UT WOS:000438469300013
DA 2023-12-05
ER
PT J
AU Jiang, XX
Liu, GR
Wang, M
Liu, WB
Tang, C
Li, L
Zheng, MH
AF Jiang, Xiaoxu
Liu, Guorui
Wang, Mei
Liu, Wenbin
Tang, Chen
Li, Li
Zheng, Minghui
TI Case study of polychlorinated naphthalene emissions and factors
influencing emission variations in secondary aluminum production
LA English
DT Article
DE Secondary aluminum production; Smelting stages; Polychlorinated
naphthalene; Solid residues; Chloride additives
ID DIBENZO-P-DIOXINS; POLYCYCLIC AROMATIC-HYDROCARBONS; ATMOSPHERIC
EMISSION; RELATIVE POTENCIES; COKING INDUSTRIES; BIPHENYLS; PLANT;
METALLURGY; RESPONSES; SEDIMENT
AB Secondary aluminum production has been recognized as an important source of
polychlorinated naphthalenes (PCNs). Large variations in PCN emissions as the
smelting process proceeds have not been determined. In this study, solid and
gaseous discharges, including fly ash, slag, and stack gas samples collected from
four secondary smelting plants during different smelting stages were analyzed for
PCNs. The average emission factor of Sigma(1-8)PCNs to air was calculated to be
17.4 mg t(-1), with a range of 4.3-29.5 mg t(-1). The average emission factors of
Sigma(1-8)PCNs from fly ash and slag were 55.5 ng t(-1) and 0.13 ng t(-1),
respectively. The derived emission factors may enable a more accurate estimation of
annual emissions and a more comprehensive knowledge of the distribution of PCNs
emitted from secondary aluminum production. The emission levels and characteristics
of PCNs during different smelting stages were compared. Possible factors, including
the organic impurities from aluminum scrap, fuel, and chloride additives, which
could contribute to variations in PCN emissions and characteristics were discussed.
These results may provide useful information for developing better control
strategies for reducing PCN emissions in secondary aluminum production. (C) 2015
C1 [Jiang, Xiaoxu; Liu, Guorui; Wang, Mei; Liu, Wenbin; Tang, Chen; Li, Li; Zheng,
Minghui] Chinese Acad Sci, Res Ctr Ecoenvironm Sci, State Key Lab Environm Chem &
Ecotoxicol, Beijing 100085, Peoples R China.
C3 Chinese Academy of Sciences; Research Center for Eco-Environmental
Sciences (RCEES)
RP Liu, GR (corresponding author), Chinese Acad Sci, Res Ctr Ecoenvironm Sci, State
Key Lab Environm Chem & Ecotoxicol, POB 2871, Beijing 100085, Peoples R China.
EM grliu@rcees.ac.cn; zhengmh@rcees.ac.cn
RI liu, wen/HGE-3071-2022; 刘, 国瑞/GYD-5312-2022
OI 刘, 国瑞/0000-0002-8462-6734
FU National 973 Program [2015CB453100]; National Natural Science Foundation
of China [21477147, 21477150]; Chinese Academy of Sciences [YSW2013A01]
FX We gratefully acknowledge support from the National 973 Program
(2015CB453100), National Natural Science Foundation of China (21477147,
21477150), and Chinese Academy of Sciences (YSW2013A01).
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NR 36
TC 21
Z9 21
U1 3
U2 85
PI AMSTERDAM
SN 0304-3894
EI 1873-3336
J9 J HAZARD MATER
PD APR 9
PY 2015
VL 286
BP 545
EP 552
DI 10.1016/j.jhazmat.2015.01.009
PG 8
GA CE6QN
UT WOS:000351963100063
PM 25637821
OA Green Published
DA 2023-12-05
ER
PT J
AU Fu, XJ
Wen, GH
Tang, P
Liu, Q
Zhou, ZY
AF Fu, X. J.
Wen, G. H.
Tang, P.
Liu, Q.
Zhou, Z. Y.
TI Effects of CaO/Al2O3 ratio on crystallisation
behaviour of CaO-Al2O3 based mould fluxes for high
aluminium TRIP steel
LA English
DT Article
DE CaO-Al2O3 based mould fluxes; High aluminium TRIP steel; Crystallisation
tendency
AB When CaO-Al2O3 based mould fluxes for casting high aluminium transformation
induced plasticity steel are used, some problems such as thick slag rims and low
slag consumption resulted in the failure of sequence casting. The main reason for
those problems is the strong crystallisation tendency of mould fluxes. In this
paper, an HF-200 mould slag film simulator, hot thermocouple technique, scanning
electron microscope and X-ray diffraction were applied to investigate the
crystallisation tendency of mould fluxes at different CaO/Al2O3 ratios. The results
showed that the thickness of slag film varied with CaO/Al2O3 ratio, being a minimum
at 1.5 where the crystallisation tendency was weakest. With the increase in
CaO/Al2O3 ratio, the precipitated crystal changed from CaF2 and LiAlO2 to Ca3Al2O6
and CaO. In order to reduce the yield of thick slag rim and improve consumption,
the optimum CaO/Al2O3 ratio of mould fluxes is 0.9-2.0.
C1 [Fu, X. J.; Wen, G. H.; Tang, P.; Liu, Q.; Zhou, Z. Y.] Chongqing Univ, Coll Mat
Sci & Engn, Chongqing 400044, Peoples R China.
RP Wen, GH (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
EM wengh@cqu.edu.cn
National Natural Science Foundation of China (Grant No. 51274260).
CR Becker J. J., 2005, AISTECH 2005 P I STE, V11, P99
Blazek K., 2011, ECCC METEC DUSS GERM, P1
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[王欢 WANG Huan], 2011, [北京科技大学学报, Journal of University Science and
[王欢 Wang Huan], 2010, [过程工程学报, The Chinese Journal of Process
Wen GH, 2008, J IRON STEEL RES INT, V15, P32, DOI 10.1016/S1006-706X(08)60140-5
[杨波 Yang Bo], 2011, [过程工程学报, The Chinese Journal of Process Engineering],
V11, P349
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V10, P1153
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NR 27
TC 21
Z9 24
U1 1
U2 16
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD JUN
PY 2014
VL 41
IS 5
BP 342
EP 349
DI 10.1179/1743281213Y.0000000156
PG 8
GA AI7JP
UT WOS:000337065400004
DA 2023-12-05
ER
PT J
AU Liu, JH
Wang, GX
Bao, YP
Yang, Y
Yao, W
Cui, XN
AF Liu Jian-hua
Wang Guo-xuan
Bao Yan-ping
Yang Yan
Yao Wei
Cui Xiao-ning
TI Inclusion Variations of Hot Working Die Steel H13 in Refining Process
LA English
DT Article
DE hot working die steel; ESR; cleanness; refining slag; modification
AB Inclusion variations of die steel H13, including changes of species,
morphologies, compositions, amounts and sizes, in the production of EAF -> LF -> VD
-> ingot casting -> electro-slag refining (ESR) procedure, were investigated by
systematic sampling, and analyzed with scanning electron microscope (SEM), energy
dispersive spectrum (EDS), and metallographic microscope. The variation mechanism
was studied by comprehensive analysis of total oxygen, nitrogen, and acid soluble
aluminum as well as chemical test of refining slag. Based on the investigations,
technical measures for cleanness improvement were discussed. The results show that
oxide inclusions in H13 steel change from irregular Al2O3 -> near globular CaO-MgO-
Al2O3 and CaO-Al2O3-SiO2 complex inclusions -> finer CaO-Al2O3-SiO2 inclusions with
higher CaO content -> CaO-Al2O3-SiO2 inclusions with higher Al2O3 content and
irregular MgO-Al2O3 inclusions -> fine irregular MgO-Al2O3-CaS inclusions in
various steps of the production; the variations are related with changes of acid
soluble aluminum content, reactions between slag and steel, re-oxidation of liquid
steel during casting, and refining of ESR. It is also found that Al2O3 inclusions
are modified by refining slag in LF and VD refining; and ESR plays a good role in
inclusion removal, especially in controlling the large linear VC-CrC-MoC inclusions
distributed in grain boundaries. It is suggested that casting protection should be
improved, and the basicity of refining slag and acid soluble aluminum content in
steel should be raised.
C1 [Liu Jian-hua; Bao Yan-ping; Yang Yan] Univ Sci & Technol Beijing, Met Engn
Inst, Beijing 100083, Peoples R China.
[Wang Guo-xuan; Yao Wei; Cui Xiao-ning] Zhongyuan Special Steel Co Ltd, Ctr
Tech, Jiyuan 454685, Henan, Peoples R China.
RP Liu, JH (corresponding author), Univ Sci & Technol Beijing, Met Engn Inst,
EM liujianhua@163.com
FU National Science and Technology Support Plan of China [2009AA04Z163]
FX Item Sponsored by National Science and Technology Support Plan of China
(2009AA04Z163)
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NR 11
TC 21
Z9 21
U1 0
U2 30
PI BEIJING
SN 1006-706X
PD NOV
PY 2012
VL 19
IS 11
BP 1
EP 7
PG 7
GA 107RB
UT WOS:000316237400001
DA 2023-12-05
ER
PT J
AU Yang, XH
Long, H
Cheng, GG
Wu, CC
Wu, B
AF Yang Xiaohong
Long Hu
Cheng Guoguang
Wu Chengchuan
Wu Bin
TI Effect of refining slag containing Ce2O3 on steel
cleanliness
SO JOURNAL OF RARE EARTHS
LA English
DT Article
DE Ce2O3 slag; inclusion; cleanliness; rare earths
ID CAO-SIO2-AL2O3 SLAGS; DISSOLUTION; BEHAVIOR; CERIUM; ALLOY; GD; LA; ND
AB The effect of pre-melting refining slag containing different contents of Ce2O3
on the absorption and modification of Al2O3 inclusion in an Al-killed steel was
investigated through the slag/steel reaction experiment at 1600 degrees C. It was
found that the replacement of 10 wt.% Al2O3 with Ce2O3 for 50 wt.%CaO-33 wt.%Al2O3-
7 wt.%MgO-10 wt.%SiO2 refining slag promoted the slag absorption ability of alumina
inclusion, which made the total oxygen content determined by infrared absorption
method decrease from 100 to 25 ppm in 15 min. The Mg-Al-Ce-O type inclusion was
also detected in the as-solidified samples by scanning electron microscopy (SEM).
Thermodynamic analysis indicated that the Ce2O3 center dot Al2O3 type inclusions
would be formed with the cerium content in the range of 6.9 ppb to 3.6 ppm when the
content of aluminum was 0.01 wt.%.
C1 [Yang Xiaohong; Long Hu; Cheng Guoguang; Wu Chengchuan; Wu Bin] Univ Sci &
RP Cheng, GG (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
EM chengguoguang@metall.ustb.edu.cn
RI yang, xiao/HJI-7815-2023
FX Project supported by the National Natural Science Foundation of China
(50734008)
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PI AMSTERDAM
SN 1002-0721
J9 J RARE EARTH
JI J. Rare Earths
PD NOV
PY 2011
VL 29
IS 11
BP 1079
EP 1083
DI 10.1016/S1002-0721(10)60602-3
PG 5
WC Chemistry, Applied
SC Chemistry
GA 863HX
UT WOS:000298154500016
DA 2023-12-05
ER
PT J
AU Zheng, GH
Kozinski, JA
AF Zheng, GH
Kozinski, JA
TI Solid waste remediation in the metallurgical industry: Application and
environmental impact
SO ENVIRONMENTAL PROGRESS
LA English
DT Article
AB This paper describes problems associated with the remediation of solid
metallurgical wastes, primary manufacture of major metals (iron, copper, aluminum,
zinc and lead). It focuses on three types of solid wastes: slags, dusts and
sludges.
It has been shown that solid waste remediation technologies, such as
stabilization or solidification, incineration, and hydro-chemical metal recovery
have been applied in the industry and new technologies such as plasma- and
vitrification-processing of solid wastes are under development. On the whole,
however, solid residue remediation remains relatively uncommon. In addition,
currently applied technologies are unable to solve the complex problems of
metallurgical solid wastes (e.g., simultaneous destruction of toxins and extraction
of multiple metals).
A new thermal process applicable to direct ironmaking that would achieve
significant utilization of zinc residues has been proposed. It has been suggested
that the high-temperature treatment of wastes in which metallurgical furnaces are
used as remediation reactors holds great potential as an alternative disposal
method.
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NR 34
TC 21
Z9 22
U1 1
U2 11
PU JOHN WILEY & SONS INC
PI HOBOKEN
PA 111 RIVER ST, HOBOKEN, NJ 07030 USA
SN 0278-4491
J9 ENVIRON PROG
JI Environ. Prog.
PD WIN
PY 1996
VL 15
IS 4
BP 283
EP 292
DI 10.1002/ep.670150419
PG 10
WC Engineering, Environmental; Engineering, Chemical; Environmental
Sciences
GA VZ006
UT WOS:A1996VZ00600013
DA 2023-12-05
ER
PT J
AU KOROUSIC, B
AF KOROUSIC, B
TI FUNDAMENTAL THERMODYNAMIC ASPECTS OF THE CAO-AL2O3-SIO2 SYSTEM
SO STEEL RESEARCH
LA English
DT Article
ID COMPUTER-PROGRAM; EQUILIBRIUM
AB The most important metallurgical effects of ladle treatment of aluminium-killed
steels with calcium, are associated with the modification of alumina inclusion.
For the development of the deoxidation-control model for inclusions, the
thermodynamic slag model, based on the Gibbs energy minimization and modelling
approaches postulated from J. Hastie et al., was used to calculate component oxide
activities in the system CaO-Al2O3 and part of systems 3CaO.Al2O3-SiO2, 12
CaO.7Al2O3-SiO2 and CaO.Al2O3 - SiO2 at 1600-degrees-C.
RP KOROUSIC, B (corresponding author), INST MET & TECHNOL,DEPT
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NR 15
TC 21
Z9 24
U1 0
U2 5
PI DUSSELDORF
SN 0177-4832
J9 STEEL RES
JI Steel Res.
PY 1991
VL 62
IS 7
BP 285
EP 288
DI 10.1002/srin.199101296
PG 4
GA FX875
UT WOS:A1991FX87500002
DA 2023-12-05
ER
PT J
AU FISCHER, WA
BARDENHE.PW
AF FISCHER, WA
BARDENHE.PW
TI EQUILIBRIA BETWEEN MANAGANESE ALUMINIUM AND OXYGEN-CONTAINING IRON MELTS
AND THEIR SLAGS IN A MANGANESE-DIOXIDE CRUCIBLE AT 1530 TO 1700 DEGREES
C
SO ARCHIV FUR DAS EISENHUTTENWESEN
LA English
DT Article
CR CHIPMAN J, 1961, T METALL SOC AIME, V221, P1277
DEENTREMONT JC, 1963, T AIME, V227, P14
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[10.1002/srin.195601412, DOI 10.1002/SRIN.195601412]
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MITT MAXPLANCKI EISE, P870
1963, J IRON STEEL I, V201, P116
1961, ARCH EISENHUTTENWES, V32, P1
1955, ARCH EISENHUTTENWES, V26, P567
NR 19
TC 21
Z9 21
U1 0
U2 0
PI DUSSELDORF
SN 0003-8962
J9 ARCH EISENHUTTENWES
PY 1968
VL 39
IS 9
BP 637
EP &
DI 10.1002/srin.196803570
PG 0
GA B8469
UT WOS:A1968B846900002
DA 2023-12-05
ER
PT J
AU Valeev, D
Bobylev, P
Osokin, N
Zolotova, I
Rodionov, I
Salazar-Concha, C
Verichev, K
AF Valeev, Dmitry
Bobylev, Petr
Osokin, Nikita
Zolotova, Irina
Rodionov, Ilia
Salazar-Concha, Cristian
Verichev, Konstantin
TI A review of the alumina production from coal fly ash, with a focus in
Russia
LA English
DT Review
DE Coal fly ash; Waste utilization; Alumina; Acid leaching; Metals
extraction
ID ACID-LEACHING ROUTES; HIGH-PURITY ALCL3-CENTER-DOT-6H(2)O; FEED
MATERIALS; RED MUD; CHLORIDE HEXAHYDRATE; EXTRACTING ALUMINA;
THERMAL-ACTIVATION; IRON(III) REMOVAL; GASIFICATION SLAG; HYDROGEN
SULFATE
AB Coal combustion used by the Combined heat and power plants (CHPs) generates
solid wastes -coal fly ash (CFA). Up to 22% of the total electricity supply in
Russian is coal-generated, this value is forecasted to not decrease until 2035,
which in the next 14 years will translate into the accumulation of more than 260 Mt
of CFA on the CHPs landfills. Following the Government recently presenting a
roadmap towards the ramp-up of the CFA utilization from the current 8%-50% by 2035,
the highly developed aluminum industry in Russia amidst the lack of its own bauxite
sources is currently considering the utilization of CFA as an aluminum oxide-rich
raw material for the alumina production. The present review localizes the largest
sources of CFA in Russia, summarizes the annual CFA accumulation rates, and its
stored volumes, and the chemical composition of the CFA generated in Russia. In
this review, the actual acidic methods for alumina production (hydrochloric acid
and ammonium bisulfate/ sulfuric acid) were considered. Alumina powder obtained by
acid methods was analyzed for the quality re-quirements of the Russian aluminum
smelters to forward the case for the CFA's wide adoption as the raw ma-terial in
both Russia's and worldwide aluminum industry.
C1 [Valeev, Dmitry] Russian Acad Sci, Vernadsky Inst Geochem & Analyt Chem, Lab
Sorpt Methods, Moscow 119991, Russia.
[Bobylev, Petr] Minist Energy Russian Federat, Dept Coal Ind, Moscow 125993,
Russia.
[Osokin, Nikita; Zolotova, Irina] Financial Univ Govt Russian Federat, Ctr
Sectoral Res & Consulting, Moscow 127083, Russia.
[Osokin, Nikita; Zolotova, Irina] Natl Assoc Secondary Mat Applicat, Moscow
115054, Russia.
[Rodionov, Ilia] Graph Innovat & Technol, 1 Res Dr, Dartmouth, NS B2Y 4M9,
Canada.
[Salazar-Concha, Cristian] Univ Austral Chile, Adm Inst, Fac Econ & Adm Sci,
Valdivia, Chile.
[Verichev, Konstantin] Univ Austral Chile, Inst Civil Engn, Fac Engn Sci,
Valdivia, Chile.
C3 Russian Academy of Sciences; Vernadsky Institute of Geochemistry &
Analytical Chemistry; Financial University Under the Government of
Russian Federation; Universidad Austral de Chile; Universidad Austral de
Chile
RP Valeev, D (corresponding author), Russian Acad Sci, Vernadsky Inst Geochem &
Analyt Chem, Lab Sorpt Methods, Moscow 119991, Russia.
EM dmvaleev@yandex.ru
RI Valeev, Dmitry/A-9683-2016; Concha, Cristian Eduardo
Salazar/AAK-8636-2020; Verichev, Konstantin/AAC-9438-2019;
Salazar-Concha, Cristian/AGO-1053-2022
OI Valeev, Dmitry/0000-0002-8820-7502; Concha, Cristian Eduardo
Salazar/0000-0002-1807-6535; Verichev, Konstantin/0000-0001-6523-1238;
Salazar-Concha, Cristian/0000-0002-1807-6535; Rodionov,
Ilia/0000-0001-8821-2152
FU Russian Science Foundation [21-79-00295]; Russian Science Foundation
[21-79-00295] Funding Source: Russian Science Foundation
FX The present study was funded by the Russian Science Foundation project
No 21-79-00295.
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NR 258
TC 20
Z9 20
U1 21
U2 70
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD AUG 20
PY 2022
VL 363
AR 132360
DI 10.1016/j.jclepro.2022.132360
EA MAY 2022
PG 23
& Ecology
GA 1Z1BN
UT WOS:000808567600001
DA 2023-12-05
ER
PT J
AU Zulkifly, K
Cheng-Yong, H
Yun-Ming, L
Abdullah, MMA
Shee-Ween, O
Khalid, MSB
AF Zulkifly, Khairunnisa
Cheng-Yong, Heah
Yun-Ming, Liew
Abdullah, Mohd Mustafa Al Bakri
Shee-Ween, Ong
Khalid, Mohd Suhaimi Bin
TI Effect of phosphate addition on room-temperature-cured fly
ash-metakaolin blend geopolymers
LA English
DT Article
DE Blend geopolymer; Fly ash; Metakaolin; Aluminium Phosphate; Room
temperature
ID PHOSPHORIC-ACID SOLUTION; RICE HUSK ASH; MECHANICAL-PROPERTIES;
COMPRESSIVE STRENGTH; SODIUM WATERGLASS; REACTION-KINETICS; CONCRETE;
ALUMINUM; KAOLIN; SLAG
AB This paper details the influence of NaOH concentration, solid-to-liquid (S/L)
and sodium silicate-to-sodium hydroxide (Na2SiO3/NaOH) ratios, and the role of
aluminum phosphate on the compressive strength development of the fly ash-
metakaolin (FA-MK) blend geopolymer. The blended geopolymer was prepared with FA:
MK at a ratio of 1:1, activated with a sodium-based alkali activator and then cured
at room temperature. The optimum FA-MK blend geopolymer was formulated using a 10 M
NaOH solution, a S/L ratio of 1.2, and a Na2SiO3/NaOH ratio of 2.6. Monoaluminium
phosphate (MAP) and aluminum dihydrogen triphosphate (ATP) were added as the source
of aluminium phosphate. The FA-MK blend geopolymers have compressive strengths of
63.7 MPa and 55.5 MPa after being cured for 28 days with the addition of 1 wt% of
MAP and ATP, respectively. The strength enhancement was assumed to be dictated by
the formation of a matrix with a higher cross-linking geopolymer framework. The
microstructure of blend geopolymer with MAP and ATP was smoother and compact
compared to those without phosphate addition. In comparison, MAP addition in blend
geopolymer yielded better physical and mechanical properties. (C) 2020 Elsevier
C1 [Zulkifly, Khairunnisa; Cheng-Yong, Heah; Yun-Ming, Liew; Abdullah, Mohd Mustafa
Al Bakri; Shee-Ween, Ong] Univ Malaysia Perlis, Ctr Excellence Geopolymer & Green
Technol, Sch Mat Engn, CEGeoGTech, Kangar 01000, Perlis, Malaysia.
[Cheng-Yong, Heah] Univ Malaysia Perlis, Fac Engn Technol, Kampus Uniciti Alam,
Padang Besar 02100, Perlis, Malaysia.
[Khalid, Mohd Suhaimi Bin] Sultan Azlan Shah Power Stn, Chem Serv & Environm
Tech Support Sect, TNB Janamanjung Sdn Bhd, Seri Manjung, Perak, Malaysia.
C3 Universiti Malaysia Perlis; Universiti Malaysia Perlis
RP Cheng-Yong, H (corresponding author), Univ Malaysia Perlis, Ctr Excellence
Geopolymer & Green Technol, Sch Mat Engn, CEGeoGTech, Kangar 01000, Perlis,
Malaysia.; Cheng-Yong, H (corresponding author), Univ Malaysia Perlis, Fac Engn
Technol, Kampus Uniciti Alam, Padang Besar 02100, Perlis, Malaysia.
EM cyheah@unimap.edu.my
RI HEAH, CHENG YONG/S-7139-2019; Liew, Yun Ming/S-7164-2019; Ong, Shee
ween/ABA-9926-2021; Abdullah, Mohd Mustafa Al Bakri/C-9844-2012
OI HEAH, CHENG YONG/0000-0001-7093-7833; Liew, Yun
Ming/0000-0001-6600-4969; Ong, Shee ween/0000-0003-0256-6916; Abdullah,
Mohd Mustafa Al Bakri/0000-0002-9779-8586
FU Ministry of Higher Education Malaysia through Fundamental Research Grant
Scheme [FRGS/1/2015/TK05/UNIMAP/02/2]; European Union [H2020-MSC
A-RISE-2015-689857-PRIGeoC]
FX The authors would like to acknowledge the funding support from Ministry
of Higher Education Malaysia through Fundamental Research Grant Scheme
(FRGS/1/2015/TK05/UNIMAP/02/2) and ``Partnership for Research in
Geopolymer Concrete"(H2020-MSC A-RISE-2015-689857-PRIGeoC) sponsored by
the European Union.
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NR 80
TC 20
Z9 21
U1 9
U2 55
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD FEB 8
PY 2021
VL 270
AR 121486
DI 10.1016/j.conbuildmat.2020.121486
EA JAN 2021
PG 13
GA PS6KE
UT WOS:000608034600099
DA 2023-12-05
ER
PT J
AU Zhang, SP
Ghouleh, Z
He, Z
Hu, LL
Shao, YX
AF Zhang, Shipeng
Ghouleh, Zaid
He, Zhen
Hu, Lingling
Shao, Yixin
TI Use of municipal solid waste incineration bottom ash as a supplementary
cementitious material in dry-cast concrete
LA English
DT Article
DE Municipal solid waste incineration; Incineration bottom ash;
Supplementary cementitious material; Waste reuse; Dry-cast concrete
ID MSWI BOTTOM; FLY-ASH; MICROSTRUCTURE; HYDRATION; MORTARS; SLAG
AB This study evaluates the feasibility of partially replacing Portland cement in
concrete with bottom ash (BA) from municipal solid waste incineration (MSWI). The
challenge with this ash lies in its susceptibility to react expansively in alkaline
conditions, leading to cracking when used in conventional high-slump concrete. This
expansive behavior was confirmed to be the result of the dissolution of the ash's
aluminum metal content and consequent formation of hydrogen gas. The aim of this
study was to explore the suitability of BA as a cementitious additive in zero-slump
dry-cast concrete instead. The premise was that dry-cast could better diffuse the
generated gas and avoid internal pressure build-up. Results from isothermal
calorimetry and thermal gravimetric analysis (TGA) clearly correlate enhancements
in early-age cement hydration and pozzolanic reactivity. Scanning electron
microscope (SEM) images revealed voids channels and larger aggregation formation in
the BA applied concrete paste. Dry-cast concrete containing 20% BA replacement of
cement exhibited higher strengths than ordinary Portland cement (OPC) reference
samples at every test age up to 90 days, with the ultimate strength of BA concrete
being 18% higher than that of OPC concrete. The addition of BA also improved
resistance to freeze-thaw damage. The study found that MSWI-BA can impart
enhancements to dry-cast concrete, qualifying it as a potentially suitable
supplementary cementitious material. Use of this otherwise landfilled ash as raw
feedstock in concrete-making demonstrates a greener approach to building - scoring
favorably in environmental performance for being relevant to resource conservation,
landfill diversion, and waste-recycling. (C) 2020 Elsevier Ltd. All rights
reserved.
C1 [Zhang, Shipeng; Ghouleh, Zaid; Shao, Yixin] McGill Univ, Dept Civil Engn & Appl
Mech, 817 Sherbrooke St West, Montreal, PQ H3A 2K6, Canada.
[He, Zhen; Hu, Lingling] Wuhan Univ, State Key Lab Water Resources & Hydropower
Engn S, Wuhan 430072, Peoples R China.
C3 McGill University; Wuhan University
RP Shao, YX (corresponding author), McGill Univ, Dept Civil Engn & Appl Mech, 817
Sherbrooke St West, Montreal, PQ H3A 2K6, Canada.
EM yixin.shao@mcgill.ca
RI hu, ling/GWC-1104-2022
OI Zhang, Shipeng/0000-0003-2433-549X
FU Natural Science and Engineering Research Council (NSERC) of Canada;
Emerald Energy from Waste (EFW) incinerator in Brampton, Ontario, Canada
FX The authors gratefully acknowledge the support of the Natural Science
and Engineering Research Council (NSERC) of Canada, and the Emerald
Energy from Waste (EFW) incinerator in Brampton, Ontario, Canada.
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NR 43
TC 20
Z9 20
U1 11
U2 39
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JAN 10
PY 2021
VL 266
AR 120890
DI 10.1016/j.conbuildmat.2020.120890
PN A
PG 12
GA PI0LU
UT WOS:000600793000009
DA 2023-12-05
ER
PT J
AU Bian, ZZ
Feng, YL
Li, HR
AF Bian, Zhen-zhong
Feng, Ya-li
Li, Hao-ran
TI Extraction of valuable metals from Ti-bearing blast furnace slag using
ammonium sulfate pressurized pyrolysis-acid leaching processes
LA English
DT Article
DE Ti-bearing blast furnace slag; ammonium sulfate; pressurized pyrolysis;
high value products
ID THERMAL-DECOMPOSITION; TITANIUM; RECOVERY; SERPENTINE; SEPARATION;
BEHAVIOR; SI
AB A novel method of extracting valuable metals from Ti-bearing blast furnace slag
(TBBF slag) via pressure pyrolysis of recyclable ammonium sulfate (AS)-acid
leaching process was proposed. The results show that when pressurized roasting at
an AS-to-slag mass ratio 3:1 and 370 degrees C for 90 min, the extraction rates of
titanium, aluminum and magnesium reached 94.5%, 91.9% and 97.4%, respectively. The
acid leaching solution was subjected to re-crystallization in a boiling state to
obtain a titanium product having a TiO2 content of 94.1%. The above crystallization
mother liquor was adjusted to pH=6 and pH >= 12.2, respectively, and then qualified
Al2O3 and MgO products were obtained. The analysis through XRD and SEM-EDS proves
that the main phases in roasted samples were NH4AlSO4, CaSO4 and TiOSO4. The
thermodynamic analysis presents that the main minerals of perovskite, spinel and
diopside in raw ore could spontaneously react with the intermediate produced by AS
under optimal conditions.
C1 [Bian, Zhen-zhong; Feng, Ya-li] Univ Sci & Technol Beijing, Sch Civil & Resource
[Li, Hao-ran] Chinese Acad Sci, Inst Proc Engn, State Key Lab Biochem Engn,
C3 University of Science & Technology Beijing; Chinese Academy of Sciences;
Institute of Process Engineering, CAS
RP Feng, YL (corresponding author), Univ Sci & Technol Beijing, Sch Civil &
Resource Engn, Beijing 100083, Peoples R China.; Li, HR (corresponding author),
Chinese Acad Sci, Inst Proc Engn, State Key Lab Biochem Engn, Beijing 100190,
Peoples R China.
EM ylfeng126@126.com; hrli@ipe.ac.cn
RI wei, li/ISB-3361-2023; Bian, Zhenzhong/ABE-1605-2021; wei,
li/GSD-3630-2022; Li, Hao/GPS-9834-2022; Li, Li/IAQ-0885-2023
FU China Ocean Mineral Resources RD Association [DY135-B2-15]; Major
Science and Technology Program for Water Pollution Control and
Treatment, China [2015ZX07205-003]; National Natural Science Foundation
of China [21176242, 21176026]
FX Project (DY135-B2-15) supported by China Ocean Mineral Resources R&D
Association; Project (2015ZX07205-003) supported by Major Science and
Technology Program for Water Pollution Control and Treatment, China;
Projects (21176242, 21176026) supported by the National Natural Science
Foundation of China
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NR 37
TC 20
Z9 22
U1 2
U2 40
PU ELSEVIER
PI AMSTERDAM
SN 1003-6326
EI 2210-3384
PD OCT
PY 2020
VL 30
IS 10
BP 2836
EP 2847
DI 10.1016/S1003-6326(20)65425-5
PG 12
GA OS3PG
UT WOS:000590076600003
DA 2023-12-05
ER
PT J
AU Ji, ZH
Su, LY
Pei, YS
AF Ji, Zehua
Su, Liya
Pei, Yuansheng
TI Synthesis and toxic metals (Cd, Pb, and Zn) immobilization properties of
drinking water treatment residuals and metakaolin-based geopolymers
SO MATERIALS CHEMISTRY AND PHYSICS
LA English
DT Article
DE Solid waste; Heavy metal; Immobilization; High strength; Metakaolin
ID ORE PROCESSING RESIDUE; ASH-BASED GEOPOLYMER; FLY-ASH; HEAVY-METALS;
MECHANICAL-PROPERTIES; COMPRESSIVE STRENGTH; STEEL SLAG; SEDIMENTS;
REMOVAL; WASTE
AB Using aluminum/iron-based drinking water treatment residuals (DWTR) to replace
metakaolin (MK) in geopolymerization can improve resource utilization from solid
waste and reduce the cost of geopolymer preparation. This study researched the
preparation feasibility of geopolymer with DWTR and MK and investigated its
immobilization performance on toxic heavy metals. Results indicated that a
composite geopolymer with higher mechanical strength was successfully prepared with
DWTR and MK. The characterization results showed that the microstructure of the
geopolymer was more stable with curing time, and the geopolymeric process with
suitable proportion can be completed in a shorter time. According to the leaching
properties results, the immobilization efficiency of heavy metals was between 97.79
and 99.72%. The immobilization efficiency of Cd was significantly higher than Pb
and Zn, and the immobilization mechanism of Cd was different from those of Pb and
Zn. This study indicated that the DWTR could be used as a substitute material for
MK in geopolymer preparation, which provides a cost-effective method for strength
enhancement of geopolymers.
C1 [Ji, Zehua; Su, Liya; Pei, Yuansheng] Beijing Normal Univ, Key Lab Water &
Sediment Sci, Minist Educ, Sch Environm, 19 Xinjiekouwai St, Beijing 100875,
Peoples R China.
C3 Beijing Normal University
RP Pei, YS (corresponding author), Beijing Normal Univ, Key Lab Water & Sediment
Sci, Minist Educ, Sch Environm, 19 Xinjiekouwai St, Beijing 100875, Peoples R
China.
EM yspei@bnu.edu.cn
FU Major Science and Technology Program for Water Pollution Control and
Treatment [2018ZX07110004-01]; National Natural Science Foundation of
China [51579009, 51879012]; Beijing Municipal Science and Technology
Plan Projects [Z181100005518005]
FX This work was financially supported by the Major Science and Technology
Program for Water Pollution Control and Treatment (Project no.
2018ZX07110004-01), the National Natural Science Foundation of China
(Project no. 51579009, 51879012), and the Beijing Municipal Science and
Technology Plan Projects (Project no. Z181100005518005).
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NR 46
TC 20
Z9 22
U1 7
U2 50
PI LAUSANNE
SN 0254-0584
EI 1879-3312
J9 MATER CHEM PHYS
JI Mater. Chem. Phys.
PD FEB 15
PY 2020
VL 242
AR 122535
DI 10.1016/j.matchemphys.2019.122535
PG 9
GA KN3OI
UT WOS:000514749800095
DA 2023-12-05
ER
PT J
AU Gurmessa, B
AF Gurmessa, Biyensa
TI Soil acidity challenges and the significance of liming and organic
amendments in tropical agricultural lands with reference to Ethiopia
SO ENVIRONMENT DEVELOPMENT AND SUSTAINABILITY
LA English
DT Review
DE Al toxicity; Environmental sustainability; Liming; Soil health; Soil
organic carbon
ID ALUMINUM TOXICITY; LIME APPLICATION; TILLAGE SYSTEM; ALKALINE SLAG; CROP
YIELD; BIOCHAR; PHOSPHORUS; NITROGEN; CARBON; FERTILIZER
AB Globally, about 30% of the ice-free land, comprising large proportion of
agricultural land, is affected by soil acidity which is potentially limiting
agricultural productivity and causing environmental challenges. On the other hand,
it is well documented that liming can curb the situation and boost agricultural
production when appropriately applied. However, it is not well understood why the
tendency of farmers toward liming is generally poor in tropical smallholder farming
systems. Thus, this review is aimed to critically evaluate the effect of liming on
crop yield, analyze the significance of organic amendment as an alternative to
liming to treat acid soils and identify the socioeconomic challenges obstructing
the implementation of soil acidity treatment. With this review, the possible link
of land management and soil acidity is also evaluated to showcase if approaches to
any other land management could have negative or positive effects on soil acidity.
To understand the effect of management on soil acidity, a logistic regression was
run using soil data from the Harmonized World Soil Database, taking soil organic
carbon (SOC) as an explanatory variable and pH as a dependent variable. With this
review, studies from science, socioeconomics and policy focusing on soil acidity
and its management were assessed. The literature showed liming can increase crop
yield up to 0.5 t ha(-1). The regression analysis to support this review also
revealed a positive relationship between SOC and pH, implying the strong effect of
land management on soil acidity. This further reveals that a bad management of soil
organic matter can lead to an exacerbation of soil acidity. In other words,
effective soil acidity management in the region requires an integrated approach
that involves combined application of organic amendments, liming and applying
optimum inorganic fertilizers. In short, the principle of integrated soil fertility
management can be applicable to mitigate soil acidity problems in the region. This,
however, needs to be complemented with improved policies that incorporate effective
incentive mechanisms.
C1 [Gurmessa, Biyensa] Dilla Univ, Dilla, Ethiopia.
C3 Dilla University
RP Gurmessa, B (corresponding author), Dilla Univ, Dilla, Ethiopia.
EM biyensa@gmail.com
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OI Dubiwak, Biyensa Gurmessa/0000-0003-1882-9207
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NR 99
TC 20
Z9 20
U1 11
U2 67
PU SPRINGER
PI DORDRECHT
SN 1387-585X
EI 1573-2975
J9 ENVIRON DEV SUSTAIN
JI Environ. Dev. Sustain.
PD JAN
PY 2021
VL 23
IS 1
BP 77
EP 99
DI 10.1007/s10668-020-00615-2
EA JAN 2020
PG 23
WC Green & Sustainable Science & Technology; Environmental Sciences
(SSCI)
SC Science & Technology - Other Topics; Environmental Sciences & Ecology
GA PR5ST
UT WOS:000515762200001
DA 2023-12-05
ER
PT J
AU Li, XM
Zhi, LF
He, C
Kong, LX
Bai, J
Guhl, S
Meyer, B
Li, W
AF Li, Xiaoming
Zhi, Lifei
He, Chong
Kong, Lingxue
Bai, Jin
Guhl, Stefan
Meyer, Bernd
Li, Wen
TI The factors on metallic iron crystallization from slag of direct coal
liquefaction residue
SiO2-Al2O3-Fe2O3-
CaO-MgO-TiO2-Na2O-K2O system in the
entrained flow gasification condition
SO FUEL
LA English
DT Article
DE Direct coal liquefaction residue; Slag; Iron crystallization;
Agglomeration; Thermodynamic modelling
ID ASH FUSION TEMPERATURES; VISCOSITY BEHAVIOR; PRECIPITATION; PREDICTION;
SIMULATION; GASIFIER; CALCIUM; OXIDE
AB The gasification of direct coal liquefaction residue (DCLR) enhances the overall
economy of the direct coal liquefaction process. However, the DCLR ash is rich in
iron due to pyrite as the catalyst during liquefaction. Coal blending plan with
DCLR for gasification should consider the possibility of metallic iron
crystallization and agglomeration ahead of suitable viscosity range. In this study,
the iron behavior in the DCLR slag in the gasification condition was discussed by
the thermodynamic modelling of SiO2-Al2O3-Fe2O3-CaO-MgO-TiO2-Na2OK2O. Results show
that the metallic iron forms only in the dry feed entrained flow gasifier for the
high content of reducing gases. The metallic iron crystallizes when Fe2+ of the
liquid phase fails to be stabilized by -Si-O. The competition reaction with -Si-O
between Ca2+ and Fe2+ and the formation of calcium aluminum-silicate also
contribute the metallic iron crystallization. In the gasification condition, the
metallic iron crystallization can be inhibited by decreasing the iron content/a
value (a= CaO/(SiO2+ Al2O3), mass ratio) or by increasing S/A (S/A= SiO2/Al2O3,
mass ratio) of DCLR ash. Finally, the DCLR blends with 3.5 wt% sand/8.0 wt%
mullite/50.0 wt % Dalai Nur coal/90.0 wt% Duolun coal is the feasible feedstock for
pulverized coal gasifier, because the temperature of iron crystallization is below
the tapping temperature of 1350 degrees C and the viscosity is less than 25 Pa.s.
C1 [Li, Xiaoming; Zhi, Lifei] Taiyuan Univ Sci & Technol, Chem & Biol Engn Coll,
[He, Chong; Kong, Lingxue; Bai, Jin; Li, Wen] Chinese Acad Sci, Inst Coal Chem,
State Key Lab Coal Convers, Taiyuan 030001, Shanxi, Peoples R China.
[He, Chong] Univ Chinese Acad Sci, Beijing 100049, Peoples R China.
[Guhl, Stefan; Meyer, Bernd] Tech Univ Bergakad Freiberg, Inst Energy Proc Engn
& Chem Engn, D-09599 Freiberg, Germany.
C3 Taiyuan University of Science & Technology; Chinese Academy of Sciences;
Institute of Coal Chemistry, CAS; Chinese Academy of Sciences;
University of Chinese Academy of Sciences, CAS; Technical University
Freiberg
RP Zhi, LF (corresponding author), Taiyuan Univ Sci & Technol, Chem & Biol Engn
Coll, Taiyuan 030024, Shanxi, Peoples R China.; He, C; Bai, J (corresponding
author), Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal Convers, Taiyuan
030001, Shanxi, Peoples R China.
EM Lifeizhi@yeah.net; hechong14@mails.ucas.ac.cn; stone@sxicc.ac.cn
OI , Chong/0000-0002-3264-3196; Bai, Jin/0000-0002-8623-1656
FU NSFC-DFG [21761132032]; Natural Science Foundation of Shanxi Province
[201801D121050, 201703D421033, U1510201]; Science and technology
innovation project of colleges and universities in Shanxi [2017158];
Shanxi Scholarship Council of China [2017-086]; CAS equipment project;
Youth Innovation Promotion Association, CAS [2011138]; Natural Science
Foundation of China [U1510201, U1703252]; Natural Science Foundation of
Xinjiang Province [U1703252]
FX This work was supported by the NSFC-DFG (Grant number 21761132032),
Natural Science Foundation of Shanxi Province (Grant numbers
201801D121050 and 201703D421033), Science and technology innovation
project of colleges and universities in Shanxi (Grant number 2017158),
Shanxi Scholarship Council of China (Grant number 2017-086), Joint
Foundation of the Natural Science Foundation of China and Shanxi
Province (Grant number U1510201), Joint Foundation of the Natural
Science Foundation of China and Xinjiang Province (Grant number
U1703252), CAS equipment project, and the Youth Innovation Promotion
Association, CAS (Grant number 2011138).
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NR 32
TC 20
Z9 22
U1 3
U2 77
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD JUN 15
PY 2019
VL 246
BP 417
EP 424
DI 10.1016/j.fuel.2019.03.017
PG 8
GA HP5YF
UT WOS:000461758800045
DA 2023-12-05
ER
PT J
AU Kumar, D
Pistorius, PC
AF Kumar, Deepoo
TI Rate of MgO Pickup in Alumina Inclusions in Aluminum-Killed Steel
LA English
DT Article
ID NONMETALLIC INCLUSIONS; AL; KINETICS
AB This work aims to clarify the rate and mechanism of MgO pickup by alumina
inclusions and the effect of oxide impurities in MgO crucibles on this
transformation. Two MgO crucibles from different batches from the same supplier
were used in laboratory experiments with Al-killed steel. A kinetic model was
developed, based on mass-transfer control in the liquid steel. Rate constants were
fitted using inclusion analysis. The rate of magnesium transfer from the two types
of crucibles was found to differ by a factor of 20; faster magnesium transfer was
associated with formation of a slag layer on the inner surface of the crucible wall
(rather than a solid spinel product layer). The kinetic model was also used to
simulate industrial scale ladle refining (1) to illustrate the effects of total
oxygen concentration and (2) to evaluate the contribution of steel-refractory
reaction (in addition to steel-slag reaction) on the rate of MgO pickup in alumina
inclusion. The rate of MgO pickup was higher with a lower inclusion concentration.
For ladle desulfurization, the extent of MgO pickup in inclusions is directly
linked to the extent of desulfurization; both reactions are controlled by the
oxygen potential at the steel-slag interface.
C1 [Kumar, Deepoo; Pistorius, Petrus Christiaan] Carnegie Mellon Univ, Ctr Iron &
Steelmaking Res, Pittsburgh, PA 15213 USA.
RP Pistorius, PC (corresponding author), Carnegie Mellon Univ, Ctr Iron &
Steelmaking Res, Pittsburgh, PA 15213 USA.
RI Kumar, Deepoo/AAP-4932-2021; Pistorius, Petrus Christiaan/A-8247-2011
OI Kumar, Deepoo/0000-0002-4396-6097; Pistorius, Petrus
Christiaan/0000-0002-2966-1879
FU [MCF-677785]
FX Support of this work by the industrial members of the Center for Iron
and Steelmaking Research is gratefully acknowledged. We also acknowledge
use of the Materials Characterization Facility, Carnegie Mellon
University, supported by Grant No. MCF-677785.
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NR 26
TC 20
Z9 24
U1 0
U2 12
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD FEB
PY 2019
VL 50
IS 1
BP 181
EP 191
DI 10.1007/s11663-018-1436-z
PG 11
Engineering
GA HH9PG
UT WOS:000456070300019
DA 2023-12-05
ER
PT J
AU Tabatabaei, Y
Coley, KS
Irons, GA
Sun, S
AF Tabatabaei, Yousef
Coley, Kenneth S.
Irons, Gordon A.
Sun, Stanley
TI Model of Inclusion Evolution During Calcium Treatment in the Ladle
Furnace
LA English
DT Article
ID SLAG-METAL; KINETIC-MODEL; MOLTEN STEEL; LIQUID-IRON; ALUMINUM; OXYGEN
AB Calcium treatment of steel is typically employed to modify alumina inclusions to
liquid calcium aluminates. However, injected calcium also reacts with the dissolved
sulfur to form calcium sulfide. The current work aims to develop a kinetic model
for the evolution of oxide and sulfide inclusions in Al-killed alloyed steel during
Ca treatment in the ladle refining process. The model considers dissolution of the
calcium from the calcium bubbles into the steel and reduction of calcium oxide in
the slag to dissolved calcium. A steel-inclusion kinetic model is used for mass
transfer to the inclusion interface and diffusion within the calcium aluminate
phases formed on the inclusion. The inclusion-steel kinetic model is then coupled
with a previously developed steel-slag kinetic model. The coupled inclusion-steel-
slag kinetic model is applied to the chemical composition changes in molten steel,
slag, and evolution of inclusions in the ladle. The result of calculations is found
to agree well with an industrial heat for species in the steel as well as
inclusions during Ca treatment.
C1 [Tabatabaei, Yousef; Coley, Kenneth S.; Irons, Gordon A.] McMaster Univ, Dept
Mat Sci & Engn, Steel Res Ctr, 1280 Main St W, Hamilton, ON L8S 4L7, Canada.
[Sun, Stanley] ArcelorMittal Global R&D Hamilton, 1330 Burlington St E,
Hamilton, ON L8N 3J5, Canada.
C3 McMaster University
RP Tabatabaei, Y (corresponding author), McMaster Univ, Dept Mat Sci & Engn, Steel
Res Ctr, 1280 Main St W, Hamilton, ON L8S 4L7, Canada.
EM tabatasy@mcmaster.ca
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NR 43
TC 20
Z9 22
U1 2
U2 42
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2018
VL 49
IS 4
BP 2022
EP 2037
DI 10.1007/s11663-018-1266-z
PG 16
Engineering
GA GM8IO
UT WOS:000438469300041
DA 2023-12-05
ER
PT J
AU Calvo, WA
Ortega, P
Velasco, MJ
Muñoz, V
Pena, P
Martinez, AGT
AF Calvo, W. A.
Ortega, P.
Velasco, M. J.
Munoz, V.
Pena, P.
Tomba Martinez, A. G.
TI Characterization of alumina-magnesia-carbon refractory bricks containing
aluminium and silicon
LA English
DT Article
DE Al2O3; MgO; Carbon; Refractories
AB The present paper is a continuation of previous ones focused on the
characterization of alumina-magnesia carbon refractories (AMC) bricks. Unlike those
characterised materials which only have aluminium as an antioxidant, a brick also
containing silicon is comparatively analysed in this paper. Along with metallic
aluminium, silicon is among the most commonly used antioxidant additives in oxide-C
refractories, but the studies on the incorporation of this metal into AMC bricks
are rather limited.
In this work, several complementary techniques were used in combination to
achieve a detailed characterization in relation to the physical and chemical
characteristics and thermal evolution of the Si-containing AMC refractory: X-ray
fluorescence, plasma emission spectroscopy, gravimetry, granulometry, X-ray
diffraction, differential thermal and thermogravimetric analyses, reflection
optical and scanning electron microscopies, mercury intrusion porosimetry, and
density, porosity, permanent linear change and permeability measurements. In
addition, the characterization was completed by evaluating the chemical resistance
to air and to a basic slag and calculating the equilibrium composition of the brick
when it is subjected to high temperatures (up to 1400 degrees C). A comparison with
the results obtained for previously characterised AMC bricks with similar MgO
contents and metallic aluminium as an antioxidant was also made. The presence of
silicon was related to finer open porosity and higher oxidation resistance at high
temperature (1400 degrees C).
C1 [Calvo, W. A.; Munoz, V.; Tomba Martinez, A. G.] Univ Nacl Mar del Plata,
CONICET, Fac Ingn, Inst Invest Ciencia & Tecnol Mat INTEMA, Av JB Justo 4302, RA-
7600 Mar Del Plata, Buenos Aires, Argentina.
[Ortega, P.; Velasco, M. J.; Pena, P.] CSIC, ICV, Kelsen 5, Madrid 28049, Spain.
C3 National University of Mar del Plata; Consejo Nacional de
Investigaciones Cientificas y Tecnicas (CONICET); Consejo Superior de
Investigaciones Cientificas (CSIC); CSIC - Instituto de Ceramica y
Vidrio (ICV)
RP Martinez, AGT (corresponding author), Univ Nacl Mar del Plata, CONICET, Fac
Ingn, Inst Invest Ciencia & Tecnol Mat INTEMA, Av JB Justo 4302, RA-7600 Mar Del
Plata, Buenos Aires, Argentina.
EM agtomba@fi.mdp.edu.ar
OI PILAR, PENA/0000-0001-6312-7373
FU Agencia Nacional de Promocion Cientifica y Tecnologica (ANPCyT) of
Argentina [1887, 1215]
FX This work was supported by the Agencia Nacional de Promocion Cientifica
y Tecnologica (ANPCyT) (PICT2006 No. 1887 and PICT2012 N.1215) of
Argentina under projects "Degradacion termoquimica y termomecanica de
refractarios oxido-C de uso siderurgico", PICT2006 No. 1887 and
"Degradacion quimica de refractarios de uso siderurgico", PICT2012 No.
1215. The authors would like to thank Dr. P.G. Galliano for providing
the material and participating in useful discussions, Mrs. M.L. Dignani
for performing the permeability measurements, and Dra. E. Brandaleze for
the opportunity to use the FactSage software.
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NR 26
TC 20
Z9 23
U1 1
U2 17
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD JUN 1
PY 2018
VL 44
IS 8
BP 8842
EP 8855
DI 10.1016/j.ceramint.2018.02.069
PG 14
GA GD5CI
UT WOS:000430522200015
DA 2023-12-05
ER
PT J
AU Sankar, K
Stynoski, P
Al-Chaar, GK
Kriven, WM
AF Sankar, Kaushik
Stynoski, Peter
Al-Chaar, Ghassan K.
Kriven, Waltraud M.
TI Sodium silicate activated slag-fly ash binders: Part I - Processing,
microstructure, and mechanical properties
LA English
DT Article
DE fly ash; geopolymers; polycondensation; slag; strength
ID GEOPOLYMERS; ALUMINOSILICATE; KINETICS
AB Alkali silicate activated slag and class F fly ash-based binders are ambient
curing, structural materials that are feasible replacements for ordinary Portland
cement (OPC). They exhibit advantageous mechanical properties and less
environmental impact than OPC. In this work, five sodium silicate activated slag-
fly ash binder mixtures were developed and their compressive and flexural strengths
were studied as a function of curing temperature and time. It was found that the
strongest mixture sets at ambient temperature and had a Weibull average flexural
strength of 5.7 +/- 1.5MPa and Weibull average compressive strength of 60 +/- 8MPa
at 28days. While increasing the slag/fly ash ratio accelerated the strength
development, the cure time was decreased due to the formation of calcium silicate
hydrate (C-S-H), calcium aluminum silicate hydrate (C-A-S-H), and (Ca,Na) based
geopolymer. The density, microstructure, and phase evolution of ambient-cured,
heat-cured, and heat-treated binders were studied using pycnometry, scanning
electron microscopy, energy dispersive X-ray spectroscopy (SEM-EDS), and X-ray
diffraction (XRD). Heat-cured binders were more dense than ambient-cured binder. No
new crystalline phases evolved through 28days in ambient- or heat-cured binders.
C1 [Sankar, Kaushik; Kriven, Waltraud M.] Univ Illinois, Dept Mat Sci & Engn,
Urbana, IL 61801 USA.
[Stynoski, Peter; Al-Chaar, Ghassan K.] US Army Engn Res & Dev Ctr ERDC,
Construct Engn Res Lab CERL, Champaign, IL USA.
United States Department of Defense; United States Army; U.S. Army Corps
of Engineers; U.S. Army Engineer Research & Development Center (ERDC);
Construction Engineering Research Laboratory (CERL)
RP Kriven, WM (corresponding author), Univ Illinois, Dept Mat Sci & Engn, Urbana,
IL 61801 USA.
EM kriven@illinois.edu
RI Sankar, Kaushik/Y-2152-2019
OI Sankar, Kaushik/0000-0001-8837-7854; Kriven,
Waltraud/0000-0002-2983-5760
CR [Anonymous], 2015, TYPICAL PROPERTY DAT
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NR 32
TC 20
Z9 20
U1 4
U2 51
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD JUN
PY 2018
VL 101
IS 6
BP 2228
EP 2244
DI 10.1111/jace.15391
PG 17
GA GB2MP
UT WOS:000428887500005
DA 2023-12-05
ER
PT J
AU Sreenivasan, H
Kinnunen, P
Heikkinen, EP
Illikainen, M
AF Sreenivasan, Harisankar
Kinnunen, Paivo
Heikkinen, Eetu-Pekka
Illikainen, Mirja
TI Thermally treated phlogopite as magnesium-rich precursor for alkali
activation purpose
LA English
DT Article
DE Alkali activated material; Geopolymer; Phlogopite; Thermal treatment;
Calcination
ID BLAST-FURNACE SLAG; INORGANIC POLYMERS; REACTIVE MGO; DRYING SHRINKAGE;
HYDRATION; STRENGTH; CEMENT; ASH; BINDERS; GEOPOLYMERISATION
AB Alkali-activated materials (AAMs), sometimes called geopolymers, have wide
industrial relevance and are produced through alkaline activation of alumina and
silica-rich precursors, including industrial side streams. It has been observed
that MgO content in AAMs results in improved mechanical properties. However, most
of the suitable MgO sources are either prohibitively expensive or carbonate-based,
which leads to higher CO2 emissions. Phlogopite is an attractive source of MgO as
it is carbonate-free and locally abundant. Besides MgO, phlogopite also contains
significant quantities of silica and alumina, making it a viable candidate for
alkali activation. However, an alkaline solubility test in NaOH revealed phlogopite
to be highly inert, with both silicon (Si) and aluminum (Al) solubility at around 1
wt% of the original material. In this work, thermal treatment was considered to
improve the alkali activation potential of phlogopite. Thermal treatment was found
to be successful; the resulting glassy material showed 45% Si and 33% Al release
into the solution, on a par with highly soluble metakaolin (26% Si and 40% Al).
During the solubility test, significant quantities of magnesium and iron were also
released but they did not stay in the solution. Rather, they formed precipitated
products, the main one of which was meixnerite (Mg6Al2(OH)(18)center dot 4H(2)O), a
hydrotalcite-like compound. The resulting alkali-soluble glass with phlogopite
chemical composition can be used as a carbonate-free source of magnesium in alkali
activation purposes. However, any commercial application should allow for due
consideration of cost.
C1 [Sreenivasan, Harisankar; Kinnunen, Paivo; Illikainen, Mirja] Univ Oulu, Fibre &
Particle Engn Res Unit, Pentti Kaiteran Katu 1, Oulu 90014, Finland.
[Kinnunen, Paivo] Imperial Coll London, Dept Civil & Environm Engn, London SW7
2BU, England.
[Heikkinen, Eetu-Pekka] Univ Oulu, Proc Met Res Unit, POB 4300, Oulu 90014,
Finland.
C3 University of Oulu; Imperial College London; University of Oulu
RP Kinnunen, P (corresponding author), Univ Oulu, Fibre & Particle Engn Res Unit,
EM paivo.kinnunen@oulu.fi
RI Kinnunen, Paivo/I-3430-2012
OI Kinnunen, Paivo/0000-0001-8490-1890; Illikainen,
Mirja/0000-0001-7545-4574
FU project "Novel synthesis methods for porous ceramics from mine
tailings"; Academy of Finland [292526]; Academy of Finland (AKA)
[292526, 292526] Funding Source: Academy of Finland (AKA)
the project "Novel synthesis methods for porous ceramics from mine
tailings," funded by Academy of Finland (292526). The authors would also
like to thank Jarno Karvonen for his help with XRF measurement, Elisa
Wirkkala with solubility measurements and Sami Saukko with STEM
measurement.
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NR 42
TC 20
Z9 21
U1 2
U2 14
PI OXFORD
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD NOV
PY 2017
VL 113
BP 47
EP 54
DI 10.1016/j.mineng.2017.08.003
PG 8
GA FJ0CQ
UT WOS:000412376500007
DA 2023-12-05
ER
PT J
AU Wei, RR
Lv, XW
Yang, MR
Xu, J
AF Wei, Ruirui
Lv, Xuewei
Yang, Mingrui
Xu, Jian
TI Effect of ultrasonic vibration treatment on solid-state reactions
between Fe2O3 and CaO
SO ULTRASONICS SONOCHEMISTRY
LA English
DT Article
DE Calcium ferrite; Ultrasonic vibration; Rietveld structure refinement;
Sintering
ID IRON-ORE SINTER; MECHANICAL-PROPERTIES; DISSOLUTION KINETICS; CALCIUM
FERRITE; SILICO-FERRITE; ALUMINUM; SLAG; AIR; MICROSTRUCTURE; BEHAVIOR
AB In the present study, ultrasonic vibration was applied to the solid-state
reaction between Fe2O3 and CaO. The effect of the ultrasonic vibration treatment on
the formation of CaFe2O4 (CF) from the solid-state reaction was investigated by X-
ray diffraction (XRD) and the Rietveld structure refinement method. The results
indicated that the solid-state reaction between Fe2O3 and CaO was accelerated by
ultrasonic treatment (UT), which efficiently lowered the formation temperature of
the solid-state CF and increased the quantity formed by enhancing the mass transfer
process of the reactions. Without the UT, CF and Ca2Fe2O5 (C2F) were produced at
750 degrees C and the mass fractions of CF and C2F increased with the experiment
temperature, with approximately 47.76% CF and 40.66% C2F produced at 850 degrees C.
With the UT, mass fractions of 5.67% CF and 18.20% C2F were formed at 700 degrees
C, and increasing the experiment temperature enhanced the formation of CF and C2F.
Moreover, a significantly greater amount of CF than C2F was formed when the
temperature exceeded 700 degrees C. A CF mass fraction of approximately 98.73% was
obtained by UT at 850 degrees C, much higher than the 47.76% obtained without UT.
In addition, increasing the ultrasonic power influenced the formation of the CF
phase. The CF content increased from 19% to 7734% with increasing ultrasonic power
from 0 to 89% x 2 kW. Furthermore, a prolonged UT time also promoted the formation
of solid phase CF. The mass fraction of CF ranged from 19% to 77.34% when the UT
time was varied from 0 to 150 min. (C) 2017 Elsevier B.V. All rights reserved.
C1 [Wei, Ruirui; Lv, Xuewei; Yang, Mingrui; Xu, Jian] Chongqing Univ, Sch Mat Sci &
Engn, Chongqing 400044, Peoples R China.
RP Lv, XW (corresponding author), Chongqing Univ, Sch Mat Sci & Engn, Chongqing
EM wrui1990@outlook.com; lvxuewei@163.com
RI Yang, Fei/JLM-3367-2023; Xu, Jian/Y-9405-2019
OI Xu, Jian/0000-0002-7565-9665
FU Natural Science Fund outstanding youth project funding [51522403];
Chongqing Youth Science and Technology Talent Training Project
[cstc2014kjrc-qnrc90001]
FX This study was performed with the financial support of Natural Science
Fund outstanding youth project funding (No. 51522403) and Chongqing
Youth Science and Technology Talent Training Project
(cstc2014kjrc-qnrc90001).
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Yu B, 2016, METALL MATER TRANS B, V47, P2063, DOI 10.1007/s11663-016-0627-8
NR 27
TC 20
Z9 20
U1 2
U2 51
PI AMSTERDAM
SN 1350-4177
EI 1873-2828
J9 ULTRASON SONOCHEM
JI Ultrason. Sonochem.
PD SEP
PY 2017
VL 38
BP 281
EP 288
DI 10.1016/j.ultsonch.2017.03.023
PG 8
WC Acoustics; Chemistry, Multidisciplinary
SC Acoustics; Chemistry
GA EZ6FV
UT WOS:000404814700028
PM 28633827
DA 2023-12-05
ER
PT J
AU Shi, RY
Li, JY
Xu, RK
Qian, W
AF Shi, Ren-yong
Li, Jiu-yu
Xu, Ren-kou
Qian, Wei
TI Ameliorating effects of individual and combined application of biomass
ash, bone meal and alkaline slag on acid soils
SO SOIL & TILLAGE RESEARCH
LA English
DT Article
DE Biomass ash; Bone meal; Alkaline slag; Amelioration of acid soil;
Exchangeable aluminum; Available heavy metals
ID PLANTATION
AB Incubation experiments with biomass ash (BA), bone meal (BM) and alkaline slag
(AS) applied alone and together were conducted to ameliorate acidity and increase
nutrient contents of five Ultisols collected from four provinces of southern China.
The results showed that the ameliorating effect of the combined application of
three amendments on soil acidity was greater than that of BA + BM or their single
applications. The combined application of BA, BM and AS increased the pH by 0.63-
1.37 for five Ultisols. The most significant decrease of soil exchangeable acidity
was also observed in the treatments of BA + BM + AS by 80.1-96.9% for five
Ultisols. Meanwhile, the combined application of the amendments greatly increased
the exchangeable potassium, calcium and magnesium of the five soils, respectively,
by 0.4-3.8, 1.9-10 and 1.7-9.7 times. The contents of available phosphorus of the
five soils were also increased significantly by 0.6-184 times due to the
application of BA + HBM + AS. In general, the application of the amendments did not
increase available heavy metals in the soils in this short-term incubation
experiment, but the potential risk of the amendments applied should be further
assessed under field conditions through long-term experiments. (C) 2016 Elsevier
C1 [Shi, Ren-yong; Li, Jiu-yu; Xu, Ren-kou; Qian, Wei] Chinese Acad Sci, Inst Soil
Sci, State Key Lab Soil & Sustainable Agr, POB 821, Nanjing, Jiangsu, Peoples R
China.
[Shi, Ren-yong] Univ Chinese Acad Sci, Beijing 100049, Peoples R China.
EM rkxu@issas.ac.cn
FU National Key Basic Research Program of China [2014CB441003]
China (Grant Number: 2014CB441003).
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NR 16
TC 20
Z9 35
U1 5
U2 81
PI AMSTERDAM
SN 0167-1987
EI 1879-3444
J9 SOIL TILL RES
JI Soil Tillage Res.
PD SEP
PY 2016
VL 162
BP 41
EP 45
DI 10.1016/j.still.2016.04.017
PG 5
WC Soil Science
SC Agriculture
GA DO4DG
UT WOS:000377731400006
DA 2023-12-05
ER
PT J
AU Yu, D
Chattopadhyay, K
AF Yu, D.
Chattopadhyay, K.
TI Numerical simulation of copper recovery from converter slags by the
utilisation of spent potlining (SPL) from aluminium electrolytic cells
LA English
DT Article
DE Cu converter slag; Matte; Spent potlining; SPL; Slag cleaning; FactSage
ID FURNACE
AB An innovative method was devised to improve copper recovery and operational
efficiency of the Cu converter slag-cleaning furnace, by utilising both carbon and
fluoride values of an otherwise environmental hazardous material (i.e. spent
potlining (SPL)) produced from the aluminium industry. Results based on numerical
modelling show that 90% Cu recovery could be achieved by adding as little as 3-4
wt-% of SPL to the molten converter slag. The fluorides and sodium-containing
compounds in the SPL reduced the slag viscosity, resulting in a much faster
settling rate of matte droplets. In this process, the SPL could be detoxified by
destroying the cyanides to form harmless N-2 gas, and inertising the fluorides in a
much diluted form in the ferro-silicate slag, ensuring a safe disposal to the
environment.
C1 [Yu, D.; Chattopadhyay, K.] Univ Toronto, Dept Mat Sci & Engn, Proc Met &
Modelling Grp, 184 Coll St,Suite 140, Toronto, ON M5S 3E4, Canada.
C3 University of Toronto
RP Yu, D (corresponding author), Univ Toronto, Dept Mat Sci & Engn, Proc Met &
Modelling Grp, 184 Coll St,Suite 140, Toronto, ON M5S 3E4, Canada.
EM dawei.yu@mail.utoronto.ca
RI Yu, Dawei/AAE-7736-2021; Chattopadhyay, Kinnor/K-4806-2018; Yu,
Dawei/T-4077-2018
OI Chattopadhyay, Kinnor/0000-0002-0755-8846; Yu, Dawei/0000-0001-7606-4148
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NR 37
TC 20
Z9 21
U1 0
U2 42
PI ABINGDON
SN 0008-4433
EI 1879-1395
J9 CAN METALL QUART
JI Can. Metall. Q.
PY 2016
VL 55
IS 2
BP 251
EP 260
DI 10.1080/00084433.2016.1181314
PG 10
GA DM6NN
UT WOS:000376469800016
DA 2023-12-05
ER
PT C
AU Al Naimi, KM
Delclos, T
Calvet, N
AF Al Naimi, Kholoud M.
Delclos, Thomas
Calvet, Nicolas
BE Yan, J
Shamim, T
Chou, SK
Li, H
TI Industrial waste produced in the UAE, valuable high-temperature
materials for thermal energy storage applications
SO CLEAN, EFFICIENT AND AFFORDABLE ENERGY FOR A SUSTAINABLE FUTURE
SE Energy Procedia
LA English
CT 7th International Conference on Applied Energy (ICAE)
CY MAR 28-31, 2015
CL Abu Dhabi, U ARAB EMIRATES
DE Thermal energy storage (TES); high-temperature; industrial waste;
furnace slags; aluminum dross; pot skimming
ID ALUMINUM DROSS; MOLTEN-SALTS
AB Several industrial waste from metal industries in the UAE have been identified
to be recycled as low-cost materials for high-temperature thermal energy storage
(TES) systems development. Electric arc furnace (EAF) slag, ladle furnace (LF)
slag, aluminum pot skimming (APS) and aluminum white dross (AWD) have been
chemically and thermally characterized. Chemical analysis showed that these
materials contain relatively inert components and are non-hazardous in general
(neglected amount of heavy metals). In addition, except for APS, these wastes were
in general stable at high temperatures up to 1100 degrees C after performing one or
two thermal cycles. (C) 2015 The Authors. Published by Elsevier Ltd.
C1 [Al Naimi, Kholoud M.; Delclos, Thomas; Calvet, Nicolas] Masdar Inst Sci &
Technol, Dept Mech & Mat Engn, Inst Ctr Energy IEnergy, Abu Dhabi, U Arab Emirates.
C3 Khalifa University of Science & Technology
RP Calvet, N (corresponding author), Masdar Inst Sci & Technol, Dept Mech & Mat
Engn, Inst Ctr Energy IEnergy, POB 54224, Abu Dhabi, U Arab Emirates.
EM ncalvet@masdar.ac.ae
CR Calvet N, ASME 6 EN SUST C MIN
Faik A, 2012, SOL ENERGY, V86, P139, DOI 10.1016/j.solener.2011.09.014
Gil A, 2014, EUR C THER EN STOR M
Gómez A, 2008, MATER TRANS, V49, P728, DOI 10.2320/matertrans.MRA2007129
Kere A, P INNOSTOCK 2012 C 1
Meffre A, P SOLARPACES 2011 C
Py X, 2001, J SOLAR ENERGY ENG, V133
The statistics portal, 2014, ALUMINUM PRODUCTION
NR 12
TC 20
Z9 21
U1 1
U2 4
PI AMSTERDAM
PA SARA BURGERHARTSTRAAT 25, PO BOX 211, 1000 AE AMSTERDAM, NETHERLANDS
SN 1876-6102
J9 ENRGY PROCED
PY 2015
VL 75
BP 2087
EP 2092
DI 10.1016/j.egypro.2015.07.320
PG 6
WC Energy & Fuels; Environmental Sciences
SC Energy & Fuels; Environmental Sciences & Ecology
GA BD4SH
UT WOS:000361030003054
OA gold
DA 2023-12-05
ER
PT J
AU Li, JJ
Wang, J
Chen, HY
Sun, BD
AF Li, Jiajing
Wang, Jun
Chen, Haiyan
Sun, Baode
TI Microstructure observation of β-sialon-15R ceramics synthesized from
aluminum dross
LA English
DT Article
DE Hot pressing; Microstructure-nal; Sialon; Aluminum dross
ID ALN-POLYTYPOID CERAMICS; ALPHA SIALON POWDERS; CARBOTHERMAL REDUCTION;
NITRIDATION; (CA,MG)-ALPHA-SIALON; SLAG
AB Fully dense beta-sialon-15R multiphase ceramics were synthesized by hot pressing
sintering using aluminum dross as raw material. Transmission electron microscopy
(TEM) was used to study the microstructure, notably for the impurity and glass
phase. The results show that beta-sialon grains are generally equiaxed, and 15R AlN
polytypoid grains show a fibre-like morphology. The main impurity phase is Fe5Si3.
High resolution electron microscopy (HREM) results confirm the interface between
beta-sialon grains and/or 15R grains to be clean in the sample synthesized at 1750
degrees C, and the glassy phase only exist in triple junctions and pockets. AlN
polytypoids in the multiphase ceramics provide a path to reduce the glass phase
formed from the oxide impurity in aluminum dross. (C) 2011 Elsevier Ltd and Techna
C1 [Li, Jiajing; Wang, Jun; Sun, Baode] Shanghai Jiao Tong Univ, State Key Lab Met
Matrix Composites, Shanghai 200240, Peoples R China.
[Chen, Haiyan] Shanghai Maritime Univ, Inst Marine Mat Sci & Engn, Shanghai
C3 Shanghai Jiao Tong University; Shanghai Maritime University
RP Wang, J (corresponding author), Shanghai Jiao Tong Univ, State Key Lab Met
Matrix Composites, Shanghai 200240, Peoples R China.
EM junwang@sjtu.edu.cn
RI Chen, Haiyan/HGB-6216-2022; Chen, Haiyan/C-8109-2012
FU Shanghai Municipal Science and Technology Commission [07dz12028,
08xd14231]
FX This work is financially supported by Research Project (Nos. 07dz12028
and 08xd14231) from the Shanghai Municipal Science and Technology
Commission.
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NR 15
TC 20
Z9 27
U1 1
U2 32
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
J9 CERAM INT
JI Ceram. Int.
PD MAY
PY 2012
VL 38
IS 4
BP 3075
EP 3080
DI 10.1016/j.ceramint.2011.12.006
PG 6
GA 922BV
UT WOS:000302522700064
DA 2023-12-05
ER
PT J
AU Goto, H
Miyazawa, K
AF Goto, H
Miyazawa, K
TI Reoxidation behavior of molten steel in non-killed and Al-killed steels
LA English
DT Article
DE oxide; oxygen; deoxidation; reoxidation; manganese; aluminum; slag;
inclusion; steel
AB The effect of soluble oxygen on the reoxidation behavior by slag has been
investigated by comparing the oxygen content and oxide formation of non-killed
steel containing a soluble oxygen content of approximately 50 to 250 mass ppm with
those of Al-killed steel containing less soluble oxygen. In the non-killed steel,
oxides are not formed in molten steel even when oxygen is supplied from slag
because it does not contain aluminum which has strong affinity for oxygen. The
soluble oxygen content simply increases. In the Al-killed steel, however, the
oxygen supplied from slag reacts with aluminum to form alumina and most of them
float out.
C1 Nippon Steel Corp Ltd, Kimitsu Works, Chiba 2991141, Japan.
Nippon Steel Corp Ltd, Proc Res Technol Labs, Futtsu, Chiba 2938511, Japan.
C3 Nippon Steel & Sumitomo Metal Corporation; Nippon Steel & Sumitomo Metal
Corporation
RP Goto, H (corresponding author), Nippon Steel Corp Ltd, Kimitsu Works, Chiba
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1984, 19 COMM STEELM JAP S
NR 8
TC 20
Z9 21
U1 0
U2 2
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 1998
VL 38
IS 3
BP 256
EP 259
PG 4
GA ZW882
UT WOS:000074457800006
OA gold
DA 2023-12-05
ER
PT J
AU Li, GQ
Suito, H
AF Li, GQ
Suito, H
TI Electrochemical measurement of critical supersaturation in Fe-O-M (M=Al,
Si, and Zr) and Fe-O-Al-M (M=C, Mn, Cr, Si, and Ti) melts by solid
electrolyte galvanic cell
LA English
DT Article
DE deoxidation equilibrium; critical supersaturation; aluminum deoxidation;
solid electrolyte; zirconia; mullite
ID LIQUID-IRON; OXYGEN EQUILIBRIUM; SLAGS; THERMODYNAMICS; NITROGEN; ALLOY
AB The supersaturation ratio with respect to alumina precipitation, S-Al2O3
(=(partial derivative(Al)(2) .partial derivative(O)(3))(ss)/(partial derivative(Al)
(2) .partial derivative(O)(3))eq), in Fe-0-0.008 similar to 0.090mass%Al melt was
electrochemically measured at 1873K in an Al2O3 crucible by blowing CO2 gas or
adding an Fe-2mass%Al alloy intermittently, using plug-type ZrO2-9mol%MgO and tube-
type mullite probes. The S-ZrO2 (=(partial derivative(Zr).partial derivative(O)
(2))ss/(partial derivative(Zr).partial derivative(O)(2))eq) value in Fe-O-0.04mass
%Zr melt was also measured at 1873 K in a ZrO2-11mol%CaO crucible by adding an Fe-
4mass%Zr alloy. As a result, the critical values for log S-Al2O3 and log S-ZrO2
were 3.5 and 1.3, respectively, No supersaturation for the precipitation of SiO2
was observed. The presence of solute element M (M=C, Mn, Cr, Si, and Ti) in an Fe-
O-0.148 similar to 0.158mass%/Al melt was found to significantly influence the
supersaturation phenomenon.
RP Li, GQ (corresponding author), TOHOKU UNIV,INST ADV MAT PROC,AOBA
KU,SENDAI,MIYAGI 980,JAPAN.
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NR 26
TC 20
Z9 20
U1 0
U2 2
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 1997
VL 37
IS 8
BP 762
EP 769
PG 8
GA XR236
UT WOS:A1997XR23600005
OA gold
DA 2023-12-05
ER
PT J
AU CHIARENZELLI, J
SCRUDATO, R
WUNDERLICH, M
RAFFERTY, D
JENSEN, K
OENGA, G
ROBERTS, R
PAGANO, J
AF CHIARENZELLI, J
SCRUDATO, R
WUNDERLICH, M
RAFFERTY, D
JENSEN, K
OENGA, G
ROBERTS, R
PAGANO, J
TI PHOTODECOMPOSITION OF PCBS ABSORBED ON SEDIMENT AND INDUSTRIAL-WASTE -
IMPLICATIONS FOR PHOTOCATALYTIC TREATMENT OF CONTAMINATED SOLIDS
SO CHEMOSPHERE
LA English
DT Article
ID AQUEOUS SUSPENSIONS; POLYCHLORINATED-BIPHENYLS; PHOTODECHLORINATION;
DEGRADATION; SOLUBILITY; LIGHT; TIO2
AB PCBs in contaminated sediment and soil have been photodegraded in slurry
suspension with TiO2 and simulated solar illumination without pre-treatment or
amendments. Degradation of 81% of the PCBs in St. Lawrence River sediment was
achieved in a 24 h irradiation period. Replicate experiments using five times as
much sediment and half the light intensity yielded similar results. The observed
degradation rates of individual PCB congeners correspond with gas chromatograph
retention time and chlorine number. Lesser and ortho chlorinated PCBs are
preferentially photodecomposed. The solubility of individual congeners controls the
observed rate of decomposition by regulation of the transfer of PCBs to the aqueous
phase and thus effectively retards access to the catalyst (anatase). The rate and
degree of photodegradation can be enhanced by the use of lower wavelength
ultraviolet light which leads to hydroxylation of PCB congeners increasing
solubility and accessibility to photocatalytic reactions. Photodecomposition of
PCBs in a slurry composed of furnace ash, core sands, and aluminum-rich (>45%
Al2O3) slag from an aluminum foundry was increased from 45 to 88% during a 24 h
irradiation period by using low wattage UVC lamps instead of solar equivalent
illumination.
RP CHIARENZELLI, J (corresponding author), SUNY COLL OSWEGO,ENVIRONM RES CTR,319
PIEZ HALL,OSWEGO,NY 13126, USA.
OI Pagano, James/0000-0001-8278-6905
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NR 19
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Z9 21
U1 0
U2 8
PI OXFORD
SN 0045-6535
J9 CHEMOSPHERE
JI Chemosphere
PD SEP
PY 1995
VL 31
IS 5
BP 3259
EP 3272
DI 10.1016/0045-6535(95)00174-7
PG 14
GA RW143
UT WOS:A1995RW14300008
DA 2023-12-05
ER
PT J
AU Zhao, YL
Qiu, JP
Wu, PQ
Guo, ZB
Zhang, SY
Sun, XG
AF Zhao, Yingliang
Qiu, Jingping
Wu, Pinqi
Guo, Zhenbang
Zhang, Shiyu
Sun, Xiaogang
TI Preparing a binder for cemented paste backfill using low-aluminum slag
and hazardous oil shale residue and the heavy metals immobilization
effects
LA English
DT Article
DE Cement paste back fill; Oil shale residue; Ettringite; Heavy metals
immobilization
ID MSWI FLY-ASH; ACTIVATED SLAG; SEQUENTIAL EXTRACTION; COMPRESSIVE
STRENGTH; HYDRATION BEHAVIOR; ALKALINE; PERFORMANCE; ADMIXTURES;
POZZOLAN; PRODUCT
AB The high cost and carbon emission of ordinary Portland cement (OPC) increase the
burden of mining industry and aggravate environmental pollution. In this study, a
cheaper and greener binder was prepared using low aluminum slag and calcined oil
shale residue (COSR) as main precursors to provide an alternative cementing
material for cemented paste backfill (CPB). The influence of COSR content on the
properties of the CPB sample was investigated, including rheological properties,
setting time, mechanical strength, and pore structure. Characterization of binder
sample was then conducted via isothermal calorimetric analysis, X-ray diffraction
(XRD), thermogravimetry (TG), and scanning electron microscope (SEM). The optimal
mix proportion of binder was 56 wt% slag, 24 wt% COSR, 15 wt% flue gas
desulfurization gypsum (FGDG), and 5 wt% OPC. The solid waste utilization rate in
the binder production reached 95%, considered an eco-friendly binder. Besides, the
best performance of the binder was mainly due to the optimal Al2O3 and CaO content,
leading to large amounts of precipitated ettringite. It then contributed to a
denser structure with high mechanical strength. Furthermore, the sequential
extraction test showed that the heavy metal in the solidified CPB sample existed
mainly as a residual fraction, contributing to the superior immobilization effects.
(C)& nbsp;2022 Elsevier B.V. All rights reserved.
C1 [Zhao, Yingliang; Qiu, Jingping; Wu, Pinqi; Guo, Zhenbang; Zhang, Shiyu; Sun,
Xiaogang] Northeastern Univ, Coll Resources & Civil Engn, Shenyang, Peoples R
China.
[Zhao, Yingliang; Qiu, Jingping; Wu, Pinqi; Guo, Zhenbang; Zhang, Shiyu; Sun,
Xiaogang] Northeastern Univ, Sci & Technol Innovat Ctr Smart Water & Resource,
Shenyang, Peoples R China.
C3 Northeastern University - China; Northeastern University - China
RP Qiu, JP (corresponding author), Northeastern Univ, Coll Resources & Civil Engn,
Shenyang, Peoples R China.
EM qiujingping@mail.neu.edu.cn
RI Zhao, Yingliang/AFA-2467-2022
OI Zhang, Shiyu/0000-0002-6999-415X
FU National Key Research and Development Pro-gram [2019YFC1907202]; Key
Research and Development Project of Liaoning [2020JH1/10300005]
FX The supports of the National Key Research and Development Pro-gram,
2019YFC1907202, Key Research and Development Project of Liaoning,
2020JH1/10300005. Besides, the authors would like to thank Fan Yao from
Shiyanjia Lab ( www.shiyanjia.com ) for the isothermal cal-orimeter
test. Additionally, special thanks are due to the instrumental analysis
from Analytical and Testing Center, Northeastern University.
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NR 79
TC 19
Z9 19
U1 5
U2 25
PU ELSEVIER
PI AMSTERDAM
SN 0032-5910
EI 1873-328X
J9 POWDER TECHNOL
JI Powder Technol.
PD FEB
PY 2022
VL 399
AR 117167
DI 10.1016/j.powtec.2022.117167
EA FEB 2022
PG 11
SC Engineering
GA 0Z3II
UT WOS:000790973700011
DA 2023-12-05
ER
PT J
AU Zhang, N
Hedayat, A
Sosa, HGB
Tupa, N
Morales, IY
Loza, RSC
AF Zhang, Nan
Hedayat, Ahmadreza
Sosa, Hector Gelber Bolanos
Tupa, Nestor
Morales, Isaac Yanqui
Loza, Reynaldo Sabino Canahua
TI Crack evolution in the Brazilian disks of the mine tailings-based
geopolymers measured from digital image correlations: An experimental
investigation considering the effects of class F fly ash additions
LA English
DT Article
DE Geopolymer; Mine tailings; Digital image correlation; Crack propagation;
Splitting tensile strength; Brazilian test
ID MECHANICAL-PROPERTIES; UNIAXIAL COMPRESSION; PARTIAL REPLACEMENT;
FRACTURE PROPERTIES; THERMAL-STABILITY; FLEXURAL STRENGTH; FURNACE SLAG;
SILICA FUME; CONCRETE; METAKAOLIN
AB Mine tailings-based geopolymer was proved to be successfully created with
enhanced strength for potentially construction and building materials applications.
Through geopolymerization, the mining wastes can be reused and the storage,
economic, and environmental issues can be mitigated. However, the geopolymerization
effect was relatively limited comparing to the ordinary Portland concrete.
Therefore, the additions of amorphous supplementary fly ash were considered in the
paper. In this study, class F fly ash was utilized as an amorphous additive and the
additional aluminum source to adjust the Si: Al ratio for better geopolymerization
effects. To better understand the mechanical and fracture behavior of the
geopolymer after adding fly ash, the Brazilian indirect tensile tests were then
conducted to evaluate the influence of different fly ash additions, 5%, 10%, 15%,
and 20%, on the tensile strength of the geopolymer. Meanwhile, besides the load-
displacement relationships, the digital image correlation was used to investigate
the crack initiation and propagation in the geopolymer disks with respect to
different fly ash additions. The crack evolution was evaluated from the full-field
strain field from digital image correlation. Crack opening displacements, failure
patterns, and strain evolutions for the geopolymer disks with different fly ash
additions were examined. Results showed that, under the presented sample curing
condition, the geopolymer with 15% fly ash addition had the largest tensile
strength. Geopolymer disks without and with lower fly ash additions had plastic
deformation prior to the peak load that can obviously be classified into three
different stages. The geopolymer made without and with lower fly ash additions had
both tensile and shear crack modes.
C1 [Zhang, Nan; Hedayat, Ahmadreza] Colorado Sch Mines, 1500 Illinois St, Golden,
CO 80401 USA.
[Sosa, Hector Gelber Bolanos; Tupa, Nestor; Morales, Isaac Yanqui; Loza,
Reynaldo Sabino Canahua] Univ Nacl San Agustin Arequipa, Arequipa, Arequipa, Peru.
C3 Colorado School of Mines; Universidad Nacional de San Agustin de
Arequipa
RP Zhang, N (corresponding author), Colorado Sch Mines, 1500 Illinois St, Golden,
CO 80401 USA.
EM zhangnan@mines.edu
RI Tupa, Nestor/AHC-8922-2022; Hedayat, Ahmadreza/B-9282-2018
OI Tupa, Nestor/0000-0001-7182-235X; Yanqui Morales,
Isaac/0000-0002-4527-5353; Hedayat, Ahmadreza/0000-0002-7143-7272;
Zhang, Nan/0000-0002-6207-000X
FU Universidad Nacional de San Agustin (UNSA); Colorado School of Mines
FX The financial support provided by the Universidad Nacional de San
Agustin (UNSA) through the joint Center for Mining Sustainability with
the Colorado School of Mines is highly acknowledged.
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NR 92
TC 19
Z9 19
U1 3
U2 17
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD NOV 15
PY 2021
VL 47
IS 22
BP 32382
EP 32396
DI 10.1016/j.ceramint.2021.08.138
EA SEP 2021
PG 15
GA WC0UG
UT WOS:000703979000001
DA 2023-12-05
ER
PT J
AU Padamata, SK
Yasinskiy, A
Polyakov, P
AF Padamata, Sai Krishna
Yasinskiy, Andrey
Polyakov, Peter
TI A Review of Secondary Aluminum Production and Its Byproducts
SO JOM
LA English
DT Review
ID SALT-CAKE; DROSS; WASTE; LIBS; IDENTIFICATION; HYDROLYSIS; FILTRATION;
SEPARATION; CERAMICS; REMOVAL
AB Secondary aluminum production is required for the conservation of the
environment. It can significantly reduce greenhouse gas emissions and energy
consumption and reduce the consumption of alumina, a source of primary aluminum.
Secondary aluminum production requires sorting processes for the metal scrap before
starting the refining process. Salt slags generated from both primary and secondary
aluminum production need to be recycled/treated as they are considered hazardous
byproducts. This review paper discusses the methods used for sorting and refining
aluminum waste and managing and utilizing slag cakes/slag from recycling
techniques.
C1 [Padamata, Sai Krishna; Yasinskiy, Andrey; Polyakov, Peter] Siberian Fed Univ,
Lab Phys & Chem Met Proc & Mat, Krasnoyarsk 600025, Russia.
[Yasinskiy, Andrey] Rhein Westfal TH Aachen, IME Proc Met & Met Recycling,
Intzestr 3, D-52056 Aachen, Germany.
C3 Siberian Federal University; RWTH Aachen University
RP Yasinskiy, A (corresponding author), Siberian Fed Univ, Lab Phys & Chem Met Proc
& Mat, Krasnoyarsk 600025, Russia.; Yasinskiy, A (corresponding author), Rhein
Westfal TH Aachen, IME Proc Met & Met Recycling, Intzestr 3, D-52056 Aachen,
Germany.
EM ayasinskiykrsk@gmail.com
RI Padamata, Sai Krishna/M-6040-2019; Yasinskiy, Andrey/O-2093-2019
OI Padamata, Sai Krishna/0000-0001-6592-6531; Yasinskiy,
Andrey/0000-0002-7170-2160
FU RFBR [18-29-24122]
FX The reported study was funded by RFBR according to the research project
No 18-29-24122.
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NR 72
TC 19
Z9 22
U1 21
U2 95
PU SPRINGER
PI NEW YORK
SN 1047-4838
EI 1543-1851
J9 JOM-US
JI JOM
PD SEP
PY 2021
VL 73
IS 9
BP 2603
EP 2614
DI 10.1007/s11837-021-04802-y
EA JUL 2021
PG 12
Engineering; Mineralogy; Mining & Mineral Processing
SC Materials Science; Metallurgy & Metallurgical Engineering; Mineralogy;
Mining & Mineral Processing
GA UF3AX
UT WOS:000679610000001
DA 2023-12-05
ER
PT J
AU Liu, FQ
Xie, MZ
Yu, GQ
Ke, CY
Zhao, HL
AF Liu, Fengqin
Xie, Mingzhuang
Yu, Guoqing
Ke, Chaoyang
Zhao, Hongliang
TI Study on Calcination Catalysis and the Desilication Mechanism for Coal
Gangue
LA English
DT Article
DE resource utilization; coal gangue; calcination; secondary aluminum
dross; catalytic effect; mineral separation
ID FLY-ASH; ALUMINA; EXTRACTION; ACTIVATION; SEPARATION; ZEOLITE; SILICA
AB Coal gangue is a solid waste discharged during coal mining, which not only
occupies large land resources but also brings about certain risks to the
environment. The alumina and silica minerals in coal gangue are the major resources
and difficult to separate from each other, which hinders the resource utilization
of coal gangue. The catalytic effect of various additives on the phase
transformation process of coal gangue is studied in this paper to strengthen the
separation of silica from alumina minerals and to increase the resource utilization
rate of coal gangue. The study results show that the silica-containing minerals in
coal gangue can be promoted to transform into mullite by alumina-based additives.
The soluble active silica is released during phase transformation in the
calcination process, which has a positive effect on the caustic desilication after
calcination. The secondary aluminum dross has a positive catalytic effect on the
active silica released during calcination. The alumina to silica ratio of the
desilication product can be increased from 0.91 to 1.94 and the desilication rate
can be increased from 42.99 to 56.16% by 6% secondary aluminum dross addition. The
solid slag after desilication can be used to extract an alumina source for the
synthesis of molecular sieve products with the silica source obtained by the
desilication process so that the high-value resource utilization of coal gangue can
be realized.
C1 [Liu, Fengqin; Xie, Mingzhuang; Yu, Guoqing; Zhao, Hongliang] Univ Sci & Technol
Beijing, State Key Lab Adv Met, Beijing 100083, Peoples R China.
[Liu, Fengqin; Xie, Mingzhuang; Yu, Guoqing; Zhao, Hongliang] Univ Sci & Technol
[Ke, Chaoyang] Inner Mongolia Risheng Recycling Resource Co Ltd, Hohhot 010206,
Peoples R China.
Technology Beijing
RP Liu, FQ; Zhao, HL (corresponding author), Univ Sci & Technol Beijing, State Key
Lab Adv Met, Beijing 100083, Peoples R China.; Liu, FQ; Zhao, HL (corresponding
author), Univ Sci & Technol Beijing, Sch Met & Ecol Engn, Beijing 100083, Peoples R
China.
EM liufq@ustb.edu.cn; zhaohl@ustb.edu.cn
RI Xie, Mingzhuang/AAR-7696-2021
FU National Key Research and Development Program of China [2019YFC1908403]
Program of China (2019YFC1908403).
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NR 24
TC 19
Z9 20
U1 19
U2 86
PI WASHINGTON
SN 2168-0485
PD AUG 2
PY 2021
VL 9
IS 30
BP 10318
EP 10325
DI 10.1021/acssuschemeng.1c03276
EA JUL 2021
PG 8
GA TX3OT
UT WOS:000683000400029
DA 2023-12-05
ER
PT J
AU Yang, RH
He, TS
AF Yang, Renhe
He, Tingshu
TI Influence of liquid accelerators combined with mineral admixtures on
early hydration of cement pastes
LA English
DT Article
DE Liquid accelerators; Mineral admixtures; Cement pastes; Early hydration;
Morphology
ID EARLY AGE HYDRATION; ALKALI-FREE; FLY-ASH; PORTLAND-CEMENT; SHOTCRETE;
SULFATE; EVOLUTION; MICROSTRUCTURE; TEMPERATURE; MATRICES
AB The main purpose of this paper was to investigate the influence of different
liquid accelerators (AR, liquid accelerator based on sodium aluminate; AS, liquid
accelerator based on aluminum sulfate; AF, liquid accelerator based on
fluoroaluminate) and mineral admixtures (fly ash, slag and silica fume) on the
setting time of cement pastes and compressive strength of mortar. In addition, the
early hydration process of cement pastes with different mineral admixtures in the
presence of AR, AS and AF was explored by isothermal calorimetry, and the crystals
composition and micro morphology of hydration products were analyzed by XRD and
SEM. The results indicated that in the presence of 7.0% AF, the initial and final
setting time of cement pastes with 10% and 5% silica fume are 0.67 min and 1.47
min, respectively. In the presence of 4.0% AR, the mortar with 10% silica fume
reaches the highest value of 16.8 MPa. In addition, when the dosages of AF and
silica fume are 7.0% and 10%, the first exothermic peak value of paste is 87.79
mW/g. Furthermore, in the presence of liquid accelerators, different mineral
admixtures also have great influence on the morphology and crystals composition of
hydration products.
C1 [Yang, Renhe; He, Tingshu] Xian Univ Architecture & Technol, Coll Mat Sci &
Engn, Xian 710055, Shaanxi, Peoples R China.
C3 Xi'an University of Architecture & Technology
RP Yang, RH; He, TS (corresponding author), Xian Univ Architecture & Technol, Coll
Mat Sci & Engn, Xian 710055, Shaanxi, Peoples R China.
EM yangrenhe@xauat.edu.cn; hetingshu@xauat.edu.cn
RI He, Xiang/IUN-5330-2023
OI He, Xiang/0000-0003-4648-201X
FU Building Engineering Materials Research Institute of Xi'an University of
Architecture Technology
FX The authors are grateful to the Building Engineering Materials Research
Institute of Xi'an University of Architecture & Technology for its help
and support during the experiment.
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NR 54
TC 19
Z9 19
U1 2
U2 45
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD AUG 9
PY 2021
VL 295
AR 123659
DI 10.1016/j.conbuildmat.2021.123659
EA MAY 2021
PG 14
GA SV4JF
UT WOS:000663785900011
DA 2023-12-05
ER
PT J
AU Nguyen, H
Kunther, W
Gijbels, K
Samyn, P
Carvelli, V
Illikainen, M
Kinnunen, P
AF Hoang Nguyen
Kunther, Wolfgang
Gijbels, Katrijn
Samyn, Pieter
Carvelli, Valter
Illikainen, Mirja
Kinnunen, Paivo
TI On the retardation mechanisms of citric acid in ettringite-based binders
LA English
DT Article
DE Hydration; Retardation; Thermodynamic calculations; Ettringite;
Monosulfate
ID QUANTITATIVE PHASE-ANALYSIS; HYDRATION KINETICS; PORTLAND-CEMENT;
ORGANIC-ACIDS; CITRATE; COMPLEXATION; ADMIXTURES; SPECIATION; RETARDERS;
YEELIMITE
AB This study aims to obtain insights into the retardation mechanism of citric acid
in an ettringite-based binder from ladle slag and gypsum. The hydration kinetics
and phase assemblage of the binder were experimentally investigated and
thermodynamically modelled. Additionally, the effects of citric acid on synthetic
ettringite were studied to obtain further understanding of the interaction between
this organic ligand and the crystal. Experimental results reveal that citric acid
works as an inhibitor of ettringite's formation leading to the precipitation of
monosulfate and gypsum; the ettringite surface blockage by citrate ligand
effectively prevents precipitation of this crystal. This leads to an overestimation
in the precipitation of ettringite in the thermodynamic model due to this kinetic
barrier imposed by the ligand. Thermodynamic modelling suggests ettringite,
monosulfate, aluminum hydroxide, and stratlingite as main hydrates in this binder,
whereas an intermixed C-(A-)S-H gel was observed experimentally instead of
stratlingite.
C1 [Hoang Nguyen; Illikainen, Mirja; Kinnunen, Paivo] Univ Oulu, Fibre & Particle
Engn Res Unit, Pentti Kaiteran Katu 1, Oulu 90014, Finland.
[Kunther, Wolfgang] Tech Univ Denmark, Dept Civil Engn, DK-2800 Lyngby, Denmark.
[Gijbels, Katrijn] Hasselt Univ, Nucl Technol Ctr, Agoralaan,Gebouw H, B-3590
Diepenbeek, Belgium.
[Samyn, Pieter] Hasselt Univ, Appl & Analyt Chem, IMO, Agoralaan,Gebouw D, B-
3590 Diepenbeek, Belgium.
[Carvelli, Valter] Politecn Milan, Dept ABC, Piazza Leonardo Da Vinci 32, I-
20133 Milan, Italy.
C3 University of Oulu; Technical University of Denmark; Hasselt University;
Hasselt University; Polytechnic University of Milan
RP Nguyen, H (corresponding author), Univ Oulu, Fibre & Particle Engn Res Unit,
EM hoang.nguyen@oulu.fi; wolku@byg.dtu.dk; katrijn.gijbels@uhasselt.be;
pieter.samyn@uhasselt.be; valter.carvelli@polimi.it;
mirja.illikainen@oulu.fi; paivo.kinnunen@oulu.fi
RI Kunther, Wolfgang/AAT-8044-2021; Kunther, Wolfgang/AAI-2529-2021
OI Nguyen, Hoang/0000-0003-3716-8504; Illikainen,
Mirja/0000-0001-7545-4574; Kunther, Wolfgang/0000-0003-4885-2395
FU Business Finland in the ERA-MIN 2 Innovation program (EU Horizon 2020
program) [8904/31/2017]; UniOGS (the University of Oulu Graduate
School); Academy of Finland [322085, 329477, 326291]; Centre for
Material Analysis, University of Oulu, Finland; Academy of Finland (AKA)
[329477] Funding Source: Academy of Finland (AKA)
FX This work is a part of the FLOW Project (project number 8904/31/2017)
funded by Business Finland in the ERA-MIN 2 Innovation program (EU
Horizon 2020 program). SSAB Europe Oy is acknowledged for providing
ladle slag. The authors thank Dr. Dmitrii Kulik (Paul Scherrer
Institute) with the help in creating citrate ligand in GEMS and valuable
instruction, Prof. Jorgen Skibsted (Aarhus University) for fruitful
discussion on 29Si MAS NMR, and Viljami Viinikka and Durgaprasad Ramteke
for the support during lab work. Hoang Nguyen gratefully acknowledges
financial support from travel grant of UniOGS (the University of Oulu
Graduate School) for his research visit in Technical University of
Denmark. P.K. acknowledges financial support from Academy of Finland
(grants 322085, 329477 and 326291). A part of material characterization
was carried out with the support of the Centre for Material Analysis,
University of Oulu, Finland.
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NR 40
TC 19
Z9 19
U1 10
U2 26
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD FEB
PY 2021
VL 140
AR 106315
DI 10.1016/j.cemconres.2020.106315
PG 13
GA PT6ZW
UT WOS:000608762600026
DA 2023-12-05
ER
PT J
AU Yoldi, M
Korili, SA
Gil, A
AF Yoldi, M.
Korili, S. A.
Gil, A.
TI Efficient recovery of aluminum from saline slag wastes
LA English
DT Article
DE Industrial waste valorization; High-value-added products; Aluminum
extraction; Alkaline extraction; Hazardous waste
ID SALT CAKE; DROSS; VALORIZATION; MANAGEMENT
AB This work presents the procedure to improve the aluminum extracted from a
hazardous waste from the recycling of aluminum, aluminum that could be used in the
production of value-added materials, as well as with the generation of non-
hazardous waste. The aluminum waste was treated under reflux and stirring with NaOH
aqueous solutions taking into account two concentrations (1 and 2 mol/dm(3)),
various times of extraction (1, 2 and 4 h) and 4th consecutive steps of extraction
in order to obtain solutions with Al3+. The activation of the waste by milling is
also analyzed. After extraction, the solution is filtered to separate an aqueous
solution that contain the extracted Al3+ and a residual waste. A maximum of 7.54
g/dm(3) of aluminum was extracted in the first step, for a total accumulated of
9.59 g/dm(3) of aluminum. The 'extracted aluminum can be used to synthesize added-
value Products applied as adsorbents and catalysts. Finally, the residual waste
generated was characterized by N-2 adsorption at -196 degrees C, X-ray diffraction,
X-ray fluorescence, energy-dispersive X-ray and scanning electron microscopy in
order to apply it as in future works adsorbent or catalyst.
European Regional Development Fund (ERDF); Government of Navarra
[MAT2016-78863-C2-1-R, PI017 CORRAL]; Santander Bank
Regional Development Fund (ERDF) and the Government of Navarra through
projects MAT2016-78863-C2-1-R and PI017 CORRAL. MY thanks Government of
Navarra for technologists recruitment. AG and EGFO also thank Santander
Bank for funding through the Research Intensification Program.
CR Davies M, 2008, MINER ENG, V21, P605, DOI 10.1016/j.mineng.2007.12.001
Li Q, 2018, HYDROMETALLURGY, V182, P121, DOI 10.1016/j.hydromet.2018.10.015
10.1016/j.jenvman.2018.06.068
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10.1016/j.resconrec.2017.11.026
10.1016/j.minpro.2012.03.011
10.1016/j.micromeso.2019.06.009
NR 18
TC 19
Z9 21
U1 7
U2 67
PI OXFORD
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD AUG 15
PY 2019
VL 140
AR 105884
DI 10.1016/j.mineng.2019.105884
PG 8
GA IW3KL
UT WOS:000484878800008
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Olmeda, J
Missana, T
Grandia, F
Grivé, M
García-Gutiérrez, M
Mingarro, M
Alonso, U
Colàs, E
Henocq, P
Munier, I
Robinet, JC
AF Olmeda, J.
Missana, T.
Grandia, F.
Grive, M.
Garcia-Gutierrez, M.
Mingarro, M.
Alonso, U.
Colas, E.
Henocq, P.
Munier, I
Robinet, J. C.
TI Radium retention by blended cement pastes and pure phases (C-S-H and
C-A-S-H gels): Experimental assessment and modelling exercises
LA English
DT Review
DE Radium; Radionuclide; Adsorption; Cement; C-S-H; C-A-S-H
ID HYDRATED CALCIUM SILICATES; SOLUBILITY; ALUMINUM; SORPTION; ALKALI; NMR;
BINDING; RADIONUCLIDES; MECHANISMS; CHLORIDE
AB Cementitious materials are planned to be used in current designs of geological
disposal of radioactive waste. Their main function is the structural reinforcement,
but they could contribute to the retention of some radio-nuclides via adsorption
and/or precipitation. In this work, a set of laboratory experiments has been
performed to determine the capacity of blended cement (CEM V/A) containing fly ash
(FA) and blast furnace slag (BFS) to adsorb radium. The study has focused on the
hydrated cement paste (HCP) with different degradation states and on cement
representative pure phases (C-S-H and C-A-S-H at variable Ca/Si and Al/Si ratios).
The experimental results show that retention of Ra by hydrated cements is high; C-
S-H and C-A-S-H phases were proven to be very relevant in Ra uptaking, with log Kd
up to 4.2 and 5.1, respectively. The adsorption of radium into these phases is
interpreted to be driven by surface complexation on weak and strong silanols-like
sites and ionic exchange with Ca. Since Ra adsorption has been proven to be
inversely proportional to dissolved Ca content, an enhanced adsorption capacity of
the cementitious hydrates (C-S-H phases) is expected as degradation of cement
proceeds.
C1 [Olmeda, J.; Grandia, F.; Grive, M.; Colas, E.] Amphos 21 Consulting SL, C
Venecuela 103, Barcelona 08019, Spain.
[Missana, T.; Garcia-Gutierrez, M.; Mingarro, M.; Alonso, U.] CIEMAT, Phys Chem
Actinides & Fiss Prod Unit, Dept Environm, Ave Complutense 40, Madrid 28040, Spain.
[Henocq, P.; Munier, I; Robinet, J. C.] Andra, 1-7 Rue Jean Monnet,Parc Croix
Blanche, F-92298 Chatenay Malabry, France.
C3 Centro de Investigaciones Energeticas, Medioambientales Tecnologicas
RP Olmeda, J (corresponding author), Amphos 21 Consulting SL, C Venecuela 103,
Barcelona 08019, Spain.
EM javier.olmeda@amphos21.com
RI Alonso, Ursula/L-8457-2014; Garcia-Gutierrez, Miguel/M-1651-2014;
Missana, Tiziana/E-4646-2010; Robinet, Jean-Christophe/S-7776-2016;
Mingarro, Manuel/AAB-2414-2019
OI Alonso, Ursula/0000-0002-2668-4725; Garcia-Gutierrez,
Miguel/0000-0001-6551-2873; Missana, Tiziana/0000-0003-3052-5185;
Robinet, Jean-Christophe/0000-0002-3529-6003; Mingarro,
Manuel/0000-0001-6413-1956
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[Anonymous], 2013, US GEOLOGICAL SURVEY
[Anonymous], THESIS
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NR 63
TC 19
Z9 19
U1 1
U2 40
PI OXFORD
SN 0883-2927
J9 APPL GEOCHEM
JI Appl. Geochem.
PD JUN
PY 2019
VL 105
BP 45
EP 54
DI 10.1016/j.apgeochem.2019.04.004
PG 10
GA HZ5BM
UT WOS:000468865600005
DA 2023-12-05
ER
PT J
AU Tan, HB
Nie, KJ
He, XY
Guo, YL
Zhang, X
Deng, XF
Su, Y
Yang, J
AF Tan, Hongbo
Nie, Kangjun
He, Xingyang
Guo, Yulin
Zhang, Xun
Deng, Xiufeng
Su, Ying
Yang, Jin
TI Effect of organic alkali on compressive strength and hydration of
wet-grinded granulated blast-furnace slag containing Portland cement
LA English
DT Article
DE Hydration; Wet grinding; Granulated blast-furnace slag; Dissolution
ID POLYCARBOXYLATE SUPERPLASTICIZER; SUPERABSORBENT POLYMERS; PORE
STRUCTURE; SILICA FUME; TRIETHANOLAMINE; FINENESS; TRIISOPROPANOLAMINE;
MICROSTRUCTURE; PERFORMANCE; DURABILITY
AB In this study, a commercially available ground granulated blast-furnace slag
(GGBS) was further processed by wet grinding, and WGGBS (wet-grinded GGBS) slurry
with superfine particles was obtained. To avoid self-hydration of slag and augment
the grinding efficiency, one commercially available polycarboxylate
superplasticizer was added. The binder, composed of 10.0% cement and 90.0% WGGBS
with the addition of 0.05% triethanolamine (TEA) and 0.05% triisopropanolamine
(TIPA), was designed; the cement was added to provide alkali environment and
calcium ions, and organic alkali was used to promote the dissolution of GGBS. The
compressive strength of mortar and hydration mechanism was investigated. The
results showed that wet grinding exhibited high grinding efficiency; D(50) value of
particle size distribution of WGGBS was reduced from 18 mu m to 2.10 mu m by wet
grinding for one hour. Compressive strength of hardened WGGBS mortar was 20 MPa and
28 MPa at 7 d and 28 d, and 10% cement replacement ratio of the WGGBS increased the
strength to 24.6 MP at 7 d and 32.2 MPa at 28 d. Furthermore, in C-WGGBS, 0.05% TEA
increased the 7 d strength by 23%, with the value of 30.27 MPa, but 0.05%TIPA
slightly reduced it to 23.5 MPa, with a decrease by 5%. Mechanism behind the
increase was due to the accelerated formation of hydrotalcite-like phase, despite
the retarding effect on formation of C-(A)S-H gel; the slight decline by TIPA was
mainly because of the retarding effect of formation of C-(A)S-H gel as well as its
air-entraining effect. Moreover, both TEA and TIPA increased the 28 d strength of
cement-WGGBS system, because TEA and TIPA were able to facilitate ferric and
aluminum dissolution and expedite the formation of C-(A)S-H gel as well as
hydrotalcite-like phase. Additionally, it was worth noting that 0.05% TEA could
make 28 d strength of the binder, composed of only 10% cement, reach 43.7 MPa, in
accordance with the requirement of 42.5 grade cement. (C) 2019 Elsevier Ltd. All
rights reserved.
C1 [Tan, Hongbo; Nie, Kangjun; Guo, Yulin; Zhang, Xun; Deng, Xiufeng] Wuhan Univ
Technol, State Key Lab Silicate Mat Architectures, Wuhan 430070, Hubei, Peoples R
China.
[He, Xingyang; Su, Ying; Yang, Jin] Hubei Univ Technol, Sch Civil Engn
Architecture & Environm, Wuhan 430070, Hubei, Peoples R China.
[He, Xingyang; Su, Ying; Yang, Jin] Hubei Univ Technol, Bldg Waterproof Engn &
Technol Res Ctr Hubei Prov, Wuhan 430070, Hubei, Peoples R China.
Environm, Wuhan 430070, Hubei, Peoples R China.
EM hexycn@163.com
RI Deng, Xiufeng/GWC-8986-2022; Yang, Jin/AAY-3338-2021; Tan,
Hongbo/Q-5972-2018
OI Yang, Jin/0000-0002-5332-7862; Tan, Hongbo/0000-0003-1706-9939
FU Major Technical Innovation Project in Hubei Province of China
[2018AAA002]
FX All the authors gratefully acknowledge financial support from Major
Technical Innovation Project in Hubei Province of China (2018AAA002).
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NR 50
TC 19
Z9 19
U1 1
U2 43
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD MAY 10
PY 2019
VL 206
BP 10
EP 18
DI 10.1016/j.conbuildmat.2019.02.028
PG 9
GA HV8QY
UT WOS:000466249200002
DA 2023-12-05
ER
PT J
AU Pan, XY
Li, JY
Deng, KY
Xu, RK
Shen, RF
AF Pan, Xiao-Ying
Li, Jiu-Yu
Deng, Kai-Ying
Xu, Ren-Kou
Shen, Ren-Fang
TI Four-year effects of soil acidity amelioration on the yields of canola
seeds and sweet potato and N fertilizer efficiency in an ultisol
SO FIELD CROPS RESEARCH
LA English
DT Article
DE Alkaline slag; Organic materials; Acidic soil; Crop yield; Nutrients
uptake; Nitrogen utilization efficiency
ID INDUSTRIAL BY-PRODUCTS; NUTRIENT-UPTAKE; ALKALINE SLAG; ORGANIC-MATTER;
CROP YIELD; BIOMASS ASH; BONE MEAL; ALUMINUM; MAIZE; STRAW
AB A four-year field experiment was conducted in Langxi, Anhui province, China to
investigate the ameliorated effects of various amendments on soil acidity, soil
fertility properties, yields of canola seeds and sweet potato, nutrients uptake,
and nitrogen utilization efficiency by the crops. The nine treatments used were
control, lime, alkaline slag (AS), peanut straw (PS), canola straw (CS), organic
manure (OM), AS + PS, AS + CS, AS + OM. The chemical fertilizers with 150.0 kg ha(-
1) N, 150.0 kg ha(-1) P2O5, and 150.0 kg ha(-1) K2O were applied for all treatments
in canola season, while 90.0 kg ha(-1) N, 90.0 kg ha(-1) P2O5, and 90.0 kg ha(-1)
K2O in sweet potato season. Application of lime, AS, AS + PS, AS + CS, and AS + OM
increased soil pH and decreased soil exchangeable Al3+. AS + OM showed the greatest
ameliorating effect on soil acidity, and soil pH of the treatment increased by 0.45
compared with control. Application of AS + OM also led to greater reduction in soil
exchangeable Al3+ and greater increase in soil exchangeable calcium and magnesium
compared with lime, AS, AS + PS, and AS + CS. Applying amendments alone and
combined promoted the physiological nitrogen use efficiency (PNUE) and nitrogen
partial factor productivity (PFPN) of canola and sweet potato, thus increased the
uptake of N, P, K, Ca, and Mg by the crops, and the yields of canola seeds and
sweet potato. The application of AS + OM showed the greatest effect on the PFPN of
canola among the treatments, while AS + CS was the best treatment for sweet potato
in this aspect. The yield of canola seeds in AS + OM treatment was 2.61 Mg ha(-1),
and 5.84 times greater than that of control, while that of sweet potato in AS + CS
treatment was 8.07 Mg ha(-1), and 32% greater than control. In conclusion, AS + CS,
AS + PS, and AS + OM were the good way to ameliorate soil acidity, increase use
efficiency of nutrients and promote crop production and the AS + OM is the best one
in these treatments.
C1 [Pan, Xiao-Ying; Li, Jiu-Yu; Deng, Kai-Ying; Xu, Ren-Kou; Shen, Ren-Fang]
Chinese Acad Sci, Inst Soil Sci, State Key Lab Soil & Sustainable Agr, Nanjing
[Pan, Xiao-Ying] Univ Chinese Acad Sci, Beijing 100049, Peoples R China.
C3 Chinese Academy of Sciences; Chinese Academy of Sciences; University of
Chinese Academy of Sciences, CAS
EM rkxu@issas.ac.cn
RI Shen, Ren Fang/C-4195-2013
OI Pan, Xiao-ying/0000-0003-0011-8255
Strategic Priority Research Program of the Chinese Academy of Sciences
[XDB15030000]; National Natural Science Foundation of China [41877102]
FX This study was supported by the National Key Research and Development of
China (No. 2016YFD0200302), the Strategic Priority Research Program of
the Chinese Academy of Sciences (No. XDB15030000) and the National
Natural Science Foundation of China (No. 41877102).
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NR 61
TC 19
Z9 20
U1 6
U2 79
PI AMSTERDAM
SN 0378-4290
EI 1872-6852
J9 FIELD CROP RES
JI Field Crop. Res.
PD MAY 1
PY 2019
VL 237
BP 1
EP 11
DI 10.1016/j.fcr.2019.03.019
PG 11
WC Agronomy
SC Agriculture
GA HY6PJ
UT WOS:000468251900001
DA 2023-12-05
ER
PT J
AU Wetzig, T
Baaske, A
Karrasch, S
Brachhold, N
Rudolph, M
Aneziris, CG
AF Wetzig, Tony
Baaske, Andreas
Karrasch, Sven
Brachhold, Nora
Rudolph, Martin
Aneziris, Christos G.
TI Application of exchangeable carbon-bonded alumina foam filters in an
industrial tundish for the continuous casting of steel
LA English
DT Article
DE Continuous casting; Steel melt filtration; Carbon-bonded alumina;
Ceramic foam filter; Non-metallic inclusions
ID INCLUSION REMOVAL; TRANSPORT; QUALITY; METALS; FLOW; MOLD
AB Various melt refining techniques were developed in the past and led to ongoing
improvement of casting quality. One of these processes is the so-called metal melt
filtration, which became state of the art especially in aluminum foundry operations
by using ceramic foam filters. Attempts to adapt the technique for the continuous
casting of steel showed numerous difficulties due to the severe thermomechanical
conditions and the high quantity of processed melt. Premature blockage or failure
of ceramic foam filters implemented in the tundish promoted the application of flow
control devices and multi-hole filters as alternatives. In the present study, a new
approach for ceramic foam filters in the continuous casting of steel was tested.
Thereby, the main disadvantage of limited filter service lifetime was circumvented
by the application of an exchangeable filter system without disturbing the
underlying continuous casting process. Cylindrical carbon-bonded alumina foam
filters were prepared and mounted on alumina-carbon shafts using different
adhesives and slag protection measures. The filters were immersed by a crane into
the steel melt in an industrial tundish with 80 t capacity. During each test, one
batch with approximately 380 t of steel was cast at over 1550 degrees C before
removing the filter. The application of high alumina mortar as adhesive and a
compact filter geometry without macro channels proved to be essential for the
successful operation. Samples of the corresponding filter were analyzed by digital
light microscopy, X-ray diffraction, scanning electron microscopy, energy-
dispersive X-ray spectroscopy and electron backscatter diffraction. The
complementary investigations revealed the formation of pronounced clogging layers
based on aluminum-rich calcium aluminates, which can be clearly distinguished from
the synthetic slag material containing silicon and other trace elements. At the
bottom of the filter pronounced clusters of coral-like and plate-like inclusions
were observed, which approached the filter surface by buoyancy.
C1 [Wetzig, Tony; Brachhold, Nora; Aneziris, Christos G.] Tech Univ Bergakad
Freiberg, Inst Ceram Glass & Construct Mat, Agricolastr 17, D-09599 Freiberg,
Germany.
[Baaske, Andreas; Karrasch, Sven] Thyssenkrupp Steel Europe AG, Kaise Wilhelm
Str 100, D-47166 Duisburg, Germany.
[Rudolph, Martin] Tech Univ Bergakad Freiberg, Inst Mat Sci Struct Res, Gustav
Zeuner Str 5, D-09599 Freiberg, Germany.
C3 Technical University Freiberg; ThyssenKrupp AG; Technical University
Freiberg
RP Wetzig, T (corresponding author), TU Bergakad Freiberg, Agricolastr 17, D-09599
Freiberg, Germany.
EM tony.wetzig@ikgb.tu-freiberg.de
OI Wetzig, Tony/0000-0002-2944-2473
FU German Research Foundation, Germany (DFG) [CRC920]; thyssenkrupp Steel
Europe AG
FX The authors thank the German Research Foundation, Germany (DFG) for the
financial support of the subproject T01 within the framework of the
Collaborative Research Center (CRC920). Further thanks go to
thyssenkrupp Steel Europe AG for the great collaboration and support as
well as to Dr.-Ing. Gert Schmidt for his assistance regarding the SEM
investigations.
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[No title captured]
NR 40
TC 19
Z9 19
U1 1
U2 25
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD DEC 15
PY 2018
VL 44
IS 18
BP 23024
EP 23034
DI 10.1016/j.ceramint.2018.09.105
PG 11
GA HD2MU
UT WOS:000452345500126
DA 2023-12-05
ER
PT J
AU Humad, AM
Provis, JL
Cwirzen, A
AF Humad, Abeer M.
Provis, John L.
Cwirzen, Andrzej
TI Alkali activation of a high MgO GGBS - fresh and hardened properties
LA English
DT Article
DE compressive strength; curing; setting properties
ID BLAST-FURNACE SLAG; SODIUM-CARBONATE; MECHANICAL-PROPERTIES; S-H;
WORKABILITY; STRENGTH; CONCRETE; TEMPERATURE; HYDRATION; BINDERS
AB In this study, concretes and pastes were produced from a high magnesium oxide
(MgO) ground granulated blast furnace slag (magnesium oxide content 16.1 wt%) by
alkali activation with various amounts and combinations of sodium carbonate and
sodium silicate. Sodium carbonate activators tended to reduce slump compared to
sodium silicate at the same dose, and, in contrast to the literature for many blast
furnace slags with more moderate magnesium oxide, to shorten the initial and final
setting times in comparison with concretes activated by sodium silicate for dosages
less than 10 wt%. Higher heat curing temperatures and the use of larger dosages of
alkali activators resulted in higher early-age compressive cube strength values.
The X-ray diffraction analysis of 7 and 28 d old pastes activated with sodium
carbonates revealed formation of gaylussite, calcite, nahcolite and calcium-
aluminium-silicate-hydrate (C-A-S-H) gel. Curing at 20 degrees C appeared to
promote dissolution of gaylussite and calcite, while heat curing promoted their
replacement with C-A-S-H, which also resulted in higher ultimate cube compressive
strength values. Conversely, mixes activated with sodium silicate contained less
crystalline phases and more disordered gel, which strengthened the binder matrix.
C1 [Humad, Abeer M.; Cwirzen, Andrzej] Lulea Univ Technol, Struct Engn Div, Lulea,
Sweden.
[Humad, Abeer M.] Babylon Univ, Civil Engn Dept, Babylon, Iraq.
[Provis, John L.] Univ Sheffield, Dept Mat Sci & Engn, Sheffield, S Yorkshire,
England.
C3 Lulea University of Technology; University of Babylon; University of
Sheffield
RP Humad, AM (corresponding author), Lulea Univ Technol, Struct Engn Div, Lulea,
Sweden.; Humad, AM (corresponding author), Babylon Univ, Civil Engn Dept, Babylon,
Iraq.
EM abeer.humad@ltu.se
RI Provis, John/AAR-3260-2020; cwirzen, andrzej/AAV-1299-2021; Provis, John
L/A-7631-2008; Humad, Abeer/AAT-5691-2020
Humad, Abeer/0000-0002-5328-4073; Cwirzen, Andrzej/0000-0001-6287-2240
FU Iraqi Ministry of Higher Education and Scientific Research, Iraq
FX This research was funded by the Iraqi Ministry of Higher Education and
Scientific Research, Iraq. The authors would like to thank the technical
staff of the laboratory at Lulea University of Technology, Sweden, and
Dr Oday Hussein and Dr Xinyuan Ke (University of Sheffield, UK) for
conducting the XRF analysis.
CR [Anonymous], 2009, 1239032009 BSI EN
[Anonymous], 2015, C143C143M15A ASTM IN
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8846(02)01096-7
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L
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NR 41
TC 19
Z9 20
U1 2
U2 34
PU ICE PUBLISHING
PI WESTMINISTER
SN 0024-9831
EI 1751-763X
J9 MAG CONCRETE RES
JI Mag. Concr. Res.
PD DEC
PY 2018
VL 70
IS 24
BP 1256
EP 1264
DI 10.1680/jmacr.17.00436
PG 9
GA HA4IE
UT WOS:000450222300002
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Madadian, E
Crowe, C
Lefsrud, M
AF Madadian, Edris
Crowe, Christine
Lefsrud, Mark
TI Evaluation of composite fiber-plastics biomass clinkering under the
gasification conditions
LA English
DT Article
DE Gasification; Fiber; Plastic; Clinker; Slag; Refuse-derived-fuel
ID GASOLINE-RANGE HYDROCARBONS; HIGH-DENSITY POLYETHYLENE; FLUIDIZED-BED
REACTOR; OPERATING-CONDITIONS; SI ALLOYS; TEMPERATURE; WASTE;
PRETREATMENT; PYROLYSIS; RECOVERY
AB Cross contamination and non-recyclables remain after the separation of valuables
in the recycling process, especially with commingled or single stream recycling
systems. Therefore, some carbonaceous fractions of recyclables, such as plastics
and fibers, are left as a potential biomass feedstock for the thermochemical or
thermal conversion processes. However, this fraction of waste is more likely to be
highly contaminated and challenging, or may become unpredictable during its reuse
in the thermal conversion process for heat and power applications. The current
study aims to find how the increase in plastic specifically in the recycled fiber
stream may affect the performance of a downdraft gasifier. Therefore, the effect of
plastic combined with fiber feedstock during gasification has been investigated.
For this purpose, three different plastic percentages of 2%, 5%, and 10% mixed with
fiber were studied. The results showed that higher plastic-containing feedstock has
higher energy content; however, the higher plastic content causes mechanical
performance issues inside the reactor and does not necessarily guarantee greater
biomass heating value. Furthermore, gasifying the higher plastic percentage results
in a temperature drop across the reactor. This change in temperature is the result
of thermal reactions of fiber material mixed with plastic that generates firm
clinkers and interrupts the normal conditions in the reactor. The clinker
predominantly contains aluminum, silicon, calcium and sodium that originate from
the source of fiber and plastic. This research has shown that a mixture of silicon
with aluminum, calcium and sodium under high temperatures result in the generation
of a solid clinker that ultimately moves through the reactor and deposits at the
bottom of the reactor. (C) 2017 Elsevier Ltd. All rights reserved.
C1 [Madadian, Edris; Crowe, Christine; Lefsrud, Mark] McGill Univ, Dept Bioresource
Engn, Macdonald Campus,Macdonald Stewart Bldg 21, Ste Anne De Bellevue, PQ H9X 3V9,
Canada.
C3 McGill University
RP Crowe, C (corresponding author), McGill Univ, Dept Bioresource Engn, Macdonald
Campus,Macdonald Stewart Bldg 21, Ste Anne De Bellevue, PQ H9X 3V9, Canada.
EM edris.madadian@mail.mcgill.ca; christine.crowe@mail.mcgill.ca
FU BioFuelNet Canada, a network focusing on the development of advanced
biofuels
FX This research is funded by BioFuelNet Canada, a network focusing on the
development of advanced biofuels. BioFuelNet is a member of the Networks
of Centres of Excellence of Canada program.
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NR 41
TC 19
Z9 19
U1 0
U2 19
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD OCT 15
PY 2017
VL 164
BP 137
EP 145
DI 10.1016/j.jclepro.2017.06.070
PG 9
& Ecology
GA FF8TM
UT WOS:000409290700013
DA 2023-12-05
ER
PT J
AU Wang, JY
Xu, Y
Wang, LS
Zhao, LS
Wang, Q
Cui, DL
Long, ZQ
Huang, XW
AF Wang, Jinyu
Xu, Yang
Wang, Liangshi
Zhao, Longsheng
Wang, Qiang
Cui, Dali
Long, Zhiqi
Huang, Xiaowei
TI Recovery of rare earths and aluminum from FCC catalysts manufacturing
slag by stepwise leaching and selective precipitation
LA English
DT Article
DE REEs; Aluminum; Recovery; FCC catalyst; FCC waste slag
ID ACID; ELEMENTS; KINETICS; ASH; TECHNOLOGIES; BAUXITE
AB A stepwise leaching process was developed to recover rare earth elements (REEs)
and aluminum (Al) from FCC catalysts manufacturing slag (FCC waste slag), with NaOH
and HCl. The FCC waste slag was treated with 2.5 mol/L NaOH at 293 K for 0.5 h to
convert 72.4% of Al into NaAlO2. Then, the caustic conversion residue was decompose
using 3 mol/L HCl to control leaching pH at 1.5 under 293 K for 3 h. Leaching
efficiencies of 94.2%, 98.6% and 98.8% for Al, La and Ce, respectively, were
achieved. 98.7% purity of rare earths oxide (REO) product was obtained after
further treatments including oxalic acid precipitation and calcination. The filter
liquor of oxalic acid precipitation was recycled to acid leaching step to recover
the remaining Al. 97.6% REEs and 98.4% Al were recovered in total. Furthermore, the
polymerization of metal ions and silicates were found and confirmed by IR and XRD
analysis.
C1 [Wang, Jinyu; Xu, Yang; Wang, Liangshi; Zhao, Longsheng; Wang, Qiang; Cui, Dali;
Long, Zhiqi; Huang, Xiaowei] Natl Engn Res Ctr Rare Earth Mat, Gen Res Inst
Nonferrous Met, Beijing 100088, Peoples R China.
RP Wang, LS (corresponding author), Natl Engn Res Ctr Rare Earth Mat, Gen Res Inst
Nonferrous Met, Beijing 100088, Peoples R China.
EM wls1657@163.com
OI Wang, Liangshi/0000-0003-4432-0842
FU Ministry of Industry and Information Technology of China; Beijing Nova
Program [Z161100004916108]
FX This work was supported by Rare-earth Adjustment Upgrade Projects of
Nova Program (grant numbers Z161100004916108).
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NR 30
TC 19
Z9 20
U1 0
U2 16
PU ELSEVIER SCI LTD
PI OXFORD
EI 2213-3437
PD AUG
PY 2017
VL 5
IS 4
BP 3711
EP 3718
DI 10.1016/j.jece.2017.07.018
PG 8
SC Engineering
GA FH4QO
UT WOS:000411143200069
DA 2023-12-05
ER
PT J
AU Liu, HP
Ma, LP
Huang, XF
Yang, J
Tang, JX
Yang, J
Li, JD
Jiang, M
AF Liu, Hongpan
Ma, Liping
Huang, Xiaofeng
Yang, Jie
Tang, Jianxiao
Yang, Jing
Li, Jianduo
Jiang, Ming
TI Phase transformation of glass-ceramics produced by naturally cooled
yellow phosphorus slag during calcination
LA English
DT Review
DE Naturally cooled phosphorus slag; Glass-ceramics; Phase transformation;
Process prediction
ID PRECIPITATED SILICA; ASH; CRYSTALLIZATION; REMOVAL
AB Naturally cooled phosphorus slag is formed during the production of phosphorus,
which contributes to a serious environmental pollution. The crystallization
kinetics has already been evaluated in previously published studies during the
process of CaO-Al2O3 SiO2(CAS) glass-ceramics preparation from naturally cooling
phosphorus slag. This study was focused on calculating the thermodynamic
equilibrium phases of Ca, Al and Si using FactSage6.4 thermodynamic software
package at different temperatures. X-ray diffraction, Fourier transform infrared
spectroscopy and Scanning electron microscopy were employed to examine the phase
status of Ca, Al and Si elements. The results showed that phase transformation
started at 450 degrees C and formation of liquid slag phase occurred at 950 degrees
C in naturally cooled yellow phosphorus slag heated to molten state. The calcium-
containing phase had changed to CaO(slag) and Ca-3(PO4)(2) at high temperatures.
Also, aluminum-containing components present in liquid Al2O3 slag phase formed at
1000 degrees C and silica-containing phase at high temperatures were dominated by
SiO2, CaSiO3, and SiO2(-slag). Finally, SiO2 and further migration to molten
SiO2(slag) were noticed as the temperature rose. (C) 2017 Elsevier B.V. All rights
reserved.
C1 [Liu, Hongpan; Ma, Liping; Huang, Xiaofeng; Yang, Jie; Tang, Jianxiao; Yang,
Jing; Li, Jianduo; Jiang, Ming] Kunming Univ Sci & Technol, Fac Environm Sci &
[Jiang, Ming] Yunnan Agr Univ, Coll Resources & Environm, Kunming 650201,
Yunnan, Peoples R China.
C3 Kunming University of Science & Technology; Yunnan Agricultural
University
RP Ma, LP (corresponding author), Kunming Univ Sci & Technol, Fac Environm Sci &
EM lipingma_kmust@163.com
RI ma, li/HOH-7275-2023
FU Fund for Analyzing and Testing of Kunming University of Science and
Technology [2016P2014607009, 2016T11304019]
FX The authors thank the support of Fund for Analyzing and Testing of
Kunming University of Science and Technology (2016P2014607009,
2016T11304019).
10.1134/S0040579513040027
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NR 27
TC 19
Z9 22
U1 4
U2 60
PI LAUSANNE
SN 0925-8388
EI 1873-4669
J9 J ALLOY COMPD
JI J. Alloy. Compd.
PD JUL 25
PY 2017
VL 712
BP 510
EP 516
DI 10.1016/j.jallcom.2017.04.134
PG 7
GA EV6LN
UT WOS:000401881000065
DA 2023-12-05
ER
PT J
AU Yang, HL
Ye, JS
Wu, XL
Peng, YS
Fang, Y
Zhao, XB
AF Yang, Hulin
Ye, Jiansong
Wu, Xiaoliang
Peng, Yongsheng
Fang, Yi
Zhao, Xinbing
TI Optimum Composition of
CaO-SiO2-Al2O3-MgO Slag for Spring
Steel Deoxidized by Si and Mn in Production
LA English
DT Article
ID DEOXIDATION EQUILIBRIA; INCLUSIONS
AB The relations between plasticity of inclusions and contents of oxygen, aluminum,
and sulfur in molten steel were overall discussed by thermodynamics and FactSage
software. Then, the optimum compositions of slag were obtained and the activities
of components of refining slag system were analyzed. Finally, experiments were
carried out based on the results of calculation. According to the relations, it
could achieve better effect to improve basicity R (R = CaO/SiO2 by mass pct) and
C/A (C/A = CaO/Al2O3 by mass pct) in the low melting temperature [<= 1673 K (<=
1400 degrees C)] region of refining slag as far as possible. For the CaO-SiO2-
Al2O3-MgO slag, the optimum compositions are MgO: 5- 9 pct, CaO: 47.4-50.2 pct,
SiO2: 41.9-45.6 pct and Al2O3: <= 2.79 pct, respectively, in which the basicity is
at the range of 1.0 to 1.19 and C/A is above 9.0. It is proved by experiments that
the plasticity of inclusions and the contents of [O], [Al], and [S] can be
controlled effectively by the optimum composition of refining slag, and the high
cleanness is achieved in spring wire rods. (C) The Minerals, Metals & Materials
Society and ASM International 2016
C1 [Yang, Hulin; Ye, Jiansong; Wu, Xiaoliang; Peng, Yongsheng] Hangzhou Iron &
Steel Grp Co, Ctr Technol, Hangzhou 310022, Zhejiang, Peoples R China.
[Yang, Hulin; Fang, Yi] Hangzhou Iron & Steel Grp Co, Elect Furnace Co LTD,
Hangzhou 310022, Zhejiang, Peoples R China.
[Zhao, Xinbing] Zhejiang Univ, Dept Mat & Ecol Engn, Hangzhou 310007, Zhejiang,
Peoples R China.
RP Yang, HL (corresponding author), Hangzhou Iron & Steel Grp Co, Ctr Technol,
Hangzhou 310022, Zhejiang, Peoples R China.; Yang, HL (corresponding author),
Hangzhou Iron & Steel Grp Co, Elect Furnace Co LTD, Hangzhou 310022, Zhejiang,
Peoples R China.
EM yanghulin2612261@163.com
RI Zhao, X. B./E-4458-2010
FU Hangzhou Iron and Steel Group Company, Hangzhou, Zhejiang, China
FX The authors would like to acknowledge the financial support from
Hangzhou Iron and Steel Group Company, Hangzhou, Zhejiang, China.
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NR 18
TC 19
Z9 26
U1 0
U2 19
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD APR
PY 2016
VL 47
IS 2
BP 1435
EP 1444
DI 10.1007/s11663-015-0581-x
PG 10
Engineering
GA DL2HN
UT WOS:000375454700061
DA 2023-12-05
ER
PT C
AU Abyzov, VA
AF Abyzov, V. A.
BE Radionov, AA
TI Lightweight Refractory Concrete Based on Aluminum-Magnesium-Phosphate
Binder
SO 2ND INTERNATIONAL CONFERENCE ON INDUSTRIAL ENGINEERING (ICIE-2016)
SE Procedia Engineering
LA English
CT 2nd International Conference on Industrial Engineering (ICIE)
CY MAY 19-20, 2016
CL Chelyabinsk, RUSSIA
DE Cellular refractory concrete; Lightweight concrete; Heat-resistant
concrete; Refractory concrete; Phosphate binder; Aluminum magnesium-
phosphate binder
ID SLAGS
AB The paper is discussing the results of works on preparation of refractory
concrete based on aluminum-magnesia-phosphate binder. The modification of magnesia
phosphate binder by aluminum allows increasing the stability of the binder, as well
as the material working temperature. The choice of aluminum is based on the fact
that aluminum-phosphate binders are the most refractory. Corundum manufacturing
waste and used aluminum-chromium catalyst IM-2201 were used as aggregates. These
are dispersed alumina industrial waste that does not require additional milling.
The basic properties of aggregates have been tested. Heat-resistant phosphate
cellular concrete with working temperature up to 1600 degrees C was developed.
Cellular concrete does not require heat treatment; its hardening is due to the
exothermic reaction of aluminum metal and phosphate binder. The phase composition
of the phosphate cement was investigated after curing and burning. The effect of
aggregate type on phase composition was detected. The earlier formation of stable
high-refractory aluminum phosphates was observed. The main refractory properties of
the cellular concrete were tested. It is found that the obtained material is not
inferior to cellular concrete with aluminum-phosphate binder. (C) 2016 The Authors.
Published by Elsevier Ltd.
C1 [Abyzov, V. A.] South Ural State Univ, 76 Lenin Ave, Chelyabinsk 454080, Russia.
C3 South Ural State University
RP Abyzov, VA (corresponding author), South Ural State Univ, 76 Lenin Ave,
Chelyabinsk 454080, Russia.
EM abuzovva@susu.ru
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9374-1
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NR 21
TC 19
Z9 21
U1 0
U2 21
PI AMSTERDAM
SN 1877-7058
J9 PROCEDIA ENGINEER
PY 2016
VL 150
BP 1440
EP 1445
DI 10.1016/j.proeng.2016.07.077
PG 6
WC Engineering, Industrial
SC Engineering
GA BG3KL
UT WOS:000387965000221
OA gold
DA 2023-12-05
ER
PT J
AU López-Delgado, A
Fillali, L
Jiménez, JA
López-Andrés, S
AF Lopez-Delgado, Aurora
Fillali, Laila
Jimenez, Jose A.
Lopez-Andres, Sol
TI Synthesis of α-alumina from a less common raw material
SO JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
LA English
DT Article
DE Alpha-alumina; Boehmite; Sol-gel; Non-conventional raw material
ID HAZARDOUS-WASTE; LOW-TEMPERATURE; GAMMA-ALUMINA; GEL METHOD;
NANOCRYSTALLINE; BOEHMITE; HYDROLYSIS
AB A nanostructured alpha-Al2O3 with particle size lower than 100 nm was obtained
from a hazardous waste generated in slag milling process by the aluminium industry.
The route developed to synthesize alumina consisted of two steps: in the first one,
a precursor of alumina, boehmite, gamma-AlOOH was obtained by a sol-gel method. In
the second step, the alumina was obtained by calcination of the precursor boehmite
(xerogel). Calcination in air was performed at two different temperatures, i.e.
1,300 and 1,400 A degrees C, to determine the influence of this parameter on the
quality of resulting alumina. X-Ray diffraction patterns and transmission electron
microscopy images of calcined powers revealed beside corundum the presence of
transition aluminas and some rest of amorphous phase in the sample prepared at
1,300 A degrees C. The increase of the calcinations temperature to 1,400 A degrees
C favors the formation of an almost single-phase corundum powder. The transition of
theta- to alpha-Al2O3 was followed by means of infrared spectroscopy, since it is
accompanied by the disappearance of the IR band frequencies associated with
tetrahedral sites (AlO4 sites), giving rise to a spectrum dominated by Al3+ ions in
octahedral sites (AlO6) characteristic of corundum.
C1 [Lopez-Delgado, Aurora; Fillali, Laila; Jimenez, Jose A.] CSIC, Natl Ctr Met
Res, Madrid 28040, Spain.
[Fillali, Laila; Lopez-Andres, Sol] UCM, Dept Crystallog & Mineral, Fac Geol,
Madrid 28040, Spain.
C3 Consejo Superior de Investigaciones Cientificas (CSIC); Complutense
RI Lopez-Delgado, Aurora/D-3785-2012; Jimenez, Jose A./H-2644-2015
OI Lopez-Delgado, Aurora/0000-0002-0121-9501; Jimenez, Jose
A./0000-0003-4272-6873; Lopez-Andres, Sol/0000-0003-2052-1674
FU CSIC
FX The authors thank the company Recuperaciones y Reciclajes Roman S.L.
(Fuenlabrada, Madrid, Spain) for supplying the waste and CSIC for the
financial support.
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TC 19
Z9 20
U1 0
U2 43
PU SPRINGER
PI DORDRECHT
SN 0928-0707
J9 J SOL-GEL SCI TECHN
JI J. Sol-Gel Sci. Technol.
PD OCT
PY 2012
VL 64
IS 1
BP 162
EP 169
DI 10.1007/s10971-012-2843-2
PG 8
GA 025CX
UT WOS:000310163400021
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Lee, CG
Park, JA
Kim, SB
AF Lee, Chang-Gu
Park, Jeong-Ann
Kim, Song-Bae
TI Phosphate removal from aqueous solutions using slag microspheres
SO DESALINATION AND WATER TREATMENT
LA English
DT Article
DE Slag microspheres; Phosphate removal; Sorption; Batch experiment; Column
experiment
ID BASIC OXYGEN FURNACE; PHOSPHORUS REMOVAL; BLAST-FURNACE; CONVERTER SLAG;
STEEL SLAG; HYDROXYAPATITE CRYSTALLIZATION; ADSORPTION; WATER;
MECHANISMS; FILTERS
AB The objective of this study was to investigate phosphate removal from aqueous
solutions using slag microspheres produced from converter furnace steel slag (CFSS)
via a slag atomizing process. Batch and column experiments were performed to
examine phosphate removal efficiency of the slag microspheres. X-ray fluorescence
analysis indicated that the slag microspheres were composed of calcium (40.7%) and
iron (25.1%) as well as silica (SiO2), magnesium, aluminum, and manganese. X-ray
diffractometer patterns demonstrated that srebrodolskite (dicalcium ferrite,
Ca2Fe2O5), magnetite (Fe3O4), and hematite (Fe2O3) were the major constituents of
the slag microspheres. Based on kinetic experiments, the reaction reached
equilibrium after around 9 h. Based on equilibrium experiments, the maximum removal
capacity was 10.95 mgP g(-1) from the Langmuir-Freundlich isotherm model. When the
solution pH was increased from 3.2 to 9.2, the removal capacity decreased by one
order of magnitude from 3.16 +/- 0.04 to 0.35 +/- 0.15 mgP g(-1). This indicates
that adsorption on metal hydroxide surfaces may play a major role in the phosphate
removal process using slag microspheres. The decreasing tendency of removal
capacity with increasing pH may be attributed to the surface charge of the slag
microspheres, which have a point of zero charge (PZC) of 7.6. These results also
demonstrated that nitrate (NO3-), chloride (Cl-), and sulfate (SO42-) had minimal
effects on the removal of phosphate at anion concentrations ranging from 0 to 100
mM while bicarbonate greatly interfered with the removal of phosphate resulting in
a 87% reduction of the removal capacity. In column experiments, a phosphate removal
capacity of 2.27 mgP g(-1) was achieved (initial phosphate concentration = 200 mgP
l(-1)). This study demonstrates the potential use of slag microspheres as granular
filter media in flow-through systems for phosphate removal.
C1 [Kim, Song-Bae] Seoul Natl Univ, Dept Rural Syst Engn, Res Inst Agr & Life Sci,
[Lee, Chang-Gu; Park, Jeong-Ann] Seoul Natl Univ, Environm Biocolloid Engn Lab,
C3 Seoul National University (SNU); Seoul National University (SNU)
RP Kim, SB (corresponding author), Seoul Natl Univ, Dept Rural Syst Engn, Res Inst
Agr & Life Sci, Seoul 151921, South Korea.
EM songbkim@snu.ac.kr
OI Lee, Chang-Gu/0000-0002-2304-8635
FU National Research Foundation of Korea; Ministry of Education, Science
and Technology, Republic of Korea [2011-0009688]; National Research
Foundation of Korea [2011-0009688] Funding Source: Korea Institute of
Science & Technology Information (KISTI), National Science & Technology
Information Service (NTIS)
FX This research was supported by the National Research Foundation of
Korea, funded by the Ministry of Education, Science and Technology,
Republic of Korea (grant number 2011-0009688).
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NR 36
TC 19
Z9 25
U1 2
U2 62
PU DESALINATION PUBL
PI HOPKINTON
PA 36 WALCOTT VALLEY DRIVE,, HOPKINTON, MA 01748 USA
SN 1944-3994
EI 1944-3986
J9 DESALIN WATER TREAT
JI Desalin. Water Treat.
PD JUN
PY 2012
VL 44
IS 1-3
BP 229
EP 236
DI 10.1080/19443994.2012.691738
PG 8
GA 949PX
UT WOS:000304589200028
DA 2023-12-05
ER
PT J
AU Lin, YM
Zhou, SQ
Shih, SI
Lin, SL
Wang, LC
Wu, ZS
AF Lin, Yi-Ming
Zhou, Shao-Qi
Shih, Shun-I
Lin, Sheng-Lun
Wang, Lin-Chi
Wu, Zong-Sian
TI Fate of Polychlorinated Dibenzo-p-dioxins and Dibenzofurans
during the Thermal Treatment of Electric Arc Furnace Fly Ash
SO AEROSOL AND AIR QUALITY RESEARCH
LA English
DT Article
DE PCDD/Fs; EAF fly ash; Thermal treatment
ID SOLID-WASTE INCINERATOR; SECONDARY ALUMINUM SMELTERS; SINTER PLANT
WORKERS; STACK FLUE-GASES; METALLURGICAL PROCESSES; STEEL-INDUSTRY;
VITRIFICATION; EMISSIONS; PCDD/F; EXTRACTION
AB Thermal treatment is often employed to recover the metals contained in electric
arc furnace (EAF) fly ash, which is considered a major source of PCDD/Fs. After the
present treatment, the mass and volume of untreated material (EAF fly ash + cullet)
were significantly reduced by 44.2 and 89.2%, respectively; meanwhile the density
increased significantly by 476%. These results indicate that the mass and volume of
EAF fly ash can be effectively reduced to benefit the further disposal in landfill.
Additionally, this study also investigated the fate of polychlorinated dibenzo-p-
dioxins and dibenzofurans (PCDD/Fs) during the thermal treatment. For the EAF fly
ash with an original PCDD/F content of 1414 ng I-TEQ/kg, 99.58% solid destruction
efficiency (SDE) was achieved with thermal treatment at 1450 degrees C. The total
PCDD/F I-TEQ contents in ingot and slag were thus reduced to 9.83 and 6.44 ng I-
TEQ/kg, respectively. The residual PCDD/F I-TEQ content in slag was far below the
soil disposal limit in Taiwan (1000 ng I-TEQ/kg). After PCDD/Fs were decomposed in
a secondary combustion chamber at 1200 degrees C, the thermal treatment without air
pollution control devices (APCDs) displayed an overall 91.28% destruction removal
efficiency (DRE(W/OAPCD)). Furthermore, the total PCDD/F I-TEQ concentrations in
the cooling unit, filter and PUF cartridge were reduced to 1340, 131 and 383 pg I-
TEQ/Nm(3), respectively. Notably, their total amount, 1736 pg I-TEQ/Nm(3), exceeded
the emission limit in Taiwan (400 or 1000 pg I-TEQ/Nm(3)). The cooling unit and
filter used as APCDs in this study could significantly lower the PCDD/F I-TEQ. The
amount of residual PCDD/Fs captured in the PUF cartridge, was low enough (< 400 pg
I-TEQ/Nm(3)) to be directly emitted into the atmosphere. Consequently, the thermal
treatment with APCDs in this study was able to effectively reduce the PCDD/F
contents in EAF fly ash, while the metal contents were recovered as the ingot.
C1 [Shih, Shun-I] Kun Shan Univ, Dept Environm Engn, Tainan 71003, Taiwan.
[Lin, Yi-Ming; Zhou, Shao-Qi] S China Univ Technol, Coll Environm Sci & Engn,
Guangzhou 510640, Peoples R China.
[Lin, Sheng-Lun; Wu, Zong-Sian] Natl Cheng Kung Univ, Dept Environm Engn, Tainan
70101, Taiwan.
[Wang, Lin-Chi] Cheng Shiu Univ, Super Micro Mass Res & Technol Ctr, Kaohsiung
83347, Taiwan.
C3 Kun Shan University; South China University of Technology; National
Cheng Kung University; Cheng Shiu University
RP Shih, SI (corresponding author), Kun Shan Univ, Dept Environm Engn, 949 Da Wan
Rd, Tainan 71003, Taiwan.
EM ssi10@mail.ksu.edu.tw; cbmsgml@gmail.com
RI Lin, Sheng-Lun/A-5139-2016; Wang, Lin-Chi/A-1397-2012; wang,
lin/HHM-2225-2022; wang, lin/HZK-4145-2023
OI Lin, Sheng-Lun/0000-0003-2035-7456; Wang, Lin-Chi/0000-0002-5126-1046;
zhou, shao qi/0000-0001-9838-3983
FU National Science Council in Taiwan [98-2221-E-168-007-]
FX This research was supported in part by the National Science Council in
Taiwan (Grant 98-2221-E-168-007-). The authors also thank Prof. G.P.
Chang-Chien, Mr. Paul Steed, Mr. C.W. Wang and Ms. C.H. Chen for their
insightful discussions and great help in the experimental works.
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NR 52
TC 19
Z9 19
U1 1
U2 30
PU TAIWAN ASSOC AEROSOL RES-TAAR
PI TAICHUNG COUNTY
PA CHAOYANG UNIV TECH, DEPT ENV ENG & MGMT, PROD CTR AAQR, NO 168, JIFONG E
RD, WUFONG TOWNSHIP, TAICHUNG COUNTY, 41349, TAIWAN
SN 1680-8584
J9 AEROSOL AIR QUAL RES
JI Aerosol Air Qual. Res.
PD OCT
PY 2011
VL 11
IS 5
BP 584
EP 595
DI 10.4209/aaqr.2011.07.0099
PG 12
GA 861ET
UT WOS:000298002700013
OA gold
DA 2023-12-05
ER
PT J
AU Karantzalis, AE
Lekatou, A
Georgatis, M
Poulas, V
Mavros, H
AF Karantzalis, A. E.
Lekatou, A.
Georgatis, M.
Poulas, V.
Mavros, H.
TI Casting-Based Production of Al-TiC-AlB2 Composite Material
Through the Use of KBF4 Salt
SO JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE
LA English
DT Article
DE Al-matrix composites; halide salts; melt inoculation; TiC reinforcement
ID B MASTER ALLOYS; METAL-MATRIX COMPOSITES; C PHASE-DIAGRAM; MOLTEN
ALUMINUM; MECHANICAL-PROPERTIES; TIC PARTICLES; HALIDE SALTS; AL-B;
MELTS; TIB2
AB High volume fraction TiC-AlB2 reinforced Al composite material has been produced
by a casting process based on the use of KBF4 salt. The reaction between the salt
compound led to the release of AlB2 precipitates in commercial purity Al melt
whereas the improved wettability between the TiC particles and the formed slag
caused their spontaneous entry. The resulting double reinforced composite showed no
sign of severe TiC dissolution-reaction.
C1 [Karantzalis, A. E.; Lekatou, A.; Georgatis, M.; Poulas, V.; Mavros, H.] Univ
Ioannina, Dept Mat Sci & Engn, GR-45110 Ioannina, Hellas, Greece.
C3 University of Ioannina
RP Karantzalis, AE (corresponding author), Univ Ioannina, Dept Mat Sci & Engn, Univ
Campus, GR-45110 Ioannina, Hellas, Greece.
EM alekatou@cc.uoi.gr
RI Lekatou, Angeliki/AAG-4783-2019
OI Lekatou, Angeliki G./0000-0001-7951-4431
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NR 30
TC 19
Z9 22
U1 0
U2 14
PU SPRINGER
PI NEW YORK
SN 1059-9495
J9 J MATER ENG PERFORM
JI J. Mater. Eng. Perform.
PD MAR
PY 2011
VL 20
IS 2
BP 198
EP 202
DI 10.1007/s11665-010-9668-3
PG 5
GA 719ZL
UT WOS:000287249900006
DA 2023-12-05
ER
PT J
AU Kim, HS
Park, JW
An, YJ
Bae, JS
Han, C
AF Kim, Hyung-Seok
Park, Joo-Won
An, Yong-Jun
Bae, Jong-Soo
Han, Choon
TI Activation of Ground Granulated Blast Furnace Slag Cement by Calcined
Alunite
LA English
DT Article
DE ground granulated blast furnace slag (GGBFS); activator; alunite;
potassium aluminum sulfate; ettringite
ID MECHANICAL-PROPERTIES; MICROSTRUCTURE; PERMEABILITY; CONCRETE
AB To enhance the early strength of grounded granulated blast furnace slag (GGBFS)
blended cement, the activation characteristics of GGBFS were examined by a
potassium aluminum sulfate (PSA) clinker, consisting of KAl(SO4)(2) and amorphous
Al2O3 by calcining alunite [K2SO4 center dot Al-2(SO4)(3)center dot 4Al(OH)(3)] at
650 degrees C for 30 min. The PSA clinker reacted with calcium hydroxide and gypsum
to form ettringite (3CaO center dot Al2O3 center dot 3CaSO(4)center dot 32H(2)O,
AFt) by following reaction: 2KAl(SO4)(2) + 2Al(2)O(3) + 13Ca(OH)(2) + 5(CaSO4
center dot 2H(2)O) + 74H(2)O -> 3(3CaO center dot Al2O3 center dot 3CaSO(4)center
dot 32H(2)O) + 2KOH. Mortar was prepared by mixing a blended cement of GGBFS and
ordinary Portland cement (OPC) with PSA clinker as activator. The compressive
strength of the GGBFS blended cement mortar was compared with that of OPC mortar.
When the PSA clinker and gypsum activator was added to the blended cement of GGBFS
and OPC, the hydration products investigated by DTA and X-ray diffraction were
mainly ettringite and calcium silicate hydrate(C-S-H) gel. The early and long-term
strengths of the GGBFS blended cement were higher than those of OPC. Therefore, PSA
clinker as activator was shown to improve the early and long-term strengths of
GGBFS blended cement. [doi:10.2320/matertrans.M2010350]
C1 [Park, Joo-Won; Bae, Jong-Soo; Han, Choon] Kwangwoon Univ, Dept Chem Engn,
Seoul, South Korea.
[Kim, Hyung-Seok] Korea Inst Geosci & Mineral Resources, Minerals & Mat Proc
Div, Taejon, South Korea.
[An, Yong-Jun] Univ Sci & Technol, Dept Resource Recycling Engn, Taejon, South
Korea.
C3 Kwangwoon University; Korea Institute of Geoscience & Mineral Resources
(KIGAM)
RP Han, C (corresponding author), Kwangwoon Univ, Dept Chem Engn, Seoul, South
Korea.
EM chan@kw.ac.kr
FU Korea Evaluation Institute of Industrial Technology (KEIT) [10035222,
10035123] Funding Source: Korea Institute of Science & Technology
Information (KISTI), National Science & Technology Information Service
(NTIS)
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PU JAPAN INST METALS & MATERIALS
PI SENDAI
SN 1345-9678
EI 1347-5320
J9 MATER TRANS
JI Mater. Trans.
PD FEB
PY 2011
VL 52
IS 2
BP 210
EP 218
PG 9
Engineering
GA 745SS
UT WOS:000289186800015
OA Bronze
DA 2023-12-05
ER
PT J
AU Monaghan, BJ
Chapman, MW
Nightingale, SA
AF Monaghan, B. J.
Chapman, Michael W.
Nightingale, Sharon A.
TI Carbon Transfer in the Lower Zone of a Blast Furnace
LA English
CT Seetharaman Seminar on Materials Processing Towards Properties
CY JUN 14-15, 2010
CL Stockholm, SWEDEN
DE coke dissolition; ironmaking; wetting
ID COKE DISSOLUTION; KINETICS; IRON; ALUMINATE; MECHANISM
AB In this paper results from an investigation focused on coke/iron reactions
occurring in the hearth of a blast furnace, below the slag layer, are presented. In
this region, as coke dissolves in the iron there is the potential for a mineral
layer to form and persist at the coke/iron interface and inhibit the rate of coke
dissolution. Key findings of the investigation include that the composition of the
mineral layer was principally composed of oxides of aluminium and calcium, present
as various calcium aluminates and that the morphology of the layer profoundly
affected the rate of carbon transfer. Follow-up up studies on the kinetics of
carbon transfer focussed on how the wetting and interfacial characteristics of iron
on the calcium aluminates would affect iron penetration of the mineral layer are
also reported and discussed as was a new material, called coke analogue, that could
be used in the study of real industrial coke. Analysis of the wetting behaviour of
liquid iron on alumina and the calcium aluminates investigated indicated that iron
wetting of the mineral layer was not a key parameter in coke dissolution in iron
for the coke composition studied. The brief details given for the coke analogue
indicated that it did replicate coke dissolution behaviour in iron, though more
experimental work is required to fully understand and exploit the potential of this
material.
C1 [Monaghan, B. J.; Nightingale, Sharon A.] Univ Wollongong, PYROmet Res Grp,
Wollongong, NSW 2522, Australia.
C3 University of Wollongong
RP Monaghan, BJ (corresponding author), Univ Wollongong, PYROmet Res Grp,
Wollongong, NSW 2522, Australia.
EM monaghan@uow.edu.au
OI Monaghan, Brian/0000-0002-6341-3588
FU BlueScope Steel; Australian Research Council
FX The authors would like to thank Dr David Wexler at the University of
Wollongong and Dr John Mathieson and Dr Robert Nightingale of BlueScope
Steel for their support and advice during this study. The Australian
Research Council is acknowledged for their financial support of the
research programme.
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NR 17
TC 19
Z9 22
U1 2
U2 13
PI WEINHEIM
SN 1611-3683
EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD OCT
PY 2010
VL 81
IS 10
BP 829
EP 833
DI 10.1002/srin.201000143
PG 5
GA 672RZ
UT WOS:000283605900004
DA 2023-12-05
ER
PT J
AU Ono, H
Nakajima, K
Maruo, R
Agawa, S
Usui, T
AF Ono, Hideki
Nakajima, Keiji
Maruo, Ryota
Agawa, Shingo
Usui, Tateo
TI Formation Conditions of Mg2TiO4 and
MgAl2O4 in Ti-Mg-Al Complex Deoxidation of Molten
Iron
LA English
CT Conference on Cutting Edge of Studies in Inclusions and Precipitates
Behavior Related to Microstructure Control
CY SEP, 2008
CL Kumamoto, JAPAN
DE inclusion; steelmaking; deoxidation; equilibrium
ID LIQUID-IRON; TITANIUM; THERMODYNAMICS; EQUILIBRIA; MAGNESIUM
AB It is important to study the complex deoxidation equilibrium of molten iron in
Ti-Mg-Al system from the view point of inclusion control. The equilibrium
experiments between molten iron and TiOx-MgO-Al2O3 slag and the thermodynamic
calculation on the complex deoxidation are conducted at 1973 K in the present
study. The liquid phase region of TiOx-MgO-Al2O3 system in equilibrium with molten
iron is clarified at 1973 K. The equilibrium compounds which are coexisted with the
slag on the liquidus curve in the system are identified to be Mg2TiO4, and MgAl2O4.
The equilibrium relation between the deoxidation products (Mg2TiO4 or MgAl2O4) and
the composition of solute elements in steel is investigated, and the conditions
that Mg2TiO4 forms instead of MgAl2O4 nor Al2O3 are examined in the complex
deoxidation of Ti-Mg-Al system. When the aluminum content of molten iron is under 4
mass ppm, Mg2TiO4 forms over the wide concentration range. The concentration range
of MgAl2O4 formation widens as the aluminum content of molten iron increases. It is
necessary to increase Mg content and to decrease Al content in order to form
Mg2TiO4 in the Ti-Mg-Al complex deoxidation of molten iron in the range Ti<0.01
mass%. However, it is difficult in the range of Ti>0.01 mass% to form Mg2TiO4.
C1 [Ono, Hideki; Usui, Tateo] Osaka Univ, Grad Sch Engn, Div Mat & Mfg Sci, Suita,
Osaka 5650871, Japan.
[Nakajima, Keiji] Royal Inst Technol, Dept Mat Sci & Engn, Div Appl Proc Met,
SE-10044 Stockholm, Sweden.
C3 Osaka University; Royal Institute of Technology
RP Ono, H (corresponding author), Osaka Univ, Grad Sch Engn, Div Mat & Mfg Sci, 2-1
Yamadaoka, Suita, Osaka 5650871, Japan.
CR Cha WY, 2006, ISIJ INT, V46, P987, DOI 10.2355/isijinternational.46.987
Pak JJ, 2007, ISIJ INT, V47, P16, DOI 10.2355/isijinternational.47.16
Takamura J., 1990, P 6 INT IR STEEL C, P591
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2004, 182 183 NISH MEM SEM, P128
NR 14
TC 19
Z9 22
U1 0
U2 8
PI TOKYO
JAPAN
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2009
VL 49
IS 7
SI SI
BP 957
EP 964
PG 8
GA 475LW
UT WOS:000268361800005
OA gold
DA 2023-12-05
ER
PT J
AU Dill, HG
Techmer, A
Weber, B
Füssl, M
AF Dill, H. G.
Techmer, A.
Weber, B.
Fuessl, M.
TI Mineralogical and chemical distribution patterns of placers and
ferricretes in Quaternary sediments in SE Germany:: The impact of nature
and man on the unroofing of pegmatites
SO JOURNAL OF GEOCHEMICAL EXPLORATION
LA English
DT Article
DE placers; ferricretes; pegmatite; human impact; quaternary; SE Germany
ID GLACIAL DEPOSITS; ALLUVIAL-FAN; NE BAVARIA; LUMINESCENCE; ORIGIN;
ILMENITE; RUTILE; MINERALIZATION; PSEUDORUTILE; PROVINCE
AB Placer deposits mark the ultimate stage of mineral separation in elastic
sediments by physical processes in an aquatic regime, whereas duricrusts are an
example of extreme element separation by chemical processes in continental
environments of deposition. in Quaternary sediments in SE Germany such contrasting
types of sediments formed on the NE Bavarian Basement which is underlain by
metamorphic and pegmatitic rocks reflecting intense primary element differentiation
by themselves.
The placer deposits were subdivided into trap and bed placers. Together with
three types of encrustation they were put into a scheme illustrating six stages of
land formation. The first-mentioned group of placer deposits formed from the Late
Cretaceous to the Late Tertiary on a vast peneplain under subtropical conditions
(stages I-II). Towards the Quaternary its more acidic meteoric fluids turned
alkaline and linear erosion gradually replaced peneplanation as the main process of
shaping the landscape (stage III). Evidence for these types of alluvial-fluvial Ti
and Sn heavy mineral accumulations and the subtropical climatic conditions can only
be found in the major placer mineral aggregates nigrine and cassiterite which
preserved a great variety of marker minerals in fractures and vugs. Duricrust I
consist of aluminum-phosphate (APS)-bearing phoscretes. Bed placer deposition
started off with colluvial to alluvial placers passing eventually into fluvial
placers (stages IV-V). Type II duricrusts evolved under humid temperate conditions
in the aftermaths of the glacial period. Per-descensum fluids provoked the
precipitation of these phosphate-bearing ferricretes. The elastic sediments were
reworked in a low-sinuosity fluvial drainage system during stage VI. In addition to
the ferricretes mentioned above another type of ferrous encrustations was added to
the depositional system by man in form of fayalite-bearing slags from blast
furnaces. These smelting artifacts were dumped on the floodplain of the modem river
system and kilns which they derived from, were fed with phosphorous iron from
duricrusts of type II. Age data for the latest stages of placer formation have been
obtained from radio-carbon dating of drift wood and luminescence analyses of quartz
and feldspar in placer deposits. These data reveal that morphological processes
sparking placer deposition have obviously been influenced by the intensive clearing
of settlers in the "Oberpfalzer Wald" (=Forest of Upper Palatinate).
The results of the present study may be of assistance to geomorphologists
dealing with continental placer deposits (Sn, Ti, Ce, Zr) and chemical sediments
(ferricretes, phoscretes) which developed in-situ on ancient and modem peneplains.
This is true for geomorphologists in academia and consulting companies alike.
Archaeometallurgists may benefit from these results as they were investigating
smelting residues scattered within alluvial and fluvial deposits of Quaternary age.
Commonly they focus their attention on waste disposals and smelting sites and to a
lesser extent on reworked smelting residues in drainage systems. The target group
number one is among exploration geologists who are in search of continental placer
deposits and want to know more about the elastic dispersion haloes around
phosphate- and oxide-bearing pegmatites. Alluvial to fluvial placer deposits
containing stable and ultrastable heavy minerals may well be preserved as to their
mineralogical composition and chemical patterns even through long-lasting periods
of shaping the landscape. These mineralogical and chemical patterns can be used to
reconstruct the original morphology of a pegmatitic body which today is present
only as "pegmatite ruin". (C) 2007 Published by Elsevier B.V.
C1 [Dill, H. G.] Fed Inst Geosci & Nat Resources, D-30631 Hannover, Germany.
[Techmer, A.] Leibnitz Inst Appl Geosci, D-30631 Hannover, Germany.
C3 Leibniz Institut fur Angewandte Geophysik (LIAG)
RP Dill, HG (corresponding author), Fed Inst Geosci & Nat Resources, POB 510163, D-
30631 Hannover, Germany.
EM dill@bgr.de
RI Dill, Harald Gerold/JEF-6442-2023
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NR 75
TC 19
Z9 19
U1 0
U2 6
PU ELSEVIER
PI AMSTERDAM
SN 0375-6742
EI 1879-1689
J9 J GEOCHEM EXPLOR
JI J. Geochem. Explor.
PD JAN
PY 2008
VL 96
IS 1
BP 1
EP 24
DI 10.1016/j.gexplo.2007.06.003
PG 24
GA 258ZC
UT WOS:000252907900001
DA 2023-12-05
ER
PT J
AU Park, JH
Song, HS
Min, DJ
AF Park, JH
Song, HS
Min, DJ
TI Reduction Behavior of EAF slags containing Cr2O3
using aluminum at 1793 K
LA English
DT Article
DE reduction kinetics; EAF slag; stainless steelmaking; reduction degree;
diffusional mass transfer; mass transfer coefficient; reduction rate
constant; diffusion coefficient; activity
ID STAINLESS STEELMAKING; CHROMIUM-OXIDE; FURNACE SLAGS; CARBON
AB The simultaneous reduction kinetics of Cr2O3, MnO, FeO, and SiO2 in the EAF slag
by aluminum has been investigated at 1793 K to understand the reduction mechanism
of each oxide in the stainless steelmaking conditions. The reduction degree of MnO
reached about 90% and that of FeO and Cr2O3 reached about 80% for 5 min. The
reduction degree of SiO2 continuously increased up to about 55% for 20 min,
followed by a constant value. The reduction of each oxide by aluminum was found to
be controlled by the diffusional mass transfer process in slag phase from the
simple kinetic analysis. The mass transfer coefficient of each oxide was in order
of 'MnO>Cr(2)O(3)congruent toFeOmuch greater thanSiO(2)' in the present system. The
reduction rate constant (log K-o(MO), where MO represents Cr2O3, FeO, MnO, and
SiO2) linearly increases by increasing the product of diffusion coefficient and the
activity of each oxide (log[D(M)(.)a(MO)]) in the slag.
C1 POSCO, Tech Res Lab, Stainless Steel Res Grp, Pohang 790785, South Korea.
POSCO, Stainless Steel Dept, Stainless Steelmaking Technol Dev Grp, Pohang
Yonsei Univ, Dept Met Syst Engn, Seoul 120749, South Korea.
C3 POSCO; POSCO; Yonsei University
RP Park, JH (corresponding author), POSCO, Tech Res Lab, Stainless Steel Res Grp,
RI Min, DongJoon/G-7724-2012
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NR 13
TC 19
Z9 21
U1 0
U2 9
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2004
VL 44
IS 5
BP 790
EP 794
PG 5
GA 823CR
UT WOS:000221587800003
OA gold
DA 2023-12-05
ER
PT J
AU DAVIES, TJ
EMBLEM, HG
HARABI, A
NWOBODO, CS
OGWU, AA
TSANTZALOU, V
AF DAVIES, TJ
EMBLEM, HG
HARABI, A
NWOBODO, CS
OGWU, AA
TSANTZALOU, V
TI CHARACTERIZATION AND PROPERTIES OF ALUMINA-CHROME REFRACTORIES
SO BRITISH CERAMIC TRANSACTIONS AND JOURNAL
LA English
DT Article
AB Resistance to slag attack and thermal shock damage in alumina refractories is
improved by adding chromium(III) oxide. In a study of alumina-chrome refractories,
preparation procedures, grain growth, densification and change in corundum lattice
parameters were studied in sintered compacts made from aluminium(III)
oxide/chromium(III) oxide mixtures. High energy milling gave powders which
densified at low temperatures; grain growth also occurred. XRD confirmed solid
solution formation and showed that for "MA95" and "A17 Reactive" aluminas the
corundum lattice dimensions contracted with 7 wt% chromium(III) oxide, but expanded
with other compositions. With "AMS9" alumina and 7 wt% chromium(III) oxide a high
temperature (1700-degrees-C) and a long time (12 h) of sintering gave minimum
average grain size. The modulus of rupture at ambient temperature of a series of
compacts prepared from "AMS9" alumina with varying amounts of chromium(III) oxide
was minimum in the range 8-10 wt% chromium(III) oxide. The hot (1150-degrees-C)
modulus of rupture of a series of ethyl-silicate-bonded alumina-chrome refractories
also showed a minimum, at 7 wt% chromium(III) oxide. The good densification,
uniform grain growth and consistent mechanical properties observed in sintered
compacts prepared from powders with small and uniform particle size suggests why
alumina-chrome refractories resist slag attack and thermal shock damage.
C1 UNIV MANCHESTER,MANCHESTER ROYAL INFIRM,MANCHESTER M13 9WL,LANCS,ENGLAND.
C3 University of Manchester
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PU INST OF CERAMICS
PI STOKE-ON-TRENT
PA SHELTON HOUSE, STOKE-ON-TRENT, ENGLAND ST4 2DR
SN 0307-7357
J9 BRIT CERAM TRANS J
PD MAY-JUN
PY 1992
VL 91
IS 3
BP 71
EP 76
PG 6
GA JB743
UT WOS:A1992JB74300002
DA 2023-12-05
ER
PT J
AU Walkley, B
Ke, XY
Provis, JL
Bernal, SA
AF Walkley, Brant
Ke, Xinyuan
Provis, John L.
Bernal, Susan A.
TI Activator Anion Influences the Nanostructure of Alkali-Activated Slag
Cements
SO JOURNAL OF PHYSICAL CHEMISTRY C
LA English
DT Article
ID C-S-H; SOLID-STATE NMR; LAYERED DOUBLE HYDROXIDES; BLAST-FURNACE SLAG;
MAS NMR; ALUMINUM INCORPORATION; HYDRATION PRODUCTS; PHASE EVOLUTION;
AL-27 NMR; SI-29
AB Alkali-activated materials are promising low-carbon alternatives to Portland
cement; however, there remains an absence of a fundamental understanding of the
effect of different activator types on their reaction products at the atomic scale.
Solid-state Al-27 and Si-29 magic angle spinning (MAS) nuclear magnetic resonance
(NMR) spectroscopy and H-1-Si-29 cross-polarization MAS NMR spectroscopy are used
to reveal the effect of the activator anion on the nanostructure, cross-linking,
and local hydration of aged alkali-activated slag cements. The main reaction
product identified is a mixed cross-linked/non-cross-linked sodium-substituted
calcium aluminosilicate hydrate (C-(N)-A-S-H) gel with a structure comparable to
tobermorite 11 angstrom. Analysis of cross-polarization kinetics revealed that a
higher content of soluble silicate in the activator promoted the incorporation of
Al into the aluminosilicate chains of C-(N)-A-S-H gels, charge-balanced
preferentially by protons within the gel interlayer. In sodium carbonate-activated
slag cements, aluminosilicate chains of C-(N)-A-S-H gels are instead charge-
balanced preferentially by Ca2+ or A(lV) ions. Hydrotalcite was observed as a
secondary reaction product independent of the activator used and in higher
quantities as the content of sodium carbonate in the activator increases. The
presence of soluble silicates in the activator promotes the formation of an Al-rich
sodium aluminosilicate hydrate (N-A-S-H) gel which was not identified when using
sodium carbonate as the activator. These results demonstrate that the anion type in
the activator promotes significant differences in the nanostructure and local
hydration of the main binding phases forming in alkali-activated slag cements. This
explains the significant differences in properties identified when using these
different activators.
C1 [Ke, Xinyuan] Univ Bath, Dept Architecture & Civil Engn, Bath BA2 7AY, Avon,
England.
[Walkley, Brant; Ke, Xinyuan; Provis, John L.; Bernal, Susan A.] Univ Sheffield,
Dept Mat Sci & Engn, Sheffield S1 3JD, S Yorkshire, England.
[Walkley, Brant] Univ Sheffield, Dept Chem & Biol Engn, Sheffield S1 3JD, S
Yorkshire, England.
[Bernal, Susan A.] Univ Leeds, Sch Civil Engn, Leeds LS2 9JT, W Yorkshire,
England.
C3 University of Bath; University of Sheffield; University of Sheffield;
University of Leeds
RP Walkley, B; Bernal, SA (corresponding author), Univ Sheffield, Dept Mat Sci &
Engn, Sheffield S1 3JD, S Yorkshire, England.; Walkley, B (corresponding author),
Univ Sheffield, Dept Chem & Biol Engn, Sheffield S1 3JD, S Yorkshire, England.;
Bernal, SA (corresponding author), Univ Leeds, Sch Civil Engn, Leeds LS2 9JT, W
Yorkshire, England.
EM b.walkley@sheffield.ac.uk; s.a.bernallopez@leeds.ac.uk
RI Bernal, Susan A/E-8938-2011; Provis, John/AAR-3260-2020
OI Provis, John/0000-0003-3372-8922; Walkley, Brant/0000-0003-1069-1362;
Ke, Xinyuan/0000-0002-1239-6861
FU Engineering and Physical Sciences Research Council (EPSRC), UK
[EP/M003272/1]; EPSRC through EC fellowship [EP/R001642/1]; EPSRC
[EP/M003272/1, EP/R001642/1] Funding Source: UKRI
FX This study has been funded by the Engineering and Physical Sciences
Research Council (EPSRC), UK, through grant EP/M003272/1. Participation
of S.A. Bernal was partially funded by the EPSRC through EC fellowship
EP/R001642/1. All solid-state NMR spectra were obtained at the EPSRC UK
National Solid-state NMR Service at Durham, and we thank Dr David
Apperley for his assistance with acquiring the data. We also thank the
anonymous reviewers of an earlier version of this article for their
constructive input regarding interpretation of some of the NMR data.
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Walkley B, 2020, J PHYS CHEM C, V124, P1681, DOI 10.1021/acs.jpcc.9b10133
10.1016/j.cemconres.2017.05.006
10.1016/j.cemconres.2016.08.010
NR 59
TC 18
Z9 18
U1 2
U2 24
PI WASHINGTON
SN 1932-7447
EI 1932-7455
J9 J PHYS CHEM C
JI J. Phys. Chem. C
PD SEP 23
PY 2021
VL 125
IS 37
BP 20727
EP 20739
DI 10.1021/acs.jpcc.1c07328
EA SEP 2021
PG 13
WC Chemistry, Physical; Nanoscience & Nanotechnology; Materials Science,
Multidisciplinary
GA UZ2CC
UT WOS:000702017100056
OA Green Published, Green Accepted, hybrid
DA 2023-12-05
ER
PT J
AU Alvarez-Ayuso, E
Murciego, A
AF Alvarez-Ayuso, E.
Murciego, A.
TI Stabilization methods for the treatment of weathered arsenopyrite mine
wastes: Arsenic immobilization under selective leaching conditions
LA English
DT Article
DE Mine wastes; Arsenic; Stabilization; Calcite; Ferric sulfate; Aluminum
salt slags
ID SEQUENTIAL EXTRACTION PROCEDURE; AMORPHOUS FERRIC ARSENATE; IRON-OXIDE;
CRYSTALLINE SCORODITE; PHASE-TRANSFORMATIONS; CONTAMINATED SOILS;
SURFACE-CHEMISTRY; AQUEOUS-SOLUTION; MOBILITY; FERRIHYDRITE
AB The release of arsenic from weathered arsenopyrite mine wastes represents a
grave environmental issue, especially when dealing with former mining areas. The
evaluation and development of measures to manage this type of wastes in a
sustainable and economic way are required. In this study different methods based on
the application of chemical amendments were assessed as stabilization systems. For
this purpose, weathered arsenopyrite mine wastes with the occurrence of amorphous
ferric arsenates (AFA)/scorodite as main secondary products, as determined by X-ray
diffraction (XRD) and polarizing microscopy, were used. Stabilization studies were
performed employing two different amendments applied at diverse doses, namely a
combination of calcite and ferric sulfate (CC + Fe(III) salt) and a by-product
generated from the processing of aluminum salt slags (BP-AlOx). The efficacy of
such treatments was assessed using both batch and column leaching essays. Under the
equilibrium conditions imposed by the applied standard batch leaching tests, both
of the treatments at their optimal conditions attained important reductions in the
leachable As concentrations (95-98% and 52-79%, respectively), making mine wastes
acceptable at controlled landfills as established by international legislation.
Nevertheless, under flow leaching conditions the treatment employing CC + Fe(III)
salt was shown not to be an appropriate long-term stabilization method. Conversely,
the treatment with BP-AlOx proved to be more perdurable, decreasing considerably
the As release (>50%) under prolonged leaching conditions. This stabilization
system allowed simultaneously an important transformation of AFA to scorodite.
Additionally, it partially neutralized the acidity generated from mine wastes
without exceeding the pH values above which the solubilization of scorodite could
be enhanced importantly. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Alvarez-Ayuso, E.] IRNASA CSIC, Dept Environm Geochem, C Cordel de Merinas 40-
52, Salamanca 37008, Spain.
[Murciego, A.] Salamanca Univ, Dept Geol, Plza Caidos S-N, Salamanca 37008,
Spain.
de Recursos Naturales y Agrobiologia de Salamanca (IRNASA)
RP Alvarez-Ayuso, E (corresponding author), IRNASA CSIC, Dept Environm Geochem, C
Cordel de Merinas 40-52, Salamanca 37008, Spain.
EM esther.alvarez@irnasa.csic.es
RI Álvarez-Ayuso, Esther/K-9129-2017
OI Álvarez-Ayuso, Esther/0000-0003-2243-8639; Murciego Murciego,
Ascension/0000-0001-7364-6927
FU Ministerio de Ciencia, Innovacion y Universidades (MCIU)
[RTI2018-095433-B-I00]; Spain/Agencia Estatal de Investigacion (AEI);
Spain/Fondo Europeo de Desarrollo Regional (FEDER), UE
FX The present study was carried out under the project TERMET (Grant
number: RTI2018-095433-B-I00) funded by Ministerio de Ciencia,
Innovacion y Universidades (MCIU), Spain/Agencia Estatal de
Investigacion (AEI), Spain/Fondo Europeo de Desarrollo Regional (FEDER),
UE. The authors acknowledge Rafael Lopez Jimenez and BEFESA for
supplying the by-product from the processing of aluminum salt slags.
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NR 83
TC 18
Z9 19
U1 2
U2 47
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD FEB 10
PY 2021
VL 283
AR 125265
DI 10.1016/j.jclepro.2020.125265
PG 18
& Ecology
GA PU0XA
UT WOS:000609031900003
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Li, ZF
Zhang, J
Li, SC
Lin, CJ
Gao, YF
Liu, C
AF Li, Zhaofeng
Zhang, Jian
Li, Shucai
Lin, Chunjin
Gao, Yifan
Liu, Chao
TI Feasibility of preparing red mud-based cementitious materials:
Synergistic utilization of industrial solid waste, waste heat, and tail
gas
LA English
DT Article
DE Red mud-based cementitious materials; Waste heat; Tail gas; Carbonation
disposal; High-temperature disposal; Synergy theory
ID FLY-ASH; CARBONATION
AB In order to address the environmental problems caused by red mud and other
industrial by-products, a new concept was proposed to use red mud to prepare
cementitious materials by incorporating other solid wastes, waste heat, and tail
gas. The feasibility of this synergistic concept was verified by laboratory-scale
tests, and the effect of tail gas and waste heat on solid wastes was revealed by
FTIR (Fourier transform infrared spectroscopy), XRD (X-ray diffraction), and SEM-
EDS (Scanning electron microscopy-Energy Dispersive Spectroscopy), and the key
device for carbonation disposal was developed. The results showed that the
cementitious reactivity of industrial solid wastes can be improved by carbonation
disposal of tail gas. The cementitious reactivity of Sintered red mud, coal gangue,
fly ash, and Bayer red mud was increased by 49.8%, 4.4%, 9.5% and 18.9%,
respectively. The multi-solid waste system with Bayer red mud, steel slag, carbide
slag, aluminum ash, and flue gas desulfurization gypsum can generate high
performance red mud-based cementitious materials (RCM) with a compressive strength
of 8.8 MPa at 1 d under the circumstance of high temperature disposal. And RCM
consists of 2CaO center dot SiO2, 3CaO center dot Al2O3, and CaO center dot (Al2O3
+ Fe2O3). In addition, the mechanical strength and soundness of RCM can be improved
by the carbonation of tail gas. This innovative concept provides a way for the mass
utilization of red mud along with other solid wastes, waste heat and tail gas
through the relevant cementitious materials for use in transportation construction,
and shed light on the cleaner production of industry. (C) 2020 Elsevier Ltd. All
rights reserved.
C1 [Li, Zhaofeng; Zhang, Jian; Li, Shucai; Lin, Chunjin; Gao, Yifan; Liu, Chao]
Shandong Univ, Geotech & Struct Engn Res Ctr, Jinan 250061, Shandong, Peoples R
China.
RP Li, ZF (corresponding author), Shandong Univ, Geotech & Struct Engn Res Ctr,
Jinan 250061, Shandong, Peoples R China.
EM lizf@sdu.edu.cn
RI zhang, yuyang/IVV-5089-2023; Lu, Xiaomei/IUQ-2139-2023; Wang,
Nan/JLL-3980-2023
FU Young Scientists Funds of National Natural Science Foundation of China
[51709158]; China Postdoctoral Science Foundation [2018M632676]; Major
basic Project of Shandong Provincial Natural Science Foundation of China
[ZR2017ZC0734]; Major Project of Chinese National Programs for
Fundamental Research and Development [2017YFC0703100]
FX This study was financially supported by the Young Scientists Funds of
National Natural Science Foundation of China (Grants Nos. 51709158), the
China Postdoctoral Science Foundation Funded Project (No. 2018M632676),
the Major basic Project of Shandong Provincial Natural Science
Foundation of China (Project Nos. ZR2017ZC0734), the Major Project of
Chinese National Programs for Fundamental Research and Development
(Project No. 2017YFC0703100).
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NR 37
TC 18
Z9 22
U1 23
U2 134
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD FEB 20
PY 2021
VL 285
AR 124896
DI 10.1016/j.jclepro.2020.124896
EA JAN 2021
PG 12
& Ecology
GA PU7LD
UT WOS:000609481900015
DA 2023-12-05
ER
PT J
AU Santamaría, L
Vicente, MA
Korili, SA
Gil, A
AF Santamaria, L.
Vicente, M. A.
Korili, S. A.
Gil, A.
TI Saline slag waste as an aluminum source for the synthesis of Zn-Al-Fe-Ti
layered double-hydroxides as catalysts for the photodegradation of
emerging contaminants
LA English
DT Article
DE aluminum industrial waste; Photocatalyst; Adsorption; Diclofenac;
Salicylic acid; Hydrotalcite; Layered double hydroxides; Saline slags
ID HYDROTALCITE-LIKE COMPOUNDS; PHOTOCATALYTIC DEGRADATION; EFFICIENT
PHOTOCATALYSTS; MIXED OXIDES; PHENOL; PHARMACEUTICALS; REDUCTION;
REMOVAL; LDH; VALORIZATION
AB In this work, aluminum extracted from saline slag waste is valorized to create a
layered doublehydroxide series containing zinc and various proportions of
aluminum/titanium. Materials were synthesized by the co-precipitation method with
an Me2+/Me3+ molar ratio of 3:1 and tested for the removal of diclofenac and
salicylic acid from water under UV radiation. The incorporation of 5 wt% iron by
wet impregnation is evaluated. In addition, another series of zinc, aluminum/iron
materials with and without 5 wt% impregnated titanium are tested as catalysts for
comparison. Structural characterization and comparison of the two series was
performed by powder X-ray diffraction (PXRD), nitrogen adsorption at 77 K, scanning
electron microscopy (SEM), X-ray photoelectron spectroscopy (XPS) and temperature-
programmed reduction (TPR) measurements. The uncalcinated samples had a typical
hydrotalcite structure with a high crystallinity; the presence of ZnO, ZnFe2O4 or
Fe3O4 was found after calcination. The specific surface areas of the dried samples
ranged from 78 to 199 m(2)/g, being highest for Zn6Al0.5Ti1.5. Overall, the results
showed that the ZnAlTi series were more effective catalysts than ZnAlFe for
photodegradation of the emerging contaminants diclofenac and salicylic acid, under
UV light at 298 K, considering two concentrations of the organic molecules (5 and
50 mu mol/dm(3)). (C) 2020 Elsevier B.V. All rights reserved.
C1 [Santamaria, L.; Korili, S. A.; Gil, A.] Univ Publ Navarra, Dept Ciencias,
INAMAT, Edificio Acebos,Campus Arrosadia, Pamplona 31006, Spain.
[Vicente, M. A.] Univ Salamanca, GIR QUESCAT, Dept Quim Inorgan, Salamanca
37008, Spain.
RP Gil, A (corresponding author), Univ Publ Navarra, Dept Ciencias, INAMAT,
Edificio Acebos,Campus Arrosadia, Pamplona 31006, Spain.
RI Santamaría, Leticia/ABD-2455-2020; Santamaría, Leticia/K-2587-2018;
Leticia/0000-0003-1248-341X; Vicente, Miguel Angel/0000-0002-6714-0249;
Gil, Antonio/0000-0001-9323-5981
FU Spanish Ministry of Economy, Industry and Competitiveness (AEI/MINECO)
[MAT2016-78863-C2-R]; European Regional Development Fund (ERDF)
[MAT2016-78863-C2-R]; Government of Navarra [PI017-PI039 CORRAL];
Universidad Publica de Navarra; Banco Santander
through projects PI017-PI039 CORRAL. LS thanks the Universidad Publica
de Navarra for a pre-doctoral grant. AG also thanks Banco Santander for
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NR 56
TC 18
Z9 18
U1 1
U2 149
PI LAUSANNE
SN 0925-8388
EI 1873-4669
J9 J ALLOY COMPD
JI J. Alloy. Compd.
PD NOV 30
PY 2020
VL 843
AR 156007
DI 10.1016/j.jallcom.2020.156007
PG 11
GA MV1QH
UT WOS:000556137300004
OA Green Published, Green Accepted
DA 2023-12-05
ER
PT J
AU Font, A
Soriano, L
Tashima, MM
Monzó, J
Borrachero, MV
Payá, J
AF Font, Alba
Soriano, Lourdes
Tashima, Mauro M.
Monzo, Jose
Borrachero, Maria Victoria
Paya, Jordi
TI One-part eco-cellular concrete for the precast industry: Functional
features and life cycle assessment
LA English
DT Article
DE One-part alkali-activated material; Cellular concrete; Life cycle
assessment; CO2 emissions; Blast furnace slag; Biomass ash
ID INORGANIC POLYMER COMPOSITES; ASSESSMENT LCA; ALKALI; SLAG; GEOPOLYMER;
WASTE; STRENGTH; ENERGY
AB This paper focuses on investigating greener alternatives of cellular concrete
technology to fulfil current searches for a shift to circular economy. A novel one-
part eco-cellular concrete (ECC-OP) was developed and studied. The one-part alkali
activated materials (AAM-OP) and new alkali-activated cellular concrete (AACC)
technologies were combined to develop greener alternative of cellular concrete
production. The progressive steps from traditional cellular concrete (TCC) based on
ordinary Portland cement (OPC) and commercial aluminium powder (A) to a 100% waste-
based cellular concrete are presented. Blast furnace slag (BFS) was the precursor,
RHA was employed as the silica source, olive stone biomass ash (OBA) was the alkali
source and recycled aluminium foil (AR) was employed as an aerating agent. The
functional features of the materials were studied and compared to those established
by the European standard and the American Concrete Institute (ACI) Committee 523
guides. The new ECC-OP with a bulk density, compressive strength and thermal
conductivity that respectively equal 660 kg/m(3), 6.3 MPa and 0.20 W/ mK was
obtained. Finally, a cradle-to-gate life cycle assessment (LCA) was made, where the
industrial process of a masonry unit manufacture was raised by using each studied
material. A 96% reduction in the kgCO(2)eq per m(3) of material was reached with
the new proposed ECC-OP compared to TCC manufacturing. (C) 2020 Elsevier Ltd. All
rights reserved.
C1 [Font, Alba; Soriano, Lourdes; Monzo, Jose; Borrachero, Maria Victoria; Paya,
Jordi] Univ Politecn Valencia, Inst Ciencia & Tecnol Hormigon, Grp Invest Quim Mat
Construcc, ICITECH,GIQUIMA Grp, Valencia, Spain.
[Tashima, Mauro M.] Univ Estadual Paulista UNESP, Fac Engn Ilha Solteira, MAC
Grp Pesquisa Mat Alternat Construcao, Ilha Solteira, SP, Brazil.
C3 Universitat Politecnica de Valencia; Universidade Estadual Paulista
RP Payá, J (corresponding author), Univ Politecn Valencia, Inst Ciencia & Tecnol
Hormigon, Grp Invest Quim Mat Construcc, ICITECH,GIQUIMA Grp, Valencia, Spain.
EM jjpaya@cst.upv.es
RI Soriano, Lourdes/F-7471-2014; Tashima, Mauro M./G-9134-2014
OI Soriano, Lourdes/0000-0002-5749-4609; Tashima, Mauro
M./0000-0003-0885-9293; Borrachero/0000-0002-7873-0658
CR AENOR, 2013, 1745 AENOR UNEEN
AENOR, 2001, 77213 AENOR UNEEN
AENOR, 2016, 77212011A1 AENOR UNE
AENOR, 2016, 77142011A1 AENOR UNE
[Anonymous], 2018, EC CIRC SECT CONSTR
[Anonymous], 2011, 20502011 PAS
ASTM International, 2008, D533414 ASTM ASTM IN
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NR 55
TC 18
Z9 18
U1 3
U2 26
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD OCT 1
PY 2020
VL 269
AR 122203
DI 10.1016/j.jclepro.2020.122203
PG 14
& Ecology
GA ND0MS
UT WOS:000561603100035
DA 2023-12-05
ER
PT J
AU Lodeiro, IG
Cristelo, N
Palomo, A
AF Garcia Lodeiro, I.
Cristelo, N.
Palomo, A.
TI Use of industrial by-products as alkaline cement activators
LA English
DT Article
DE Low cost activators; Fly ash; Blast furnace slag; Geopolymer
ID FLY-ASH; MECHANICAL STRENGTH; MORTARS; ALUMINA
AB Alkaline (or geopolymer) cements have proven to be a sustainable alternative to
the ordinary portland cement material. The laboratory reagents normally used as
alkaline activators constitute the most costly and on occasion polluting
constituents of such cementitious systems. This study aimed to explore the use of a
disposed cleaning solution (CS), coming from the aluminium transformation industry,
as an activator for high and low calcium aluminosilicate precursors. For that a
Blast Furnace Slag (BFS) and a type F-Fly Ash (FA) were used. Precursors activated
with a traditional NaOH solutions were used as a reference. Kinetics of reactions
(isothermal calorimetry) were evaluated and mechanical strength of hardened pastes
determined. The nature of the reaction products generated in this new systems were
also identified by using XRD, FTIR, SEM and Si-29 and Al-27 MAS NMR. The findings
showed that the CS can be effectively used to prepare cementitious materials,
particularly when applied to CaO-SiO2-Al2O3 system precursors such as BFS, which
require lower alkalinity than FA-based precursors. The nature of the reaction
products generated in the CS alkali activated systems was similar than those
observed in the reference systems, however Al richer reaction products were
observed in the former. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Garcia Lodeiro, I.; Palomo, A.; Fernandez-Jimenez, A.] Eduardo Torroja Inst
Construct Sci IETcc CSIC, Madrid 28033, Spain.
[Cristelo, N.] Univ Tras Os Montes & Alto Douro, Dept Engn, CQVR, P-5000801 Vila
Real, Portugal.
Tras-os-Montes & Alto Douro
RP Lodeiro, IG (corresponding author), Eduardo Torroja Inst Construct Sci IETcc
CSIC, Madrid 28033, Spain.
EM iglodeiro@ietcc.csic.es
RI Cristelo, Nuno Miguel/B-3636-2010; Fernández, ANA Maria/G-2597-2016;
Garcia-Lodeiro, Ines/ABG-8528-2020
OI Cristelo, Nuno Miguel/0000-0002-3600-1094; Fernández, ANA
Maria/0000-0002-5721-2923; Garcia-Lodeiro, Ines/0000-0003-1778-1651
FU Spanish Ministry of Science, Innovation and Universities
[BIA2016-76466-R]; ERDF [RTC2016-4872-S]; European Union [734833]; Marie
Curie Actions (MSCA) [734833] Funding Source: Marie Curie Actions (MSCA)
FX This research was funded by the Spanish Ministry of Science, Innovation
and Universities under project BIA2016-76466-R and ERDF under project
RTC2016-4872-S (principal investigators Angel Palomo and Ana
Fernandez-Jimenez). In addition, thanks the project from the European
Union's Horizon 2020 research and innovation programme under the Marie
Sklodowska-Curie grant agreement No 734833
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PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD AUG 30
PY 2020
VL 253
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PG 11
GA LW8FS
UT WOS:000539379300008
DA 2023-12-05
ER
PT J
AU Duan, SC
Shi, X
Zhang, MC
Li, B
Yang, WS
Wang, F
Guo, HJ
Guo, J
AF Duan, Sheng-Chao
Shi, Xiao
Zhang, Man-Cang
Li, Bin
Yang, Wen-Sheng
Wang, Fei
Guo, Han-Jie
Guo, Jing
TI Effect of Slag Composition on the Deoxidation and Desulfurization of
Inconel 718 Superalloy by ESR Type Slag Without Deoxidizer Addition
LA English
DT Article
ID SULFUR; BEHAVIOR; STEEL; ALUMINUM; KINETICS; MODEL; CAF2; NI; MECHANISM;
CAO-AL2O3
AB Effects of slag composition and alloy content as well as temperature on the
deoxidation and desulfurization of Inconel 718 superalloy by CaF2-CaO-Al2O3-MgO-
TiO2 ESR-type slag without the addition of a deoxidizer were systematically
investigated by laboratory-scale experiments and the developed mass transfer model.
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a double-layer crucible. The results showed that the oxygen content decreased with
an increase of CaO, MgO and CaF2 content in the slag at 1773 K, and CaO has a great
influence on the deoxidation of Inconel 718 alloy compared with MgO and CaF2 in
slag, which was responsible for the decrease in equilibrium content of sulfur in
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20 ppm in master alloys to about 10 and 6 ppm in alloy ingots at 1773 K,
respectively. Properly increasing the Al and Ti content only lowered the oxygen and
sulfur content in the nickel-based alloy to a limited extent when satisfying the
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Han-Jie; Guo, Jing] USTB, Sch Met & Ecol Engn, 30 Xueyuan Rd, Beijing 100083,
Peoples R China.
[Duan, Sheng-Chao; Shi, Xiao; Zhang, Man-Cang; Li, Bin; Yang, Wen-Sheng; Guo,
Han-Jie; Guo, Jing] USTB, Beijing Key Lab Special Melting & Preparat High E,
[Wang, Fei] Tianjin Cisri Harder Mat & Technol Co Ltd, CISRI, Tianjin 301721,
Peoples R China.
RP Guo, HJ (corresponding author), USTB, Sch Met & Ecol Engn, 30 Xueyuan Rd,
RI Duan, Shengchao/M-1269-2017
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NR 73
TC 18
Z9 18
U1 6
U2 21
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD FEB
PY 2020
VL 51
IS 1
BP 353
EP 364
DI 10.1007/s11663-019-01729-3
PG 12
Engineering
GA KJ2IK
UT WOS:000511881200034
DA 2023-12-05
ER
PT J
AU Azof, FI
Vafeias, M
Panias, D
Safarian, J
AF Azof, Fabian Imanasa
Vafeias, Michail
Panias, Dimitrios
Safarian, Jafar
TI The leachability of a ternary
CaO-Al2O3-SiO2 slag produced from
smelting-reduction of low-grade bauxite for alumina recovery
SO HYDROMETALLURGY
LA English
DT Article
DE Low-grade bauxite; Smelting-reduction; Aluminate slag; Alumina;
Leachability; Leaching residue
ID CALCIUM-CARBONATE; PRECIPITATION; MECHANISM
AB A combination of smelting-reduction of bauxite and leaching treatment of the
produced slag for alumina recovery is known as the Pedersen process. The process is
considered to be more sustainable for producing metallurgical-grade alumina than
the Bayer process as it does not produce bauxite residue (red mud), which is one of
the most abundant industrial byproducts in the world. In this work, the
leachability of a ternary CaO-Al2O3-SiO2 slag produced from smelting-reduction of
low-grade bauxite has been studied. The obtained calcium aluminate-slag consists of
Ca12Al14O33 and CaAl2O4 phases with minor amounts of complex oxide phases. A
leaching series have been carried out at different temperatures,
Na2O(carbonate):Na2O(caustic) concentration ratios. The composition of solids and
leaching liquors were analyzed for measuring the recovery of the aluminum and
silicon. The results show that the highest aluminum extraction extent in the
current study is 46.7%, which is achieved at a temperature of 75 degrees C, 1 atm,
in 60 g/L Na2O(carbonate) solution, in 30 min of leaching time. A passive calcium -
containing layer at the slag's surface acts as a mass transfer barrier for the
reactants and products of the leaching reactions, making their diffusion the rate-
limiting step. A high concentration of Na2O(caustic) may decrease the aluminum
extraction of the slag as a result of insufficient carbonate anions in the system,
where the dissolved aluminum reacts with the calcium cations and produce 3CaO
center dot Al2O3 center dot 6H(2)O phase.
C1 [Azof, Fabian Imanasa; Safarian, Jafar] Norwegian Univ Sci & Technol NTNU, Dept
Mat Sci & Engn, Trondheim, Norway.
[Vafeias, Michail; Panias, Dimitrios] NTUA, Sch Min & Met Engn, Athens, Greece.
C3 Norwegian University of Science & Technology (NTNU); National Technical
University of Athens
RP Azof, FI (corresponding author), Norwegian Univ Sci & Technol NTNU, Dept Mat Sci
& Engn, Trondheim, Norway.
EM fabian.i.azof@ntnu.no
RI Panias, Dimitrios/AAO-1296-2021
FU Research Domain 5 Materials and the Society in SFI Metal Production
[237738]
FX The NTNU has funded the research and supported by the Research Domain 5
Materials and the Society in SFI Metal Production (Project no. 237738).
The School of Mining and Metallurgical Engineering, NTUA, is
acknowledged for the use of leaching reactor, ICP-OES, and XRF analyzer.
The scientific support from the ENSUREAL Horizon 2020 project is also
acknowledged.
CR [Anonymous], 2018, THE LOCAL
[Anonymous], 2016, GUARD
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NR 35
TC 18
Z9 18
U1 1
U2 11
PU ELSEVIER
PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD JAN
PY 2020
VL 191
AR 105184
DI 10.1016/j.hydromet.2019.105184
PG 12
GA KO0CA
UT WOS:000515212700019
DA 2023-12-05
ER
PT J
AU Teoh, F
Veksha, A
Chia, VWK
Udayanga, WDC
Mohamed, DKB
Giannis, A
Lim, TT
Lisak, G
AF Teoh, Florence
Veksha, Andrei
Chia, Victor W. K.
Udayanga, W. D. Chanaka
Mohamed, Dara Khairunnisa Binte
Giannis, Apostolos
Lim, Teik-Thye
Lisak, Grzegorz
TI Nickel-based catalysts for steam reforming of naphthalene utilizing
gasification slag from municipal solid waste as a support
SO FUEL
LA English
DT Article
DE Catalytic steam reforming; Gasification slag; Support coating;
Naphthalene; Nickel catalyst
ID CONSTRUCTION MATERIAL PROPERTIES; TEMPERATURE ARC GASIFICATION; BIOMASS
GASIFICATION; HYDROGEN-PRODUCTION; CARBON DEPOSITION; MODEL-COMPOUND;
TAR REMOVAL; GAS; DECOMPOSITION; PYROLYSIS
AB Nickel-based catalysts were synthesized using gasification slag as an abundant
and inexpensive material with high mechanical strength. The synthesis procedure
comprised of etching of gasification slag with hydrofluoric acid, aluminum
hydroxide addition, impregnation with Ni and calcination. The naphthalene reforming
activity was tested at 850 degrees C and 24,000 h(-1) gas hourly space velocity in
the presence of 50 ppmv H2S and 300 ppmv HCl in gas. The presence of aluminum
hydroxide and an oxidizing environment during the calcination process were
essential for preparation of active catalysts. The addition of 30% of aluminum
hydroxide to gasification slag improved the dispersion of Ni oxide and increased
the Brunauer-Emmett-Teller (BET) specific surface area determined by N-2 adsorption
at -196 degrees C from 4.5 to 15.0 m(2) g(-1) as compared to the catalyst without
aluminum hydroxide. This resulted in the increased naphthalene conversion from 35
to 86%. The activity of Ni in synthesized slag catalyst was approximately 3.2 times
higher than in commercial catalyst due to the deposition of Ni on the outer surface
of catalyst particles. The deposited Al and Ni species were firmly attached to the
slag particles during calcination at 500-1000 degrees C. While high calcination
temperature was beneficial for high mechanical strength of catalyst, the procedure
should be conducted under oxidizing environment. When calcination was carried out
in N-2 environment at 1000 degrees C, the sintering of catalyst particles and
encapsulation of Ni occurred, which drastically decreased the BET specific surface
area to 0.4 m(2) g(-1) and naphthalene conversion to 30%. These negative effects
could be prevented when air was used during calcination, which facilitated earlier
crystallization and inhibited excessive sintering of catalyst, thus, maintaining
the high catalytic activity.
C1 [Teoh, Florence; Veksha, Andrei; Chia, Victor W. K.; Udayanga, W. D. Chanaka;
Mohamed, Dara Khairunnisa Binte; Giannis, Apostolos; Lim, Teik-Thye; Lisak,
Grzegorz] Nanyang Technol Univ, Nanyang Environm & Water Res Inst, Residues &
Resource Reclamat Ctr, 1 Cleantech Loop,CleanTech One, Singapore 637141, Singapore.
[Teoh, Florence] Nanyang Polytech, Sch Chem & Life Sci, 180 Ang Mo Kio Ave 8,
[Udayanga, W. D. Chanaka; Mohamed, Dara Khairunnisa Binte; Lim, Teik-Thye;
Lisak, Grzegorz] Nanyang Technol Univ, Sch Civil & Environm Engn, Singapore 639798,
Singapore.
[Giannis, Apostolos] TUC, Sch Environm Engn, Politechnioupolis 73100, Chania,
Greece.
C3 Danish Hydraulic Institute (DHI); Nanyang Technological University &
National Institute of Education (NIE) Singapore; Nanyang Technological
University; Nanyang Polytechnic; Nanyang Technological University &
National Institute of Education (NIE) Singapore; Nanyang Technological
University
RP Veksha, A; Lisak, G (corresponding author), Nanyang Technol Univ, Nanyang
Environm & Water Res Inst, Residues & Resource Reclamat Ctr, 1 Cleantech
Loop,CleanTech One, Singapore 637141, Singapore.
EM aveksha@ntu.edu.sg; g.lisak@ntu.edu.sg
RI Giannis, Apostolos/AAI-1258-2021; Lisak, Grzegorz/F-3123-2019; Lisak,
Grzegorz/ABC-3061-2020; Lim, Teik Thye/A-3790-2011
OI Giannis, Apostolos/0000-0003-4230-9092; Lisak,
Grzegorz/0000-0003-1662-0709; Lim, Teik Thye/0000-0002-0386-0394; Teoh,
Florence/0009-0007-1199-3932
FU Nanyang Environment and Water Research Institute, Nanyang Technological
University (Singapore); Economic Development Board (Singapore)
FX The authors would like to acknowledge the Nanyang Environment and Water
Research Institute, Nanyang Technological University (Singapore) and
Economic Development Board (Singapore) for financial support of this
research.
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NR 56
TC 18
Z9 21
U1 6
U2 81
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD OCT 15
PY 2019
VL 254
AR 115561
DI 10.1016/j.fuel.2019.05.144
PG 9
GA IL0IJ
UT WOS:000476980200108
DA 2023-12-05
ER
PT J
AU Zhang, ZL
Lü, HH
Li, XZ
Li, XM
Ran, SL
Chen, ZY
Yang, YX
Wu, XR
Li, LS
AF Zhang, Zhengli
Lu, Huihong
Li, Xiazhang
Li, Xiaomao
Ran, Songlin
Chen, Zhiyuan
Yang, Yongxiang
Wu, Xingrong
Li, Liaosha
TI Conversion of
CaTi1-xMnxO3-δ-Based
Photocatalyst for Photocatalytic Reduction of NO via Structure-Reforming
of Ti-Bearing Blast Furnace Slag
LA English
DT Article
DE Photo NH3-SCR; Ti-bearing blast furnace slag; High value-added
recycling; In-situ doped modification; Environmental protection
ID SELECTIVE CATALYTIC-REDUCTION; VISIBLE-LIGHT; NH3; SCR; SR; CA;
NANOCOMPOSITES; REMOVAL; ATIO(3); CATIO3
AB In this work, a novel low-cost and robust approach is developed to covert Ti-
bearing blast furnace slag (Ti-slag) to the main feed stock of photoassisted NH3
selective catalytic reduction (Photo NH3-SCR) of NO with high performance. The
CaTi(1-x)Mn(x)O(3-delta )catalyst was directly extracted from the Ti-bearing slag
with MnO, in situ modification and Na2CO3 reformation followed by dilute
hydrochloric acid leaching and water washing. Various methods were employed to
characterize the structure changes of the slag in the preparation processes of MnO2
in situ doping, Na2CO3 reforming, and leaching. Mn element can be incorporated into
the perovskite CaTiO3 with 0.16 to 1.79 wt % depending on the amount of MnO2 added
in Ti-slag at 1500 degrees C. It is interesting to note that the amount of Mn
incorporated into the perovskite decreases remarkably with increasing the
additional amount of MnO2 in the in situ doped modification, which reaches a
maximum of 9.54 wt % for the reformed slag of 5 wt % MnO2 addition. Moreover, most
of the Si has been transferred to the sodium aluminum oxide instead of diopside,
which is easily removed in the following leaching stage. Further semiquant
crystalline analysis shows that there is 99 wt % of perovsvkite CaTi1-xMnxO3-delta
with 1 wt % hexamagnesium manganese(IV) oxide in the slag after leaching with 5 wt
% MnO2 addition, and the catalyst shows more than 93% NO removal efficiency at 300
degrees C in photoassisted NH3-SCR performance. The present study proposes a new
route for the high value-added recycling of silicate minerals and wastes via
structure-reforming with in situ optimization of secondary resources.
C1 [Zhang, Zhengli; Lu, Huihong; Li, Xiaomao; Ran, Songlin; Wu, Xingrong; Li,
Liaosha] Anhui Univ Technol, Key Lab Met Emiss Reduct & Resources Recycling, Minist
Educ, Maanshan 243002, Peoples R China.
[Lu, Huihong; Li, Xiaomao; Ran, Songlin; Wu, Xingrong; Li, Liaosha] Anhui Univ
Technol, Anhui Prov Key Lab Met Engn & Resources Recycling, Maanshan 243002,
Peoples R China.
[Li, Xiazhang] Changzhou Univ, Adv Catalysis & Green Mfg Collaborat Innovat Ctr,
Changzhou 213164, Peoples R China.
[Chen, Zhiyuan; Yang, Yongxiang] Delft Univ Technol, Dept Mat Sci & Engn, NL-
2628 CD Delft, Netherlands.
C3 Anhui University of Technology; Anhui University of Technology;
Changzhou University; Delft University of Technology
RP Lü, HH (corresponding author), Anhui Univ Technol, Key Lab Met Emiss Reduct &
Resources Recycling, Minist Educ, Maanshan 243002, Peoples R China.; Lü, HH
(corresponding author), Anhui Univ Technol, Anhui Prov Key Lab Met Engn & Resources
Recycling, Maanshan 243002, Peoples R China.
EM lv_huihong@163.com
RI li, xiazhang/HGC-1936-2022; yang, yx/GZM-0464-2022; Yang,
Yuxuan/JEZ-4150-2023; wu, jun/ISB-8607-2023; li, xiao/HKV-8405-2023;
liang, YU/IYT-4334-2023
OI li, xiazhang/0000-0002-2528-4121; Lu, Huihong/0000-0002-2522-8234;
liang, YU/0009-0007-3922-3454
FU National Natural Science Foundation of China [U1660110, U1860102]; Key
Research Program of the Education Commission of Anhui Province of China
[KJ2018A0067]; Anhui Innovation Team Project of New Technology in
Materialization of Metallurgical Solid Wastes; Chinese Scholarship
Council (CSC)
FX The authors greatly acknowledge the National Natural Science Foundation
of China (Grant No. U1660110 and U1860102), the Key Research Program of
the Education Commission of Anhui Province of China (KJ2018A0067) and
Anhui Innovation Team Project of New Technology in Materialization of
Metallurgical Solid Wastes. The authors are also very grateful to Prof.
Jilt Sietsma and Dr. Xueqing Zhang from TU Delft and Mr. Chang Liu from
Anhui University of Technology for the data analysis and experimental
assistance, respectively. H. H. Lu's stay at TU Delft for the part of
the present work in The Netherlands is financially supported by the
Chinese Scholarship Council (CSC) as a visiting scholar.
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NR 44
TC 18
Z9 23
U1 6
U2 88
PI WASHINGTON
SN 2168-0485
PD JUN 17
PY 2019
VL 7
IS 12
BP 10299
EP 10309
PG 21
GA IE2UW
UT WOS:000472240900017
DA 2023-12-05
ER
PT J
AU Si, RZ
Guo, SC
Dai, QL
AF Si, Ruizhe
Guo, Shuaicheng
Dai, Qingli
TI Influence of calcium content on the atomic structure and phase formation
of alkali-activated cement binder
LA English
DT Article
DE atomic structure; calcium hydroxide; geopolymer; pair distribution
function; phase formation
ID C-S-H; FLY-ASH; SILICA REACTION; MICROSTRUCTURAL DEVELOPMENT; ALUMINUM
INCORPORATION; SLAG; METAKAOLIN; HYDROXIDE; MECHANISM; KINETICS
AB The effects of calcium on the atomic structure of alkali-activated binder
materials were investigated. The alkali-activated binder samples with varied Ca/Si
ratios were first statically examined with both the X-ray diffraction (XRD) and
total scattering function analysis. The added calcium can reorder the atomic
structure of the alkali-activated materials and enhance its crystallization based
on the X-ray pair distribution function (PDF) and XRD analysis. In situ PDF
experiments were undertaken to examine the evolution of the atomic structure of
calcium-contained geopolymer. The increase in calcium content accelerated the
dissolution of precursor and the formation of the binder. It was shown that the
additional Ca(OH)(2) could serve as nucleation sites for the precipitation of
sodium aluminosilicate hydrate gel to accelerate the reaction. PDF analysis and XRD
characterization enable the examination of the phase development of alkali-
activated materials at the atomic scale.
C1 [Si, Ruizhe; Guo, Shuaicheng; Dai, Qingli] Michigan Technol Univ, Dept Civil &
Environm Engn, 1400 Townsend Dr, Houghton, MI 49931 USA.
C3 Michigan Technological University
RP Guo, SC; Dai, QL (corresponding author), Michigan Technol Univ, Dept Civil &
Environm Engn, 1400 Townsend Dr, Houghton, MI 49931 USA.
EM sguo3@mtu.edu; qingdai@mtu.edu
RI Guo, Shuaicheng/X-7669-2019; Dai, Qingli/E-2901-2015
OI Guo, Shuaicheng/0000-0002-7658-0457; Dai, Qingli/0000-0001-7760-8012
FU U.S. Department of Energy (DOE)
FX U.S. Department of Energy (DOE)
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NR 58
TC 18
Z9 22
U1 5
U2 58
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD MAR
PY 2019
VL 102
IS 3
BP 1479
EP 1494
DI 10.1111/jace.15968
PG 16
GA HM6TM
UT WOS:000459610500067
DA 2023-12-05
ER
PT J
AU Chen, J
Shevchenko, M
Hayes, PC
Jak, E
AF Chen, Jiang
Shevchenko, Maksym
Hayes, Peter Charles
Jak, Evgueni
TI A Phase Equilibrium of the Iron-rich Corner of the CaO-FeO-
Fe2O3-SiO2 System in Air and the
Determination of the SFC Primary Phase Field
LA English
DT Article
DE SFC; phase equilibria; liquidus; slags; CaO-FeO-Fe2O3-SiO2
ID SOLID-SOLUTION LIMITS; AENIGMATITE STRUCTURE-TYPE; SILICO-FERRITE;
CRYSTAL-STRUCTURE; ALUMINUM SFCA; CALCIUM; STABILITY; HOMOLOG; OXIDE;
ATM
AB Experimental studies of the CaO-FeO-Fe2O3-SiO2 system in air from 1 200 degrees
C to 1 260 degrees C have been carried out in the Fe -rich region with particular
focus on the phase equilibria associated with silico-ferrite of calcium (SFC)
phase. The measurements have been made possible through the use of a modified
experimental technique involving high temperature equilibration and rapid quenching
followed by electron probe X-ray microanalysis (EPMA). Isothermal sections for 1
220 degrees C, 1 240 degrees C, 1 255 degrees C and 1 260 degrees C are reported
providing information on the limits of stability of the SFC solid solution and the
liquidus in the SFC primary phase field for the first time.
C1 [Chen, Jiang; Shevchenko, Maksym; Hayes, Peter Charles; Jak, Evgueni] Univ
Queensland, Pyromet Innovat Ctr, Sch Chem Engn, Brisbane, Qld 4072, Australia.
C3 University of Queensland
RP Shevchenko, M (corresponding author), Univ Queensland, Pyromet Innovat Ctr, Sch
Chem Engn, Brisbane, Qld 4072, Australia.
EM m.shevchenko@uq.edu.au
RI Shevchenko, Maksym/HNP-0886-2023
OI Shevchenko, Maksym/0000-0002-9420-9336; Hayes,
Peter/0000-0002-9257-9253; Jak, Evgueni/0000-0002-7768-1874
FU Baosteel Australia Joint Research Centre (BAJC)
FX This research was supported financially by the Baosteel Australia Joint
Research Centre (BAJC). The authors wish to thank the members of the
Baosteel Ironmaking Institute for their collaboration; in particular
Director, Xiaoming Mao and Mr Qi Wei.
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598
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2016-162
0137-5
9740-5
NR 34
TC 18
Z9 18
U1 0
U2 14
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2019
VL 59
IS 5
BP 795
EP 804
PG 10
GA IA2QT
UT WOS:000469406900007
DA 2023-12-05
ER
PT J
AU Harada, A
Matsui, A
Nabeshima, S
Kikuchi, N
Miki, Y
AF Harada, Akifumi
Matsui, Akitoshi
Nabeshima, Seiji
Kikuchi, Naoki
Miki, Yuji
TI Effect of Slag Composition on MgO•Al2O3
Spinel-Type Inclusions in Molten Steel
LA English
DT Article
DE inclusion; spinel; slag composition; kinetic calculation
ID STAINLESS-STEELS; KINETIC-MODEL; ALUMINUM; PREDICT; METAL
AB It is well known that the formation of MgO center dot Al2O3 spinel-type
inclusions is affected by the slag composition. To clarify the effect of the slag
composition on the formation of spinel-type inclusions, laboratory -scale
experiments were carried out in 30 kg -scale induction furnace. Changes in the
composition of inclusions were investigated with different slag compositions. As
the CaO/SiO2 and CaO/Al2O3 of the slag increased, spinel-type inclusions were
observed, and the total Mg content and average composition of MgO in the inclusions
were also higher. On the other hand, the total Mg content and average composition
of MgO in inclusions decreased with decreasing CaO/SiO2 and CaO/Al2O3 of the slag,
and most inclusions were Al2O3-type inclusions including a small amount of MgO.
Based on the experimental results, a kinetic analysis was carried out using a
calculation model to simulate the reactions between the molten steel, slag,
refractory and inclusions in order to evaluate the effect of the slag composition
on inclusions. The calculated results of the inclusion composition were in good
agreement with the experimental results. In this experimental system, the total Mg
content and spinel-type inclusions were suppressed due to a decrease in the
activity of MgO in the slag and an increase in the oxygen activity at the interface
between the molten steel and slag when the CaO/SiO2 and CaO/Al2O3 of the slag were
lower. Therefore, the formation of spinel-type inclusions can be determined by the
relationship between the MgO activity of the slag and the interfacial activity of
oxygen.
C1 [Harada, Akifumi; Matsui, Akitoshi; Nabeshima, Seiji; Kikuchi, Naoki; Miki,
Yuji] JFE Steel Corp, Steel Res Lab, 1 Kokan Cho, Fukuyama, Hiroshima 7218510,
Japan.
[Nabeshima, Seiji] Mizushima Ferroalloy Corp, 1-1 Kawasakidori, Kurashiki,
Okayama 7128513, Japan.
C3 JFE Holdings, Inc.; JFE Steel
RP Harada, A (corresponding author), JFE Steel Corp, Steel Res Lab, 1 Kokan Cho,
Fukuyama, Hiroshima 7218510, Japan.
EM ak-harada@jfe-steel.co.jp
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NR 15
TC 18
Z9 22
U1 1
U2 14
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 9
BP 1546
EP 1552
PG 7
GA FI4DE
UT WOS:000411919100008
OA gold
DA 2023-12-05
ER
PT J
AU Wang, H
Zhong, YB
Li, Q
Li, WQ
Ren, WL
Lei, ZS
Ren, ZM
He, Q
AF Wang, Huai
Zhong, Yunbo
Li, Qiang
Li, Wanqin
Ren, Weili
Lei, Zuosheng
Ren, Zhongming
He, Qiong
TI Influences of the Transverse Static Magnetic Field on the Droplet
Evolution Behaviors during the Low Frequency Electroslag Remelting
Process
LA English
DT Article
DE electroslag remelting; low frequency current; droplet evolution; static
magnetic field; electromagnetic vibration
ID ELECTROMAGNETIC VIBRATIONS; ALUMINUM-ALLOYS; ESR FURNACE; STEEL;
SIMULATION; MODEL; POWER; MOLD; FLOW
AB To visualize the electroslag remelting (ESR) process, a transparent experimental
model was adopted. The droplet evolution process at the consumable electrode tip
was recorded by a high-speed camera. Different intensities of the transverse static
magnetic field (TSMF) were imposed during the ESR process with a low frequency
current of 5 Hz. The representative processes of formation and detachment of the
droplets under different conditions were given. The results showed that when the
intensities of the TSMF were equal or greater than 0.3 T, the droplet evolution
processes would be influenced remarkably. When the TSMF reached 0.5 T, the liquid
neck would be broken up into two arrays of smaller droplets. The mechanism of the
breakup phenomenon appearing on the droplet neck was discussed. Statistical
analysis of the videos captured by the high-speed camera under different conditions
had been done. The results showed that the separation degree of the droplet necks
and the remelting rate could be increased to a certain extent as the increase of
the TSMF. The features of the collected droplets with the TSMF of 0.7 T showed a
smaller average size and more tiny droplets comparing with what were obtained
without the external magnetic field. The decrease of the droplet size and the
generation of numerous tiny droplets enlarged the interfacial area between metal
and slag tremendously.
C1 [Wang, Huai; Zhong, Yunbo; Li, Qiang; Li, Wanqin; Ren, Weili; Lei, Zuosheng;
Ren, Zhongming] Shanghai Univ, State Key Lab Adv Special Steels, Shanghai 200072,
Peoples R China.
[He, Qiong] Shanghai Univ, Microelect R&D Ctr, Shanghai 200072, Peoples R China.
C3 Shanghai University; Shanghai University
RP Zhong, YB (corresponding author), Shanghai Univ, State Key Lab Adv Special
Steels, Shanghai 200072, Peoples R China.
EM yunboz@staff.shu.edu.cn
RI lei, zs/HOF-2747-2023; Zhong, Yun/HCH-6868-2022
FU National Key Research and Development Program of China [2016YFB0300401];
Science and Technology Commission of Shanghai Municipality [13JC1402500,
15520711000]; Independent Research and Development Project of State Key
of Advanced Special Steel, Shanghai University [SKLASS2015-Z021,
SELF-2014-02]
FX The authors gratefully acknowledged the financial support of the
National Key Research and Development Program of China (2016YFB0300401),
Science and Technology Commission of Shanghai Municipality (Key Project
No. 13JC1402500, 15520711000), and Independent Research and Development
Project of State Key of Advanced Special Steel, Shanghai University
(SKLASS2015-Z021, SELF-2014-02).
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NR 31
TC 18
Z9 19
U1 3
U2 35
PI TOKYO
JAPAN
SN 0915-1559
EI 1347-5460
J9 ISIJ INT
JI ISIJ Int.
PY 2017
VL 57
IS 12
BP 2157
EP 2164
PG 8
GA FR3UR
UT WOS:000418992600010
OA gold
DA 2023-12-05
ER
PT J
AU Zhang, Y
Zhang, TA
Dreisinger, D
Lv, GZ
Zhang, GQ
Zhang, WG
Liu, Y
AF Zhang, Ying
Zhang, Ting-An
Dreisinger, David
Lv, Guo-Zhi
Zhang, Guo-Quan
Zhang, Wei-Guang
Liu, Yan
TI Extraction of vanadium from direct acid leach solution of converter
vanadium slag
LA English
DT Article
DE Vanadium; direct leaching; solvent extraction; separation;
multi-elements; stripping; FT-IR
ID SOLVENT-EXTRACTION; MONO-2-ETHYLHEXYL ESTER; SELECTIVE RECOVERY;
PHOSPHORIC-ACID; ION-EXCHANGE; LACTIC-ACID; STONE COAL; CYANEX 272;
D2EHPA; SEPARATION
AB Direct acid leaching of converter vanadium slag by titanium dioxide waste is
eco-friendly and efficient, but with low selectivity. This novel technique can
result in a vanadium solution which contains chromium(III), aluminium(III),
magnesium(II), manganese(II) and high amount of iron(II) and iron(III). Bis (2-
ethylhexyl) phosphoric acid (D2EHPA)and tri-butyl-phosphate (TBP) diluted with
sulphonated kerosene were applied for vanadium extraction from the multi-element
leach solution. The effects of the initial pH, concentration of D2EHPA, ratio of
organic to aqueous phase, and the extraction time on the extraction efficiency of
vanadium were investigated in saponification and unsaponifiable systems,
respectively. The results showed that the vanadium extraction percentage can be up
to 97% and the iron extraction percentage can be less than 10% in a thirteen-stage
counter-current simulation test and the separation coefficient between vanadium and
iron can reach to 109.8. Furthermore, vanadium(IV) can also be separated from other
impurities such as aluminium(III), magnesium(II), manganese(II), chromium(III)
efficiently. The loaded organic phase was stripped by 184 g L-1 sulphuric acid
solution in a three-stage counter-current stripping process and with the total
vanadium stripping percentage of greater than 99.5%. In the end, the vanadium
pentoxide products with a purity of 99.14% were obtained.
C1 [Zhang, Ying; Zhang, Ting-An; Lv, Guo-Zhi; Zhang, Guo-Quan; Zhang, Wei-Guang;
Liu, Yan] Northeastern Univ, Minist Educ, Key Lab Ecol Utilizat Multimet Intergrown
Ores, Shenyang 100819, Liaoning, Peoples R China.
[Zhang, Ying; Zhang, Ting-An; Lv, Guo-Zhi; Zhang, Guo-Quan; Zhang, Wei-Guang;
Liu, Yan] Northeastern Univ, Sch Met, Shenyang 100819, Liaoning, Peoples R China.
[Zhang, Ying; Dreisinger, David] Univ British Columbia, Dept Mat Engn,
Vancouver, BC V6T 1Z4, Canada.
C3 Northeastern University - China; Northeastern University - China;
University of British Columbia
RP Zhang, TA (corresponding author), Northeastern Univ, Minist Educ, Key Lab Ecol
Utilizat Multimet Intergrown Ores, Shenyang 100819, Liaoning, Peoples R China.;
Zhang, TA (corresponding author), Northeastern Univ, Sch Met, Shenyang 100819,
Liaoning, Peoples R China.; Zhang, TA (corresponding author), Univ British
Columbia, Dept Mat Engn, Vancouver, BC V6T 1Z4, Canada.
EM zta2000@163.net
RI zhang, ting/IYT-0642-2023
OI ZHANG, TING'AN/0000-0002-9778-5259
FU National Natural Science Foundation of China [U1202274, 51504059];
National Science and Technology Support Program [2012BAE01B02];
Fundamental Research Funds for the Central Universities [N100302005];
Doctoral Fund Project [20120042110011]
Foundation of China (Nos. U1202274, 51504059), the National Science and
Technology Support Program (No. 2012BAE01B02), the Fundamental Research
Funds for the Central Universities (No. N100302005), the Doctoral Fund
Project (No. 20120042110011).
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NR 34
TC 18
Z9 18
U1 5
U2 59
PI ABINGDON
SN 0008-4433
EI 1879-1395
J9 CAN METALL QUART
JI Can. Metall. Q.
PY 2017
VL 56
IS 3
BP 281
EP 293
DI 10.1080/00084433.2017.1327501
PG 13
GA FC7SU
UT WOS:000407043300005
DA 2023-12-05
ER
PT J
AU Guo, J
Seo, MD
Shi, CB
Cho, JW
Kim, SH
AF Guo, Jing
Seo, Myung-Duk
Shi, Cheng-Bin
Cho, Jung-Wook
Kim, Seon-Hyo
TI Control of Crystal Morphology for Mold Flux During High-Aluminum AHSS
Continuous Casting Process
LA English
DT Article
ID CRYSTALLIZATION BEHAVIORS; MELT; SLAG; TRANSITION; VISCOSITY; GROWTH;
RATIO
AB In the present manuscript, the efforts to control the crystal morphology are
carried out aiming at improving the lubrication of lime-alumina-based mold flux for
casting advanced high-strength steel with high aluminum. Jackson alpha factors for
crystals of melt crystallization in multi-component mold fluxes are established and
reasonably evaluated by applying thermodynamic databases to understand the crystal
morphology control both in lime-alumina-based and lime-silica-based mold fluxes.
The results show that Jackson alpha factor and supercooling are the most critical
factors to determine the crystal morphology in a mold flux. Crystals precipitating
in mold fluxes appear with different morphologies due to their different Jackson
alpha factors and are likely to be more faceted with higher Jackson alpha factor.
In addition, there is a critical supercooling degree for crystal morphology
dendritic transition. When the supercooling over the critical value, the crystals
transform from faceted shape to dendritic ones in morphology as the kinetic
roughening occurs. Typically, the critical supercooling degrees for cuspidine
dendritic transition in the lime-silica-based mold fluxes are evaluated to be
between 0.05 and 0.06. Finally, addition of a small amount of Li2O in the mold flux
can increase the Jackson alpha factor and decrease the supercooling for cuspidine
precipitation; thus, it is favorable to enhance a faceted cuspidine crystal.
C1 [Guo, Jing; Kim, Seon-Hyo] Pohang Univ Sci Technol POSTECH, Dept Mat Sci & Engn,
[Guo, Jing] Univ Sci & Technol Beijing, Sch Met & Ecol Engn, Beijing 100083,
Peoples R China.
[Seo, Myung-Duk] Casting & Forging Business Grp, Doosan Heavy Ind & Construct,
Chang Won 642792, South Korea.
[Shi, Cheng-Bin] Univ Sci & Technol Beijing, State Key Lab Adv Met, Beijing,
Peoples R China.
Pohang, South Korea.
C3 Pohang University of Science & Technology (POSTECH); University of
Science & Technology Beijing; Doosan Heavy Industries & Construction
Co., Ltd.; University of Science & Technology Beijing; Pohang University
of Science & Technology (POSTECH)
RP Cho, JW (corresponding author), Pohang Univ Sci & Technol POSTECH, Grad Inst
Ferrous Technol, Pohang, South Korea.
RI Cho, Jung-Wook/A-8142-2013; Shi, Chengbin/J-1262-2016
OI Cho, Jung-Wook/0000-0003-2364-1938; Shi, Chengbin/0000-0001-8127-3382
FU Ministry of Trade, Industry & Energy (MOTIE) of Korea within Global
Excellence Technology Innovation [10045029]; Korea Evaluation Institute
of Industrial Technology (KEIT) [10045029] Funding Source: Korea
Institute of Science & Technology Information (KISTI), National Science
& Technology Information Service (NTIS)
FX We gratefully acknowledge the financial support from the Ministry of
Trade, Industry & Energy (MOTIE) of Korea, within the Global Excellence
Technology Innovation (Grant No. 10045029).
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NR 41
TC 18
Z9 19
U1 0
U2 17
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2016
VL 47
IS 4
BP 2211
EP 2221
DI 10.1007/s11663-016-0697-7
PG 11
Engineering
GA DQ9DG
UT WOS:000379510000016
OA Green Published, Bronze
DA 2023-12-05
ER
PT J
AU Dai, X
He, J
Bai, J
Huang, Q
Wen, XD
Xie, L
Luo, K
Zhang, J
Li, W
Du, SY
AF Dai, Xin
He, Jian
Bai, Jin
Huang, Qing
Wen, Xiaodong
Xie, Lu
Luo, Kan
Zhang, Jian
Li, Wen
Du, Shiyu
TI Ash Fusion Properties from Molecular Dynamics Simulation: Role of the
Ratio of Silicon and Aluminum
SO ENERGY & FUELS
LA English
DT Article
ID BORN REPULSIVE PARAMETERS; COMPUTER-SIMULATION; PRESSURE PROPERTIES;
ALKALI HALIDES; IONIC SIZES; COAL ASH; SLAGS; MELTS; NANOPARTICLES;
FUSIBILITY
AB Molecular dynamics simulations are adopted to investigate the effect of the
ratio of silicon and aluminum (S/A) contents on ash fusion properties and to
predict the theoretical melting points and viscosities. The melting points are
identified by the variation of the volume and mean square displacement, while
viscosities are calculated by the Green-Kubo formula. The melting point is
determined to be higher for coal ash systems with higher S/A ratios. The analyses
of the radial distribution function and oxygen contents are performed to illustrate
the structural evolution during the melting process. The interactions of different
types are analyzed to explain the trend of melting points for various S/A ratios.
The main structural features during slag melting are found to be the conversion of
the oxygen atoms from the tricluster type to the bridging type. The viscosities of
the slag systems near melting points are determined to be correlated to the S/A
ratio as well. The computational results from this work may provide new insight
into the mechanism of slag tapping.
C1 [Dai, Xin; Bai, Jin; Wen, Xiaodong; Li, Wen] Chinese Acad Sci, Inst Coal Chem,
State Key Lab Coal Convers, Taiyuan 030001, Shanxi, Peoples R China.
[He, Jian] Chinese Acad Sci, Dalian Inst Chem Phys, Dept Biotechnol, Ctr
Translat Med, Dalian 116023, Liaoning, Peoples R China.
[Huang, Qing; Luo, Kan; Zhang, Jian; Du, Shiyu] Chinese Acad Sci, Ningbo Inst
Mat Technol & Engn, Engn Lab Specialty Fibers & Nucl Energy Mat, Ningbo 315201,
Zhejiang, Peoples R China.
[Xie, Lu] Beihang Univ, Sch Phys & Nucl Energy Engn, Beijing 100191, Peoples R
China.
Academy of Sciences; Dalian Institute of Chemical Physics, CAS; Chinese
Academy of Sciences; Ningbo Institute of Materials Technology and
Engineering, CAS; Beihang University
RP Bai, J; Wen, XD (corresponding author), Chinese Acad Sci, Inst Coal Chem, State
Key Lab Coal Convers, Taiyuan 030001, Shanxi, Peoples R China.; Du, SY
(corresponding author), Chinese Acad Sci, Ningbo Inst Mat Technol & Engn, Engn Lab
Specialty Fibers & Nucl Energy Mat, Ningbo 315201, Zhejiang, Peoples R China.
EM stone@sxicc.ac.cn; wxd@sxicc.ac.cn; dushiyu@nimte.ac.cn
RI 黄, 庆/I-9225-2016; huang, qing/AAD-3909-2019; Dai, Xin/L-8442-2019; He,
Jian/N-9434-2017
OI 黄, 庆/0000-0001-7083-9416; huang, qing/0000-0001-7083-9416; Dai,
Xin/0000-0002-3893-1578; Luo, Kan/0000-0002-8639-6135; He,
Jian/0000-0002-1426-7799; Bai, Jin/0000-0002-8623-1656
51409070]; Shanxi Province Science Foundation for Youths [2015021055];
Joint Foundation of Natural Science Foundation of China [U1261209];
Shenhua Group Corporation, Ltd. [U1261209]; Chinese Academy of Sciences
(CAS)/State Administration of Foreign Experts Affairs (SAFEA)
International Partnership Program for Creative Research Teams;
Fundamental Research Funds for the Central Universities [HEUCFD1421];
Foundation of State Key Laboratory of Coal Conversion [J15-16-301]; Key
Technology of Nuclear Energy, CAS Interdisciplinary Innovation Team of
Chinese Academy of Science; CAS Interdisciplinary Innovation Team of
Chinese Academy of Science
FX The authors acknowledge the financial support provided by the National
Natural Science Foundation of China (21406254, 21476247, and 51409070),
the Shanxi Province Science Foundation for Youths (2015021055), the
Joint Foundation of Natural Science Foundation of China and Shenhua
Group Corporation, Ltd. (U1261209), the Chinese Academy of Sciences
(CAS)/State Administration of Foreign Experts Affairs (SAFEA)
International Partnership Program for Creative Research Teams, the
Fundamental Research Funds for the Central Universities (HEUCFD1421),
the Foundation of State Key Laboratory of Coal Conversion (Grant
J15-16-301), and the Key Technology of Nuclear Energy, 2014, CAS
Interdisciplinary Innovation Team of Chinese Academy of Science and the
computing resources from the Supercomputer Center in Lvliang and
Information Technology at Purdue (ITaP) at Purdue University.
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NR 30
TC 18
Z9 19
U1 0
U2 62
PI WASHINGTON
SN 0887-0624
EI 1520-5029
J9 ENERG FUEL
JI Energy Fuels
PD MAR
PY 2016
VL 30
IS 3
BP 2407
EP 2413
DI 10.1021/acs.energyfuels.5b02586
PG 7
GA DH1RO
UT WOS:000372562800098
DA 2023-12-05
ER
PT J
AU Fu, XJ
Wen, GH
Liu, Q
Tang, P
Li, JZ
Li, W
AF Fu, Xiaojin
Wen, Guanghua
Liu, Qiang
Tang, Ping
Li, Juzhong
Li, Wei
TI Development and Evaluation of CaO-SiO2 Based Mould Fluxes for
Casting High Aluminum TRIP Steel
LA English
DT Article
DE mould fluxes; high aluminum TRIP steel; CaO-SiO2 slag system
ID HIGH AL STEEL; BEHAVIOR
AB Due to its high content in Al-TRIP steel, Al is easily to react with SiO2 in
mould fluxes during the continuous casting process, which results in the drastic
decrease of SiO2 content, increase of Al2O3 content and the basicity (R=CaO/SiO2),
respectively. The magnitude change of physical properties of the slag can affect
continuous casting process and the surface quality of slabs. Especially, the change
of basicity influenced the crystallization property, and thus influenced the heat
transfer of mould fluxes. In this study, three CaO-SiO2 based mould fluxes A, B,
and C with different basicity (A was the originally used mould fluxes, B and C were
the newly developed mould fluxes) were used to cast high aluminum TRIP steel with
0.80-1.00% Al and 0.085-0.115% carbon. The property change of mould fluxes and its
influence on the quality of the slab surface were evaluated. It is indicated that
appropriate increase of the basicity of base mould fluxes was beneficial to improve
the crystallization property of spent slag and for the inhibition of heat transfer
so as to reduce the occurrence of cracking and depression on the slab surface
effectively. And also, it can shorten the time of slag-metal reaction reaching
dynamic equilibrium and the length of transition slab with defect on surface in the
start casting stage. Accordingly, the quality of slab cast by mould fluxes C was
the best.
C1 [Fu, Xiaojin; Wen, Guanghua; Liu, Qiang; Tang, Ping] Chongqing Univ, Coll Mat
Sci & Engn, Chongqing 400044, Peoples R China.
[Li, Juzhong; Li, Wei] Wuhan Iron & Steel Co Ltd, Wuhan 430080, Peoples R China.
C3 Chongqing University; China Baowu Steel Group
RP Fu, XJ (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
EM fu-xj2007@163.com
National Natural Science Foundation of China (Grant No.: 51274260). The
special efforts of Wuhan Iron and Steel Company Limited (WISCO) are also
greatly appreciated.
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Zhu Z. M., 2008, China patent, Patent No. 200710042540
NR 25
TC 18
Z9 19
U1 2
U2 14
PI WEINHEIM
SN 1611-3683
EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD FEB
PY 2015
VL 86
IS 2
BP 110
EP 120
DI 10.1002/srin.201300473
PG 11
GA CA9CZ
UT WOS:000349219300002
DA 2023-12-05
ER
PT J
AU Magallanes-Rivera, RX
Escalante-García, JI
AF Magallanes-Rivera, R. X.
Escalante-Garcia, J. I.
TI Hemihydrate or waste anhydrite in composite binders with blast-furnace
slag: Hydration products, microstructures and dimensional stability
LA English
DT Article
DE Gypsum; Granulated blast-furnace slag; Silica fume; Fly ash; Reaction;
Hydration products; Microstructure; Ettringite
ID FLY-ASH; GYPSUM; STRENGTH; FLUOROGYPSUM; REACTIVITY; PASTES; BLENDS
AB This paper presents results of an investigation of calcium sulphate-blast
furnace slag binders cured for up to 600 days with small additions of fly-ash or
silica fume. Hemihydrate and fluorgypsum were used as the calcium sulphate sources.
The binders showed good mechanical and hydraulic properties; the water resistance
was attributed to the formation of C-S-H with Ca/Si ratio between 1.08 and 1.78
finely intermixed with the gypsum initially formed. Ettringite was formed after the
reaction between gypsum and aluminum from the slag and fly ash; however, its
formation was hindered in the presence of silica fume, which improved the
dimensional stability. (C) 2014 Elsevier Ltd. All rights reserved.
C1 [Magallanes-Rivera, R. X.; Escalante-Garcia, J. I.] IPN, Ctr Invest & Estudios
Avanzados, Unidad Saltillo, Saltillo 25000, Coahuila, Mexico.
C3 Instituto Politecnico Nacional - Mexico
RP Magallanes-Rivera, RX (corresponding author), UANL, Acad Grp Concrete Technol,
Fac Ingn Civil, San Nicolas De Los Garza 66450, NL, Mexico.
EM ricardo.magallanesrv@uanl.edu.mx
RI Magallanes-Rivera, Ricardo/AAH-7820-2020; Escalante-Garcia, J
Ivan/A-1038-2008; Magallanes-Rivera, Ricardo/B-4817-2019
OI Magallanes-Rivera, Ricardo/0000-0002-3504-720X; Escalante-Garcia, J
Ivan/0000-0001-8128-943X; Magallanes-Rivera, Ricardo/0000-0002-3504-720X
FU Conacyt; [CB53563-Y]
FX Thanks to Conacyt for the scholarship of R.X. Magallanes-Rivera, and the
financial support through project CB53563-Y.
CR [Anonymous], 2004, NMXC414ONNCCE2004
[Anonymous], 2001, NMXC418ONNCCE2001
[Anonymous], 2002, NMXC085ONNCCE2002
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NR 33
TC 18
Z9 18
U1 3
U2 43
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD NOV 30
PY 2014
VL 71
BP 317
EP 326
DI 10.1016/j.conbuildmat.2014.08.054
PG 10
GA AU2WL
UT WOS:000345475300035
DA 2023-12-05
ER
PT J
AU Todoroki, H
Kirihara, F
Kanbe, Y
Miyazaki, Y
AF Todoroki, Hidekazu
Kirihara, Fumiaki
Kanbe, Yuichi
Miyazaki, Yoshiharu
TI Effect of Compositions of Non-metallic Inclusions on CC Nozzle Clogging
of a Fe-Cr-Ni-Mo System Stainless Steel
LA Japanese
DT Article
DE high alloy; stainless steel; inclusion; spinel; nozzle clogging;
continuous casting
ID DEOXIDATION EQUILIBRIA; SPINEL INCLUSIONS; SLAG COMPOSITION; ALLOYS;
304-STAINLESS-STEEL; ALUMINUM; THERMODYNAMICS; MECHANISM; AL
AB A study was carried out to understand the effect of non-metallic inclusion
compositions on nozzle clogging of a Fe-Cr-Ni-Mo system stainless steel, aiming at
developing the consecutive continuous casting technology of two ladles. At first,
nozzle clogging took place leading to the reduction in casting speed. It was found
that the major oxide phase in the accretion observed on the nozzle wall consisted
of MgO center dot Al2O3 spinel oxides. The inclusions observed in the sample taken
from the tundish were spinel which was consistent with the accretion composition.
The phase stability diagram was calculated with the thermodynamic data to
understand how to control the inclusion compositions to prevent nozzle clogging. It
was suggested that the inclusion composition should be controlled to MgO with high
melting point as a countermeasure. It was confirmed that this control brought the
successful casting practices avoiding nozzle clogging. The consistency of the
inclusion compositions with the phase stability diagram proved the validity to
apply thermodynamic data based on the standard taking infinite dilute solution for
the present alloy system.
C1 [Todoroki, Hidekazu; Kirihara, Fumiaki; Kanbe, Yuichi] Nippon Yakin Kogyo Co
Ltd, Tech Res Ctr, Kawasaki Ku, Kawasaki, Kanagawa 2108558, Japan.
[Miyazaki, Yoshiharu] Nippon Yakin Kogyo Co Ltd, Technol Dev Dept, Kawasaki,
Kanagawa 2108558, Japan.
RP Todoroki, H (corresponding author), Nippon Yakin Kogyo Co Ltd, Tech Res Ctr,
Kawasaki Ku, 4-2 Kojimacho, Kawasaki, Kanagawa 2108558, Japan.
EM todoroki@nyk.co.jp
OI TODOROKI, HIDEKAZU/0009-0007-2654-1584
CR Ehara Y, 2007, TETSU TO HAGANE, V93, P475, DOI 10.2355/tetsutohagane.93.475
Nakazato H., 2007, ISIJ INT, V47, P365
Ogibayashi S., 1994, Refractories, V46, P166
SASAI K, 1993, TETSU TO HAGANE, V79, P1067, DOI
10.2355/tetsutohagane1955.79.9_1067
Todoroki H., 2009, PROF AS STEEL 2009 I
NR 21
TC 18
Z9 20
U1 0
U2 12
PI TOKYO
JAPAN
SN 0021-1575
EI 1883-2954
J9 TETSU TO HAGANE
PY 2014
VL 100
IS 4
SI SI
BP 539
EP 547
DI 10.2355/tetsutohagane.100.539
PG 9
GA CC2LZ
UT WOS:000350177800013
OA gold
DA 2023-12-05
ER
PT J
AU Chen, M
Raghunath, S
Zhao, BJ
AF Chen, Mao
Raghunath, Sreekanth
Zhao, Baojun
TI Viscosity of SiO2-"FeO"-Al2O3 System in
Equilibrium with Metallic Fe
LA English
DT Article
ID SILICATE-GLASSES; MELTS; ALUMINUM
AB The present study delivered the measurements of viscosities in SiO2-"FeO"-Al2O3
system in equilibrium with metallic Fe. The rotational spindle technique was used
in the measurements at the temperature range of 1473 K to 1773 K (1200 A degrees C
to 1500 A degrees C). Molybdenum crucibles and spindles were employed in all
measurements. The Fe saturation condition was maintained by an iron plate placed at
the bottom of the crucible. The equilibrium compositions of the slags were measured
by EPMA after the viscosity measurements. The effect of up to 20 mol. pct Al2O3 on
the viscosity of the SiO2-"FeO" slag was investigated. The "charge compensation
effect" of the Al2O3 and FeO association has been discussed. The modified quasi-
chemical viscosity model has been optimized in the SiO2-"FeO"-Al2O3 system in
equilibrium with metallic Fe to describe the viscosity measurements of the present
study.
C1 [Chen, Mao; Raghunath, Sreekanth; Zhao, Baojun] Univ Queensland, Sch Chem Engn,
Brisbane, Qld, Australia.
RP Chen, M (corresponding author), Univ Queensland, Sch Chem Engn, Brisbane, Qld,
Australia.
EM baojun@uq.edu.au
RI Chen, Mao/HZL-4582-2023; Chen, Mao/U-8787-2019; Zhao, Baojun/C-1566-2016
OI Chen, Mao/0000-0002-8642-1062; Zhao, Baojun/0000-0002-3423-496X
FU University of Queensland International Research Tuition Award (UQIRTA);
China Scholarship Council (CSC)
FX The authors would like to thank Ms. Jie Yu for the lab assistance in
development of the viscosity measurement technique and Profs. Evgueni
Jak and Peter Hayes for useful discussions. The authors also thank the
University of Queensland International Research Tuition Award (UQIRTA)
and China Scholarship Council (CSC) for providing scholarships for Mao
Chen.
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NR 20
TC 18
Z9 19
U1 0
U2 10
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2013
VL 44
IS 4
BP 820
EP 827
DI 10.1007/s11663-013-9831-y
PG 8
Engineering
GA 181LU
UT WOS:000321669900007
DA 2023-12-05
ER
PT J
AU Arifvianto, B
Wibisono, SKA
Mahardika, M
AF Arifvianto, B.
Wibisono, Suyitno K. A.
Mahardika, M.
TI Influence of grit blasting treatment using steel slag balls on the
subsurface microhardness, surface characteristics and chemical
composition of medical grade 316L stainless steel
SO SURFACE & COATINGS TECHNOLOGY
LA English
DT Article
DE Steel slag balls; Grit blasting treatment; 316L stainless steel; Surface
and subsurface characteristics
ID MECHANICAL ATTRITION TREATMENT; SEVERE PLASTIC-DEFORMATION; AISI 316L;
CORROSION BEHAVIOR; PARTICLE EROSION; ALUMINUM-OXIDE; TREATMENT SMAT;
PURE TITANIUM; AIR BLAST; ROUGHNESS
AB Slag is a residue from the steel making processes which is at present still
considered as an industrial waste due to its low utility. In this paper, the
spherical steel slag balls obtained from the slag atomization process are evaluated
for use in grit blasting treatment of medical grade 316L stainless steel. The
modification in subsurface microhardness, surface characteristics (morphology,
roughness, mass loss) and chemical composition of the stainless steel after the
grit blasting treatment with these particles is examined. The blasting treatment
was carried out for 5-20 min using steel slag balls with a size of 1-2 mm in
diameter and 0.7 MPa compressed air flow in normal direction toward the surface of
the specimen. The result shows the increasing subsurface microhardness, surface
irregularity and roughness of the stainless steel by this treatment. Surface
material removal takes place as well during the blasting treatment as indicated by
the mass loss of the specimen. The mechanisms of the subsurface microhardness
modification as well as those for the surface roughness and mass loss evolution
during the grit blasting treatment are elucidated in this paper. The blasting
treatment with the steel slag balls also introduces some bioactive elements such as
Ca, Si and Mg on the specimen surface. In conclusion, the grit blasting treatment
using the steel slag balls has potential for improving mechanical properties and
bioactivity of stainless steel based biomedical implants. (C) 2012 Elsevier B.V.
C1 [Arifvianto, B.; Wibisono, Suyitno K. A.; Mahardika, M.] Gadjah Mada Univ, Ctr
Innovat Med Equipments & Devices CIMEDs, Dept Mech & Ind Engn, Fac Engn, Yogyakarta
55281, Indonesia.
C3 Gadjah Mada University
RP Arifvianto, B (corresponding author), Gadjah Mada Univ, Ctr Innovat Med
Equipments & Devices CIMEDs, Dept Mech & Ind Engn, Fac Engn, Jl Grafika 2,
Yogyakarta 55281, Indonesia.
EM b.arifvianto@gmail.com
RI Arifvianto, Budi/K-1779-2019; Arifvianto, Budi/D-9344-2013
OI Arifvianto, Budi/0000-0003-4039-4641
FU Department of Mechanical and Industrial Engineering, Gadjah Mada
University, Indonesia [1228/H1.17/TKMPS/PL/2012]
FX Some parts of this work are financially funded by The Graduate Program,
Department of Mechanical and Industrial Engineering, Gadjah Mada
University, Indonesia (Grant No. 1228/H1.17/TKMPS/PL/2012).
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NR 38
TC 18
Z9 18
U1 0
U2 23
PI LAUSANNE
SN 0257-8972
J9 SURF COAT TECH
JI Surf. Coat. Technol.
PD OCT 15
PY 2012
VL 210
BP 176
EP 182
DI 10.1016/j.surfcoat.2012.09.014
PG 7
WC Materials Science, Coatings & Films; Physics, Applied
GA 035KL
UT WOS:000310945300022
DA 2023-12-05
ER
PT J
AU Chen, QY
Johnson, DC
Zhu, LY
Yuan', MH
Hills, CD
AF Chen, Quanyuan
Johnson, D. C.
Zhu, Lingyun
Yuan', Menghong
Hills, C. D.
TI Accelerated carbonation and leaching behavior of the slag from iron and
steel making industry
SO JOURNAL OF UNIVERSITY OF SCIENCE AND TECHNOLOGY BEIJING
LA English
DT Article
DE carbonation; slag; cement; leachate; durability
ID CONCRETE; CEMENTS; MODEL
AB Ground granulated blast furnace slag (GGBFS) and steelmaking slag have been used
as a raw material for cement production or as an aggregate to make concrete, which
contribute aluminum, calcium, iron, and silicon oxides. The suitability of the slag
for a particular application depends on its reactivity, cost, availability, and its
influence on the properties of the resulting concrete. For the interest of
durability studying of concrete in the presence of slag, the accelerated
carbonation products and leaching behavior of the slag and Portland cement (PC)
were studied. The experimental results confirmed that the slag was more resistant
to carbonation compared to PC. The carbonation degree of GGBFS reduced by 17.74%;
and the carbonation degrees of steelmaking slags reduced by 9.51%-11.94%.
Carbonation neutralized the alkaline nature of the hydrated pastes and gave rise to
the redox potential of the leachate slightly (30-77 mV). The carbonation also
increased the release of most of the elements presented, except for calcium, to the
aqueous environment. It is concluded that blend cements (PC plus slag) have
economical advantages and better durability compared to PC.
C1 Donghua Univ, Sch Environm Sci & Engn, Shanghai 200051, Peoples R China.
Univ Greenwich, Sch Sci, Chatham ME4 4TB, Kent, England.
Donghua Univ, Sch Informat Sci & Technol, Shanghai 200051, Peoples R China.
C3 Donghua University; University of Greenwich; Donghua University
RP Chen, QY (corresponding author), Donghua Univ, Sch Environm Sci & Engn, Shanghai
EM qychen@duh.edu.cn
RI Hills, Colin D/C-2012-2008
OI quanyuan, chen/0000-0002-2771-2361
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NR 16
TC 18
Z9 21
U1 2
U2 36
PU INT JOURNAL MINERALS METALLURGY & MATERIALS, EDITORIAL DEPT
PI BEIJING
PA 30 XUEYUANLU, BEIJING 100083, PEOPLES R CHINA
SN 1005-8850
J9 J UNIV SCI TECHNOL B
JI J. Univ. Sci. Technol. Beijing
PD AUG
PY 2007
VL 14
IS 4
BP 297
EP 301
DI 10.1016/S1005-8850(07)60058-9
PG 5
Mineral Processing
GA 210RN
UT WOS:000249473400002
DA 2023-12-05
ER
PT J
AU Siemer, DD
AF Siemer, DD
TI Hydroceramics, a "new" cementitious waste form material for US
defense-type reprocessing waste
SO MATERIALS RESEARCH INNOVATIONS
LA English
DT Article
DE radioactive waste; waste form; concretes; vitrification; hydroceramics;
leach tests; alternative waste forms; HLW
ID DISPOSAL
AB A "hydroceramic" (HC) is a concrete which possesses mineralogy similar to the
zeolitized rock indigenous to the USA's current "basis" high level radioactive
waste (HLW) repository site, Yucca Mountain (YM). It is made by curing a mixture of
inorganic waste, calcined clay, vermiculite, Na2S, NaOH, plus water under
hydrothermal conditions. The product differs from conventional Portland cement
and/or slag-based concretes ("grouts") in that it is primarily comprised of alkali
aluminosilicate "cage minerals" (cancrinites, sodalites, and zeolites)rather than
hydrated calcium silicates (C-S-H in cement-chemistry shorthand). Consequently it
micro-encapsulates individual salt molecules thereby rendering them less leachable
than they are from conventional grouts. A fundamental difference between the
formulations of HCs and radwaste-type glasses is that the latter contain
insufficient aluminum to form insoluble minerals with all of the alkali metals in
them. This means that the imposition of worst-case "repository failure"
(hydrothermal) conditions would cause a substantial fraction of such glasses to
alter to water-soluble forms. Since the same conditions tend to reduce the
solubility of HC concretes, they constitute a more rugged immobilization sub-
system. This paper compares leach characteristics of HCs with those of radwaste-
type glasses and points out why hydroceramic solidification makes more sense than
vitrification for US defense-type reprocessing waste.
RP Siemer, DD (corresponding author), 12 N 3167 E, Idaho Falls, ID 83415 USA.
EM siemdd@inel.gov
CR American Nuclear Society, ANSIANS1611986
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2000, TRICITY HERALD 0808
TRICITY HERALD 0423
NR 34
TC 18
Z9 27
U1 2
U2 15
PU MANEY PUBLISHING
PI LEEDS
SN 1432-8917
EI 1433-075X
J9 MATER RES INNOV
JI Mater. Res. Innov.
PD SEP
PY 2002
VL 6
IS 3
BP 96
EP 104
DI 10.1007/s10019-002-0193-3
PG 9
GA 608JG
UT WOS:000178842300003
DA 2023-12-05
ER
PT J
AU Neuschutz, D
AF Neuschutz, D
TI Plasma processing of dusts and residues
SO PURE AND APPLIED CHEMISTRY
LA English
CT 12th International Symposium on Plasma Chemistry
CY AUG 21-26, 1995
CL MINNEAPOLIS, MN
AB The use of plasma furnaces for the recycling of metal scrap, of metallurgical
residues and of fly-ashes from municipal solid waste (MSW) and sewage sludge (SS)
incineration is reviewed. Aluminium dress, titanium scrap, spent automotive
catalysts and stainless steelmaking dust are examples of current plasma melting
applications. Whereever possible, hollow graphite electrodes tend to replace water-
cooled metal torches. This trend also holds for plasma processing of MSW and SS
incineration residues. In comparative pilot tests with these residues carried out
with transferred-are metal plasma torches and with graphite electrodes,
respectively, no difference in processing behavior was observed. Under oxidizing
conditions in the furnaces and in the off-gas systems, any de novo synthesis of
dioxins was avoided and a vitrified slag, a small off-gas volume and a secondary
fly-ash mainly containing volatile chlorides and sulfates were obtained.
RP Neuschutz, D (corresponding author), RHEIN WESTFAL TH AACHEN,LEHRSTUHL THEORET
HUTTENKUNDE,D-52056 AACHEN,GERMANY.
CR Alexopoulou I.E., 1994, ERZMETALL, V47, P651
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JB STAHL 1995, V1
NR 27
TC 18
Z9 18
U1 0
U2 5
PU BLACKWELL SCIENCE LTD
PI OXFORD
PA OSNEY MEAD, OXFORD, OXON, ENGLAND OX2 0EL
SN 0033-4545
J9 PURE APPL CHEM
JI Pure Appl. Chem.
PD MAY
PY 1996
VL 68
IS 5
BP 1159
EP 1165
DI 10.1351/pac199668051159
PG 7
SC Chemistry
GA UV437
UT WOS:A1996UV43700028
OA Green Submitted, Bronze
DA 2023-12-05
ER
PT J
AU TANABE, J
SUITO, H
AF TANABE, J
SUITO, H
TI EFFECT OF TELLURIUM ON SUPERSATURATION IN ALUMINUM DEOXIDIZED
LIQUID-IRON
LA English
DT Article
ID CAO-AL2O3 MELTS; OXYGEN; EQUILIBRIUM; NITROGEN
AB The effect of tellurium addition on supersaturation observed in aluminum
deoxidized liquid iron was studied at 1873 K, using CaO-Al2O3 slags in an alumina
crucible. Supersaturated oxygen content for a given aluminum level decreased with
the addition of tellurium as a result of lowering the interfacial energy between
liquid iron and alumina and promoting the elimination of precipitated alumina by
notation. Furthermore, the degree of lowering of oxygen content was found to
increase with a decrease in cooling rate. Tellurium distribution ratio between
liquid iron and CaO-Al2O3 slags was determined as a function of aluminum content.
RP TANABE, J (corresponding author), TOHOKU UNIV, INST ADV MAT PROC, SENDAI, MIYAGI
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NR 23
TC 18
Z9 19
U1 0
U2 0
PU SPRINGER
PI NEW YORK
SN 1073-5615
PD FEB
PY 1995
VL 26
IS 1
BP 95
EP 101
DI 10.1007/BF02648982
PG 7
Engineering
GA QD551
UT WOS:A1995QD55100011
DA 2023-12-05
ER
PT J
AU Liu, X
Feng, P
Cai, YX
Yu, XH
Liu, Q
AF Liu, Xin
Feng, Pan
Cai, Yuxi
Yu, Xiaohan
Liu, Qi
TI Carbonation behaviors of calcium silicate hydrate (C-S-H): Effects of
aluminum
LA English
DT Article
DE C-(A)-S-H; Carbonation; Kinetics; Carbonation products
ID QUANTITATIVE-ANALYSIS; CO2 EMISSIONS; CEMENT; SLAG; AL-27; KINETICS
AB The cement systems containing supplementary cementitious materials (SCMs)
usually present lower resistance to carbonation compared with ordinary Portland
cement (OPC) systems. However, the contribution of the main component in these
systems, calcium aluminum silicate hydrate (C-A-S-H), to carbonation still remains
unclear. In this study, the carbonation behaviors of C-S-H and C-A-S-H were
compared by accelerated carbonation experiments. FTIR, XRD, TGA, NMR, and electron
microscope were integrated to reveal the kinetics and thermodynamics of C-(A)-S-H
carbonation. It is concluded that the carbonation of C-(A)-S-H experiences three
periods including dissolution, diffusion, and stationary period, turning into
calcium carbonate with different poly morphs, calcium and aluminum modified silica
gel. In the end product of carbonation, aluminum modified silica gel is observed to
have a similar Al/Si to the initial C-A-S-H. But such small incorporation of
aluminum into C-S-H structure (maximum Al/Si ~ 0.1) can hardly have a significant
effect on its resistance to carbonation.
C1 [Liu, Xin; Feng, Pan; Cai, Yuxi; Yu, Xiaohan; Liu, Qi] Southeast Univ, Sch Mat
Sci & Engn, Jiangsu Key Lab Construct Mat, Nanjing 211189, Peoples R China.
[Feng, Pan] State Key Lab High Performance Civil Engn Mat, Nanjing 210008,
Peoples R China.
C3 Southeast University - China
RP Feng, P (corresponding author), Southeast Univ, Sch Mat Sci & Engn, Jiangsu Key
Lab Construct Mat, Nanjing 211189, Peoples R China.; Feng, P (corresponding
author), State Key Lab High Performance Civil Engn Mat, Nanjing 210008, Peoples R
China.
EM pan.feng@seu.edu.cn
OI Liu, Xin/0000-0002-4143-680X
51825203, 52050128]; Science and Technology Innovation 2025 Major
Project of Ningbo [2020Z040]; State Key Laboratory of High Performance
Civil Engineering Materials Open Fund [2018CEM001]; Innovandi - The
Global Cement and Concrete Research Network; Scientific Research
Foundation of Graduate School of Southeast University [YBPY2144]
FX This work was financially supported by National Natural Science
Foundation of China (Nos. 51890904, 52078126, 51825203, and 52050128) ;
Science and Technology Innovation 2025 Major Project of Ningbo (No.
2020Z040) , and State Key Laboratory of High PerformanceCivil
Engineering Materials Open Fund (No. 2018CEM001) . The authors would
also like to thank the financial support from Innovandi - The Global
Cement and Concrete Research Network (Innovandi is a research consortium
which is the initiative of the GCCA) , and thank Shiyanjia Lab (
www.shiyanjia.com ) for the 27Al NMR measurements. X. Liu is also
gratefully acknowledged for the support by the Scientific Research
Foundation of Graduate School of Southeast University (No. YBPY2144) .
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NR 48
TC 17
Z9 17
U1 13
U2 70
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD MAR 28
PY 2022
VL 325
AR 126825
DI 10.1016/j.conbuildmat.2022.126825
EA FEB 2022
PG 8
GA ZN6WA
UT WOS:000765170700004
DA 2023-12-05
ER
PT J
AU Kolesnikov, AS
Serikbaev, BE
Zolkin, AL
Kenzhibaeva, GS
Isaev, GI
Botabaev, NE
Shapalov, SK
Kolesnikova, OG
Iztleuov, GM
Suigenbayeva, AZ
Kutzhanova, AN
Asylbekova, DD
Ashirbaev, KA
Alchinbaeva, OZ
Kolesnikova, VA
AF Kolesnikov, A. S.
Serikbaev, B. E.
Zolkin, A. L.
Kenzhibaeva, G. S.
Isaev, G. I.
Botabaev, N. E.
Shapalov, Sh. K.
Kolesnikova, O. G.
Iztleuov, G. M.
Suigenbayeva, A. Zh.
Kutzhanova, A. N.
Asylbekova, D. D.
Ashirbaev, Kh. A.
Alchinbaeva, O. Z.
Kolesnikova, V. A.
TI Processing of Non-Ferrous Metallurgy Waste Slag for its Complex Recovery
as a Secondary Mineral Raw Material
SO REFRACTORIES AND INDUSTRIAL CERAMICS
LA English
DT Article
DE industrial waste; Waelz process slag dumps; iron-containing additive;
Portland cement clinker
AB The article presents an overview of the methods of processing slag from Waelz
process, and various approaches employed by scientists globally, aimed at
processing such slags. Despite several listed methods of processing slag from Waelz
process, none entails a sufficient complex nature of its processing. In addition,
the slag processed from the Waelz process, found in the dumps, has not been used as
a secondary raw material to date. The elemental chemical composition of the slag
has been determined, represented by compounds of calcium, silicon, iron, aluminum,
carbon, and heavy non-ferrous metals, namely zinc and lead. Thus, it has been
established that these slags continue to pollute the environment for many years.
C1 [Kolesnikov, A. S.; Serikbaev, B. E.; Kenzhibaeva, G. S.; Botabaev, N. E.;
Shapalov, Sh. K.; Kolesnikova, O. G.; Iztleuov, G. M.; Suigenbayeva, A. Zh.;
Asylbekova, D. D.; Ashirbaev, Kh. A.; Kolesnikova, V. A.] MO Auezov South
Kazakhstan Univ, Shymkent, Kazakhstan.
[Zolkin, A. L.] Povolzhskiy State Univ Telecommun & Informat, Samara, Russia.
[Isaev, G. I.; Alchinbaeva, O. Z.] Khoja Ahmed Yasavi Int Kazakh Turkish Univ,
Turkestan, Kazakhstan.
[Kutzhanova, A. N.] Almaty Technol Univ, Alma Ata, Kazakhstan.
C3 Povolzhskiy State University of Telecommunications & Informatics; Akhmet
Yassawi International Kazakh-Turkish University
RP Kolesnikov, AS (corresponding author), MO Auezov South Kazakhstan Univ,
Shymkent, Kazakhstan.
EM kas164@yandex.kz
RI Kolesnikov, Alexandr S/O-3154-2017; Kolesnikova, Olga G/JMB-5733-2023
OI Kolesnikov, Alexandr S/0000-0002-8060-6234; Kolesnikova, Olga
G/0000-0001-6871-8367; Kutzhanova, Askan/0000-0003-3931-2792; Zolkin,
Alexander/0000-0001-5806-9906; Kenzhibayeva, Gulmira/0000-0001-6494-835X
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NR 59
TC 17
Z9 17
U1 1
U2 14
PU SPRINGER
PI NEW YORK
SN 1083-4877
EI 1573-9139
J9 REFRACT IND CERAM+
JI Refract. Ind. Ceram.
PD NOV
PY 2021
VL 62
IS 4
BP 375
EP 380
DI 10.1007/s11148-021-00611-7
EA DEC 2021
PG 6
GA XO5DP
UT WOS:000728464100006
DA 2023-12-05
ER
PT J
AU Luo, ZT
Hao, YH
Mu, YD
Tang, CB
Liu, XH
AF Luo, Zhongtao
Hao, Yuhua
Mu, Yuandong
Tang, Changbo
Liu, Xiaohai
TI Solidification/stabilization of red mud with natural radionuclides in
granular blast furnace slag based geopolymers
LA English
DT Article
DE Red mud; GBFS; Geopolymers; Radioactivity; Activity concentration index
ID FLY-ASH; RADIOLOGICAL CHARACTERIZATION; BUILDING-MATERIALS;
PORTLAND-CEMENT; RADIOACTIVITY; CONCRETE; IMMOBILIZATION; CONSTRUCTION;
COMPOSITES; RESIDUE
AB Red mud is a NORM residue of aluminum industry, and its large storage endangers
environmental safety. In this study, red mud was used to prepare geopolymers to
dilute its radioactivity. The activity concentrations of 226Ra, 232Th and 40K of
geopolymers with different contents of red mud (0, 30, 50, 70 wt%) were
investigated, and the activity concentration index, annual effective dose and
shielding rate were calculated to evaluate the radiological safety and
solidification effect of geopolymers. The solidification/stabilization mechanism of
geopolymers was discussed by using X-ray diffraction (XRD), scanning electron
microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR). The results
showed that the hydration process of geopolymers had a solidification effect on the
radionuclides contained in red mud. When the red mud content was 30 wt%, the
radioactivity was within the safety threshold as a building material, and the
compressive strength of the geopolymers reached 72.19 MPa. The maximum red mud
content in geopolymers was 40.81 wt% by fitting. The adsorption effect and the
encapsulation effect of C-S-H gel could promote the solidification/stabilization of
radionuclides of red mud in geopolymers. This research provides a perspective for
the radiological safety of the red mud based geopolymers in construction materials.
C1 [Luo, Zhongtao; Hao, Yuhua; Mu, Yuandong; Tang, Changbo; Liu, Xiaohai] Zhengzhou
Univ, Sch Mat Sci & Engn, Zhengzhou 450001, Peoples R China.
C3 Zhengzhou University
RP Liu, XH (corresponding author), Zhengzhou Univ, Sch Mat Sci & Engn, Zhengzhou
EM liuxiaohai@zzu.edu.cn
OI Liu, Xiaohai/0000-0002-8357-109X
China (No.52074245).
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NR 42
TC 17
Z9 17
U1 8
U2 26
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JAN 17
PY 2022
VL 316
AR 125916
DI 10.1016/j.conbuildmat.2021.125916
EA DEC 2021
PG 9
GA XY4TQ
UT WOS:000736967300004
DA 2023-12-05
ER
PT J
AU Hu, SH
Ni, YG
Yin, Q
Wang, JK
Lv, LQ
Cen, KF
Zhou, H
AF Hu, Shihao
Ni, Yuguo
Yin, Qi
Wang, Jiankang
Lv, Laiquan
Cen, Kefa
Zhou, Hao
TI Research on element migration and ash deposition characteristics of
high-alkali coal in horizontal liquid slagging cyclone furnace
SO FUEL
LA English
DT Article
DE High-alkali coal; Liquid slagging cyclone furnace; Element migration;
Deposition characteristics; Crystal structure
ID GASIFICATION PERFORMANCE; SODIUM TRANSFORMATION; TEMPERATURE
AB Hongshaquan coal (HSQ), a kind of high-alkali and rich-iron coal, is burned in a
20 MW liquid slagging cyclone furnace. The migration and transformation
characteristics of elements are examined. The deposition probe and oil cooling
circulation system are used to investigate the ash deposition characteristics of
HSQ. In addition, the microscopic morphology, crystal structure and chemical
composition of the slag are studied to explain the effect of element migration on
ash deposition and slag. The results show that the growth process of deposition on
probe 1 can be divided into four stages. The final stable relative heat flux of
probe 1 and probe 2 is 0.585 and 0.85, respectively. The average concentration of
Na2O in ash is 4.53%. Na, K, Ca, Mg and S are enriched in the low temperature area
of the boiler to form sulfate which leads to the agglomeration of ash particles.
The main mineral phases of the slag are silicates and iron-containing compounds.
The average concentration of Fe2O3 in the slag sample is 36.73%. Iron will be
enriched in the slag and form a low-temperature eutectic with the silicon-calcium-
magnesium-aluminum system to reduce the melting point of the ash. The granulated
slag has a lower degree of crystallinity and is closer to the characteristics of
glassy slag, which is due to the low content of Na2O, CaO and high silicon-to-
aluminum ratio in the ash.
C1 [Hu, Shihao; Ni, Yuguo; Yin, Qi; Wang, Jiankang; Lv, Laiquan; Cen, Kefa; Zhou,
Hao] Zhejiang Univ, Inst Thermal Power Engn, State Key Lab Clean Energy Utilizat,
Hangzhou 310027, Peoples R China.
RP Zhou, H (corresponding author), Zhejiang Univ, Inst Thermal Power Engn, State
Key Lab Clean Energy Utilizat, Hangzhou 310027, Peoples R China.
EM zhouhao@zju.edu.cn
FX This work was supported by National Natural Science Foundation of China
(52036008).
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NR 21
TC 17
Z9 20
U1 3
U2 38
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD JAN 15
PY 2022
VL 308
AR 121962
DI 10.1016/j.fuel.2021.121962
EA SEP 2021
PG 10
GA WK2GG
UT WOS:000709548700008
DA 2023-12-05
ER
PT J
AU Coetsee, T
De Bruin, FJ
AF Coetsee, Theresa
De Bruin, Frederik Johannes
TI Improved Titanium Transfer in Submerged Arc Welding of Carbon Steel
through Aluminum Addition
LA English
DT Article
DE Pyrometallurgy; melting; titanium; control; welding
ID SLAG-METAL REACTIONS; OXYGEN CONTAMINATION; MICROSTRUCTURE; TOUGHNESS;
CHEMISTRY; FLUXES
AB In Submerged Arc Welding of carbon steel, element transfer of Titanium from the
molten flux to the weld metal is limited to small quantities as reported in
literature, 310 ppm maximum. This limitation is due to the high oxygen potential
prevailing at the molten flux-weld pool interface. The results presented here
illustrate the use of Al powder in combination with Ti powder to improve Ti
transfer into the weld metal to 4% Ti, and still maintain high oxygen content in
the weld metal at 509 ppm to form inclusions. This is important in SAW because, in
addition to higher Ti in the weld pool, high ppm O is required in the weld pool to
form Ti-oxide inclusions in the weld metal to induce acicular ferrite (AF)
formation. Oxide inclusions in the weld metal form possible nucleation sites for
acicular ferrite formation to improve weld metal strength and toughness. The
results confirm that the oxygen potential at the flux-weld pool interface may be
lowered by Al powder addition to increase Ti powder transfer into the weld pool,
without interfering with oxygen transfer from the plasma arc to the weld pool.
Results from welding tests made in the absence of Al and Ti metal powder are used
as a base case comparison to explain the process reactions in Submerged Arc Welding
in the presence of Ti and Al metal powder.
C1 [Coetsee, Theresa; De Bruin, Frederik Johannes] Univ Pretoria, Dept Met Engn &
Mat Sci, Pretoria, South Africa.
RP Coetsee, T (corresponding author), Univ Pretoria, Private Bag X20, ZA-0028
Pretoria, South Africa.
EM theresa.coetsee@up.ac.za
RI Coetsee, Theresa/AAD-2204-2020; De Bruin, Frederik
Johannes/IZE-6573-2023
OI Coetsee, Theresa/0000-0003-2028-5755; De Bruin, Frederik
Johannes/0000-0001-7102-7508
FU National Research Foundation of South Africa [BRICS171211293679]
FX This work is funded in part by the National Research Foundation of South
Africa [BRICS171211293679. Research innovation originator is Frederik de
Bruin.
CR [Anonymous], 2021, ESAB TECHNICAL HDB S
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NR 25
TC 17
Z9 17
U1 0
U2 6
PI PHILADELPHIA
SN 0882-7508
EI 1547-7401
PD AUG 18
PY 2022
VL 43
IS 6
BP 771
EP 774
DI 10.1080/08827508.2021.1945595
EA JUN 2021
PG 4
GA 1H8FO
UT WOS:000667552600001
DA 2023-12-05
ER
PT J
AU Khanna, R
Konyukhov, YV
Ikram-ul-haq, M
Burmistrov, I
Cayumil, R
Belov, VA
Rogachev, SO
Leybo, DV
Mukherjee, PS
AF Khanna, R.
Konyukhov, Y., V
Ikram-ul-haq, M.
Burmistrov, I
Cayumil, R.
Belov, V. A.
Rogachev, S. O.
Leybo, D., V
Mukherjee, P. S.
TI An innovative route for valorising iron and aluminium oxide rich
industrial wastes: Recovery of multiple metals
LA English
DT Article
DE Sustainability; Waste oxides; Ferroalloys; Valorisation; Material
recovery; Biomass
ID RED MUD; BAUXITE RESIDUE; ASH; RESOURCE; BIOMASS; COPPER; PLANT; SLAG
AB Several industrial wastes including biomass, fly ashes, red mud, mill scales,
water treatment residues, have significant concentrations of metal oxides: Fe2O3,
Al2O3, TiO2, SiO2 etc. Several efforts have been made towards recovering metals
within these wastes. Rather than recovering one metal at a time, we report a novel
approach for simultaneously extracting multiple metals from mixed oxides in a
single process step. Using three distinct furnaces/heating regimes, the
carbothermic reduction of Fe2O3/Al2O3/SiO2 system was investigated at 1450-1700
degrees C for up to 2 h over a wide composition range. Complete reduction was
achieved for both Fe2O3 and SiO2 in all cases leading to the formation of Fe and
Fe-Si alloys. The reduction of alumina at moderate temperatures was the key
challenge. No alumina reduction was observed during reductions at 1450 degrees C. A
partial reduction of alumina and the formation of Fe-Al alloys was detected in the
Al2O3/Fe2O3/C system at 1550 degrees C. The formation of Fe-Si-Al alloys was also
observed in the Fe2O3/SiO2/Al2O3/C system at 1550 degrees C. Complete reduction of
alumina was observed at 1600-1700 degrees C, even for up to 50 wt% alumina in the
system. Optimal operating conditions and reference standards were established for
the simultaneous recovery of multiple metals from waste oxides. While conserving
natural resources, this novel route will lower the burden on waste storage
facilities with significant contributions to the economic and environmental
sustainability of industrial waste management.
C1 [Khanna, R.; Ikram-ul-haq, M.] Univ New South Wales, Sch Mat Sci & Engn, Sydney,
NSW 2052, Australia.
[Konyukhov, Y., V] Natl Univ Sci & Technol MISiS, Dept Funct Nanosyst & High
Temp Mat, Moscow 119049, Russia.
[Burmistrov, I] Plekhanov Russian Univ Econ, Engn Ctr, Moscow 117997, Russia.
[Cayumil, R.] Univ Andres Bello, Fac Ingn, Antonio Varas 880, Santiago, Chile.
[Belov, V. A.; Rogachev, S. O.] Natl Univ Sci & Technol MISiS, Dept Phys Met &
Phys Strength, Moscow 119049, Russia.
[Leybo, D., V] Natl Univ Sci & Technol MISiS, Lab Inorgan Nanomat, Moscow
119049, Russia.
[Mukherjee, P. S.] CSIR, Inst Minerals & Mat Technol, Bhubaneswar 751013,
Orissa, India.
C3 University of New South Wales Sydney; National University of Science &
Technology (MISIS); Plekhanov Russian University of Economics;
Universidad Andres Bello; National University of Science & Technology
(MISIS); National University of Science & Technology (MISIS); Council of
Scientific & Industrial Research (CSIR) - India; CSIR - Institute of
Minerals & Materials Technology (IMMT)
RP Khanna, R (corresponding author), Univ New South Wales, Sch Mat Sci & Engn,
Sydney, NSW 2052, Australia.
EM rita.khanna66@gmail.com
RI Rogachev, Stanislav/A-2207-2014; Burmistrov, Igor
Nikolaevich/A-8212-2014
OI Burmistrov, Igor Nikolaevich/0000-0003-0776-2465; Rogachev,
Stanislav/0000-0001-7769-7748; Cayumil, Romina/0000-0002-1675-1015
FU Department of Science and Technology (DST) India under the
Australia-India Strategic Research Fund Round 6
FX Authors gratefully acknowledge Department of Science and Technology
(DST) India for providing financial support for this project under the
Australia-India Strategic Research Fund Round 6.
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NR 51
TC 17
Z9 17
U1 2
U2 19
PI LONDON
SN 0301-4797
EI 1095-8630
J9 J ENVIRON MANAGE
PD OCT 1
PY 2021
VL 295
AR 113035
DI 10.1016/j.jenvman.2021.113035
EA JUN 2021
PG 11
GA TT0DV
UT WOS:000680023300003
PM 34167061
DA 2023-12-05
ER
PT J
AU Wu, J
Zheng, XY
Yang, AW
Li, YB
AF Wu Jun
Zheng Xi-yao
Yang Ai-wu
Li Yan-bo
TI Experimental study on the compressive strength of muddy clay solidified
by the one-part slag-fly ash based geopolymer
SO ROCK AND SOIL MECHANICS
LA Chinese
DT Article
DE geopolymer; slag; fly ash; unconfined compressive strength;
micro-analysis
ID CEMENT; BEHAVIOR
AB To solve the issues of insufficient early strength of cement solidified muddy
clay and high pollution,high energy consumption and high-costinduced by the
application of cement binder,theone-part slag-fly ash(SL-FA) based geopolymer was
adopted as the binder torsolidify the muddyclay. The effects of theratio of
slagtofly ashinsilicon-aluminum (Si-Al)rawmaterials, theratio of solid activator
toSi-Alraw material and the ratio of water to binder on the mechanical properties
of geopolymer solidified muddy clay were studied through the unconfined compression
test. The micro-analysis (i.e., scanning electron microscope and energy dispersive
spectrometer) was also conducted to investigate the development of the
microstructure of the muddy clay solidified by the one-part SL-FA based geopolymer.
The experimental results showed that when the Si-Al raw material was composed of
90% slag and 10% fly ash by mass, the mass ratio of alkali activator to Si-Al raw
material was 0.15, and the mass ratio of water to binder was 0.7, the 14-day
compressive strength of the geopolymer solidified muddy clay could reach 1.5 MPa.
It was also found that the main hydration products of the slag-fly ash based
geopolymer were amorphous hydrated calcium silicate hydrates and hydrated calcium
aluminate hydrates, which is the main reason for the improvement of the compressive
strength of solidified clay. The micro-structure of geopolymer solidified muddy
clay was connected by hydrated calcium silicate hydrates and calcium aluminate
hydrates. The results provide a certain theoretical basis for the practical
application of one-part slag-fly ash based geopolymer as the soil binder in the
improvement of muddy clay.
C1 [Wu Jun; Zheng Xi-yao] Shanghai Univ Engn Sci, Coll Urban Railway Transportat,
[Yang Ai-wu] Donghua Univ, Coll Environm Sci & Engn, Shanghai 201620, Peoples R
China.
[Li Yan-bo] Yancheng Inst Technol, Sch Mat Sci & Engn, Yancheng 221051, Jiangsu,
Peoples R China.
C3 Shanghai University of Engineering Science; Donghua University; Yancheng
Institute of Technology
RP Wu, J (corresponding author), Shanghai Univ Engn Sci, Coll Urban Railway
Transportat, Shanghai 201620, Peoples R China.
EM cvewujun@163.com; wayyjk@dhu.edu.cn
RI Wu, Jun/CAG-4971-2022
China(51978440, 52078288).
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NR 21
TC 17
Z9 23
U1 10
U2 32
PU SCIENCE PRESS
PI BEIJING
SN 1000-7598
J9 ROCK SOIL MECH
JI Rock Soil Mech.
PD MAR 11
PY 2021
VL 42
IS 3
BP 647
EP 655
DI 10.16285/j.rsm.2020.0918
PG 9
WC Engineering, Geological
SC Engineering
GA SW9SV
UT WOS:000664854500007
DA 2023-12-05
ER
PT J
AU Wattez, T
Patapy, C
Frouin, L
Waligora, J
Cyr, M
AF Wattez, Thomas
Patapy, Cedric
Frouin, Laurent
Waligora, Julien
Cyr, Martin
TI Interactions between alkali-activated ground granulated blastfurnace
slag and organic matter in soil stabilization/solidification
SO TRANSPORTATION GEOTECHNICS
LA English
DT Article
DE Stabilization/solidification; Boring mud; Alkali-activated slag; Organic
matter; Folin-Lowry method
ID FLY-ASH GEOPOLYMER; HUMIC-ACID; MECHANICAL-PROPERTIES; SULFATE ATTACK;
PORE SOLUTION; STABILIZATION; CALCIUM; CEMENT; SUBSTANCES; EXTRACTION
AB This paper presents novel findings regarding the use of alkali-activated slag
for the development of road applications and, more particularly, how the
interactions that occur between the binder and the organic matter originally
present in the soil can strongly affect its reactivity in the process of
stabilization and solidification. The study uses mechanical performances and
macroscopic characterization, such as isothermal calorimetry and thermogravimetric
analysis of the pure binders as well as of the soil-binder mixes in order to
characterize the hydration mechanisms. By analyzing the chemical composition of
organic matter extracted with three different alkaline activators, it is shown that
both humic and fulvic acids are strong complexing agents, not only of calcium and
aluminum ions, as noted in the existing scientific literature, but also of highly
soluble silicon. In this study, only sodium hydroxide activated slag was found to
be a suitable alkali-activated binder for subbase layer development.
C1 [Wattez, Thomas; Patapy, Cedric; Cyr, Martin] Univ Toulouse, UPS, INSA,
LMDC,Genie Civil, 135 Ave Rangueil, F-31077 Toulouse 04, France.
[Frouin, Laurent] ECOCEM Mat, 4 Pl Louis Armand, F-75012 Paris, France.
[Waligora, Julien] EIFFAGE Infrastruct, 8 Rue Dauphine, F-69960 Corbas, France.
C3 Universite de Toulouse; Universite Toulouse III - Paul Sabatier
RP Wattez, T (corresponding author), Univ Toulouse, UPS, INSA, LMDC,Genie Civil,
135 Ave Rangueil, F-31077 Toulouse 04, France.
EM twattez@ecocem.ie
RI CYR, Martin/A-8953-2013
OI CYR, Martin/0000-0002-5012-9131
FU Eiffage Infrastructures; Ecocem Materials
FX The authors would like to acknowledge Eiffage Infrastructures and Ecocem
Materials for their financial support in the carrying out of this work.
They would also like to acknowledge Maud Schiettekatte, Mansour Bounouba
and Stephane Le Blond du Plouy, research engineers at the Laboratoire
Materiaux et Durabilite des Constructions (LMDC, UPS - INSA Toulouse),
the Laboratoire de l'Ingenierie des Systemes Biologiques et Procedes
(LISBP, INSA Toulouse) and the Centre de Microcaracterisation Raimond
Castaing (UMS 3623, CNRS), respectively, for their help with the
stabilized soils pore solution analysis, the Folin-Lowry method for
humic acid concentration measurements and the SEM images and
compositions of the soil and precipitated organic matter.
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TC 17
Z9 18
U1 7
U2 38
PU ELSEVIER
PI AMSTERDAM
SN 2214-3912
J9 TRANSP GEOTECH
JI Transp. Geotech.
PD JAN
PY 2021
VL 26
AR 100412
DI 10.1016/j.trgeo.2020.100412
EA JAN 2021
PG 17
WC Engineering, Civil; Engineering, Geological
SC Engineering
GA PT2FZ
UT WOS:000608435900002
DA 2023-12-05
ER
PT J
AU Choi, JS
Park, TJ
Min, DJ
AF Choi, Joon Sung
Park, Tae Jun
Min, Dong Joon
TI Structure-property relationship amphoteric oxide systems via phase
stability and ionic structural analysis
LA English
DT Article
DE activation energy; aluminosilicates; Raman spectroscopy; silicates;
slags
ID IRON REDOX EQUILIBRIA; SILICATE-BASED SLAGS; SULFIDE CAPACITY;
LOCAL-STRUCTURE; VISCOSITY; RAMAN; GLASSES; MELTS; ALUMINUM; CAO-SIO2
AB The effects of basicity and amphoteric oxides (Al(2)O(3)and FetO) on the
structure-property relationships of CaO-SiO2-(Al(2)O(3)and FetO) and CaO-SiO2-
Al2O3-FetO slags were investigated to determine the constitutional effects on the
structure of high-temperature ionic melts. The proportion of Q(n)species, which is
determined by Raman spectroscopy, and the viscosity measured by the rotating
cylinder method are both correlated and shown together with the slag structure
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relationship with basicity (CaO/SiO2), including an inflection point at CaO/SiO2 =
1.0 resulting from the stability and Q(n)-dominant unit of the melt, which changes
close to the wollastonite (CaSiO3) congruent point. This inflection point changes
with the increasing amphoteric oxide content (Al(2)O(3)and FetO) because of the
change in the dominant polymeric unit (Si4+-O-Si4+-> M4+-O-Si4+; M: Al and Fe), in
accordance with the equilibrated primary phases. As the Al(2)O(3)content increased,
the viscosity and activation energy of slags both drastically increased owing to
the change in the flow unit (Si-O-Si, Al-O-Si, and Al-O-Al). In contrast, as FetO
increased, the viscosity and activation energy (E-eta) of slags decreased because
of the change in the flow unit (Si-O-Si, Fe-O-Si, and Fe-O-Fe). Ultimately, the
flow unit (T-O-T; T = Si, Al, and Fe) and activation energy of the slags were found
to be closely related to the solid primary phase on the phase diagram, and the
physical-property-structure relationship was determined from the phase stability.
C1 [Choi, Joon Sung; Min, Dong Joon] Yonsei Univ, Dept Mat Sci & Engn, Seoul 03722,
South Korea.
[Park, Tae Jun] R&D Ctr Hyundai Steel Co, Ironmaking Res Team, Dangjin Si, South
Korea.
RP Min, DJ (corresponding author), Yonsei Univ, Dept Mat Sci & Engn, Seoul 03722,
South Korea.
EM chemical@yonsei.ac.kr
OI Choi, Joon Sung/0000-0002-8560-1598; Park, Tae Jun/0000-0002-5830-1039;
Min, Dong Joon/0000-0003-3091-2038
FU Korea Research Foundation [NRF-2017R1D1A1A02018514]
FX Korea Research Foundation, Grant/Award Number: NRF-2017R1D1A1A02018514
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NR 60
TC 17
Z9 17
U1 2
U2 28
PU WILEY
PI HOBOKEN
SN 0002-7820
EI 1551-2916
J9 J AM CERAM SOC
PD JAN
PY 2021
VL 104
IS 1
BP 140
EP 156
DI 10.1111/jace.17432
EA SEP 2020
PG 17
GA OT4PI
UT WOS:000567974400001
DA 2023-12-05
ER
PT J
AU Deng, G
He, YJ
Lu, LN
Hu, SG
AF Deng, Gao
He, Yongjia
Lu, Linnu
Hu, Shuguang
TI Evolution of aluminate hydrate phases in fly ash-cement system under the
sulfate conditions
LA English
DT Article
DE Fly ash; Pozzolanic reaction; Sulfate attack; Aluminate hydrates;
Ettringite
ID C-S-H; BLAST-FURNACE SLAG; MAS NMR; PORTLAND CEMENTS; CHEMICAL
ACTIVATORS; POZZOLANIC REACTION; NANOMETER CHANNEL; PART I; ATTACK;
CONCRETE
AB The aluminate hydrate phases play an important role in the sulfate attack of
concrete. In this paper, the aluminum hydrate phases evolution of fly ash blended
cement paste powders immersed in different sodium sulfate solution is studied. In
order to accelerate the reaction, the fly ash blended cement paste powders are
immersed in different sulfate solution at ambient temperature up to 28 d. The
results show that the hydration of fly ash and the distribution of aluminum
hydrates phases in the hydration products of fly ash-cement blends are
significantly influenced by the sulfate. The addition of fly ash into the cements
introduces the reactive Al3+ into the systems, leading to an increase of Al(IV)/Si
and mean chain length of C-A-S-H. Furthermore, although the pozzolanic reaction of
fly ash consumes the calcium hydroxide, where the calcium hydroxide is required for
the formation of ettringite, the addition of fly ash is favorable for the formation
of ettringite. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Deng, Gao; He, Yongjia; Hu, Shuguang] Wuhan Univ Technol, State Key Lab
Silicate Mat Architectures, Luoshi Rd 122, Wuhan 430070, Peoples R China.
[Deng, Gao; He, Yongjia; Hu, Shuguang] Wuhan Univ Technol, Sch Mat Sci & Engn,
Wuhan 430070, Peoples R China.
[Lu, Linnu] Wuhan Univ Technol, Sch Sci, Hubei Key Lab Theory & Applicat Adv Mat
Mech, Luoshi Rd 122, Wuhan 430070, Peoples R China.
RP He, YJ (corresponding author), Wuhan Univ Technol, State Key Lab Silicate Mat
Architectures, Luoshi Rd 122, Wuhan 430070, Peoples R China.; Lu, LN (corresponding
author), Wuhan Univ Technol, Sch Sci, Hubei Key Lab Theory & Applicat Adv Mat Mech,
Luoshi Rd 122, Wuhan 430070, Peoples R China.
EM hyj@whut.edu.cn; lln@whut.edu.cn
RI He, Yongjia/AAC-6475-2021
OI Deng, Gao/0000-0002-6977-0658
FU National Key R&D Program of China [2017 YFB0310001]; National Natural
Science Foundation of China [51772226, 51972249]; Hubei Technology
Innovation Key Program [2018AAA004]
FX The work presented in this paper was supported by the National Key R&D
Program of China (No. 2017 YFB0310001), the National Natural Science
Foundation of China (No. 51772226, No. 51972249) and the Hubei
Technology Innovation Key Program (2018AAA004).
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NR 43
TC 17
Z9 17
U1 6
U2 33
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD AUG 20
PY 2020
VL 252
AR 119045
DI 10.1016/j.conbuildmat.2020.119045
PG 11
GA LV9XS
UT WOS:000538801700026
DA 2023-12-05
ER
PT J
AU Huan, SX
Wang, YW
Peng, JP
Di, YZ
Li, B
Zhang, LD
AF Huan, Shuxing
Wang, Yaowu
Peng, Jianping
Di, Yuezhong
Li, Bo
Zhang, Lida
TI Recovery of aluminum from waste aluminum alloy by low-temperature molten
salt electrolysis
LA English
DT Article
DE Aluminum recovery; Current efficiency; Low-temperature electrolysis;
Electrowinning of aluminum; Cyclic voltammetry curve
ID FLY-ASH; ELECTRODEPOSITION; AL; SOLVENT
AB Large amounts of industrial waste discharge have serious implications for the
environment. The production of coarse Al-Si alloy by carbothermal reduction is
considered to be one potential method for making use of industrial aluminiferous
waste slag. Here, we discuss the influence of different processing parameters on
electrolytic refining of aluminum alloy and investigate the mechanism of extracting
Al from coarse Al-Si alloy in a low-temperature molten salt system. Aluminum is
obtained with the use of coarse Al-Si alloy as a soluble anode in the AlCl3-NaCl-
KCl molten salt system. The current efficiency reached over 94% when the
electrolysis temperature was 170 degrees C, the current density was 30 mA/cm(2) and
electrolysis was performed for 1.5 h. In the electrolysis process, Al in the coarse
Al-Si alloy was present in the form of Al2Cl7- and AlCl4-, which precipitated at
the cathode. The purity of aluminum electrodeposited on the aluminum cathode was
99.3%.
C1 [Huan, Shuxing; Wang, Yaowu; Peng, Jianping; Di, Yuezhong; Li, Bo; Zhang, Lida]
Northeastern Univ, Sch Met, Shenyang 110819, Peoples R China.
RP Wang, YW (corresponding author), Northeastern Univ, Sch Met, Shenyang 110819,
Peoples R China.
EM wangyw@smm.neu.edu.cn
RI PENG, Jian-ping/AAG-2146-2021
OI Peng, Jianping/0000-0003-0720-2257
FU National Key R&D Program of China [2018YFC1901905]; Fundamental Research
Funds for the Central Universities [N162502002]; National Science
FX The authors would like to thank the National Key R&D Program of China
(2018YFC1901905), the Fundamental Research Funds for the Central
Universities (N162502002), and National Science Foundation of China
(51774080) for the financial support.
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Z9 20
U1 16
U2 72
PI OXFORD
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD AUG 1
PY 2020
VL 154
AR 106386
DI 10.1016/j.mineng.2020.106386
PG 7
GA LT2UC
UT WOS:000536926200004
DA 2023-12-05
ER
PT J
AU Wang, Z
Wen, GH
Liu, Q
Huang, SH
Tang, P
Yu, L
AF Wang, Zhe
Wen, Guanghua
Liu, Qiang
Huang, Shuheng
Tang, Ping
Yu, Liang
TI Estimating the thermal conductivity of CaO-Al2O3
-SiO2 slags by equilibrium molecular dynamics simulations
LA English
DT Article
DE Thermal conductivity; Molecular dynamics; Structural property;
CaO-Al2O3-SiO2 slags
ID NATURAL SILICATE MELTS; COMPUTER-SIMULATION; FUSED-SILICA; PRESSURE;
LIQUIDS; MOLD; SOLIDIFICATION; TEMPERATURE; CRYSTALS; ALUMINUM
AB The thermal conductivity of the molten CaO-Al2O3-SiO2 (CAS) system was
calculated by using equilibrium molecular dynamics (EMD) simulation. Most of the
thermal conductivities determined by the EMD simulation are in good agreement with
the values by the experimental method, of which the Pearson coefficient and mean
standard deviations are 0.57 and 0.228, respectively. After removing the
controversial samples, the Pearson coefficient and mean standard deviations were
improved to 0.85 and 0.08, respectively. Further structure analysis showed that the
thermal conductivity of the CAS melt depends on not only the percentage of the
bridge oxides but also the function of Ca2+, which prompted the increase of the
thermal conductivity of CAS slags. The combination of the Al2O3 and SiO2 structures
may increase the thermal conductivity of CAS melt. In summary, EMD simulation can
be widely applied to estimate the thermal conductivity of the silicate melt as well
as the mechanism research.
C1 [Wang, Zhe; Wen, Guanghua; Liu, Qiang; Tang, Ping; Yu, Liang] Chongqing Univ,
[Wang, Zhe; Wen, Guanghua; Liu, Qiang; Tang, Ping; Yu, Liang] Chongqing Univ,
Chongqing Key Lab Vanadium Titanium Met & New Mat, Chongqing 400044, Peoples R
China.
[Huang, Shuheng] Chongqing Univ, Coll Bioengn, Chongqing 400044, Peoples R
China.
C3 Chongqing University; Chongqing University; Chongqing University
RP Wang, Z; Wen, GH (corresponding author), Chongqing Univ, Coll Mat Sci & Engn,
EM zhewang@cqu.edu.cn; wengh@cqu.edu.cn
RI Wang, Zhe/AAO-9330-2020
OI Wen, Guanghua/0000-0002-5485-906X; Wang, Zhe/0000-0003-0217-2909
FU Graduate Scientific Research and Innovation Foundation of Chongqing,
China [CYB19002]; National Natural Science Foundation of China
[51574050]
FX This work was supported by the Graduate Scientific Research and
Innovation Foundation of Chongqing, China [grant number CYB19002], and
the National Natural Science Foundation of China [grant number
51574050].
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NR 52
TC 17
Z9 17
U1 8
U2 38
PU ELSEVIER
PI AMSTERDAM
SN 0022-3093
EI 1873-4812
PD MAR 1
PY 2020
VL 531
AR 119851
DI 10.1016/j.jnoncrysol.2019.119851
PG 8
GA LE9BN
UT WOS:000527022700008
DA 2023-12-05
ER
PT J
AU Li, B
Li, N
Brouwer, HJH
Yu, QL
Chen, W
AF Li, Bo
Li, Neng
Brouwer, H. J. H.
Yu, Qingliang
Chen, Wei
TI Understanding hydrogen bonding in calcium silicate hydrate combining
solid-state NMR and first principle calculations
LA English
DT Article
DE Calcium silicate hydrate; Solid state NMR; Hydrogen bonding; First
principle calculation
ID C-S-H; CEMENT; ALUMINUM; MODEL; SLAG
AB Mechanisms of hydrogen bonding and molecular structure in the C-S-H are
investigated by combining results of Si-29, H-1 solid SSNMR analysis and first
principle calculations. First principle calculations for H-1 chemical shifts are
used to correlate the observed H-1 SSNMR spectra with the underlying structure of
various hydrogen bonds between different silicon moieties and hydrogen groups in
the C-S-H gels. The results show that strong hydrogen bonds are formed between
water and terminal silicate sites or silanols, between adjacent terminal silanols
and terminal silicate sites, between water or terminal silanols and hydroxyl groups
bonded with interlayer calcium ions. Strong hydrogen bonds are favored to form in
C-S-H with high Ca/Si molar ratios. The hydrogen bonding in terminal silicate sites
is stronger than those in the paring or bridging silicate sites. New insights into
the changes of basal spacing, Ca/Si ratio and H2O/Si ratio of in the molecular
structure of C-S-H are presented based on the mechanism of hydrogen bonding. (C)
C1 [Li, Bo; Li, Neng; Chen, Wei] Wuhan Univ Technol, State Key Lab Silicate Mat
Architectures, Wuhan, Peoples R China.
[Li, Bo] Wuhan Univ Technol, Sch Mat Sci & Engn, Wuhan, Peoples R China.
[Li, Neng] Wuhan Univ Technol, Res Ctr Mat Genome Engn, Wuhan, Peoples R China.
[Brouwer, H. J. H.; Yu, Qingliang] Eindhoven Univ Technol, Dept Built Environm,
Eindhoven, Netherlands.
University of Technology; Eindhoven University of Technology
RP Chen, W (corresponding author), Wuhan Univ Technol, State Key Lab Silicate Mat
Architectures, Wuhan, Peoples R China.
EM chen.wei@whut.edu.cn
RI Chen, Wei/HIR-5463-2022; Yu, Qingliang/J-4079-2019; Li, Neng/S-1296-2017
OI Chen, Wei/0000-0003-1802-1304; Yu, Qingliang/0000-0001-8578-3945;
Brouwers, Jos/0000-0002-8291-5444; Li, Neng/0000-0001-9633-6702
Fundamental Research Funds for the Central Universities [WUT:
2017-YB-008]; National Key Research and Development Program of China
[2016YFB0303501, BY115J004]
FX This research has been financially supported by the National Natural
Science Foundation of China (project 51672199 and 51972248), the
Fundamental Research Funds for the Central Universities (WUT:
2017-YB-008), National Key Research and Development Program of China
(Project 2016YFB0303501), research project BY115J004. We thank Dr.
Xiaoyun Li from State Key Laboratory of Silicate Materials for
Architectures, Chaofeng He and Yunyun Zou from Shiyanjia lab
(www.shiyanjia.com) for assistance with the SSNMR tests.
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NR 31
TC 17
Z9 18
U1 7
U2 52
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD FEB 10
PY 2020
VL 233
AR 117347
DI 10.1016/j.conbuildmat.2019.117347
PG 10
GA KL2YS
UT WOS:000513295100054
OA Green Published
DA 2023-12-05
ER
PT J
AU Abd-El-Raoof, F
Tawfik, A
Komarneni, S
Ahmed, SE
AF Abd-El-Raoof, F.
Tawfik, A.
Komarneni, S.
Ahmed, S. E.
TI Hydrotalcite and hydrocalumite as resources from waste materials of
concrete aggregate and Al-dross by microwave-hydrothermal process
LA English
DT Article
DE Dolomitic waste; Al-dross waste treatment; Layer double hydroxides;
Microwave-hydrothermal process
ID LAYERED DOUBLE HYDROXIDES; ALKALI-ACTIVATED SLAG; CHLORIDE BINDING;
HAZARDOUS-WASTE; CRYSTAL-GROWTH; GEL; CORROSION; HYDRATION; AL2O3; ANION
AB Hydrotalcite (HT) and hydrocalumite (HC) were synthesized from active MgO, CaO
and Al2O3 in the presence of K2CO3 using microwave-hydrothermal (M-H) process at
100 degrees C/1 h. The above active oxides were prepared via HCl leaching of
dolomite (fine waste of concrete aggregate) and Al-dross waste, precipitated as
hydroxides and then activated by calcination. The prepared materials were
characterized via XRD, FTIR and TEM.
Results showed that chemical recycling of Al-dross and dolomite wastes produced
aluminum, magnesium and calcium hydroxides from which their active oxides produced
at 600, 900 and 1000 degrees C, respectively. The M-H treatment of MgO/Al2O3 (4:1)
slurry of the active oxides for 1 h at 100 degrees C resulted in Mg2Al(OH)(7) in
amorphous plate-like shape while the CaO/Al2O3 (4:1) slurry under the same
conditions provided semi-crystalline multi-phases. These phases were identified
through X-ray diffraction (XRD) analysis as Katoite [Ca3Al2(OH)(12)] and calcium
aluminum hydroxides [Ca2Al(OH)(7)center dot 3H(2)O]. In the presence of K2CO3,
MgO/Al2O3 and CaO/Al2O3 slurries produced nano-sized crystalline hydrotalcite or
hydrocalumite as deduced from XRD, FTIR and TEM results. (C) 2019 Elsevier Ltd. All
rights reserved.
C1 [Abd-El-Raoof, F.; Tawfik, A.; Ahmed, S. E.] Natl Res Ctr, Refractories Ceram &
Bldg Mat Dept, Cairo 12311, Egypt.
[Komarneni, S.] Penn State Univ, Mat Res Inst, Dept Ecosyst Sci & Management,
Energy & Environm Lab 204, University Pk, PA 16802 USA.
C3 Egyptian Knowledge Bank (EKB); National Research Centre (NRC);
Pennsylvania Commonwealth System of Higher Education (PCSHE);
University Park
RP Tawfik, A (corresponding author), Natl Res Ctr, Refractories Ceram & Bldg Mat
Dept, Cairo 12311, Egypt.
EM tawfik_omar76@yahoo.com; at.ahmed@nrc.sci.eg
RI Omar, Ahmed Tawfik Ahmed/ABG-1568-2021; Abd-EL-Raoof, Fawzia
Mohamed/N-6672-2018; Tawfik, Ahmed/ABC-9828-2021; Abd-EL-Raoof,
Fawzia/S-7947-2016
OI Omar, Ahmed Tawfik Ahmed/0000-0002-5830-6788; Tawfik,
Ahmed/0000-0002-1429-8202; Abd-EL-Raoof, Fawzia/0000-0002-4890-0425
FU United States Agency of International Developments (USAID)
FX The authors acknowledge the United States Agency of International
Developments (USAID) for funding a part of this research.
CR Abd-El-Raoof F., 2016, 1 INT C FUT EN GEOL
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NR 41
TC 17
Z9 18
U1 5
U2 58
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD MAY 20
PY 2019
VL 207
BP 10
EP 16
DI 10.1016/j.conbuildmat.2019.02.105
PG 7
GA HY6QA
UT WOS:000468253600002
OA hybrid
DA 2023-12-05
ER
PT J
AU Pérez-Villarejo, L
Bonet-Martínez, E
Eliche-Quesada, D
Sánchez-Soto, PJ
Rincón-López, JM
Castro-Galiano, E
AF Perez-Villarejo, L.
Bonet-Martinez, E.
Eliche-Quesada, D.
Sanchez-Soto, P. J.
Ma Rincon-Lopez, J.
Castro-Galiano, E.
TI Biomass fly ash and aluminium industry slags-based geopolymers
LA English
DT Article
DE Geopolymers; Alkali-activation; Biomass fly ash; Aluminium industry slag
ID MICROSTRUCTURE; SPECTROSCOPY; METAKAOLIN
AB Geopolymers are a new class of non-Portland cements produced using an alumino-
silicate material and an activating solution, which is mainly composed of sodium or
potassium and waterglass to be subsequently cured at relatively low temperatures.
Those can be formulated by adding natural minerals, waste and/or industrial by-
products. The study investigates the microstructural properties of geopolymers
synthesized from metakaolin (MK) and the admixture of fly ash (FBA) and aluminium
industry slags (AIS) at different ages of curing. Five different geopolymer
compositions were prepared and characterized by XRD, ATR-FTIR and SEM/EDS. The
study revealed that geopolymeric gels are identified, which show mainly glassy
microstructures, in agreement with the X-ray amorphous diffraction patterns, broad
FTIR features and confirmed by SEM/EDS, with promising results prior to an
industrial scale. (C) 2018 Elsevier B.V. All rights reserved.
C1 [Perez-Villarejo, L.; Bonet-Martinez, E.; Eliche-Quesada, D.; Castro-Galiano,
E.] Univ Jaen, Dept Chem Environm & Mat Engn, Campus Lagunillas S-N, Jaen 23071,
Spain.
[Sanchez-Soto, P. J.] Joint Ctr Spanish Natl Res Council CSIC Univ Sevi, Mat Sci
Inst Sevilla ICMS, C Amer Vespucio 49, Seville 41092, Spain.
[Ma Rincon-Lopez, J.] UMH, Dept Agrochem & Environm, Res Grp GLASSCErinCON T,
Alicante, Spain.
C3 Universidad de Jaen; Consejo Superior de Investigaciones Cientificas
(CSIC); Instituto de Ciencia de Materiales de Sevilla (ICMS-CSIC);
Universidad Miguel Hernandez de Elche
RP Pérez-Villarejo, L (corresponding author), Univ Jaen, Dept Chem Environm & Mat
Engn, Campus Lagunillas S-N, Jaen 23071, Spain.
EM lperezvi@ujaen.es
RI Pérez-Villarejo, Luis/AAL-9906-2020; Castro, Eulogio/E-5910-2011;
Pérez-VIllarejo, Luis/L-8368-2014; Eliche Quesad, Dolores/B-4155-2015;
Sanchez-Soto, Pedro J/I-3554-2014; Eliche-Quesada, Dolores/AAK-6602-2020
OI Pérez-Villarejo, Luis/0000-0002-6912-9844; Castro,
Eulogio/0000-0003-1719-6049; Pérez-VIllarejo, Luis/0000-0002-6912-9844;
Eliche Quesad, Dolores/0000-0003-3803-9595; Sanchez-Soto, Pedro
J/0000-0002-2901-2975; Bonet Martinez, Eduardo/0000-0003-2289-5661
FU Project "Valuation of various types of ash for the obtaining of new
sustainable ceramic materials", Own Plan University of Jaen - Caja Rural
of Jaen [UJA2014/06/13]
FX This work has been funded by the Project "Valuation of various types of
ash for the obtaining of new sustainable ceramic materials"
(UJA2014/06/13), Own Plan University of Jaen, sponsored by Caja Rural of
Jaen.
CR Benito P, 2013, APPL CLAY SCI, V73, P1, DOI 10.1016/j.clay.2013.03.008
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NR 11
TC 17
Z9 18
U1 1
U2 41
PI AMSTERDAM
SN 0167-577X
EI 1873-4979
J9 MATER LETT
JI Mater. Lett.
PD OCT 15
PY 2018
VL 229
BP 6
EP 12
DI 10.1016/j.matlet.2018.06.100
PG 7
GA GQ1NW
UT WOS:000441401500003
DA 2023-12-05
ER
PT J
AU Kim, MS
Kang, YB
AF Kim, Min-Su
Kang, Youn-Bae
TI Development of a multicomponent reaction rate model coupling
thermodynamics and kinetics for reaction between high Mn-high Al steel
and CaO-SiO2-type molten mold flux
SO CALPHAD-COMPUTER COUPLING OF PHASE DIAGRAMS AND THERMOCHEMISTRY
LA English
DT Article
DE Flux-steel reaction; High Mn-high Al steel; CaO-SiO2-type mold flux
ID TRACER DIFFUSIVITY; REACTION-MECHANISM; AL2O3/SIO2 RATIO; LIQUID-IRON;
SLAG-METAL; MELTS; ALUMINUM; OXYGEN; DESULFURIZATION; ACCUMULATION
AB A new multi-component reaction model was developed in order to describe complex
reaction phenomena between a high Mn-high Al steel and a CaO-SiO2-type molten mold
flux. This model is an extension of Robertson's multicomponent mixed-transport-
control theory (Robertson et al., 1984) [7], where rate controlling step is assumed
to be a mass transport of diffusing species in a boundary layer, while chemical
equilibrium is assumed at the reaction interface. This model also employs a CALPHAD
type multicomponent-multiphase thermodynamic calculations for chemical equilibria
at the interface. By explicitly taking into account 1) local equilibrium at the
liquid steel-liquid flux interface, 2) flux density equations for each diffusing
species in the steel and the flux phases, and 3) instantaneous change of mass
transfer coefficients of all diffusing species in the flux phase by varying
viscosity of the flux, previous laboratory scale experimental data could be well
explained under various [pet Al](0), [pct Si](0) in the liquid steel, (pet
CaO)/(pct SiO2), (pct Al2O3)(0), (pet MgO)(0) in the liquid flux, and reaction
temperature. From the model calculations under the various [pet Al](0), it was
concluded that the present reaction model can be successfully applicable from low
[pct Al] to high [pct Al] conditions in liquid steel. The present model was further
extended in simulating composition change in a mold flux in a continuous casting
mold, where the steel and the flux continuously enter and leave. The model
calculations show good agreement with pilot plant scale data available in
literature. From the calculation results under different casting variables such as
[pct Al](0), mold flux pool depth, and mold flux consumption rate, the Al2O3
accumulation in the CaO-SiO2-type mold flux during the continuous casting was
discussed.
C1 [Kim, Min-Su; Kang, Youn-Bae] Pohang Univ Sci & Technol, Grad Inst Ferrous
Technol, Pohang 37673, Kyungbuk, South Korea.
[Kim, Min-Su] Korean Inst Ind Technol, Jeonbuk Reg Div, Kimje 54325, Jeonbuk,
South Korea.
C3 Pohang University of Science & Technology (POSTECH); Korea Institute of
Industrial Technology (KITECH)
RP Kang, YB (corresponding author), Pohang Univ Sci & Technol, Grad Inst Ferrous
Technol, Pohang 37673, Kyungbuk, South Korea.
EM ybkang@postech.ac.kr
RI Kang, Youn-Bae/AAU-5544-2021
OI Kang, Youn-Bae/0000-0003-0615-0168
CR Bale CW, 2016, CALPHAD, V54, P35, DOI 10.1016/j.calphad.2016.05.002
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NR 34
TC 17
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U1 4
U2 21
PI OXFORD
SN 0364-5916
EI 1873-2984
J9 CALPHAD
JI Calphad-Comput. Coupling Ph. Diagrams Thermochem.
PD JUN
PY 2018
VL 61
BP 105
EP 115
DI 10.1016/j.calphad.2018.02.010
PG 11
WC Thermodynamics; Chemistry, Physical; Materials Science,
Multidisciplinary; Metallurgy & Metallurgical Engineering
SC Thermodynamics; Chemistry; Materials Science; Metallurgy & Metallurgical
Engineering
GA GH9PQ
UT WOS:000434001700011
DA 2023-12-05
ER
PT J
AU Li, SS
Zou, XL
Zheng, K
Lu, XG
Xu, Q
Chen, CY
Zhou, ZF
AF Li, Shangshu
Zou, Xingli
Zheng, Kai
Lu, Xionggang
Xu, Qian
Chen, Chaoyi
Zhou, Zhongfu
TI Direct production of TiAl3 from Ti/Al-containing oxides
precursors by solid oxide membrane (SOM) process
LA English
DT Article
DE TiAl3; Electro-deoxidation; SOM; Oxides; CaCl2
ID MOLTEN CALCIUM-CHLORIDE; THERMAL-EXPLOSION SYNTHESIS; ELECTROCHEMICAL
REDUCTION; TITANIUM-DIOXIDE; 3-PHASE INTERLINES; LIQUID AL; METAL;
AL3TI; CACL2; SALT
AB TiAl3 intermetallic has been successfully synthesized by the electrochemical
deoxidation of the Ti/Al-containing oxides precursors including TiO2/Al2O3 mixture
and titanium-rich slag/Al2O3 mixture at 1000 degrees C and 3.8 V in molten CaCl2. A
solid oxide membrane (SOM) tube filled with carbon-saturated liquid tin was served
as inert anode, and the pressed pellet of Ti/Al-containing oxides precursors was
used as cathode during the electrochemical deoxidation process. The results show
that the reduction proceeds through a serious of individual stages, which mainly
involve the formation-decomposition of calcium titanium/aluminum oxides and the
formation of TiAlx alloys. The analysis of the partially reduced cathode pellet
confirms that the three phases interlines (3PIs) reaction area gradually expands
from the pellet's surface to its centre. The morphology of the TiAl3 obtained from
TiO2/Al2O3 precursor exhibits a homogeneous nodular structure. The final product
produced from the titanium-rich slag/Al2O3 precursor contains TiAl3 and Ll(2)
Ti0.75Fe0.25Al3. In addition, the porous TiAl3 with high porosity can be prepared
by using NaCl as the space-holder material. The results demonstrate that the SOM
process has the potential to be used for the facile production of Ti-Al alloys from
complex oxides precursors. (C) 2017 Elsevier B.V. All rights reserved.
C1 [Li, Shangshu; Zou, Xingli; Zheng, Kai; Lu, Xionggang; Xu, Qian; Zhou, Zhongfu]
Shanghai Univ, State Key Lab Adv Special Steel, Shanghai 200072, Peoples R China.
[Li, Shangshu; Zou, Xingli; Zheng, Kai; Lu, Xionggang; Xu, Qian; Zhou, Zhongfu]
Shanghai Univ, Shanghai Key Lab Adv Ferromet, Shanghai 200072, Peoples R China.
[Li, Shangshu; Zou, Xingli; Zheng, Kai; Lu, Xionggang; Xu, Qian; Zhou, Zhongfu]
Shanghai Univ, Sch Mat Sci & Engn, Shanghai 200072, Peoples R China.
[Zou, Xingli] Univ Texas Austin, Dept Chem, Ctr Electrochem, Austin, TX 78712
USA.
[Chen, Chaoyi] Guizhou Univ, Sch Mat & Met, Guiyang 550025, Guizhou, Peoples R
China.
[Zhou, Zhongfu] Aberystwyth Univ, Inst Math & Phys, Aberystwyth SY23 3BZ, Dyfed,
Wales.
C3 Shanghai University; Shanghai University; Shanghai University;
University of Texas System; University of Texas Austin; Guizhou
University; Aberystwyth University
RP Zou, XL; Lu, XG (corresponding author), Shanghai Univ, State Key Lab Adv Special
Steel, Shanghai 200072, Peoples R China.; Zou, XL; Lu, XG (corresponding author),
Shanghai Univ, Shanghai Key Lab Adv Ferromet, Shanghai 200072, Peoples R China.;
Zou, XL; Lu, XG (corresponding author), Shanghai Univ, Sch Mat Sci & Engn, Shanghai
EM xinglizou@shu.edu.cn; luxg@shu.edu.cn
OI Zou, Xingli/0000-0002-6608-8311
51574146, 51664005]; Science and Technology Commission of Shanghai
Municipality [14JC1491400]; National Basic Research Program of China
[2014CB643403]; Shanghai Municipal Education Commission
China (Nos. 51225401, 51304132, 51574146 and 51664005), the Science and
Technology Commission of Shanghai Municipality (No. 14JC1491400), the
National Basic Research Program of China (No. 2014CB643403) and the
Young Teacher Training Program of Shanghai Municipal Education
Commission.
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NR 45
TC 17
Z9 17
U1 1
U2 60
PI LAUSANNE
SN 0925-8388
EI 1873-4669
J9 J ALLOY COMPD
JI J. Alloy. Compd.
PD DEC 15
PY 2017
VL 727
BP 1243
EP 1252
DI 10.1016/j.jallcom.2017.08.213
PG 10
GA FJ4MH
UT WOS:000412712900150
DA 2023-12-05
ER
PT J
AU Wang, DX
Ling, X
Peng, H
Cui, ZW
Yang, XJ
AF Wang, Dongxiang
Ling, Xiang
Peng, Hao
Cui, Zhenwei
Yang, Xinjun
TI High-temperature analogy experimental investigation on dry granulating
characteristic of rotating disk for waste heat utilization of molten
slag
SO APPLIED THERMAL ENGINEERING
LA English
DT Article
DE Waste heat; Molten slag; Dry granulation; Rotating disk; Particle
ID BLAST-FURNACE SLAG; ORGANIC RANKINE-CYCLE; LIGAMENT FORMATION; SPINNING
DISK; PERFORMANCE ANALYSIS; COLD EXPERIMENTS; ENERGY RECOVERY;
GASIFICATION; ATOMIZATION; LIQUID
AB Dry granulation process is one of the most promising methods for waste heat
utilizing from molten slag. The net heat recovery efficiency and recycling costs of
slag particles are mainly governed by the granulating characteristic. This paper
performed a high-temperature analogy experiment by rotating disk with molten
aluminum as the medium. The results indicated that the mean size of particles grew
with the increasing of feed rate and cooling air rate, decreasing in rotating
speed. The cooling air rate showed a little effect on the size distribution of the
main particles, while lowered the production yield. The circularity shape factor of
particles was mainly influenced by the rotating speed, cooling air rate and the
oxide film formed on the particle surface. The liquid film breakup mode and cooling
rate of particles played significant roles in the formation of filaments. In the
fully-ligament mode, lower mass fraction of filaments was generated, while the
filaments increased rapidly once the liquid film broke up by sheet mode. It was
suggested in the granulation of blast furnace slag that, the particle
characteristics should directly be governed by rotating speed, and the cooling air
rate must be controlled strictly. (C) 2017. lsevier Ltd. All rights reserved.
C1 [Wang, Dongxiang; Cui, Zhenwei; Yang, Xinjun] Jiangnan Univ, Sch Mech Engn,
Jiangsu Key Lab Adv Food Mfg Equipment & Technol, 1800 Li Hu Rd, Wuxi 214122,
Peoples R China.
[Wang, Dongxiang; Ling, Xiang; Peng, Hao; Yang, Xinjun] Nanjing Tech Univ,
Jiangsu Key Lab Proc Enhancement & New Energy Equ, 5 Xin Mo Fan Rd, Nanjing 210009,
C3 Jiangnan University; Nanjing Tech University
RP Wang, DX (corresponding author), Jiangnan Univ, Sch Mech Engn, Jiangsu Key Lab
Adv Food Mfg Equipment & Technol, 1800 Li Hu Rd, Wuxi 214122, Peoples R China.;
Wang, DX; Ling, X (corresponding author), Nanjing Tech Univ, Jiangsu Key Lab Proc
Enhancement & New Energy Equ, 5 Xin Mo Fan Rd, Nanjing 210009, Jiangsu, Peoples R
China.
EM dxwahg85@hotmail.com; xling@njtech.edu.cn
RI Wang, Dongxiang/G-9216-2012
OI Wang, Dongxiang/0000-0002-0473-9297
Fundamental Research Funds for the Central Universities [JUSRP115A11];
Jiangsu Key Laboratory of Process Enhancement and New Energy Equipment
Technology (Nanjing Tech University)
FX The authors gratefully acknowledge the financial support provided by the
National Natural Science Foundation of China (Grant numbers 51606086,
51406078), Fundamental Research Funds for the Central Universities
(Grant numbers JUSRP115A11) and Jiangsu Key Laboratory of Process
Enhancement and New Energy Equipment Technology (Nanjing Tech
University).
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TC 17
Z9 20
U1 4
U2 93
PI OXFORD
SN 1359-4311
J9 APPL THERM ENG
JI Appl. Therm. Eng.
PD OCT
PY 2017
VL 125
BP 846
EP 855
DI 10.1016/j.applthermaleng.2017.07.075
PG 10
WC Thermodynamics; Energy & Fuels; Engineering, Mechanical; Mechanics
SC Thermodynamics; Energy & Fuels; Engineering; Mechanics
GA FG3BG
UT WOS:000410011200076
DA 2023-12-05
ER
PT J
AU Chen, PC
Liu, KH
Ma, HW
AF Chen, Pi-Cheng
Liu, Kun-Hsing
Ma, Hwong-wen
TI Resource and waste-stream modeling and visualization as decision support
tools for sustainable materials management
LA English
DT Article
DE Sustainable materials management; Sankey diagram; Material flow
analysis; Input output model; Inter-agency collaboration
ID SUBSTANCE FLOW-ANALYSIS; GLOBAL FLOW; ALUMINUM; CYCLE
AB Sustainable Materials Management requires the knowledge of complex material flow
system. However, it's difficult for the policy maker and industries to know the
flows for the lack of the expertise to implement material flow analysis. Facing
this issue, we designed a web-based tool to generate interactive Sankey diagrams
for developing strategies to sustainably manage resource and waste flows through a
complex economy. By examining the opportunities across a material's lifecycle, this
tool supports sustainable materials management, which is important in reducing
environmental pressures and the demand for resource extraction. Three applications
were developed for (1) tracking resource flows along supply chains, (2) identifying
economic activities that cause waste generation, and (3) tracing the material
footprints for a sector. To finish the applications, we integrated a comprehensive
resource and waste database with several input output analysis based material flow
models. For easy recognition of the key flows and activities, Sankey diagrams can
be generated using a data-visualization technology. This article demonstrates the
material management practices that can be discovered with the information of the
flow system from the applications. Examine the flow paths of resources, several
practices for sand and gravels are formulated based on the key activities in
processing or using the material. Overviewing the driving forces of industrial
wastes, we also pinpoint the practices to reduce the generation of coal ash.
Tracking the resource footprints of economic activities, we highlight that the
construction sector can use the cement made from blast furnace slag as to reduce
the footprint. Also, we explain how this approach facilitates the coordination of
government's interagency actions and the engagement of private sectors. (C) 2017
C1 [Ma, Hwong-wen] Natl Taiwan Univ, Grad Inst Environm Engn, 71 Chou Shan Rd,
Taipei 106, Taiwan.
[Chen, Pi-Cheng] Natl Cheng Kung Univ, Dept Environm Engn, 1 Univ Rd, Tainan
701, Taiwan.
[Liu, Kun-Hsing] Ind Technol Res Inst, Green Energy & Environm Res Labs, 195,Sec
4,Zhongxing Rd, Zhudong Township 310, Hsinchu County, Taiwan.
C3 National Taiwan University; National Cheng Kung University; Industrial
Technology Research Institute - Taiwan
RP Ma, HW (corresponding author), Rm 401,71 Chou Shan Rd, Taipei 10673, Taiwan.
EM hwma@ntu.edu.tw
RI Chen, Pi-Cheng/ABI-0628-2022
OI Chen, Pi-Cheng/0000-0002-1830-8877; MA, HWONG-WEN/0000-0002-7595-2343
FU EPA Taiwan [EPA-104-H103-02-A091]
FX We would like to thank ChiPing Sun, the manager in the Information
Science Center of Industrial Technology Research Institute for the
assistance in system programming. This research was supported by the EPA
Taiwan under the SMM Project No. EPA-104-H103-02-A091.
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NR 36
TC 17
Z9 17
U1 0
U2 38
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAY 1
PY 2017
VL 150
BP 16
EP 25
DI 10.1016/j.jclepro.2017.02.173
PG 10
& Ecology
GA ES8ZQ
UT WOS:000399846100002
DA 2023-12-05
ER
PT J
AU Chun, TJ
Long, HM
Li, JX
AF Chun, Tiejun
Long, Hongming
Li, Jiaxin
TI Alumina-Iron Separation of High Alumina Iron Ore by Carbothermic
Reduction and Magnetic Separation
SO SEPARATION SCIENCE AND TECHNOLOGY
LA English
DT Article
DE carbothermic reduction; high alumina iron ore; magnetic separation;
removing alumina
ID FLOTATION; BENEFICIATION
AB The carbothermic reduction of high alumina iron ore in the absence/presence of
sodium carbonate (Na2CO3) was carried out for alumina-iron separation by wet
magnetic separation. Sodium carbonate is found to be capable of improving the
separation of alumina and iron, as well as increasing the particle size of metallic
iron significantly. When the high alumina ore briquettes were reduced at 1050
degrees C for 80 min, the average particle size of metallic iron was approximately
100 mu m in the presence of sodium carbonate, which is bigger than the size of 50
mu m in the absence of sodium carbonate. Compared with the absence of sodium
carbonate, the Al2O3 content of iron concentrate decreased from 4.33% to 1.29%,
while the Al2O3 removal rate increased from 43.70% to 83.37% with the addition of
9% sodium carbonate. Experimental evidence showed that Na2CO3 reacted with Al2O3
and SiO2 to form sodium silicate, aluminum silicate, and sodium aluminosilicate,
and decreased the content of Fe in the slags, which improved the separation between
the alumina and iron during the magnetic separation.
Color versions of one or more of the figures in the article can be found online
at
[GRAPHICS]
.
C1 [Chun, Tiejun; Long, Hongming; Li, Jiaxin] Anhui Univ Technol, Sch Met Engn,
Maanshan 243002, Peoples R China.
C3 Anhui University of Technology
RP Long, HM (corresponding author), Anhui Univ Technol, Sch Met Engn, Maanshan
EM springcsu@126.com
OI CHUN, Tiejun/0000-0003-3436-2360; Long, Hongming/0000-0002-0955-2608
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Rocha L, 2010, MINER ENG, V23, P842, DOI 10.1016/j.mineng.2010.03.009
Shi A. J., 1999, CHINA MINING MAGAZIN, V42, P168
Thella JS, 2012, POWDER TECHNOL, V217, P418, DOI 10.1016/j.powtec.2011.10.058
Wills B.A., 2006, MINERAL PROCESSING T
Zhu DQ, 2013, INT J MIN MET MATER, V20, P505, DOI 10.1007/s12613-013-0758-8
NR 12
TC 17
Z9 22
U1 0
U2 33
PI PHILADELPHIA
SN 0149-6395
EI 1520-5754
J9 SEP SCI TECHNOL
JI Sep. Sci. Technol.
PD MAR 24
PY 2015
VL 50
IS 5
BP 760
EP 766
DI 10.1080/01496395.2014.959601
PG 7
WC Chemistry, Multidisciplinary; Engineering, Chemical
SC Chemistry; Engineering
GA CC1OS
UT WOS:000350111300016
DA 2023-12-05
ER
PT J
AU Fallah-Mehrjardi, A
Hayes, PC
Jak, E
AF Fallah-Mehrjardi, Ata
Hayes, Peter C.
Jak, Evgueni
TI Investigation of Freeze-Linings in Aluminum Production Cells
LA English
DT Article
ID HEAT-TRANSFER COEFFICIENT; CRYOLITE; SYSTEMS; PART; SLAG; BEHAVIOR;
MODEL
AB The molten cryolite bath creates chemically a very aggressive environment in the
Hall-H,roult cell, and thus, the formation of a protective solid layer (freeze-
lining) on the cell wall is essential for the operation of the present cell
designs. To provide further information on the formation of the freeze-lining
deposit in this system, laboratory-based studies were undertaken using an air-
cooled probe technique The effects of process conditions, i.e., time, bath
agitation, and superheat on the microstructures, morphologies of the phases, and
the phase assemblages adjacent to the deposit/bath interface were investigated. A
detailed microstructural analysis of the steady-state deposits shows that a dense
sealing primary-phase layer of cryolite solid solution was formed at the interface
of the bath deposit for the process conditions examined. The formation of sealing
primary-phase layer at the bath/deposit interface explicitly indicates that the
deposit/liquid bath interface temperature is equal to that of the liquidus of the
bulk bath. The experimentally investigated liquidus temperature and subliquidus
equilibria differ significantly from those previously reported. (C) The Minerals,
Metals & Materials Society and ASM International 2014
C1 [Fallah-Mehrjardi, Ata; Hayes, Peter C.; Jak, Evgueni] Univ Queensland, Sch Chem
Engn, PYROSEARCH, St Lucia, Qld, Australia.
RP Fallah-Mehrjardi, A (corresponding author), Univ Queensland, Sch Chem Engn,
PYROSEARCH, Level 3, St Lucia, Qld, Australia.
EM ata.fallah@uq.edu.au
OI Jak, Evgueni/0000-0002-7768-1874; Hayes, Peter/0000-0002-9257-9253
FU CSIRO Flagship Collaboration Fund Break-through Technology for Primary
Aluminum
FX This research was undertaken with financial support from the CSIRO
Flagship Collaboration Fund Break-through Technology for Primary
Aluminum.
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y
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8
9
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5
Verscheure K, 2006, METALL MATER TRANS B, V37, P929, DOI 10.1007/BF02735015
NR 45
TC 17
Z9 17
U1 0
U2 10
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD AUG
PY 2014
VL 45
IS 4
BP 1232
EP 1247
DI 10.1007/s11663-014-0078-z
PG 16
Engineering
GA AN1SV
UT WOS:000340364800010
DA 2023-12-05
ER
PT J
AU Chen, KN
Zhao, KQ
Zhang, HH
Sun, QF
Wu, ZL
Zhou, YM
Zhong, YC
Ke, F
AF Chen, Kaining
Zhao, Keqiang
Zhang, Houhu
Sun, Qinfang
Wu, Zhilin
Zhou, Yongmin
Zhong, Yongchao
Ke, Fan
TI Phosphorus removal from aqueous solutions using a synthesized adsorbent
prepared from mineralized refuse and sewage sludge
SO ENVIRONMENTAL TECHNOLOGY
LA English
DT Article
DE synthesized adsorbent; mineralized refuse; sewage sludge; isotherm
equations; desorbability
ID WASTE-WATER TREATMENT; PHOSPHATE ADSORPTION; WETLAND; RETENTION; SAND;
SLAG
AB Mineralized refuse and sewage sludge generated from solid waste from municipal
landfills and sewage treatment plants were sintered as a cost-effective adsorbent
for the removal of phosphorus. Compared with the Freundlich model, phosphorus
adsorption on the synthesized adsorbent, zeolite and ironstone was best described
by the Langmuir model. Based on the Langmuir model, the maximum adsorption capacity
of the synthesized adsorbent (9718mgkg(-1)) was 13.7 and 25.4 times greater than
those of zeolite and ironstone, respectively. The desorbability of phosphorus from
the synthesized adsorbent was significantly lower than that of zeolite. Moreover,
phosphorus removal using the synthesized adsorbent was more tolerant to pH
fluctuations than zeolite and ironstone for the removal of phosphorus from aqueous
solutions. The immobilization of phosphorus onto the synthesized adsorbent was
attributed to the formation of insoluble calcium, aluminium and iron phosphorus.
The heavy metal ion concentrations of the leachate of the synthesized adsorbent
were negligible. The synthesized adsorbent prepared from mineralized refuse and
sewage sludge was cost-effective and possessed a high adsorptive capacity for
phosphorus removal from aqueous solutions.
C1 [Chen, Kaining; Ke, Fan] Chinese Acad Sci, Nanjing Inst Geog & Limnol, State Key
Lab Lake Sci & Environm, Nanjing, Jiangsu, Peoples R China.
[Zhao, Keqiang; Zhang, Houhu; Sun, Qinfang; Wu, Zhilin] Nanjing Inst Environm
Sci, Nanjing, Jiangsu, Peoples R China.
[Zhou, Yongmin; Zhong, Yongchao] Nanjing Univ Technol, Coll Mat Sci & Engn,
Nanjing, Jiangsu, Peoples R China.
C3 Chinese Academy of Sciences; Nanjing Institute of Geography & Limnology,
CAS; Nanjing Tech University
RP Zhao, KQ (corresponding author), Nanjing Inst Environm Sci, Nanjing, Jiangsu,
Peoples R China.
EM kqzhao@nies.org
RI chen, kai/IWV-0528-2023; Wu, Zhilin/GRO-0136-2022
OI Wu, Zhilin/0000-0002-0910-5808
FU Natural Science Foundation of China [41005090]; Major Science and
Technology Program for Water Pollution Control and Treatment
[2012ZX07103-002]; Ministry of Environmental Protection's Special Funds
for Scientific Research on Public Causes [201109024]
FX This study was supported financially by the Natural Science Foundation
of China (No. 41005090), the Major Science and Technology Program for
Water Pollution Control and Treatment (2012ZX07103-002) and Ministry of
Environmental Protection's Special Funds for Scientific Research on
Public Causes (201109024).
CR Abou Taleb MF, 2008, J HAZARD MATER, V159, P372, DOI
10.1016/j.jhazmat.2008.02.028
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for the Examination of Water and Wastewater, P20
Babatunde AO, 2008, CHEM ENG J, V136, P108, DOI 10.1016/j.cej.2007.03.013
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Cao F. Y., 2009, ENV SCI MANAGE, V34, P50
Dunne EJ, 2005, WATER RES, V39, P4355, DOI 10.1016/j.watres.2005.09.007
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Jellali S, 2010, J HAZARD MATER, V184, P226, DOI 10.1016/j.jhazmat.2010.08.026
Liu CJ, 2007, J ENVIRON SCI, V19, P1166, DOI 10.1016/S1001-0742(07)60190-9
Lou ZY, 2011, BIORESOURCE TECHNOL, V102, P2328, DOI
10.1016/j.biortech.2010.10.086
Molle P, 2005, WATER SCI TECHNOL, V51, P193, DOI 10.2166/wst.2005.0318
Prochaska CA, 2006, ECOL ENG, V26, P293, DOI 10.1016/j.ecoleng.2005.10.009
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9797(02)00008-5
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Wei XC, 2008, WATER RES, V42, P3275, DOI 10.1016/j.watres.2008.04.005
Wu DY, 2006, J COLLOID INTERF SCI, V304, P300, DOI 10.1016/j.jcis.2006.09.011
Zhao YC, 2007, J ENVIRON MANAGE, V82, P32, DOI 10.1016/j.jenvman.2005.11.015
NR 36
TC 17
Z9 18
U1 3
U2 85
PI ABINGDON
SN 0959-3330
EI 1479-487X
J9 ENVIRON TECHNOL
JI Environ. Technol.
PD JUN 1
PY 2013
VL 34
IS 11
BP 1489
EP 1496
DI 10.1080/09593330.2012.758659
PG 8
GA 166QD
UT WOS:000320571300016
PM 24191483
DA 2023-12-05
ER
PT J
AU Lamut, J
Falkus, J
Jurjevec, B
Knap, M
AF Lamut, J.
Falkus, J.
Jurjevec, B.
Knap, M.
TI INFLUENCE OF INCLUSIONS MODIFICATION ON NOZZLE CLOGGING
SO ARCHIVES OF METALLURGY AND MATERIALS
LA English
DT Article
DE clogging; inclusion modification; spinel; calcium aluminates; calcium
manganese sulphides
ID MECHANISM; STEEL
AB During the secondary refining of high strength steel in a ladle furnace aluminum
is used for the melt deoxidation. Aluminates inclusions are modified with a calcium
silicon injection in a melt. On the basis of the binary diagram CaO-Al2O3 solid and
liquid calcium aluminates with different composition and shape are formed after
calcium treatment. During the calcium silicon injection manganese sulphide is also
modified and CaS or (Ca,Mn)S is formed and wrapped around calcium aluminates.
Because of rising of calcium bubbles during the calcium silicon injection a
powerful melt stirring occurs. This enables inclusion coagulation and a reaction
with a slag. Additionally, the MgO center dot Al2O3 spinels are formed.
Clogging of a tundish nozzle may occur during continuous casting of steel
billets. Scull which forms on the nozzle's inner wall consists of spinel, calcium
aluminates with various composition and calcium manganese sulphide.
C1 [Lamut, J.; Jurjevec, B.; Knap, M.] Univ Ljubljana, Fac Nat Sci, Ljubljana 1000,
Slovenia.
[Falkus, J.] AGH Univ Sci & Technol, Fac Met Engn & Ind Comp Sci, PL-30059
Krakow, Poland.
C3 University of Ljubljana; AGH University of Krakow
RP Lamut, J (corresponding author), Univ Ljubljana, Fac Nat Sci, Askerceva Cesta
12, Ljubljana 1000, Slovenia.
RI Falkus, Jan/K-6570-2012; Knap, Matjaž/AAO-9462-2020
CR KOR GJW, 1972, METALL TRANS, V3, P2343, DOI 10.1007/BF02647036
Lamut J., 2007, P 13 SEM PROC MET OM, P134
Ogibayashi S., 1992, 75 ISS STEELM C TOR
SHIN YK, 1988, IRONMAK STEELMAK, V15, P143
Sowa L, 2011, ARCH METALL MATER, V56, P359, DOI 10.2478/v10172-011-0038-4
UEMURA K, 1992, ISIJ INT, V32, P150, DOI 10.2355/isijinternational.32.150
*VDEH, 1995, SLAG ATL
Vermeulen Y, 2002, ISIJ INT, V42, P1234, DOI 10.2355/isijinternational.42.1234
NR 11
TC 17
Z9 21
U1 1
U2 21
PU POLSKA AKAD NAUK, POLISH ACAD SCIENCES, INST METALL & MATER SCI PAS
PI WARSZAWA
PA PL, 00-901 WARSZAWA, POLAND
SN 1733-3490
EI 2300-1909
J9 ARCH METALL MATER
JI Arch. Metall. Mater.
PY 2012
VL 57
IS 1
BP 319
EP 324
DI 10.2478/v10172-012-0029-0
PG 6
GA 941HE
UT WOS:000303953500042
OA Bronze
DA 2023-12-05
ER
PT J
AU Qin, GL
Wang, GG
Zou, ZD
AF Qin Guo-liang
Wang Guo-gang
Zou Zeng-da
TI Effects of activating flux on CO2 laser welding process of
6013 Al alloy
LA English
DT Article
DE laser welding; aluminum alloy; activating flux; weld appearance; gas
pore
AB In order to increase the absorption of laser energy and improve the weld
appearance in laser welding of Al alloy, 1.8 mm-6013 Al alloy plate was welded by
activating flux CO2 laser welding. Activating flux includes oxide and fluoride,
which was coated on the workpiece surface before welding. The experimental results
show that the activating flux can effectively improve the absorption of CO2 laser
energy and increase the amount of the molten base metal. The improvement on the
absorption of laser energy by oxide activating flux is greater than that by
fluoride activating flux or two-component activating flux, but the slag
detachability made from both the single activating flux and two-activating flux is
poor. The gas pore sensitivity with oxide activating flux is much higher than that
with fluoride activating flux in CO2 laser welding of 6013 Al alloy.
C1 [Qin Guo-liang] Harbin Inst Technol, State Key Lab Adv Welding & Joining, Harbin
[Qin Guo-liang; Wang Guo-gang; Zou Zeng-da] Shandong Univ, Sch Mat Sci &
Technol, Jinan 250061, Peoples R China.
C3 Harbin Institute of Technology; Shandong University
RP Qin, GL (corresponding author), Harbin Inst Technol, State Key Lab Adv Welding &
Joining, Harbin 150001, Peoples R China.
EM glqin@sdu.edu.cn
FU State Key Laboratory of Advanced Welding and Joining, Harbin Institute
of Technology, China
FX Foundation item: Project supported by State Key Laboratory of Advanced
Welding and Joining, Harbin Institute of Technology, China
CR Ding F., 2003, CHINA WELD, V12, P83
GONG Shui-li, 2009, P 28 INT C APPL LAS, V102, P198
Howse DS, 2000, SCI TECHNOL WELD JOI, V5, P189, DOI 10.1179/136217100101538191
Kazakov Y. V., 2002, WELD INT, V16, P886
Klimpel A., 2003, WELD INT, V17, P684, DOI [10.1533/wint.2003.3196, DOI
10.1533/WINT.2003.3196]
Kuo M, 2001, SCI TECHNOL WELD JOI, V6, P17, DOI 10.1179/136217101101538497
Liu FY, 2003, ACTA METALL SIN, V39, P875
Liu FY, 2003, T NONFERR METAL SOC, V13, P876
Liu JH, 2005, P SOC PHOTO-OPT INS, V5629, P202, DOI 10.1117/12.577884
PARSHIN SG, 2011, WELDING INT, V25, P3
Paskell T, 1997, WELD J, V76, P57
[单际国 SHAN Jiguo], 2008, [焊接学报, Transactions of the China Welding
Institution], V29, P8
[孙昊 SUN Hao], 2007, [焊接学报, Transactions of the China Welding Institution],
V28, P49
Sun Z, 2004, SCI TECHNOL WELD JOI, V9, P337, DOI 10.1179/136217104225021571
[王成涛 WANG Chengtao], 2008, [现代化工, Modern Chemical Industry], V28, P38
NR 15
TC 17
Z9 21
U1 1
U2 31
PU ELSEVIER
PI AMSTERDAM
SN 1003-6326
EI 2210-3384
PD JAN
PY 2012
VL 22
IS 1
BP 23
EP 29
DI 10.1016/S1003-6326(11)61134-5
PG 7
GA 886HX
UT WOS:000299846300004
DA 2023-12-05
ER
PT J
AU Ene, A
Popescu, IV
Ghisa, V
AF Ene, Antoaneta
Popescu, Ion V.
Ghisa, Valentin
TI STUDY OF TRANSFER EFFICIENCIES OF MINOR ELEMENTS DURING STEELMAKING BY
NEUTRON ACTIVATION TECHNIQUE
SO ROMANIAN REPORTS IN PHYSICS
LA English
DT Article
DE minor elements; transfer efficiency; steelmaking; neutron activation
technique
AB Neutron activation analysis was applied to investigate the behaviour of some
metallurgical materials (pig iron, scrap, lime, LD steel, refining slag, sludge,
ferroalloys, aluminum, coke, deoxidized steel, final slag) involved in the
steelmaking process in LD converter in the Iron and Steel Works at Galati
(Romania). The purpose of this work was to determine the transfer efficiencies of
some minor and trace elements (Mn, Al, V, Cu, As, W) from the converter charge to
the metallic bath during the two stages of the steelmaking process: refining and
deoxidation.
C1 [Ene, Antoaneta] Dunarea de Jos Univ Galati, Galati 800201, Romania.
[Popescu, Ion V.] Valahia Univ Targoviste, Targoviste 130024, Romania.
[Popescu, Ion V.] Horia Hulubei Natl Inst Phys & Nucl Engn, Bucharest, Romania.
[Ghisa, Valentin] Ovidius Univ Constanta, Constanta 8700, Romania.
C3 Dunarea De Jos University Galati; Valahia University of Targoviste;
Horia Hulubei National Institute of Physics & Nuclear Engineering;
Ovidius University
RP Ene, A (corresponding author), Dunarea de Jos Univ Galati, Domneasca 111, Galati
800201, Romania.
EM aene@ugal.ro; ivpopes@valahia.ro
RI Ene, Antoaneta/C-1386-2011
OI Ene, Antoaneta/0000-0002-6976-0767; Popescu, Ion V./0000-0002-4589-7208
CR Bodsworth C., 1972, PHYS CHEM IRON STEEL
CAHN RW, 1992, MAT SCI TECHNOLOGY C, V7, P95
ELKHATIB AM, 1986, ISOTOPENPRAXIS, V22, P239, DOI 10.1080/10256018608623657
HOSTE J, 1961, NUCLEONICS, V19, P118
Popescu I, 1996, J RADIOAN NUCL CH LE, V213, P369, DOI 10.1007/BF02162935
RAOOF MA, 1980, J RADIOANAL CHEM, V60, P273, DOI 10.1007/BF02518304
Yusfin YS, 1999, METALLURGIST+, V43, P211, DOI 10.1007/BF02466965
NR 8
TC 17
Z9 17
U1 0
U2 9
PU EDITURA ACAD ROMANE
PI BUCURESTI
PA CALEA 13 SEPTEMBRIE NR 13, SECTOR 5, BUCURESTI 050711, ROMANIA
SN 1221-1451
EI 1841-8759
J9 ROM REP PHYS
JI Rom. Rep. Phys.
PY 2009
VL 61
IS 1
BP 165
EP 171
PG 7
WC Physics, Multidisciplinary
SC Physics
GA 443CV
UT WOS:000265888700014
DA 2023-12-05
ER
PT C
AU Johansen, K
Aune, JA
Bruno, M
Schei, A
AF Johansen, K
Aune, JA
Bruno, M
Schei, A
BE Crepeau, PN
TI Aluminum carbothermic technology Alcoa-Elkem advanced reactor process
SO LIGHT METALS 2003
SE Light Metals
LA English
CT Light Metals Symposium held at the 132nd TMS Annual Meeting
CY MAR 02-06, 2003
CL SAN DIEGO, CA
AB This paper presents a new approach for developing a reactor design and complete
processing concept for carbothermic reduction of aluminum.
The process consists of several reactions which are described in the
thermodynamics section of the paper. The aluminum-producing reaction runs at
temperatures around 2050degrees-2100degreesC in the slag Al4C3-Al2O3. At these
temperatures, Al and Al2O vapors form and leave the reaction zone with the CO. The
Al2O and Al content of the exit gases decrease and the C content of the alloy
product increases with increasing Al4C3 content of the slag. The energy and At
content of the gases are recovered in a vapor recovery step in which they are
countercurrently contacted with carbon materials. The Al-C alloy product must be
decarbonized to attain commercial grade aluminum, with the resulting Al4C3 being
recycled to the metal producing step. Several processing options have been
identified for C removal. The task of the process designer is to attain the various
partial reactions at favorable conditions and combine them in an overall process
that gives high At recovery and low C content of the final product. The heat and
mass transfer kinetics of the process steps are not well known, and the
thermochemical data is uncertain. Therefore the theoretical potential of the
process has to be verified by process experiments in a reasonably large scale.
Major design challenges from earlier efforts to develop a carbothermic reduction
process for aluminum have been reviewed and a tailor-made multi-stage reactor
design and processing concept has been developed, based on utilizing Elkem's
inventory of proprietary reactor technology modules.
A modular test program has been designed to verify the technical feasibility of
the processing concept. Several successful test campaigns have been performed
verifying the technical feasibility of the first stage and critical elements of the
second stage. Additional module tests are being conducted on the vapor recovery
step and an integrated reactor is being constructed for verification of all stages
combined.
In addition to Alcoa funding, the program is supported by the US Department of
Energy and the Norwegian Research Council through the KLIMATEK-foundation.
C1 Elkem ASA Res, Kristiansand, Norway.
RP Johansen, K (corresponding author), Elkem ASA Res, Kristiansand, Norway.
CR FRUEHAN R, 2002, MECH RATE REACTION A
Johansen K, 2003, LIGHT MET, P401
Motzfeldt K, 2001, HIGH TEMP MAT PR-ISR, V20, P241
QUI C, 1995, Z METALLKD, V86, P198
ROHA D, 1998, COMMUNICATION
Roine A., 1997, OUTOKUMPU HSC CHEM W
NR 7
TC 17
Z9 20
U1 0
U2 6
PI WARRENDALE
SN 0147-0809
BN 0-87339-531-X
J9 LIGHT MET
PY 2003
BP 401
EP 406
PG 6
Engineering
GA BW64R
UT WOS:000182684700059
DA 2023-12-05
ER
PT J
AU Kawakami, M
Takenaka, T
Ishikawa, M
AF Kawakami, M
Takenaka, T
Ishikawa, M
TI Electrode reactions in dc electroslag remelting of steel rod
LA English
CT 6th International Conference on Molten Slags, Fluxes and Salts
CY JUN 12-17, 2000
CL STOCKHOLM, SWEDEN
AB The non-metallic inclusion content increased significantly when a steel rod of
Fe-Ni was remelted by dc electroslag remelting. The silicon content increased
slightly. The manganese and sulphur contents did not change. The total aluminium
content in the ingot was max. 0.7%, while that in the electrode was only 10 ppm.
The aluminium cations Al3+ in the slag are reduced to metallic aluminium at the
slag/electrode interface, while O-2(-) anions are oxidised to dissolved (O) under
bar in the metal pool. This Al and (O) under bar subsequently recombine to form
alumina inclusions in the metal pool. The inclusion content was dependent on the
alumina content in the slag. When a rod of plain carbon steel was remelted,
however, the increase in nonmetallic inclusion content was as little as one-tenth
of that for the remelted Fe-Ni rod. The non-metallic inclusion content was
independent of the polarity of the electrode.
C1 Toyohashi Univ Technol, Toyohashi, Aichi 4418580, Japan.
C3 Toyohashi University of Technology
RP Kawakami, M (corresponding author), Toyohashi Univ Technol, Toyohashi, Aichi
4418580, Japan.
CR HIROSE Y, 1977, TETSU TO HAGANE, V63, P2208
INOUYE M, 1975, TETSU TO HAGANE, V61, P139
Kawakami M, 1977, TETSU TO HAGANE, V63, P2161
KAWAKAMI M, 1997, P 5 INT C MOLT SLAGS, P477
KOJIMA Y, 1977, TETSU TO HAGANE, V63, P2191
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NR 12
TC 17
Z9 22
U1 0
U2 7
PU MANEY PUBLISHING
PI LEEDS
SN 0301-9233
J9 IRONMAK STEELMAK
PD AUG
PY 2002
VL 29
IS 4
BP 287
EP 292
DI 10.1179/030192302225005132
PG 6
GA 593CB
UT WOS:000177973000008
DA 2023-12-05
ER
PT J
AU McKay, S
Hunter, NS
Normanton, AS
Ludlow, V
Hewitt, PN
Harris, B
AF McKay, S
Hunter, NS
Normanton, AS
Ludlow, V
Hewitt, PN
Harris, B
TI Continuous casting mould powder evaluation
LA English
DT Article
AB A continuous casting mould powder must satisfy various requirements including
thermal insulation, chemical insulation, inclusion absorption, lubrication, and
promotion of uniform heat transfer from the solidifying steel strand to the copper
mould. The relative importance of these properties varies according to the type of
steel cast, the prevailing casting conditions, and the end steel requirements.
Development of mould powders at Corus UK Ltd involves plant based trials of
different powders whose properties influence the above characteristics of which
heat transfer is a major consideration. Particular use is made of mould thermal
monitoring which, although primarily designed for sticker breakout detection, is
now finding increasing use as an investigative tool in mould slag assessment. Both
static and dynamic plant data are now available relating mould slag heat transfer
performance to casting conditions and this paper describes some recent
investigative work carried out by the Aluminium & Steel Casting Department of
Teesside Technology Centre, Corus UK Ltd. The study shows that using a combination
of plant based observation and laboratory analysis, a greater depth in
understanding of mould powder performance can be realised, yielding important
information for future powder development. (C) 2002 IoM Communications Ltd.
C1 Corus UK Ltd, Teeside Technol Ctr, Grangetown TS6 6UB, Cleveland, England.
RP McKay, S (corresponding author), Corus UK Ltd, Teeside Technol Ctr, POB 11,
Grangetown TS6 6UB, Cleveland, England.
Bommaraju R., 1991, ISS STEELMAKING C P, V74, P131
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NR 5
TC 17
Z9 18
U1 0
U2 4
PU MANEY PUBLISHING
PI LEEDS
SN 0301-9233
J9 IRONMAK STEELMAK
PD JUN
PY 2002
VL 29
IS 3
BP 185
EP 190
DI 10.1179/030192302225004142
PG 6
GA 573ZM
UT WOS:000176863900005
DA 2023-12-05
ER
PT J
AU LOPEZ, FA
SAINZ, E
FORMOSO, A
ALFARO, I
AF LOPEZ, FA
SAINZ, E
FORMOSO, A
ALFARO, I
TI THE RECOVERY OF ALUMINA FROM SALT SLAGS IN ALUMINUM REMELTING
LA English
DT Article
AB This work descrobes a preliminary study which looks at the possibility of
producing a mixture of alumina and spinal by sintering waste produced in the
hydrolysis of slag from aluminium remelting in rotary furnaces. The process
initially involves grinding the slag and carrying out grain screening and sizing,
which leads to the recovery of most of the aluminium metal found in the original
material. It then involves the water leaching of the non-metal part of the slag,
once this been ground to a grain diameter of less than 500 mu m. The fraction which
is not soluble in water is pelletized and then calcined in an oxidizing atmosphere
to produce a mixture made up of alpha-Al2O3 and MgO.Al2O3, which can have different
industrial applications (in particular fused grains, cement, glass, foundry and
steel mixes, refractory, mineral wool, abrasives, ceramic fibres and catalysers).
Finally the products obtained from the sintering process are analysed, and the
effect of temperature on eliminating impurities and the conversions that take place
between the different alumina phases are studied.
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RP LOPEZ, FA (corresponding author), CSIC,NATL CTR MET RES,AVDA GREGORIO AMO 8,E-
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NR 27
TC 17
Z9 17
U1 0
U2 5
PI OXFORD
SN 0008-4433
J9 CAN METALL QUART
JI Can. Metall. Q.
PD JAN-MAR
PY 1994
VL 33
IS 1
BP 29
EP 33
PG 5
GA MR998
UT WOS:A1994MR99800004
DA 2023-12-05
ER
PT J
AU Yang, P
Liu, L
Suo, YL
Qu, HS
Xie, G
Zhang, CX
Deng, SC
Lv, Y
AF Yang, Pan
Liu, Lang
Suo, Yonglu
Qu, Huisheng
Xie, Geng
Zhang, Caixin
Deng, Shunchun
Lv, Yin
TI Investigating the synergistic effects of magnesia-coal slag based solid
waste cementitious materials and its basic characteristics as a backfill
material
LA English
DT Article
DE Mine backfill; Magnesium-coal slag; Mining cementitious material;
Resource utilization; Synergistic effects
ID GAS DESULFURIZATION GYPSUM; BETA-DICALCIUM SILICATE; HEAVY-METAL;
FLY-ASH; STEEL SLAG; HYDRATION; SYSTEMS; IMMOBILIZATION; COMPONENTS;
KINETICS
AB Applying solid waste resources as backfill material can reduce both the cost of
backfill and the environmental problems caused by solid waste landfills. In this
paper, the synergistic reaction effects of solid waste modified magnesia slag
(MMS), coal gasification slag (CGS), and desulfurized gypsum (DG) as magnesium-coal
slag based cementitious materials (MCC) and their preliminary feasibility as mining
cementitious materials in synergy with coal gangue for the preparation of backfill
materials are investigated. The results show that the order of the compressive
strength of the cementitious systems is ternary system > binary system > monolithic
system, which proves the existence of synergistic effect among MMS, CGS, and DG and
determines the optimal dosing of each raw material in the ternary system. At early
ages, the physical effect of CGS and the chemical effect of DG in the ternary
system can promote the hydration reaction of MMS, but the synergistic effect
between the three is weak; At later ages, a synergistic effect occurred among
silica-aluminate depolymerization in CGS, dissolved sulfate from DG and hydration
products from MMS, which promoted the production of more hydration products
calcium-silicate(aluminum)-hydrate (C-S(A)-H) and AFt, and improved the compressive
strength. In addition, the strength, fluidity and leaching of the backfill material
prepared by MCC in collaboration with coal gangue can meet the preliminary
feasibility for mine backfill. In the present work, the full solid waste MCC is
developed to completely replace cement and use it to prepare backfill materials,
which is of great importance to the comprehensive utilization of bulk solid waste,
the reduction of backfill costs, and the enhancement of the economic and ecological
interests of mines.
C1 [Yang, Pan; Liu, Lang; Suo, Yonglu; Qu, Huisheng; Xie, Geng; Zhang, Caixin;
Deng, Shunchun; Lv, Yin] Xian Univ Sci & Technol, Energy Sch, Xian 710054, Peoples
R China.
[Liu, Lang; Suo, Yonglu] Minist Educ China, Key Lab Western Mines & Hazards
Prevent, Xian 710054, Peoples R China.
C3 Xi'an University of Science & Technology; Ministry of Education, China
RP Liu, L (corresponding author), Xian Univ Sci & Technol, Energy Sch, Xian 710054,
Peoples R China.
EM YangPan@xust.edu.cn; liulang@xust.edu.cn; zhangcaixin@stu.xust.edu.cn;
Dengshunchun@stu.xust.edu.cn; 21203226082@stu.xust.edu.cn
RI Xie, Geng/HMP-3102-2023; suo, yonglu/IZQ-3077-2023; Yang,
Pan/HHS-7765-2022
OI Xie, Geng/0000-0002-6802-7301; suo, yonglu/0000-0001-8755-0432;
FU National Natural Science Founda- tion of China [52222404, 52074212,
51874229]
FX This research was supported by the National Natural Science Founda- tion
of China (Nos. 52222404, 52074212, 51874229) .
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NR 75
TC 16
Z9 16
U1 58
U2 77
PU ELSEVIER
PI AMSTERDAM
SN 0048-9697
EI 1879-1026
PD JUL 1
PY 2023
VL 880
AR 163209
DI 10.1016/j.scitotenv.2023.163209
EA APR 2023
PG 15
GA F6QE9
UT WOS:000983563400001
PM 37001664
DA 2023-12-05
ER
PT J
AU Zhang, QL
Zhang, BY
Feng, Y
Qi, CC
Chen, QS
Xiao, CC
AF Zhang, Qinli
Zhang, Bingyi
Feng, Yan
Qi, Chongchong
Chen, Qiusong
Xiao, Chongchun
TI Hydration development of blended cement paste with granulated copper
slag modified with CaO and Al2O3
LA English
DT Article
DE Granulated copper slag; Modification; Blended cement paste; Pozzolanic
activity
ID BLAST-FURNACE SLAG; MECHANICAL-PROPERTIES; PORTLAND-CEMENT;
MICROSTRUCTURE; WASTE; ACTIVATION; BACKFILL; HEAT; TCLP
AB Granulated copper slag (GCS) is currently applied to partial cement replacement
as a supplementary cementitious material (SCM), but with a low rate due to its low
pozzlanic activity. In this contribution we introduce an approach to enhance the
reactivity of GCS by modifying the mineral structure using calcium oxide (CaO) and
aluminum oxide (Al2O3) both by 10 wt.%, in a molten state. Blended cement pastes
were formulated using cement (70 wt.%) and the modified GCS (30 wt.%). The
development of hydration heat and strength were examined using isothermal
calorimetry and strength tests, respectively. The mineral composition and
microstructure of hydration products for different reaction periods were examined
using X-ray diffraction (XRD) and scanning electron microscopy-energy disper-sive
X-ray spectroscopy (SEM-EDS). Also, toxicity characteristic leaching procedure
(TCLP) was performed on the samples. Results showed an increase in the hydration
heat emission rate from the early hydration and the compressive strength of blended
cement paste after curing for 28 days, indicating that the addition of CaO and
Al2O3 in GCS improves pozzolanic activity. XRD and SEM-EDS analysis indicated that
the modified GCS consumed more calcium hydroxide (CH) accompanied by increased
generation of calcium silicate hydrate (C-S-H) gels in blended cement with a
microstructure containing more gel phases and fewer pores, forming a more compact
structure. Leaching of heavy metals of paste samples was lower than Environmental
Protection Agency (EPA) limit. It is possible to apply the modified GCS as a
sustainable material to promote cleaner production for cement and concrete
industries. (c) 2022 The Authors. Published by Elsevier B.V.
C1 [Zhang, Qinli; Zhang, Bingyi; Feng, Yan; Qi, Chongchong; Chen, Qiusong; Xiao,
Chongchun] Cent South Univ, Sch Resources & Safety Engn, Changsha 410083, Hunan,
Peoples R China.
[Xiao, Chongchun] Feny Co Ltd, Changsha 410083, Hunan, Peoples R China.
RP Feng, Y (corresponding author), Cent South Univ, Sch Resources & Safety Engn,
EM yan.feng@csu.edu.cn
RI Qi, Chongchong/K-1167-2019
OI Qi, Chongchong/0000-0001-5189-1614
52004330]; Science and Technology Innovation Program of Hunan Province
[2021RC3125]
FX This work was financially supported by National Natural Science
Foundation of China (No. 52104156, No. 5207435, and No. 52004330) and
the Science and Technology Innovation Program of Hunan Province (No.
2021RC3125).
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NR 61
TC 16
Z9 16
U1 6
U2 45
PU ELSEVIER
PI AMSTERDAM
SN 2238-7854
EI 2214-0697
PD MAY-JUN
PY 2022
VL 18
BP 909
EP 920
DI 10.1016/j.jmrt.2022.03.008
EA MAR 2022
PG 12
Engineering
GA 1C5BG
UT WOS:000793133900003
OA gold
DA 2023-12-05
ER
PT J
AU Kan, LL
Wang, F
AF Kan, Lili
Wang, Fei
TI Mechanical properties of high ductile alkali-activated fiber reinforced
composites incorporating red mud under different curing conditions
LA English
DT Article
DE Mechanical properties; High ductile; Alkali-activated composite; Red
mud; Curing conditions; Sustainability
ID ASH-BASED GEOPOLYMERS; FLY-ASH; STEADY-STATE; STRENGTH; CEMENT;
BEHAVIOR; MORTAR; ECC; NANOINDENTATION; FEASIBILITY
AB Red mud (RM) is an industrial by-product created during the production of
alumina/aluminium that has engendered severe environmental concerns arising from
its improper disposal. To mitigate the negative environmental impact of RM waste
and produce a sustainable material having high mechanical performance (particularly
ductility) for a variety of applications, this study developed an alkali-activated
fiber reinforced composite (AAFRC) using RM, ground granulated blast-furnace slag
(or slag), and silica fume as the precursors. The effects of two different curing
conditions (ambient-curing and heat-curing) on the mechanical properties and
microscopic characteristics of the material were systematically investigated. The
heat-cured RM-derived AAFRC exhibited excellent tensile strain capacity (or
ductility) of up to 5.6%, which was significantly higher than that of its
counterpart that was cured under ambient condition. Despite the reduction in
strength caused by heat-curing, AAFRC retained adequate tensile and compressive
strengths of 4.0 and 75 MPa, respectively. The results of threepoint bending,
single crack tensile, and single fiber pullout tests provided reasonable
explanations for the tensile behaviors of the studied material. Scanning electron
microscopy revealed that a less compacted matrix was formed in the RM composite due
to heat-curing. The combined results from energy dispersive spectroscopy and
nanoindentation tests indicated that adding red mud did not alter the types of
reaction products for the material, which were similar in composition to
conventional alkali-activated slag while also including C-A-S-H and N-A-SH gels in
addition to a type of layered double hydroxide. These findings can serve as
theoretical guidelines for the future design and application of eco-friendly, high-
ductile cementless composites prepared from RM waste.
C1 [Kan, Lili; Wang, Fei] Univ Shanghai Sci & Technol, Sch Environm & Architecture,
C3 University of Shanghai for Science & Technology
RP Kan, LL (corresponding author), Univ Shanghai Sci & Technol, Sch Environm &
Architecture, Shanghai 200093, Peoples R China.
EM Kanlili@usst.edu.cn
FX The authors sincerely acknowledge the financial support from the
National Natural Science Foundation of China (Project No. 51508329).
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NR 81
TC 16
Z9 16
U1 4
U2 25
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD JAN 15
PY 2022
VL 48
IS 2
BP 1999
EP 2011
DI 10.1016/j.ceramint.2021.09.285
EA NOV 2021
PG 13
GA XG2GK
UT WOS:000724576400001
DA 2023-12-05
ER
PT J
AU Milad, A
Ali, ASB
Babalghaith, AM
Memon, ZA
Mashaan, NS
Arafa, S
Yusoff, NIM
AF Milad, Abdalrhman
Ali, Ahmed Suliman B.
Babalghaith, Ali Mohammed
Memon, Zubair Ahmed
Mashaan, Nuha S.
Arafa, Salaheddin
Md. Yusoff, Nur Izzi
TI Utilisation of Waste-Based Geopolymer in Asphalt Pavement Modification
and Construction-A Review
SO SUSTAINABILITY
LA English
DT Review
DE geopolymers; eco-friendly; asphalt pavement industry; hot-mix asphalt;
warm-mix asphalt; reclaimed asphalt pavement; industrial wastes
ID WARM-MIX ASPHALT; LIFE-CYCLE ASSESSMENT; FLY-ASH; PERFORMANCE
EVALUATION; RUTTING RESISTANCE; STRENGTH; NANOCLAY; POLYMER; BINDER;
MICROSTRUCTURE
AB The use of geopolymer in pavement constructions is strongly encouraged. Many
studies have demonstrated the vast potential of using industrial-by-products-based
geopolymers. This paper discusses the modification of asphalt binders with
geopolymers, namely geopolymer-modified asphalt (GMA) and geopolymer-modified
asphalt mixture (GMAM). In addition, curing geopolymer materials, engineering
properties, production techniques, and prospective utilisation in the pavement
construction, such as durability and sustainability, are also discussed. The
literature review showed that many industrial by-products, including red mud, blast
furnace slag, fly ash, and mine waste, are used to produce geopolymers because of
the metal components such as silicon and aluminium in these materials. The
geopolymers from these materials influence the rheological and physical properties
of asphalt binders. Geopolymers can enhance asphalt mixture performance, such as
stability, fatigue, rutting, and low-temperature cracking. The use of geopolymers
in asphalt pavement has beneficial impacts on sustainability and economic and
environmental benefits.
C1 [Milad, Abdalrhman; Md. Yusoff, Nur Izzi] Univ Kebangsaan Malaysia, Dept Civil
Engn, Bangi 43600, Selangor, Malaysia.
[Ali, Ahmed Suliman B.; Arafa, Salaheddin] Univ Tun Hussein Onn Malaysia, Fac
Civil Engn & Built Environm, Parit Raja 86400, Johor, Malaysia.
[Babalghaith, Ali Mohammed] Univ Malaya, Dept Civil Engn, Ctr Transportat Res,
Fac Engn, Kuala Lumpur 50603, Malaysia.
[Memon, Zubair Ahmed] Prince Sultan Univ PSU, Dept Engn Management, Coll Engn,
Riyadh 11586, Saudi Arabia.
[Mashaan, Nuha S.] Curtin Univ, Sch Civil & Mech Engn, Bentley, WA 6102,
Australia.
C3 Universiti Kebangsaan Malaysia; University of Tun Hussein Onn Malaysia;
Universiti Malaya; Curtin University
RP Milad, A (corresponding author), Univ Kebangsaan Malaysia, Dept Civil Engn,
Bangi 43600, Selangor, Malaysia.; Memon, ZA (corresponding author), Prince Sultan
Univ PSU, Dept Engn Management, Coll Engn, Riyadh 11586, Saudi Arabia.
EM miladabdalrhman@siswa.ukm.edu.my; algowel@yahoo.com;
bablgeath@hotmail.com; zamemon@psu.edu.sa; nuhas.mashaan1@curtin.edu.au;
arafa.uthm@gmail.com; izzi@ukm.edu.my
RI Milad, Abdalrhman/AAP-7145-2021; Mashaan, Nuha S/B-5443-2011;
Babalghaith, ALI Mohammed/T-2515-2017
OI Milad, Abdalrhman/0000-0002-3336-0657; Mashaan, Nuha
S/0000-0002-0331-4254; Babalghaith, ALI Mohammed/0000-0003-3736-8813;
Md. Yusoff, Nur Izzi/0000-0003-4449-4981; Memon,
Zubair/0000-0003-1605-0566
FU Prince Sultan University
FX Prince Sultan University support for paying the Article Processing
Charges (APC) of this publication.
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NR 97
TC 16
Z9 18
U1 7
U2 53
PU MDPI
PI BASEL
EI 2071-1050
J9 SUSTAINABILITY-BASEL
JI Sustainability
PD MAR
PY 2021
VL 13
IS 6
AR 3330
DI 10.3390/su13063330
PG 21
WC Green & Sustainable Science & Technology; Environmental Sciences;
Environmental Studies
(SSCI)
GA RV3XP
UT WOS:000645770200001
DA 2023-12-05
ER
PT J
AU Guo, QH
Huang, YC
Gong, Y
Zhuang, XD
Richter, A
Yu, GS
AF Guo, Qinghua
Huang, Yuchen
Gong, Yan
Zhuang, Xiaodong
Richter, Andreas
Yu, Guangsuo
TI Recovered Carbon from Coal Gasification Fine Slag as Electrocatalyst for
Oxygen Reduction Reaction and Zinc-Air Battery
SO ENERGY TECHNOLOGY
LA English
DT Article
DE coal gasification; fine slag; oxygen reduction reaction; zinc– air
batteries
AB The coal gasification industry produces a large amount of coarse and fine slag.
Such slag, which is composed mainly of carbon residues and inorganic species, e.g.,
silicon, calcium, magnesium, and aluminum, becomes a tough problem because of the
environmental concerns and high reusage cost. Benefiting from the carbon-rich
feature, such cheap byproducts of the coal gasification industry can be used as
precursors to prepare porous carbons for energy conversion and storage. Herein, new
porous carbons are prepared by treating carbon-rich fine slag by direct acid
etching and ammonia activation. The oxygen reduction reaction performance of as-
developed porous carbons as electrocatalysts is evaluated in alkaline media. Then,
such porous carbons are further utilized as air cathodes for a zinc-air battery and
reach a power density of 88 mW cm(-2) at the current density of 154.9 mA cm(-2).
All these results indicate that fine slag, a byproduct of the coal gasification
industry, has a great potential to be reused as a high-value electrocatalyst and
electrode for energy conversion and storage.
C1 [Guo, Qinghua; Huang, Yuchen; Gong, Yan; Yu, Guangsuo] East China Univ Sci &
Technol, Inst Clean Coal Technol, Shanghai 200237, Peoples R China.
[Zhuang, Xiaodong] Shanghai Jiao Tong Univ, Sch Chem & Chem Engn, Shanghai Key
Lab Elect Insulat & Thermal Ageing, State Key Lab Met Matrix Composites,Mesoentropy
M, Shanghai 200240, Peoples R China.
[Richter, Andreas] Tech Univ Bergakad Freiberg, Inst Energy Proc Engn & Chem
Engn, Fuchsmuhlenweg 9, D-09599 Freiberg, Germany.
[Yu, Guangsuo] Ningxia Univ, State Key Lab High Efficiency Coal Utilizat & Gre,
Yinchuan 750021, Ningxia, Peoples R China.
C3 East China University of Science & Technology; Shanghai Jiao Tong
University; Technical University Freiberg; Ningxia University
RP Guo, QH (corresponding author), East China Univ Sci & Technol, Inst Clean Coal
Technol, Shanghai 200237, Peoples R China.; Richter, A (corresponding author), Tech
Univ Bergakad Freiberg, Inst Energy Proc Engn & Chem Engn, Fuchsmuhlenweg 9, D-
09599 Freiberg, Germany.
EM gqh@ecust.edu.cn; zhuang@sjtu.edu.cn
RI Richter, Andreas/AAC-1953-2020; Zhuang, Xiaodong/A-1519-2012
OI Richter, Andreas/0000-0002-8493-8690; Zhuang,
Xiaodong/0000-0002-4090-0420
FU National Key R&D Program of China [2017YFB0602404]; National Natural
Science Foundation of China [21761132034]; NSFC Excellent Young
Scientists Fund [51722304]; NSFC [21720102002, 51973114, 51811530013];
Shanghai Pujiang Talent Program [18PJ1406100]; SMSTC [19JC412600]
FX This work was supported by the National Key R&D Program of China
(2017YFB0602404) and National Natural Science Foundation of China
(21761132034). X.Z. is thankful for the financial support from the NSFC
Excellent Young Scientists Fund (51722304), NSFC (21720102002, 51973114,
51811530013), Shanghai Pujiang Talent Program (18PJ1406100), and SMSTC
(19JC412600).
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NR 54
TC 16
Z9 16
U1 14
U2 128
PI WEINHEIM
SN 2194-4288
EI 2194-4296
J9 ENERGY TECHNOL-GER
JI Energy Technol.
PD APR
PY 2021
VL 9
IS 4
AR 2000890
DI 10.1002/ente.202000890
EA FEB 2021
PG 8
WC Energy & Fuels
SC Energy & Fuels
GA RJ7VF
UT WOS:000618961000001
DA 2023-12-05
ER
PT J
AU Liu, WZ
Aldahri, T
Ren, S
Xu, CC
Rohani, S
Liang, B
Li, C
AF Liu, Weizao
Aldahri, Tahani
Ren, Shan
Xu, Chunbao Charles
Rohani, Sohrab
Liang, Bin
Li, Chun
TI Solvent-free synthesis of hydroxycancrinite zeolite microspheres during
the carbonation process of blast furnace slag
LA English
DT Article
DE Blast furnace slag; Zeolite; Mineralization; CO2 capture;
Crystallization
ID INDIRECT MINERAL CARBONATION; DIRECT AQUEOUS CARBONATION;
CANCRINITE-TYPE ZEOLITE; CO2 SEQUESTRATION; FLY-ASH; PHASE-DIAGRAMS;
DISSOLUTION; DIOXIDE; OPTIMIZATION; RECOVERY
AB CO2 mineralization is a technological solution to reduce anthropogenic CO2
emissions. It is more cost-effective to use industrial wastes as feedstock than
natural minerals and eliminate some of the energy-consuming operations, to recover
various value-added byproducts. In this study, hydroxycancrinite zeolite was
synthesized by a solvent-free method during the carbonation of blast furnace slag
(BFS) as the waste feedstock. The effects of various process factors such as the
alkaline dosage, crystallization temperature, and crystallization batch time on the
synthesis of hydroxycancrinite were systematically investigated. A well-
crystallized spherical hydroxycancrinite was obtained by mixing with NaOH solid and
then crystallizing at 100 degrees C for 4 h. The as-synthesized products were
characterized by X-ray diffraction, Fourier transform infrared spectroscopy,
scanning electron microscope, thermogravimetric analysis, and Brunauer-Emmett-
Teller analysis. The results revealed that pure microspheres of hydroxycancrinites
are obtained with a diameter of similar to 1 mu m and a surface area of 37.2
m(2)/g. Based on the material balance and preliminary economic evaluation, 361 kg
CO2/t BFS can be stored by calcium and magnesium components, whereas almost all of
the silicon and aluminum are recovered as value-added zeolites, which significantly
improve the process economy. (C) 2020 Elsevier B.V. All rights reserved.
C1 [Liu, Weizao; Ren, Shan] Chongqing Univ, Coll Mat Sci & Engn, Chongqing 400044,
Peoples R China.
[Liang, Bin; Li, Chun] Sichuan Univ, Sch Chem Engn, Chengdu, Peoples R China.
[Aldahri, Tahani; Xu, Chunbao Charles; Rohani, Sohrab] Western Univ, Dept Chem &
Biochem Engn, London, ON, Canada.
[Aldahri, Tahani] Taibah Univ, Dept Phys, Madinah, Saudi Arabia.
C3 Chongqing University; Sichuan University; Western University (University
of Western Ontario); Taibah University
RP Xu, CC; Rohani, S (corresponding author), Western Univ, Dept Chem & Biochem
Engn, London, ON, Canada.
EM cxu6@uwo.ca; srohani@uwo.ca
RI Liang, Bin/JHU-0581-2023
OI Liu, Weizao/0000-0003-0976-2864; Xu, Chunbao/0000-0001-6543-3817
[2016YFB0600904]; Natural Science and Engineering Research Council of
Canada (NSERC)
(2016YFB0600904), and Natural Science and Engineering Research Council
of Canada (NSERC) via the Discovery Grants awarded to Drs. Xu and
Rohani.
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NR 59
TC 16
Z9 17
U1 2
U2 94
PI LAUSANNE
SN 0925-8388
EI 1873-4669
J9 J ALLOY COMPD
JI J. Alloy. Compd.
PD DEC 20
PY 2020
VL 847
AR 156456
DI 10.1016/j.jallcom.2020.156456
PG 10
GA NT8ZE
UT WOS:000573225700012
DA 2023-12-05
ER
PT J
AU Moukannaa, S
Bagheri, A
Benzaazoua, M
Sanjayan, JG
Pownceby, MI
Hakkou, R
AF Moukannaa, S.
Bagheri, A.
Benzaazoua, M.
Sanjayan, J. G.
Pownceby, M., I
Hakkou, R.
TI Elaboration of alkali activated materials using a non-calcined red clay
from phosphate mines amended with fly ash or slag: A structural study
LA English
DT Article
DE Red clay; Mine waste valorization; Alkali activation; Compressive
strength; Microstructure
ID THERMAL-RESISTANCE; COMPOSITE; STRENGTH; ALUMINUM; MORTAR;
SOLIDIFICATION/STABILIZATION; GEOPOLYMERISATION; TECHNOLOGY; STABILITY;
TAILINGS
AB This study aims to explore the feasibility of using waste red clay from a
sedimentary, interlayered phosphate deposit to produce a geopolymer mortar without
any pre-treatment. Alkali activated mortars were prepared by mixing fly ash or slag
with red clay and sand, using different fly ash or slag/red clay ratios. The
effects of sodium silicate to sodium hydroxide ratio (SS/SH) and curing time on the
mortar's properties were studied. The results showed that compared to fly ash-based
alkali activated materials, an increase of the slag content resulted in the
formation of dense mortars while in the case of fly ash based-samples more porous
mortars were formed when the fly ash amount was increased. The mineralogical
investigations indicated a partial contribution of montmorillonite and palygorskite
from the clay to the alkali activation reaction. The mechanical properties of the
materials were promising with a maximum compressive strength of up to 39 MPa
obtained for the mixture of fly ash and red clay at a fly ash/red clay ratio of 2
and a SS/SH of 1.
C1 [Moukannaa, S.; Hakkou, R.] Univ Cadi Ayyad, Fac Sci & Tech, Av A Khattabi,BP
549, Marrakech 40000, Morocco.
[Moukannaa, S.; Hakkou, R.] Mohammed VI Polytech Univ, Lot 660 Hay Moulay
Rachid, Bengurir, Morocco.
[Moukannaa, S.; Bagheri, A.; Sanjayan, J. G.] Swinburne Univ Technol, Fac Sci
Engn & Technol, Dept Civil & Construct Engn, Hawthorn, Vic 3122, Australia.
[Benzaazoua, M.] Univ Quebec Abitibi Temiscamingue UQAT, 445 Blvd Univ, Rouyn
Noranda, PQ J9X 5E4, Canada.
[Pownceby, M., I] CSIRO Mineral Resources, Private Bag 10, Clayton, Vic 3169,
Australia.
C3 Cadi Ayyad University of Marrakech; Mohammed VI Polytechnic University;
Swinburne University of Technology; University of Quebec; University
Quebec Abitibi-Temiscamingue; Commonwealth Scientific & Industrial
Research Organisation (CSIRO)
RP Moukannaa, S (corresponding author), Univ Cadi Ayyad, Fac Sci & Tech, Av A
Khattabi,BP 549, Marrakech 40000, Morocco.
EM samira.moukannaa@um6p.ma
RI Pownceby, Mark Ian/GLN-6915-2022
OI Pownceby, Mark Ian/0000-0002-7061-2489
FU Swinburne University of Technology; Mohammed VI Polytechnic University
FX This work was supported by Swinburne University of Technology and
Mohammed VI Polytechnic University.
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NR 51
TC 16
Z9 16
U1 2
U2 14
PI LAUSANNE
SN 0254-0584
EI 1879-3312
J9 MATER CHEM PHYS
PD DEC 1
PY 2020
VL 256
AR 123678
DI 10.1016/j.matchemphys.2020.123678
PG 10
GA OH6KY
UT WOS:000582701400052
DA 2023-12-05
ER
PT J
AU Yang, T
Zhang, ZH
Wang, Q
Wu, QS
AF Yang, Tao
Zhang, Zuhua
Wang, Qiang
Wu, Qisheng
TI ASR potential of nickel slag fine aggregate in blast furnace slag-fly
ash geopolymer and Portland cement mortars
LA English
DT Article
DE Alkali-silica reaction; Nickel slag; Geopolymer; Portland cement
ID ALKALI-SILICA REACTION; FERRONICKEL SLAG; ACTIVATED SLAG; AMORPHOUS
SILICA; CONCRETE; CALCIUM; DISSOLUTION; ALUMINUM; GEL; SUITABILITY
AB Utilizing nickel slag as aggregates in concrete production proposes an economic
option for recycling this industrial by-product, and meanwhile preserves the
natural rock aggregate resources. Thus, there is an urgent need to further explore
the potentially alkali-silica reaction (ASR) nature. This study investigates the
ASR of high-magnesium nickel slag (HMNS) fine aggregate in the fly ash-blast
furnace slag geopolymer and Portland cement (PC) mortars. No obvious ASR product is
observed in the mortars with HMNS fine aggregate, which exhibit lower ASR expansion
than the mortars with ASR reactive sand. In the geopolymer mortars, the reactive Al
species initially dissolved from HMNS promote the formation of aluminum-containing
alkalis silicate gel layer covered on the surface of HMNS grains. This provides a
diffuse barrier to protect the inner silica against further attack of alkalis, and
consequently mitigates the deleterious ASR. In the PC mortars, the pozzolanic
reaction of HMNS improves the consumption of portlandite in the pore solution to
reduce the alkalinity and calcium content, resulting in a suppression to the ASR
degradation. The accelerated mortar bar test shows that HMNS is reliable for the
utilization without deleterious ASR expansion risk. (C) 2020 Published by Elsevier
Ltd.
C1 [Yang, Tao; Wu, Qisheng] Yancheng Inst Technol, Sch Mat Engn, Yancheng 224051,
[Yang, Tao] Univ Leeds, Sch Civil Engn, Leeds LS2 9JT, W Yorkshire, England.
Applicat Tec, Changsha 410082, Hunan, Peoples R China.
[Wang, Qiang] Tsinghua Univ, Dept Civil Engn, Beijing 100084, Peoples R China.
C3 Yancheng Institute of Technology; University of Leeds; Hunan University;
Tsinghua University
RP Zhang, ZH (corresponding author), Hunan Univ, Coll Civil Engn, Key Lab Green &
Adv Civil Engn Mat & Applicat Tec, Changsha 410082, Hunan, Peoples R China.
EM Zuhua.Zhang@usq.edu.au
RI Zhang, Zuhua/AAK-5391-2020
OI Zhang, Zuhua/0000-0002-7153-5120; Qiang, Wang/0000-0003-4124-352X; Yang,
Tao/0000-0002-4879-8256
51572234]; Natural Science Foundation of Jiangsu Province of China
[BK20170476]; Yancheng Institute of Technology [XJR2019019]
FX Acknowledged financial supports include the National Natural Science
Foundation of China (51702278, 51878263, 51572234), the Natural Science
Foundation of Jiangsu Province of China (BK20170476), the funding for
school-level research projects of Yancheng Institute of Technology (No.
XJR2019019).
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PG 9
GA OH4HM
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DA 2023-12-05
ER
PT J
AU Alharbi, N
Varela, B
Hailstone, R
AF Alharbi, Najat
Varela, Benjamin
Hailstone, Richard
TI Alkali-activated slag characterization by scanning electron microscopy,
X-ray microanalysis and nuclear magnetic resonance spectroscopy
LA English
DT Article
DE Granulated blast-furnace slag; Alkali-activated cement; SEM; TEM; NMR
ID S-H; CEMENT PASTES; PORE SOLUTION; HYDRATION; GELS
AB The alkali activation of blast furnace slag has the potential to reduce the
environmental impact of cementitious materials and to be applied in geographic
zones where weather is a factor that negatively affects performance of materials
based on Ordinary Portland Cement. Blast furnace slag is a highly heterogeneous
material. It is well known that its chemical composition affects the physical
properties of the alkali activated material, however there is little work on how
these inhomogeneities affect the microstructure. In this study we characterize
blast furnace slag activated with KOH using several methods: X-ray diffraction
(XRD), transmission electron microscopy (TEM), nuclear resonance magnetic
spectroscopy (NMR), scanning electron microscopy (SEM), energy-dispersive X-ray
spectroscopy (EDS), and quantitative element mapping. Attention is focused on
delineating the phases before and after the alkali activation. The unactivated slag
shows two distinctive phases. After alkali activation, several chemical changes
were detected. One of the phases of the unactivated slag splits into three new
phases with distinct chemical composition-one is rich in hydrotalcite and two
phases where calcium aluminum silicate hydrate (C-A-S-H) is predominant. A fourth
phase was the particles carried over from the unactivated slag, but with
significant changes in the chemical composition. NMR results show the formation of
tobermorite-like structure in which Al substitutes for Si.
C1 [Alharbi, Najat; Hailstone, Richard] Rochester Inst Technol, Ctr Imaging Sci, 54
Lomb Mem Dr, Rochester, NY 14623 USA.
[Varela, Benjamin] New Mexico Inst Min & Technol, 801 LeRoy Pl, Socorro, NM
87801 USA.
C3 Rochester Institute of Technology; New Mexico Institute of Mining
Technology
RP Varela, B (corresponding author), New Mexico Inst Min & Technol, 801 LeRoy Pl,
Socorro, NM 87801 USA.
EM Benjamin.Varela@nmt.edu
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Consultants
NR 21
TC 16
Z9 16
U1 2
U2 30
PI NEW YORK
SN 1044-5803
EI 1873-4189
J9 MATER CHARACT
JI Mater. Charact.
PD OCT
PY 2020
VL 168
AR 110504
DI 10.1016/j.matchar.2020.110504
PG 11
GA NR7HJ
UT WOS:000571731500002
DA 2023-12-05
ER
PT J
AU Meng, FY
Li, XS
Shi, L
Li, YJ
Gao, F
Wei, YZ
AF Meng, Fanyue
Li, Xinsheng
Shi, Lei
Li, Yuanjian
Gao, Feng
Wei, Yuezhou
TI Selective extraction of scandium from bauxite residue using ammonium
sulfate roasting and leaching process
LA English
DT Article
DE Bauxite residue; Scandium; Ammonium sulfate; Roasting; Leaching
ID RED MUD; THERMAL-DECOMPOSITION; GREEK BAUXITE; RECOVERY; MECHANISM;
TITANIUM; IRON; SLAG
AB Bauxite residue, as an important source of scandium, is an alkaline industrial
waste generated during the Bayer process for alumina production. A novel method for
selective extraction of scandium from bauxite residue was proposed by ammonium
sulfate roasting and water leaching. During the roasting process, ammonium sulfate
could selectively react with Sc, Al and Fe in the bauxite residue to produce
respective metal ammonium sulfates, and then which were completely decomposed to
their respective metal sulfates at 550 degrees C. The sulfates of iron (III) and
aluminum were decomposed to their respective metal oxides at about 700 degrees C,
whereas the scandium sulfate remained stable. In the leaching process, the scandium
sulfate could be selectively leached with water from roasted residues while other
elements mainly remained in the leaching residue. The extraction efficiency of
scandium reached above 90% under the optimum conditions.
C1 [Meng, Fanyue; Li, Xinsheng; Shi, Lei; Li, Yuanjian; Gao, Feng; Wei, Yuezhou]
Guangxi Univ, Sch Resources Environm & Mat, Nanning 530004, Guangxi, Peoples R
China.
[Meng, Fanyue; Li, Xinsheng; Shi, Lei; Li, Yuanjian; Gao, Feng; Wei, Yuezhou]
Guangxi Univ, Guangxi Key Lab Proc Nonferrous Met & Featured Ma, Nanning 530004,
Peoples R China.
[Wei, Yuezhou] Shanghai Jiao Tong Univ, Sch Nucl Sci & Engn, Shanghai 200240,
Peoples R China.
C3 Guangxi University; Guangxi University; Shanghai Jiao Tong University
RP Li, XS (corresponding author), Guangxi Univ, Sch Resources Environm & Mat,
Nanning 530004, Guangxi, Peoples R China.
EM xinshengli@gxu.edu.cn
RI Li, Yuan/GXV-1310-2022; li, xin/HHS-9461-2022; Wei, Yue/HPG-0214-2023
OI Gao, Feng/0000-0003-0676-1030
FU Natural Science Foundation of Guangxi [2017GXNSFAA198176,
2017GXNSFAA198206]; Science and Technology Major Project of Guangxi
Province [AA17204100, AA18118030]
FX This work was supported by the Natural Science Foundation of Guangxi
(No. 2017GXNSFAA198176, 2017GXNSFAA198206), and Science and Technology
Major Project of Guangxi Province (No. AA17204100, AA18118030).
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U2 53
PI OXFORD
SN 0892-6875
J9 MINER ENG
JI Miner. Eng.
PD OCT 1
PY 2020
VL 157
AR 106561
DI 10.1016/j.mineng.2020.106561
PG 9
GA NH2WW
UT WOS:000564536800009
DA 2023-12-05
ER
PT J
AU van Deventer, JSJ
White, CE
Myers, RJ
AF van Deventer, Jannie S. J.
White, Claire E.
Myers, Rupert J.
TI A Roadmap for Production of Cement and Concrete with Low-CO2
Emissions
LA English
DT Article
DE Alkali-activated material; Cementitious materials; Commercialisation;
Durability; Standards; Thermodynamic modelling
ID C-S-H; ALKALI-SILICA REACTION; ACTIVATED SLAG CEMENT; BLAST-FURNACE
SLAG; MERCURY INTRUSION POROSIMETRY; HYDRATED PORTLAND CEMENTS; SERVICE
LIFE PREDICTION; FLY-ASH; PORE STRUCTURE; REINFORCED-CONCRETE
AB This review will show that low-CO2 cements can be produced to give superior
durability, based on a sound understanding of their microstructure and how it
impacts macro-engineering properties. For example, it is essential that aluminium
is available in calcium-rich alkali-activated systems to offset the
depolymerisation effect of alkali cations on C-(N-)A-S-H gel. The upper limit on
alkali cation incorporation into a gel greatly affects mix design and source
material selection. A high substitution of cement clinker in low-CO2 cements may
result in a reduction of pH buffering capacity, hence susceptibility to carbonation
and corrosion of steel reinforcement. With careful mix design, a more refined pore
structure and associated lower permeability can still give a highly durable
concrete. It is essential to expand thermodynamic databases for current and
prospective cementitious materials so that concrete performance and durability can
be predicted when using low-CO2 binders. Cationic copolymer and amphoteric
plasticisers, when available commercially, will enhance the development of alkali-
activated materials. The development of supersonic shockwave reactors will enable
the conversion of a wide range of virgin and secondary source materials into
cementitious materials, replacing blast furnace slag and coal fly ash that have
dwindling supply. A major obstacle to the commercial adoption of low-CO2 concrete
is the prescriptive nature of existing standards and design codes, so there is an
urgent need to shift towards performance-based standards. The roadmap presented
here is not an extension of current cement practice, but a new way of integrating
fundamental research, equipment innovation, and commercial opportunity.
[GRAPHICS]
.
C1 [van Deventer, Jannie S. J.] Zeobond Pty Ltd, POB 23450, Docklands, Vic 8012,
Australia.
[van Deventer, Jannie S. J.] Univ Melbourne, Dept Chem Engn, Melbourne, Vic
3010, Australia.
[White, Claire E.] Princeton Univ, Andlinger Ctr Energy & Environm, Dept Civil &
Environm Engn, Princeton, NJ 08544 USA.
[Myers, Rupert J.] Imperial Coll London, Dept Civil & Environm Engn, London,
England.
C3 University of Melbourne; Princeton University; Imperial College London
RP van Deventer, JSJ (corresponding author), Zeobond Pty Ltd, POB 23450, Docklands,
Vic 8012, Australia.; van Deventer, JSJ (corresponding author), Univ Melbourne,
Dept Chem Engn, Melbourne, Vic 3010, Australia.
EM jannie@zeobond.com; whitece@princeton.edu; r.myers@imperial.ac.uk
RI White, Claire E/A-1722-2011; Myers, Rupert Jacob/H-8449-2019
OI White, Claire E/0000-0002-4800-7960; Myers, Rupert
Jacob/0000-0001-6097-2088; Van Deventer, Jannie/0000-0001-7783-9398
FU Engineering and Physical Sciences Research Council of the U.K.
[EP/S006079/1]; EPSRC [EP/R010161/1]; UKCRIC Coordination Node, EPSRC
[EP/R017727/1]; MRSEC Center from the National Science Foundation, USA
[DMR-1420541]; [1362039]; [1553607]; EPSRC [EP/R017727/1,
EP/S006079/2, EP/S006079/1] Funding Source: UKRI
FX RJM acknowledges funding provided by the Engineering and Physical
Sciences Research Council of the U.K. (EP/S006079/1). The research
leading to this publication benefitted from EPSRC funding under Grant
No. EP/R010161/1 and from support from the UKCRIC Coordination Node,
EPSRC grant number EP/R017727/1, which funds UKCRIC's ongoing
coordination. CEW acknowledges financial support from Grant os. 1362039
and 1553607 and the MRSEC Center (Grant No. DMR-1420541) from the
National Science Foundation, USA. Access to the Princeton Institute for
Computational Science and Engineering (PICSciE) and the Office of
Information Technology's High Performance Computing Center and
Visualization Laboratory at Princeton University is acknowledged.
Unpublished pore structure and permeability data were obtained and
analysed by Kengran Yang, Anna Blyth and Bridget Zakrzewski (Princeton
University).
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NR 216
TC 16
Z9 16
U1 1
U2 34
PU SPRINGER
PI DORDRECHT
SN 1877-2641
EI 1877-265X
PD SEP
PY 2021
VL 12
IS 9
SI SI
BP 4745
EP 4775
DI 10.1007/s12649-020-01180-5
EA AUG 2020
PG 31
GA TR1AW
UT WOS:000557738100001
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Gruszczynski, M
Lenart, M
AF Gruszczynski, Maciej
Lenart, Malgorzata
TI Durability of mortars modified with the addition of amorphous aluminum
silicate and silica fume
SO THEORETICAL AND APPLIED FRACTURE MECHANICS
LA English
DT Article
DE Cement mortar; Shrinkage; Strength; Freeze-thaw resistance; Water
absorption; Amorphous aluminum silicate; Silica fume
ID BLAST-FURNACE SLAG; FLY-ASH; COMPRESSIVE STRENGTH; CEMENTITIOUS
MATERIALS; PARTIAL REPLACEMENT; CONCRETE; PERFORMANCE; BEHAVIOR; CEMENTS
AB In modern concrete technology, the use of various types of additives and
admixtures is standard. They not only affect the mechanical properties of cement
composites but also significantly facilitate the formation of a concrete mix. The
paper presents the effect of the content of silica fume (SF) and an amorphous
aluminum silicate (AAS) on selected properties of cement mortars, such as flexural
and compressive strength, water absorption, freeze-thaw resistance, and shrinkage.
The dynamics of strength development, determined after 7, 28, and 90 days of
maturing of test samples, are also presented in the paper. Mortars modified with
the addition of amorphous aluminum silicate in amounts of 5% and 10% of the cement
mass exhibited increased flexural strength within the range of 25-30% in comparison
with standard mortar and mortar modified with the addition of SF of the same
amount. In the case of compressive strength, both additives resulted in similar
increases in the strength within the whole maturation period. The freeze-thaw
resistance tests showed that the mortars with the addition of AAS were the most
resistant to variable freezing and thawing cycles, in relation both to the control
mortar and to the mortar modified by SF. The application of AAS resulted in a
significant reduction of shrinkage strain (by more than twice) in comparison with
mortars prepared with the analogous amount of silica fume.
C1 [Gruszczynski, Maciej; Lenart, Malgorzata] Cracow Univ Technol, Ul Warszawska
24, PL-31155 Krakow, Poland.
C3 Cracow University of Technology
RP Gruszczynski, M (corresponding author), Cracow Univ Technol, Ul Warszawska 24,
PL-31155 Krakow, Poland.
EM mgruszczynski@pk.edu.pl
RI Lenart, Malgorzata/AAF-4901-2019
OI Lenart, Malgorzata/0000-0002-0698-4835
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NR 44
TC 16
Z9 16
U1 2
U2 11
PU ELSEVIER
PI AMSTERDAM
SN 0167-8442
EI 1872-7638
J9 THEOR APPL FRACT MEC
JI Theor. Appl. Fract. Mech.
PD JUN
PY 2020
VL 107
AR 102526
DI 10.1016/j.tafmec.2020.102526
PG 8
WC Engineering, Mechanical; Mechanics
SC Engineering; Mechanics
GA LG3MD
UT WOS:000528008200011
DA 2023-12-05
ER
PT J
AU Xu, B
Chen, SJ
Tashiro, S
Jiang, F
Nguyen, VA
Tanaka, M
AF Xu, Bin
Chen, Shujun
Tashiro, Shinichi
Jiang, Fan
Van Anh Nguyen
Tanaka, Manabu
TI Material flow analyses of high-efficiency joint process in VPPA keyhole
flat welding by X-ray transmission system
LA English
DT Article
DE Environment-friendly; VPPA welding; Three-dimensional keyhole detouring
flow; X-ray observation; Flow velocity measurement
ID NUMERICAL-SIMULATION; ALUMINUM-ALLOY; PLASMA; POOL; MICROSTRUCTURE;
MECHANISM; GMAW
AB The consideration of environment-friendly and low energy consumption tends to
control and guide the progress of metal joint manufacturing processes. Variable
polarity plasma arc (VPPA) welding is an environment-friendly, high quality and
efficiency joint method for aluminum alloys due to its characteristics of such as
little welding fume, and high energy density etc. However, the three-dimensional
morphology and physical phenomena of penetration weld pool in VPPA welding are not
clearly understood, which slows down its process development and optimization. This
work aims to clarify the three-dimensional keyhole detouring flow of VPPA welding
for aluminum alloy. The liquid metal distribution of penetration weld pool was
generally obtained by metallographic observation. The measurement results show that
the liquid metal layer attached to the three-dimensional keyhole boundary is thin.
And the liquid metal mainly distributes in the bottom side of the keyhole. In order
to understand the weld pool dynamics, the stereo synchronous imaging of tungsten
tracer particles using two sets of X-ray transmission system was adopted, for the
first time, to measure the 3D velocity field of convection flow inside weld pool of
VPPA welding of aluminum alloy in real time. The flow on the weld pool surface at
different locations of keyhole boundary was also measured by tracing zirconia and
slag particles. The liquid metal flows simultaneously to the top and around the
keyhole. The metal at the bottom of keyhole's front wall, flows around the keyhole
towards the backside, then separately flows to top side and bottom side, forming a
vertical stationary point. The key to weld and avoid defect proofing are to ensure
stable detouring flow on the keyhole bottom and proper stationary point position.
C1 [Xu, Bin; Chen, Shujun; Jiang, Fan] Beijing Univ Technol, Engn Res Ctr Adv Mfg
Technol Automot Components, Minist Educ, Beijing 100124, Peoples R China.
[Xu, Bin; Tashiro, Shinichi; Van Anh Nguyen; Tanaka, Manabu] Osaka Univ, Joining
& Welding Res Inst, Osaka 5670047, Japan.
[Xu, Bin] Shandong Jianzhu Univ, Sch Mat Sci & Engn, Jinan 250101, Peoples R
China.
[Van Anh Nguyen] Murata Welding Labs Ltd, Yodogawaku 4-6-11, Osaka 5320012,
Japan.
C3 Beijing University of Technology; Osaka University; Shandong Jianzhu
University
RP Tashiro, S (corresponding author), Osaka Univ, Joining & Welding Res Inst, Osaka
5670047, Japan.
EM tashiro@jwri.osaka-u.ac.jp
RI NGUYEN, VAN ANH/AAY-8164-2021; Van, Anh/AAO-8149-2020
OI NGUYEN VAN, ANH/0000-0002-1670-2328
FU National Natural Science Foundation of China [51875004]; Beijing Natural
Science Foundation [3172004]; China Scholarship Council (CSC);
International Research Cooperation Seed Fund of Beijing University of
Technology [2018B16]; open project of Beijing Engineering Researching
Center of Laser Technology [BG0046-2018-09]; Beijing University of
Technology
FX This work is Supported by National Natural Science Foundation of China
(No.51875004), Beijing Natural Science Foundation (3172004), the China
Scholarship Council (CSC) for one-year study in Osaka University for Bin
Xu, the China Scholarship Council (CSC) for one-year study in University
of Alberta for Fan Jiang, International Research Cooperation Seed Fund
of Beijing University of Technology (No. 2018B16), the open project of
Beijing Engineering Researching Center of Laser Technology
(BG0046-2018-09) and start-up funding from Beijing University of
Technology.
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Zukauskaite A., 2013, TRANSP MEANS 17 INT
NR 48
TC 16
Z9 17
U1 2
U2 23
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD MAR 20
PY 2020
VL 250
AR 119450
DI 10.1016/j.jclepro.2019.119450
PG 15
& Ecology
GA KE8WO
UT WOS:000508829800063
DA 2023-12-05
ER
PT J
AU Ji, WX
Zhang, SY
Zhao, PD
Zhang, SS
Feng, N
Lan, LP
Zhang, XG
Sun, YG
Li, YY
Ma, YL
AF Ji, Wenxin
Zhang, Shiyue
Zhao, Pengde
Zhang, Shasha
Feng, Ning
Lan, Liping
Zhang, Xiaoguang
Sun, Yonggang
Li, Yuanyuan
Ma, Yulong
TI Green Synthesis Method and Application of NaP Zeolite Prepared by Coal
Gasification Coarse Slag from Ningdong, China
SO APPLIED SCIENCES-BASEL
LA English
DT Article
DE coal gasification coarse slag; NaP zeolite; ammonia nitrogen; green
environmental
ID FLY-ASH; AMMONIA-NITROGEN; AQUEOUS-SOLUTIONS; RESIDUAL CARBON; FAUJASITE
BLOCK; SURFACE-AREA; REMOVAL; ADSORPTION; SILICA; ZSM-5
AB In view of the current and urgent environmental protection needs, the use of
industrial solid waste in China's Ningdong is becoming more and more important. In
this paper, NaP zeolite with good physical properties is synthesized by using coal
gasification coarse slag (CGCS) as the raw material, without the addition of a
silicon and aluminum source, without the addition of a template agent, and without
high-temperature calcination. Add a small amount of NaOH and deionized water to the
CGCS to adjust the molar ratio to SiO2:Al2O3:Na2O:H2O = 5.2:1.0:5.0:100. The
effects of aging time, crystallization temperature, and crystallization time
parameters on synthetic zeolite were studied. The raw materials and the obtained
zeolite were tested by XRF, XRD, SEM, FT-IR, TG-DSC, BET, and other technologies.
The results show that the specific surface area of the synthesized NaP zeolite can
reach 161.06 m(2)/g, which has the characteristics of large specific surface area,
regular morphology, and high crystallinity. We obtained NaP zeolite through a
simple and low-cost synthesis method. The synthesized NaP zeolite was used to
simulate the removal of ammonia nitrogen in wastewater, and the optimal removal
rate was 92.67%. Among them, Na+ plays an important role in the synthesis of NaP
zeolite and ion exchange with NH4+. Our research provides new ideas for solving the
large-scale accumulation of CGCS and treating ammonia nitrogen in industrial
wastewater. Thus, it is a promising green environmental protection and "treating
waste by waste" route.
C1 [Ji, Wenxin; Zhang, Shiyue; Zhao, Pengde; Feng, Ning; Sun, Yonggang; Li,
Yuanyuan; Ma, Yulong] Ningxia Univ, State Key Lab High Efficiency Utilizat Coal &
Gre, Yinchuan 750021, Ningxia, Peoples R China.
[Ji, Wenxin; Zhang, Shasha; Lan, Liping; Zhang, Xiaoguang; Sun, Yonggang; Li,
Yuanyuan; Ma, Yulong] Ningxia Univ, Coll Chem & Chem Engn, Yinchuan 750021,
Ningxia, Peoples R China.
C3 Ningxia University; Ningxia University
RP Ji, WX (corresponding author), Ningxia Univ, State Key Lab High Efficiency
Utilizat Coal & Gre, Yinchuan 750021, Ningxia, Peoples R China.; Ji, WX; Zhang, XG
(corresponding author), Ningxia Univ, Coll Chem & Chem Engn, Yinchuan 750021,
Ningxia, Peoples R China.
EM jwx@nxu.edu.cn; ndzhangxg@126.com
RI li, yuanyuan/GZA-4435-2022
FU National Science Foundation of China [21663019]; East-West Cooperation
Project of Ningxia Key R D Plan [2019BFH02014]
FX This research was funded by The National Science Foundation of China
(No. 21663019) and The East-West Cooperation Project of Ningxia Key R &
D Plan (2019BFH02014).
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NR 51
TC 16
Z9 17
U1 14
U2 121
PU MDPI
PI BASEL
EI 2076-3417
J9 APPL SCI-BASEL
JI Appl. Sci.-Basel
PD FEB
PY 2020
VL 10
IS 8
AR 2694
DI 10.3390/app10082694
PG 15
WC Chemistry, Multidisciplinary; Engineering, Multidisciplinary; Materials
Science, Multidisciplinary; Physics, Applied
SC Chemistry; Engineering; Materials Science; Physics
GA LO0XE
UT WOS:000533352100058
OA gold
DA 2023-12-05
ER
PT J
AU Walkley, B
Page, SJ
Rees, GJ
Provis, JL
Hanna, JV
AF Walkley, Brant
Page, Samuel J.
Rees, Gregory J.
Provis, John L.
Hanna, John V.
TI Nanostructure of
CaO-(Na2O)-Al2O3-SiO2-H
2O Gels Revealed by Multinuclear Solid-State Magic Angle Spinning
and Multiple Quantum Magic Angle Spinning Nuclear Magnetic Resonance
Spectroscopy
SO JOURNAL OF PHYSICAL CHEMISTRY C
LA English
DT Article
ID C-S-H; ALKALI-ACTIVATED SLAG; HYDRATED PORTLAND CEMENTS; LAYERED DOUBLE
HYDROXIDES; CALCIUM-SILICATE; MAS NMR; ALUMINUM INCORPORATION; PHASE
EVOLUTION; O-17 MAS; ALUMINOSILICATE GLASSES
AB (Calcium,alkali)-aluminosilicate gel frameworks are the basis of modern cements
and alkali-activated materials for sustainable infrastructure and radioactive waste
immobilization and also find application in glass alteration, mineral weathering,
and zeolite synthesis. Here, we resolve the nanostructure of these gels that
dictates mass transport, solubility, and mechanical properties. The key structural
motifs comprising hydrous (calcium,alkali)-aluminosilicate gels are identified via
O-17, Na-23, and Al-27 triple-quantum magic angle spinning and( 29)Si magic angle
spinning nuclear magnetic resonance spectroscopy of a novel class of
stoichiometrically controlled O-17-enriched multiphase gels. Increased Ca content
promotes low-Al, high-Ca chain- structured "C-S-H-type" products exhibiting
significant nanostructural ordering, low levels of chain cross-linking, predominant
Ca coordination of nonbridging oxygen atoms, and an increase in proton association
with CaO layers to form Ca-OH sites. Al substitution is identified in multiple
sites in the silicate chains, including cross-linking, bridging, and pairing
tetrahedra. Increased Al content increases the proportion of cross-linking sites
and gel disorder. The large increase in Si-IV-O-Al-IV sites increases the relative
amounts of Na+ and Al-V species charge-balancing AlO4- tetrahedra and results in
the formation of an additional disordered low-calcium, framework-structured alkali
aluminosilicate ("N-A-S-H-type") gel, with high Al and Na contents. Changes in bulk
composition significantly alter the nanostructures of the C-S-H-type and N-A-S-H-
type gels. Mean Si-IV-O-Al-IV bond angles for each type of Al-IV site environment
are highly consistent, with compositional changes dictating the relative
proportions of individual Al-IV species but not altering the local structure of
each Al-IV site. These findings reveal the molecular interactions governing the
(calcium,alkali)-aluminosilicate gel nanostructure, which are crucial in
controlling material properties and durability.
C1 [Walkley, Brant; Provis, John L.] Univ Sheffield, Dept Mat Sci & Engn, Sheffield
S1 3JD, S Yorkshire, England.
[Walkley, Brant] Univ Sheffield, Dept Chem & Biol Engn, Sheffield S1 3JD, S
Yorkshire, England.
[Page, Samuel J.; Rees, Gregory J.; Hanna, John V.] Univ Warwick, Dept Phys,
Coventry CV4 7AL, W Midlands, England.
C3 University of Sheffield; University of Sheffield; University of Warwick
RP Hanna, JV (corresponding author), Univ Warwick, Dept Phys, Coventry CV4 7AL, W
Midlands, England.
EM j.v.hanna@warwick.ac.uk
RI Rees, Gregory/AAQ-8688-2021; Provis, John L/A-7631-2008; Provis,
John/AAR-3260-2020
OI Rees, Gregory/0000-0002-7514-1516; Provis, John L/0000-0003-3372-8922;
Provis, John/0000-0003-3372-8922; Walkley, Brant/0000-0003-1069-1362;
Hanna, John/0000-0002-0644-3932
FU Australian Research Council (ARC) through an Australian Postgraduate
Award; Particulate Fluids Processing Centre, a Special Research Centre
of the ARC; Engineering and Physical Sciences Research Council (UK)
[EP/M003272/1]; EPSRC; BBSRC; University of Warwick; Birmingham Science
City Advanced Materials Project 1; Birmingham Science City Advanced
Materials Project 2; Advantage West Midlands; European Regional
Development Fund; EPSRC [EP/I004114/1, EP/G009511/1, EP/M004511/1,
EP/M003272/1, EP/P013171/1] Funding Source: UKRI
(ARC) through an Australian Postgraduate Award to B.W., as well as
support through the Particulate Fluids Processing Centre, a Special
Research Centre of the ARC. The University of Melbourne also provided
support through an Overseas Research Experience Scholarship to support
an extended visit of B.W. to the University of Sheffield. B.W. wishes to
thank and acknowledge Dr. John Gehman for very helpful discussions
regarding biaxial shearing of the 3QMAS NMR spectra. The participation
of J.L.P. has been supported by the Engineering and Physical Sciences
Research Council (UK) through grant EP/M003272/1. The NMR Facility in
Millburn House used in this research was funded by EPSRC, BBSRC, and the
University of Warwick and the Birmingham Science City Advanced Materials
Projects 1 and 2 and supported by Advantage West Midlands and the
European Regional Development Fund.
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NR 70
TC 16
Z9 17
U1 3
U2 39
PI WASHINGTON
SN 1932-7447
EI 1932-7455
J9 J PHYS CHEM C
JI J. Phys. Chem. C
PD JAN 16
PY 2020
VL 124
IS 2
BP 1681
EP 1694
DI 10.1021/acs.jpcc.9b10133
PG 14
WC Chemistry, Physical; Nanoscience & Nanotechnology; Materials Science,
Multidisciplinary
GA KE3OD
UT WOS:000508467700051
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Wu, JN
Lv, JW
Shang, JW
Guo, Y
Pu, GY
AF Wu Junnian
Lv Jingwen
Shang Jiangwei
Guo Yan
Pu Guangying
TI Evaluating chromium coupled with carbon metabolism and environmental
performance in the chromate industrial symbiosis network in China
LA English
DT Article
DE Industrial symbiosis (IS); Ecological network analysis (ENA); Chromium
metabolism; Carbon metabolism; Chromate industrial symbiosis network
ID INPUT-OUTPUT-ANALYSIS; PARK; FOOTPRINT; URBAN; PERSPECTIVE; CONSUMPTION;
EFFICIENCY; ECONOMY; SYSTEM
AB The pollution of toxic and carcinogenic chromium slags of the chromate industry
has been a public concern and industrial symbiosis is proved to be feasible and
efficient in recycling chromium slags. How to appraise and improve sustainability
of chromate industrial symbiosis networks is still an open problem where functional
and structural performance are key approaches to solve. This paper aims to explore
chromium and carbon metabolic behavior of a chromate industrial symbiosis network
with ecological network analysis at infra-firm level. Results show that industrial
symbiosis reduces chromium slags emissions and improves resource utilization
efficiency. Influenced by flow type and quantity, the chromium metabolism realizes
mutualism but the carbon metabolism fails due to intense competition for carbon
resource among the recycling processes (the aluminum hydroxide, sodium sulfide and
alloy steel processes). The sodium dichromate process is the largest controller on
the chromium and carbon metabolism and the sodium sulfide and alloy steel processes
both rely on carbon resource support of the sodium dichromate process even to 100%
which may explain the intense competition. Under disharmonious connection pattern
of metabolic processes, structural defects both occur to the chromium and carbon
metabolism. Even though, the chromium metabolism is closed to the stable condition
while the carbon metabolism still requires more network efficiency. Overall, the
combination of chromium and carbon metabolism provide more details in exploring
metabolic behavior of the chromate industrial symbiosis network. The applied method
may be helpful to refine management and optimization in developing industrial
symbiosis.
C1 [Wu Junnian; Lv Jingwen; Shang Jiangwei; Guo Yan; Pu Guangying] Lanzhou Univ,
Coll Earth & Environm Sci, Gansu Key, Lab Environm Pollut Predict & Control,
Lanzhou 730000, Gansu, Peoples R China.
C3 Lanzhou University
RP Wu, JN (corresponding author), Lanzhou Univ, Coll Earth & Environm Scientes,
Lanzhou, Gansu, Peoples R China.
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NR 47
TC 16
Z9 16
U1 8
U2 84
PU ELSEVIER
PI AMSTERDAM
SN 0921-3449
EI 1879-0658
PD OCT
PY 2019
VL 149
BP 188
EP 196
DI 10.1016/j.resconrec.2019.05.016
PG 9
GA IU2MK
UT WOS:000483414300019
DA 2023-12-05
ER
PT J
AU Buvignier, A
Patapy, C
Lavigne, MP
Paul, E
Bertron, A
AF Buvignier, Amaury
Patapy, Cedric
Lavigne, Matthieu Peyre
Paul, Etienne
Bertron, Alexandra
TI Resistance to biodeterioration of aluminium-rich binders in sewer
network environment: Study of the possible bacteriostatic effect and
role of phase reactivity
LA English
DT Article
DE Durability (C); Calcium aluminate cement (D); Portland cement (D);
Ground Granulated blast-furnace slag (D); Waste management (E)
ID INDUCED CONCRETE CORROSION; SULFURIC-ACID CORROSION; CEMENT PASTES;
MICROBIAL CORROSION; ORGANIC-ACIDS; DEGRADATION; DETERIORATION;
PERFORMANCE; OXIDATION; BACTERIA
AB This paper aims to better understand the mechanisms explaining the superior
resistance of calcium aluminate cement (CAC) materials compared to Portland cement
(PC) based materials in sewer networks. The bacteriostatic effect of CAC materials
on Sulfur Oxidising Bacteria (SOB) is often argued in the literature as a possible
mechanism explaining their better resistance. Reactor tests conducted on SOB
demonstrated their ability to acclimatise to high aluminium contents. More
generally, using a laboratory biodeterioration protocol reproducing aggressive
conditions, the nature of the material (CAC or PC with different slag contents) did
not significantly affect the SOB selection. Moreover the CAC materials seemed to
favour the development of a higher SOB activity (and so acid production) than PC-
based systems, leading to more aggressive conditions. Finally, the resistance of
CAC materials to biodeterioration appeared to be mainly linked to the intrinsic
resistance of phases initially present or precipitated during the deterioration
process.
C1 [Buvignier, Amaury; Lavigne, Matthieu Peyre; Paul, Etienne] Univ Toulouse, CNRS,
INRA, INSA,LISBP, 135 Ave Rangueil, F-31077 Toulouse, France.
[Buvignier, Amaury; Patapy, Cedric; Bertron, Alexandra] Univ Toulouse, INSA,
UPS, LMDC, 135 Ave Rangueil, F-31077 Toulouse, France.
C3 Universite de Toulouse; Universite Federale Toulouse Midi-Pyrenees
(ComUE); Institut National des Sciences Appliquees de Toulouse; Centre
National de la Recherche Scientifique (CNRS); INRAE; Universite de
Toulouse; Universite Toulouse III - Paul Sabatier; Universite Federale
Toulouse Midi-Pyrenees (ComUE); Institut National des Sciences
Appliquees de Toulouse
RP Bertron, A (corresponding author), Univ Toulouse, INSA, UPS, LMDC, 135 Ave
Rangueil, F-31077 Toulouse, France.
EM bertron@insa-toulouse.fr
RI Bertron, Alexandra/G-3418-2018
OI Bertron, Alexandra/0000-0002-6144-6810
FU Research Centre of Saint-Gobain Pont-a-Mousson; Institut Universitaire
de France
FX This work was funded by the Research Centre of Saint-Gobain
Pont-a-Mousson. The authors also would like to thank Institut
Universitaire de France (Research grant of A. Bertron, junior member
2016-2021) for complementary funding. The authors gratefully acknowledge
the technical staff for the experimental set up and help in the
analyses: Evrard Mengel, Maud Shiettekatte, Vanessa Mazars, and
Guillaume Lambare. The authors thank Laurent Steger and Sandrine
Geoffroy for their help with the image analysis procedure. Ecocem Ltd,
Imerys and Lafarge-Holcim are acknowledged for the supply of materials.
The authors also thank Myriam Mercade and Marie-Line de Solan Bethmale
for their assistance in the biofilm observation, and all those who
helped in the achievement of this project.
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TC 16
Z9 16
U1 1
U2 16
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD SEP
PY 2019
VL 123
AR 105785
DI 10.1016/j.cemconres.2019.105785
PG 14
GA IZ6EB
UT WOS:000487173500018
DA 2023-12-05
ER
PT J
AU Gao, JQ
Li, C
Liu, WZ
Hu, JP
Wang, L
Liu, Q
Liang, B
Yue, HR
Zhang, GQ
Luo, DM
Tang, SY
AF Gao, Jianqiu
Li, Chun
Liu, Weizao
Hu, Jinpeng
Wang, Lin
Liu, Qiang
Liang, Bin
Yue, Hairong
Zhang, Guoquan
Luo, Dongmei
Tang, Siyang
TI Process simulation and energy integration in the mineral carbonation of
blast furnace slag
LA English
DT Article
DE Blast furnace slag; Mineral carbonation; Process simulation and energy
integration; Utilization of solid residuals; Ammonium alum; Ammonium
sulfate
ID WASTE HEAT-RECOVERY; CO2 SEQUESTRATION; AMMONIUM BISULFATE;
INDUSTRIAL-WASTE; SILICATE ROCK; STEEL SLAG; CHINA IRON; CAPTURE;
OPTIMIZATION; DISSOLUTION
AB Large quantities of blast furnace (BF) slag and CO2 are discharged annually from
iron and steel industries, along with a large amount of waste heat. The mineral
carbonation of BF slag can not only reduce emissions of solid waste but also
realize the in-situ fixation of CO2 with low energy consumption if integrated with
the waste heat utilization. In this study, based on our previous works, Aspen Plus
was employed to simulate and optimize the carbonation process and integrate the
process energy. The effects of gehlenite extraction, MgSo(4) carbonation, and
aluminum ammonium sulfate crystallization were studied systematically. The
simulation results demonstrate that 2.57 kg of BF slag can sequester 1 kg of CO2,
requiring 5.34 MJ of energy (3.3 MJ heat and 2.04 MJ electricity), and this energy
includes the capture of CO2 from industrial flue gases. Approximately 60 kg net CO2
emission reduction could be achieved for the disposal of one ton of BF slag. In
addition, the by-product, aluminum ammonium sulfate, is a high value-added product.
Preliminary economic analysis indicates that the profit for the whole process is
1127 CNY per ton of BF slag processed. (C) 2018 The Chemical Industry and
Engineering Society of China, and Chemical Industry Press. All rights reserved.
C1 [Gao, Jianqiu; Li, Chun; Liu, Weizao; Hu, Jinpeng; Wang, Lin; Liu, Qiang; Liang,
Bin; Yue, Hairong; Zhang, Guoquan; Luo, Dongmei; Tang, Siyang] Sichuan Univ, Sch
Chem Engn, Chengdu 610065, Sichuan, Peoples R China.
RP Tang, SY (corresponding author), Sichuan Univ, Sch Chem Engn, Chengdu 610065,
EM siyangtang@scu.edu.cn
RI Liang, Bin/JHU-0581-2023; Liu, Weizao/K-5038-2019; yue,
Hairong/D-1874-2013
OI Liu, Weizao/0000-0003-0976-2864;
[2016YFB0600904]
FX Supported by the National Key Projects for Fundamental Research and
Development of China (2016YFB0600904).
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NR 56
TC 16
Z9 18
U1 1
U2 56
PU CHEMICAL INDUSTRY PRESS
PI BEIJING
PA NO. 3 HUIXINLI CHAOYANGQU, BEIJING 100029, PEOPLES R CHINA
SN 1004-9541
EI 2210-321X
PD JAN
PY 2019
VL 27
IS 1
BP 157
EP 167
DI 10.1016/j.cjche.2018.04.012
PG 11
SC Engineering
GA HI4RI
UT WOS:000456437800017
DA 2023-12-05
ER
PT J
AU Hou, D
Jiang, ZH
Qu, TP
Wang, DY
Liu, FB
Li, HB
AF Hou, Dong
Jiang, Zhou-hua
Qu, Tian-peng
Wang, De-yong
Liu, Fu-bin
Li, Hua-bing
TI Aluminum, titanium and oxygen control during electroslag remelting of
stainless steel based on thermodynamic analysis
LA English
DT Article
DE Electroslag remelting; Titanium control; Aluminum control; Oxygen
control; Stainless steel; Thermodynamic analysis; Ion and molecule
coexistence theory
ID MICROSTRUCTURE EVOLUTION; OXIDATION-KINETICS; ALLOYING ELEMENTS; SLAG
COMPOSITION; DEOXIDATION; INCLUSION; SILICON
AB Experimental investigation and thermodynamic calculation were carried out to
study the effect of slag on alloying elements during electroslag remelting with
developing a thermodynamic model to control titanium and aluminum in ingot. The
thermodynamic model based on ion and molecule coexistence theory and conservation
law of element atoms was established to analyze the change in aluminum and titanium
along the height of ingot. The results show that low CaO slag is suitable for
electroslag remelting of metal containing high titanium-to-aluminum ratio. As
electroslag remelting process consists of slag temperature-rising and temperature-
stable periods, TiO2 should be added into water-cooled copper mold during
temperature-rising period in order to keep the thermodynamic equilibrium between
titanium and aluminum, and the amount of TiO2 is the difference value calculated by
the reaction between titanium and alumina at 1477 and 1677 degrees C.
C1 [Hou, Dong; Qu, Tian-peng; Wang, De-yong] Soochow Univ, Sch Iron & Steel, Suzhou
[Hou, Dong; Jiang, Zhou-hua; Liu, Fu-bin; Li, Hua-bing] Northeastern Univ, Sch
Met, Shenyang 110819, Liaoning, Peoples R China.
[Wang, De-yong] State Key Lab Refractories & Met, Wuhan 430000, Hubei, Peoples R
China.
C3 Soochow University - China; Northeastern University - China
RP Qu, TP (corresponding author), Soochow Univ, Sch Iron & Steel, Suzhou 215021,
Jiangsu, Peoples R China.; Jiang, ZH (corresponding author), Northeastern Univ, Sch
Met, Shenyang 110819, Liaoning, Peoples R China.
EM jiangzh@smm.neu.edu.cn; qutianpeng@suda.edu.cn
RI 李, 花兵/IQU-2254-2023
OI 李, 花兵/0000-0002-4182-9486; Jiang, Zhouhua/0000-0001-8887-7250
FU National Natural Science Foundation of China [51674070, U1560203,
51674172]; Natural Science Foundation of Jiangsu Province [BK20150334,
20150336]; Open Foundation of The State Key Laboratory of Refractories
and Metallurgy [G201607]
FX This project is supported by the National Natural Science Foundation of
China (Grant Nos. 51674070, U1560203 and 51674172), the Natural Science
Foundation of Jiangsu Province (Grant Nos. BK20150334 and 20150336), and
the Open Foundation of The State Key Laboratory of Refractories and
Metallurgy (Grant No. G201607).
CR Chang LZ, 2009, J IRON STEEL RES INT, V16, P7, DOI 10.1016/S1006-706X(09)60052-2
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8
NR 25
TC 16
Z9 18
U1 0
U2 29
PU SPRINGER
PI NEW YORK
SN 1006-706X
EI 2210-3988
PD JAN
PY 2019
VL 26
IS 1
BP 20
EP 31
DI 10.1007/s42243-018-0107-2
PG 12
GA HM1HK
UT WOS:000459200900003
DA 2023-12-05
ER
PT J
AU Hou, ZW
Jiang, M
Yang, EJ
Gao, SY
Wang, XH
AF Hou, Ze-Wang
Jiang, Min
Yang, En-Jiao
Gao, Sheng-Ya
Wang, Xin-Hua
TI Inclusion Characterization in Aluminum-Deoxidized Special Steel with
Certain Sulfur Content Under Combined Influences of Slag Refining,
Calcium Treatment, and Reoxidation
LA English
DT Article
ID MGO-CENTER-DOT-AL2O3 SPINEL INCLUSIONS; EQUILIBRIUM-S DISTRIBUTION;
FORMATION MECHANISM; STAINLESS-STEEL; NONMETALLIC INCLUSIONS; ALLOYED
STEEL; AL; THERMODYNAMICS; DEOXIDATION; EVOLUTION
AB Inclusions in Al-killed steel with [S] of about 0.0060 to 0.0070 mass pct were
characterized and discussed, evaluating the combined effects of basic slag refining
and Ca treatment in ladle, together with reoxidation of liquid steel in casting
tundish. Inclusions were changed from Al2O3 to MgO-Al2O3 spinel and then to MgO-
Al2O3-CaO during basic slag refining. After Ca treatment, many (MgO-Al2O3)+CaS
inclusions were formed, featuring the coexistence of MgO-Al2O3 and CaS to form a
dual-phased structure. In the following Ar blowing, the number density of (MgO-
Al2O3)+CaS inclusions and pure CaS increased obviously, which implied that [Ca]
preferentially reacted with [S] rather than [O] in steel. Reoxidation in casting
tundish caused the pickup of oxygen in steel, and the rise of total oxygen (T.O)
was 0.0002mass pct; even 55t steel has been poured. As a result, the content of CaO
in inclusions increased and MgO-Al2O3-CaO inclusions were formed again.
Thermodynamic calculations revealed that the driving force was strong for the
formation of CaS-based inclusions. Higher carbon content in steel would help to
reduce oxygen content while enhancing the activity of [S] in steel, which further
stabilized the existence of CaS-based inclusions. Therefore, inclusions were mostly
the solid (MgO-Al2O3)+CaS dual-phase ones, without the formation of liquid calcium
aluminates. Contents of CaS and CaO in inclusions were affected by the [mass pct
S]/[mass pct O] ratio, which was calculated as about 4.58K and 5.34K at 1873K and
1823K, respectively. This finding implied that lower oxygen was not favorable to
prevent the solid inclusions in the calcium treatment of high carbon special steel.
C1 [Hou, Ze-Wang; Jiang, Min; Yang, En-Jiao; Gao, Sheng-Ya; Wang, Xin-Hua] Univ Sci
& Technol Beijing, Sch Met & Ecol Engn, Beijing, Peoples R China.
Engn, Beijing, Peoples R China.
RI Wang, Xin/JCE-2009-2023; Wang, Xin/HZL-4695-2023; Wang,
Xinhua/ISR-8520-2023; Wang, Xin/AAN-8435-2021; Wang,
Xiaoqiang/IQS-3727-2023; Wang, Xin/GYU-1129-2022
OI Wang, Xin/0000-0002-4457-7376; Wang, Xin/0000-0002-4457-7376;
FU China National Science Funding [51304013]
FX The authors are thankful for the support of China National Science
Funding (Grant No. 51304013) during this research.
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Ye G., 1996, ISIJ INT, pS105
Zhang XW, 2017, METALL MATER TRANS B, V48, P701, DOI 10.1007/s11663-016-0833-4
NR 53
TC 16
Z9 17
U1 1
U2 34
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD DEC
PY 2018
VL 49
IS 6
BP 3056
EP 3066
DI 10.1007/s11663-018-1365-x
PG 11
Engineering
GA HC2QV
UT WOS:000451647900012
DA 2023-12-05
ER
PT J
AU Zhang, GZ
Wang, N
Chen, M
Li, H
AF Zhang, Guangzong
Wang, Nan
Chen, Min
Li, Hui
TI Viscosity and Structure of
CaO-SiO2-"FeO"-Al2O3-MgO System during
Iron-Extracting Process from Nickel Slag by Aluminum Dross. Part 1:
Coupling Effect of "FeO" and Al2O3
LA English
DT Article
DE aluminum dross; "FeO"/Al2O3 ratio; nickel slag; slag structure;
viscosity
ID FURNACE TYPE SLAGS; AMPHOTERIC BEHAVIOR; SILICATE-GLASSES;
RAMAN-SPECTRA; MELTS; RATIO; MGO; CRYSTALLIZATION; PREDICTION; BASICITY
AB Nickel slag can be recycled as one of excellent secondary sources due to
valuable amounts of iron contents. Viscosity of CaO-SiO2-FeO-Al2O3-MgO slag system
during iron-extracting process from nickel slag by aluminum dross is investigated
from 1723 to 1873K. Evolution of viscosity and structure are studied with FeO/Al2O3
ratio decreasing from 1.69 to 0.48. Under the coupling effect of FeO and Al2O3, the
viscosity increases slowly before the reduction degree of 60% following by a
significant increase. Structure investigation shows that Al2O3 is always acting as
the network former, and the transition of dominant role from FeO to Al2O3 not only
leads to the disappearance of structural unit Q(0) in Raman spectra, but also the
occurrence of more complex unit Q(3), signifying an evident increase in the degree
of polymerization (DOP) of the slag. Additionally, the viscosity evolution during
the reduction process is calculated upon the non-isothermal thermodynamic model.
C1 [Zhang, Guangzong; Wang, Nan; Chen, Min; Li, Hui] Northeastern Univ, Sch Met,
RP Wang, N (corresponding author), Northeastern Univ, Sch Met, Shenyang 110819,
EM wangn@smm.neu.edu.cn
RI Wang, Nan/JLL-3980-2023; Wang, Nan/GRY-3150-2022; Wang,
Nan/HLV-7836-2023
OI Guangzong, Zhang/0000-0002-1689-9386
51574065, 51774073]
FX The authors thanked National Natural Science Foundation of China for the
financial support of this work (Grant Nos. 51774072, 51574066, 51574065,
51774073).
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NR 48
TC 16
Z9 17
U1 0
U2 39
PI WEINHEIM
SN 1611-3683
EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD OCT
PY 2018
VL 89
IS 10
AR 1800272
DI 10.1002/srin.201800272
PG 8
GA GV6YZ
UT WOS:000446268500014
DA 2023-12-05
ER
PT J
AU Gu, C
Bao, YP
Gan, P
Lian, JH
Münstermann, S
AF Gu, Chao
Bao, Yan-Ping
Gan, Peng
Lian, Jun-He
Muenstermann, Sebastian
TI An Experimental Study on the Impact of Deoxidation Methods on the
Fatigue Properties of Bearing Steels
LA English
DT Article
DE aluminum; bearing steel; deoxidation method; silicon; very high cycle
fatigue
ID HIGH-CYCLE FATIGUE; AL-KILLED STEEL; CRACK INITIATION; OXIDE INCLUSIONS;
STAINLESS-STEELS; SLAG COMPOSITION; REFINING PROCESS; MOLTEN STEEL; TOP
SLAG; SI
AB Strong deoxidation and weak deoxidation are two kinds of deoxidation methods
frequently applied in steelmaking. In the present study, high-carbon chromium
bearing steels are smelted with a strong deoxidizer and a weak deoxidizer,
respectively in industrial trials. The generation mechanism of inclusions is
analyzed, and the inclusion stability diagrams of the Fe-Si-Al-Mg-Mn-O system at
1873 and 1843 K are calculated. The very high cycle fatigue life of bearing steels
deoxidized with different deoxidizers is also experimentally compared. The results
showed that the evolution routes of inclusion in high-carbon chromium bearing
steels deoxidized by Si and Al are CaO-Al2O3-SiO2 -> CaO-Al2O3-SiO2-MgO and Al2O3 -
> CaO-Al2O3-SiO2-MgO, respectively. The Al content in steel is controlled by
different methods when different deoxidizers are applied. The effect of the oxide
inclusions generated during Si deoxidization on the fatigue life is lower than that
during Al deoxidization, even if the total oxygen content is slightly higher. This
effect suggests that it is not accurate to evaluate the fatigue life of steels with
the total oxygen content, and it is also desirable to produce bearing steels with
the Si deoxidation method.
C1 [Gu, Chao; Bao, Yan-Ping; Gan, Peng] Univ Sci & Technol Beijing, State Key Lab
Adv Met, Beijing 100083, Peoples R China.
[Lian, Jun-He; Muenstermann, Sebastian] Rhein Westfal TH Aachen, Steel Inst,
Intzestr 1, D-52072 Aachen, Germany.
C3 University of Science & Technology Beijing; RWTH Aachen University
RP Bao, YP (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
EM 15210951549@sina.cn
RI Lian, Junhe/C-5492-2009; Münstermann, Sebastian/E-5480-2012
OI Lian, Junhe/0000-0003-0323-3486; Münstermann,
Sebastian/0000-0002-6251-2429; Gu, Chao/0000-0002-0668-4859
FU State Key Laboratory for Advanced Metallurgy Foundation [41614014];
FX This work was financially supported by the State Key Laboratory for
Advanced Metallurgy Foundation (No. 41614014) and Natural Science
Foundation of China (No. 51404018).
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468
2014-691
NR 34
TC 16
Z9 20
U1 5
U2 40
PI WEINHEIM
SN 1611-3683
EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD SEP
PY 2018
VL 89
IS 9
AR 1800129
DI 10.1002/srin.201800129
PG 8
GA GS4EQ
UT WOS:000443590100014
DA 2023-12-05
ER
PT J
AU Li, ZH
Peethamparan, S
AF Li, Zihui
Peethamparan, Sulapha
TI Leaching resistance of alkali-activated slag and fly ash mortars exposed
to organic acid
SO GREEN MATERIALS
LA English
DT Article
DE corrosion; material characterisation; mechanisms
ID CEMENT INDUSTRY; CARBON FOOTPRINT; PORTLAND-CEMENT; CONCRETE FLOORS; PIG
HOUSES; FEED ACIDS; ATTACK; GEOPOLYMER; REDUCTION; EMISSIONS
AB This paper presents a comprehensive evaluation of the leaching resistance of
alkali-activated mortar (AAM) in an organic, acetic acid environment in comparison
with ordinary Portland cement (OPC) mortars. Two AAMs, a ground granulated blast-
furnace slag mortar and a class C fly-ash-based mortar, and two OPC mortars were
exposed to pH = 3.2 and pH = 4.0 acetic acid solutions for 90 d. Residual
compressive strength and mass changes were determined periodically to quantify the
degree of degradation caused by the organic acid exposure. Additionally, a
microstructural investigation of the degradation was performed using scanning
electron microscopy and energy-dispersive X-ray spectroscopy in order to identify
the occurrence of microscale damage after acid exposure. The leachates were
analyzed at various soaking periods using inductively coupled plasma mass
spectrometry to determine the concentration of the leached calcium (Ca), silicon
(Si), aluminum (Al), sodium (Na), sulfur (S) and other related ions. The AAM
samples exhibited enhanced leaching resistance compared to traditional OPC mortars.
C1 [Li, Zihui; Peethamparan, Sulapha] Clarkson Univ, Dept Civil & Environm Engn,
Potsdam, NY 13699 USA.
C3 Clarkson University
RP Peethamparan, S (corresponding author), Clarkson Univ, Dept Civil & Environm
EM speetham@clarkson.edu
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NR 44
TC 16
Z9 16
U1 0
U2 21
PU ICE PUBLISHING
PI WESTMINISTER
SN 2049-1220
EI 2049-1239
J9 GREEN MATER
JI Green Mater.
PD SEP
PY 2018
VL 6
IS 3
BP 117
EP 130
AR UNSP 1800021
DI 10.1680/jgrma.18.00021
PG 14
WC Green & Sustainable Science & Technology; Materials Science,
Multidisciplinary; Polymer Science
SC Science & Technology - Other Topics; Materials Science; Polymer Science
GA GW4ZJ
UT WOS:000446935800004
DA 2023-12-05
ER
PT J
AU Qiu, BB
Deng, N
Zhang, YF
Wan, HJ
AF Qiu, Bingbing
Deng, Na
Zhang, Yufeng
Wan, Haijun
TI Application of industrial solid wastes in catalytic pyrolysis
SO ASIA-PACIFIC JOURNAL OF CHEMICAL ENGINEERING
LA English
DT Review
DE catalytic mechanism optimization; catalytic pyrolysis; industrial solid
wastes; parameters
ID RED MUD; BIO-OIL; BIOMASS GASIFICATION; FLY-ASH; LIGNIN PYROLYSIS;
TEMPERATURE; PRODUCT; CONVERSION; POLYPROPYLENE; RECOVERY
AB The catalytic pyrolysis is one of the thermochemical patterns for producing
chemical products consisting of solid char, liquid oil, and pyrolytic gas. A number
of parameters affecting the catalytic pyrolysis process, yields, and properties of
products such as the temperature, residence time, heating rate, feedstock type, and
the use of catalyst were evaluated in details to promote the process of catalytic
pyrolysis. Catalytic pyrolysis has emerged with the use of a catalyst such as red
mud, fly ash, copper slag, blast furnace slag, coal gangue, and aluminum dross. In
this paper, a brief discussion with recent development on industrial solid wastes
as a catalyst in catalytic pyrolysis process is presented. In the process, the
liquid oil is of higher quality; in addition, process by-products such as solid
char can be used as an adsorbent material, while the quality of pyrolysis gases is
improved. Despite all the potential advantages with industrial solid wastes as a
catalyst, some limitations such as less reuse of catalyst and high parasitic energy
demand are still remaining. The recommended measurements for these challenges
include exploration of suitable reactor, catalyst regeneration, and catalytic
mechanism optimization.
C1 [Qiu, Bingbing; Deng, Na; Zhang, Yufeng] Tianjin Univ, Sch Environm Sci & Engn,
Tianjin Key Lab Indoor Air Environm Qual Control, Tianjin 300072, Peoples R China.
[Deng, Na; Zhang, Yufeng] MOE, Key Lab Efficient Utilizat Low & Medium Grade
Ene, Tianjin 300350, Peoples R China.
[Wan, Haijun] Cool Planet Energy Syst, 3609 Vista Mercado, Camarillo, CA 93012
USA.
C3 Tianjin University
RP Deng, N (corresponding author), Tianjin Univ, Sch Environm Sci & Engn, Tianjin
EM denglouna@tju.edu.cn
RI Zhang, Yufeng/GZL-1973-2022; wan, hai/GSM-9077-2022
FU National Natural Science Foundation of China [51406133]; Scientific
Research Foundation for the Returned Overseas of China
FX National Natural Science Foundation of China, Grant/Award Number:
51406133; Scientific Research Foundation for the Returned Overseas of
China
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NR 96
TC 16
Z9 17
U1 11
U2 153
PU WILEY
PI HOBOKEN
SN 1932-2135
EI 1932-2143
J9 ASIA-PAC J CHEM ENG
JI Asia-Pac. J. Chem. Eng.
PD JAN-FEB
PY 2018
VL 13
IS 1
AR e2150
DI 10.1002/apj.2150
PG 14
SC Engineering
GA FV1NZ
UT WOS:000424331900008
DA 2023-12-05
ER
PT J
AU Wang, KP
Jiang, M
Wang, XH
Wang, Y
Zhao, HQ
Cao, ZM
AF Wang, Kun-Peng
Jiang, Min
Wang, Xin-Hua
Wang, Ying
Zhao, Hao-Qian
Cao, Zhan-Min
TI Study on Formation Mechanism of CaO-SiO2-Based Inclusions in
Saw Wire Steel
LA English
DT Article
ID MN-KILLED STEEL; LIMITED ALUMINUM CONTENT; LIQUID-IRON; NONMETALLIC
INCLUSIONS; THERMODYNAMIC ASSESSMENT; DEOXIDATION EQUILIBRIUM; OXYGEN
EQUILIBRIUM; SLAG COMPOSITION; ALLOYED STEEL; BASICITY SLAG
AB Attempts were made to elucidate the formation mechanism of CaO-SiO2-based
inclusions in saw wires by both laboratory experiments and industrial trials. The
key point was to make clear the origin of CaO in such oxide inclusions. Probable
origins of [Ca] in steel were first discussed, which can be taken into steel from
the steel-slag reaction or ferrous alloy. As a result, slag-steel chemical reaction
equilibrium was carefully evaluated at 1873 K (1600 A degrees C) to classify the
changes of dissolved aluminum ([Al]), total magnesium (Mg), and total calcium (Ca)
in steel and the caused composition variations of inclusions. With the rise of slag
basicity from 0.5 to 1.8, [Al] was remarkably increased from 0.00045 to 0.00139
mass pct, whereas Mg varied in the range of 0.00038 to 0.00048 mass pct. By
contrast, Ca was constantly kept below 0.00003 mass pct. Accordingly, Al2O3 and MgO
in inclusions witnessed obvious rises from 5 to 23 mass pct and from 2 to 8 mass
pct, respectively. By contrast, inclusions were free of CaO when slag basicity was
below 1.5. With slag basicity further increased to 1.8, CaO witnessed a negligible
rise to only 1.0 mass pct on average. This phenomenon agreed well with
thermodynamic calculations, which revealed that chemical reaction between steel and
CaO in slag (for example, between [Si] and CaO) was weak to hardly supplying
sufficient [Ca] to steel to increase CaO in inclusions. Ca contained in ferrous
alloys as contaminations was not the cause of CaO-SiO2-based inclusions, either.
The industrial trial results indicated that CaO-SiO2-based inclusions have been
readily produced in short time just after BOF tapping. Also, a percentage of them
changed slightly with the proceeding of refining. Based on the good agreement of
laboratory, industrial, and thermodynamics calculations results, it can be
reasonably concluded that CaO-SiO2-based inclusions in saw wire were exogenous
particles from entrapped/emulsified top slag, but not products of slag-steel-
inclusion chemical reactions.
C1 [Wang, Kun-Peng; Jiang, Min; Wang, Xin-Hua; Cao, Zhan-Min] Univ Sci & Technol
[Wang, Kun-Peng; Wang, Ying; Zhao, Hao-Qian] Xingtai Iron & Steel Co Ltd, Xing
Tai City 054027, Hebei, Peoples R China.
RI Wang, Xin/GYU-1129-2022; Cao, Zhanmin/M-1575-2016; Wang,
Xin/JCE-2009-2023; Wang, Xinhua/ISR-8520-2023; Wang, Xin/HZL-4695-2023;
Wang, Xiaoqiang/IQS-3727-2023; Wang, Xin/AAN-8435-2021
OI Cao, Zhanmin/0000-0001-7682-5250; Wang, Xin/0000-0002-4457-7376; Wang,
Xin/0000-0002-4457-7376
FU National Natural Science Fund [51304013]; Xingtai Iron & Steel Co., Ltd.
FX The authors express their sincere gratitude and appreciation to the
National Natural Science Fund (Grant No. 51304013), for supporting the
laboratory experiments, and to Xingtai Iron & Steel Co., Ltd., for
supporting the industrial trials and samplings. The authors also thank
Professor Joo-Hyun Park, Hanyang University, for his valuable advice and
meaningful discussions.
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NR 38
TC 16
Z9 19
U1 0
U2 20
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD DEC
PY 2017
VL 48
IS 6
BP 2961
EP 2969
DI 10.1007/s11663-017-1055-0
PG 9
Engineering
GA FN2FJ
UT WOS:000415806100015
DA 2023-12-05
ER
PT J
AU Hybská, H
Hroncová, E
Ladomersky, J
Balco, K
Mitterpach, J
AF Hybska, Helena
Hroncova, Emilia
Ladomersky, Juraj
Balco, Karol
Mitterpach, Jozef
TI Ecotoxicity of Concretes with Granulated Slag from Gray Iron Pilot
Production as Filler
SO MATERIALS
LA English
DT Article
DE red mud; gray iron; granulated slag; concrete composite; ecotoxicity
tests
ID FOUNDRY SLAG
AB This paper focuses on research concerning the ecotoxicological properties of
granulated slag from the pilot production of gray iron with red mud addition and
concrete composites with the application of this slag. Red mud is a hazardous waste
generated in the production of aluminium oxide. Negative ecotoxicological tests
are, therefore, one of the basic prerequisites for the ability to use granulated
slag from gray iron pilot production. Granulated slag and concrete composite
samples with various ratios of granulated slag have been subject to ecotoxicity
tests: determining root growth inhibition in the highly-cultivated plant Sinapis
alba, and determining acute toxicity in Daphnia magna. The results of
ecotoxicological testing of granulated slag from gray iron standard production and
gray iron pilot production with the additive were, according to the standard (STN
83 8303), negative. Additionally, the results of ecotoxicological tests of concrete
composites were negative, with the exception of a 50% substitution of fine
aggregate with slag from gray iron pilot production.
C1 [Hybska, Helena; Mitterpach, Jozef] Tech Univ Zvolen, Fac Ecol & Environm Sci,
Dept Environm Engn, Zvolen 96001, Slovakia.
[Hroncova, Emilia; Ladomersky, Juraj] Matej Bel Univ, Fac Nat Sci, Dept Environm
Management, Banska Bystrica 97401, Slovakia.
[Balco, Karol] ZLH Plus As, Hronec 97645, Slovakia.
C3 Technical University Zvolen; Matej Bel University
RP Hroncová, E (corresponding author), Matej Bel Univ, Fac Nat Sci, Dept Environm
Management, Banska Bystrica 97401, Slovakia.
EM hybska@tuzvo.sk; emilia.hroncova@gmail.com; juraj.ladomersky@umb.sk;
karolbalco@pobox.sk; jozef.mitterpach@gmail.com
RI Ladomerský, Juraj/V-4284-2019; Mitterpach, Jozef/AAC-3160-2021;
Hroncova, Emilia/L-2355-2016
OI Ladomerský, Juraj/0000-0002-8519-1015; Mitterpach,
Jozef/0000-0001-6059-5374; Hroncova, Emilia/0000-0002-8449-9771
FU Slovak Grant Agency KEGA [KEGA 035UMB-4/2015, KEGA 030UMB-4/2017];
Slovak Grant Agency VEGA [VEGA 1/0648/17]; Slovak Research and
Development Agency [APVV-0555-07]
FX This work was supported by the Slovak Grant Agency KEGA under the
contract no. KEGA 035UMB-4/2015 and no. KEGA 030UMB-4/2017. This
research was also supported by the Slovak Grant Agency VEGA under the
contract no. VEGA 1/0648/17. This research was also supported by the
Slovak Research and Development Agency under contract no. APVV-0555-07
"Model of two-stage processing of selected inorganic wastes (with
metallurgical way) and its verification".
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NR 30
TC 16
Z9 17
U1 1
U2 16
PU MDPI AG
PI BASEL
SN 1996-1944
J9 MATERIALS
JI Materials
PD MAY
PY 2017
VL 10
IS 5
AR 505
DI 10.3390/ma10050505
PG 12
Physics
GA EZ0QQ
UT WOS:000404411000057
PM 28772864
DA 2023-12-05
ER
PT J
AU Sahin, AK
Vossenkaul, D
Stoltz, N
Stopic, S
Saridede, MN
Friedrich, B
AF Sahin, Ayfer Kilicarslan
Vossenkaul, Daniel
Stoltz, Nicolas
Stopic, Srecko
Saridede, Muhlis Nezihi
Friedrich, Bernd
TI Selectivity potential of ionic liquids for metal extraction from slags
containing rare earth elements
SO HYDROMETALLURGY
LA English
DT Article
DE NiMH battery; Rare earth; Ionic liquid; Recovery; Hydrometallurgy;
QEMSCAN
ID RECOVERY; KINETICS; CHALCOPYRITE; TEMPERATURE; BATTERIES; BEHAVIOR;
SOLVENTS; CADMIUM; IRON; GOLD
AB The recycling of rare earth elements and base metals from recycling slag powders
of nickel metal hydride (NiMH) batteries by ionic liquid leaching was studied.
Leaching tests were conducted by using the ionic liquid 1-methylimidazolium
hydrogen sulfate (HmimHSO(4)) selected after some preliminary leaching tests on
slag powders. The HinimHSO(4) concentration of aqueous ionic liquid solution was
30% (v/v) in all tests. The slag powders were ground and sieved to obtain two
different particle-size fractions namely 63-90 pm and 90-125 pm in order to
evaluate the leaching behavior and the kinetics. The most important metals present
in the initial slag powders are iron (35.70% w/w), aluminum (9.95% w/w), manganese
(3.45% w/w) and rare earth elements (REEs) such as lanthanum, cerium, neodymium and
yttrium (totally 22.50%w/w). In the leaching experiments three parameters were
studied: temperature, particle size and time. The average dissolution ratios of 63-
90 pm particle size slag powder were 100% for iron, manganese and yttrium after 2 h
at a temperature of 80 degrees C. However, the maximum leaching efficiencies were
about 15% for lanthanide and cerium and 20% for neodymium under the same
conditions. As an explanation for the low recovery rates, a phase analysis with
QEMSCAN (Quantitative Evaluation of Materials by SCANning electron microscopy)
indicated decomposition in the initial REE phases but a precipitation as sulfates.
The kinetic study of Fe and Mn dissolutions showed that the leaching process
follows the shrinking core model with an unchanged particle size controlling
diffusion through the product layer. (C) 2016 Elsevier B.V. All rights reserved.
C1 [Sahin, Ayfer Kilicarslan; Vossenkaul, Daniel; Stopic, Srecko; Friedrich, Bernd]
Rhein Westfal TH Aachen, IME Dept Proc Met & Met Recycling, Intzestr 3, D-52072
Aachen, Germany.
[Sahin, Ayfer Kilicarslan; Saridede, Muhlis Nezihi] Yildiz Tech Univ, Dept Met &
Mat Engn, Davutpasa Campus, TR-34210 Istanbul, Turkey.
[Stoltz, Nicolas] Rhein Westfal TH Aachen, IML Inst Mineral & Econ Geol,
Wullnerstr 2, D-52072 Aachen, Germany.
C3 RWTH Aachen University; Yildiz Technical University; RWTH Aachen
University
RP Sahin, AK (corresponding author), Yildiz Tech Univ, Dept Met & Mat Engn,
Davutpasa Campus, TR-34210 Istanbul, Turkey.
EM kilicarslanayfer@gmail.com
RI Stopic, Srecko/AAC-7097-2021; Friedrich, Bernd/AAM-7029-2021; Friedrich,
Bernd/AAM-7005-2021; Saridede, Muhlis Nezihi/C-5302-2019
OI Stopic, Srecko/0000-0002-1752-5378; Friedrich,
Bernd/0000-0002-2934-2034; Saridede, Muhlis Nezihi/0000-0003-1036-1339
FU Scientific and Technological Research Council of Turkey (TUBITAK)
[2214A]
FX We would like to thank The Scientific and Technological Research Council
of Turkey (TUBITAK) for its research fellowship 2214A to support Ayfer
Kilicarslan Sahin for a three-month stay at the IME Department of
Process Metallurgy and Metal Recycling, RWTH Aachen University.
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NR 29
TC 16
Z9 18
U1 2
U2 70
PU ELSEVIER
PI AMSTERDAM
SN 0304-386X
EI 1879-1158
J9 HYDROMETALLURGY
JI Hydrometallurgy
PD MAY
PY 2017
VL 169
BP 59
EP 67
DI 10.1016/j.hydromet.2016.12.002
PG 9
GA EV6KL
UT WOS:000401878200008
DA 2023-12-05
ER
PT J
AU Tang, HY
Wang, Y
Wu, T
Li, JS
Yang, SF
AF Tang, H. Y.
Wang, Y.
Wu, T.
Li, J. S.
Yang, S. F.
TI Characteristics analysis of inclusion of 60Si2Mn-Cr spring steel via
experiments and thermodynamic calculations
LA English
DT Article
DE 60Si2Mn-Cr spring steel; Inclusion modification; Spinel inclusion;
Calcium treatment; Calcium sulphide
ID AL-KILLED STEEL; DEOXIDATION EQUILIBRIA; NONMETALLIC INCLUSIONS; ALLOYED
STEEL; FATIGUE LIFE; SLAGS; MECHANISM; MG
AB A plant trial of the production of 60Si2Mn-Cr spring steel using silicon-
manganese combined with aluminium to deoxidise was performed, and the
characteristics of inclusions during ladle furnace refining, calcium treatment and
in billets were investigated by scanning electron microscope-energy dispersive
spectroscopy and thermodynamic calculations. The formation mechanisms of oxide and
CaS inclusions are discussed. The experimental observation and thermodynamic
analysis showed that calcium treatment cannot entirely modify large-size MgO center
dot Al2O3 spinel inclusions into homogeneous CaO-MgO-Al2O3 inclusions, but formed a
liquid xCaO center dot yAl(2)O(3) layer on its surface. When the Al content was
0.05 mass%, [Mg], [Ca] and [O] in molten steel could be controlled at 2.7 similar
to 5 ppm, 2.5 similar to 8 ppm and 4.1 similar to 5.2 ppm, respectively, to achieve
inclusions in the low melting point region. A large amount of CaS was generated in
the present process due to a higher sulphur concentration in the molten steel and
an excessive amount of Ca-Si wire. To avoid/reduce its formation, the sulphur
concentration should be controlled to below 70 ppm.
C1 [Tang, H. Y.; Wang, Y.; Wu, T.; Li, J. S.; Yang, S. F.] Univ Sci & Technol
RP Tang, HY (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol
EM tanghaiyan@metall.ustb.edu.cn
OI Wang, Yong/0000-0001-7585-4674
FU National Natural Science foundation of China [51374021]
FX The authors are grateful for the support of the funds by the National
Natural Science foundation of China (No. 51374021).
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NR 34
TC 16
Z9 18
U1 0
U2 35
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PY 2017
VL 44
IS 5
BP 377
EP 388
DI 10.1080/03019233.2016.1212563
PG 12
GA FD4QQ
UT WOS:000407516100009
DA 2023-12-05
ER
PT J
AU Chen, W
Li, B
Li, Q
Tian, J
AF Chen, Wei
Li, Bo
Li, Qiu
Tian, Jian
TI Effect of polyaluminum chloride on the properties and hydration of
slag-cement paste
LA English
DT Article
DE Compressive strength; Microstructure; C-A-S-H; Mean chain length; MAS
NMR
ID BLAST-FURNACE SLAG; SI/AL RATIO SYSTEMS; C-S-H; CONDENSATION-REACTIONS;
DISSOLUTION PROCESSES; GEOPOLYMER SYNTHESIS; NMR CHARACTERIZATION;
SILICATE; AL-27; ALUMINUM
AB The effect of polyaluminum chloride (PACI) on the properties and hydration of
slag-cement was investigated in this research. The PACI is added into slag-cement
mortar with dosages of one or two percent by mass. The compressive strength of
slag-cement mortar is increased with the addition of PACI after 7 days of curing. A
linear correlation between the compressive strength and porosity is found. The
hydration products are mainly AFt, hydrotalcite, Portlandite and C-A-S-H in all
pastes. Adding one percent of PACl reduced the amount of AFt and hydrotalcite due
to the favored incorporation of Al in C-A-S-H. The cross-linking degree and mean
chain length of Si/Al chain in C-A-S-H are reduced if PACI is added. The PACl
accelerated slag hydration by forming multimers, which mitigated the condensation
and precipitation of Al species and prevented the formation of dense layer
structure. The modified surface structure of slag particles favored the dissolution
of inner slag, resulting in a lower degree of polymerization and higher Al/Si
ratios in C-A-S-H which promoted the reaction rate of slag. (C) 2016 Elsevier Ltd.
C1 [Chen, Wei; Li, Bo; Li, Qiu; Tian, Jian] Wuhan Univ Technol, State Key Lab
Silicate Mat Architectures, Wuhan 430070, Peoples R China.
[Chen, Wei; Li, Bo; Tian, Jian] Wuhan Univ Technol, Sch Mat Sci & Engn, Wuhan
C3 Wuhan University of Technology; Wuhan University of Technology
RP Li, Q (corresponding author), Wuhan Univ Technol, State Key Lab Silicate Mat
EM Qiu-Li@whut.edu.cn
RI Li, Qiu/I-2616-2012; Chen, Wei/HIR-5463-2022; Tian, Jian/I-8637-2012
OI Li, Qiu/0000-0002-9128-7005; Chen, Wei/0000-0003-1802-1304;
FU Natural Science Foundation of China [51672199, 5161101154]; Fundamental
Research Funds for the Central Universities [142201001, WUT:
2014-IV-027]; State Key Laboratory of Silicate Materials for
Architectures (Wuhan University of Technology)
FX This research is financially supported by the Natural Science Foundation
of China (project 51672199, 5161101154), The Fundamental Research Funds
for the Central Universities (142201001, WUT: 2014-IV-027) and The
Research Fund of State Key Laboratory of Silicate Materials for
Architectures (Wuhan University of Technology).
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TC 16
Z9 19
U1 6
U2 38
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD OCT 15
PY 2016
VL 124
BP 1019
EP 1027
DI 10.1016/j.conbuildmat.2016.08.154
PG 9
GA DY7OQ
UT WOS:000385319300101
DA 2023-12-05
ER
PT J
AU Shahedan, NF
Abdullah, MMA
Hussin, K
Sandu, I
Ghazali, CMR
Binhussain, M
Yahya, Z
Sandu, AV
AF Shahedan, Noor Fifinatasha
Hussin, Kamarudin
Sandu, Ion
Ghazali, Che Mohd Ruzaidi
Binhussain, Mohammed
Yahya, Zarina
Sandu, Andrei Victor
TI Characterization and Design of Alkali Activated Binder for Coaling
Application
SO MATERIALE PLASTICE
LA English
DT Article
DE Alkali Activated Binder; coating; geopolymer; XRF; XRD; SEM
ID FLY-ASH; POTENTIAL APPLICATION; PROTECTION COATINGS; THERMAL-PROPERTIES;
GEOPOLYMERS; MICROSTRUCTURE; METAKAOLIN; CEMENT
AB Geopolymer has good bonding structure of amorphous inorganic polymer which has
excellent bonding agent properties and shows high bond strength in an early stage.
Therefore, inorganic material like geopolymer which have advantages in previous
research and has potential in replacing the organic materials in coating
application. The chemical composition of the geopolymer materials which were
metakaolin, ground granulate blast slag (GGBS) and fly ash contain mostly Silica
(Si) and Aluminium (Al) which were possible source material for the manufacture of
geopolymer coating. Based on Si:Al ratio and water:cement ratio were the important
factor in the process of geopolymer coating which Si:Al of 3.5 and water:cement
ratio of 0.25 gave the best result in strength in geopolymer coating. The common
techniques for coating method that have been used were brush, spraying and dipping.
From previous research, coating method influenced the greater result in fire
proofing materials and high temperature. For compositions with Si:Al = 2.5 the
adhesive strength was >3.5 MPa while for Si:Al=1 and 2 only weak adhesion to the
metal substrates was achieved in metakaolin based geopolymer coating. Fly ash
geopolymer coating has improved the compressive strength of the coatings materials
as high as 40 MPa with the high sintering temperature, 1500 degrees C. Thermal
expansion measurements in metakaolin geopolymer coating of the Si:Al = 2.5
composition revealed expansion of up to 6% at 800 degrees C, while for Si:Al = 1
and Si:Al = 2 compositions up to 4% shrinkage was observed.
C1 [Shahedan, Noor Fifinatasha; Abdullah, Mohd Mustafa Al Bakri; Hussin, Kamarudin;
Ghazali, Che Mohd Ruzaidi; Yahya, Zarina] Univ Malaysia Perlis, Ctr Excellence
Geopolymer & Green Technol CEGeoGT, Sch Mat Engn, Kangar 01007, Perlis, Malaysia.
[Abdullah, Mohd Mustafa Al Bakri; Hussin, Kamarudin; Ghazali, Che Mohd Ruzaidi]
Univ Malaysia Perlis, Fac Engn Technol, Kangar 01007, Perlis, Malaysia.
[Sandu, Ion] Alexandru Ioan Cuza Univ, Arheoinvest Interdisciplinary Platform,
Iasi 700506, Romania.
[Binhussain, Mohammed] King Abdul Aziz City Sci & Technol KACST, Riyadh 11442,
Saudi Arabia.
[Sandu, Andrei Victor] Gheorghe Asachi Tech Univ Iasi, Fac Mat Sci & Engn, Iasi
700050, Romania.
C3 Universiti Malaysia Perlis; Universiti Malaysia Perlis; Alexandru Ioan
Cuza University; GH Asachi Technical University
RP Shahedan, NF (corresponding author), Univ Malaysia Perlis, Ctr Excellence
Geopolymer & Green Technol CEGeoGT, Sch Mat Engn, POB 77,D-A Pejabat Pos Besar,
Kangar 01007, Perlis, Malaysia.
EM sfifinatasha@yahoo.com; sav@tuiasi.ro
RI Sandu, Andrei Victor/AAJ-8571-2020; SANDU, Ion/B-5797-2012; Binhussain,
Mohammed A/H-8287-2013; Ruzaidi, C. M./I-8680-2012; Sandu, Andrei
Victor/I-9320-2012; Abdullah, Mohd Mustafa Al Bakri/C-9844-2012;
Shahedan, Noor Fifinatasha/AAR-3770-2021
OI Sandu, Andrei Victor/0000-0002-9292-749X; SANDU,
Ion/0000-0003-4088-8967; Binhussain, Mohammed A/0000-0002-2553-0142;
Ruzaidi, C. M./0000-0001-5957-3557; Sandu, Andrei
Victor/0000-0002-9292-749X; Abdullah, Mohd Mustafa Al
Bakri/0000-0002-9779-8586; Shahedan, Noor
Fifinatasha/0000-0001-5390-4829; hussin, kamarudin/0000-0001-9644-4244;
Yahya, Zarina/0000-0003-1144-4945
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NR 47
TC 16
Z9 16
U1 1
U2 27
PU REVISTA CHIMIE SRL
PI BUCURESTI
PA CALES PLEVNEI NR 139A, SECTOR 6, BUCURESTI, ROMANIA
SN 0025-5289
EI 2668-8220
J9 MATER PLAST
JI Mater. Plast.
PD SEP
PY 2014
VL 51
IS 3
BP 258
EP 262
PG 5
GA AT1XI
UT WOS:000344723900007
DA 2023-12-05
ER
PT J
AU Wendling, LA
Binet, MT
Yuan, Z
Gissi, F
Koppel, DJ
Adams, MS
AF Wendling, Laura A.
Binet, Monique T.
Yuan, Zheng
Gissi, Francesca
Koppel, Darren J.
Adams, Merrin S.
TI GEOCHEMICAL AND ECOTOXICOLOGICAL ASSESSMENT OF IRON- AND STEEL-MAKING
SLAGS FOR POTENTIAL USE IN ENVIRONMENTAL APPLICATIONS
SO ENVIRONMENTAL TOXICOLOGY AND CHEMISTRY
LA English
DT Article
DE Aquatic toxicity; Leachate; Radioactivity; By-product; Metal
ID PHOSPHORUS REMOVAL; ACUTE TOXICITY; SODIUM-SULFATE; WATER; ALUMINUM;
BIOAVAILABILITY; HARDNESS; ACCLIMATION; PHOSPHATE; CHLORIDE
AB Prior to the productive use of iron- and steel-making slags as environmental
amendments, a risk assessment supported by material characterization concomitant
with leaching and ecotoxicological testing is necessary. Five iron- and steel-
making slags were characterized geochemically, and the leachability of their
elemental constituents was assessed. The toxicity of slag leachate to microalgae
(Chlorella sp.), cladocerans (Ceriodaphnia dubia), and bacteria (Vibrio fischeri)
was related to elemental composition. Slag leachates with the highest
concentrations of dissolved elements were the most toxic (10% effective
concentration [EC10] approximate to 1%), whereas those with the lowest
concentrations of elements were the least toxic (EC10 63-85%). It was not possible
to determine which elements caused the observed toxicity; however, comparisons with
contaminant guidelines and published toxicity data identified several elements of
potential environmental concern. Low to moderate activities were measured for
radionuclides in the U and Th decay chains in slags. Based on these data, some of
the slags examined herein are potentially suitable for use as environmental
amendments following 10 times dilution to ameliorate potential toxic effects
because of leachate pH. Environ Toxicol Chem 2013;32:2602-2610. (c) 2013 SETAC
C1 [Wendling, Laura A.; Yuan, Zheng] Commonwealth Sci & Ind Res Org, Floreat, WA,
Australia.
[Binet, Monique T.; Gissi, Francesca; Koppel, Darren J.; Adams, Merrin S.]
Commonwealth Sci & Ind Res Org, Lucas Heights, NSW, Australia.
C3 Commonwealth Scientific & Industrial Research Organisation (CSIRO);
Commonwealth Scientific & Industrial Research Organisation (CSIRO)
RP Wendling, LA (corresponding author), Commonwealth Sci & Ind Res Org, Floreat,
WA, Australia.
EM Laura.Wendling@csiro.au
RI Adams, Merrin S/F-3513-2011; Gissi, Francesca/N-7822-2017; Binet,
Monique T/F-2996-2011; Wendling, Laura A/A-2745-2014; Koppel, Darren
J/AAY-6884-2020
OI Adams, Merrin S/0000-0003-2849-9096; Gissi,
Francesca/0000-0002-4622-7572; Binet, Monique T/0000-0003-3502-9025;
Wendling, Laura A/0000-0002-5728-3684; Koppel, Darren
J/0000-0001-7534-237X
FU Jiangxi Provincial Department of Water Resources [KT201101]; Jiangxi
Province (Science and Technology Project) [20111BDH80019]; Jiangxi
Provincial Institute of Water Sciences
FX The authors gratefully acknowledge support from the Jiangxi Provincial
Department of Water Resources (project KT201101), Jiangxi Province
(Science and Technology Project 20111BDH80019), and the Jiangxi
Provincial Institute of Water Sciences.
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TC 16
Z9 16
U1 0
U2 36
PU WILEY
PI HOBOKEN
SN 0730-7268
EI 1552-8618
J9 ENVIRON TOXICOL CHEM
JI Environ. Toxicol. Chem.
PD NOV
PY 2013
VL 32
IS 11
BP 2602
EP 2610
DI 10.1002/etc.2342
PG 9
WC Environmental Sciences; Toxicology
SC Environmental Sciences & Ecology; Toxicology
GA 232HE
UT WOS:000325482700023
PM 23929702
DA 2023-12-05
ER
PT J
AU Zhou, HG
Jiang, ZM
Wei, SQ
AF Zhou, Hongguang
Jiang, Zhenmao
Wei, Shiqiang
TI A Novel Absorbent of Nano-Fe Loaded Biomass Char and Its Enhanced
Adsorption Capacity for Phosphate in Water
SO JOURNAL OF CHEMISTRY
LA English
DT Article
ID LAYERED DOUBLE HYDROXIDES; PHOSPHORUS REMOVAL; AQUEOUS-SOLUTION;
ALUMINUM-OXIDE; WASTE-WATER; IRON; ZEOLITE; IONS; SLAG; PARTICLES
AB A novel composite adsorbent of Fe loaded biomass char (Fe-BC) was fabricated to
treat phosphorus in water. Fe-BC was prepared by a procedure including metal
complex anion incorporation and precipitation with the pyrolysis char of corn straw
as supporting material. The abundant porous structures of the as-prepared sample
can be easily observed from its scanning electron microscopy (SEM) images.
Observations by X-ray diffraction (XRD) and X-ray photoelectron spectroscopy (XPS)
analyses show that inorganic nanoiron oxides deposited in the composite could be
amorphous hydrous iron oxide alpha-FeOOH. Adsorption of phosphate onto the Fe-BC
composite and its precursor (BC) from aqueous solutions were investigated and
discussed. The equilibrium adsorption data of phosphate was described by Langmuir
and Freundlich models, and Langmuir isotherm was found to be better fitted than
Freundlich isotherm. The maximum phosphate adsorption capacity for phosphate of Fe-
BC was as high as 35.43mg/g, approximately 2.3 times of BC at 25 degrees C. The
adsorption kinetics data were better fitted by pseudo-second-order model and
intraparticle diffusion model, indicating that the adsorption process was complex.
The Fe-BC composite has been proved as an effective adsorbent of phosphate
fromaqueous solutions owing to its unique porous structures and the greater Lewis
basicity of the alpha-FeOOH.
C1 [Zhou, Hongguang; Jiang, Zhenmao; Wei, Shiqiang] Southwest Univ, Chongqing Key
Lab Agr Resources & Environm, Key Lab Ecoenvironm Three Gorges Reservoir Reg, Coll
Resources & Environm, Chongqing 400716, Peoples R China.
C3 Southwest University - China
RP Wei, SQ (corresponding author), Southwest Univ, Chongqing Key Lab Agr Resources
& Environm, Key Lab Ecoenvironm Three Gorges Reservoir Reg, Coll Resources &
Environm, Chongqing 400716, Peoples R China.
EM sqwei@swu.edu.cn
FU National Major Science and Technology Projects for Water Pollution
Control and Management [2012ZX07104-003]; Natural Scientific Foundation
of China [21207110, 41171198]; China Postdoctoral Science Foundation
[2013M540691]; Fundamental Research Funds for the Central Universities
[XDJK2014C102]
FX This research is supported by the National Major Science and Technology
Projects for Water Pollution Control and Management (Grant no.
2012ZX07104-003), the Natural Scientific Foundation of China (Grants
nos. 21207110 and 41171198), China Postdoctoral Science Foundation
Funded Project (Grant no. 2013M540691), and the Fundamental Research
Funds for the Central Universities (Grant no. XDJK2014C102).
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10.1016/j.colsurfa.2005.09.034
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NR 63
TC 16
Z9 23
U1 4
U2 14
PU HINDAWI LTD
PI LONDON
PA ADAM HOUSE, 3RD FLR, 1 FITZROY SQ, LONDON, W1T 5HF, ENGLAND
SN 2090-9063
EI 2090-9071
J9 J CHEM-NY
JI J. Chem.
PY 2013
VL 2013
AR 649868
DI 10.1155/2013/649868
PG 9
SC Chemistry
GA 265XW
UT WOS:000327986900001
DA 2023-12-05
ER
PT J
AU Agafonov, SN
Krasikov, SA
Ponomarenko, AA
Ovchinnikova, LA
AF Agafonov, S. N.
Krasikov, S. A.
Ponomarenko, A. A.
Ovchinnikova, L. A.
TI Phase relations in the aluminothermic reduction of ZrO2
SO INORGANIC MATERIALS
LA English
DT Article
AB This paper presents thermodynamic evaluation of reactions between ZrO2 and
aluminum, which indicates that the aluminothermic reduction of zirconium oxides at
temperatures above 600A degrees C is only possible when Al (x) Zr (y) intermetallic
compounds form in the metallic phase. Thermodynamic analysis results are supported
by experimental data, which demonstrate that, at ZrO2: Al ratios in the range 0.4-
1.4, the aluminothermic reduction of ZrO2 leads predominantly to the formation of
the congruently melting compounds Al2Zr and Al3Zr. The phase formation in the slag
yields various forms of calcium aluminates and calcium zirconates and leads to a
gradual reduction in the oxidation state of the zirconium.
C1 [Agafonov, S. N.; Krasikov, S. A.; Ponomarenko, A. A.; Ovchinnikova, L. A.]
Russian Acad Sci, Inst Met, Ural Branch, Ekaterinburg 620016, Russia.
C3 Russian Academy of Sciences; Institute of Metallurgy UB RAS
RP Agafonov, SN (corresponding author), Russian Acad Sci, Inst Met, Ural Branch, Ul
Amundsena 101, Ekaterinburg 620016, Russia.
EM sankr@mail.ru
FU Ural Branch of the Russian Academy of Sciences [12-T-3-1017]
FX This work was supported by the Ural Branch of the Russian Academy of
Sciences (project no. 12-T-3-1017, basic research program, Chemistry and
Materials Science Division, Russian Academy of Sciences).
CR [Anonymous], CONSTITUTION BINARY
Napalkov V.I., 1983, LIGATURY DLYA PROIZV
Roine A., 2002, USERS GUID OUTOKUMPU
NR 3
TC 16
Z9 18
U1 1
U2 17
PU MAIK NAUKA/INTERPERIODICA/SPRINGER
PI NEW YORK
PA 233 SPRING ST, NEW YORK, NY 10013-1578 USA
SN 0020-1685
J9 INORG MATER+
JI Inorg. Mater.
PD AUG
PY 2012
VL 48
IS 8
BP 813
EP 820
DI 10.1134/S0020168512070011
PG 8
GA 974IA
UT WOS:000306425500013
DA 2023-12-05
ER
PT J
AU Shiau, JS
Liu, SH
Ho, CK
AF Shiau, Jia-Shyan
Liu, Shih-Hsien
Ho, Chung-Ken
TI Effect of Magnesium and Aluminum Oxides on Fluidity of Final Blast
Furnace Slag and Its Application
LA English
DT Article
DE blast furnace (BF) slag fluidity; liquidus temperature; viscosity;
magnesium oxide; aluminum oxide
AB Generally, decreasing slag volume of blast furnace operation can lead to the
lower fuel ratio and higher productivity. For high sinter ratio operation, one of
effective ways to obtain a lower slag volume is to reduce the gangue content of
sinter. Basically, lowering the amount of serpentine in the sinter mix is a
feasible way to produce suitable sinter with the lower gangue content. However,
this method may result in lower magnesium oxide content in the final slag that may
affect its fluidity. Hence, the objective of this study was to understand the
effect of MgO and Al2O3 on the fluidity of final slag. The liquidus temperature and
viscosity of semi-synthetic slag were measured using optical softening temperature
device and viscometer, respectively, and the data were treated to develop the
multiple-regression formula of SiO2-Al2O3-CaO-MgO-TiO2 semi-synthetic slag for
liquidus temperature, viscosity equations and iso-fluidity diagrams.
The experimental results indicated that the lower liquidus temperature and the
better viscosity stability lay in the area of MgO = 5.4%, Al2O3 = 10-15%, TiO2 =
0.5% and C/S = 1.2 for the range of composition studied. Several observations in
the iso-fluidity diagrams of blast furnace final slag have shown that liquidus
temperature decreased with decreasing MgO content and the viscosity of slag could
be regarded as being independent of MgO content in the range of MgO = 5-9%, Al2O3 =
15%, C/S = 1.0-1.2. And, slag fluidity became worse with increasing Al2O3 content
under the conditions of MgO = 5.4%, C/S = 1.2. This study suggested the MgO
contents could be lowered from current 6.5 to 5.4% in the conditions of Al2O3 =
15%, C/S = 1.2 under the stable blast furnace operation with high thermal level.
Furthermore, this recipe of lower MgO content (5.4%) had been implemented in CSC's
BF operation to reduce the slag volume, and the formula of fluidity developed in
this study had been installed in the process computer of all CSC's BFs to present
slag fluidity in real time. [doi:10.2320/matertrans.M2012170]
C1 [Shiau, Jia-Shyan; Liu, Shih-Hsien; Ho, Chung-Ken] China Steel Corp, Dept Iron &
Steel Res & Dev, Kaohsiung 81233, Taiwan.
C3 China Steel Corporation
RP Shiau, JS (corresponding author), China Steel Corp, Dept Iron & Steel Res & Dev,
Kaohsiung 81233, Taiwan.
EM jiashyanshiau@gmail.com
CR Higuchi K., 2006, NIPPON STEEL TECH RE, V96, P36
Shiau J. S., 2007, MIN METALL, V52, P44
Yi S. H., 2002, P INT BF LOW ZON SYM, P1
NR 4
TC 16
Z9 18
U1 0
U2 22
PI SENDAI
SN 1345-9678
EI 1347-5320
J9 MATER TRANS
JI Mater. Trans.
PD AUG
PY 2012
VL 53
IS 8
BP 1449
EP 1455
PG 7
Engineering
GA 011VR
UT WOS:000309194900015
OA Bronze
DA 2023-12-05
ER
PT J
AU Jiang, M
Wang, XH
Wang, WJ
AF Jiang, M.
Wang, X. H.
Wang, W. J.
TI Study on refining slags targeting high cleanliness and lower melting
temperature inclusions in Al killed steel
LA English
DT Article
DE Non-metallic inclusion; Cleanliness; Aluminium deoxidation; Slag;
Fatigue; Alloy steel
ID CRACK INITIATION; OXIDE INCLUSIONS; SPRING STEEL; FATIGUE; STRENGTH
AB Three high basicity slags (A, B and C) were used in laboratory to refine Al
killed steel to target high oxide cleanliness and low melting temperature
inclusions. Inclusions were of CaO-MgO-Al(2)O(3)-SiO(2) system after 90 min
reaction, parts of which were MgO based. Total oxygen were in the range of 0.0007-
0.0010 and 0.0005-0.0010% respectively when slag A (CaO/SiO(2), 6-8; Al(2)O(3),
similar to 40%) and slag B (CaO/SiO(2), 6-8; Al(2)O(3) similar to 30%) were
applied, with inclusions all in spherical shape and mainly < 5 mu m. Inclusion
composition concentrated in or around the lower melting point region (< 1500
degrees C) under slag A, while it became more scattered under slag B. Total oxygen
varied between 0.0008 and 0.0011% under slag C (CaO/SiO(2), 3-4; Al(2)O(3), about
20-25%). Many of the inclusions were in larger size, irregular morphology and
located far away from the lower melting point region. Formation of MgO based
inclusions closely related to solubility behaviour of MgO in the slag.
C1 [Jiang, M.] Univ Sci & Technol Beijing, Sch Mat Sci & Engn, Beijing 100083,
Peoples R China.
[Wang, X. H.; Wang, W. J.] Univ Sci & Technol Beijing, Sch Met & Ecol Engn,
Technology Beijing
RP Jiang, M (corresponding author), Univ Sci & Technol Beijing, Sch Mat Sci & Engn,
EM jiangmin820429@yahoo.com.cn
FU National Basic Research Program of China [2010CB630806]; China
Postdoctoral Science Foundation [00070153]
FX The authors thank the National Basic Research Program of China (grant
no. 2010CB630806) and the China Postdoctoral Science Foundation (grant
no. 00070153).
CR Abe T, 2003, TETSU TO HAGANE, V89, P711, DOI 10.2355/tetsutohagane1955.89.6_711
[Anonymous], J IRON STEEL I
BJORNIVAR K, 1976, SCAND J METALL, V5, P63
CHEN XW, 1991, DEOXIDATION STEELMAK
KAWAHARA J, 1992, WIRE J INT NOV, P55
KIYOSHI K, 2007, SANYO TECH REP, V14, P22
LARSSON M, 1993, MATER SCI TECH SER, V9, P235, DOI 10.1179/026708393790171980
MELANDER A, 1993, INT J FATIGUE, V15, P119, DOI 10.1016/0142-1123(93)90006-C
Wang QY, 2002, INT J FATIGUE, V24, P1269, DOI 10.1016/S0142-1123(02)00037-3
NR 17
TC 16
Z9 17
U1 0
U2 11
PU MANEY PUBLISHING
PI LEEDS
SN 0301-9233
J9 IRONMAK STEELMAK
PD JAN
PY 2012
VL 39
IS 1
BP 20
EP 25
DI 10.1179/1743281211Y.0000000043
PG 6
GA 867XT
UT WOS:000298488800003
DA 2023-12-05
ER
PT J
AU Haustein, E
Quant, B
AF Haustein, Elzbieta
Quant, Bernard
TI THE CHARACTERISTICS OF SELECTED PROPERTIES OF THE CENOSPHERES - FRACTION
OF FLY ASH BY-PRODUCT OF COAL COMBUSTION
SO GOSPODARKA SUROWCAMI MINERALNYMI-MINERAL RESOURCES MANAGEMENT
LA Polish
DT Article
DE Fly ash; cenospheres; mineral and chemical composition
ID ALUMINOSILICATE MICROSPHERES; LIGHTWEIGHT
AB The cenospheres are formed during the mineral transformation stage in coal
combustion. Their content in fly ashes from the combustion of different types of
coals varies over a rather wide range from 0.01 to 35.6 wt.%. The cenospheres has
three main elements, silicon, aluminium and iron, the oxides of which account for
about 89% of the material. Mineralogical analysis using XRD shows that as-received
cenospheres mainly contain mullite and quartz as main mineralogical phases. The
size of cenospheres varies between 5 and 500 mu m, as the most common dimension is
20-300 mu m. The cenospheres are characterized by a low bulk density (0.2-0.8
g/cm(3)) and can be easily separated by gravitational methods in the form of a
concentrate in aqueous media or collected from a water surface of lagoons intended
for storage of ash and slag waste. The unique properties of these hollow
microspheres make them amenable for wide applications. For example the cenospheres
can be used to produce various lightweight construction products, including
lightweight cements and aggregates in lightweight concrete.
C1 [Haustein, Elzbieta] Gdansk Tech Univ, Katedra Konstrukeji Betonowych &
Technologii Beto, Wydzial Inzynierii Ladowej & Srodowiska, Gdansk, Poland.
[Quant, Bernard] Gdansk Tech Univ, Katedra Technologii Wody & Sciekow, Wydzial
Inzynierii Ladowej & Srodowiska, Gdansk, Poland.
C3 Fahrenheit Universities; Gdansk University of Technology; Fahrenheit
Universities; Gdansk University of Technology
RP Haustein, E (corresponding author), Gdansk Tech Univ, Katedra Konstrukeji
Betonowych & Technologii Beto, Wydzial Inzynierii Ladowej & Srodowiska, Gdansk,
Poland.
EM elzbieta.haustein@wilis.pg.gda.pl
RI Quant, Bernard/R-5179-2016; Haustein, Elzbieta/ABB-7311-2021
OI Quant, Bernard/0000-0001-9974-5886; Haustein,
Elzbieta/0000-0002-3066-4751
CR [Anonymous], PLASTICS COMPOUND
[Anonymous], DZ U
[Anonymous], BN79672209
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9
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NR 46
TC 16
Z9 16
U1 0
U2 2
PU POLSKA AKAD NAUK, POLISH ACAD SCIENCES, MINER & ENERGY ECON RES INST PAS
PI WARSZAWA
PA PL DEFILAD 1, WARSZAWA, 00-901, POLAND
SN 0860-0953
EI 2299-2324
J9 GOSPOD SUROWCAMI MIN
JI Gospod. Surowcami. Miner.
PY 2011
VL 27
IS 3
BP 95
EP 111
PG 17
WC Mineralogy; Mining & Mineral Processing
SC Mineralogy; Mining & Mineral Processing
GA 829HF
UT WOS:000295568500006
DA 2023-12-05
ER
PT J
AU Peregrina, F
Mariscal, I
Ordóñez, R
González, P
Terefe, T
Espejo, R
AF Peregrina, F.
Mariscal, I.
Ordonez, R.
Gonzalez, P.
Terefe, T.
Espejo, R.
TI Agronomic implications of converter basic slag as a magnesium source on
acid soils
SO SOIL SCIENCE SOCIETY OF AMERICA JOURNAL
LA English
DT Article
ID ALUMINUM TOXICITY; BY-PRODUCTS; FLUORIDE COMPLEXES; CALCIUM; GYPSUM;
WHEAT; PHYTOTOXICITY; AMELIORATION; PHOSPHORUS; GROWTH
AB The feasibility of using converter basic slag (CBS) as a source of Mg for
gypsum-amended acidic soils was studied in a Plinthic Palexerult from western
Spain. An experimental farm was established and the Ap horizon of the soil was
amended with limestone (L), phosphogypsum (PG), or red gypsum (RG) to alleviate Al
toxicity. The PG and RG were supplied at 8.0 and 8.8 Mg ha(-1), respectively. In
addition, the gypsum-amended plots received either CBS at 0.9 Mg ha(-1) or
limestone at 1.1 Mg ha(-1). We studied the effects of the treatments on the
exchange complex, soil solution, and the biomass production of 'Jabato' wheat
(Triticum aestivum L.) under field and greenhouse conditions. The CBS proved highly
effective in replenishing Mg lost from the soil through application of gypsum
amendments. In the field experiment, only the RG + CBS treatment resulted in a
statistically significant increase of biomass production relative to the control.
In the greenhouse experiment, all treatments resulted in significantly increased
production relative to the control, the largest (26 times) by RG + CBS. The PG +
CBS and RG + CBS treatments resulted in significantly increased production relative
to PG + L and RG + L, which testifies to the favorable effect of the Mg supplied by
CBS. Also, the treatments including RG resulted in significantly increased
production with respect to those including PG; the increased productivity is
tentatively ascribed to a potential toxic effect of AI-F ion pairs, which were more
abundant in the soil solution of PG-treated soil.
C1 [Peregrina, F.; Mariscal, I.; Terefe, T.; Espejo, R.] Univ Politecn Madrid, ETSI
Agronomos, E-28040 Madrid, Spain.
[Terefe, T.; Espejo, R.] Spainiudad Univ, Madrid 28040, Spain.
[Ordonez, R.; Gonzalez, P.] CIFA, Cordoba 14080, Spain.
C3 Universidad Politecnica de Madrid
RP Espejo, R (corresponding author), Univ Politecn Madrid, ETSI Agronomos, Ciudad
Univ, E-28040 Madrid, Spain.
EM rafael.espejo@upm.es
RI Espejo, Rafael RE/F-5646-2016; Peregrina, Fernando/B-5188-2011;
Ordóñez-Fernández, Rafaela/C-6517-2016; Sancho, Ignacio
Mariscal/L-9323-2014
OI Espejo, Rafael RE/0000-0002-7592-2152; Peregrina,
Fernando/0000-0002-7621-7455; Ordóñez-Fernández,
Rafaela/0000-0002-8041-0549; Sancho, Ignacio
Mariscal/0000-0003-2344-6710
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NR 64
TC 16
Z9 17
U1 1
U2 11
PU WILEY
PI HOBOKEN
SN 0361-5995
EI 1435-0661
J9 SOIL SCI SOC AM J
JI Soil Sci. Soc. Am. J.
PD MAR-APR
PY 2008
VL 72
IS 2
BP 402
EP 411
DI 10.2136/sssaj2006.0197
PG 10
WC Soil Science
SC Agriculture
GA 275GP
UT WOS:000254060200013
DA 2023-12-05
ER
PT J
AU Björklund, J
Andersson, M
Jönsson, P
AF Bjorklund, J.
Andersson, M.
Jonsson, P.
TI Equilibrium between stag, steel and inclusions during ladle treatment::
comparison with production data
LA English
DT Article
DE models; activity; slag; steel; oxygen; oxide
ID SLAGS
AB The primary purpose of the investigation was to determine whether equilibrium
conditions exist between slag and steel and inclusions and steel after silicon
deoxidation and aluminium deoxidation. In doing so, the performance of three
different models for predicting oxide component activities was also evaluated. The
results from the oxide activity models were used to calculate oxygen activities in
the steel melt. Industrial data such as steel, slag and inclusion component
concentrations, as well as temperature, were used as input to the calculations. One
general conclusion drawn was that although the results from the different models
showed similar trends, the models did not predict the same actual values for
specific calculations. Predicted theoretical equilibrium oxygen activity values
were compared with plant measurements of oxygen activity. Here, it was found that
the oxygen activity values pertaining to the equilibrium between steel and
inclusions were higher than corresponding measured values. The calculations for the
equilibrium between the top slag and steel melt, however, resulted in theoretical
oxygen activity values considerably lower than corresponding measurements. It was
thus concluded that equilibrium conditions did not exist between the top slag and
the steel bulk with respect to oxygen. Overall, the models proved useful in
predicting oxide activities, but the lack of equilibrium between top slag and
molten steel made the calculation of oxygen activity difficult.
C1 Royal Inst Technol, Div Appl Proc Met, SE-10044 Stockholm, Sweden.
RP Jönsson, P (corresponding author), Royal Inst Technol, Div Appl Proc Met,
Brinellvagen 23, SE-10044 Stockholm, Sweden.
EM par@mse.kth.se
Andersson MAT, 2000, IRONMAK STEELMAK, V27, P286, DOI 10.1179/030192300677570
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EKENGARD J, THESIS KTH STOCKHOLM
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HANSEN T, THESIS KTH STOCKHOLM
Hayes P. C., 1993, PROCESS PRINCIPLES M
REINHOLDSSON F, 2005, COMMUNICATION
1984, JERNKONTORESTS FOR D
NR 11
TC 16
Z9 16
U1 1
U2 6
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD JUL
PY 2007
VL 34
IS 4
BP 312
EP 324
DI 10.1179/174328107X168039
PG 13
GA 197GD
UT WOS:000248541700006
DA 2023-12-05
ER
PT J
AU Kuss, HM
Lüngen, S
Müller, G
Thurmann, U
AF Kuss, HM
Lüngen, S
Müller, G
Thurmann, U
TI Comparison of spark OES methods for analysis of inclusions in iron base
matters
SO ANALYTICAL AND BIOANALYTICAL CHEMISTRY
LA English
CT Nonmetals in Metals 2000
CY MAR 16-17, 2000
CL UNIV MUNSTER, MUNSTER, GERMANY
HO UNIV MUNSTER
DE aluminium oxide; non-metallic inclusions; single pulse evaluation; spark
OES; steel cleanness
ID STEELS
AB A statistical model for the evaluation of the emission intensities of single
spark discharge spectra on three different spark OES instruments (ARL 4460, OBLF-
QSN 750, SpectroLab) was developed for the analysis of non-metallic inclusions in
steel. In total, the raw measurement data consists of several thousand data points
(intensities), about 2000 per element channel. A histogram (frequency distribution
of pulse height intensities) of inclusion-forming elements like Al, Ti and Mn
performed in intensity classes and the related frequencies contain the information
of the measurement. Measurement of a pure iron sample with slag powder rubbed into
the surface by single spark emission spectrometry changes the originally (nearly)
symmetrical histogram for inclusion related element signals to higher intensities.
Thus, the known asymmetry of the histograms for steel samples is explained by the
presence of inclusions. A sum of Gaussian fits representing the histogram was
expected to express the different elemental species and inclusion sizes by using
the variables mean, standard deviation and area of the peak containing the
information of the measurement. Even a less complex approximation using a sum of
two Gaussian fits is not practicable for the Al, Ti and Mn channel and the three
spectrometers due to too many variables in the fitting function resulting in a
large scattering. Coincidences of high signals in different element channels could
be seen only in terms of MnS. A further attempt was to form the second differential
of the logarithmic normal distribution and to compare the resulting partial areas
below the functional graph to get information about the asymmetry of the fitting
function of the original histogram. Two different procedures to evaluate the effect
of the inclusion concentration on the size of the partial areas were applied to
measurements on a set of synthetic samples with different concentrations of
aluminium oxide in micro alloy steel. The results of both evaluation procedures
correlate significantly with the inclusion concentrations.
C1 Univ Duisburg, Dept Analyt Chem, D-47057 Duisburg, Germany.
Thyssen Stahl AG, Forsch Zent Qualitats & Prufwesen, D-47166 Duisburg, Germany.
C3 University of Duisburg Essen; ThyssenKrupp AG
RP Kuss, HM (corresponding author), Univ Duisburg, Dept Analyt Chem, Lotharstr 1,
D-47057 Duisburg, Germany.
EM kuss@lims.uni-duisburg.de
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8
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NR 24
TC 16
Z9 16
U1 0
U2 0
PI HEIDELBERG
SN 1618-2642
EI 1618-2650
J9 ANAL BIOANAL CHEM
JI Anal. Bioanal. Chem.
PD DEC
PY 2002
VL 374
IS 7-8
BP 1242
EP 1249
DI 10.1007/s00216-002-1595-1
PG 8
WC Biochemical Research Methods; Chemistry, Analytical
SC Biochemistry & Molecular Biology; Chemistry
GA 638JE
UT WOS:000180567200012
DA 2023-12-05
ER
PT J
AU Wang, SD
AF Wang, SD
TI Alkali-activated slag: hydration process and development of
microstructure
LA English
DT Article
ID CEMENT
AB This paper presents the results of an investigation into the hydration process
and development of the microstructure of alkali-activated slag. Samples were
examined by X-ray diffraction, scanning electron microscope, X-ray microanalysis of
energy dispersive spectrum, and solid-state nuclear magnetic resonance. Hydration
products have been identified as calcium-silica-hydrate (C-S-H) gel of low Ca/Si
ratio, hydrotalcite, AFm phases and CH. It has been found that two types of AFm
phase exist, depending on the exposure conditions. The initial AFm phase is formed
through the transformation of CH and, upon exposure to air, it transforms into a
carbonated form, hemicarbonate. it has been proposed that aluminium plays a key
role in enhancing silicate polymerization. Slag compositional effects are discussed
on the formation of hydration products and the development of microstructure.
C1 Chongqing Jianzhu Univ, Dept Mat, Chongqing 400045, Peoples R China.
RP Wang, SD (corresponding author), Chongqing Jianzhu Univ, Dept Mat, Chongqing
CR FENG QL, 1990, P MAT RES SOC S, V178, P57
Gastuche MC, 1967, CLAY MINER, V7, P177
HARRISON AM, 1986, P MAT RES SOC S, V86, P199
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Wang S. D., 1995, THESIS U LONDON
WANG SD, 2000, CEMENT CONCRETE RES, V30
NR 11
TC 16
Z9 17
U1 0
U2 14
PU THOMAS TELFORD SERVICES LTD
PI LONDON
PA THOMAS TELFORD HOUSE, 1 HERON QUAY, LONDON, ENGLAND E14 4JD
SN 0951-7197
J9 ADV CEM RES
JI Adv. Cem. Res.
PD OCT
PY 2000
VL 12
IS 4
BP 163
EP 172
DI 10.1680/adcr.2000.12.4.163
PG 10
GA 362JL
UT WOS:000089774800004
DA 2023-12-05
ER
PT J
AU BERETKA, J
CIOFFI, R
SANTORO, L
VALENTI, G
AF BERETKA, J
CIOFFI, R
SANTORO, L
VALENTI, G
TI CEMENTITIOUS MIXTURES CONTAINING INDUSTRIAL-PROCESS WASTES SUITABLE FOR
THE MANUFACTURE OF PREFORMED BUILDING ELEMENTS
SO JOURNAL OF CHEMICAL TECHNOLOGY AND BIOTECHNOLOGY
LA English
DT Article
DE BINDER, CEMENT; ETTRINGITE-BASED CEMENT; WASTE UTILIZATION; HIGH ALUMINA
CEMENT; BUILDING ELEMENTS
ID HYDRATION; PHOSPHOGYPSUM
AB Mixtures made from materials containing reactive oxides of calcium, aluminium,
Sulphur and silicon which are able, upon hydration, to generate calcium
trisulphoaluminate and silicate hydrates, have been studied with a view to possible
applications in the field of preformed building elements. The materials employed
were natural gypsum, phosphogypsum, fly ash, blast furnace slag, Portland cement
and hydrated lime. The samples were cured at 55, 70 and 85-degrees-C and 100% RH
for 24 h, followed by further curing at ordinary temperatures and humidities (21-
degrees-C, 67% RH) for up to 28 days. The cured samples were tested for compressive
strength and shrinkage. It has been found that the most important effect on the
strength is due to the pre-curing temperature, while the post-curing time has much
less effect. In general, the optimum pre-curing temperature is 70-degrees-C.
Satisfactory strength results were obtained even with systems containing up to 80%
waste materials.
C1 UNIV NAPOLI FEDERICO II,DIPARTIMENTO INGN MAT & PROD,I-80125 NAPLES,ITALY.
UNIV NAPOLI FEDERICO II,DIPARTIMENTO CHIM,I-80134 NAPLES,ITALY.
UNIV BASILICATA,DIPARTIMENTO INGN & FIS AMBIENTE,I-85100 POTENZA,ITALY.
C3 University of Naples Federico II; University of Naples Federico II;
University of Basilicata
RP BERETKA, J (corresponding author), CSIRO,DIV BLDG CONSTRUCT & ENGN,POB
56,HIGHETT,VIC 3190,AUSTRALIA.
OI Cioffi, Raffaele/0000-0002-7757-6361
CR AZUMA T, 1976, JAPAN KOKAI, V76, P826
AZUMA T, 1976, GER OFFEN, V2, P310
BERETKA J, 1987, 4TH P INT C DUR BUIL, V1, P64
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BERETKA J, 1991, 3RD P NCB INT SEM CE, V3, P110
CIOFFI R, 1992, J THERM ANAL, V38, P761, DOI 10.1007/BF01979406
SANTORO L, 1984, THERMOCHIM ACTA, V74, P35, DOI 10.1016/0040-6031(84)80004-0
SANTORO L, 1986, THERMOCHIM ACTA, V98, P71, DOI 10.1016/0040-6031(86)87076-9
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1
VALENTI GL, 1988, 2ND P INT S PHOSPH M, V2, P167
NR 11
TC 16
Z9 16
U1 0
U2 5
PU JOHN WILEY & SONS LTD
PI W SUSSEX
PA BAFFINS LANE CHICHESTER, W SUSSEX, ENGLAND PO19 1UD
SN 0268-2575
J9 J CHEM TECHNOL BIOT
JI J. Chem. Technol. Biotechnol.
PD MAR
PY 1994
VL 59
IS 3
BP 243
EP 247
DI 10.1002/jctb.280590306
PG 5
WC Biotechnology & Applied Microbiology; Chemistry, Multidisciplinary;
Engineering, Environmental; Engineering, Chemical
SC Biotechnology & Applied Microbiology; Chemistry; Engineering
GA NH072
UT WOS:A1994NH07200005
DA 2023-12-05
ER
PT J
AU Zhao, ZY
Guo, KH
Wang, XL
AF Zhao, Zhiyun
Guo, Kaihua
Wang, Xiangling
TI A binder prepared by low-reactivity blast furnace slags for cemented
paste backfill: Influence of super-fine fly ash and chemical additives
LA English
DT Article
DE Cemented paste backfill; Low-carbon binders; Reaction kinetics;
Compressive strength; Superfine fly ash
ID HYDRATION MECHANISMS; GEOPOLYMER CEMENT; ACTIVATED SLAG; PART I;
PERFORMANCE; CHEMISTRY; KINETICS; HEAT
AB Alternative binders for cemented paste backfill (CPB) are necessary to be
prepared considering the high cost and environmental footprint of ordinary Portland
cement (OPC). This study focuses on the preparation of a binder using low-
reactivity blast furnace slag (BFS). Superfine fly ash (SFA) and chemical additives
(aluminum sulfate, AlS and carbide slag, CC) are used to modify the binder
properties. Both SFA and chemical additives could promote the binder reaction with
the formation of more reaction products. The pore structure was then refined;
thereby higher compressive strength was observed. Krstulovic-Dabic (K-D) model was
used to characterize the hydration process and all binders hydration mechanism was
'NG-I-D'. The synergistic effect of SFA, AlS, and CC showed the best performance,
the compressive strength of the CPB samples could reach 0.24 MPa and 2.73 MPa at 3
and 28 days using the optimal proportion. The excellent performance can be
attributed to the physical and chemical effects of the coupling actions of SFA and
chemical additives.
C1 [Zhao, Zhiyun; Wang, Xiangling] Luliang Univ, Dept Min Engn, Lvliang 033000,
Peoples R China.
[Guo, Kaihua] Luliang Univ, Dept Life Sci, Lvliang 033000, Peoples R China.
C3 Lvliang University; Lvliang University
RP Zhao, ZY (corresponding author), Luliang Univ, Dept Min Engn, Lvliang 033000,
Peoples R China.
EM zhaozhiyun2021@163.com
RI zhao, zhiyun/E-6560-2011
FU Key R&D Projects in Lvliang City [2019GYZDYF79]; Teaching reform and
innovation project of colleges and universities in Shanxi Province
[J2020353]
FX Acknowledgment The project supported by Key R&D Projects in Lvliang City
(2019GYZDYF79) ; Teaching reform and innovation project of colleges and
universities in Shanxi Province (J2020353) .
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10.1016/j.cemconres.2018.01.002
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10.1016/j.cemconcomp.2021.104236
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10.1016/j.cemconres.2013.11.013
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10.1016/j.cemconres.2008.03.004
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10.1016/j.cemconres.2019.05.008
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10.1016/j.conbuildmat.2019.03.322
Liu SH, 2015, THERMOCHIM ACTA, V605, P37, DOI 10.1016/j.tca.2015.02.013
10.1016/j.cemconres.2017.10.001
Masoudi R, 2019, CEMENT CONCRETE COMP, V103, P193, DOI
10.1016/j.cemconcomp.2019.05.001
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8
Pinto SR, 2020, CEMENT CONCRETE RES, V136, DOI 10.1016/j.cemconres.2020.106172
10.1016/j.cemconres.2015.04.013
Sun XG, 2021, POWDER TECHNOL, V393, P539, DOI 10.1016/j.powtec.2021.07.067
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Tian XC, 2021, CONSTR BUILD MATER, V297, DOI 10.1016/j.conbuildmat.2021.123657
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10.1016/j.cemconres.2011.06.003
Zhang SY, 2021, J CLEAN PROD, V283, DOI 10.1016/j.jclepro.2020.125310
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Zhao YL, 2021, J ENVIRON MANAGE, V300, DOI 10.1016/j.jenvman.2021.113760
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Zhou LF, 2021, CONSTR BUILD MATER, V301, DOI 10.1016/j.conbuildmat.2021.124296
Zhou Y, 2021, CEMENT CONCRETE COMP, V118, DOI 10.1016/j.cemconcomp.2021.103947
NR 59
TC 15
Z9 15
U1 6
U2 33
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD APR 11
PY 2022
VL 327
AR 126988
DI 10.1016/j.conbuildmat.2022.126988
EA FEB 2022
PG 11
GA ZR8CB
UT WOS:000768004700003
DA 2023-12-05
ER
PT J
AU Schade, T
Bellmann, F
Middendorf, B
AF Schade, Tim
Bellmann, Frank
Middendorf, Bernhard
TI Quantitative analysis of C-(K)-A-S-H-amount and hydrotalcite phase
content in finely ground highly alkali-activated slag/silica fume
blended cementitious material
LA English
DT Article
DE Alkali-activated materials; NMR; EDX; C-(K)-A-S-H-phase; Hydrotalcite
ID C-S-H; MAS-NMR; AL-27 NMR; SLAG; SI-29; HYDRATION; ALUMINUM; GELS;
PASTES; MODEL
AB For the development of CO2-reduced binders for structural engineering and for
predicting their performance, knowledge of the amount formed in weight fractions of
the reaction products is essential. This paper presents a method to specify the
hydration products of an alkali-activated slag/silica fume blended cementitious
material by weight. The Si-29 and Al-27 magic angle spinning (MAS) nuclear magnetic
resonance (NMR) spectroscopy to determine the C-A-S-H phases was coupled with
energy dispersive analysis (EDX) technology to determine the bound K/Si ratio.
Furthermore, the Al-27 MAS NMR was used to define the amount of hydrotalcite. With
the help of the developed model, the hydration phases of alkali-activated
slag/silica fume blended cementitious material in dependency of the activator can
be calculated. The results of the mass ratios deduced by NMR with coupled EDX was
in agreement with the loss of ignition measured by thermogravimetric analysis
(TGA). Consequently, the hydration products can be self-checked.
C1 [Schade, Tim] Global R&D HeidelbergCement AG, Oberklamweg 2-4, D-69181 Leimen,
Germany.
[Bellmann, Frank] Bauhaus Univ Weimar, Dept Construct Mat, Coudraystr 11A, 204,
D-99423 Weimar, Germany.
[Middendorf, Bernhard] Univ Kassel, Dept Struct Mat & Construct Chem,
Moenchebergstr 7, D-34125 Kassel, Germany.
C3 Bauhaus-Universitat Weimar; Universitat Kassel
RP Schade, T (corresponding author), Global R&D HeidelbergCement AG, Oberklamweg 2-
4, D-69181 Leimen, Germany.
EM tim.schade@heidelbergcement.com
OI Schade, Tim/0000-0002-3781-1953
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NR 58
TC 15
Z9 15
U1 9
U2 20
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD MAR
PY 2022
VL 153
AR 106706
DI 10.1016/j.cemconres.2021.106706
EA JAN 2022
PG 12
GA 1G5VL
UT WOS:000795915800006
DA 2023-12-05
ER
PT J
AU Yang, FM
Pang, FJ
Xie, JT
Wang, WJ
Wang, WL
Wang, ZM
AF Yang, Fengming
Pang, Fangjie
Xie, Jiateng
Wang, Weijie
Wang, Wenlong
Wang, Zengmei
TI Leaching and solidification behavior of Cu2+, Cr3+
and Cd2+ in the hydration products of calcium sulfoaluminate
cement
LA English
DT Article
DE Solid waste; Calcium sulfoaluminate cement (CSA); Heavy metals;
Leaching; Ettringite
ID PORTLAND-CEMENT; POTENTIAL APPLICATION; IMMOBILIZATION; ETTRINGITE;
STABILIZATION; STRENGTH; SYSTEMS; MATRIX; VOLUME; ASH
AB Utilization of industrial solid wastes such as aluminum dust, carbide slag, red
mud and flue gas desulfurization gypsum (FGD gypsum) as raw materials for the
production of calcium sulfoaluminate cement (CSA) is an effective way for solid
waste recycling. However, the heavy metals in these industrial solid wastes may
affect the cement hydration and environment, limiting the application of CSA from
solid wastes. In this work, to clarify the interaction between heavy metals and
CSA, as typical heavy metals, Cu2+, Cr3+ and Cd2+ were introduced with different
contents. The study found that Ca2+ in ettringite crystalline can be exchanged with
Cu2+/Cd2+, and Al3+ can be exchanged with Cr3+, and this chemical capture method
can prevent the leaching of heavy metals. The ICP-OES results show that the
retention ratios of Cu2+, Cr3+ and Cd2+ with 2 wt% dopant were above 99.99%.
Besides, the proper amount of heavy metals makes CSA hydration to maintain an
alkaline environment to facilitate the crystallization and growth of ettringite.
However, when content of Cr3+ was excessive (more than 2%), the pH value declined
severely, which was unfavorable to the stability of ettringite. The XPS results
indicated that the Cu2+, Cr3+ and Cd2+ could weaken the binding energy of Ca-O and
Al-O bond, decreasing the stability of ettringite crystal, resulting to weaken the
compressive strength of CSA, but all are acceptable. The hydration kinetics
indicate that the Cr3+ ions make the activation energy barrier to the hydration
reaction drop drastically, resultantly, accelerating the hydration process, while
Cu2+ and Cd2+ delayed the hydration process, maybe the origin of variation of
setting time.
C1 [Yang, Fengming; Pang, Fangjie; Xie, Jiateng; Wang, Zengmei] Southeast Univ, Sch
Mat Sci & Engn, Jiangsu Key Lab Construct Mat, Nanjing 211189, Peoples R China.
[Wang, Weijie] Nanjing Tech Univ, Sch Transportat Engn, Nanjing 210009, Peoples
R China.
[Wang, Wenlong] Shandong Univ, Natl Engn Lab Coal Fired Pollutants Emiss Reduct,
Jinan 250061, Peoples R China.
C3 Southeast University - China; Nanjing Tech University; Shandong
University
RP Wang, ZM (corresponding author), Southeast Univ, Sch Mat Sci & Engn, Jiangsu Key
Lab Construct Mat, Nanjing 211189, Peoples R China.; Wang, WL (corresponding
author), Shandong Univ, Natl Engn Lab Coal Fired Pollutants Emiss Reduct, Jinan
EM wwenlong@sdu.edu.cn; 101011338@seu.edu.cn
RI wang, wenlong/L-2239-2013
FU national key R&D Program of China [2020YFC1910000]; Natural Science
FX This work was financially sponsored in part by the national key R&D
Program of China (2020YFC1910000). Part of this work was supported by
the Natural Science Foundation of China (Grants No. 51978153)
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NR 43
TC 15
Z9 15
U1 14
U2 38
PU ELSEVIER
PI AMSTERDAM
EI 2352-7102
J9 J BUILD ENG
JI J. Build. Eng.
PD APR 1
PY 2022
VL 46
AR 103696
DI 10.1016/j.jobe.2021.103696
EA JAN 2022
PG 10
GA 0D7NS
UT WOS:000776178200001
DA 2023-12-05
ER
PT J
AU Huang, X
Xin, C
Li, JS
Wang, P
Liao, S
Poon, CS
Xue, Q
AF Huang, Xiao
Xin, Chen
Li, Jiang-shan
Wang, Ping
Liao, Shuai
Poon, Chi Sun
Xue, Qiang
TI Using hazardous barium slag as a novel admixture for alkali activated
slag cement
LA English
DT Article
DE Alkali activated slag; Barium slag; Unconfined compressive strength;
Pore structure; Hydration products
ID HYDRATED PORTLAND CEMENTS; BLAST-FURNACE SLAG; STRENGTH; AL-27; SI-29;
EVOLUTION; ALUMINUM
AB Barium slag (BS) is a hazardous industrial solid waste formed during the
production of barium carbonate. The accumulated stock of BS in China has exceeded
10 million tons, which urgently needs to be recycled in an efficient and
sustainable way. BS contains a lot of soluble Ba2+ with a leaching concentration up
to 2000 mg/L in water. Meanwhile, Ba2+ is an alkali-earth metal which can activate
ground granulated blast furnace slag (GGBFS). This paper explores the possibility
of incorporation BS as an admixture for alkali activated slag (AAS) cement. The
mechanical property and microstructure evolution of AAS pastes with addition of BS
are investigated in comparison with pure AAS paste. The results indicate that the
addition of BS could significantly enhance mechanical strength of AAS paste,
attributing to the increased hydration degree and the formation of dense pore
structure. In addition, the leaching concentration of Na+ shows a significant
decline by incorporation of BS in AAS paste, associated with the changed
composition of hydration products. Therefore, BS is a promising admixture for AAS
cement and holds great potential for promotion and application.
C1 [Huang, Xiao; Xin, Chen; Li, Jiang-shan; Wang, Ping; Liao, Shuai; Xue, Qiang]
Chinese Acad Sci, Inst Rock & Soil Mech, State Key Lab Geomech & Geotech Engn,
[Huang, Xiao; Xin, Chen; Li, Jiang-shan; Wang, Ping; Liao, Shuai; Poon, Chi Sun;
Xue, Qiang] IRSM CAS HK PolyU Joint Lab Solid Waste Sci, Wuhan 430071, Peoples R
China.
[Poon, Chi Sun] Hong Kong Polytech Univ, Dept Civil & Environm Engn, Hung Hom,
Kowloon, Hong Kong, Peoples R China.
C3 Chinese Academy of Sciences; Wuhan Institute of Rock & Soil Mechanics,
CAS; Hong Kong Polytechnic University
RP Li, JS; Xue, Q (corresponding author), Chinese Acad Sci, Inst Rock & Soil Mech,
State Key Lab Geomech & Geotech Engn, Wuhan 430071, Peoples R China.
EM jsli@whrsm.ac.cn; qxue@whrsm.ac.cn
RI Poon, Chi Sun/JQI-2195-2023
OI Poon, Chi Sun/0000-0003-4912-3936; Huang, Xiao/0000-0003-3344-5826
FU National Key Research and Development Program [2019YFC1804002]; National
Natural Science Foundation of China [42007260]; National Natural Science
Foundation of China/Hong Kong Research Grants Council [51861165104];
University Grants Committee Joint Research Scheme [51861165104]; China
Postdoctoral Science Foundation [2021M693364]; Youth Innovation
Promotion Association CAS [2017376]; CAS Pioneer Hundred Talents Program
in China
FX This study was financially supported by the National Key Research and
Development Program (Grant No. 2019YFC1804002) , National Natural
Science Foundation of China (Grant No. 42007260) , National Natural
Science Foundation of China/Hong Kong Research Grants Council,
University Grants Committee Joint Research Scheme (Grant No.
51861165104) , China Postdoctoral Science Foundation (2021M693364) , The
CAS Pioneer Hundred Talents Program in China and Youth Innovation
Promotion Association CAS (2017376) .
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NR 40
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Z9 18
U1 13
U2 37
PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
PD JAN
PY 2022
VL 125
AR 104332
DI 10.1016/j.cemconcomp.2021.104332
EA NOV 2021
PG 11
GA YJ1CW
UT WOS:000744276500001
DA 2023-12-05
ER
PT J
AU Occhicone, A
Vukcevic, M
Boskovic, I
Ferone, C
AF Occhicone, Alessio
Vukcevic, Mira
Boskovic, Ivana
Ferone, Claudio
TI Red Mud-Blast Furnace Slag-Based Alkali-Activated Materials
SO SUSTAINABILITY
LA English
DT Article
DE red mud; blast furnace slag; geopolymer-based materials
ID INORGANIC POLYMERS; BAUXITE RESIDUE; WASTE; IRON
AB The aluminum Bayer production process is widespread all over the world. One of
the waste products of the Bayer process is a basic aluminosilicate bauxite residue
called red mud. The aluminosilicate nature of red mud makes it suitable as a
precursor for alkali-activated materials. In this work, red mud was mixed with
different percentages of blast furnace slag and then activated by sodium silicate
solution at different SiO2/Na2O ratios. Obtained samples were characterized by
chemical-physical analyses and compressive strength determination. Very high values
of compressive strength, up to 50 MPa, even for high percentage of red mud in the
raw mixture (70 wt.% of RM in powder mixture), were obtained. In particular, the
higher compressive strength was measured for cubic samples containing 50 wt.% of
RM, which showed a value above 70 MPa. The obtained mixtures were characterized by
no or scarce environmental impact and could be used in the construction industry as
an alternative to cementitious and ceramic materials.
C1 [Occhicone, Alessio; Ferone, Claudio] Univ Naples Parthenope, Ctr Direz, Dept
Engn, Isola C4, I-80143 Naples, Italy.
[Vukcevic, Mira; Boskovic, Ivana] Univ Montenegro, Fac Met & Technol, Dzordza
Vasingtona bb, Podgorica 81000, Montenegro.
C3 Parthenope University Naples; University of Montenegro
RP Occhicone, A (corresponding author), Univ Naples Parthenope, Ctr Direz, Dept
EM alessio.occhicone001@studenti.uniparthenope.it; mirav@ucg.ac.me;
ivabo@ac.me; claudio.ferone@uniparthenope.it
RI Occhicone, Alessio/IUP-2528-2023; Ferone, Claudio/C-1175-2017
OI Occhicone, Alessio/0000-0002-3652-4987; Boskovic,
Ivana/0000-0001-5923-1215; Ferone, Claudio/0000-0002-8660-3771
FU Italian Ministry of Foreign Affairs and International Cooperation
FX This study was funded by a grant from the Italian Ministry of Foreign
Affairs and International Cooperation.
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NR 43
TC 15
Z9 15
U1 5
U2 37
PU MDPI
PI BASEL
EI 2071-1050
J9 SUSTAINABILITY-BASEL
JI Sustainability
PD OCT
PY 2021
VL 13
IS 20
AR 11298
DI 10.3390/su132011298
PG 15
WC Green & Sustainable Science & Technology; Environmental Sciences;
Environmental Studies
(SSCI)
GA WS7YT
UT WOS:000715394900001
OA gold
DA 2023-12-05
ER
PT J
AU Wang, JJ
Zhang, LF
Cheng, G
Ren, Q
Ren, Y
AF Wang, Ju-jin
Zhang, Li-feng
Cheng, Gong
Ren, Qiang
Ren, Ying
TI Dynamic mass variation and multiphase interaction among steel, slag,
lining refractory and nonmetallic inclusions: Laboratory experiments and
mathematical prediction
LA English
DT Article
DE mass transfer; steel; slag; lining refractory; nonmetallic inclusions;
kinetic model
ID KINETIC-MODEL; STAINLESS-STEEL; MOLTEN STEEL; BEHAVIOR; METAL;
DESULFURIZATION; THERMODYNAMICS; GLAZE; MGO
AB The mass transfer among the multiphase interactions among the steel, slag,
lining refractory, and nonmetallic inclusions during the refining process of a
bearing steel was studied using laboratory experiments and numerical kinetic
prediction. Experiments on the system with and without the slag phase were carried
out to evaluate the influence of the refractory and the slag on the mass transfer.
A mathematical model coupled the ion and molecule coexistence theory, coupled-
reaction model, and the surface renewal theory was established to predict the
dynamic mass transfer and composition transformation of the steel, the slag, and
nonmetallic inclusions in the steel. During the refining process, Al2O3 inclusions
transformed into MgO inclusions owing to the mass transfer of [Mg] at the
steel/refractory interface and (MgO) at the slag/refractory interface. Most of the
aluminum involved in the transport entered the slag and a small part of the
aluminum transferred to lining refractory, forming the Al2O3 or MgO center dot
Al2O3. The slag had a significant acceleration effect on the mass transfer. The
mass transfer rate (or the reaction rate) of the system with the slag was
approximately 5 times larger than that of the system without the slag. In the first
20 min of the refining, rates of magnesium mass transfer at the steel/inclusion
interface, steel/refractory interface, and steel/slag interface were x, 1.1x, and
2.2x, respectively. The composition transformation of inclusions and the mass
transfer of magnesium and aluminum in the steel were predicted with an acceptable
accuracy using the established kinetic model.
C1 [Wang, Ju-jin; Cheng, Gong; Ren, Ying] Univ Sci & Technol Beijing, Sch Met &
Ecol Engn, Beijing 100083, Peoples R China.
[Zhang, Li-feng] Yanshan Univ, State Key Lab Metastable Mat Sci & Technol,
Qinhuangdao 066004, Hebei, Peoples R China.
[Ren, Qiang] Yanshan Univ, Sch Mech Engn, Qinhuangdao 066004, Hebei, Peoples R
China.
C3 University of Science & Technology Beijing; Yanshan University; Yanshan
University
RP Ren, Y (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol Engn,
Beijing 100083, Peoples R China.; Zhang, LF (corresponding author), Yanshan Univ,
State Key Lab Metastable Mat Sci & Technol, Qinhuangdao 066004, Hebei, Peoples R
China.
EM zhanglifeng@ysu.edu.cn; yingren@ustb.edu.cn
RI Wang, Jujin/GQA-4492-2022
OI Wang, Jujin/0000-0001-8849-8592
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NR 46
TC 15
Z9 15
U1 4
U2 34
PU SPRINGER
PI NEW YORK
SN 1674-4799
EI 1869-103X
PD AUG
PY 2021
VL 28
IS 8
BP 1298
EP 1308
DI 10.1007/s12613-021-2304-4
PG 11
Mineral Processing
GA TX8QA
UT WOS:000683350100006
DA 2023-12-05
ER
PT J
AU König, K
Traven, K
Pavlin, M
Ducman, V
AF Konig, Katja
Traven, Katja
Pavlin, Majda
Ducman, Vilma
TI Evaluation of locally available amorphous waste materials as a source
for alternative alkali activators
LA English
DT Article
DE Alkali-activated materials; Alternative activators; Waste glass; Waste
mineral wool; Cathode-ray tube glass; Solubility
ID RICE HUSK ASH; SODIUM-SILICATE; GLASS POWDER; GEOPOLYMER; CEMENT;
MICROSTRUCTURE; DISSOLUTION; STRENGTH; SLAG
AB The production of alkali-activated materials with excellent mechanical
performance requires the use of water glass, which has a significant carbon
footprint. Such materials can have a lower carbon footprint if we replace water
glass with alternative activators sourced from waste. In this study, we assessed
the suitability of locally available amorphous waste materials (stone wool, glass
wool, bottle glass and cathode-ray tube glass) as a source for the preparation of
alternative alkali activators. We quantified the amount of silicon and aluminium
dissolved in the activator solutions via inductively coupled plasma-optical
emission spectrometry. The alternative activators were then used to produce alkali-
activated fly ash and slag. The compressive strength values of alkali-activated fly
ash specimens upon the addition of NaOH, water glass and the most promising
alternative activator were 38.98 MPa, 31.34 MPa and 40.37 MPa, respectively. The
compressive strength of slag specimens activated with alternative activators with
the highest concentration of dissolved silicon (21 g/L) was, however, 70% higher
than the compressive strength of slag specimens activated with only 10 M sodium
hydroxide. The compressive strength of slag specimens with the addition of the most
promising alternative activator was significantly lower (3.5 MPa) than the
compressive strength of those that had been activated by commercial water glass
(34.3 MPa).
C1 [Konig, Katja; Traven, Katja; Pavlin, Majda; Ducman, Vilma] ZAG Ljubljana,
Dimiceva 12, Ljubljana 1000, Slovenia.
RP Ducman, V (corresponding author), ZAG Ljubljana, Slovenian Natl Bldg & Civil
Engn Inst, Dimiceva 12, Ljubljana 1000, Slovenia.
EM vilma.ducman@zag.si
RI Pavlin, Majda/ABF-1585-2021; Pavlin, Majda/AAA-1892-2022
OI Pavlin, Majda/0000-0002-1701-8130; Ducman, Vilma/0000-0002-6430-3305
FU Slovenian Research Agency, Slovenia [J2-9197]
FX We acknowledge financial support from the Slovenian Research Agency,
Slovenia, through project No. J2-9197: Synthesis and characterization of
alkali activated foams based on different waste..
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NR 40
TC 15
Z9 15
U1 2
U2 14
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD FEB 15
PY 2021
VL 47
IS 4
DI 10.1016/j.ceramint.2020.10.059
EA JAN 2021
PG 10
GA PT5WU
UT WOS:000608686200004
DA 2023-12-05
ER
PT J
AU Panchmatia, P
Olvera, R
Genedy, M
Juenger, MCG
van Oort, E
AF Panchmatia, Parth
Olvera, Raul
Genedy, Moneeb
Juenger, Maria C. G.
van Oort, Eric
TI Shrinkage behavior of Portland and geopolymer cements at elevated
temperature and pressure
SO JOURNAL OF PETROLEUM SCIENCE AND ENGINEERING
LA English
DT Article
DE Fly ash (FA); Geopolymer; Chemical shrinkage; Autogenous shrinkage;
Expansive agents
ID ACTIVATED FLY-ASH; AUTOGENOUS SHRINKAGE; MECHANISMS; PERFORMANCE;
METAKAOLIN; HYDRATION; SLAG
AB Zonal isolation by cement barriers can be compromised in many different ways.
Among the most important are shrinkage of cementing slurries and contamination of
slurries with non-aqueous drilling fluids (NADF) during displacement. Class F fly
ash (FA) based alkali-activated materials, referred to as geopolymers, have shown
better compatibility with NADFs than ordinary Portland cement (OPC) slurries. This
study questioned whether the geopolymer slurries also show enhanced performance
with respect to shrinkage behavior compared to OPC slurries, especially at relevant
downhole temperatures and pressures. A novel testing technique was developed to
measure the autogenous shrinkage of OPC and geopolymer slurries subjected to
temperatures and pressures ranging up to 80 degrees C (175 degrees F) and 13.8 MPa
(2000 psi). The testing demonstrated that the total autogenous shrinkage increased
for OPC slurries and decreased for geopolymer slurries with increase in testing
temperature from 40 degrees C (104 degrees F) to 80 degrees C (175 degrees F). In
addition, an increase in testing pressure from 1.38 MPa (200 psi) to 13.8 MPa (2000
psi) resulted in a significant increase in the autogenous shrinkage for OPC
slurries when tested at 40 degrees C (104 degrees F). Furthermore, it was found
that the addition of zinc- and aluminum-based expansive agents was effective in
mitigating OPC shrinkage. A zinc-based expansive agent was particularly effective
at shrinkage mitigation for geopolymers subjected to 80 degrees C (175 degrees F)
and 13.8 MPa (2000 psi) confining pressure.
C1 [Panchmatia, Parth; Genedy, Moneeb] Univ Texas Austin, Hildebrand Dept Petr &
Geosyst Engn, Austin, TX 78712 USA.
[Olvera, Raul] Univ Texas Austin, Dept Civil & Environm Engn, Austin, TX 78712
USA.
[Juenger, Maria C. G.] Univ Texas Austin, Dept Civil Architectural & Environm
Engn, Austin, TX 78712 USA.
[van Oort, Eric] Univ Texas Austin, Hildebrand Dept Petr & Geosyst Engn, JJ King
Chair Engn, Austin, TX 78712 USA.
[Panchmatia, Parth] Kansas State Univ, Dept Civil Engn, 2113 Fiedler Hall,1701C
Platt St, Manhattan, KS 66506 USA.
C3 University of Texas System; University of Texas Austin; University of
Texas System; University of Texas Austin; University of Texas System;
University of Texas Austin; University of Texas System; University of
Texas Austin; Kansas State University
RP van Oort, E (corresponding author), Univ Texas Austin, Hildebrand Dept Petr &
Geosyst Engn, JJ King Chair Engn, Austin, TX 78712 USA.
EM vanoort@austin.utexas.edu
FU PQ Corporation; ConocoPhillips; BP; Wellset; Total; Cenovus
FX We would like to thank the members of the CODA consortium, namely PQ
Corporation, ConocoPhillips, BP, Wellset, Total, and Cenovus for their
support, guidance, and expertise. In particular, a special thank you to
Munir Aldin and William Mickelson from Metarock Laboratories, for
assisting in the development and execution of the diaphragm accumulator
test. Furthermore, we would like to thank BYK for providing expansive
agents used in this study.
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NR 45
TC 15
Z9 15
U1 4
U2 27
PU ELSEVIER
PI AMSTERDAM
SN 0920-4105
EI 1873-4715
J9 J PETROL SCI ENG
JI J. Pet. Sci. Eng.
PD DEC
PY 2020
VL 195
AR 107884
DI 10.1016/j.petrol.2020.107884
PG 8
WC Energy & Fuels; Engineering, Petroleum
GA OM4NH
UT WOS:000586002900193
DA 2023-12-05
ER
PT J
AU Sun, GW
Zhang, JJ
Yan, N
AF Sun, Guowen
Zhang, Jianjian
Yan, Na
TI Microstructural evolution and characterization of ground granulated
blast furnace slag in variant pH
LA English
DT Article
DE Ground granulated blast furnace slag; Activation mechanism; pH value;
Hydration products; Glass phase
ID ACTIVATOR TYPE; STRENGTH; CEMENT; TEMPERATURE; DISSOLUTION; HYDROLYSIS;
KINETICS; CHLORIDE
AB In order to explore the difference of the activation effect on the ground
granulated blast furnace slag (GGBFS) subjected to variant activators as well as to
further clarify the depolymerization mechanism of GGBFS, investigation on the
dissolved mechanism, hydrated characteristics and microstructural evolution were
carried out based on slag immersed in solutions with variant pH, and FTIR, NMR,
XRD, SEM and EDS were used to analyze structure of GGBFS, the change of valence and
bond, structural coordination, hydrated products, micromorphology and elements
distribution. The results show that the H+ destroyed the structure of GGBFS, and a
small amount of akermanite and gehlenite particles were formed on the surface of
slag, Ca2+, Mg2+ and Al(OH)(2+) ions were released as 3 <= pH < 7. For the pH < 3,
cauliflower-like chabazite particles were accumulated, and the dissolved Si and Al
gradually formed monomeric siloxane and hydrated aluminium complex ion [Al(H2O)(6)]
(3+), respectively. The H+ ionized by the water eroded the slag surface and
corrugated melilite particles, together with a layer of Si(OH)(4) and Al(OH)(3) gel
attached on the slag surface for pH = 7. As 7 < pH <= 12, the hydrated magnesium
aluminate and calcite particles were generated on the slag surface, and Ca2+, Mg2+
and Al(OH)(4)(-) ions were released under the influence of OH-. The Si-O-Al bond
was destructed and the monomers of Al(OH)(4)(-) and Si(OH)(4) were released for pH
> 12. The Si(OH)(4) and Al(OH)(4)(-) performed polycondensation in the presence of
the cations such as Ca2+, and that finally led to formation of large number C-(A)-
S-H with a corrugated morphology. (C) 2020 Elsevier Ltd. All rights reserved.
C1 [Sun, Guowen] Shijiazhuang Tiedao Univ, State Key Lab Mech Behav & Syst Safety
Traff Engn, Shijiazhuang 050043, Hebei, Peoples R China.
[Sun, Guowen; Zhang, Jianjian; Yan, Na] Shijiazhuang Tiedao Univ, Sch Mat Sci &
Engn, Shijiazhuang 050043, Hebei, Peoples R China.
C3 Shijiazhuang Tiedao University; Shijiazhuang Tiedao University
RP Sun, GW (corresponding author), Shijiazhuang Tiedao Univ, State Key Lab Mech
Behav & Syst Safety Traff Engn, Shijiazhuang 050043, Hebei, Peoples R China.; Sun,
GW (corresponding author), Shijiazhuang Tiedao Univ, Sch Mat Sci & Engn,
Shijiazhuang 050043, Hebei, Peoples R China.
EM sunguowen_2003@163.com
RI Zhang, Jianjian/IXD-6660-2023; zhang, jianjian/AAI-1432-2019; yan,
na/HDM-3747-2022
OI Zhang, Jianjian/0000-0001-7427-7641; zhang,
jianjian/0000-0002-5220-1280;
FU National Natural Science Foundations of China [51778378, 51478278]
FX This work was supported by the National Natural Science Foundations of
China (No. 51778378 and 51478278).
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NR 35
TC 15
Z9 15
U1 2
U2 33
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD AUG 10
PY 2020
VL 251
AR 118978
DI 10.1016/j.conbuildmat.2020.118978
PG 15
GA LR8FG
UT WOS:000535931400057
DA 2023-12-05
ER
PT J
AU Tian, C
Yuan, L
Yu, JK
Jia, DB
Yao, XL
Wen, TP
AF Tian, Chen
Yuan, Lei
Yu, Jingkun
Jia, Danbin
Yao, Xinglong
Wen, Tianpeng
TI Effect of External Electric Field Application on the Clogging Behavior
of Submerged Entry Nozzles During Aluminum-Killed Steel Casting
LA English
DT Article
ID NONMETALLIC INCLUSIONS; LIQUID-METAL; MECHANISM; OXIDE; EVOLUTION;
FERRITE; SLAG
AB Clogging behavior has been investigated by applying a direct current on a
submerged entry nozzle (SEN). The relevant experimental results verify that the
high-speed friction acting on the SEN not only leads to charging of the inclusions,
but also inhibits the clogging behavior and improves the quality of the steel.
After DC treatment, the formation of clogging in the SEN decelerates and the
stability improves, such that the density of clogging increases and the porosity of
clogging decreases significantly. Meanwhile, after applying a DC electric field,
the overall quality of steel is also improved.
C1 [Tian, Chen; Yuan, Lei; Yu, Jingkun; Jia, Danbin; Yao, Xinglong; Wen, Tianpeng]
Northeastern Univ, Sch Met, Shenyang 110819, Peoples R China.
[Yu, Jingkun] Northeastern Univ, State Key Lab Rolling & Automat, Shenyang
C3 Northeastern University - China; Northeastern University - China
RP Yuan, L (corresponding author), Northeastern Univ, Sch Met, Shenyang 110819,
Peoples R China.
EM yuanl@smm.neu.edu.cn
FU National Natural Science Foundation of China [51974074, 51874083]; State
Key Program of National Natural Science Foundation of China [51932008];
Fundamental Research Funds for the Central Universities [N2025036,
N182504009]
FX The authors express their gratitude for the financial support from the
National Natural Science Foundation of China (Grant Nos. 51974074,
51874083), the State Key Program of National Natural Science Foundation
of China (Grant No. 51932008) and the Fundamental Research Funds for the
Central Universities (Grant N2025036, N182504009).
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Engineering
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DA 2023-12-05
ER
PT J
AU Kurda, R
Silva, RV
de Brito, J
AF Kurda, Rawaz
Silva, Rui Vasco
de Brito, Jorge
TI Incorporation of Alkali-Activated Municipal Solid Waste Incinerator
Bottom Ash in Mortar and Concrete: A Critical Review
SO MATERIALS
LA English
DT Review
DE alkali-activated materials; municipal waste incinerated ashes; strength;
durability; construction materials
ID BLAST-FURNACE SLAG; FLY-ASH; COMPRESSIVE STRENGTH; GEOPOLYMER CONCRETE;
RED MUD; MECHANICAL-PROPERTIES; SILICA FUME; DURABILITY PROPERTIES;
HIGH-VOLUME; ENGINEERING PROPERTIES
AB In the light of one of the most common waste management issues in urban areas,
namely the elimination of municipal solid waste (MSW; about 486 kg of the waste per
capita were generated in the EU in 2017), this study discusses one technique as an
outlet in the construction industry for the by-product of the waste's incineration
in energy recovery facilities (i.e., MSW incinerator bottom ash-MIBA). There have
been some investigations on the use of MIBA as partial replacement of cement to be
used in cementitious composites, such as concrete and mortars. However, the waste's
incorporation ratio is limited since further products of hydration may not be
produced after a given replacement level and can lead to an unsustainable decline
in performance. In order to maximize the incorporation of MIBA, some research
studies have been conducted on the alkali activation of the waste as precursor.
Thus, this study presents an extensive literature review of the most relevant
investigations on the matter to understand the material's applicability in
construction. It analyses the performance of the alkali-activated MIBA as paste,
mortar, and concrete from different perspectives. This literature review was made
using search engines of several databases. In each database, the same search
options were repeated using combinations of various representative keywords.
Furthermore, several boundaries were made to find the most relevant studies for
further inspection. The main findings of this review have shown that the chemical
composition and reactivity of MIBA vary considerably, which may compromise
performance comparison, standardization and commercialization. There are several
factors that affect the performance of the material that need to be considered,
e.g., type and content of precursor, alkaline activator, curing temperature and
time, liquid to solid ratio, among others. MIBA-based alkali-activated materials
(AAM) can be produced with a very wide range of compressive strength (0.3-160 MPa).
The main factor affecting the performance of this precursor is the existence of
metallic aluminum (Al), which leads to damaging expansive reactions and an increase
in porosity due to hydrogen gas generation stemming from the reaction with the
alkaline activator. Several approaches have been proposed to eliminate this issue.
The most effective solution was found to be the removal of Al by means of eddy
current electromagnetic separation.
C1 [Kurda, Rawaz] Erbil Polytech Univ, Dept Civil Engn, Tech Engn Coll, Erbil
44001, Kurdistan Regio, Iraq.
[Kurda, Rawaz] Nawroz Univ, Sci Res & Dev Ctr, Duhok 42001, Kurdistan Regio,
Iraq.
[Kurda, Rawaz; Silva, Rui Vasco; de Brito, Jorge] Univ Lisbon, Inst Super Tecn,
Civil Engn Architecture & Georesources Dept, CERIS, Av Rovisco Pais, P-1049001
Lisbon, Portugal.
C3 Erbil Polytechnic University; Universidade de Lisboa; Instituto Superior
Tecnico
RP de Brito, J (corresponding author), Univ Lisbon, Inst Super Tecn, Civil Engn
Architecture & Georesources Dept, CERIS, Av Rovisco Pais, P-1049001 Lisbon,
Portugal.
EM rawaz.kurda@epu.edu.iq; rui.v.silva@tecnico.ulisboa.pt;
jb@civil.ist.utl.pt
RI Silva, Rui Vasco/D-5814-2013; Kurda, Rawaz/N-4955-2018; de Brito,
Jorge/A-4299-2008; Silva, Ana/JGM-6679-2023
OI Silva, Rui Vasco/0000-0002-2276-9721; Kurda, Rawaz/0000-0003-2429-4755;
de Brito, Jorge/0000-0001-6766-2736;
FU FCT-Foundation for Science and Technology [PTDC/ECI-CON/29196/2017];
Fundação para a Ciência e a Tecnologia [PTDC/ECI-CON/29196/2017] Funding
Source: FCT
FX This research was funded by FCT-Foundation for Science and Technology,
through the research project PTDC/ECI-CON/29196/2017 "Recycled Inorganic
Polymer Concrete: Towards a fully recycled and cement-free concrete"
(RInoPolyCrete).
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PT J
AU Majdinasab, A
Yuan, QY
AF Majdinasab, Alireza
Yuan, Qiuyan
TI Synthesis of Al-substituted 11Å tobermorite using waste glass cullet: A
study on the microstructure
LA English
DT Article
DE Tobermorite; Calcium silicate hydrate; Waste glass cullet;
Microstructure; Al-substitution
ID C-S-H; CALCIUM SILICATE HYDRATE; BLAST-FURNACE SLAG; HYDROTHERMAL
SYNTHESIS; CRYSTAL-STRUCTURE; CEMENT HYDRATION; FLY-ASH; MODEL;
SOLIDIFICATION; ALUMINUM
AB Calcium silicate hydrate (CSH), the key by-product of Portland cement hydration,
due to the structural resemblance, is mainly represented as a defect tobermorite
analog. To provide an extensive overview on the impact of Al incorporation in CSH,
synthesis of Al-substituted 11 angstrom tobermorite using waste glass cullet (WGC)
was investigated and compared with an Al-free reference. The optimal parameters of
180 degrees C curing temperature, 5h curing time, 0.5 M of activator concentration,
and Ca/Si of 0.83 were found via XRD to synthesize pure crystalline tobermorite.
SEM micrographs also showed that Al incorporation changed the tobermorite
morphology from platy-like shape to acicular crystals. The WGC synthesized
tobermorite exhibited similar thermal behavior to reference tobermorite as observed
via TGA/DSC such as the free water release at 55 degrees C, interlayer water
release at 131 degrees C, Si-O-H bond cleavage at 680 degrees C, and
recrystallization to wollastonite at 820 degrees C. Si-29 and Al-27 NMR analysis
showed that Al substitution preferably occurred at bridging (Q(2)) and branching
(Q(3)) positions. The results from this study could significantly contribute to the
application of Al-based wastes in concrete and mortar construction to improve the
microstructure of the hydration by-products.
C1 [Majdinasab, Alireza; Yuan, Qiuyan] Univ Manitoba, Dept Civil Engn, Winnipeg, MB
R3T 5V6, Canada.
C3 University of Manitoba
RP Yuan, QY (corresponding author), Univ Manitoba, Dept Civil Engn, Winnipeg, MB
R3T 5V6, Canada.
EM qiuyan.yuan@umanitoba.ca
FU Manitoba Liquor & Lotteries Corporation; Mitacs [IT08384]
FX The authors gratefully acknowledge the financial support from the
Manitoba Liquor & Lotteries Corporation and Mitacs (IT08384).
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NR 52
TC 15
Z9 15
U1 7
U2 30
PI LAUSANNE
SN 0254-0584
EI 1879-3312
J9 MATER CHEM PHYS
PD AUG 1
PY 2020
VL 250
AR 123069
DI 10.1016/j.matchemphys.2020.123069
PG 14
GA LY2MF
UT WOS:000540353500043
DA 2023-12-05
ER
PT J
AU Shedekar, VS
Penn, CJ
Pease, L
King, KW
Kalcic, MM
Livingston, SJ
AF Shedekar, Vinayak S.
Penn, Chad J.
Pease, Lindsay
King, Kevin W.
Kalcic, Margaret M.
Livingston, Stan J.
TI Performance of a Ditch-Style Phosphorus Removal Structure for Treating
Agricultural Drainage Water with Aluminum-Treated Steel Slag
SO WATER
LA English
DT Article
DE Ohio; case study; subsurface drainage; dissolved phosphorus; phosphorus
transport; phosphorus sorption materials; tile drainage; water quality;
algal bloom; eutrophication
ID INDUSTRIAL BY-PRODUCTS; LAKE-ERIE; RE-EUTROPHICATION; REDUCTION;
PHOSPHATE; RUNOFF
AB Several structural, treatment, and management approaches exist to minimize
phosphorus (P) transport from agricultural landscapes (e.g., cover cropping and
conservation tillage). However, many of these practices are designed to minimize
particulate P transport and are not as effective in controlling dissolved P (DP)
losses. Phosphorus removal structures employ a P sorption material (PSM) to trap DP
from flowing water. These structures have been successful in treating surface
runoff by utilizing aluminum (Al)-treated steel slag, but subsurface tile drainage
has never been tested with this material. The goal of this study was to evaluate
the performance and economics of a ditch-style P removal structure using Al-treated
steel slag for treating agricultural subsurface drainage discharge. The structure
treated subsurface drainage water from a 4.5 ha agricultural field with elevated
soil test P levels. Overall, the structure removed approximately 27% and 50% of all
DP and total P (TP) entering the structure, respectively (i.e., 2.4 and 9.4 kg DP
and TP removal). After an initial period of strong DP removal, the discrete DP
removal became highly variable. Flow-through analysis of slag samples showed that
the slag used to construct the structure was coarser and less sorptive compared to
the slag samples collected prior to construction that were used to design and size
the structure. Results of this study highlight the importance of correctly
designing the P removal structures using representative PSMs.
C1 [Shedekar, Vinayak S.; Kalcic, Margaret M.] Ohio State Univ, Dept Food Agr &
Biol Engn, Columbus, OH 43210 USA.
[Penn, Chad J.; Livingston, Stan J.] USDA ARS, Natl Soil Eros Lab, W Lafayette,
IN 47907 USA.
[Pease, Lindsay] Univ Minnesota Twin Cities, Dept Soil Water & Climate,
Crookston, MN 56716 USA.
[King, Kevin W.] USDA ARS, Soil Drainage Res Unit, Columbus, OH 43210 USA.
[Kalcic, Margaret M.] Ohio State Univ, Translat Data Analyt Inst, Columbus, OH
43210 USA.
C3 University System of Ohio; Ohio State University; United States
Department of Agriculture (USDA); University of Minnesota System;
University of Minnesota Twin Cities; United States Department of
Agriculture (USDA); University System of Ohio; Ohio State University
RP Shedekar, VS (corresponding author), Ohio State Univ, Dept Food Agr & Biol Engn,
Columbus, OH 43210 USA.
EM shedekar.1@osu.edu; chad.penn@usda.gov; 1pease@umn.edu;
kevin.king@usda.gov; kalcic.4@osu.edu; stan.livingston@usda.gov
RI Shedekar, Vinayak/ABF-1273-2021
OI Shedekar, Vinayak/0000-0003-2028-2108; Pease,
Lindsay/0000-0002-1276-8493; Penn, Chad/0000-0003-2644-6097
FU USDA Natural Resources Conservation Service (NRCS) Mississippi River
Basin Initiative (MRBI); USDA Conservation Effects Assessment Project
(CEAP)
FX Funding for this research was in part from USDA Natural Resources
Conservation Service (NRCS) Mississippi River Basin Initiative (MRBI)
and Conservation Effects Assessment Project (CEAP). This research is a
contribution from the USDA Long-Term Agroecosystem Research (LTAR)
network.
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NR 38
TC 15
Z9 17
U1 1
U2 12
PU MDPI
PI BASEL
EI 2073-4441
J9 WATER-SUI
JI Water
PD AUG
PY 2020
VL 12
IS 8
AR 2149
DI 10.3390/w12082149
PG 16
WC Environmental Sciences; Water Resources
SC Environmental Sciences & Ecology; Water Resources
GA NH4OI
UT WOS:000564650700001
OA gold
DA 2023-12-05
ER
PT J
AU Bae, SJ
Park, S
Lee, HK
AF Bae, S. J.
Park, Solmoi
Lee, H. K.
TI Role of Al in the crystal growth of alkali-activated fly ash and slag
under a hydrothermal condition
LA English
DT Article
DE Alkali-activated binder; Hydrothermal condition; Al2O3; MgO;
Thermodynamic modeling; Hydrotalcite; Zeolite; Characterization
ID MESOPOROUS GEOPOLYMERS; PHASE EVOLUTION; MGO; ZEOLITES; GEL;
CARBONATION; ADSORPTION; GMELINITE; STRENGTH; ALUMINUM
AB The present study investigates the role of Al in the evolution of the
crystalline phases of an alkali-activated binder. Samples were synthesized
corresponding to the binder composition with various Al2O3/Na2O and MgO/binder
ratios in a hydrothermal condition. Thermodynamic modelling was carried out to
predict the effect of the Al content in the binder composition on the formation of
Al-bearing phases. The test results showed that an increasing Al content led to the
alteration of the predominant zeolite phases in the alkali-activated binder. In
addition, MgO incorporation enhanced the reaction degree of hydration in the
alkali-activated system and the crystal growth, specifically hydrotalcite-like
phase. Consequently, the formed reaction products had a great effect on the pore
characteristics of the alkali-activated binder given their variations in the
crystal structure. (C) 2019 Elsevier Ltd. All rights reserved.
C1 [Bae, S. J.; Park, Solmoi; Lee, H. K.] Korea Adv Inst Sci & Technol, Dept Civil
& Environm Engn, 291 Daehak Ro, Daejeon 34141, South Korea.
[Park, Solmoi] Korea Adv Inst Sci & Technol, Appl Sci Res Inst, 291 Daehak Ro,
Daejeon 34141, South Korea.
C3 Korea Advanced Institute of Science & Technology (KAIST); Korea Advanced
Institute of Science & Technology (KAIST)
RP Lee, HK (corresponding author), Korea Adv Inst Sci & Technol, Dept Civil &
Environm Engn, 291 Daehak Ro, Daejeon 34141, South Korea.
EM haengki@kaist.ac.kr
RI Park, Solmoi/AHE-4311-2022; Lee, Haeng Ki/C-1640-2011; Park,
Solmoi/AAD-5326-2019; Park, Solmoi/AAA-5658-2022
OI Park, Solmoi/0000-0003-0746-3940; Lee, H.K./0000-0002-7259-4229
FU Technology Advancement Research Program (TARP) - Ministry of Land,
infrastructure and Transport of Korean government [19CTAP-C143331-02]
FX This research was supported by a grant (19CTAP-C143331-02) from
Technology Advancement Research Program (TARP) funded by Ministry of
Land, infrastructure and Transport of Korean government.
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[Anonymous], ROLE ALUMINIUM CONTE
[Anonymous], CRUCIAL INSIGHTS MIX
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[Anonymous], CERAM SOC
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NR 58
TC 15
Z9 15
U1 1
U2 23
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD APR 10
PY 2020
VL 239
AR 117842
DI 10.1016/j.conbuildmat.2019.117842
PG 12
GA KW9OZ
UT WOS:000521514300019
DA 2023-12-05
ER
PT J
AU Prostakova, V
Shishin, D
Shevchenko, M
Jak, E
AF Prostakova, Viktoria
Shishin, Denis
Shevchenko, Maksym
Jak, Evgueni
TI Thermodynamic optimization of the
Al2O3-FeO-Fe2O3-SiO2</s
ub> oxide system
LA English
DT Article
DE Thermodynamic modeling; Slags; Alumina; Silica; Iron oxide; Phase
diagrams
ID QUASI-CHEMICAL MODEL; IRON-ALUMINUM-OXYGEN; PHASE-EQUILIBRIA;
HEAT-CAPACITY; LIQUIDUS TEMPERATURES; MULLITE; PART; SOLUBILITY;
AL2O3-SIO2; SUBSOLIDUS
AB A complete literature review, critical assessment, and thermodynamic modeling of
the phase diagrams and thermodynamic properties of oxide phases in the Al2O3-FeO-
Fe2O3-SiO2 system at a total pressure of 1 atm are presented. A set of optimized
model parameters for all phases was obtained to reproduce all previously published
thermodynamic and phase equilibrium data. Some discrepancies in the literature data
were identified, particularly for liquidus measurements and the Fe3+/(Fe2+ + Fe3+)
ratio in the slag phase (liquid oxide phase) at high temperatures. Analysis of
internal consistency with the Al2O3-FeO-Fe2O3, FeO-Fe2O3-SiO2 and Al2O3-SiO2 sub-
systems allowed to resolve the discrepancies. Previously published model parameters
for the slag phase in the Al2O3-FeO-Fe2O3 system were slightly modified to achieve
better overall agreement. The final set of model parameters for oxide phases
reproduces all available data within experimental error limits. The Modified
Quasichemical Model was used for modeling of the slag phase. The models based on
the Compound Energy Formalism were applied for spinel and mullite solid oxide
solutions. The database of model parameters optimized in the present study can be
used along with software for Gibbs energy minimization to describe thermodynamic
equilibria at all compositions and oxygen partial pressures, from the lowest
corresponding to equilibrium with metal up to the highest P(O-2) of 1 atm. The
database was incorporated into the larger database for the multicomponent Al-Ca-Cu-
Fe-Mg-Pb-Zn-O-S-Si-(As, Sb, Bi, Sn, Ag, Au, Ni) chemical system and successfully
used for calculations of equilibria relevant to copper, lead, zinc smelting and
recycling.
C1 [Prostakova, Viktoria; Shishin, Denis; Shevchenko, Maksym; Jak, Evgueni] Univ
Queensland, Sch Engn, Pyromet Innovat Ctr, Brisbane, Qld 4072, Australia.
RP Prostakova, V (corresponding author), Univ Queensland, Sch Engn, Pyromet Innovat
Ctr, Brisbane, Qld 4072, Australia.
EM v.prostakova@uq.edu.au
RI Shishin, Denis/AAE-5199-2020; Shevchenko, Maksym/HNP-0886-2023
OI Shishin, Denis/0000-0003-2734-1078; Shevchenko,
Maksym/0000-0002-9420-9336; Jak, Evgueni/0000-0002-7768-1874
FU Australian Research Council [LP140100480]; Atlantic Copper; Aurubis; BHP
Billiton Olympic Dam Operation; Kazzinc Glencore; PASAR Glencore;
Outotec Oy (Espoo); Anglo American Platinum; Umicore; Rio Tinto
Kennecott; Boliden; Australian Research Council [LP140100480] Funding
Source: Australian Research Council
FX The authors would like to thank the Australian Research Council Linkage
program LP140100480, and industry partners, Atlantic Copper, Aurubis,
BHP Billiton Olympic Dam Operation, Kazzinc Glencore, PASAR Glencore,
Outotec Oy (Espoo), Anglo American Platinum, Umicore, Rio Tinto
Kennecott, and Boliden for the financial and technical support for this
research.
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NR 86
TC 15
Z9 15
U1 3
U2 26
PI OXFORD
SN 0364-5916
EI 1873-2984
J9 CALPHAD
PD DEC
PY 2019
VL 67
AR 101680
DI 10.1016/j.calphad.2019.101680
PG 16
Engineering
GA JU8QV
UT WOS:000501935500013
DA 2023-12-05
ER
PT J
AU Ye, HL
Chen, ZJ
AF Ye, Hailong
Chen, Zhijian
TI Influence of Nitrate Corrosion Inhibitors on Phase Stability of
Alkali-Activated Slag against Chloride Binding and Natural Carbonation
LA English
DT Article
DE Alkali-activated binder; Slag; Nitrate-based corrosion inhibitors;
Chloride; Carbonation
ID LAYERED DOUBLE HYDROXIDES; REINFORCED-CONCRETE; MG; HYDROTALCITES
AB Nitrate and nitrite-based corrosion inhibitors have been studied for decades for
mitigating corrosion of steel embedded in ordinary portland cement (OPC) concrete;
however, few studies are available regarding the effect of nitrate or nitrite on
the performance of alkali-activated binders. This work, for the first time,
investigates the influence of three nitrate-containing activators (i.e., sodium
nitrate, magnesium nitrate, and aluminum nitrate, each mixed with sodium hydroxide
solution) on the strength development, pore structure, phase assemblage, and phase
stability of alkali-activated slag (AAS) binders upon exposure to chloride and
natural carbonation. The results show that the addition of nitrate, regardless of
its form, does not substantially alter the type of main reacted phases, i.e.,
calcium-aluminosilicate-hydrate (C-A-S-H) and Mg-Al layered double hydroxides
(LDHs), in AAS; however, the addition of aluminum nitrate improves its compressive
strength, boosts the formation of Ca-Al LDHs (AFm-type phase), and likely inserts
nitrate anions in the interlayer of formed Ca-Al or Mg-Al LDHs. The findings
suggest that the nitrate-intercalated Ca-Al LDHs and/or Mg-Al LDHs, if formed to
some extent, can potentially release nitrate ions during chloride binding and
carbonation, working as a smart corrosion inhibitor.
C1 [Ye, Hailong; Chen, Zhijian] Univ Hong Kong, Dept Civil Engn, Pokfulam, Hong
Kong, Peoples R China.
C3 University of Hong Kong
RP Ye, HL (corresponding author), Univ Hong Kong, Dept Civil Engn, Pokfulam, Hong
Kong, Peoples R China.
EM hlye@hku.hk; zchen31@connect.hku.hk
OI Ye, Hailong/0000-0003-2665-3942
FU Hong Kong Research Grants Council [27204818]; National Natural Science
FX The authors would like to thank the financial support from the Hong Kong
Research Grants Council (Project No. 27204818) and National Natural
Science Foundation of China (Project No. 51808475). Any opinions,
findings, and conclusions or recommendations expressed in this material
are those of the authors and do not necessarily reflect the views of the
sponsors.
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NR 30
TC 15
Z9 16
U1 9
U2 59
PI RESTON
SN 0899-1561
EI 1943-5533
PD AUG 1
PY 2019
VL 31
IS 8
AR 04019160
DI 10.1061/(ASCE)MT.1943-5533.0002830
PG 7
GA ID6WB
UT WOS:000471820600028
DA 2023-12-05
ER
PT J
AU Duan, SC
Shi, X
Wang, F
Zhang, MC
Li, B
Yang, WS
Guo, HJ
Guo, J
AF Duan, Sheng-Chao
Shi, Xiao
Wang, Fei
Zhang, Man-Cang
Li, Bin
Yang, Wen-Sheng
Guo, Han-Jie
Guo, Jing
TI Investigation of desulfurization of Inconel 718 superalloys by ESR type
slags with different TiO2 content
LA English
DT Article
DE Nickel-based alloy; Desulfurization mechanism; Specific reaction
interface; Oxygen activity; Mass transfer model; Ion and molecule
coexistence theory
ID NI-BASE SUPERALLOY; METAL-SULFUR SYSTEMS; THERMODYNAMIC PROPERTIES;
STAINLESS-STEEL; PHASE-RELATIONSHIPS; ALLOYING ELEMENTS; TITANIUM;
NICKEL; ALUMINUM; KINETICS
AB In the present study, effect of CaF2-CaO-Al2O3-MgO-TiO2 slag with various TiO2
contents on the desulfurization of Inconel 718 alloy was investigated at 1773 K to
provide the fundamental information for the establishment of desulfurization
procedure during electroslag remelting (ESR) process. The melt-quenching method did
not accurately determine the change in content of sulfur and oxygen in the nickel-
based alloy with time for the present study, which uses a novel experimental
apparatus. The results indicated that the final sulfur content in the nickel-based
alloy increased from 7 to 9 ppm when the TiO2 content in slag of CaF2-CaO-Al2O3-
MgO-TiO2 system increased from 2.17 to 10% without addition of deoxidizer. In order
to further expound the desulfurization mechanism, meanwhile, the relationship
between the oxygen activity at slag-metal interface and reaction time under
conditions of various TiO2 in the slag was studied by coupling with the developed
mass transfer model. The calculated oxygen content in bulk metal has a good
corresponding relationship with the measured oxygen content in the nickel-based
alloy. The oxygen activity at slag-metal interface increased up to 9.6 ppm when
TiO2 content was 10% in the slag, giving rise to the decrease in desulfurization
ratio in high TiO2 content. The optimal condition for simultaneously ensuring low
sulfur content and maintaining oxidative elements, such as Al and Ti, uniformly
from bottom to top of the ESR ingot is also discussed. (C) 2019 The Authors.
Published by Elsevier B.V.
C1 [Duan, Sheng-Chao; Shi, Xiao; Zhang, Man-Cang; Li, Bin; Yang, Wen-Sheng; Guo,
Han-Jie; Guo, Jing] Univ Sci & Technol Beijing, Sch Met & Ecol Engn, Beijing
[Duan, Sheng-Chao; Shi, Xiao; Zhang, Man-Cang; Li, Bin; Yang, Wen-Sheng; Guo,
Han-Jie; Guo, Jing] Univ Sci & Technol Beijing, Beijing Key Lab Special Melting &
Preparat High E, Beijing 100083, Peoples R China.
[Wang, Fei] CISRI, Res Inst High Temp Mat, Beijing 100081, Peoples R China.
Technology Beijing; Central Iron & Steel Research Institute
RP Duan, SC; Guo, HJ (corresponding author), Univ Sci & Technol Beijing, Sch Met &
Ecol Engn, Beijing 100083, Peoples R China.; Duan, SC; Guo, HJ (corresponding
author), Univ Sci & Technol Beijing, Beijing Key Lab Special Melting & Preparat
High E, Beijing 100083, Peoples R China.
EM Metall_DSC@163.com; mighty_works@163.com; 18046511210@163.com;
zmc5125@163.com; libin4962337@163.com; yws3179608@163.com;
guohanne@ustb.edu.cn; guojingzq@163.com
RI Li, Bin/IQT-8772-2023; Duan, Shengchao/M-1269-2017
OI Li, Bin/0000-0002-2404-9971; Guo, Han-jie/0000-0002-6493-8853; Duan,
Shengchao/0000-0001-5007-3601
FU National Natural Science Foundation of China [U1560203, 51704021]
FX The authors would like to express their sincere thanks to senior
engineer Li-hui Han of National Experimental Teaching Demonstration
Center for Metallurgical Engineering at University of Science and
Technology Beijing (USTB) for helping to do experiments, Ph.D.
Candidates Bin Li and Shao-ying Li of School of Metallurgical and
Ecological Engineering as well as as Prof. Cheng-bin Shi of State Key
Laboratory of Advanced Metallurgy (SKL) at University of Science and
Technology Beijing (USTB) contributed to the discussion of the results.
The authors are also thankful for the support from the National Natural
Science Foundation of China (Nos. U1560203 and 51704021).
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NR 57
TC 15
Z9 15
U1 7
U2 35
PI AMSTERDAM
SN 2238-7854
EI 2214-0697
PD MAY-JUN
PY 2019
VL 8
IS 3
BP 2508
EP 2516
DI 10.1016/j.jmrt.2019.01.027
PG 9
Engineering
GA IC1YM
UT WOS:000470755800004
OA gold
DA 2023-12-05
ER
PT J
AU Meng, FQ
Liu, WZ
Chu, GR
Yue, HR
Liang, B
Wang, LM
Li, C
AF Meng, Fanqi
Liu, Weizao
Chu, Guanrun
Yue, Hairong
Liang, Bin
Wang, Liming
Li, Chun
TI Phase Diagrams of
(NH4)2SO4-Al2(SO4
)3-H2O Ternary System: Effect of Sulfuric Acid and
Its Application in Recovery of Aluminum from Coal Fly Ash
SO JOURNAL OF CHEMICAL AND ENGINEERING DATA
LA English
DT Article
ID AMMONIUM-SULFATE
AB Coal fly ash (CFA) is the powdery waste generated in coal-fired power plants.
The content of Al2O3 in CFA can be up to 40 wt % and can serve as an alternative to
bauxite for aluminum production. Recently, the ammonium sulfate (AS) roasting
process has attracted wide interest for extracting aluminum from CFA. During the
process, aluminum enters the leaching solution and forms the (NH4)(2)SO4-Al-2(SO4)
(3)-H2O ternary system or (NH4)(2)SO4-Al-2(SO4)(3)-H2SO4-H2O quaternary system. In
this study, the aforementioned phase equilibrium data were measured using the
isothermal method to minimize the water used in the leaching unit. The results
showed that the crystallization fields of NH4Al(SO4)(2)center dot 12H(2)O were
larger than those of other species, which indicates that it will easily
crystallize. The presence of H2SO4 at a concentration of 2.5 wt % had nearly no
effect on the solubilities of (NH4)(2)SO4 and Al-2(SO4)(3) but 10 wt % H2SO4
decreases the solubilities at high temperature. According to the composition of the
roasted slag obtained at 500 degrees C, the minimal liquid-to-solid ratio during
the leaching unit was calculated as 3.32 and 1.4 mL/g at SS and 80 degrees C,
respectively. Following crystallization at 25 degrees C, NH4Al(SO4)(2)center dot
12H(2)O can be recovered at crystallization ratios of 44.58% and 60.89% with
leaching at 55 and 80 degrees C, respectively. A modified process, high-temperature
leaching with cooling crystallization, is proposed. Compared to the original
process, the liquid-to-solid ratio can be decreased by approximately 66.8% and 86%
at 55 and 80 degrees C, respectively. As a result, the energy consumption during
the (NH4)(2)SO4 recycling is significantly reduced.
C1 [Meng, Fanqi; Liu, Weizao; Chu, Guanrun; Yue, Hairong; Liang, Bin; Li, Chun]
Sichuan Univ, Sch Chem Engn, Chengdu 610065, Sichuan, Peoples R China.
[Wang, Liming] Sichuan Univ, Hitech Grp Co Ltd, Chengdu 610065, Sichuan, Peoples
R China.
C3 Sichuan University; Sichuan University
RP Liu, WZ; Li, C (corresponding author), Sichuan Univ, Sch Chem Engn, Chengdu
610065, Sichuan, Peoples R China.
EM weizaol@163.com; lic@scu.edu.cn
RI Wang, Liming/N-9512-2015; Liang, Bin/JHU-0581-2023; yue,
Hairong/D-1874-2013
OI Wang, Liming/0000-0002-9470-2112; Liu, Weizao/0000-0003-0976-2864
[2016YFB0600904]; Fundamental Research Funds for the Central
(2016YFB0600904) and the Fundamental Research Funds for the Central
Universities (2012017yjsy112).
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NR 18
TC 15
Z9 16
U1 2
U2 32
PI WASHINGTON
SN 0021-9568
J9 J CHEM ENG DATA
JI J. Chem. Eng. Data
PD FEB
PY 2019
VL 64
IS 2
BP 557
EP 566
DI 10.1021/acs.jced.8b00740
PG 10
WC Thermodynamics; Chemistry, Multidisciplinary; Engineering, Chemical
SC Thermodynamics; Chemistry; Engineering
GA HM1PM
UT WOS:000459224500020
DA 2023-12-05
ER
PT J
AU Unver, IK
Terzi, M
AF Unver, I. Kursun
Terzi, M.
TI Distribution of trace elements in coal and coal fly ash and their
recovery with mineral processing practices: A review
SO JOURNAL OF MINING AND ENVIRONMENT
LA English
DT Review
DE Coal; Trace Elements; Fly Ash; Utilization
ID FIRED POWER-PLANTS; HEAVY-METALS; ANTIOXIDANT NUTRIENTS; RADIOACTIVE
ELEMENTS; IRON TOXICITY; BEHAVIOR; TURKEY; RADIONUCLIDES; COMBUSTION;
EXTRACTION
AB Today coal is among the most important energy sources. In order to meet the
world's energy demands, low-calorie lignite with a high ash content is generally
used in the large capacity coal-fired thermal power plants. As a result of coal
firing, wastes such as fly ash, slag, and flue gas are also produced. Subsequently,
toxic trace elements within coal are transferred to wastes such as slag, fly ash,
and flue gases. Large amounts of these, which are usually stored in collection
ponds or stockpiles, are problematic in terms of environment. Although coal fly ash
(CFA) has been utilized in construction and several other industries for decades,
its current ratio of utilization is still quite limited. As an important fact, CFA
also contains many valuable metals including germanium (Ge), gallium (Ga), vanadium
(V), titanium (Ti), and aluminum (Al). In addtion, coal and CFA can be regarded as
alternative sources of radioactive elements. Therefore, they also have a great
potential in terms of the precious metals and trace elements they contain. In this
study, the present literature on the distribution of trace elements in coal and
coal ash during firing and ore preparation processes and their recovery
possibilities with mineral processing practices are reviewed. While many research
works on the subject clearly indicate that the large amounts of the ashes produced
from firing of coal could be problematic in terms of environment, many studies and
practices also show that coal combustion products also have a great potential in
terms of the precious metals and trace elements.
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C3 Istanbul University
RP Unver, IK (corresponding author), Istanbul Univ, Dept Min Engn, Fac Engn,
Istanbul, Turkey.
EM ilginkur@istanbul.edu.tr
RI Terzi, Mert/C-6841-2019; Kursun, İlgin/C-6871-2019
OI Terzi, Mert/0000-0002-6727-4191; Kursun, İlgin/0000-0001-7348-6054
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NR 71
TC 15
Z9 17
U1 4
U2 52
PU SHAHROOD UNIV TECHNOLOGY
PI SHAHROUD
PA SHAHROOD UNIV TECHNOLOGY, SHAHROUD, SEMNAN 00000, IRAN
SN 2251-8592
EI 2251-8606
J9 J MIN ENVIRON
JI J. Min. Environ.
PD SUM
PY 2018
VL 9
IS 3
BP 641
EP 655
DI 10.22044/jme.2018.6855.1518
PG 15
WC Mining & Mineral Processing
SC Mining & Mineral Processing
GA GQ8BT
UT WOS:000441975600008
DA 2023-12-05
ER
PT J
AU Wang, Q
Liu, Y
Li, GQ
Gao, YM
He, Z
Li, BK
AF Wang, Qiang
Liu, Yu
Li, Guangqiang
Gao, Yunming
He, Zhu
Li, Baokuan
TI Predicting transfer behavior of oxygen and sulfur in electroslag
remelting process
SO APPLIED THERMAL ENGINEERING
LA English
DT Article
DE Electroslag remelting; Deoxidation; Desulfurization; Numerical
simulation
ID DESULFURIZATION BEHAVIOR; MATHEMATICAL-MODEL; HEAT-TRANSFER; SIMULATION;
STEEL; FLOW; SLAG
AB A transient three-dimensional (3D) comprehensive mathematical model has been
developed to understand oxygen and sulfur transfers in electroslag remelting
process. The solutions of the mass, momentum, energy and species conservation
equations were simultaneously carried out by finite volume method. The Joule
heating and Lorentz force were taken into account. The thermochemical and
electrochemical transfers of oxygen and sulfur were represented through the
application of a metallurgical thermodynamic and kinetic module. In order to obtain
the evolution of oxygen activity, the chemical reaction between dissolved aluminum
and dissolved oxygen in the metal was included. The comparison between the measured
and simulated data indicates that the model can predicate the transfer behavior
with an acceptable accuracy. The thermochemical reaction always removes oxygen and
sulfur from the metal, while the electrochemical reaction brings oxygen and sulfur
back to the metal through the metal droplet-slag interface, and takes them away
from the metal through the metal pool-slag interface. The oxygen removal ratio is
about 60%, and the contribution of the electrochemical reaction is around 82%. The
sulfur removal ratio is approximately 76%, and the contribution of the
electrochemical reaction is around 39%. (C) 2017 Elsevier Ltd. All rights reserved.
C1 [Wang, Qiang; Liu, Yu; Li, Guangqiang; Gao, Yunming; He, Zhu] Wuhan Univ Sci &
Technol, State Key Lab Refractories & Met, Wuhan 430081, Hubei, Peoples R China.
[Wang, Qiang; Liu, Yu; Li, Guangqiang; Gao, Yunming; He, Zhu] Wuhan Univ Sci &
Technol, Key Lab Ferrous Met & Resources Utilizat, Minist Educ, Wuhan 430081,
Hubei, Peoples R China.
[Li, Baokuan] Northeastern Univ, Sch Met, Shenyang 110819, Liaoning, Peoples R
China.
C3 Wuhan University of Science & Technology; Wuhan University of Science &
Technology; Northeastern University - China
RP Li, GQ (corresponding author), Wuhan Univ Sci & Technol, State Key Lab
Refractories & Met, Wuhan 430081, Hubei, Peoples R China.
EM liguangqiang@wust.edu.cn
RI , Yunming/AAE-5050-2020; Li, Guangqiang/HGE-8046-2022
OI , Yunming/0000-0001-8082-615X; Li, Guangqiang/0000-0002-4471-7439
FU National Natural Science Foundation of China [51210007, U1508214]; China
Postdoctoral Science Foundation [2016M600620]; Government of Liaoning
Province [U1508214]
FX The authors' gratitude goes to National Natural Science Foundation of
China (Grant No. 51210007) and the Key Program of Joint Funds of the
National Natural Science Foundation of China and the Government of
Liaoning Province (Grant No. U1508214), and China Postdoctoral Science
Foundation Funded Project (Grant No. 2016M600620).
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TC 15
Z9 21
U1 2
U2 26
PI OXFORD
SN 1359-4311
J9 APPL THERM ENG
JI Appl. Therm. Eng.
PD JAN 25
PY 2018
VL 129
BP 378
EP 388
DI 10.1016/j.applthermaleng.2017.10.062
PG 11
WC Thermodynamics; Energy & Fuels; Engineering, Mechanical; Mechanics
SC Thermodynamics; Energy & Fuels; Engineering; Mechanics
GA FR9QF
UT WOS:000419407500037
DA 2023-12-05
ER
PT J
AU Shi, CC
Wu, GH
Zhang, L
Zhang, XL
AF Shi, Chunchang
Wu, Guohua
Zhang, Liang
Zhang, Xiaolong
TI Al-5.5Mg-1.5Li-0.5Zn-0.07Sc-0.07Zr alloy produced by gravity casting and
heat treatment processing
SO MATERIALS AND MANUFACTURING PROCESSES
LA English
DT Article
DE Aging; Al-Mg-Li; casting; dislocation; elongation; hardening; PFZs;
solution; strength
ID AL-LI ALLOY; ALUMINUM-LITHIUM ALLOYS; MECHANICAL-PROPERTIES; MG ALLOY;
MICROSTRUCTURE; BEHAVIOR; ZR; NUCLEATION; EVOLUTION; MN
AB Al-5.5Mg-1.5Li-0.5Zn-0.07Sc-0.07Zr alloy was produced by gravity casting and
heat treatment processing. After gravity casting based on the melting processing
scheme designed specifically for the studied alloy, there was no obvious porosity
and slag. In as-cast alloy, there were many network-shaped second phase particles
enriched along the grain boundaries, most of which integrated into the -Al matrix
after solution heat treated at 500 degrees C for 10h. The grain growth was
inconspicuous, which means low grain boundary stress concentration resulted by
planar slip. To meet the requirement for industrial actuality, avoid the
excessively detrimental effect of PFZs and utilize the order hardening effect of
(Al3Li) phases sufficiently, 175 degrees C/8h was preferred as the aging regime.
Optimal comprehensive mechanical properties were obtained after solid solution heat
treated process (500 degrees C/10h) and subsequent aging treatment (175 degrees
C/8h) with elongation, yield strength, and ultimate tensile strength reaching 8.7%,
270.5MPa, and 435.5MPa, respectively.
C1 [Wu, Guohua; Zhang, Liang] Shanghai Jiao Tong Univ, Natl Engn Res Ctr Light
Alloy Net Forming, Shanghai 200240, Peoples R China.
[Wu, Guohua; Zhang, Liang] Shanghai Jiao Tong Univ, State Key Lab Met Matrix
Composites, Shanghai, Peoples R China.
C3 Shanghai Jiao Tong University; Shanghai Jiao Tong University
RP Wu, GH; Zhang, L (corresponding author), Shanghai Jiao Tong Univ, Natl Engn Res
Ctr Light Alloy Net Forming, Shanghai 200240, Peoples R China.; Wu, GH; Zhang, L
(corresponding author), Shanghai Jiao Tong Univ, State Key Lab Met Matrix
Composites, Shanghai, Peoples R China.
EM ghwu@sjtu.edu.cn; liangzhang08@sjtu.edu.cn
RI Zhang, Xiaolong/AAK-5077-2021
OI Shi, Chunchang/0000-0002-6553-6231; Zhang, Xiaolong/0000-0002-5322-0475;
zhang, liang/0000-0002-2694-1779; Wu, Guohua/0000-0001-5089-4354
FU National Key R&D Program of China [2016YFB0301003]; National Natural
Science Foundation of China [51404153]
FX This project is sponsored in part by the National Key R&D Program of
China (No. 2016YFB0301003) and National Natural Science Foundation of
China (No. 51404153).
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NR 35
TC 15
Z9 15
U1 2
U2 38
PI PHILADELPHIA
SN 1042-6914
EI 1532-2475
J9 MATER MANUF PROCESS
JI Mater. Manuf. Process.
PY 2018
VL 33
IS 8
BP 891
EP 897
DI 10.1080/10426914.2017.1401725
PG 7
WC Engineering, Manufacturing; Materials Science, Multidisciplinary
GA FW6QJ
UT WOS:000425442900013
DA 2023-12-05
ER
PT J
AU Sun, AX
Chang, YB
Liu, HJ
AF Sun, Aixi
Chang, Yubo
Liu, Hongjun
TI Metal micro-hole formation without recast layer by laser machining and
electrochemical machining
SO OPTIK
LA English
DT Article
DE Laser machining; Electrochemical machining; No recast layer; Metal
micro-hole; Optimized parameters
ID ALLOY; OPTIMIZATION; SIMULATION; ALUMINUM; STEEL
AB Laser machining and electrochemical machining (LM-ECM) of metal micro-hole is
presented in this study. Millisecond pulsed laser etches metallic materials by
thermal effect, and electrochemical machining removes recast layer. No recast layer
is produced on the wall of metal micro holes. Machining accuracy and efficiency are
improved. Prefabricated micro-hole modeling of laser machining and metal micro-hole
modeling of electrochemical machining are established. The main process parameters
of LM-ECM are determined by the models. Effects of the process parameters on
experimental results are investigated and the optimized parameters are given.
Comparison between LM-ECM and single machining approaches is made. The experimental
results revealed that the material surface of LM-ECM is cleaner than single laser
machining and do not have molten slag. There is no recast layer on the wall of the
micro-holes. Compared to single electrochemical machining, the efficiency and
accuracy of LM-ECM are improved by 51.35% and 30.43% respectively.
C1 [Sun, Aixi] Nanjing Univ Sci & Technol, Sch Mech Engn, Nanjing 210094, Jiangsu,
Peoples R China.
[Chang, Yubo] Nanjing Inst Adv Laser Technol, Nanjing 210038, Jiangsu, Peoples R
China.
[Liu, Hongjun] Shenyang Aerosp Univ, Sch Mechatron Engn, Shenyang 110136,
C3 Nanjing University of Science & Technology; Shenyang Aerospace
University
RP Liu, HJ (corresponding author), Shenyang Aerosp Univ, Sch Mechatron Engn,
EM 13386878635@163.com
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NR 20
TC 15
Z9 15
U1 6
U2 69
PU ELSEVIER GMBH
PI MUNICH
PA HACKERBRUCKE 6, 80335 MUNICH, GERMANY
SN 0030-4026
EI 1618-1336
J9 OPTIK
JI Optik
PY 2018
VL 171
BP 694
EP 705
DI 10.1016/j.ijleo.2018.06.099
PG 12
WC Optics
SC Optics
GA GT6WD
UT WOS:000444660700091
DA 2023-12-05
ER
PT J
AU Sánchez-Hernández, R
Padilla, I
López-Andrés, S
López-Delgado, A
AF Sanchez-Hernandez, Ruth
Padilla, Isabel
Lopez-Andres, Sol
Lopez-Delgado, Aurora
TI Eco-friendly bench-scale zeolitization of an Al-containing waste into
gismondine-type zeolite under effluent recycling
LA English
DT Article
DE Aluminum waste; Eco-friendly zeolitization; Bench-scale; NaP1; Mother
liquor recycling; High-CEC zeolite
ID COAL FLY-ASH; NAP ZEOLITE; HYDROTHERMAL SYNTHESIS; REMOVAL;
CRYSTALLIZATION; SLAG
AB The feasibility of developing an eco-friendly bench-scale zeolitization process
of NaP1 from an Al-containing waste and under recycling of effluents was evaluated.
Prior lab-scale tests were performed to optimize the synthesis conditions. The
mixture of effluents, i.e., mother liquors (ML) from the synthesis and rinse water
(RW) from the cleaning step of the zeolites, was recycled several times to study
the reduction of raw materials (NaOH and water) and accordingly the reduction of
costs. The bench-scale process allows the complete transformation of the waste into
NaP1 zeolite, reaching equivalent reaction yields (2.5 ton of zeolite per ton of
waste) to the lab-scale process and avoiding the generation of new solid residues.
The effect of the recycling of effluents on the physical-chemical properties of the
resulting zeolites was investigated. NaP1 zeolite was the only crystalline phase
obtained, showing morphological, textural and crystalline characteristics closely
similar to NaP1 synthesized from fresh NaOH aqueous solutions and from pure
chemical reagents. NaOH and water consumption savings of 80 and 67%, respectively,
were obtained, representing a cost reduction around 70%. These results show that
the bench-scale process to obtain NaP1 from an Al-waste with recycling of effluents
can be a more sustainable alternative compared with the traditional synthesis
methods. (C) 2017 Elsevier Ltd. All rights reserved.
C1 [Sanchez-Hernandez, Ruth; Padilla, Isabel; Lopez-Delgado, Aurora] CSIC, Natl Ctr
Met Res, Avda Gregorio Amo 8, Madrid 28040, Spain.
[Lopez-Andres, Sol] Univ Complutense Madrid, Dept Crystallog & Mineral, Fac
Geol, C Jose Antonio Novais 12, E-28040 Madrid, Spain.
C3 Consejo Superior de Investigaciones Cientificas (CSIC); Complutense
Amo 8, Madrid 28040, Spain.
RI Padilla, Isabel/I-2712-2015; Lopez-Delgado, Aurora/D-3785-2012; Padilla,
Isabel/AAI-8479-2021
OI Padilla, Isabel/0000-0001-7684-200X; Lopez-Delgado,
Aurora/0000-0002-0121-9501; Lopez-Andres, Sol/0000-0003-2052-1674;
Sanchez-Hernandez, Ruth/0000-0001-8624-3756
FU MINECO [CTM2012-34449, BES-2013-066269]
FX The authors thank: Recuperaciones y Reciclajes Roman S.L. and Metalquex
S.L. (Madrid and Zaragoza, Spain) for supplying the wastes, and Archroma
Company (Barcelona, Spain) for the use of its facilities. The authors
also thank MINECO for its financial support (Project CTM2012-34449). R.
Sanchez-Hernandez thanks MINECO for the grant BES-2013-066269.
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10.1016/j.micromeso.2016.01.037
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10.1016/j.micromeso.2014.09.033
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10.1016/j.micromeso.2007.06.002
NR 48
TC 15
Z9 15
U1 1
U2 39
PU ELSEVIER SCI LTD
PI OXFORD
SN 0959-6526
EI 1879-1786
J9 J CLEAN PROD
JI J. Clean Prod.
PD SEP 10
PY 2017
VL 161
BP 792
EP 802
DI 10.1016/j.jclepro.2017.05.201
PG 11
& Ecology
GA FD6RK
UT WOS:000407655400066
DA 2023-12-05
ER
PT J
AU Yang, JB
Li, DX
Fang, Y
AF Yang, Jingbin
Li, Dongxu
Fang, Yuan
TI Synthesis of Nanoscale
CaO-Al2O3-SiO2-H2O and
Na2O-Al2O3-SiO2-H2O Using the Hydrothermal Method and Their Characterization
SO MATERIALS
LA English
DT Article
DE C-A-S-H; N-A-S-H; hydrothermal method; alkali-activated materials;
micro-structure characterization
ID A-S-H; ACTIVATED SLAG; ALKALI-ACTIVATION; PHASE EVOLUTION; GEL BLENDS;
FLY-ASH; CALCIUM; ALUMINUM; GEOPOLYMERS; TOBERMORITE
AB C-A-S-H (CaO-Al2O3-SiO2-H2O) and N-A-S-H (Na2O-Al2O3-SiO2-H2O) have a wide range
of chemical compositions and structures and are difficult to separate from alkali-
activated materials. Therefore, it is difficult to analyze their microscopic
properties directly. This paper reports research on the synthesis of C-A-S-H and N-
A-S-H particles with an average particle size smaller than 300 nm by applying the
hydrothermal method. The composition and microstructure of the products with
different CaO(Na2O)/SiO2 ratios and curing conditions were characterized using XRD,
the RIR method, FTIR, SEM, TEM, and laser particle size analysis. The results
showed that the C-A-S-H system products with a low CaO/SiO2 ratio were mainly
amorphous C-A-S-H gels. With an increase in the CaO/SiO2 ratio, an excess of Ca(OH)
(2) was observed at room temperature, while in a high-temperature reaction system,
katoite, C4AcH11, and other crystallized products were observed. The katoite
content was related to the curing temperature and the content of Ca(OH)(2) at room
temperature were amorphous N-A-S-H gels and a small amount of sodalite. An increase
in the curing temperature promoted the formation of the crystalline products
faujasite and zeolite-P. The crystallization products consisted of only zeolite-P
in the high-temperature N-A-S-H system and its content were stable above 70%. An
increase in the Na2O/SiO2 ratio resulted in more non-bridging oxygen and the TO4
was more isolated in the N-A-S-H structure. The composition and microstructure of
the C-A-S-H and N-A-S-H system products synthesized by the hydrothermal method were
closely related to the ratio of the raw materials and the curing conditions. The
results of this study increase our understanding of the hydration products of
alkali-activated materials.
C1 [Yang, Jingbin; Li, Dongxu] Nanjing Tech Univ, Jiangsu Natl Synerget Innovat Ctr
Adv Mat SICAM, Nanjing 210009, Jiangsu, Peoples R China.
[Li, Dongxu; Fang, Yuan] Shenzhen Univ, Coll Civil Engn, Guangdong Prov Key Lab
Durabil Marine Civil Engn, Shenzhen 518060, Peoples R China.
C3 Nanjing Tech University; Shenzhen University
RP Fang, Y (corresponding author), Shenzhen Univ, Coll Civil Engn, Guangdong Prov
Key Lab Durabil Marine Civil Engn, Shenzhen 518060, Peoples R China.
EM yangjingbin@njtech.edu.cn; dongxuli@njtech.edu.cn; yuanfang@szu.edu.cn
OI Yang, Jingbin/0000-0001-5393-7583
FU National High Technology Research and Development Program of China
[2015AA034701]; Chinese National Natural Science Foundation [51508337,
51538007]; Natural Science Foundation of Guangdong Province
[2015A030310129]; Shenzhen Municipal Commission of Science and
Technology and Innovation [JCYJ20150324141711572]; Natural Science
Foundation of SZU [827000091]
FX This research was supported by National High Technology Research and
Development Program of China [Project No. 2015AA034701]; Chinese
National Natural Science Foundation [Project No. 51508337]; Chinese
National Natural Science Foundation [Project No. 51538007]; Natural
Science Foundation of Guangdong Province [Project No. 2015A030310129];
Shenzhen Municipal Commission of Science and Technology and Innovation
[Project No. JCYJ20150324141711572] and Natural Science Foundation of
SZU [Project No.827000091].
Baltakys K, 2015, REV ROM MATER, V45, P218
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2916.2010.03668.x
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1
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2916.2008.02450.x
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10.1016/j.cemconres.2016.08.010
NR 38
TC 15
Z9 15
U1 5
U2 60
PU MDPI
PI BASEL
SN 1996-1944
J9 MATERIALS
JI Materials
PD JUL
PY 2017
VL 10
IS 7
AR 695
DI 10.3390/ma10070695
PG 18
Physics
GA FC2QL
UT WOS:000406683000012
DA 2023-12-05
ER
PT J
AU Yang, CL
Wen, GH
Tang, P
AF Yang, Changlin
Wen, Guanghua
Tang, Ping
TI Non-Isothermal Crystallization Kinetics of Mold Fluxes Containing
Li2O for High Aluminum Steel Casting
LA English
DT Article
DE continuous casting; high aluminum steel; mold flux; crystallization
kinetics
ID HIGH AL STEEL; NA2O
AB When continuously casting high Al steels, CaO-SiO2 based mold fluxes can be
easier for sequence casting, but due to the significant reactions of the Al in the
metal with SiO2, slab surface quality is not desirable. When increasing basicity of
CaO-SiO2 based mold fluxes, slab surface quality can be improved, but thick slag
rim can easily be formed during cooling process. Therefore, non-isothermal
crystallization kinetics of mold fluxes used for high Al steels are studied to
optimize the crystallization behavior of "working" fluxes. Results indicate that
the addition of Li2O can decrease crystallization temperature and crystallization
rate within the range of Na2O studied. The Avrami exponent determined by Avrami
equation indicates that disk-like growth type and spherulitic-like growth type are
the main mechanisms in crystallization, which is consistent with results observed
under SEM. When mold flux contains 8% Na2O and 4.5% Li2O, the effective activation
energy is between -299 and -488 KJ mol(-1). When mold flux contains no Na2O and
6.5% Li2O, the effective activation energy is between -266 and -414 KJ mol(-1),
which indicates that Na2O-free mold fluxes containing high Li2O is beneficial for
improving crystallization characteristics and realizing sufficient lubrication.
C1 [Yang, Changlin; Wen, Guanghua; Tang, Ping] Chongqing Univ, Coll Mat Sci & Engn,
RP Yang, CL (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
EM yangcl@cqu.edu.cn
FU National Science Foundation [51274260]
FX The authors wish to express their gratitude to the National Science
Foundation (grant no. 51274260) for providing financial support which
enabled this study to be successfully carried out.
CR Abu-Sehly AA, 2009, J ALLOY COMPD, V476, P348, DOI 10.1016/j.jallcom.2008.08.059
Al-Ghamdi AA, 2011, J ALLOY COMPD, V509, P2087, DOI
10.1016/j.jallcom.2010.10.145
Fu X. J., 2014, STEEL RES INT, V86, P2
Garnier L, 2009, THERMOCHIM ACTA, V481, P32, DOI 10.1016/j.tca.2008.10.006
Ibar JP, 2013, J MACROMOL SCI B, V52, P950, DOI 10.1080/00222348.2012.746571
Jung S. S., 2014, ENVIRON SCI TECHNOL, V48, P3
Lin J., 2012, ISIJ INT, V52
Liu GT, 2014, J THERM ANAL CALORIM, V118, P1401, DOI 10.1007/s10973-014-4029-3
Street S., 2008, IRON STEEL TECHNOL, V5, P38
Wan H., 2011, J UNIV SCI TECHNOL B, V33, P5
Wang XD, 2008, METALL MATER TRANS A, V39A, P1, DOI 10.1007/s11661-007-9366-4
Wen G. H., 2007, ISIJ INT, V47, P8
Yan W., 2013, SPEC STEEL, V34, P1
Zhou L, 2015, METALL MATER TRANS E, V2, P99, DOI 10.1007/s40553-015-0047-8
NR 29
TC 15
Z9 16
U1 0
U2 16
PI WEINHEIM
SN 1611-3683
EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD JUL
PY 2016
VL 87
IS 7
BP 880
EP 889
DI 10.1002/srin.201500258
PG 10
GA DZ1PO
UT WOS:000385610500008
DA 2023-12-05
ER
PT J
AU Ren, S
Zhang, JL
Xing, XD
Su, BX
Wang, Z
Yan, BJ
AF Ren, S.
Zhang, J. L.
Xing, X. D.
Su, B. X.
Wang, Z.
Yan, B. J.
TI Effect of B2O3 on phase compositions of high Ti
bearing titanomagnetite sinter
LA English
DT Article
DE B2O3; High Ti bearing titanomagnetite sinter; Phase composition; Sinter
mechanisms
ID BLAST-FURNACE SLAG; IRON-ORE SINTER; REDUCTION DEGRADATION; VISCOSITY;
TEMPERATURE; MECHANISM; OXYGEN; STEEL; NA2O
AB The phase compositions of high Ti bearing titanomagnetite sinter with different
contents of B2O3 were studied at 1623 K under an oxygen partial pressure of 5 x
10(-3) atm. The results showed that B2O3 mainly gathered in Ca2SiO4 phase and
formed 2CaO center dot xSiO(2)center dot 2/3(1-x)(B2O3) phase. The appearance of
B2O3 can restrain the precipitation of CaTiO3 and 2CaO. xSiO(2)center dot 2/3(1-x)
(B2O3) and promote the amount of Fe bearing mineral phase in the current
experimental condition. In addition, the shape of CaTiO3 changed from bulk to strip
type with the increase in B2O3 content. The formula of silicoferrite of calcium and
aluminium changed from 1.6CaO center dot 4.9Fe(2)O(3)center dot Al2O3 center dot
1.8SiO(2) to 2.5CaO center dot 5.9Fe(2)O(3)center dot Al2O3 center dot 2.6SiO(2),
and the formula of dicalcium (boron) silicate changed from 2CaO center dot SiO2 to
2CaO center dot 0.33SiO(4)center dot 0.45B(2)O(3) when B2O3 content was from 0 to
2.0 mass-% in the sinter. The change of phase compositions with the addition of
B2O3 in the sinter will be beneficial for improving its metallurgical properties.
C1 [Ren, S.; Zhang, J. L.; Xing, X. D.; Su, B. X.; Wang, Z.; Yan, B. J.] Univ Sci &
Technol Beijing, Sch Met & Ecol Engn, Beijing 100083, Peoples R China.
[Ren, S.; Zhang, J. L.; Xing, X. D.; Su, B. X.; Wang, Z.; Yan, B. J.] Univ Sci &
Technology Beijing
RP Zhang, JL (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol
EM jeopardize@126.com
RI zhang, jian/HPD-1712-2023
OI Yan, Baijun/0000-0003-4306-9043
FU National Basic Research Program of China (973 Program) [2012CB720401];
Natural Science Foundation of China; Baosteel [51134008]
FX The present work was supported by National Basic Research Program of
China (973 Program) (grant no. 2012CB720401) and Natural Science
Foundation of China and Baosteel under grant no. 51134008.
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Jiang D. J., 2011, SINTERING PELLETIZIN, V37, P6
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0087-4
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NR 22
TC 15
Z9 16
U1 3
U2 17
PU MANEY PUBLISHING
PI LEEDS
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD AUG
PY 2014
VL 41
IS 7
BP 500
EP 506
DI 10.1179/1743281213Y.0000000145
PG 7
GA AW2UM
UT WOS:000346144700004
DA 2023-12-05
ER
PT J
AU Abbasalizadeh, A
Seetharaman, S
Teng, L
Sridhar, S
Grinder, O
Izumi, Y
Barati, M
AF Abbasalizadeh, Aida
Seetharaman, Seshadri
Teng, Lidong
Grinder, Olle
Izumi, Yukari
Barati, Mansoor
TI Highlights of the Salt Extraction Process
SO JOM
LA English
DT Article
ID EUTECTIC LICL-KCL
AB This article presents the salient features of a new process for the recovery of
metal values from secondary sources and waste materials such as slag and flue
dusts. It is also feasible in extracting metals such as nickel and cobalt from ores
that normally are difficult to enrich and process metallurgically. The salt
extraction process is based on extraction of the metals from the raw materials by a
molten salt bath consisting of NaCl, LiCl, and KCl corresponding to the eutectic
composition with AlCl3 as the chlorinating agent. The process is operated in the
temperature range 973 K (700 degrees C) to 1173 K (900 degrees C). The process was
shown to be successful in extracting Cr and Fe from electric arc furnace (EAF)
slag. Electrolytic copper could be produced from copper concentrate based on
chalcopyrite in a single step. Conducting the process in oxygen-free atmosphere,
sulfur could be captured in the elemental form. The method proved to be successful
in extracting lead from spent cathode ray tubes. In order to prevent the loss of
AlCl3 in the vapor form and also chlorine gas emission at the cathode during the
electrolysis, liquid aluminum was used. The process was shown to be successful in
extracting Nd and Dy from magnetic scrap. The method is a highly promising process
route for the recovery of strategic metals. It also has the added advantage of
being environmentally friendly.
C1 [Abbasalizadeh, Aida; Seetharaman, Seshadri; Teng, Lidong] Royal Inst Technol,
Stockholm, Sweden.
[Seetharaman, Seshadri; Grinder, Olle] Salt Extract AB, Stockholm, Sweden.
[Sridhar, Seetharaman] Univ Warwick, Coventry CV4 7AL, W Midlands, England.
[Izumi, Yukari] Kitakyushu Inst Technol, Kitakyushu, Fukuoka, Japan.
[Barati, Mansoor] Univ Toronto, Toronto, ON, Canada.
C3 Royal Institute of Technology; University of Warwick; University of
Toronto
RP Abbasalizadeh, A (corresponding author), Royal Inst Technol, Stockholm, Sweden.
EM aidaa@kth.se; raman@kth.se; lidong@kth.se; s.seetharaman@warwick.ac.uk;
grinder@algonet.se; HCA00324@nifty.com; mansoor.barati@utoronto.ca
CR Abbasalizadeh A., 2013, UNPUB
Abbasalizadeh A., 2012, 5 C ION LIQ COIL C P
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10.1016/j.electacta.2004.09.013
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0728(03)00092-5
Fukasawa K, 2011, J NUCL MATER, V414, P265, DOI 10.1016/j.jnucmat.2011.04.002
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Grinder S.S., 2009, Patent No. [WO 2009/139715 Al, 2009139715]
Hamel C, 2004, ELECTROCHIM ACTA, V49, P4467, DOI 10.1016/j.electacta.2004.05.003
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The Doe Run Company, GLASS REC OPT
Yamana H, 2006, J ALLOY COMPD, V408, P66, DOI 10.1016/j.jallcom.2005.04.104
NR 21
TC 15
Z9 17
U1 1
U2 32
PU SPRINGER
PI NEW YORK
SN 1047-4838
EI 1543-1851
J9 JOM-US
JI JOM
PD NOV
PY 2013
VL 65
IS 11
BP 1552
EP 1558
DI 10.1007/s11837-013-0752-7
PG 7
GA 258ZE
UT WOS:000327496400026
DA 2023-12-05
ER
PT J
AU Wu, L
Pei, F
Chen, Y
Li, SQ
AF Wu Long
Pei Fen
Chen Yu
Li Shi-qi
TI Experimental Study on Deep Desulfurizer in LF Process
LA English
DT Article
DE refining slag; deep-desulfurization; sulfur distribution ratio;
desulfurization rate
ID SLAGS
AB CaO-Al2O3-SiO2-CaF2-MgO was selected as the slag system for desulfurization in
LF process. The reaction between steel and slag during desulfurization has been
simulated by using Factsage software to study the influence of component on the
sulfur distribution ratio. In order to research the influence of CaO content,
aluminum powder content and its granularity on desulfurization, laboratory
experiments have been carried out in a 200 kg inductive furnace. Results showed
that the optimal composition of deep desulfurizer is w(CaO) = 64% and aluminium
powder 10% with a granularity of 30 pm. Industrial trials showed that the main
composition range of final slag in LF process is w(CaO) = 53. 0% - 57. 0%,
w(Al2O3), = 23. 4 % - 25. 1%, w(SiO2), = 8. 1% - 10. 0%, and w(CaF2) = 3. 2% - 4.
7%. The sulfur mass percent in steel is lower than 0. 0008% with a desulfurization
rate above 89%. According to the result of industrial production, this desulfurizer
could meet the production requirement for ultra-low sulfur steel, of which sulfur
mass percent is under 0. 0015%.
C1 [Wu Long; Li Shi-qi] Univ Sci & Technol Beijing, Met & Ecol Engn Sch, Beijing
[Pei Fen] Beijing Shenwu Environm & Energy Technol Co Grp, Beijing 102200,
Peoples R China.
[Chen Yu] Xinxing Pipes Xinjiang Resources Dev Ltd Co, Urumqi 830000, Xinjiang,
Peoples R China.
RP Wu, L (corresponding author), Univ Sci & Technol Beijing, Met & Ecol Engn Sch,
EM jieke8857@126.com
FU National Key Technology Research and Development Program in 11th
Five-Year Plan of China [2007BAF08B01-03]
FX Foundation Item:Item Sponsored by National Key Technology Research and
Development Program in 11th Five-Year Plan of China (2007BAF08B01-03)
CR CHEN Song-lin, 2009, STEELMAKING, V25, P37
[郝宁 HAO Ning], 2006, [北京科技大学学报, Journal of University Science and
Hong SC, 2007, MET MATER INT, V13, P439, DOI 10.3365/MMI.2007.12.439
[金利玲 JIN Liling], 2007, [北京科技大学学报, Journal of University Science and
LI Liang, 2007, RES IRON STEEL, V35, P8
Mauro P., 2005, P INT OFFSH POL ENG, P31
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[张彩军 ZHANG Caijun], 2006, [钢铁, Iron and Steel], V41, P31
NR 17
TC 15
Z9 16
U1 0
U2 6
PU SPRINGER
PI NEW YORK
SN 1006-706X
EI 2210-3988
PD APR
PY 2012
VL 19
IS 4
BP 17
EP 21
DI 10.1016/S1006-706X(12)60081-8
PG 5
GA 959ND
UT WOS:000305318300004
DA 2023-12-05
ER
PT J
AU Severin, T
Rehren, T
Schleicher, H
AF Severin, Thorsten
Rehren, Thilo
Schleicher, Helmut
TI Early metal smelting in Aksum, Ethiopia: copper or iron?
SO EUROPEAN JOURNAL OF MINERALOGY
LA English
DT Article
DE archaeometallurgy; iron; copper; smelting; Aksum; Ethiopia; archaeology;
slag; mass balance estimate
AB A selection of archaeometallurgical remains from the 3rd/4th century A.D., found
in Aksum, Ethiopia, were analysed in order to determine the nature of the process
by which they were produced, i.e. copper or iron smelting. Chemical and
mineralogical analyses excluded a relationship to copper smelting; instead, all
samples are consistent with a highly efficient iron smelting operation using the
bloomery process and slag tapping furnaces. A lateritic iron ore containing at
least 80 wt% FeO was smelted, resulting in an estimated one unit by weight of iron
metal produced for every unit by weight of slag left behind, and little erosion of
furnace wall material. The zoning of spinels, with chromium- and aluminium-rich
inner parts and mixed hercynitic-ulvitic outer rims, reflects the evolution of the
melt phase under strongly reducing conditions.
C1 [Rehren, Thilo] UCL Qatar, Education City, Doha, Qatar.
[Severin, Thorsten; Schleicher, Helmut] Univ Hamburg, Mineral Petrog Inst, D-
20146 Hamburg, Germany.
C3 University College Of London In Qatar; University of Hamburg
RP Rehren, T (corresponding author), UCL Qatar, POB 23689, Education City, Doha,
Qatar.
EM th.rehren@ucl.ac.uk
RI Schleicher, Helmut/E-4371-2018; Rehren, Thilo/C-1567-2008
OI Schleicher, Helmut/0000-0003-4972-3966; Rehren,
Thilo/0000-0002-9169-1198
FU Mineralogisch-Petrographisches Institut of the University of Hamburg;
Wolfson Archaeological Science Laboratory, UCL Institute of Archaeology
FX The study presented here is based on Professor Ziegert's research
project "Untersuchungen zu Ursachen, Verlauf und Folgen ausgewahlter
Umbruchsperioden der athiopischen Geschichte". We are grateful for his
encouragement to undertake this study, and the provision of the sample
material for analysis. The analytical work was carried out by Thorsten
Severin as part of the examination requirements for the degree of
Diplom-Geologe at the University of Hamburg. We gratefully acknowledge
the support from colleagues at the Mineralogisch-Petrographisches
Institut of the University of Hamburg (thin section sample preparation
and electron probe micro-analysis) and the Wolfson Archaeological
Science Laboratory, UCL Institute of Archaeology (powder preparation and
XRF analysis), respectively. We are grateful for the detailed comments
from the anonymous reviewers who helped to improve the quality of the
manuscript and illustrations. All remaining errors are ours.
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NR 39
TC 15
Z9 15
U1 0
U2 18
PU E SCHWEIZERBARTSCHE VERLAGSBUCHHANDLUNG
PI STUTTGART
PA NAEGELE U OBERMILLER, SCIENCE PUBLISHERS, JOHANNESSTRASSE 3A, D 70176
STUTTGART, GERMANY
SN 0935-1221
EI 1617-4011
J9 EUR J MINERAL
JI Eur. J. Mineral.
PD DEC
PY 2011
VL 23
IS 6
BP 981
EP 992
DI 10.1127/0935-1221/2011/0023-2167
PG 12
WC Mineralogy
WE Science Citation Index Expanded (SCI-EXPANDED); Arts & Humanities Citation
Index (A&HCI)
SC Mineralogy
GA 870KX
UT WOS:000298669300012
DA 2023-12-05
ER
PT J
AU Garcia-Valles, M
Avila, G
Martinez, S
Terradas, R
Nogués, JM
AF Garcia-Valles, M.
Avila, G.
Martinez, S.
Terradas, R.
Nogues, J. M.
TI Acoustic barriers obtained from industrial wastes
SO CHEMOSPHERE
LA English
DT Article
DE Al-slag; recycling; wastes; thermal insulate; acoustical insulation
ID PRESSED BODIES; RICH WASTES; SLUDGE; BEHAVIOR
AB Acoustic pollution is an environmental problem that is becoming increasingly
more important in our society. Likewise, the accumulation of generated waste and
the need for waste management are also becoming more and more pressing. In this
study we describe a new material-called PROUSO-obtained from industrial wastes.
PROUSO has a variety of commercial and engineering, as well as building,
applications. The main raw materials used for this environmentally friendly
material come from slag from the aluminium recycling process, dust from the marble
industry, foundry sands, and recycled expanded polystyrene from recycled packaging.
Some natural materials, such as plastic clays, are also used. To obtain PROUSO we
used a conventional ceramic process, forming new mineral phases and incorporating
polluted elements into the structure. Its physical properties make PROUSO an
excellent acoustic and thermal insulation material. It absorbs 95% of the sound in
the frequency band of the 500 Hz. Its compressive strength makes it ideal for use
in ceramic wall building. (C) 2008 Elsevier Ltd. All rights reserved.
C1 [Garcia-Valles, M.] Univ Barcelona, Dpt Cristallografia Mineral, E-08028
Barcelona, Spain.
Univ Barcelona, Dip Minerals, E-08028 Barcelona, Spain.
C3 University of Barcelona; University of Barcelona
RP Garcia-Valles, M (corresponding author), Univ Barcelona, Dpt Cristallografia
Mineral, E-08028 Barcelona, Spain.
EM maitegarciavalles@ub.edu
RI Martínez, Salvador/L-5777-2014; Garcia-Valles, Maite/L-5696-2014
OI Martínez, Salvador/0000-0002-3346-3947; Garcia-Valles,
Maite/0000-0003-1117-1705
CR [Anonymous], 2004, VII International Conference on Molten Slags and Salts
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NR 21
TC 15
Z9 17
U1 0
U2 18
PI OXFORD
SN 0045-6535
EI 1879-1298
J9 CHEMOSPHERE
JI Chemosphere
PD JUL
PY 2008
VL 72
IS 7
BP 1098
EP 1102
DI 10.1016/j.chemosphere.2008.03.039
PG 5
GA 331PL
UT WOS:000258024300016
PM 18514765
DA 2023-12-05
ER
PT J
AU Zhang, BQ
Fang, HS
Lu, L
Lai, MO
Ma, HT
Li, JG
AF Zhang, BQ
Fang, HS
Lu, L
Lai, MO
Ma, HT
Li, JG
TI Synthesis mechanism of an Al-Ti-C grain refiner master alloy prepared by
a new method
SO METALLURGICAL AND MATERIALS TRANSACTIONS A-PHYSICAL METALLURGY AND
MATERIALS SCIENCE
LA English
DT Article
ID MODEL
AB The mechanisms of in-situ synthesis of an Al-Ti-C grain-refiner master alloy,
prepared by adding a powder mixture of potassium titanium fluoride and carbon into
an aluminum melt, have been systematically studied. It was found that vigorous
reactions occurred at the initial stage of reaction and then slowed down. After
about 20 minutes, the reactions, which led the formation of blocky titanium
aluminides and submicron titanium carbides in the aluminum matrix, appeared to
reach completion. Potassium titanium fluoride reacted with aluminum and carbon at
724 degreesC and 736 degreesC, respectively, resulting in the formation of titanium
aluminides and titanium carbides in the aluminum matrix as well as in the formation
of a low-melting-point slag of binary potassium aluminofluorides. The reaction
between potassium titanium fluoride and carbon is believed to be the predominant
mechanism in the synthesis of TiC by this method.
C1 Tsing Hua Univ, Dept Mat Sci & Engn, Beijing 100084, Peoples R China.
C3 Tsinghua University
RP Zhang, BQ (corresponding author), Tsing Hua Univ, Dept Mat Sci & Engn, Beijing
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NR 19
TC 15
Z9 20
U1 0
U2 12
PI WARRENDALE
SN 1073-5623
J9 METALL MATER TRANS A
JI Metall. Mater. Trans. A-Phys. Metall. Mater. Sci.
PD AUG
PY 2003
VL 34A
IS 8
BP 1727
EP 1733
DI 10.1007/s11661-003-0316-5
PG 7
Engineering
GA 705MT
UT WOS:000184399400014
DA 2023-12-05
ER
PT S
AU Wegener, P
Krag, H
Rex, D
Bendisch, J
Klinkrad, H
AF Wegener, P
Krag, H
Rex, D
Bendisch, J
Klinkrad, H
BE Flury, W
Klinkrad, H
TI The orbital distribution and dynamics of solid rocket motor particle
clouds for an implementation into the master debris model
SO SPACE DEBRIS
SE ADVANCES IN SPACE RESEARCH
LA English
CT B0.2 Symposium of COSPAR Scientific Commission B on Space Debris at the
32nd COSPAR Scientific Assembly
CY JUL 12-19, 1998
CL NAGOYA, JAPAN
AB In its current 1997 release version the MASTER space debris model considers
orbital fragmentations to be the main source for the generation of space debris,
while other sources are not taken into account. For this reason, the actual
reference population is dominated by particles originating from 127 historical
fragmentation events, mainly explosions. Since these explosion fragments can not
account for aluminum oxide particles or paint materials identified in the course of
the chemical analysis of impact crater residuals, MASTER currently is upgraded to
cover additional source terms in its population generation module. Besides micro
debris sources like surface degradation or impact ejecta, generation mechanisms for
larger scale particles like NaK droplets will be considered in the next MASTER
release. Additionally, orbital firings of Solid Rocket Motors (SRMs) as a
contributor to both size regimes are planned to be included. To implement all these
additional source terms, a variety of sub-models reflecting the generation
processes had to be derived. In this context, the diversity of Al2O3 dust and slag
objects exhausted from SRM burns in terms of basic generation characteristics as
well as in orbital dynamcis of the particle cloud has been reviewed and results
documenting the influence of this source on the debris environment are presented.
(C) 1999 COSPAR. Published by Elsevier Science Ltd.
C1 Tech Univ Braunschweig, Inst Flight Mech & Spaceflight Technol, D-38106
Braunschweig, Germany.
ESOC, ESA, D-64293 Darmstadt, Germany.
C3 Braunschweig University of Technology; European Space Agency
RP Wegener, P (corresponding author), Tech Univ Braunschweig, Inst Flight Mech &
Spaceflight Technol, Hans Sommer Str 5, D-38106 Braunschweig, Germany.
CR AKIBA R, 1990, 901367 AIAA
JACKSON A, 1997, ESA
MEYER RX, 1992, J PROPULSION POWER, V8
Mueller A.C., 1985, ADV SPACE RES, V5, P77, DOI [DOI 10.1016/0273-1177(85)90389-
8, 10.1016/0273-1177(85)90389-8.]
OJAKANGAS GW, 1996, J SPACECRAFT ROCKETS, V33
SHEEKS BJ, 1997, 1997 SPAC CONTR C 27
NR 6
TC 15
Z9 17
U1 0
U2 3
PU PERGAMON PRESS LTD
PI OXFORD
PA THE BOULEVARD LANGFORD LANE KIDLINGTON, OXFORD OX5 1GB, ENGLAND
SN 0273-1177
J9 ADV SPACE RES
PY 1999
VL 23
IS 1
BP 161
EP 164
DI 10.1016/S0273-1177(98)00242-7
PG 4
WC Engineering, Aerospace; Astronomy & Astrophysics; Geosciences,
Multidisciplinary; Meteorology & Atmospheric Sciences
SC Engineering; Astronomy & Astrophysics; Geology; Meteorology &
Atmospheric Sciences
GA BM98C
UT WOS:000080334700019
DA 2023-12-05
ER
PT J
AU Odeigah, PG
Ijimakinwa, J
Lawal, B
Oyeniyi, R
AF Odeigah, PG
Ijimakinwa, J
Lawal, B
Oyeniyi, R
TI Genotoxicity screening of leachates from solid industrial wastes
evaluated with the Allium test
SO ATLA-ALTERNATIVES TO LABORATORY ANIMALS
LA English
CT 14th Annual Congress of the Scandinavian-Society-for-Cell-Toxicology on
In Vitro Toxicology
CY SEP 05-08, 1996
CL UPPSALA, SWEDEN
DE Allium test; genotoxicity; industrial waste; environmental monitoring
ID SEDIMENT; WATER; ACTIVATION; CHEMICALS; PLANTS
AB Six solid wastes from the metal industry, from the chemical industry and from
the production of pesticides were investigated for their toxic and genotoxic
properties by using the Allium test. To simulate environmental conditions and
better assess their environmental impact, the solid wastes were leached with water,
and the water-extractable micropollutants were lyophilised before screening. The
mean root lengths of onions exposed to different concentrations of the leachates
were measured, and EC50 values were determined from the growth curves. The EC50
values of the wastes were ranked, in the order: organochlorine pesticide waste,
settling tank sludge from a chemical company, paint sludge, lead slag, steel slag
and aluminium slag. The leachates were also mitodepressive, and caused significant
increases in the frequency of chromosome aberrations. These results demonstrate
that the Allium test is a useful screening test for the evaluation and ranking of
toxic industrial waste.
C1 UNIV LAGOS,DEPT SCI BIOL,GENET LAB,LAGOS,NIGERIA.
C3 University of Lagos
CR BESSI H, 1992, ENVIRON TOXIC WATER, V7, P71, DOI 10.1002/tox.2530070107
DONNELLY KC, 1985, HAZARD WASTE HAZARD, V2, P191, DOI 10.1089/hwm.1985.2.191
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8618(1988)7[529:CCAMPO]2.0.CO;2
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8
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HOPKE PK, 1982, ENVIRON SCI TECHNOL, V16, P140, DOI 10.1021/es00097a005
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PANDA KK, 1989, SCI TOTAL ENVIRON, V79, P25, DOI 10.1016/0048-9697(89)90050-8
PLEWA MJ, 1982, CHEM MUTAGENS, V7, P401
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SANDHU SS, 1991, MUTAT RES, V257, P19, DOI 10.1016/0165-1110(91)90017-P
WEST WR, 1988, ENVIRON SCI TECHNOL, V22, P224, DOI 10.1021/es00167a016
NR 18
TC 15
Z9 18
U1 0
U2 2
PU FRAME
PI NOTTINGHAM
PA RUSSELL & BURCH HOUSE 96-98 NORTH SHERWOOD ST, NOTTINGHAM, NOTTS,
ENGLAND NG1 4EE
SN 0261-1929
J9 ATLA-ALTERN LAB ANIM
JI ATLA-Altern. Lab. Anim.
PD MAY-JUN
PY 1997
VL 25
IS 3
BP 311
EP 321
PG 11
WC Medicine, Research & Experimental
SC Research & Experimental Medicine
GA XC771
UT WOS:A1997XC77100018
DA 2023-12-05
ER
PT J
AU DROUET, MG
HANDFIELD, M
MEUNIER, J
LAFLAMME, CB
AF DROUET, MG
HANDFIELD, M
MEUNIER, J
LAFLAMME, CB
TI DROSS TREATMENT IN A ROTARY ARC FURNACE WITH GRAPHITE-ELECTRODES
SO JOM-JOURNAL OF THE MINERALS METALS & MATERIALS SOCIETY
LA English
DT Article
AB Aluminum baths are always covered with a layer of dross resulting from the
aluminum surface oxidation. This dross represents 1-10% of the melt and may contain
up to 75 wt.% aluminum. Since aluminum production is highly energy intensive,
dross recycling is very attractive from both energy and economic standpoints. The
conventional recycling process using salt rotary furnaces is thermally inefficient
and environmentally unacceptable because of the production of salt slags. Hydro-
Quebec has developed a new technology using a rotary arc furnace with graphite
electrodes. This process provides aluminum recovery rates of 80-90%, using a highly
energy efficient, environmentally sound production method.
RP DROUET, MG (corresponding author), HYDRO QUEBEC,LTEE,DEPT IND PLASMA,600 RUE
MONTAGUE,POB 990,SHAWINIGAN G9N 7N5,PQ,CANADA.
CR DROUET MG, 1993, Patent No. 5245627
Lavoie S, 1991, LIGHT MET, P981
NR 2
TC 15
Z9 16
U1 0
U2 1
PI WARRENDALE
PA 420 COMMONWEALTH DR, WARRENDALE, PA 15086
SN 1047-4838
J9 JOM-J MIN MET MAT S
JI JOM-J. Miner. Met. Mater. Soc.
PD MAY
PY 1994
VL 46
IS 5
BP 26
EP 27
DI 10.1007/BF03220691
PG 2
GA NJ968
UT WOS:A1994NJ96800005
DA 2023-12-05
ER
PT J
AU LEE, CM
CHOI, IS
BAK, BG
LEE, JM
AF LEE, CM
CHOI, IS
BAK, BG
LEE, JM
TI PRODUCTION OF HIGH-PURITY ALUMINUM KILLED STEEL
SO REVUE DE METALLURGIE-CAHIERS D INFORMATIONS TECHNIQUES
LA English
CT 1992 STEELMAKING CONF
CY DEC 16-17, 1992
CL PARIS, FRANCE
AB The manufacturing technique of D and I steel has been improved at Pohang Works,
Posco. The improvement of slag control, the utilization of RH-OB flux refining
facility and the application of tundish filtering dam allowed the improvement of
steel cleanness for D and I steel. Consequently, the flange crack ratio of D and I
steel was significantly reduced.
RP LEE, CM (corresponding author), POSCO,POHANG WORKS,POHANG,SOUTH KOREA.
CR OKOHIRA K, 1974, TETSU TO HAGANE, V60, P26
TSUBOTA K, 1990, 6TH P INT IR STEEL C, V3, P637
NR 2
TC 15
Z9 16
U1 0
U2 1
PU REVUE DE METALLURGIE
PI NANTERRE CEDEX
PA LES FONTENELLES, 1 RUE DE CRAIOVA, 92024 NANTERRE CEDEX, FRANCE
SN 0035-1563
J9 REV METALL-PARIS
JI Rev. Metall.-Cah. Inf. Techn.
PD APR
PY 1993
VL 90
IS 4
BP 501
EP 506
PG 6
GA LM415
UT WOS:A1993LM41500006
DA 2023-12-05
ER
PT J
AU HESS, E
CHEN, K
ACOSTA, P
BRENT, D
FENDELL, F
AF HESS, E
CHEN, K
ACOSTA, P
BRENT, D
FENDELL, F
TI EFFECT OF ALUMINIZED-GRAIN DESIGN ON SLAG ACCUMULATION
SO JOURNAL OF SPACECRAFT AND ROCKETS
LA English
DT Article
ID SOLID ROCKET MOTORS; FLOWS
AB A parametric investigation was carried out, by analytic and numeric solution of
a simple Eulerian-potential-flow/Lagrangian-particle-tracking formulation, of the
effect of metallized-grain configuration on the retention of slag within the cavity
of a first-stage-type solid-rocket-propellant motor. In particular, a relatively
short motor with the grain deeply slotted near the aft end, a relatively long motor
also with the grain deeply slotted near the aft end, and a long "conocyl" motor
with axially distributed slots (such that much of the aft end was grain filled
during the entire burn) were compared. The same initial grain bore and the same
casing diameter pertained to all three motors, and in each case the nozzle was
taken to be deeply recessed ("submerged"). It was found that, over a wide range of
plausible particle sizes, the accumulation of slag (here, molten aluminum oxide) at
the aft end is appreciably less for the short motor and for the conocyl motor than
for the long motor. Further, it was found that the effect of a plausible flight-
acceleration history on slag retention, relative to a standard-gravity calculation,
would be discernible only for larger particle sizes, above roughly 200-mum
diameter.
RP HESS, E (corresponding author), TRW CO INC,CTR PROPULS TECHNOL & FLUID
MECH,SPACE & TECHNOL GRP,REDONDO BEACH,CA 90278, USA.
CR BARTLEY CE, 1959, JET PROPULSION ENGIN, V12, P521
BATCHELOR GK, 1967, INTRO FLUID MECHANIC, P536
BORAAS S, 1984, J SPACECRAFT ROCKETS, V21, P47, DOI 10.2514/3.8606
BRENT D, 1991, COMMUNICATION
CARRIER G, 1991, J PROPUL POWER, V7, P185, DOI 10.2514/3.23311
CHANG IS, 1980, AIAA J, V18, P1455, DOI 10.2514/3.50905
CULICK FEC, 1966, AIAA J, V4, P1462, DOI 10.2514/3.3709
HALOULAKOS VE, 1991, J PROPUL POWER, V7, P14, DOI 10.2514/3.23288
KLIEGEL JR, 1963, 9 S INT COMB, P811
MA YC, 1991, J PROPUL POWER, V7, P700, DOI 10.2514/3.23382
Price EW, 1984, FUNDAMENTALS SOLID P, P479, DOI
10.2514/5.9781600865671.0479.0513
Rudinger G., 1980, FUNDAMENTALS GAS PAR, P1
WAESCHE RHW, 1989, J PROPUL POWER, V5, P650, DOI 10.2514/3.23202
NR 13
TC 15
Z9 17
U1 1
U2 3
PU AMER INST AERONAUT ASTRONAUT
PI RESTON
PA 1801 ALEXANDER BELL DRIVE, STE 500, RESTON, VA 22091
SN 0022-4650
J9 J SPACECRAFT ROCKETS
JI J. Spacecr. Rockets
PD SEP-OCT
PY 1992
VL 29
IS 5
BP 697
EP 703
DI 10.2514/3.55646
PG 7
SC Engineering
GA JR777
UT WOS:A1992JR77700013
DA 2023-12-05
ER
PT J
AU Jiang, DD
Shi, CJ
Zhang, ZH
AF Jiang, Dongdong
Shi, Caijun
Zhang, Zuhua
TI Recent progress in understanding setting and hardening of
alkali-activated slag (AAS) materials
LA English
DT Article
DE Slag; AAS; Alkali -activated slag materials; Hydration product;
Microstructure; Thermodynamic modelling
ID BLAST-FURNACE SLAG; CALCIUM SILICATE HYDRATE; AGE REACTION-KINETICS; S-H
GEL; SODIUM-SILICATE; DRYING SHRINKAGE; FLY-ASH; MICROMECHANICAL
PROPERTIES; PHASE EVOLUTION; PORE STRUCTURE
AB Alkali-activated slag (AAS with type of slag being blast-furnace slag) binders
possesses substantially different hydration mechanisms from Portland cement (PC)
binders, leading to distinct setting and hardening behavior. Due to the highly
amorphous nature of both of raw materials and hydration products, the
characterization of hydrate assemblages and microstructural development of AAS
materials is challenging. In the past decades, there has been increasing
investigation interests in disclosing the nature of aluminum and sodium containing
calcium silicate hydrate gel with undefined stoichiometry (C-(N-)A-S-H) along with
the existence of intimately intermixed secondary phases. This paper provides an
overview on the recent research progress and understanding of the complex alkali-
activation reaction process from the perspectives of hydration kinetics, products
and micro-structure development. This is critical to the interpretation and control
of setting and hardening of AAS materials at the early age. In addition, based on
available information, hydration mechanisms of different AAS binders are proposed.
For such a complex system, thermodynamic modelling and molecular dynamic modelling
have shown their power to correlate the microstructure development and the
macroscale behavior of AAS materials, which are discussed in this paper.
C1 [Jiang, Dongdong; Shi, Caijun; Zhang, Zuhua] Hunan Univ, Coll Civil Engn, Key
Lab Green & Adv Civil Engn Mat & Applicat Tech, Changsha 410082, Peoples R China.
[Jiang, Dongdong; Shi, Caijun; Zhang, Zuhua] Hunan Univ, Int Innovat Ctr Green &
Adv Civil Engn Mat Hunan P, Changsha 410082, Peoples R China.
[Jiang, Dongdong; Shi, Caijun; Zhang, Zuhua] Hunan Univ, Key Lab Bldg Safety &
Energy Efficiency, Minist Educ, Changsha 410082, Peoples R China.
C3 Hunan University; Hunan University; Hunan University
RP Shi, CJ; Zhang, ZH (corresponding author), Hunan Univ, Coll Civil Engn, Key Lab
Green & Adv Civil Engn Mat & Applicat Tech, Changsha 410082, Peoples R China.
EM cshi@hnu.edu.cn; zuhuazhang@hnu.edu.cn
RI Zhang, Zuhua/AAK-5391-2020
OI Zhang, Zuhua/0000-0002-7153-5120
FU National Science Foundation of China; [U2001225]; [51878263]
FX Acknowledgement The authors are grateful of the financial support by the
National Science Foundation of China projects U2001225 and 51878263.
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NR 163
TC 14
Z9 14
U1 21
U2 53
PU ELSEVIER SCI LTD
PI OXFORD
SN 0958-9465
EI 1873-393X
PD NOV
PY 2022
VL 134
AR 104795
DI 10.1016/j.cemconcomp.2022.104795
EA OCT 2022
PG 19
GA 5R7GS
UT WOS:000874675100001
DA 2023-12-05
ER
PT J
AU Ooi, WE
Liew, YM
Heah, CY
Abdullah, MMA
Li, LY
Ho, L
Loong, FK
Shee-Ween, O
Ng, HT
Ng, YS
Jaya, NA
AF Ooi Wan-En
Liew Yun-Ming
Heah Cheng-Yong
Li, Long-Yuan
Ho, Li Ngee
Loong, Foo Kai
Shee-Ween, Ong
Ng Hui-Teng
Ng Yong-Sing
Jaya, Nur Ain
TI Comparative mechanical and microstructural properties of high calcium
fly ash one-part geopolymers activated with
Na2SiO3-anhydrous and NaAlO2
LA English
DT Article
DE One-part geopolymer; High calcium fly ash; Sodium aluminate; Anhydrous
sodium metasilicate
ID SILICA; PHASE; BINDERS; SLAG
AB This paper investigates the effect of varying solid alkali activators on the
fresh and hardened properties and microstructural changes of one-part geopolymers
(OPGs). Single and binary solid alkali activators were used to activate high
calcium fly ash. The alkali activators were either solely sodium metasilicate
(Na2SiO3) or a combination of sodium aluminate (NaAlO2) and sodium metasilicate
(Na2SiO3)(.) The OPG activated with anhydrous Na2SiO3 achieved an excellent 28-day
compressive strength of 83.6 MPa while OPG activated with NaAlO2 and Na2SiO3
attained a compressive strength of 45.1 MPa. The Na(2)SiO(3)activated OPG
demonstrated better fluidity than the OPG activated with NaAlO2 and Na2SiO3 due to
the thixotropic behaviour caused by the NaAlO2. The Na2SiO3-activated OPG consisted
of sodium-calcium aluminium silicate hydrate ((N,C)-A-S-H) gel phase, while the OPG
activated with NaAlO2 and Na2SiO3 comprised of the coexistence of sodium aluminium
silicate hydrate (N-A-S-H) and calcium aluminium silicate hydrate (C-A-S-H) gel
phases. Regardless of the distinctive properties, the OPGs are adequate for
building materials applications. (C) 2021 The Author(s). Published by Elsevier B.V.
C1 [Ooi Wan-En; Liew Yun-Ming; Heah Cheng-Yong; Abdullah, Mohd Mustafa Al Bakri;
Shee-Ween, Ong; Ng Hui-Teng; Ng Yong-Sing; Jaya, Nur Ain] Univ Malaysia Perlis, Ctr
Excellence CEGeoGTech, Geopolymer & Green Technol, Perlis 01000, Malaysia.
[Ooi Wan-En; Liew Yun-Ming; Abdullah, Mohd Mustafa Al Bakri; Ho, Li Ngee; Shee-
Ween, Ong; Ng Hui-Teng; Ng Yong-Sing; Jaya, Nur Ain] Univ Malaysia Perlis, Fac Chem
Engn Technol, Perlis 01000, Malaysia.
[Heah Cheng-Yong] Univ Malaysia Perlis, Fac Mech Engn Technol, Perlis 01000,
Malaysia.
[Li, Long-Yuan] Plymouth Univ, Sch Engn Comp & Math, Drake Circus Plymouth,
Plymouth PL4 8AA, Devon, England.
[Loong, Foo Kai] Univ Malaysia Perlis, Inst Nano Elect Engn INEE, Perlis 01000,
Malaysia.
C3 Universiti Malaysia Perlis; Universiti Malaysia Perlis; Universiti
Malaysia Perlis; University of Plymouth; Universiti Malaysia Perlis
RP Liew, YM (corresponding author), Univ Malaysia Perlis, Ctr Excellence
CEGeoGTech, Geopolymer & Green Technol, Perlis 01000, Malaysia.; Liew, YM
(corresponding author), Univ Malaysia Perlis, Fac Chem Engn Technol, Perlis 01000,
Malaysia.
EM ymliew@unimap.edu.my
RI Foo, Kai Loong/D-2035-2015; Ng, Hui-Teng/GYU-1877-2022; li,
long/HOF-6990-2023; Liew, Yun Ming/S-7164-2019; Abdullah, Mohd Mustafa
Al Bakri/C-9844-2012; Li, Ly/JCD-4746-2023; HEAH, CHENG
YONG/S-7139-2019; Ong, Shee ween/ABA-9926-2021; Li, Li/IAQ-0885-2023;
Ho, Li Ngee/AGP-2572-2022
OI Foo, Kai Loong/0000-0001-6009-860X; Ng, Hui-Teng/0000-0003-0185-5046;
Liew, Yun Ming/0000-0001-6600-4969; Abdullah, Mohd Mustafa Al
Bakri/0000-0002-9779-8586; HEAH, CHENG YONG/0000-0001-7093-7833; Ong,
Shee ween/0000-0003-0256-6916; Li, Long-yuan/0000-0002-5982-0965; Ng,
Yong Sing/0000-0002-9302-3978; Ho, Li Ngee/0000-0001-9935-8595
FU Ministry of Higher Education Malaysia [FRGS/1/2020/TK01/UNIMAP/02/2]
FX This work was supported by Fundamental Research Grant Scheme
(FRGS/1/2020/TK01/UNIMAP/02/2) from the Ministry of Higher Education
Malaysia.
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NR 46
TC 14
Z9 14
U1 7
U2 24
PU ELSEVIER
PI AMSTERDAM
SN 2238-7854
EI 2214-0697
PD NOV-DEC
PY 2021
VL 15
BP 3850
EP 3866
DI 10.1016/j.jmrt.2021.10.018
EA OCT 2021
PG 17
Engineering
GA WN9II
UT WOS:000712078600002
DA 2023-12-05
ER
PT J
AU Coetsee, T
De Bruin, F
AF Coetsee, Theresa
De Bruin, Frederik
TI Application of Copper as Stabiliser in Aluminium Assisted Transfer of
Titanium in Submerged Arc Welding of Carbon Steel
SO PROCESSES
LA English
DT Article
DE oxygen potential; titanium; aluminium; copper; metal powder; submerged
arc welding
ID SLAG-METAL REACTIONS; CHEMISTRY; MN; TI
AB The element transfer of Ti from molten flux to the weld metal is limited to less
than 310 ppm Ti in the submerged arc welding of carbon steel. This limitation is
due to the high oxygen partial pressure prevailing at the molten flux-weld pool
interface. Our previous study illustrated that the use of Al powder in combination
with Ti powder improves the transfer of Ti to the weld metal to 4% Ti, whilst
maintaining 509 ppm O in the weld metal. The weld metal ppm O should be controlled
at 200 to 500 ppm O to maintain weld metal toughness. In this study, the addition
of Cu powder with Ti and Al powder is applied to illustrate the stabiliser effect
of Cu in the weld pool. The role of Cu as weld pool stabiliser is due to its
decrease of the temperature required to melt Ti into the weld pool, so increasing
the quantity of metal powder melted into the weld pool. The weld metal composition
improved to 5.1% Ti, 3.6% Cu, and 371 ppm O. Thus, the role of Al in controlling
the partial oxygen pressure at the molten flux-weld pool interface is maintained in
the presence of Cu powder.
C1 [Coetsee, Theresa; De Bruin, Frederik] Univ Pretoria, Dept Mat Sci & Met Engn,
ZA-0002 Pretoria, South Africa.
RP Coetsee, T (corresponding author), Univ Pretoria, Dept Mat Sci & Met Engn, ZA-
0002 Pretoria, South Africa.
EM theresa.coetsee@up.ac.za; jdb.1953@gmail.com
RI De Bruin, Frederik Johannes/IZE-6573-2023
OI De Bruin, Frederik Johannes/0000-0001-7102-7508; Coetsee,
Theresa/0000-0003-2028-5755
FU National Research Foundation of South Africa [BRIC171211293679]
FX FundingThis research was funded in part by the National Research
Foundation of South Africa, grant number BRIC171211293679.
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PD OCT
PY 2021
VL 9
IS 10
AR 1763
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PG 11
SC Engineering
GA WN5QB
UT WOS:000711820900001
DA 2023-12-05
ER
PT J
AU Samanta, NS
Banerjee, S
Mondal, P
Anweshan
Bora, U
Purkait, MK
AF Samanta, Niladri Shekhar
Banerjee, Sirsak
Mondal, Piyal
Anweshan
Bora, Utpal
Purkait, Mihir K.
TI Preparation and characterization of zeolite from waste Linz-Donawitz
(LD) process slag of steel industry for removal of Fe3+ from
drinking water
SO ADVANCED POWDER TECHNOLOGY
LA English
DT Article
DE Zeolite; Fe3+ adsorption; LD slag; Langmuir isotherm; Multistage
diffusion
ID BASIC OXYGEN FURNACE; IRON REMOVAL; GROUNDWATER; ADSORPTION; MANGANESE;
FLUORIDE; EQUILIBRIUM; EXTRACTION; AMMONIUM; CATALYST
AB Cubical-shaped zeolite A was synthesized from the Linz-Donawitz (LD) process
slag of the Steel Industry, utilizing conventional fusion-assisted hydrothermal
treatment. Morphological and Physico-chemical characterizations were performed by
various characterization techniques. A weight ratio of 1:1.2 (LD-slag: NaOH) was
maintained during fusion, which provides a better binding effect with better
mechanical stability to the zeolite framework. Fe3+ adsorption studies were
performed at 273, 298, 303, and 308 K, respectively, within the range of 10-40 mg L
(1) Fe3+ ion concentration for kinetic and isotherm studies. A maximum adsorption
capacity of 27.55 mg g (1) was obtained at a 1.4 g L (1) adsorbent dosage, with
99.99% Fe3+ ion removal. Moreover, the Fe3+ adsorption study obeyed the pseudo-
second-order kinetic model, whereas multistage diffusion controlled the adsorption
process. Langmuir isotherm model best fitted the equilibrium data suggesting the
highly negative charge over the adsorbent surface played a vital role in the
electrostatic attraction of Fe3+ ions. Isomorphic replacement of silicon by
aluminum ion imparted a highly negative charge over the zeolite surface in the
primary structure unit. For real-life sample drinking water, the Fe3+ ion removal
efficiency increases to 97.7%. (C) 2021 The Society of Powder Technology Japan.
Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights
reserved.
C1 [Samanta, Niladri Shekhar; Bora, Utpal; Purkait, Mihir K.] Indian Inst Technol
Guwahati, Ctr Environm, Gauhati 781039, Assam, India.
[Banerjee, Sirsak; Mondal, Piyal; Anweshan; Purkait, Mihir K.] Indian Inst
Technol Guwahati, Dept Chem Engn, Gauhati 781039, Assam, India.
Technology (IIT) - Guwahati; Indian Institute of Technology System (IIT
System); Indian Institute of Technology (IIT) - Guwahati
RP Purkait, MK (corresponding author), Indian Inst Technol Guwahati, Dept Chem
Engn, Gauhati 781039, Assam, India.
EM mihir@iitg.ac.in
RI Bora, Utpal/E-3574-2010
OI Bora, Utpal/0000-0002-7403-0152; , Anweshan/0000-0002-4101-1721
FU DST (Department of Science and Technology) in New Delhi
[DST/TM/WTI/WIC/2K17/84 (G)]
FX This work is supported by a grant (DST/TM/WTI/WIC/2K17/84 (G)) from the
DST (Department of Science and Technology) in New Delhi. Any opinions,
findings, and conclusions expressed in this paper are those of the
authors and do not necessarily reflect the views of DST, New Delhi.
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PU ELSEVIER
PI AMSTERDAM
SN 0921-8831
EI 1568-5527
J9 ADV POWDER TECHNOL
JI Adv. Powder Technol.
PD SEP
PY 2021
VL 32
IS 9
BP 3372
EP 3387
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PG 16
SC Engineering
GA UJ1SW
UT WOS:000691075100005
DA 2023-12-05
ER
PT J
AU Perumal, P
Kiventerä, J
Illikainen, M
AF Perumal, Priyadharshini
Kiventera, Jenni
Illikainen, Mirja
TI Influence of alkali source on properties of alkali activated silicate
tailings
LA English
DT Article
DE Alkali activation; Silicate tailings; Sodium sulphate; Sodium carbonate;
Strength
ID C-S-H; SODIUM-CARBONATE; MINE TAILINGS; FLY-ASH; SLAG; HYDRATION;
EVOLUTION; MAGNESIUM; PERFORMANCE; CHEMISTRY
AB Mining activities are inevitable for the growing industrialization and
urbanization in the world. Disposal of mine tailings creates a severe impact to the
environment and ultimately to the society. Identifying the applications of mine
tailings as potential secondary raw materials would help the mining industries in
achieving circular economy. Alkali activation of tailings for their utilization as
building materials or backfill in mining sites is one such popular technique. In
this paper, mechanically treated silicate tailings rich in magnesium/aluminum
content were chosen, to be used as aluminosilicate precursors. The effect of
different alkaline sources was accessed by using sodium silicate (Na2SiO3), sodium
sulphate (Na2SO4) and sodium carbonate (Na2CO3) as activators. Alkali activated
tailings pastes were studied by examining the compressive strength and
microstructural properties. High magnesium tailings show good strength results with
sodium silicate activator whereas sulphate-based activator performed well in high
alumina tailings. Sodium carbonate seems to be efficient in early phases but does
not display improvement in later ages. This behavior of alkali activated tailings
with different alkali sources were tried to be correlated with the mineralogy of
the tailings and its reactivity using FTIR, XRD and TGA.
C1 [Perumal, Priyadharshini; Kiventera, Jenni; Illikainen, Mirja] Univ Oulu, Fac
Technol, Fibre & Particle Engn Res Unit, POB 4300, Oulu, Finland.
RP Perumal, P (corresponding author), Univ Oulu, Fac Technol, Fibre & Particle Engn
Res Unit, POB 4300, Oulu, Finland.
EM mail2pridha@gmail.com
RI ; Perumal, Priyadharshini/P-7995-2018
OI Illikainen, Mirja/0000-0001-7545-4574; Perumal,
Priyadharshini/0000-0002-7731-2016
FU project GEOMINS [Steps towards the use of mine tailings in geopolymer
materials: reactivity, CO2 sequestration and heavy metal stabilization]
- Academy of Finland [319676]; European Union's Horizon 2020 research
and inno-vation programme under the Marie Skodowska Curie grant
[839848]; Marie Curie Actions (MSCA) [839848] Funding Source: Marie
Curie Actions (MSCA); Academy of Finland (AKA) [319676, 319676] Funding
Source: Academy of Finland (AKA)
the project GEOMINS [grant #319676: Steps towards the use of mine
tailings in geopolymer materials: reactivity, CO2 sequestration and
heavy metal stabilization] funded by Academy of Finland. The authors
appreciate the contribution from companies, Boliden and Sibelco for
arranging the tailings for this work. PP acknowledges the funding
received from the European Union's Horizon 2020 research and inno-vation
programme under the Marie Skodowska Curie grant agreement No [839848] .
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NR 54
TC 14
Z9 15
U1 2
U2 29
PI LAUSANNE
SN 0254-0584
EI 1879-3312
J9 MATER CHEM PHYS
PD OCT 1
PY 2021
VL 271
AR 124932
DI 10.1016/j.matchemphys.2021.124932
EA JUL 2021
PG 10
GA UA3JX
UT WOS:000685059400004
DA 2023-12-05
ER
PT J
AU Sreenivasan, H
Adesanya, E
Niu, H
Perumal, P
Kantola, AM
Telkki, VV
Huttula, M
Cao, W
Provis, JL
Illikainen, M
Kinnunen, P
AF Sreenivasan, Harisankar
Adesanya, Elijah
Niu, He
Perumal, Priyadharshini
Kantola, Anu M.
Telkki, Ville-Veikko
Huttula, Marko
Cao, Wei
Provis, John L.
Illikainen, Mirja
Kinnunen, Paivo
TI Evidence of formation of an amorphous magnesium silicate (AMS) phase
during alkali activation of (Na-Mg) aluminosilicate glasses
LA English
DT Article
DE Fate of magnesium; Amorphous magnesium silicate phase; Geopolymers;
Alkali activated materials; Hydrotalcite
ID FLY-ASH; THERMAL-DECOMPOSITION; STRUCTURAL EVOLUTION; NICKEL SLAG;
AL-27; MAS; HYDRATION; CEMENTS; O-17
AB There is some ambiguity regarding the fate of Mg during the alkali activation of
Mg-rich precursors within the broader field of alkali activated materials (AAMs).
The present work addresses this issue by studying the reaction products in AAMs
synthesized from (Na-Mg) aluminosilicate glasses. Here, instead of magnesium
silicate hydrate (M-S-H) phase, Mg exclusively forms an amorphous magnesium
silicate (AMS) phase. Compared to M-S-H, AMS is a more depolymerized phase, which
has not previously been well documented. The formation of AMS seems to be driven by
the high charge density of the Mg cation which effectively stabilizes the
depolymerized silicate species. We also show that the lack of hydrotalcite-group
phases is due to aluminum depletion by zeolite formation. This work highlights the
need to consider the existence of the AMS phase in Mg-containing AAMs, especially
in complex systems, where its identification may be difficult.
C1 [Sreenivasan, Harisankar; Adesanya, Elijah; Niu, He; Perumal, Priyadharshini;
Illikainen, Mirja; Kinnunen, Paivo] Univ Oulu, Fibre & Particle Engn Res Unit, POB
4300, FI-90014 Oulu, Finland.
[Huttula, Marko; Cao, Wei] Univ Oulu, Nano & Mol Syst Res Unit, POB 3000, FI-
90014 Oulu, Finland.
[Kantola, Anu M.; Telkki, Ville-Veikko] Univ Oulu, Fac Sci, NMR Res Unit, POB
3000, FI-90014 Oulu, Finland.
[Provis, John L.] Univ Sheffield, Dept Mat Sci & Engn, Sir Robert Hadfield Bldg,
C3 University of Oulu; University of Oulu; University of Oulu; University
of Sheffield
RP Kinnunen, P (corresponding author), Univ Oulu, Fibre & Particle Engn Res Unit,
POB 4300, FI-90014 Oulu, Finland.
EM paivo.kinnunen@oulu.fi
RI Cao, Wei/J-9354-2015; Niu, He/GNH-3651-2022; Kantola, Anu/AAQ-4577-2021;
Provis, John/AAR-3260-2020; Niu, He/ABS-0624-2022; Perumal,
Priyadharshini/P-7995-2018
OI Cao, Wei/0000-0003-3139-1780; Niu, He/0000-0001-9424-1937; Kantola,
Anu/0000-0003-1945-9201; Provis, John/0000-0003-3372-8922; Niu,
He/0000-0001-9424-1937; Perumal, Priyadharshini/0000-0002-7731-2016;
FU European Union's Horizon 2020 research and innovation programme under
the Marie Sklodowska-Curie COFUND Grant [713606]; Kvantum institute
(University of Oulu); Academy of Finland [322085, 329477, 326291,
289649, 319216]; Centre for Material Analysis, University of Oulu,
Finland; Academy of Finland (AKA) [319216, 329477, 319216, 322085,
329477] Funding Source: Academy of Finland (AKA)
the European Union's Horizon 2020 research and innovation programme
under the Marie Sklodowska-Curie COFUND Grant Agreement no. 713606
(I4FUTURE). P.K. acknowledges financial support from Kvantum institute
(University of Oulu) and Academy of Finland (grants 322085, 329477 and
326291). A.M.K and V.-V.T. acknowledge the financial support from
Kvantum institute (University of Oulu) and Academy of Finland (grants
#289649 and 319216). The authors would also like to thank Marcin Selent
for his help with XRD measurement, Pasi Juntunen with SEM measurement
and Tommi Kokkonen with glass synthesis and TG-MS measurements. This
work/part of the work was carried out with the support of the Centre for
Material Analysis, University of Oulu, Finland.
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NR 39
TC 14
Z9 14
U1 3
U2 29
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD JUL
PY 2021
VL 145
AR 106464
DI 10.1016/j.cemconres.2021.106464
EA APR 2021
PG 15
GA SF5YO
UT WOS:000652831000015
OA hybrid, Green Accepted, Green Published
DA 2023-12-05
ER
PT J
AU Ibrahim, MM
El-Sheshtawy, HS
Abd El-Magied, MO
Dhmees, AS
AF Ibrahim, Mohamed M.
El-Sheshtawy, Hamdy S.
Abd El-Magied, Mahmoud O.
Dhmees, Abdelghaffar S.
TI Mesoporous Al2O3 derived from blast furnace slag
as a cost-effective adsorbent for U(VI) removal from aqueous solutions
SO INTERNATIONAL JOURNAL OF ENVIRONMENTAL ANALYTICAL CHEMISTRY
LA English
DT Article
DE Al2O3; blast furnace slag; removal; uranium
ID SOLID-PHASE EXTRACTION; URANIUM EXTRACTION; SILICA; ADSORPTION; AMINE
AB This work provides an environmental approach to utilise Blast furnace slag (BFS)
waste for the processing of aluminium oxide (Al2O3-BFS) as an efficient adsorbent
for uranium removal from wastewater. The composition of BFS is less variable and
this makes it a low cost and abundant raw material for preparing a solid base
Al2O3-BFS. The silica material was initially removed and then the aluminium content
was separated by precipitation with sodium hydroxide depending on pH control (pH
5.5). The raw BFS and Al2O3-BFS were characterised via various methods, such as;
XRD, Zeta potential, N-2 adsorption-desorption isotherm, DLS, and FT-IR. BFS
exhibited the typical type III isotherm with an H3-type hysteresis loop. The curve
of Al2O3-BFS exhibited the typical IV isotherms with a H2-type hysteresis loop. The
BET surface and average pore sizes of the Al2O3-BFS are 137.7 m2 g-1 and 3.9 nm,
respectively. Experiments and discussions were performed in terms of balance,
isothermal, kinetic, and applicability. The finding provides proof of the ability
of synthesised Al2O3-BFS to remove U(VI) ions from wastewater as an efficient
adsorbent with a maximum sorption capacity value of 62 mg/g. The pseudo second,
Langmuir and Dubinin-Radushkevich models were found suitable to explain the rate
kinetics and isotherm of uranium removal. Uranium sorption on Al2O3-BFS may occur
via inner-sphere complex and ion-exchange between uranium ions and HO-Al2O3-BFS
groups. The higher elution efficiency of Al2O3-BFS indicates a promising adsorbent
in the technology of U(VI) removal.
C1 [Ibrahim, Mohamed M.] Taif Univ, Coll Sci, Dept Chem, At Taif, Saudi Arabia.
[El-Sheshtawy, Hamdy S.] Kafrelsheikh Univ, Chem Dept, Kafrelsheikh, Egypt.
[Abd El-Magied, Mahmoud O.] Nucl Mat Author, Dept Isotopes Geol, Cairo, Egypt.
[Dhmees, Abdelghaffar S.] Egyptian Petr Res Inst, Dept Anal & Evaluat, Cairo,
Egypt.
C3 Taif University; Egyptian Knowledge Bank (EKB); Kafrelsheikh University;
Egyptian Knowledge Bank (EKB); Nuclear Materials Authority (NMA);
Egyptian Knowledge Bank (EKB); Egyptian Petroleum Research Institute
(EPRI)
RP Dhmees, AS (corresponding author), Egyptian Petr Res Inst, Dept Anal & Evaluat,
Cairo, Egypt.
EM abdel_ghffar@yahoo.com
RI Dhmees, Abdelghaffar/A-4435-2019; Abd El-Magied, Mahmoud O/B-8758-2018
OI Dhmees, Abdelghaffar/0000-0003-0320-6648; Abd El-Magied, Mahmoud
O/0000-0002-7744-1483; Ibrahim, Mohamed/0000-0002-4351-009X
FU Taif University, Taif, Saudi Arabia [TURSP-2020/05]
FX The authors acknowledge Taif University Researchers Supporting Project
number (TURSP-2020/05), Taif University, Taif, Saudi Arabia.
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NR 43
TC 14
Z9 14
U1 6
U2 53
PI ABINGDON
SN 0306-7319
EI 1029-0397
J9 INT J ENVIRON AN CH
JI Int. J. Environ. Anal. Chem.
PD OCT 21
PY 2023
VL 103
IS 13
BP 2948
EP 2964
DI 10.1080/03067319.2021.1900150
EA APR 2021
PG 17
WC Chemistry, Analytical; Environmental Sciences
SC Chemistry; Environmental Sciences & Ecology
GA L5CJ1
UT WOS:000635832800001
DA 2023-12-05
ER
PT J
AU Brial, V
Tran, H
Sorelli, L
Conciatori, D
Ouellet-Plamondon, CM
AF Brial, Victor
Tran, Hang
Sorelli, Luca
Conciatori, David
Ouellet-Plamondon, Claudiane M.
TI Evaluation of the reactivity of treated spent pot lining from primary
aluminum production as cementitious materials
LA English
DT Article
DE Reactivity tests; Low caustic leaching liming process; Treated spent pot
lining; Blended cement; Hazardous waste; Aluminum; Supplementary
cementitious materials; Resource recycling
ID MERCURY INTRUSION POROSIMETRY; PORE STRUCTURE; PORTLAND-CEMENT; SILICA
FUME; CALCINED CLAYS; MINERAL ADMIXTURES; HYDRATION REACTION; QUARTZ
POWDER; FLY-ASH; LIMESTONE
AB Aluminum Spent Pot lining (SPL) is an industrial hazardous waste generated from
aluminum electrolysis cells. The SPL separates in two parts, the first cut is rich
in carbonaceous materials and the second cut is rich in vitrified refractory.
Treating second cut SPL by the Low Caustic Leaching and Liming (LCL&L) process
generates an inert non-hazardous residue, called LCLL Ash. This product is mainly
composed of stable crystalline phases such as corundum, albite, nepheline with some
amount graphite. Ground as a fine powder, LCLL Ash could be used in cement as a
supplementary cementitious material (SCM). This paper focuses on the investigation
of LCLL Ash reactivity and its improvement by calcination at 1050 degrees C.
Reactivity was evaluated with multiple tests, such as compressive strength activity
index, Frattini test and Rilem R-3 tests followed by XRD analysis. An inert SCMs
(limestone, filler, and quartz) and reactive SCMs (slag, fly ash, silica fume) were
used as references. The results show that LCLL Ash in cement shows inert properties
similar to quartz with a retarder effect below 7 days and a high alkali content.
Moreover, the temperature of the Rilem R-3 tests, shows expansion in the paste due
to LCLL Ash hydro reactivity. This expansion was not observed with LCLL Ash blended
cement mortar. Calcination improved significantly the reactivity of LCLL Ash by
generating higher reactive silica and alumina content. Notably, calcined LCLL Ash
showed reaction properties similar to a calcined clay. Finally, neither delay on
hydration nor expansion was observed with calcined LCLL Ash.
C1 [Brial, Victor; Ouellet-Plamondon, Claudiane M.] Ecole Technol Super, Dept
Construct Engn, 1100 Rue Notre Dame Ouest, Montreal, PQ H3C 1K3, Canada.
[Tran, Hang; Sorelli, Luca; Conciatori, David] Univ Laval, Dept Civil & Water
Engn, Quebec City, PQ, Canada.
C3 University of Quebec; Ecole de Technologie Superieure - Canada; Laval
University
RP Ouellet-Plamondon, CM (corresponding author), Ecole Technol Super, Dept
Construct Engn, 1100 Rue Notre Dame Ouest, Montreal, PQ H3C 1K3, Canada.
EM claudiane.ouellet-plamondon@etsmtl.ca
RI Tran, Hang/GYQ-6408-2022
OI Conciatori, David/0000-0002-1187-4868; Sorelli,
Luca/0000-0003-3046-5450; Ouellet-Plamondon,
Claudiane/0000-0003-3795-4791; Brial, Victor/0000-0002-1899-2912
FU NSERC CRD grant program [CRDPJ 515485 -17]; CRITM consortium; Rio Tinto;
Ciment Quebec Inc.
FX The authors are grateful to NSERC CRD grant program (CRDPJ 515485 -17),
CRITM consortium, Rio Tinto and Ciment Qu ' ebec Inc. for their
financial support for this project.
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NR 85
TC 14
Z9 14
U1 3
U2 20
PU ELSEVIER
PI AMSTERDAM
SN 0921-3449
EI 1879-0658
PD JUL
PY 2021
VL 170
AR 105584
DI 10.1016/j.resconrec.2021.105584
EA APR 2021
PG 14
GA TA5SQ
UT WOS:000667309200027
OA Green Accepted
DA 2023-12-05
ER
PT J
AU Lou, WB
Zhang, Y
Zhang, Y
Zheng, SL
Sun, P
Wang, XJ
Li, JZ
Qiao, S
Zhang, Y
Wenzel, M
Weigand, JJ
AF Lou, Wen-bo
Zhang, Yang
Zhang, Ying
Zheng, Shi-li
Sun, Pei
Wang, Xiao-jian
Li, Jian-zhong
Qiao, Shan
Zhang, Yi
Wenzel, Marco
Weigand, Jan J.
TI Leaching performance of Al-bearing spent LiFePO4 cathode
powder in H2SO4 aqueous solution
LA English
DT Article
DE LiFePO4; aluminum; leaching performance; leaching kinetics
ID LITHIUM-ION BATTERIES; KINETICS; ALUMINUM; METALS; EXTRACTION;
PHOSPHATE; RECOVERY; CATALYST; SLAG
AB The leaching performance and leaching kinetics of LiFePO4 (LFP) and Al in Al-
bearing spent LFP cathode powder were systematically studied. The effects of
temperature (273-368 K), stirring speed (200-950 r/min), reaction time (0-240 min),
acid-to-material ratio (0.1:1-1:1 mL/g) and liquid-to-solid ratio (3:1-9:1 mL/g) on
the leaching process were investigated. The results show that the concentration of
reactants and the temperature have a greater impact on the leaching of Al. Under
the optimal conditions, leaching efficiencies of LFP and Al are 91.53% and 15.98%,
respectively. The kinetic study shows that the leaching of LFP is kinetically
controlled by mixed surface reaction and diffusion, with an activation energy of
22.990 kJ/mol; whereas the leaching of Al is only controlled by surface chemical
reaction, with an activation energy of 46.581 kJ/mol. A low leaching temperature
can effectively suppress the dissolving of Al during the acid leaching of the spent
LFP cathode material.
C1 [Lou, Wen-bo; Li, Jian-zhong] Northeastern Univ, Sch Met, Shenyang 110819,
Peoples R China.
[Lou, Wen-bo; Zhang, Yang; Zhang, Ying; Zheng, Shi-li; Wang, Xiao-jian; Qiao,
Shan; Zhang, Yi] Chinese Acad Sci, Inst Proc Engn, CAS Key Lab Green Proc & Engn,
[Sun, Pei] Univ Utah, Mat Sci & Engn, Salt Lake City, UT 84112 USA.
[Wenzel, Marco; Weigand, Jan J.] Tech Univ Dresden, Fac Chem & Food Chem, D-
01062 Dresden, Germany.
C3 Northeastern University - China; Chinese Academy of Sciences; Institute
of Process Engineering, CAS; Utah System of Higher Education; University
of Utah; Technische Universitat Dresden
RP Zhang, Y; Zheng, SL (corresponding author), Chinese Acad Sci, Inst Proc Engn,
CAS Key Lab Green Proc & Engn, Beijing 100190, Peoples R China.
EM zhangying@ipe.ac.cn; slzheng@ipe.ac.cn
RI Sun, Pei/ABE-6221-2021; wu, p/JDW-5015-2023; Weigand, Prof. Dr.
Jan/O-8792-2018
OI Weigand, Prof. Dr. Jan/0000-0001-7323-7816
FU Key Deployment Projects of Chinese Academy of Sciences [ZDRW_CN_2020-1];
Sino-German Cooperation Research Project under the Natural Science
Foundation of China [51761135108]; German Research Foundation
[392417756]; CAS Interdisciplinary Innovation Team
FX The authors acknowledge the funding support from the Key Deployment
Projects of Chinese Academy of Sciences (ZDRW_CN_2020-1), the
Sino-German Cooperation Research Project under the Natural Science
Foundation of China (51761135108) and the German Research Foundation
(392417756), and the CAS Interdisciplinary Innovation Team.
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NR 35
TC 14
Z9 15
U1 11
U2 48
PU ELSEVIER
PI AMSTERDAM
SN 1003-6326
EI 2210-3384
PD MAR
PY 2021
VL 31
IS 3
BP 817
EP 831
DI 10.1016/S1003-6326(21)65541-3
EA MAR 2021
PG 15
GA RA8NX
UT WOS:000631677900023
OA gold
DA 2023-12-05
ER
PT J
AU Wang, Z
Wen, GH
Liu, Q
Tang, P
Jiang, WB
Huang, SH
AF Wang, Zhe
Wen, Guanghua
Liu, Qiang
Tang, Ping
Jiang, Wenbo
Huang, Shuheng
TI A Comprehensive Investigation on the Microstructure and Thermal
Conductivity of CaO-Al2O3 Based Mold Slags:
Equilibrium Molecular Dynamics Simulations
LA English
DT Article
AB The microstructure and thermal conductivity of the CaO-Al2O3-based (CA-based)
mold slags are crucial for casting high aluminum steel. Herein, the microstructure
and thermal conductivity of the CA-based mold slags were systematically
investigated by using molecular dynamics (MD). Moreover, the effects of the
CaO/Al2O3 mole (C/A) ratio and CaO/SiO2 mole (C/S) ratio on the microstructure and
thermal conductivity of CA-based mold slags were studied. The results showed that
the Al-O structure plays a skeleton role in the CA-based mold slags. The thermal
conductivity of molten CA-based mold slags increases first and then decreases with
increasing C/A ratio. The thermal conductivity of molten CaO-Al2O3-SiO2-MgO-Na2O
(CASMN) slag is affected by the combination of short- and medium-range order
structures.
C1 [Wang, Zhe; Wen, Guanghua; Liu, Qiang; Tang, Ping; Jiang, Wenbo] Chongqing Univ,
[Wang, Zhe; Wen, Guanghua; Liu, Qiang; Tang, Ping; Jiang, Wenbo; Huang, Shuheng]
Chongqing Univ, State Key Lab Mech Transmiss, Chongqing 400044, Peoples R China.
[Huang, Shuheng] Chongqing Univ, Coll Bioengn, Chongqing 400044, Peoples R
China.
C3 Chongqing University; Chongqing University; Chongqing University
RP Wen, GH (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
EM wengh@cqu.edu.cn; shhuang@cqu.edu.cn
OI Wang, Zhe/0000-0003-0217-2909
FU Graduate Scientific Research and Innovation Foundation of Chongqing,
China [CYB19002]; National Natural Science Foundation of China
[51574050]
FX This study was funded by the Graduate Scientific Research and Innovation
Foundation of Chongqing, China (Grant Number CYB19002), and the National
Natural Science Foundation of China (Grant Number 51574050).
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NR 58
TC 14
Z9 14
U1 8
U2 35
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD JUN
PY 2021
VL 52
IS 3
BP 1574
EP 1581
DI 10.1007/s11663-021-02124-7
EA MAR 2021
PG 8
Engineering
GA SA1OJ
UT WOS:000629199300002
DA 2023-12-05
ER
PT J
AU Zhao, HL
Ma, BZ
Hong, S
Huang, H
Liu, FQ
Sohn, HY
AF Zhao, Hongliang
Ma, Baozhong
Hong, Shuang
Huang, Hao
Liu, Fengqin
Sohn, Hong Yong
TI Recovery of Copper and Cobalt from Converter Slags via
Reduction-Sulfurization Smelting Using Spent Pot Lining as the Reductant
LA English
DT Article
DE spent pot lining; converter slag; matte; copper; cobalt; recovery
AB Large amounts of solid wastes are produced in copper and aluminum smelting
processes, which not only cause losses of valuable resources but also threaten the
ecology and environment. In this study, a reduction-sulfurization smelting method
was used for recovering Cu and Co from converter slags by using spent pot lining
(SPL) as the reductant. CaO was added to fix the fluorine from SPL into the cleaned
slag. Thermodynamic analysis and experiments were performed to verify the
feasibility and determine the optimal conditions of this smelting process. The
optimum reductant addition of spent cathode carbon block (SCCB) and spent SiC side
block (SSCB) was 8-12 wt %, and the copper and cobalt recovery reached more than 98
and 96%, respectively. The addition of 10 wt % CaO for SCCB improved slag viscosity
and promoted the separation between slag and matte/alloy and fixed fluorine in the
cleaned slag in the form of insoluble calcium fluoride. The metallized Cu-Co matte
was obtained, in which Cu mainly existed in the form of sulfide and Co mainly
existed in the form of an iron cobalt alloy.
C1 [Zhao, Hongliang; Ma, Baozhong; Liu, Fengqin] Univ Sci & Technol Beijing, State
Key Lab Adv Met, Beijing 100083, Peoples R China.
[Zhao, Hongliang; Ma, Baozhong; Hong, Shuang; Huang, Hao; Liu, Fengqin] Univ Sci
& Technol Beijing, Sch Met & Ecol Engn, Beijing 100083, Peoples R China.
[Zhao, Hongliang; Sohn, Hong Yong] Univ Utah, Dept Mat Sci & Engn, Salt Lake
City, UT 84112 USA.
Technology Beijing; Utah System of Higher Education; University of Utah
RP Liu, FQ (corresponding author), Univ Sci & Technol Beijing, State Key Lab Adv
Met, Beijing 100083, Peoples R China.; Liu, FQ (corresponding author), Univ Sci &
Technol Beijing, Sch Met & Ecol Engn, Beijing 100083, Peoples R China.
EM liufq@ustb.edu.cn
FU National Natural Science Foundation of China [51974018]; Guangxi
Innovation-Driven Development Project [AA18242042-1]; Fundamental
Research Funds for the Central Universities [FRF-TP-19-016A3]; China
Scholarship Council
China (51974018), the Guangxi InnovationDriven Development Project
(AA18242042-1), and the Fundamental Research Funds for the Central
Universities (FRF-TP-19-016A3). The authors also thank the China
Scholarship Council for providing Chinese Government Scholarship to H.Z.
to study as a Visiting Scholar in H.Y.S.'s laboratory at the University
of Utah.
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NR 44
TC 14
Z9 14
U1 10
U2 71
PI WASHINGTON
SN 2168-0485
PD MAR 22
PY 2021
VL 9
IS 11
BP 4234
EP 4246
DI 10.1021/acssuschemeng.1c00444
EA MAR 2021
PG 13
GA RI2SF
UT WOS:000636758600029
DA 2023-12-05
ER
PT J
AU Wittkowski, A
Schirmer, T
Qiu, H
Goldmann, D
Fittschen, UEA
AF Wittkowski, Alena
Schirmer, Thomas
Qiu, Hao
Goldmann, Daniel
Fittschen, Ursula E. A.
TI Speciation of Manganese in a Synthetic Recycling Slag Relevant for
Lithium Recycling from Lithium-Ion Batteries
SO METALS
LA English
DT Article
DE lithium; engineered artificial minerals (EnAM); X-ray absorption near
edge structure (XANES); powder X-ray diffraction (PXRD); electron probe
microanalysis (EPMA); melt experiments
ID HYDROGEN-SULFIDE; SPECTROSCOPY; OXIDE
AB Lithium aluminum oxide has previously been identified to be a suitable compound
to recover lithium (Li) from Li-ion battery recycling slags. Its formation is
hampered in the presence of high concentrations of manganese (9 wt.% MnO2). In this
study, mock-up slags of the system Li2O-CaO-SiO2-Al2O3-MgO-MnOx with up to 17 mol%
MnO2-content were prepared. The manganese (Mn)-bearing phases were characterized
with inductively coupled plasma optical emission spectrometry (ICP-OES), X-ray
diffraction (XRD), electron probe microanalysis (EPMA), and X-ray absorption near
edge structure analysis (XANES). The XRD results confirm the decrease of LiAlO2
phases from Mn-poor slags (7 mol% MnO2) to Mn-rich slags (17 mol% MnO2). The Mn-
rich grains are predominantly present as idiomorphic and relatively large (>50 mu
m) crystals. XRD, EPMA and XANES suggest that manganese is present in the form of a
spinel solid solution. The absence of light elements besides Li and O allowed to
estimate the Li content in the Mn-rich grain, and to determine a generic
stoichiometry of the spinel solid solution, i.e., (Li(2x)Mn(1-x)2+)(1+x)(Al(2-
z),Mn-z(3+))O-4. The coefficients x and z were determined at several locations of
the grain. It is shown that the aluminum concentration decreases, while the
manganese concentration increases from the start (x: 0.27; z: 0.54) to the end (x:
0.34; z: 1.55) of the crystallization.
C1 [Wittkowski, Alena; Fittschen, Ursula E. A.] Tech Univ Clausthal, Inst Inorgan &
Analyt Chem, Arnold Sommerfeld Str 4, D-38678 Clausthal Zellerfeld, Germany.
[Schirmer, Thomas] Tech Univ Clausthal, Inst Disposal Res, Dept Mineral,
Geochem,Salt Deposits, Adolph Roemer Str 2A, D-38678 Clausthal Zellerfeld, Germany.
[Qiu, Hao; Goldmann, Daniel] Tech Univ Clausthal, Inst Mineral & Waste Proc,
Dept Mineral & Waste Proc, Waste Disposal & Geomech, Walther Nernst Str 9, D-38678
Clausthal Zellerfeld, Germany.
C3 TU Clausthal; TU Clausthal; TU Clausthal
RP Fittschen, UEA (corresponding author), Tech Univ Clausthal, Inst Inorgan &
Analyt Chem, Arnold Sommerfeld Str 4, D-38678 Clausthal Zellerfeld, Germany.
EM alena.wittkowski@tu-clausthal.de; thomas.schirmer@tu-clausthal.de;
hao.qiu@tu-clausthal.de; daniel.goldmann@tu-clausthal.de;
ursula.fittschen@tu-clausthal.de
RI Qiu, Hao/ABU-1105-2022; fittschen, ursula e a/Q-1049-2015
OI Qiu, Hao/0000-0002-7519-0916;
FU Clausthal University of Technology in the course of a joint research
project, "Engineering and Processing of Artificial Minerals for an
Advanced Circular Economy Approach for Finely Dispersed Critical
Elements" (EnAM)
FX This research was funded by the Clausthal University of Technology in
the course of a joint research project, "Engineering and Processing of
Artificial Minerals for an Advanced Circular Economy Approach for Finely
Dispersed Critical Elements" (EnAM).
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NR 27
TC 14
Z9 15
U1 0
U2 14
PU MDPI
PI BASEL
EI 2075-4701
J9 METALS-BASEL
JI Metals
PD FEB
PY 2021
VL 11
IS 2
AR 188
DI 10.3390/met11020188
PG 20
Engineering
GA QN9OS
UT WOS:000622779700001
DA 2023-12-05
ER
PT J
AU Paudel, SR
Yang, MJ
Gao, ZL
AF Paudel, Shree Raj
Yang, Mijia
Gao, Zhili
TI pH Level of Pore Solution in Alkali-Activated Fly-Ash Geopolymer
Concrete and Its Effect on ASR of Aggregates with Different Silicate
Contents
LA English
DT Article
DE Geopolymer; Alkali-silica reaction (ASR); Pore solution; Fly ash;
Expansion
ID CHLORIDE CONTAMINATED CONCRETE; PORTLAND-CEMENT; SLAG MORTARS
AB Durability has always been a major concern in concrete-based infrastructures.
Alkali-silica reaction (ASR) is the result of a chemical reaction between hydroxyl
ions in pore water and silica from aggregates and cement of the concrete matrix.
Geopolymer is a type of alkaline reactivated binder which can be synthesized by a
polycondensation reaction of geopolymeric precursors and alkali polysilicates. Due
to the alkaline solution brought in by alkali polysilicates, it is intuitive that a
higher alkaline concentration in pore solutions of geopolymer concrete will
adversely affect long-term performance. This study researched the preceding
hypothesis and reports the finding of an experimental investigation of alkali-
silica reaction between reactive aggregates and the geopolymer matrix. Specimens
were prepared using Class C fly ash with a high CaO content and three types of
aggregates (granite, carbonate, and gravel), each with different alkaline activator
ratios and Na2O doses. Each aggregate also had different percentages of silicate
and aluminum content. Mechanical testing of potential resistivity of the aggregates
was performed via length change. Pore solution of the hardened geopolymer concrete
was extracted and the pH value of the pore solution was determined. Results suggest
that the extent of ASR reaction based on the presence of all three types of
aggregates in fly ash-based geopolymer concrete is substantially smaller than that
of ordinary portland cement (OPC)-based concrete. Scanning electron microscopy
(SEM) and Fourier-transform infrared spectroscopy (FTIR) tests also revealed that
the amount ASR gel formed in geopolymer is less than that formed in ordinary
portland cement concrete. Hence, utilizing ASR vulnerable aggregates in the
production of geopolymer concrete might be permissible.
C1 [Paudel, Shree Raj; Yang, Mijia] North Dakota State Univ, Dept Civil & Environm
Engn, Fargo, ND 58108 USA.
[Gao, Zhili] North Dakota State Univ, Dept Construct Management & Engn, Fargo,
ND 58108 USA.
C3 North Dakota State University Fargo; North Dakota State University Fargo
RP Yang, MJ (corresponding author), North Dakota State Univ, Dept Civil & Environm
Engn, Fargo, ND 58108 USA.
EM Mijia.yang@ndsu.edu
RI Yang, Mijia/B-1847-2008
OI Yang, Mijia/0000-0002-5781-8765
FU North Dakota Department of transportation
FX The authors thank the North Dakota Department of transportation for the
financial support of this research. The findings in this paper are
solely the authors' interpretation.
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NR 36
TC 14
Z9 14
U1 4
U2 22
PI RESTON
SN 0899-1561
EI 1943-5533
PD SEP 1
PY 2020
VL 32
IS 9
AR 04020257
DI 10.1061/(ASCE)MT.1943-5533.0003344
PG 12
GA OO6IS
UT WOS:000587481800038
DA 2023-12-05
ER
PT J
AU Ye, HL
Huang, L
AF Ye, Hailong
Huang, Le
TI Degradation mechanisms of alkali-activated binders in sulfuric acid: The
role of calcium and aluminum availability
LA English
DT Article
DE Alkali-activated binders; Sulfuric acid attack; Sodium calcium
aluminosilicate hydrate (NCASH); Ettringite; Gypsum
ID S-H GELS.; GEOPOLYMER MATERIALS; PHASE ASSEMBLAGE; SLAG; RESISTANCE;
MICROSTRUCTURE; SHRINKAGE; SODIUM; SILICA; DURABILITY
AB Although alkali-activated binders (AABs) show a stronger resistance against
sulfuric acid (H2SO4) attack than ordinary Portland cement (OPC), it remains
unclear how the resistance capacity is affected by the compositional variability of
gel products, i.e., sodium calcium aluminosilicate hydrate (N-C-A-S-H). In this
work, the compositional and molecular alteration of synthetic N-C-A-S-H exposed to
1.0%, 2.5%, and 5.0% H2SO4 solutions are studied. The results show that the
formation of ettringite is less favored than gypsum when the calcium availability
is limited, despite sufficient aluminum sources. The calcium and aluminum dissolved
from N-C-A-S-H can contribute to the ettringite formation even though the AFm
phases are present, particularly for those with relatively high Ca/Si and Al/Si
ratios. The aluminum content in AABs controls the AFm formation and Al/Si ratio of
N-C-A-S-H, thus affecting the condition for ettringite and gypsum precipitation.
The presence of calcium in the atomic structure of N-C-A-S-H makes it more
susceptible to the acid-induced degradation and polymerization. (C) 2020 Elsevier
C1 [Ye, Hailong; Huang, Le] Univ Hong Kong, Dept Civil Engn, Pokfulam, Hong Kong,
Peoples R China.
C3 University of Hong Kong
RP Ye, HL; Huang, L (corresponding author), Univ Hong Kong, Dept Civil Engn,
Pokfulam, Hong Kong, Peoples R China.
EM hlye@hku.hk; huangle@hku.hk
OI Ye, Hailong/0000-0003-2665-3942
FU Hong Kong Research Grants Council [17200719]
FX The financial support from Hong Kong Research Grants Council (Project
number: 17200719) is greatly appreciated. Any opinions, findings and
conclusions or recommendations expressed in this material are those of
the authors and do not necessarily reflect the views of the sponsors.
10.1016/j.cemconres.2018.06.011
[Anonymous], CEM CONCR RES
10.1016/j.conbuildmat.2013.01.018
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10.1016/j.conbuildmat.2017.03.238
10.1016/j.conbuildmat.2016.06.099
10.1016/j.cemconres.2004.10.042
NR 50
TC 14
Z9 15
U1 3
U2 17
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD JUN 20
PY 2020
VL 246
AR 118477
DI 10.1016/j.conbuildmat.2020.118477
PG 10
GA LF3GR
UT WOS:000527309800040
DA 2023-12-05
ER
PT J
AU Zhang, CD
Hu, B
Wang, HG
Mingyu,
Wang, XW
AF Zhang, Changda
Hu, Bin
Wang, Huaguang
Wang, Mingyu
Wang, Xuewen
TI Recovery of valuable metals from copper slag
SO MINING METALLURGY & EXPLORATION
LA English
DT Article
DE Copper slag; Sulfation roasting; Sulfate decomposition roasting; Water
leaching
ID REDUCTION-MAGNETIC SEPARATION; CONVERTER SLAG; NICKEL; TEMPERATURE;
VALUES; COBALT
AB The copper smelting process produces plenty of copper slag every year, which is
a hazardous solid waste, but a secondary resource. In the present study, the
extraction of copper, nickel, and cobalt from copper slag was investigated through
the process of sulfation roasting-water leaching and the process of sulfation
roasting-sulfate decomposition roasting-water leaching respectively. Compared with
the process of sulfation roasting-water leaching, the process of sulfation
roasting-sulfate decomposition roasting-water leaching is a better choice, which
could not only get almost the same leaching of copper, nickel, and cobalt as the
former process, but has a lower leaching of iron and aluminum. For the process of
sulfation roasting-sulfate decomposition roasting-water leaching, the leaching of
Cu, Ni, and Co reached up to 74.2%, 71.1%, and 69.6% respectively, under the
optimal conditions including sulfation roasted with 80 wt% sulfuric acid addition
at 200 degrees C for 60 min and sulfate decomposition roasted at 650 degrees C for
60 min, followed by water leached at 90 degrees C for 30 min with a liquid-solid
ratio of 2 ml/g. The leaching of Fe and Al was only 4.9% and 17.6%.
C1 [Zhang, Changda; Hu, Bin; Wang, Mingyu; Wang, Xuewen] Cent South Univ, Sch Met &
Environm, Changsha 410083, Peoples R China.
[Wang, Huaguang] Michigan Technol Univ, Dept Mat Sci & Engn, Houghton, MI 49931
USA.
C3 Central South University; Michigan Technological University
RP Mingyu, (corresponding author), Cent South Univ, Sch Met & Environm, Changsha
EM wmydxx@163.com
RI wang, mingyu/E-5977-2016
OI wang, mingyu/0000-0001-8317-4708
FU National Natural Science Foundation of China [51974369]; Natural Science
Foundation of Hunan Province [2016JJ2142]
FX This study was financially supported by the National Natural Science
Foundation of China (51974369) and the Natural Science Foundation of
Hunan Province (2016JJ2142).
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NR 21
TC 14
Z9 14
U1 2
U2 56
PI HEIDELBERG
SN 2524-3462
EI 2524-3470
J9 MINING METALL EXPLOR
JI Mining Metall. Explor.
PD AUG
PY 2020
VL 37
IS 4
BP 1241
EP 1251
DI 10.1007/s42461-020-00224-7
EA MAY 2020
PG 11
GA MH4TK
UT WOS:000530237000001
DA 2023-12-05
ER
PT J
AU Cao, X
Kong, LX
Bai, J
Zhao, HL
Ge, ZF
Li, HZ
Bai, ZQ
Li, W
AF Cao, Xi
Kong, Lingxue
Bai, Jin
Zhao, Huiling
Ge, Zefeng
Li, Huaizhu
Bai, Zongqing
Li, Wen
TI Effect of water vapor on viscosity behavior of coal slags with high
silicon-aluminum level under gasification condition
SO FUEL
LA English
DT Article
DE Coal gasification; Slagging gasifiers; Viscosity behavior; Coal slag
with high silicon-aluminum level; Water vapor
ID DISSOLUTION MECHANISMS; RHYOLITIC MELTS; PHASE-FORMATION; ASH SLAGS;
FLOW; TEMPERATURE; SOLUBILITY; H2O; MODEL; IRON
AB For the slagging gasifiers, the slag viscosity behavior is a critical parameter
for the smooth slag tapping and long term operation. Water vapor is an important
component of the syngas in the gasifier, especially for coal water slurry
gasification. This paper presents the results of a study to investigate the effect
of water vapor on viscosity behavior of coal slags with high silicon-aluminum
level. The viscosities of three synthetic coal slags with different Si/Al ratios
(mass ratio of SiO2 and Al2O3) was measured in argon with 10%, 20% and 30% water
vapor as a function of temperature. As the water vapor proportion increased, the
viscosity of the slag with high silicon-aluminum level at same temperature
increased slightly. Besides, the slag with Si/Al of 2.0 transformed from a glassy
slag to a crystalline one when the water vapor proportion was increase up to 30%.
The oxidation state of iron of the slags was not affected by the increase in water
vapor proportion under Ar with water vapor condition. Analysis of the slag
structure demonstrated that water vapor entering the slag was benefit to the
formation of Si-O-Si bridges and [AlO4](5-) structure. Meanwhile, activation energy
for viscous flow (E-eta) increased with the increasing water vapor proportion.
Water vapor also promotes crystallization and growth of crystals of the slag with
high silicon-aluminum level during cooling, leading to the increase in the
temperature of critical viscosity (T-cv).
C1 [Cao, Xi; Kong, Lingxue; Bai, Jin; Zhao, Huiling; Ge, Zefeng; Li, Huaizhu; Bai,
Zongqing; Li, Wen] Chinese Acad Sci, Inst Coal Chem, State Key Lab Coal Convers,
[Cao, Xi; Ge, Zefeng] Univ Chinese Acad Sci, Beijing 100049, Peoples R China.
RP Bai, J (corresponding author), Chinese Acad Sci, Inst Coal Chem, State Key Lab
Coal Convers, Taiyuan 030001, Shanxi, Peoples R China.
EM stone@sxicc.ac.cn
OI Bai, Jin/0000-0002-8623-1656
FU National Key R&D program of China [2017YFB0602603]; Joint Foundation of
Natural Science Foundation of China and Shanxi Province [U1510201];
NSFC-DFG [21761132032]; Joint Foundation of Natural Science Foundation
of China and Xinjiang [U1703252]; Youth Innovation Promotion
Association, CAS; International Partnership Program of Chinese Academy
of Sciences [122214KYSB20170020]
FX This work was supported by the National Key R&D program of China [grant
number 2017YFB0602603], Joint Foundation of Natural Science Foundation
of China and Shanxi Province [grant number U1510201], NSFC-DFG [grant
number 21761132032], Joint Foundation of Natural Science Foundation of
China and Xinjiang [grant number U1703252], Youth Innovation Promotion
Association, CAS, International Partnership Program of Chinese Academy
of Sciences [grant number 122214KYSB20170020].
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NR 43
TC 14
Z9 15
U1 4
U2 80
PU ELSEVIER SCI LTD
PI OXFORD
SN 0016-2361
EI 1873-7153
J9 FUEL
JI Fuel
PD JAN 15
PY 2020
VL 260
AR 116351
DI 10.1016/j.fuel.2019.116351
PG 9
GA JG2DB
UT WOS:000491885400025
DA 2023-12-05
ER
PT J
AU Akturk, B
Nayak, S
Das, S
Kizilkanat, AB
AF Akturk, Busra
Nayak, Sumeru
Das, Sumanta
Kizilkanat, Ahmet B.
TI Microstructure and Strength Development of Sodium Carbonate-Activated
Blast Furnace Slags
LA English
DT Article
DE Alkali-activated materials; Compressive strength development;
Microstructure; Slag; Sodium carbonate
ID HYDRATION PROPERTIES; THERMAL-PROPERTIES; REACTION-KINETICS; CEMENT;
HYDROTALCITE; REACTIVITY; EVOLUTION; PRODUCTS; WASTE; GLASS
AB This paper presents the study of alkali-activated slags where sodium carbonate
acts as a primary activator. The slow activation mechanism of sodium carbonate is
accelerated by sodium hydroxide and with traces of calcium hydroxide. Strength
development and the progress of hydration of the mixes were studied with the phase
transformation and development of microstructural features through quantitative
techniques such as thermogravimetric analysis and phase-identification techniques
such as Fourier transform infrared spectroscopy and X-ray diffraction. Sodium
carbonate replacement with sodium hydroxide and the presence of calcium hydroxide
in the binder as a replacement for the slag enhances the rate of dissolution of
slag, leading to faster strength development. Calcium hydroxide significantly
increases the compressive strength, even at an early age. On the other hand, sodium
hydroxide substitution is effective at later ages of the reaction when used at high
dosages (e.g., 40%). Formation of strength-giving phases such as hydrotalcite and
calcium aluminum silicate hydrate are confirmed with microstructure analysis and
explain the strength development.
C1 [Akturk, Busra; Kizilkanat, Ahmet B.] Yildiz Tech Univ, Dept Civil Engn,
Construct Mat Div, Davutpasa Campus, TR-34220 Istanbul, Turkey.
[Nayak, Sumeru; Das, Sumanta] Univ Rhode Isl, Dept Civil & Environm Engn,
Kingston, RI 02881 USA.
C3 Yildiz Technical University; University of Rhode Island
RP Kizilkanat, AB (corresponding author), Yildiz Tech Univ, Dept Civil Engn,
Construct Mat Div, Davutpasa Campus, TR-34220 Istanbul, Turkey.
EM bucar@yildiz.edu.tr; sumeru@uri.edu; sumanta_das@uri.edu;
bkkanat@yildiz.edu.tr
RI Akturk, Busra/AEZ-1900-2022; Akturk, Busra/JCO-1851-2023; Das,
Sumanta/HKW-0326-2023
OI Akturk, Busra/0000-0003-1484-7758; Akturk, Busra/0000-0003-1484-7758;
Das, Sumanta/0000-0001-5339-7708; Nayak, Sumeru/0000-0002-5133-230X
FU Yildiz Technical University Research Foundation [2016-05-01-DOP03]
FX This work was supported by the research grant of Yildiz Technical
University Research Foundation (Project No. 2016-05-01-DOP03).
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NR 49
TC 14
Z9 14
U1 8
U2 58
PI RESTON
SN 0899-1561
EI 1943-5533
PD NOV 1
PY 2019
VL 31
IS 11
AR 04019283
DI 10.1061/(ASCE)MT.1943-5533.0002944
PG 11
GA IY1XK
UT WOS:000486184800012
OA Green Submitted
DA 2023-12-05
ER
PT J
AU Braz, IG
Shinzato, MC
Montanheiro, TJ
de Almeida, TM
Carvalho, FMD
AF Braz, Inara Guglielmetti
Shinzato, Mirian Chieko
Montanheiro, Tarcisio Jose
de Almeida, Thelma Miranda
de Souza Carvalho, Flavio Machado
TI Effect of the Addition of Aluminum Recycling Waste on the Pozzolanic
Activity of Sugarcane Bagasse Ash and Zeolite
LA English
DT Article
DE Aluminum hydroxide; Pozzolanic activity; Hydrated products; Carbonation
ID PORTLAND-CEMENT; HYDRATION; MORPHOLOGY; CONCRETE; INDUSTRY; PHASES;
LIME; SLAG
AB The pozzolanic activity of aluminum recycling waste (AW) was evaluated along
with sugarcane bagasse ash (BA) and zeolite (ZE) to give a more sustainable use.
These materials were characterized and submitted to the pozzolanic activity test by
a modified Chapelle test and the compressive strength of mortars prepared with
limestone Portland cement (LPC). The final solids were characterized again to
determine the hydrated products. The main reactive chemical components of AW are
Al2O3 and MgO, which are in the form of hydroxides, such as nordstrandite (Al(OH)
(3)), meixnerite ([Mg5Al3(OH)(16)][(OH)(3)(H2O)(4)]), brucite (Mg(OH)(2)) and
magnesium chloride hydroxide hydrate (Mg-3(OH)(5)Cl4H(2)O). All of the studied
materials were classified as pozzolans by the modified Chapelle test, and the main
hydrated products formed in the AW sample were katoite, ettringite, talc and
amesite. When mixed with BA and ZE, C-A-S-H and C-S-H phases were also formed. The
C-S-H phases and portlandite were detected only in the solids of the modified
Chapelle test of BA and ZE. Calcite was present in all samples, indicating that
part of the Ca(OH)(2) was consumed by the carbonation process. The compressive
strength test of mortars revealed that only ZE is a pozzolan. In mortars containing
AW the production of ettringite and calcium carboaluminate increased due to the
reactions of aluminum, respectively, with gypsum and calcite present in LPC. In
addition to portlandite, C-S-H was formed only in the BA and ZE mortars. Although
hydration reactions were not sufficient to form C-S-H in AW mortar, reactive
aluminum favors the formation of primary ettringite.
C1 [Braz, Inara Guglielmetti; Shinzato, Mirian Chieko; de Almeida, Thelma Miranda]
Univ Fed Sao Paulo, Inst Ciencias Ambientais Quim & Farmaceut, Rua Sao Nicolau 210,
BR-09913030 Diadema, SP, Brazil.
[Montanheiro, Tarcisio Jose] Inst Geol Estado Sao Paulo, Rua R Joaquim Tavora
822, BR-04018032 Sao Paulo, SP, Brazil.
[de Souza Carvalho, Flavio Machado] Univ Sao Paulo, Inst Geociencias, Rua Lago
562, BR-05508080 Sao Paulo, SP, Brazil.
C3 Universidade Federal de Sao Paulo (UNIFESP); Universidade de Sao Paulo
RP Shinzato, MC (corresponding author), Univ Fed Sao Paulo, Inst Ciencias
Ambientais Quim & Farmaceut, Rua Sao Nicolau 210, BR-09913030 Diadema, SP, Brazil.
EM inaragbraz@gmail.com; mirian.chieko@unifesp.br;
tarcisio.montanheiro@gmail.com; thelmamda@gmail.com; flavioms@usp.br
RI carvalho, flavio M S/O-3831-2014
FU FAPESP [2011/13168-1]; CAPES; Fundacao de Amparo a Pesquisa do Estado de
Sao Paulo (FAPESP) [11/13168-1] Funding Source: FAPESP
FX We thank FAPESP (2011/13168-1) for financial support and CAPES for the
scholarship for MSc Inara G. Braz. Special thanks to Mrs. Elizabeth
Almeida of Reciclagem de Metais Fernao Dias Ltda., NIPE (UNIFESP-Campus
Diadema), Celta Brasil and Industria Santa Rosa. We also thank the
anonymous referees for their valuable comments.
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Zhang Z., 1995, PROGRAM ABSTRACTS ZE, P221
NR 80
TC 14
Z9 15
U1 2
U2 23
PU SPRINGER
PI DORDRECHT
SN 1877-2641
EI 1877-265X
PD NOV
PY 2019
VL 10
IS 11
BP 3493
EP 3513
DI 10.1007/s12649-018-0342-6
PG 21
GA JF1YK
UT WOS:000491182900028
DA 2023-12-05
ER
PT J
AU Zhao, PD
Zhang, H
Yu, J
Gao, HJ
Cao, Y
Zhu, YQ
Zhao, HZ
AF Zhao, Pengda
Zhang, Han
Yu, Jun
Gao, Hongjun
Cao, Yang
Zhu, Yuqian
Zhao, Huizhong
TI Conditions for mutual conversion of Cr(III) and Cr(IV) in aluminum
chromium slag
LA English
DT Article
DE Aluminum chromium slag; Refractory; Hexavalent chromium
ID HEXAVALENT CHROMIUM; OXIDATION
AB The conditions for the mutual conversion of Cr(III) and Cr(VI) are investigated
to realize safe application of aluminum chromium slag. Aluminum chromium slag is
sintered with conventional refractory oxides in different atmospheres and at
different temperatures to examine the phase of the sample and its Cr(VI) content in
an aqueous solution. The results show that the slag system contains CaO and MgO
that facilitate Cr(VI) formation, Al2O3 that inhibits Cr(VI) formation, TiO2,
Fe2O3, and SiO2 that reduce Cr(VI) to Cr(III). In a reducing atmosphere, even if
the alkaline environment condition is satisfied, Cr(VI) in the aluminum chromium
slag is reduced to Cr(III), thus detoxifying the slag. In addition, under alkaline
environment and oxidizing atmosphere conditions, the slag temperature corresponding
to the transition of Cr(VI) to Cr(III) is between 900 degrees C and 1000 degrees C.
Thus, the transition of Cr(III) to Cr(VI) in aluminum chromium slag requires three
conditions, alkaline environment, oxidizing atmosphere, and high temperature, and
all the three conditions are indispensable. Consequently, the safe application of
aluminum chromium slag can be realized by controlling the conditions for the mutual
conversion of Cr (III) and Cr (VI). (C) 2019 Published by Elsevier B.V.
C1 [Zhao, Pengda; Zhang, Han; Yu, Jun; Zhao, Huizhong] Wuhan Univ Sci & Technol,
State Key Lab Refractories & Met, Wuhan 430081, Hubei, Peoples R China.
[Gao, Hongjun; Cao, Yang; Zhu, Yuqian] Jinzhou Ji Xin High Temp Mat Co Ltd,
Jinzhou 121005, Peoples R China.
C3 Wuhan University of Science & Technology
RP Zhao, HZ (corresponding author), Wuhan Univ Sci & Technol, State Key Lab
Refractories & Met, Wuhan 430081, Hubei, Peoples R China.
EM wustnano@163.com
FX This work was Project 51804233, supported by the National Natural
Science Foundation of China. We would also like to thank Editage
[www.editage.cn] for English language editing.
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NR 14
TC 14
Z9 17
U1 5
U2 50
PI LAUSANNE
SN 0925-8388
EI 1873-4669
J9 J ALLOY COMPD
JI J. Alloy. Compd.
PD JUN 5
PY 2019
VL 788
BP 506
EP 513
DI 10.1016/j.jallcom.2019.02.093
PG 8
GA HQ9SE
UT WOS:000462767000059
DA 2023-12-05
ER
PT J
AU Prentice, DP
Walkley, B
Bernal, SA
Bankhead, M
Hayes, M
Provis, JL
AF Prentice, Dale P.
Walkley, Brant
Bernal, Susan A.
Bankhead, Mark
Hayes, Martin
Provis, John L.
TI Thermodynamic modelling of BFS-PC cements under temperature conditions
relevant to the geological disposal of nuclear wastes
LA English
DT Article
ID C-S-H; BLAST-FURNACE SLAG; HYDRATION TEMPERATURE; CURING TEMPERATURE;
PART I; PHASES; MICROSTRUCTURE; IMMOBILIZATION; HYDROGARNET; CHEMISTRY
AB Intermediate level waste produced in UK nuclear power generation is encapsulated
or immobilised in blended cements comprising blast furnace slag (BFS) and Portland
cement (PC), to be emplaced in a proposed geological disposal facility (GDF). The
wasteforms are expected to be exposed to temperatures from 35 to 80 degrees C
during the initial 150 years of GDF operation. Thermodynamic modelling is applied
here to describe the phase assemblages of hydrated 1:1, 3:1 and 9:1 BFS-PC blends,
with the participation of hydrogarnet as an important phase above 60 degrees C. The
chemical composition of the main phase forming in these systems, an aluminium rich
calcium silicate hydrate (C-A-S-H), was well described by a solid-solution model
with explicit Al incorporation, although the Al/Si ratio was systematically
slightly under-predicted. The developed thermodynamic model predicts the correct
phase assemblage across varying temperature regimes, making it a valuable tool to
assess the effects of temperature on cements.
C1 [Prentice, Dale P.; Walkley, Brant; Bernal, Susan A.; Provis, John L.] Univ
Sheffield, Dept Mat Sci & Engn, Sheffield S1 3JD, S Yorkshire, England.
[Bernal, Susan A.] Univ Leeds, Sch Civil Engn, Woodhouse Lane, Leeds LS2 9JT, W
Yorkshire, England.
[Bankhead, Mark; Hayes, Martin] Natl Nucl Lab, Chadwick House,Warrington
Rd,Birchwood Pk, Warrington WA3 6AE, Cheshire, England.
C3 University of Sheffield; University of Leeds
RP Bernal, SA; Provis, JL (corresponding author), Univ Sheffield, Dept Mat Sci &
Engn, Sheffield S1 3JD, S Yorkshire, England.; Bernal, SA (corresponding author),
Univ Leeds, Sch Civil Engn, Woodhouse Lane, Leeds LS2 9JT, W Yorkshire, England.
EM S.A.BernalLopez@Leeds.ac.uk; j.provis@sheffield.ac.uk
RI Provis, John/AAR-3260-2020; Bernal, Susan A/E-8938-2011; Prentice,
Dale/ABE-2008-2020; Provis, John L/A-7631-2008
OI Provis, John/0000-0003-3372-8922; Prentice, Dale/0000-0002-4980-8751;
Provis, John L/0000-0003-3372-8922; Walkley, Brant/0000-0003-1069-1362
FU National Nuclear Laboratory; EPSRC through an iCASE Award; EPSRC
[EP/R001642/1]; UK Department of Energy and Climate Change; EPSRC
[EP/R001642/1] Funding Source: UKRI
FX D. Prentice is grateful to the National Nuclear Laboratory and EPSRC for
sponsoring his PhD research studies through an iCASE Award. The
participation of S.A. Bernal in this study was sponsored by EPSRC
through her Early Career Fellowship (EP/R001642/1). This research was
performed in part at the MIDAS Facility, at the University of Sheffield,
which was established with support from the UK Department of Energy and
Climate Change.
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NR 67
TC 14
Z9 14
U1 0
U2 9
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD MAY
PY 2019
VL 119
BP 21
EP 35
DI 10.1016/j.cemconres.2019.02.005
PG 15
GA HT3RZ
UT WOS:000464482200003
DA 2023-12-05
ER
PT J
AU Rashkovskiy, SA
AF Rashkovskiy, Sergey A.
TI Formation of solid residues in combustion of boron-containing solid
propellants
SO ACTA ASTRONAUTICA
LA English
CT 7th European Conference on Aeronautics and Space Sciences (EUCASS)
CY JUL 03-06, 2017
CL Milan, ITALY
DE Boron-containing solid propellant; Boron particle conglomeration; Slag
formation; Numerical simulation
ID DIRECT NUMERICAL-SIMULATION; ALUMINUM AGGLOMERATION; METAL
AGGLOMERATION; PARTICLES; MODEL; MICROSTRUCTURE
AB Boron-containing solid propellants are promising propellants for ducted rockets.
The experimental data show that combustion of boron-containing propellants is
accompanied by an intense conglomeration of the boron particles near the burning
surface. As a result, the boron particles conglomerates which are the branched
coral structures composed of sintered boron particles are formed in combustion of
boron-containing solid propellants. This results in decrease in combustion
efficiency of ducted rockets. To calculate the ignition and combustion of a
conglomerate in the secondary combustor of a ducted rocket, it is necessary to know
the size, structure and shape of the boron particle conglomerates that can
significantly affect these processes. In this paper, we consider a model and a
method for calculating the boron particles conglomeration in combustion of the
boron-containing solid propellants. The process of the boron particles
conglomeration is considered as a result of competition between two main processes:
the formation of adhesive bonds between the contacting boron particles and rupture
of these bonds under the action of the aerodynamic detached force from the side the
flow of gaseous combustion products of solid propellant. The criterion of formation
of residues (slag) on the burning surface of boron-containing propellants is
considered. It is shown that depending on the propellant burning rate law, two
different types of propellants with different conglomeration behavior can exist.
The results of calculations of the boron particles conglomeration which demonstrate
the slag formation are shown.
C1 [Rashkovskiy, Sergey A.] Russian Acad Sci, Ishlinsky Inst Problems Mech, 101-1
Vernadskogo Ave, Moscow 119526, Russia.
[Rashkovskiy, Sergey A.] Tomsk State Univ, 36 Lenina Ave, Tomsk 634050, Russia.
C3 Russian Academy of Sciences; Ishlinsky Institute for Problems in
Mechanics RAS; Tomsk State University
RP Rashkovskiy, SA (corresponding author), Russian Acad Sci, Ishlinsky Inst
Problems Mech, 101-1 Vernadskogo Ave, Moscow 119526, Russia.
EM rash@ipmnet.ru
RI Rashkovskiy, Sergey/HNJ-0002-2023; Rashkovskiy, Sergey A/J-7781-2013
OI Rashkovskiy, Sergey A/0000-0001-5683-5988
FU Tomsk State University competitiveness improvement program
[AAAA-A17-117021310385-6]
FX This work was done on the theme of the State Task No.
AAAA-A17-117021310385-6. Funding was provided in part by the Tomsk State
University competitiveness improvement program.
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NR 24
TC 14
Z9 16
U1 4
U2 25
PI OXFORD
SN 0094-5765
EI 1879-2030
J9 ACTA ASTRONAUT
JI Acta Astronaut.
PD MAY
PY 2019
VL 158
BP 277
EP 285
DI 10.1016/j.actaastro.2019.03.034
PG 9
SC Engineering
GA HS6KZ
UT WOS:000463982100028
DA 2023-12-05
ER
PT J
AU Yan, W
Chen, WQ
Yang, YD
McLean, A
AF Yan, Wei
Chen, Weiqing
Yang, Yindong
McLean, Alexander
TI Viscous characteristics and modelling of
CaO-Al2O3-based mould flux with
B2O3 as a substitute for CaF2
LA English
DT Article
DE CaO-Al2O3-based mould flux; fluoride-free; low-fluoride; viscosity;
modelling
ID VISCOSITY; CRYSTALLIZATION; CAO-SIO2; SLAG
AB Following a series of laboratory studies on the development of fluoride-free or
low-fluoride CaO-Al2O3-based mould flux for continuous casting of high-aluminium
steel, the viscosity properties of CaO-Al2O3-based mould flux with B2O3 as a
substitute for CaF2 were investigated using the rotating cylinder method. It was
found that B2O3 behaved in a similar manner to CaF2 in changing the viscosity of
the flux system. From calculations of the viscous activation energies, it was found
that similar changes in the concentrations of CaF2 and B2O3 resulted in almost the
same changes in activation energy. A viscosity prediction model was developed using
the optical basicity concept as an indicator of melt behaviour. Predicted viscosity
values showed good agreement with measurements reported in the literature.
C1 [Yan, Wei; Chen, Weiqing] Univ Sci & Technol, State Key Lab Adv Met, Beijing
[Yang, Yindong; McLean, Alexander] Univ Toronto, Dept Mat Sci & Engn, Toronto,
ON, Canada.
RP Yan, W (corresponding author), Univ Sci & Technol, State Key Lab Adv Met,
RI chen, weiqing/G-3874-2011
FU China Postdoctoral Science Foundation [2016M600920]; Fundamental
Research Funds for the Central Universities [FRF-TP-16-020A1];
Independent R&D Funds of State Key Laboratory of Advanced Metallurgy
[41616008]
FX This work was financially supported by the China Postdoctoral Science
Foundation (2016M600920), the Fundamental Research Funds for the Central
Universities (FRF-TP-16-020A1) and the Independent R&D Funds of State
Key Laboratory of Advanced Metallurgy (41616008).
Choi SY, 2004, J NON-CRYST SOLIDS, V345, P157, DOI
10.1016/j.jnoncrysol.2004.08.015
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Lee IR, 1993, P C CONT CAST STEEL
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8620.2013.01.013, DOI 10.3969/J.ISSN.1003-8620.2013.01.013]
NR 23
TC 14
Z9 14
U1 3
U2 22
PI ABINGDON
SN 0301-9233
EI 1743-2812
J9 IRONMAK STEELMAK
PD APR 21
PY 2019
VL 46
IS 4
BP 347
EP 352
DI 10.1080/03019233.2017.1394033
PG 6
GA HT5LJ
UT WOS:000464604900005
DA 2023-12-05
ER
PT J
AU Gao, YX
Leng, M
Chen, YF
Chen, ZC
Li, JL
AF Gao, Yuxiang
Leng, Mei
Chen, Yangfan
Chen, Zhichao
Li, Jiangling
TI Crystallization Products and Structural Characterization of
CaO-SiO2-Based Mold Fluxes with Varying
Al2O3/SiO2 Ratios
SO MATERIALS
LA English
DT Article
DE crystallization products; structure; Al2O3; SiO2 ratio; mold flux
ID RAMAN-SPECTRA; SYSTEM; VISCOSITY; TITANIUM; STEEL; SLAGS; CAF2
AB During the casting of high aluminum steel, the dramatic increase in the
Al2O3/SiO2 ratio is inevitable, resulting in significant changes of the
crystallization behavior, which would result in heat transfer and lubrication
problems. Crystallization products and structure characterization of glassy CaO-
SiO2-based mold fluxes with different Al2O3/SiO2 ratios were experimentally
investigated using a differential scanning calorimetry technique and Raman
spectroscopy. With increasing Al2O3/SiO2 ratios, the following results were
obtained. The crystallization temperature and the crystallization products are
changed. With increasing Al2O3/SiO2 ratios from 0.088 to 0.151, the crystallization
temperature first increases greatly from 1152 degrees C to 1354 degrees C, and then
moderately increases. The crystallization ability of the mold flux is strengthened.
The species of the precipitated crystalline phase change from two kinds, i.e.,
Ca4Si2O7F2 and Ca2SiO4, to four kinds, i.e., Ca4Si2O7F2, Ca2SiO4,
2CaOAl(2)O(3)SiO(2) and Ca12Al14O32F2, the crystallization ability of Ca4Si2O7F2 is
gradually attenuated, but other species show the opposite trend. The results of
Raman spectroscopy indicate that Al3+ mainly acts as a network former by the
information of [AlO4]-tetrahedral structural units, which can connect with [SiO4]-
tetrahedral by the formation of new bridge oxygen of Al-O-Si linkage, but there is
no formation of Al-O-Al linkage. The linkage of Al-O-Si increases and that of Si-O-
Si decreases. The polymerization degree of the network and the average number of
bridging oxygens decrease. Further, the relatively strong Si-O-Si linkage gradually
decreases and the relatively weak Al-O-Si gradually increases. The change of the
crystalline phase was interpreted from the phase diagram and structure.
C1 [Gao, Yuxiang; Leng, Mei; Chen, Yangfan; Chen, Zhichao; Li, Jiangling] Chongqing
Univ, Coll Mat Sci & Engn, Chongqing 400044, Peoples R China.
[Gao, Yuxiang; Leng, Mei; Chen, Yangfan; Chen, Zhichao; Li, Jiangling] Chongqing
Univ, Chongqing Key Lab Vanadium Titanium Met & New Mat, Chongqing 400044, Peoples
R China.
C3 Chongqing University; Chongqing University
RP Li, JL (corresponding author), Chongqing Univ, Coll Mat Sci & Engn, Chongqing
400044, Peoples R China.; Li, JL (corresponding author), Chongqing Univ, Chongqing
Key Lab Vanadium Titanium Met & New Mat, Chongqing 400044, Peoples R China.
EM 20162805@cqu.edu.cn; 201809021083@cqu.edu.cn; 20162806@cqu.edu.cn;
20162749@cqu.edu.cn; lijiangling@cqu.edu.cn
OI Chen, Zhichao/0000-0001-9666-4183
FU Natural Science Foundation of China [51704050]; China Postdoctoral
Science Foundation [2017M612905]; Fundamental Research Funds for the
Central Universities [2018CDXYCL0018]; National Training Program of
Innovation and Entrepreneurship for Undergraduates [201810611046]
FX This research was funded by [Natural Science Foundation of China] grant
number [51704050], [China Postdoctoral Science Foundation] grant number
[2017M612905], [Fundamental Research Funds for the Central Universities]
grand number [2018CDXYCL0018] and [National Training Program of
Innovation and Entrepreneurship for Undergraduates] grand number
[201810611046].
CR ALBERTO HV, 1995, PHYS CHEM GLASSES, V36, P114
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NR 26
TC 14
Z9 15
U1 0
U2 10
PU MDPI
PI BASEL
SN 1996-1944
J9 MATERIALS
JI Materials
PD JAN 2
PY 2019
VL 12
IS 2
AR 206
DI 10.3390/ma12020206
PG 12
Physics
GA HM8GY
UT WOS:000459719000010
OA gold, Green Submitted, Green Published
DA 2023-12-05
ER
PT J
AU Heo, JH
Park, JH
AF Heo, Jung Ho
Park, Joo Hyun
TI Thermochemical analysis for the reduction behavior of FeO in EAF slag
via Aluminothermic Smelting Reduction (ASR) process: Part II.
Effect of aluminum dross and lime fluxing on Fe and Mn recovery
LA English
DT Article
DE Electric arc furnace (EAF) slag; Aluminothermic smelting reduction
(ASR); Al dross; Iron recovery; Lime fluxing; Apparent viscosity;
Thermochemical computation
ID WASTE; SEPARATION; REUSE
AB We investigated Fe recovery from EAF slag by means of aluminothermic smelting
reduction (ASR) at 1773 K with Al dross as the reductant, especially the effect of
the added amount of the fluxing agent CaO on the Fe recovery. The maximum reaction
temperature calculated using FactSage (TM) 7.0 decreased with increasing CaO
addition, but the experimentally measured maximum temperatures increased with
increasing CaO addition. We calculated the amounts of various phases before and
after Al dross addition under different conditions of added CaO. FeO and Al2O3
contents in molten slag sharply varied within the first 5 min of the reaction,
stabilizing soon thereafter. The aluminothermic reduction of FeO appeared to
proceed rapidly and in good stoichiometric balance, based upon the mass balance
between the consumption of FeO and MnO (Delta FeO and MnO)A and the production of
Al2O3 (Al2O3).A Iron recovery from EAF slag was maximized at about 90% when 40 g of
CaO was added to 100 g slag. Furthermore, Mn could also be reduced from the EAF
slags by the metallic Al in the Al dross reductant. The solid compounds of spinel
(MgO center dot Al2O3) and MgO were precipitated from the slag during the FeO
reduction reaction, as confirmed by means of XRD analysis and thermochemical
computations. To maximize Fe recovery from EAF slag, it is crucial to control the
slag composition, namely to ensure high fluidity by suppressing the formation of
solid compounds.
C1 [Heo, Jung Ho; Park, Joo Hyun] Hanyang Univ, Dept Mat Engn, Ansan 426791, South
Korea.
South Korea.
OI Heo, Jungho/0000-0001-6674-7279
CR Das BR, 2007, MINER ENG, V20, P252, DOI 10.1016/j.mineng.2006.09.002
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2916.2004.00496.x
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Kevorkijan VM, 1999, COMPOS SCI TECHNOL, V59, P1745, DOI 10.1016/S0266-
3538(99)00034-2
5
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Manfredi O, 1997, JOM-J MIN MET MAT S, V49, P48, DOI 10.1007/s11837-997-0012-9
3
SOTO H, 1986, CONSERV RECYCLING, V9, P45, DOI 10.1016/0361-3658(86)90133-5
Takeuchi A., 1996, J JPN I LIGHT MET, V46, P592, DOI DOI 10.2464/jilm.46.592
TURKDOGAN ET, 1980, J CLEAN PROD
Ueda M, 1999, J JPN I MET, V63, P279, DOI 10.2320/jinstmet1952.63.3_279
NR 21
TC 14
Z9 15
U1 0
U2 23
PI OXFORD
SN 0364-5916
EI 1873-2984
J9 CALPHAD
PD SEP
PY 2017
VL 58
BP 229
EP 238
DI 10.1016/j.calphad.2017.02.004
PG 10
Engineering
GA FH0ZN
UT WOS:000410869300021
DA 2023-12-05
ER
PT J
AU Shi, RY
Li, JY
Ni, N
Mehmood, K
Xu, RK
Qian, W
AF Shi, Ren-yong
Li, Jiu-yu
Ni, Ni
Mehmood, Khalid
Xu, Ren-kou
Qian, Wei
TI Effects of biomass ash, bone meal, and alkaline slag applied alone and
combined on soil acidity and wheat growth
SO JOURNAL OF SOILS AND SEDIMENTS
LA English
DT Article
DE Alkaline slag; Biomass ash; Bone meal; Heavy metals; Pot experiment;
Soil acidity amelioration
ID INDUSTRIAL BY-PRODUCTS; LONG-TERM FERTILIZATION; MINERALOGICAL
IMPLICATIONS; ALUMINUM TOXICITY; ULTISOL PROFILE; SOUTHERN CHINA; CROP
RESIDUES; WOOD ASH; RED SOIL; PLANT
AB Purpose The purpose of this study is to examine the effects of combined
application of biomass ash (BA), bone meal (BM), and alkaline slag (AS) on soil
acidity, nutrient contents, uptake of the nutrients by wheat, and wheat growth.
Materials and methods A pot experiment with an Ultisol collected from Anhui
province, China, was conducted to compare the effects of BA, BM, and AS applied
alone and combined on soil acidity; soil nutrient contents; uptake of N, P, K, Ca,
and Mg by wheat, and wheat growth.
Result and discussion Application of BA, BM, and AS alone and combined increased
soil pH and decreased soil exchangeable Al3+. BA + BM + AS showed the greatest
ameliorating effect on soil acidity, and soil pH of the treatment increased by 1.24
units compared with control. Application of BA + BM + AS reduced soil exchangeable
Al3+ and increased soil exchangeable calcium and magnesium to a greater extent than
BA + BM and single application of the amendments. The BM-containing amendments
substantially increased soil available phosphorous by 66-93% compared with control.
Application of the amendments alone and combined enhanced the uptake of N, P, K,
Ca, and Mg by wheat and thus promoted wheat growth and increased yield of wheat
grains. Application of BA + BM + AS and BA + BM showed greater effects on nutrient
uptake and wheat growth than single application of the amendments. Wheat straw
weights of the two treatments were 11.1 and 10.1 times greater than that of
control. The data were 2.7, 4.8, and 5.6 times for the treatments of BA, AS, and
BM. The contents of Cd, Cr, Zn, and Cu in wheat grains were lower than standard
limits, except for the single BA treatment.
Conclusion BA + BM + AS is the best choice for amelioration of acid soils and
promotion of crop production.
C1 [Shi, Ren-yong; Li, Jiu-yu; Ni, Ni; Mehmood, Khalid; Xu, Ren-kou; Qian, Wei]
Chinese Acad Sci, Inst Soil Sci, State Key Lab Soil & Sustainable Agr, POB 821,
Nanjing, Jiangsu, Peoples R China.
[Shi, Ren-yong; Ni, Ni; Mehmood, Khalid] Univ Chinese Acad Sci, Beijing 100049,
Peoples R China.
EM rkxu@issas.ac.cn
RI Mehmood, Khalid/JKI-9220-2023
OI Mehmood, Khalid/0000-0001-7721-219X
National Key Basic Research Program of China [2014CB441003]
FX This study was supported by the National Key Research and Development of
China (No. 2016YFD0200302) and the National Key Basic Research Program
of China (No. 2014CB441003).
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10.1016/j.biortech.2010.11.018
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NR 41
TC 14
Z9 17
U1 1
U2 76
PI HEIDELBERG
SN 1439-0108
EI 1614-7480
J9 J SOIL SEDIMENT
JI J. Soils Sediments
PD AUG
PY 2017
VL 17
IS 8
BP 2116
EP 2126
DI 10.1007/s11368-017-1673-9
PG 11
WC Environmental Sciences; Soil Science
SC Environmental Sciences & Ecology; Agriculture
GA FA6VA
UT WOS:000405581200010
DA 2023-12-05
ER
PT C
AU DeLuca, LT
Maggi, F
Dossi, S
Fassina, M
Paravan, C
Sossi, A
AF DeLuca, Luigi T.
Maggi, Filippo
Dossi, Stefano
Fassina, Marco
Paravan, Christian
Sossi, Andrea
BE DeLuca, LT
Shimada, T
Sinditskii, VP
Calabro, M
TI Prospects of Aluminum Modifications as Energetic Fuels in Chemical
Rocket Propulsion
SO CHEMICAL ROCKET PROPULSION: A COMPREHENSIVE SURVEY OF ENERGETIC
MATERIALS
SE Springer Aerospace Technology
LA English
CT 12th International Workshop on Combustion and Propulsion - New Energetic
Materials for Space Exploration
CY JUN 09-10, 2014
CL Politecnico Milano, Campus Bovisa, Milan, ITALY
HO Politecnico Milano, Campus Bovisa
ID CONDENSED COMBUSTION PRODUCTS; SOLID-PROPELLANTS; BURNING SURFACE;
POCKET MODEL; AGGLOMERATION; IGNITION; TEMPERATURE; REACTIVITY;
EXPLOSION; KINETICS
AB The use of metals as high-energy fuels has been for long time a common approach
to increase performance of chemical rocket propulsion in general. This effort was
initially triggered by theoretical thermochemical considerations, but under real
operating conditions, a series of collateral and unforeseen effects occurred, with
both positive and negative consequences. After six decades, the use of micron-sized
Al is the most common practice at industrial level for solid rocket propulsion in
particular. Yet attempts are under way to mitigate some of the most deleterious
effects: notably, the two-phase flow losses and slag accumulation taking place in
gasdynamic nozzles. In this paper, a range of modified Al powders is discussed,
going from nano-sized uncoated to coated Al particles and from chemically to
mechanically activated micron-sized Al. These variants are duly characterized and
comparatively tested under laboratory burning conditions. Due to page limitations,
mainly the class of aluminized composite propellants (ammonium perchlorate/inert
binder) and operating conditions often used in space applications are investigated.
The reader is cautioned to avoid making generalizations to other formulations and
conditions based on this limited dataset. Each of the tested Al variants has its
own properties, and implementation in full-scale propulsive systems needs to be
carefully evaluated for an overall assessment. The recommended strategy for best
results is a dual mode Al mixture, synergistically exploiting each component. Other
metal fuels, especially hydrides and boron compounds, are examined as well. New
trends, capable of drastically changing the current situation but still in their
infancy as of this writing, are briefly discussed at the end of the paper.
C1 [DeLuca, Luigi T.; Maggi, Filippo; Dossi, Stefano; Fassina, Marco; Paravan,
Christian; Sossi, Andrea] Politecn Milan, Dept Aerosp Sci & Technol, Space Prop Lab
SPLab, I-20156 Milan, Italy.
C3 Polytechnic University of Milan
RP DeLuca, LT (corresponding author), Politecn Milan, Dept Aerosp Sci & Technol,
Space Prop Lab SPLab, I-20156 Milan, Italy.
EM luigi.deluca@polimi.it; filippo.maggi@polimi.it;
stefano.dossi@polimi.it; marco.fassina@polimi.it;
christian.paravan@polimi.it; andrea.sossi@mail.polimi.it
RI paravan, christian/AFK-5240-2022; Maggi, Filippo/C-7094-2008; paravan,
christian/AAG-3817-2022
OI Maggi, Filippo/0000-0001-9657-8955; DOSSI, STEFANO/0000-0003-3156-1663
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NR 90
TC 14
Z9 17
U1 1
U2 21
PU SPRINGER-VERLAG BERLIN
PI BERLIN
PA HEIDELBERGER PLATZ 3, D-14197 BERLIN, GERMANY
SN 1869-1730
EI 1869-1749
BN 978-3-319-27748-6; 978-3-319-27746-2
J9 SPRINGER AEROSP TECH
PY 2017
BP 191
EP 233
DI 10.1007/978-3-319-27748-6_8
PG 43
WC Engineering, Aerospace; Energy & Fuels
SC Engineering; Energy & Fuels
GA BH3QR
UT WOS:000399931600008
DA 2023-12-05
ER
PT J
AU Keeping, MG
Miles, N
Rutherford, RS
AF Keeping, Malcolm G.
Miles, Neil
Rutherford, R. Stuart
TI Liming an acid soil treated with diverse silicon sources: Effects on
silicon uptake by sugarcane (Saccharum spp. hybrids)
SO JOURNAL OF PLANT NUTRITION
LA English
DT Article
DE acid soils; aluminum; calcium silicate slag; lime; plant stress;
silicon; sugarcane
ID MEDIATED ALLEVIATION; WALKER LEPIDOPTERA; ALUMINUM TOXICITY; VASCULAR
PLANTS; UPLAND RICE; RESISTANCE; AVAILABILITY; SOLUBILITY; MECHANISMS;
FERTILITY
AB Highly weathered soils are typically acid, with low plant-available silicon
(Si), and may also be high in soluble aluminum (Al). We tested whether pre-liming
an acid soil prior to silicate fertilizer application improved Si uptake by
sugarcane (Saccharum spp. hybrids), feasibly through elimination of reactive Al.
Three trials with potted sugarcane were grown in an acid soil. Treatments included
11 different Si sources and 1- or 3-month pre-liming periods. Soil and plant tissue
Si content and yield were determined. Pre-liming for a 1- or 3-month period did not
increase plant Si uptake and reduced available soil Si throughout. Alkaline Si
sources produced significantly more plant-available Si and greater plant uptake
than non-alkaline sources. Silicon and lime treatments did not significantly
increase yield. We conclude that pre-liming an acid soil before Si application is
unlikely to significantly improve Si uptake by sugarcane.
C1 [Keeping, Malcolm G.; Miles, Neil; Rutherford, R. Stuart] South African
Sugarcane Res Inst, Private Bag X02, ZA-4300 Mt Edgecombe, South Africa.
[Keeping, Malcolm G.] Univ Witwatersrand, Sch Anim Plant & Environm Sci,
Johannesburg, South Africa.
[Miles, Neil] Univ KwaZulu Natal, Sch Agr Earth & Environm Sci,
Pietermaritzburg, South Africa.
[Rutherford, R. Stuart] Univ KwaZulu Natal, Sch Life Sci, Durban, South Africa.
C3 University of Witwatersrand; University of Kwazulu Natal; University of
Kwazulu Natal
RP Keeping, MG (corresponding author), South African Sugarcane Res Inst, Private
Bag X02, ZA-4300 Mt Edgecombe, South Africa.
EM malcolm.keeping@sugar.org.za
RI Keeping, Malcolm G/J-5959-2019
OI Keeping, Malcolm G/0000-0003-2992-4066
FU South African Sugarcane Research Institute; National Research Foundation
(South Africa) [77035]
FX Funding for this study was provided by the South African Sugarcane
Research Institute and the National Research Foundation (South Africa)
(grant number 77035).
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NR 81
TC 14
Z9 14
U1 0
U2 27
PI PHILADELPHIA
SN 0190-4167
EI 1532-4087
J9 J PLANT NUTR
JI J. Plant Nutr.
PY 2017
VL 40
IS 10
BP 1417
EP 1436
DI 10.1080/01904167.2016.1267751
PG 20
WC Plant Sciences
SC Plant Sciences
GA FC9BN
UT WOS:000407135900006
DA 2023-12-05
ER
PT J
AU Bernal, SA
AF Bernal, Susan A.
TI Microstructural Changes Induced by CO2 Exposure in
Alkali-Activated Slag/Metakaolin Pastes
LA English
DT Article
DE alkali-activation; blast furnace slag; metakaolin; accelerated
carbonation
ID X-RAY-DIFFRACTION; C-S-H; ACCELERATED CARBONATION; SLAG; GEOPOLYMERS;
CEMENT; MICROSCOPY; EVOLUTION; FTIR; GELS
AB The structural changes induced by accelerated carbonation in alkali-activated
slag/metakaolin (MK) cements were determined. The specimens were carbonated for 540
h in an environmental chamber with a CO2 concentration of 1.0 +/- 0.2%, a
temperature of 20 +/- 2 degrees C, and relative humidity of 65 +/- 5%. Accelerated
carbonation led to decalcification of the main binding phase of these cements,
which is an aluminum substituted calcium silicate hydrate (C-(N-)A-S-H) type gel,
and the consequent formation of calcium carbonate. The sodium-rich carbonates trona
(Na2CO3 center dot NaHCO3 center dot 2H(2)O) and gaylussite (Na2Ca(CO3)(2)center
dot 5H(2)O) were identified in cements containing up to 10 wt.% MK as carbonation
products. The formation of these carbonates is mainly associated with the chemical
reaction between the CO2 and the free alkalis present in the pore solution. The
structure of the carbonated cements is dominated by an aluminosilicate hydrate (N-
A-S-H) type gel, independent of the MK content. The N-A-S-H type gels identified
are likely to be derived both from the activation reaction of the MK, forming a
low-calcium gel product that does not seem to undergo structural changes upon CO2
exposure, and the decalcification of C-(N-) A-S-H type gel. The carbonated pastes
present a highly porous microstructure, more notable as the content of MK content
in the cement increases, which might have a negative impact on the durability of
these materials in service.
C1 [Bernal, Susan A.] Univ Sheffield, Dept Civil & Struct Engn, Sheffield, S
Yorkshire, England.
RP Bernal, SA (corresponding author), Univ Sheffield, Dept Civil & Struct Engn,
EM s.bernal@sheffield.ac.uk
RI Bernal, Susan A/E-8938-2011
FU UK Engineering and Physical Sciences Research Council [EP/M003272/1]; US
Department of Energy, Office of Science, Office of Basic Energy Sciences
[DE-AC02-06CH11357]; EPSRC [EP/M003272/1] Funding Source: UKRI;
Engineering and Physical Sciences Research Council [EP/M003272/1]
Funding Source: researchfish
FX This work was supported in part by the UK Engineering and Physical
Sciences Research Council through grant EP/M003272/1. Use of the
Advanced Photon Source at Argonne National Laboratory (ANL) was
supported by the US Department of Energy, Office of Science, Office of
Basic Energy Sciences, under Contract No. DE-AC02-06CH11357. Prof. Ruby
Mejia de Gutierrez (U. del Valle, Colombia), Prof. John Provis (U.
Sheffield, UK), and Dr. Volker Rose (ANL, USA) are greatly acknowledged
for the valuable discussions and support during the execution of this
study.
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NR 40
TC 14
Z9 14
U1 2
U2 26
PI LAUSANNE
SN 2296-8016
J9 FRONT MATER
JI Front. Mater.
PD SEP 16
PY 2016
VL 3
AR 43
DI 10.3389/fmats.2016.00043
PG 10
GA EK0VK
UT WOS:000393645000001
OA gold, Green Accepted, Green Published
DA 2023-12-05
ER
PT J
AU Ma, AH
Jia, QM
Su, HY
Zhi, YF
Tian, N
Wu, J
Shan, SY
AF Ma, AiHua
Jia, QingMing
Su, HongYing
Zhi, YunFei
Tian, Na
Wu, Jing
Shan, ShaoYun
TI Study of CO2 cyclic absorption stability of CaO-based
sorbents derived from lime mud purified by sucrose method
LA English
DT Article
DE Lime mud; Sucrose method; Cyclic capture CO2; Rejects-bauxite-tailings;
Precalcination; Doping
ID CALCIUM LOOPING PROCESS; CAPTURE PERFORMANCE; STEEL SLAG; OXIDE; WASTE;
ENHANCEMENT; CARBONATION; SORPTION
AB Using lime mud (LM) purified by sucrose method, derived from paper-making
industry, as calcium precursor, and using mineral rejects-bauxite-tailings (BTs)
from aluminum production as dopant, the CaO-based sorbents for high-temperature CO2
capture were prepared. Effects of BTs content, precalcining time, and temperature
on CO2 cyclic absorption stability were illustrated. The cyclic carbonation
behavior was investigated in a thermogravimetric analyzer (TGA). Phase composition
and morphologies were analyzed by XRD and SEM. The results reflected that the as-
synthesized CaO-based sorbent doped with 10 wt% BTs showed a superior CO2 cyclic
absorption-desorption conversion during multiple cycles, with conversion being > 38
% after 50 cycles. Occurrence of Ca12Al14O33 phase during precalcination was
probably responsible for the excellent CO2 cyclic stability.
C1 [Ma, AiHua; Jia, QingMing; Su, HongYing; Zhi, YunFei; Tian, Na; Wu, Jing; Shan,
ShaoYun] Kunming Univ Sci & Technol, Sch Chem Engn, Kunming 650093, Peoples R
China.
RP Shan, SY (corresponding author), Kunming Univ Sci & Technol, Sch Chem Engn,
Kunming 650093, Peoples R China.
EM shansy411@163.com
RI tian, na/GVR-9226-2022
FU National Natured Science Foundation of China [2014FB129, 51104075,
51364023, 31160146]
FX The National Natured Science Foundation of China (No. 2014FB129,
51104075, 51364023, and 31160146) provided financial supports for this
work.
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NR 34
TC 14
Z9 16
U1 3
U2 49
PI HEIDELBERG
SN 0944-1344
EI 1614-7499
PD FEB
PY 2016
VL 23
IS 3
BP 2530
EP 2536
DI 10.1007/s11356-015-5477-4
PG 7
GA DB2YO
UT WOS:000368376800052
PM 26423292
DA 2023-12-05
ER
PT C
AU Murthy, IN
Babu, NA
Rao, JB
AF Murthy, I. Narasimha
Babu, N. Arun
Rao, J. Babu
BE Ghosh, SK
TI High Carbon Ferro Chrome Slag - Alternative Mould Material for Foundry
Industry
SO WASTE MANAGEMENT FOR RESOURCE UTILISATION
SE Procedia Environmental Sciences
LA English
CT 5th International Conference on Solid Waste Management (IconSWM)
CY NOV 25-27, 2015
CL Bengaluru, INDIA
DE Silica sand; Fe-Cr slag; CO2 process; Mould properties; AA2024 Castings
AB High silica sand is commonly used in foundry industry for sand moulds making.
Various efforts are being made to use the industrial wastes as an alternate molding
material in foundry to conserve the natural resources; and effective utilization of
the industrial waste to sustain the industrialization. Ferro chrome (Fe-Cr) slag
has many of the same attributes of the sand. In this paper investigations were
carried out on comparative mould and casting properties of high silica sand and Fe-
Cr slag for foundry applications. A series of sand tests were carried out on silica
sand, Fe-Cr slag individually and various combinations of these two. The process
parameters considered for this investigation were % of Sodium silicate, CO2 gassing
time, and mould setting time. Two types of moulds were made with 100% Fe-Cr Slag
and 100% Silica Sand individually with 8% Sodium Silicate and 15Seconds CO2 gassing
time. AA2024 Aluminium alloy cylindrical castings were made through these two
moulds; castings were investigated for its microstructure and hardness studies.
Results reveal that standard samples with Fe-Cr slag can be prepared; these shows
smooth surface finish and accurate dimensions on par with the sand samples. The
mould permeability, compression and shear strength results showed Fe-Cr Slag will
be a suitable candidate for either partial or full replacement of molding sand.
Enhanced mould properties were observed for Fe-Cr slag than silica sand. Good
surface finish castings with enhanced mechanical properties and fine grain
microstructures were produced by Fe-Cr slag moulds. (C) 2016 The Authors. Published
by Elsevier Ltd. This is an open Access article under the CC BY-NC-ND license.
C1 [Murthy, I. Narasimha; Rao, J. Babu] Andhra Univ, Dept Met Engn, Visakhapatnam,
Andhra Pradesh, India.
[Babu, N. Arun] Khammam Inst Technol & Sci, Dept Mech Engn, Khammam, India.
C3 Andhra University
RP Rao, JB (corresponding author), Andhra Univ, Dept Met Engn, Visakhapatnam,
Andhra Pradesh, India.
EM baburaojinugu@yahoo.com
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TC 14
Z9 14
U1 0
U2 2
PI AMSTERDAM
SN 1878-0296
J9 PROCEDIA ENVIRON SCI
PY 2016
VL 35
BP 597
EP 609
DI 10.1016/j.proenv.2016.07.046
PG 13
WC Engineering, Environmental
SC Engineering
GA BG2EZ
UT WOS:000387295000062
OA gold
DA 2023-12-05
ER
PT J
AU Himpel, G
Herrmann, M
Höhn, S
AF Himpel, Gert
Herrmann, Mathias
Hoehn, Soeren
TI Comparison of the high-temperature corrosion of aluminium nitride,
alumina, magnesia and zirconia ceramics by coal ashes
LA English
DT Article
DE Corrosion; Aluminium nitride; Magnesia; Zirconia; Gasification reactor
ID GASIFICATION; REFRACTORIES
AB Higher-grade reactor lining materials are needed to withstand the higher working
temperatures and gas pressures used in gasification reactors to improve their
efficiency. Both conventional oxide materials and nonoxide materials such as SiC
and AlN are suitable refractory materials for the reducing atmospheres prevailing
in gasifiers. Interactions between the reactor lining and the slag constitute the
main corrosion mechanism. In previous investigations on the high-temperature
corrosion of aluminium nitride by coal ash [1] AlN materials were tested in basic
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compared with that of alumina, magnesia and zirconia. (C) 2015 Elsevier Ltd and
C1 [Himpel, Gert; Herrmann, Mathias; Hoehn, Soeren] IKTS, Fraunhofer Inst Ceram
Technol & Syst, D-01277 Dresden, Germany.
C3 Fraunhofer Gesellschaft
RP Herrmann, M (corresponding author), IKTS, Fraunhofer Inst Ceram Technol & Syst,
Winterbergstr 28, D-01277 Dresden, Germany.
EM Gert.Himpel@ikts.fraunhofer.de; Mathias.Herrmann@ikts.fraunhofer.de;
Soeren.Hoehn@ikts.fraunhofer.de
OI Herrmann, Mathias/0000-0003-3264-8672; Hohn, Soren/0000-0002-9738-9192
FU German Energy Raw Material Centre; German Federal Ministry of Education
and Research (BMBF); company Vattenfall Europe Mining Generation
[03IS20021D]; company RWE Power [03IS20021D]; company ROMONTA
[03IS20021D]; company MIBRAG [03IS20021D]
FX This research was conducted under the auspices of the German Energy Raw
Material Centre within the framework of the project 'Technologies for
the post-oil era'. The German Energy Raw Material Centre is promoted
mainly by the German Federal Ministry of Education and Research (BMBF)
as well as the companies Vattenfall Europe Mining & Generation, RWE
Power, ROMONTA and MIBRAG, all acting as direct network partners funding
the research project (Grant number 03IS20021D). This alliance is
strengthened by a further 14 partners providing complementary project
support.
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TC 14
Z9 14
U1 2
U2 41
PU ELSEVIER SCI LTD
PI OXFORD
SN 0272-8842
EI 1873-3956
J9 CERAM INT
JI Ceram. Int.
PD AUG
PY 2015
VL 41
IS 7
BP 8288
EP 8298
DI 10.1016/j.ceramint.2015.02.052
PG 11
GA CJ7WS
UT WOS:000355711700003
DA 2023-12-05
ER
PT J
AU Yang, D
Wang, XH
Yang, GW
Wei, PY
He, JP
AF Yang, Die
Wang, Xinhua
Yang, Guangwei
Wei, Pengyuan
He, Jinping
TI Inclusion Evolution and Estimation during Secondary Refining in Calcium
Treated Aluminum Killed Steels
LA English
DT Article
DE inclusion evolution; estimation; secondary refining; calcium treatment;
thermodynamic model
ID DISSOLUTION; DEOXIDATION; MECHANISMS; PARTICLES; BEHAVIOR; SLAGS
AB The objective of this study was to investigate the evolution of inclusions
during secondary refining in aluminum killed steels. As calcium treatment is also
used to modify solid alumina inclusions to liquid or partially liquid calcium
aluminates for keeping free from nozzle clogging, a thermodynamic model has been
calculated using Factsage to predict the type of calcium aluminates and sulfides
present in the steel. The results showed that alumina generated from deoxidation
had transformed to MgO-Al2O3 spinel with a small amount of CaO by using high
basicity and high Al2O3 slag during ladle furnace (LF) refining. Though soft
blowing after LF refining is benefit for the removal of inclusions by floatation,
vigorous stirring which may make slag layer exposing an "eye" to air reoxidation
should be avoided. After calcium treatment, the inclusions were restricted mainly
to globular calcium aluminates and the sulfur in the steel was associated with
these inclusions as calcium sulfide. The ND (number density) of inclusions seems to
appear a similar tendency to the size distribution of smaller inclusions, and the
similar change between the AF (area fraction) of inclusions and the total oxygen
content of the steel can be also found by careful comparison. Predicted inclusion
type in the steel were validated with measurement based on samples collected from
industrial heats and a reasonable range of Ca content was also given for the
experimental steel.
C1 [Yang, Die; Wang, Xinhua; Yang, Guangwei; Wei, Pengyuan] Univ Sci & Technol
[He, Jinping] WISCO, CSP Branch Strip Plant, Wuhan 430083, Peoples R China.
RP Yang, D (corresponding author), Univ Sci & Technol Beijing, Sch Met & Ecol Engn,
EM yangdie2010@gmail.com
RI Wang, Xinhua/ISR-8520-2023; Wang, Xiaoqiang/IQS-3727-2023; Wang,
Xin/AAN-8435-2021; Wang, Xin/JCE-2009-2023
OI Wang, Xin/0000-0002-4457-7376; Wang, Xin/0000-0002-4457-7376
FU National Basic Research Program of China [2010CB630806]
FX The authors gratefully express their appreciation to National Basic
Research Program of China (Grant No. 2010CB630806) for supporting this
work. Also, they thank Mr Jinping HE and Long QIAN in WISCO of China for
their great help in this work.
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U2 27
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EI 1869-344X
J9 STEEL RES INT
JI Steel Res. Int.
PD NOV
PY 2014
VL 85
IS 11
BP 1517
EP 1524
DI 10.1002/srin.201300393
PG 8
GA AT2GJ
UT WOS:000344751100004
DA 2023-12-05
ER
PT J
AU Zhang, S
Gong, XZ
Wang, Z
Cao, JW
Guo, ZC
AF Zhang, Shuang
Gong, Xuzhong
Wang, Zhi
Cao, Jianwei
Guo, Zhancheng
TI Preparation of block CaO from carbide slag and its compressive strength
improved by H3PO4
SO INTERNATIONAL JOURNAL OF MINERAL PROCESSING
LA English
DT Article
DE Carbide slag; H3PO4; Block CaO; Molding; Compressive strength
ID ALUMINUM PHOSPHATE; ACETYLENE; BENTONITE; XONOTLITE; LIME
AB The effects of H3PO4 on the compressive strength of block CaO, phase composition
and morphology of calcined carbide slag were investigated. The results indicated
that block CaO could be prepared from carbide slag through molding and calcination.
H3PO4 had a promotive effect on the compressive strength of block CaO, which
reached the maximum value at 32 MPa with a H3PO4 content of 4%. Meanwhile, the
compressive strength of block CaO increased with an increase of molding pressure.
Moreover, the P-containing phase in carbide slag shifted from hydro-phosphate to
phosphate after calcination. The close connection on the surface of particles was
enhanced by the formation of phosphate. (C) 2014 Elsevier B.V. All rights reserved.
C1 [Zhang, Shuang; Gong, Xuzhong; Wang, Zhi; Cao, Jianwei; Guo, Zhancheng] Chinese
Acad Sci, Inst Proc Engn, Natl Engn Lab Hydromet Cleaner Prod Technol, Beijing
[Guo, Zhancheng] Univ Sci & Technol Beijing, State Key Lab Adv Met, Beijing
University of Science & Technology Beijing
RP Gong, XZ (corresponding author), 1 ZhongGuanCun North Second St, Beijing 100190,
Peoples R China.
EM shuang19870602@163.com; xzgong@ipe.ac.cn
RI Guo, Z. C./AAS-1733-2021
FU National High-Technology Development Program of China (863 Project)
[2011AA06A107]
FX The authors are grateful to appreciate the financial support by the
National High-Technology Development Program of China "Calcium-based
waste multistage cycle and high value utilization technology of salt
chemical" (863 Project, project number 2011AA06A107).
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PI AMSTERDAM
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J9 INT J MINER PROCESS
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PD JUN 10
PY 2014
VL 129
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EP 11
DI 10.1016/j.minpro.2014.04.003
PG 6
GA AK7NN
UT WOS:000338615100002
DA 2023-12-05
ER
PT J
AU Wang, L
Yang, XL
Rachel, K
Wang, Y
Tong, DL
Ye, M
Jiang, X
AF Wang Lei
Yang Xing-Lun
Rachel, K.
Wang Yu
Tong De-Li
Ye Mao
Jiang Xin
TI Combined Use of Alkaline Slag and Rapeseed Cake to Ameliorate Soil
Acidity in an Acid Tea Garden Soil
SO PEDOSPHERE
LA English
DT Article
DE amelioration; amendments; lime; pH
ID ORGANIC RESIDUES; NITROGEN-CYCLE; BY-PRODUCTS; PH CHANGES;
ACIDIFICATION; ALUMINUM; ADDITIONS; WHEAT; NITRIFICATION; SATURATION
AB Rapeseed cake (RC), the residue of rapeseed oil extraction, is effective for
improving tea (Camellia sinensis) quality, especially taste and aroma, but it has
limited ability to ameliorate strongly acidic soil. In order to improve the liming
potential of RC, alkaline slag (AS), the by-product of recovery of sodium
carbonate, was incorporated. Combined effects of different levels of RC and AS on
ameliorating acidic soil from a tea garden were investigated. Laboratory
incubations showed that combined use of AS and RC was an effective method to reduce
soil exchangeable acidity and Al saturation and increase base saturation, but not
necessarily for soil pH adjustment. The release of alkalinity from the combined
amendments and the mineralization of organic nitrogen increased soil pH initially,
but then soil pH decreased due to nitrifications. Various degrees of nitrification
were correlated with the interaction of different Ca levels, pH and N contents.
When RC was applied at low levels, high Ca levels from AS repressed soil
nitrification, resulting in smaller pH fluctuations. In contrast, high AS
stimulated soil nitrification, when RC was applied at high levels, and resulted in
a large pH decrease. Based on the optimum pH for tea production and quality, high
ratios of AS to RC were indicated for soil acidity amelioration, and 8.0 g kg(-1)
and less than 2.5 g kg(-1) were indicated for AS and RC, respectively. Further,
field studies are needed to investigate the variables of combined amendments.
C1 [Wang Lei; Yang Xing-Lun; Wang Yu; Tong De-Li; Ye Mao; Jiang Xin] Chinese Acad
Sci, Inst Soil Sci, State Key Lab Soil & Sustainable Agr, Nanjing 210008, Jiangsu,
Peoples R China.
[Wang Lei] Minist Environm Protect, Nanjing Inst Environm Sci, Nanjing 210042,
[Rachel, K.] Massey Univ, Palmerston North 4474, New Zealand.
C3 Chinese Academy of Sciences; Institute of Soil Science, CAS; Massey
University
RP Jiang, X (corresponding author), Chinese Acad Sci, Inst Soil Sci, State Key Lab
EM jiangxin@issas.ac.cn
FU National Key Technology R&D Program of China [2009BADC6B02]; National
Environmental Protection Public Benefit Research Foundation of China
[2013467036]; National Natural Science Foundation of China [41030531,
40701078]
FX Supported by the National Key Technology R&D Program of China (No.
2009BADC6B02), the National Environmental Protection Public Benefit
Research Foundation of China (No. 2013467036), and the National Natural
Science Foundation of China (Nos. 41030531 and 40701078).
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Zhao W, 2007, PLANT SOIL, V297, P213, DOI 10.1007/s11104-007-9334-1
Zhao X, 2009, SOIL BIOL BIOCHEM, V41, P2584, DOI 10.1016/j.soilbio.2009.08.022
NR 36
TC 14
Z9 17
U1 8
U2 71
PU SCIENCE PRESS
PI BEIJING
SN 1002-0160
J9 PEDOSPHERE
JI Pedosphere
PD APR
PY 2013
VL 23
IS 2
BP 177
EP 184
DI 10.1016/S1002-0160(13)60005-3
PG 8
WC Soil Science
SC Agriculture
GA 111IF
UT WOS:000316514300005
DA 2023-12-05
ER
PT J
AU El-Shazly, AH
Daous, MA
AF El-Shazly, A. H.
Daous, M. A.
TI Kinetics and Performance of Phosphate Removal from Hot Industrial
Effluents Using a Continuous Flow Electrocoagulation Reactor
SO INTERNATIONAL JOURNAL OF ELECTROCHEMICAL SCIENCE
LA English
DT Article
DE Electrocoagulation; phosphate removal; flow systems; waste treatment
ID WASTE-WATER TREATMENT; FLY-ASH; AQUEOUS-SOLUTION; ADSORPTION; ALUMINUM;
COAGULATION; ELECTRODES; SLAG
AB This work investigates the reaction kinetics of phosphate removal from hot
industrial effluent streams in a continuous-recirculating electrocoagulation
reactor using monopolar aluminum electrodes. The effects of several variables on
the unit performance were also investigated. Results show that the rate of
phosphate removal follows a first order reaction kinetics and that the percent of
phosphate removal increases by increasing the solution circulation flow rate,
increasing current density, and the solution temperature while it was found to
decrease by increasing the initial phosphate ions concentration. Data generated in
this study allow for a thorough analysis of the electrocoagulation reaction
kinetics, the reaction activation energy, and the reaction rate controlling
mechanism as well as the effects of several important parameters on the reactor's
performance and the phosphate removal process economic viability.
C1 [El-Shazly, A. H.; Daous, M. A.] King Abdulaziz Univ, Fac Engn, Chem & Mat Engn
Dept, Jeddah 21413, Saudi Arabia.
C3 King Abdulaziz University
RP El-Shazly, AH (corresponding author), King Abdulaziz Univ, Fac Engn, Chem & Mat
Engn Dept, Jeddah 21413, Saudi Arabia.
EM elshazly_a@yahoo.com
RI Daous, Muhammad A/E-8107-2012
OI Daous, Muhammad A/0000-0001-9630-8779; Elshazly,
Ahmed/0000-0003-1957-1471
FU King Abdulaziz University, Jeddah, Saudi Arabia [351-135-1431]
FX This work was funded by the Deanship of Scientific Research of King
Abdulaziz University, Jeddah, Saudi Arabia under grant No.
(351-135-1431).
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NR 31
TC 14
Z9 14
U1 0
U2 16
PU ESG
PI BELGRADE
PA BORIVOJA STEVANOVICA 25-7, BELGRADE, 11000, SERBIA
SN 1452-3981
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JI Int. J. Electrochem. Sci.
PD JAN
PY 2013
VL 8
IS 1
BP 184
EP 194
PG 11
WC Electrochemistry
SC Electrochemistry
GA 112AE
UT WOS:000316562800015
DA 2023-12-05
ER
PT J
AU Wang, L
Butterly, CR
Yang, XL
Wang, Y
Herath, HMSK
Jiang, X
AF Wang, L.
Butterly, C. R.
Yang, X. L.
Wang, Y.
Herath, H. M. S. K.
Jiang, X.
TI Use of crop residues with alkaline slag to ameliorate soil acidity in an
Ultisol
SO SOIL USE AND MANAGEMENT
LA English
DT Article
DE Alkaline slag; crop residues; soil acidity amelioration
ID PH CHANGES; NITROGEN DYNAMICS; ORGANIC RESIDUES; CARBON; MINERALIZATION;
ALUMINUM; MANURE; DECOMPOSITION; TOXICITY; CATION
AB Information regarding the interaction between liming agents and crop residues on
soil acidity amelioration is limited. A laboratory incubation study was undertaken
to investigate the combined application of alkaline slag (AS, the major component
is CaO) and crop residues with different C/N ratios and ash alkalinity content.
Incorporation of amendments was effective in reducing soil exchangeable acidity and
Al saturation and increasing exchangeable base cations (P < 0.05), but the effect
of AS on soil pH adjustment was reduced when added with a high amount of residue
with a low C/N ratio. Initial increases in soil pH were attributed to the release
of alkalinity from the combined amendments and the mineralization of organic
nitrogen (N). During subsequent incubation, the soil pH decreased because of
nitrification. Crop residues with a high C/N ratio increased N immobilization and
reduced net nitrification, resulting in a slight pH decrease. Crop residues with a
low C/N ratio resulted in a sharp decrease in soil pH when applied with low levels
of AS because of stimulated soil nitrification, whereas high AS had no consistent
effect on net nitrification. Hence, compared to the control (pH = 4.21), a large
increase in soil pH occurred, especially when peanut straw was applied at 10 g/kg
(pH = 5.16). It is suggested that crop residues with high C/N ratio and also
combined with a liming agent such as AS are preferred to ameliorate soil acidity.
The liming effect of AS is likely to be negated if added in combination with
residues with high N contents.
C1 [Wang, L.; Yang, X. L.; Wang, Y.; Jiang, X.] Chinese Acad Sci, Inst Soil Sci,
State Key Lab Soil & Sustainable Agr, Nanjing 210008, Peoples R China.
[Wang, L.; Wang, Y.] Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R
China.
[Butterly, C. R.] La Trobe Univ, Dept Agr Sci, Bundoora, Vic 3086, Australia.
[Herath, H. M. S. K.] Massey Univ, New Zealand Biochar Res Ctr, Inst Nat
Resources, Palmerston North 4442, New Zealand.
[Herath, H. M. S. K.] Uva Wellassa Univ, Dept Export Agr, Fac Anim Sci & Export
Agr, Badulla 9000, Sri Lanka.
Academy of Sciences; University of Chinese Academy of Sciences, CAS; La
Trobe University; Massey University; Uva Wellassa University
RP Jiang, X (corresponding author), Chinese Acad Sci, Inst Soil Sci, State Key Lab
EM jiangxin@issas.ac.cn
RI Butterly, Clayton/E-6266-2011; Zhang, Yiyang/HZI-3668-2023
OI Butterly, Clayton/0000-0002-2576-1223;
FU Key Projects of National Research Program of China [2009BADC6B02]
FX This work was possible because of the financial support of the Key
Projects of National Research Program of China (2009BADC6B02). We thank
the two anonymous referees for their helpful comments.
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NR 33
TC 14
Z9 21
U1 2
U2 48
PU WILEY-BLACKWELL
PI HOBOKEN
SN 0266-0032
J9 SOIL USE MANAGE
JI Soil Use Manage.
PD JUN
PY 2012
VL 28
IS 2
BP 148
EP 156
DI 10.1111/j.1475-2743.2012.00396.x
PG 9
WC Soil Science
SC Agriculture
GA 960PB
UT WOS:000305399300002
DA 2023-12-05
ER
PT C
AU Muñoz, V
Martinez, AGT
AF Munoz, V.
Tomba Martinez, A. G.
BE Armas, AF
TI Thermal evolution of Al2O3-MgO-C refractories
SO 11TH INTERNATIONAL CONGRESS ON METALLURGY & MATERIALS SAM/CONAMET 2011
SE Procedia Materials Science
LA English
CT 11th International Congress on Metallurgy and Materials (SAM-CONAMET)
CY OCT 18-21, 2011
CL Rosario, ARGENTINA
DE Al2O3-MgO-C refractories; Thermal evolution; X-ray diffraction
ID GRAPHITE
AB In spite of the high cost of bauxite, Al2O3-MgO-C refractory bricks (AMC) are
widely used for steelmaking vessel working linings due to their excellent
properties: high temperature mechanical strength and high resistances to both
thermal spalling and slag corrosion.
In part, these properties stem from the thermal evolution of the phases and the
microstructure of AMC refractories, such as the transformation of the aluminum
metal (usually added as antioxidant) in Al4C3 and the formation of spinel
(MgAl2O4). In this work, the thermal evolution of the phases of three different AMC
commercial bricks used in sidewalls and bottom of steelmaking ladles between 400
and 1400 C in air was studied. The variation of the mineralogical composition was
analyzed using X-ray diffraction and the differences found between the materials
were related to their compositional and microstructural differences. With this aim,
an exhaustive characterization of the as-received refractory materials by several
analytical techniques was also carried out. (C) 2012 Published by Elsevier Ltd.
Selection and/or peer-review under responsibility of SAM/CONAMET 2011, Rosario,
Argentina.
C1 [Munoz, V.; Tomba Martinez, A. G.] Univ Nacl Mar del Plata, Fac Ingn, Inst
Invest Ciencia & Tecnol Mat INTEMA, CONICET, Mar Del Plata, Argentina.
C3 Consejo Nacional de Investigaciones Cientificas y Tecnicas (CONICET);
National University of Mar del Plata
RP Muñoz, V (corresponding author), Univ Nacl Mar del Plata, Fac Ingn, Inst Invest
Ciencia & Tecnol Mat INTEMA, CONICET, Mar Del Plata, Argentina.
EM vanesam@fi.mdp.edu.ar
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NR 16
TC 14
Z9 14
U1 0
U2 3
PI AMSTERDAM
SN 2211-8128
J9 PROC MAT SCI
PY 2012
VL 1
BP 410
EP 417
DI 10.1016/j.mspro.2012.06.055
PG 8
Engineering
GA BDQ19
UT WOS:000314406000054
OA gold
DA 2023-12-05
ER
PT J
AU Chen, C
Wang, J
Shu, D
Li, P
Xue, J
Sun, BD
AF Chen, Chong
Wang, Jun
Shu, Da
Li, Pan
Xue, Jing
Sun, Baode
TI A Novel Method to Remove Iron Impurity from Aluminum
LA English
DT Article
DE aluminum; electroslag refining; iron; purification; phase diagram
calculation
ID ALLOYS; INTERMETALLICS; TITANIUM; MN
AB A novel method for iron removal from aluminum by electroslag refining using KCl-
NaCl-Na3AlF6 flux containing P was studied. After electroslag relining, the Fe
content in commercial purity aluminum decreased from 0.48% to 0.30 mass%, and the
mechanical properties of commercial purity aluminum were improved, especially in
tensile elongation increased by 33%. XRD and TEM analysis of the sludge indicated
that the reaction between the melt and the molten slag to form Fe2P in the
electroslag refining process was the main reason for iron reduction. The
thermodynamic phase diagram calculation for Al-Fe-P system accounts for the
formation of Fe2P theoretically in the electroslag refining process.
[doi:10.2320/matertrans.M2011108]
C1 [Chen, Chong; Wang, Jun; Shu, Da; Li, Pan; Xue, Jing; Sun, Baode] Shanghai Jiao
Tong Univ, Sch Mat Sci & Engn, Shanghai 200240, Peoples R China.
C3 Shanghai Jiao Tong University
RP Wang, J (corresponding author), Shanghai Jiao Tong Univ, Sch Mat Sci & Engn,
EM chenchongsjtu@sjtu.edu.cn; junwang@sjtu.edu.cn
RI Shu, Da/I-4546-2016
OI Shu, Da/0000-0003-2563-2998
Foundation of China (Nos. 50825401 and 50821003). The authors are
grateful to the researchers in the Instrumental Analysis Center of
Shanghai Jiao Tong University for their help.
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U2 32
PI SENDAI
SN 1345-9678
EI 1347-5320
J9 MATER TRANS
JI Mater. Trans.
PD AUG
PY 2011
VL 52
IS 8
SI SI
BP 1629
EP 1633
PG 5
Engineering
GA 831EO
UT WOS:000295711700021
OA Bronze
DA 2023-12-05
ER
PT J
AU Zhang, GH
Chou, KC
AF Zhang Guo-hua
Chou Kuo-chih
TI Diffusion Coefficient of Calcium Ion in
CaO-Al2O3-SiO2 Melts
LA English
DT Article
DE Nernst-Einstein equation; diffusion coefficient; electrical
conductivity; Arrhenius law
ID TRACER DIFFUSIVITY; ELECTRICAL-CONDUCTIVITY; CAO-SIO2 MELTS;
MOLECULAR-DYNAMICS; SELF-DIFFUSION; SLAGS; 1600-DEGREES-C
AB The Nernst-Einstein equation is used to calculate the diffusion coefficient of
calcium ion in the CaO-Al2O3-SiO2 system based on the data Cif the density and
electrical conductivity. It is assumed that all the aluminium ions form tetrahedral
structure and merge with chain or ring in the case of molar concentration of CaO
higher than Al2O3. And in this. case, calcium ion is assumed to be the conclusive
charge carrier. A formula between the diffusion coefficient and concentration of
calcium ion as well as temperature is deduced, which gives an increasing function
relation between the diffusion coefficient and the concentration of calcium ions.
C1 [Zhang Guo-hua; Chou Kuo-chih] Univ Sci & Technol Beijing, Met & Ecol Engn Sch,
[Chou Kuo-chih] Shanghai Univ, Dept Mat Sci & Engn, Shanghai 200072, Peoples R
China.
C3 University of Science & Technology Beijing; Shanghai University
RP Zhang, GH (corresponding author), Univ Sci & Technol Beijing, Met & Ecol Engn
Sch, Beijing 100083, Peoples R China.
EM zgh920@126.com
RI Zhang, He/GXN-0028-2022; Zhang, Guo-Hua/AAM-7264-2021
FX Item Sponsored by National Natural Science Foundation of China
(50774004)
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NR 19
TC 14
Z9 14
U1 1
U2 18
PI BEIJING
SN 1006-706X
EI 2210-3988
PD MAR
PY 2011
VL 18
IS 3
BP 13
EP 16
DI 10.1016/S1006-706X(11)60030-7
PG 4
GA 774VQ
UT WOS:000291415300003
DA 2023-12-05
ER
PT J
AU Changizi, A
Kalkanli, A
Sevinc, N
AF Changizi, Ahmad
Kalkanli, Ali
Sevinc, Naci
TI Production of in situ aluminum-titanium diboride master alloy formed by
slag-metal reaction
LA English
DT Article
DE Master alloy; TiB(2); Grain refinement; In situ; Slag-metal reaction
ID AL; COMPOSITES; MELTS
AB Al-TiB(2) master alloys have received much attention in recent years owing to
their potential as efficient grain refiners for aluminum foundry alloys. In this
study, the process of production of master alloys was investigated to develop a low
cost method, namely, slag-metal reaction. This method can be used to fabricate Al-
TiB2 master alloy in situ from the TiO(2)-H(3)BO(3)-Na(3)AlF(6) and Al system.
Since the price of the raw materials is low and the technology is simple, the
processing technique appears to reduce the cost of the master alloy. Because of
exothermic reactions, not much energy is needed to melt materials. In this process,
Titanium diboride particles were formed in situ through the reactions of TiO(2),
H(3)BO(3) and Na(3)AlF(6). Results showed that when the aluminum melted, the
condensed TiB(2) particles that formed in situ were spherical with an average
diameter of 1 mu m. Furthermore, these TiB(2) particles were distributed uniformly
through the master alloy. (C) 2010 Elsevier B.V. All rights reserved.
C1 [Changizi, Ahmad; Kalkanli, Ali; Sevinc, Naci] Middle E Tech Univ, Dept Met &
Mat Engn, TR-06531 Ankara, Turkey.
C3 Middle East Technical University
RP Changizi, A (corresponding author), Middle E Tech Univ, Dept Met & Mat Engn, TR-
06531 Ankara, Turkey.
EM ah_chang@alumni.concordia.ca
RI kalkanli, ali/AAO-5759-2021
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Wang XM, 2005, J ALLOY COMPD, V403, P283, DOI 10.1016/j.jallcom.2005.04.204
Yue NL, 1999, COMPOS STRUCT, V47, P691, DOI 10.1016/S0263-8223(00)00037-4
Zhu H, 2007, T NONFERR METAL SOC, V17, P590, DOI 10.1016/S1003-6326(07)60139-3
NR 16
TC 14
Z9 15
U1 0
U2 13
PI LAUSANNE
SN 0925-8388
J9 J ALLOY COMPD
JI J. Alloy. Compd.
PD JAN 12
PY 2011
VL 509
IS 2
BP 237
EP 240
DI 10.1016/j.jallcom.2010.08.089
PG 4
GA 690AL
UT WOS:000284972200012
DA 2023-12-05
ER
PT J
AU Mukhopadhyay, S
AF Mukhopadhyay, S.
TI Improved sol gel spinel (MgAl2O4) coatings on
graphite for application in carbon containing high alumina castables
SO JOURNAL OF SOL-GEL SCIENCE AND TECHNOLOGY
LA English
DT Article
DE Coatings; Graphite; Refractories; Sol gel; Spinel
ID OXIDATION RESISTANCE; WATER-WETTABILITY; SURFACE; DYNAMICS; MULLITE;
OXIDE
AB An improved sol gel coating of magnesium aluminate spinel (MgAl2O4) over flaky
graphite was prepared by aluminium-sec-butoxide and magnesium nitrate. The
mechanism of evolution of an extended thin film of spinel was investigated by
Fourier transform infrared spectroscopy, differential thermal analysis, scanning
electron microscopy and energy dispersive spectral analysis. Atomic force
microscope and field emission scanning electron microscope studies were conducted
to differentiate between the topography and microstructural characteristics of as-
received and coated graphites. X-ray photoelectron spectroscopy was performed to
substantiate the elemental composition of spinel film over graphite. Oxidation
resistance and water-wettability of coated graphite were examined respectively by
thermogravimetry analysis and moisture requirement during installation of a carbon
containing refractory castable composition. Apparent porosity, bulk density and
slag corrosion resistance of those castables were better than that documented in
our previous work.
C1 Univ Calcutta, Ceram Engn Sect, Dept Chem Technol, Kolkata 700009, India.
C3 University of Calcutta
RP Mukhopadhyay, S (corresponding author), Univ Calcutta, Ceram Engn Sect, Dept
Chem Technol, 92 APC Rd, Kolkata 700009, India.
EM msunanda_cct@yahoo.co.in
CR AEGERTER MA, 1989, SOL GEL SCI TECHNOLO, P356
Ansar SA, 2010, CERAM INT, V36, P1837, DOI 10.1016/j.ceramint.2010.03.035
Banerjee A, 2009, CERAM INT, V35, P381, DOI 10.1016/j.ceramint.2007.11.009
Banerjee S., 1998, MONOLITHIC REFRACTOR, P56
Brinker CJ, 1990, SOL GEL SCI PHYS CHE, P239
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de Oliveira I.R., 2000, CERAMICA, V46, P186
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2916.1993.tb03669.x
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Moreno-Castilla C, 2000, CARBON, V38, P1995, DOI 10.1016/S0008-6223(00)00048-8
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2916.2009.03133.x
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2916.1988.tb05837.x
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X
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RAHAMAN MN, 2007, CERAMIC PROCESSING, P13
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10.1016/j.jeurceramsoc.2008.01.020
SARASWATI V, 1987, J MATER SCI, V22, P2529, DOI 10.1007/BF01082141
Schl R., 1994, PROGR INTERCALATION, P83
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Sorokina NE, 2001, INORG MATER+, V37, P360, DOI 10.1023/A:1017575710886
Ting CJ, 1999, J AM CERAM SOC, V82, P841, DOI 10.1111/j.1151-2916.1999.tb01844.x
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Zhang ZR, 2002, J AM CHEM SOC, V124, P12294, DOI 10.1021/ja0208299
ZHEN CZ, 2006, J AM CERAM SOC, V89, P3635
NR 35
TC 14
Z9 18
U1 0
U2 27
PU SPRINGER
PI DORDRECHT
SN 0928-0707
EI 1573-4846
J9 J SOL-GEL SCI TECHN
JI J. Sol-Gel Sci. Technol.
PD OCT
PY 2010
VL 56
IS 1
BP 66
EP 74
DI 10.1007/s10971-010-2275-9
PG 9
GA 651SJ
UT WOS:000281947100010
DA 2023-12-05
ER
PT J
AU Xu, KD
AF Xu Kuangdi
TI CERTAIN BASIC SUBJECTS ON CLEAN STEEL
SO ACTA METALLURGICA SINICA
LA Chinese
DT Article
DE clean steel; cleanness; total oxygen content; inclusion shape control;
ultra-low sulphur steel; ultra-low phosphorus steel
ID CLEANLINESS; FUNDAMENTALS; STEELMAKING; SLAGS
AB Clean steel is a general designation of certain types of steel with higher
cleanness upgraded gradually by steel factories with promotion of process and
equipment step by step according to the customer demands on product quality. The
requirements for cleanness of typical steel and the possible lowest level of
impurity in commercial steel since last half century were introduced. The total
oxygen content in steel is extremely important for its cleanness. Relevant theories
of changes and decreases of total oxygen content during refining and solidification
processes used by major steel factories at home and abroad were enumerated.
Decreasing the inclusion amount and controlling its shape are also key tasks for
clean steel production. The influences of deoxidization products, reoxidation of
deoxidizer as well as top slag composition and refractory materials on the
cleanness were mentioned separately, inclusion control in stainless steel series
430 and optimum stirring intensity in refining process were introduced, the theory
foundation of inclusion transformation in aluminum-killed steel treated by calcium
was briefly outlined, the metallurgical principles of ultra-low phosphorus steel
and ultra-low sulphur steel productions were emphasized, ultra-low sulphur and
sulphide shape control which are required by anti-HIC of linepipe steel was
introduced, the possible ways of removing other impurities from steel were also
discussed.
C1 [Xu Kuangdi] Chinese Acad Engn, Beijing 100088, Peoples R China.
[Xu Kuangdi] Shanghai Univ, Shanghai 200072, Peoples R China.
C3 Shanghai University
RP Xu, KD (corresponding author), Chinese Acad Engn, Beijing 100088, Peoples R
China.
Birat JP, 2001, IRONMAK STEELMAK, V28, P152, DOI 10.1179/030192301677885
Burty M, 2000, REV METALL-PARIS, V97, P775, DOI 10.1051/metal/200097060775
[崔健 Cui Jian], 2005, [中国工程科学, Engineering Science], V7, P21
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KIM DS, 2004, REV METALL, P291
KNUPPEL H, 1964, STAHL EISEN, V81, P1347
KREUTGER HW, 1972, STAHL EISEN, V92, P766
Liu Z. Z., 2000, IRON STEEL, V35, P64
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POIRIER J, 2000, REV METALL CIT, P1145
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NR 26
TC 14
Z9 35
U1 0
U2 9
PU SCIENCE PRESS
PI BEIJING
SN 0412-1961
J9 ACTA METALL SIN
JI Acta Metall. Sin.
PD MAR 11
PY 2009
VL 45
IS 3
BP 257
EP 269
PG 13
GA 432TO
UT WOS:000265157300001
DA 2023-12-05
ER
PT J
AU Dashevskii, VY
Makarova, NN
Grigorovitch, KV
Kanevskii, AG
Kashin, VI
AF Dashevskii, VY
Makarova, NN
Grigorovitch, KV
Kanevskii, AG
Kashin, VI
TI Deoxidation equilibrium of aluminum and silicon in the liquid
iron-nickel alloys
LA English
DT Article
DE deoxidation equilibrium; aluminum; silicon; iron-nickel melts;
thermodynamic analysis; experimental study
ID OXYGEN
AB Thermodynamic analysis and experiments showed the deoxidation ability of
aluminum in the iron-nickel melts to be lower than that in pure iron and nickel.
With an increase in the nickel content, the deoxidation ability of aluminum
decreases to about 50% Ni and then it rises. In pure nickel, the deoxidation
ability of aluminum is almost equal to that in pure iron. On one hand, this can be
explained by an increase in the bond strength of aluminum with this melt when the
nickel content rises (gamma(Al(Fe))degrees = 0.049, gamma(Al(Ni))degrees = 0.00022)
and, on the other hand, by a decrease in that of oxygen (gamma(O(Fe))degrees =
0.0105, gamma O(Ni)degrees = 0.357). Curves of the oxygen solubility pass through
the minimum whose location is independent of the nickel content in melt. The
minimum oxygen concentrations are reached at similar to 0.2% Al; the further
additions of aluminum result in a rise in the oxygen concentration. Experimental
and calculated results are in good agreement.
Complex deoxidation of Fe-40% Ni with aluminum and silicon has been
experimentally studied. The formation of solutions and chemical compounds between
oxides of these elements promotes the participation of silicon in the deoxidation.
The lower oxygen concentrations are reached after the combined deoxidation in
comparison with the aluminum deoxidation. However, when the aluminum content rises
in the melt at the same silicon concentration, this difference decreases; at a
certain aluminum concentration, its deoxidation power becomes equal to that of
complex action of aluminum and silicon. This occurs due to an increase in the
content of aluminum oxide in slag. When the slag is saturated with aluminum oxide
(a(Al2O3) = 1), silicon does not take part in the deoxidation.
C1 Russian Acad Sci, Baikov Inst Met & Mat Sci, Moscow 119991, Russia.
Science (IMET RAS)
RP Dashevskii, VY (corresponding author), Russian Acad Sci, Baikov Inst Met & Mat
Sci, Leninskii Prosp 49, Moscow 119991, Russia.
RI Dashevskii, Veniamin/J-9400-2013; Grigorovich, Konstantin V/A-6636-2016;
Kanevskii, Akim G./ABA-7028-2021
OI Dashevskii, Veniamin/0000-0002-0379-5094; Kanevskii, Akim
G./0000-0002-9280-9442; Grigorovich, Konstantin/0000-0002-5669-4262
CR CHIANG T, 1976, METALL TRANS B, V7, P453, DOI 10.1007/BF02652717
Dashevskii VY, 2003, ISIJ INT, V43, P1487, DOI 10.2355/isijinternational.43.1487
DASHEVSKII VY, 1997, METALL, V1, P3
FROHBERG MG, 1990, Z METALLKD, V81, P513
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KULIKOV IS, 1954, IZV AKAD SC USSR OTN, V10, P23
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1988, STEELMAKING DATA SOU, P325
NR 12
TC 14
Z9 23
U1 0
U2 8
PI TOKYO
SN 0915-1559
J9 ISIJ INT
JI ISIJ Int.
PY 2005
VL 45
IS 1
BP 8
EP 11
PG 4
GA 919HP
UT WOS:000228609300002
OA gold
DA 2023-12-05
ER
PT J
AU Satyanarayana, K
Subramaniam, K
Raghunath, AV
Ramanaiah, GV
AF Satyanarayana, K
Subramaniam, K
Raghunath, AV
Ramanaiah, GV
TI Inductively coupled plasma atomic emission spectrometric determination
of gallium, phosphorus and other oxo-anion forming elements in
geological materials
SO ANALYST
LA English
DT Article
DE gallium determination; phosphorus determination; oxo-anion forming
elements; geological materials; inductively coupled plasma atomic
emission spectrometry
ID ABSORPTION SPECTROMETRY; SOLVENT-EXTRACTION; BORON; ALUMINUM; THALLIUM;
SAMPLES; METALS
AB A simple and rapid inductively coupled plasma atomic emission spectrometric
method for the determination of Ga, P and other oxo-anion forming elements such as
Mo, V, Cr, B and W in a variety of geological materials is described. The samples
are fused with potassium hydroxide, iron carrier solution is added to act as a
coagulant for the suspended particles, and after settling, the aqueous leachate is
aspirated into the plasma for optical emission measurements. The method is accurate
and precise, offering a relative standard deviation ranging from less than 1%
(0.42% for WO3 at the 1.30% level) to 5.26% (for Cr at the 10.4 ppm level) for all
the elements studied. Interference studies were performed for the four most
sensitive lines and the most suitable analyte(s) lines selected. The method was
applied to a number of international reference standards, viz., SY-2, SY-3, MRG-1,
G-2, DR-N, SO-1, SO-2, SO-4, ASK-1, ASK-2, NIST SRMs NBS 69b, 696, 697 and 698, for
Ga and other elements except for W. For W, two international reference standards,
viz., CT-1 and GXR-4, together with some tungsten-mineralized and Nb/Ta-bearing tin
slag samples, were analysed and the results are presented. The most probable Ga
values are assigned to four international reference bauxite samples (NIST SRMs 69b,
696, 697 and 698) based on the present investigations. Further, a new set of
experimental conditions are described for the determination of P in the presence of
Cu-rich (up to 600 mu g ml(-1) in the final solution) samples, after a thorough
investigation. The method allows the determination of B down to 5 mu g g(-1), Ga,
Mo, V, Cr and W down to 10 mu g g(-1) and P down to 100 mu g g(-1) in the types of
samples mentioned above.
RP Satyanarayana, K (corresponding author), DEPT ATOM ENERGY,ATOM MINERALS DIV,CHEM
LAB,HYDERABAD 500016,ANDHRA PRADESH,INDIA.
CR [Anonymous], 1987, Inductively coupled plasmas in analytical atomic spectrometry
[Anonymous], INDUCTIVELY COUPLE 1
[Anonymous], 1987, INDUCTIVELY COUPLE 2
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BURTON JD, 1972, HDB GEOCHEMISTRY, V2
CHOWDARY GS, 1992, ATOM SPECTROSC, V6, P213
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Sandell E.B., 1959, COLORIMETRIC DETERMI
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THOMSON M, 1989, HDB INDUCTIVELY COUP
WALSH JN, 1985, ANALYST, V110, P959, DOI 10.1039/an9851000959
WELZ B, 1985, ATOMIC ABSORPTION SP
WINGE RK, 1985, INDUCTIVELY COUPLED, P20
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NR 43
TC 14
Z9 14
U1 0
U2 7
PI CAMBRIDGE
PA THOMAS GRAHAM HOUSE, SCIENCE PARK MILTON ROAD, CAMBRIDGE, CAMBS, ENGLAND
CB4 4WF
SN 0003-2654
J9 ANALYST
JI Analyst
PD JUN
PY 1996
VL 121
IS 6
BP 825
EP 830
DI 10.1039/an9962100825
PG 6
WC Chemistry, Analytical
SC Chemistry
GA UQ742
UT WOS:A1996UQ74200023
DA 2023-12-05
ER
PT J
AU Besga, G
Pinto, M
Rodriguez, M
Lopez, FA
Balcazar, N
AF Besga, G
Pinto, M
Rodriguez, M
Lopez, FA
Balcazar, N
TI Agronomic and nutritional effects of Linz-Donawitz slag application to
two pastures in Northern Spain
SO NUTRIENT CYCLING IN AGROECOSYSTEMS
LA English
DT Article
DE fertilization; heavy metals; liming; pastures; slag; soil pH
ID NEW-ZEALAND SOILS; CHEMICAL-COMPOSITION; WHITE CLOVER; LIME; ALUMINUM;
RYEGRASS; PHOSPHORUS; NITROGEN
AB Most grassland soils in western European countries are acidic in their natural
state and require a liming material to bring them to their optimum pH. A study was
conducted to determine whether Linz-Donawitz (LD) slag, a by-product of the iron
and steelmaking industry, could be used as a dolomitic agent for pastures. Six
rates of slag (0, 1, 1.5, 3, 5, and 7.5 t ha(-1)), with and without fertilizer,
were investigated for their effects on soil properties, pasture yield and botanical
composition, and herbage mineral concentrations. The three-year study was conducted
on a newly established pasture of perennial ryegrass (Lolium perenne L.), cocksfoot
(Dactylis glomerata L.), and white clover (Trifolium repens L.), and on a resident
pasture dominated by Yorkshire fog (Holcus lanatus L.) and browntop (Agrostis
tenuis Sibth.). Application of slag increased soil pH (0.15 and 0.11 units per ton
of slag applied at Derio and Abadiano, respectively) and decreased Al percentage of
the soil complex to levels not considered harmful to plant growth. Exchangeable Ca
increased markedly and exchangeable Mg slightly. In general, herbage Ca and Mg
concentrations increased accordingly to their increase in the soil, while Fe, Mn,
Cu, and Zn decreased with increasing rates of slag. LD slag appears to be a useful
liming material for correcting soil acidity in pasture soils. and for increasing Ca
and Mg, and decreasing Mn concentrations, in herbage.
RP Besga, G (corresponding author), SERV INVESTIGAC & MEJORA AGRARIA,BERREAGA
1,BIZKAIA 48160,SPAIN.
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10.1080/00288233.1983.10427024
10.1080/00288233.1985.10427001
EDMEADES DC, 1985, P WORKSH LIM NZ AGR, P65
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*IHOBE, 1994, CAL SUEL VAL IND EV, P19
JACKSON WA, 1967, SOIL ACIDITY LIMING, V12
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10.2136/sssaj1970.03615995003400020022x
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*MAFF, 1981, AN AGR MAT RB427
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*SAS I, 1988, SAS US GUID
SMILLIE GW, 1987, SOIL SCI SOC AM J, V51, P1169, DOI
10.2136/sssaj1987.03615995005100050014x
SMITH FW, 1988, PLANT ANAL INTERPRET
SYERS JK, 1985, P WORKSH LIM NZ AGR, P55
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WILLIAMS WM, 1988, CAB INT, P299
ZASOSKI RJ, 1977, COMMUN SOIL SCI PLAN, V8, P425, DOI 10.1080/00103627709366735
NR 36
TC 14
Z9 14
U1 0
U2 8
PI DORDRECHT
SN 1385-1314
J9 NUTR CYCL AGROECOSYS
JI Nutr. Cycl. Agroecosyst.
PY 1996
VL 46
IS 3
BP 157
EP 167
DI 10.1007/BF00420550
PG 11
WC Soil Science
SC Agriculture
GA WN699
UT WOS:A1996WN69900001
DA 2023-12-05
ER
PT J
AU BRAITHWAITE, RSW
KAMPF, AR
PRITCHARD, RG
LAMB, RPH
AF BRAITHWAITE, RSW
KAMPF, AR
PRITCHARD, RG
LAMB, RPH
TI THE OCCURRENCE OF THIOSULFATES AND OTHER UNSTABLE SULFUR SPECIES AS
NATURAL WEATHERING PRODUCTS OF OLD SMELTING SLAGS
SO MINERALOGY AND PETROLOGY
LA English
DT Article
AB Orthorhombic barium thiosulfate monohydrate, triclinic barium thiosulfate
fluoride, triclinic barium sulfite and monoclinic hydrated barium aluminium
trisulfide hydroxide have been isolated and identified as natural weathering
products in old smelting mill slags. None of them have been found in nature before,
but two of them are known as laboratory products. They represent a stepwise
sequence in sulfur oxidation numbers and are potential intermediates in the
familiar but little-understood oxidation of sulfides to sulfates and thus throw
light on the mechanism of the natural oxidation of sulfide ores. The nature of
these phases and co-existing species suggests formation between about Eh - 0.45 v
at pH 11 and Eh - 0.6 v at pH 13.
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NAT HIST MUSEUM LOS ANGELES,LOS ANGELES,CA 90007.
RP BRAITHWAITE, RSW (corresponding author), UNIV MANCHESTER,INST SCI & TECHNOL,DEPT
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NR 19
TC 14
Z9 14
U1 0
U2 0
PU SPRINGER-VERLAG WIEN
PI VIENNA
PA SACHSENPLATZ 4-6, PO BOX 89, A-1201 VIENNA, AUSTRIA
SN 0930-0708
J9 MINER PETROL
JI Mineral. Petrol.
PY 1993
VL 47
IS 2-4
BP 255
EP 261
PG 7
WC Geochemistry & Geophysics; Mineralogy
SC Geochemistry & Geophysics; Mineralogy
GA KV441
UT WOS:A1993KV44100009
DA 2023-12-05
ER
PT J
AU Wang, YR
Cao, YB
Zhang, ZH
Zhang, P
Ma, YW
Wang, AG
Wang, H
AF Wang, Yanru
Cao, Yubin
Zhang, Zuhua
Zhang, Peng
Ma, Yuwei
Wang, Aiguo
Wang, Hao
TI Intrinsic sulfuric acid resistance of C-(N)-A-S-H and N-A-S-H gels
produced by alkali-activation of synthetic calcium aluminosilicate
precursors
LA English
DT Article
DE Alkali-activation; Acid degradation; C-(N)-A-S-H; Durability; N-A-S-H
ID FLY-ASH; PORTLAND-CEMENT; PHASE EVOLUTION; MAS-NMR; SLAG; DURABILITY;
GEOPOLYMER; STRENGTH; AL-27; SI-29
AB This study investigates the decomposition of alkali-activated materials (AAMs)
in sulfuric acid solution. Four sodium-containing calcium aluminium-substituted
silicate hydrate (C-(N)-A-S-H) and aluminosilicate hydrate (N -A-S-H) gels with
designed Ca/Si and Si/Al ratios are produced with synthetic calcium aluminosilicate
powders. The formation of additional calcium products in Ca-rich and Al-sufficient
sample is likely helpful to retard the attack of sulfuric acid on the
C-(N)-A-S-H/N-A-S-H gels. The Si-O bond strength of N-A-S-H gel appears weaker than
that of C-(N)-A-S-H gel. The calcium in the gels prevents the leaching of silicon
from gels. The length of silicon chains in the C-(N)-A-S-H gel increases with
increased Si/Al ratio while exposure to acid solution. The chain length of the N-A-
S-H gel increases with reduced Si/Al ratio. C-(N)-A-S-H gels show a higher
resistance to leaching than N-A-S-H gel, while the latter has a high resistance to
depolymerization under acid attack. This study provides a basic route to understand
the effect of AAMs composition on acid resistance.
C1 [Wang, Yanru; Cao, Yubin; Wang, Hao] Univ Southern Queensland, Ctr Future Mat,
Toowoomba, Qld 4350, Australia.
[Zhang, Zuhua] Tongji Univ, Sch Mat Sci & Engn, Key Lab Adv Civil Engn Mat,
Minist Educ, Shanghai 201804, Peoples R China.
[Zhang, Peng] Qingdao Univ Technol, Sch Civil Engn, Qingdao 266033, Peoples R
China.
[Ma, Yuwei] Guangzhou Univ, Res Ctr Wind Engn & Engn vibrat, Guangzhou 510006,
Peoples R China.
[Wang, Aiguo] Anhui Jianzhu Univ, Anhui key Lab Adv Bldg Mat, Hefei 230022,
Peoples R China.
C3 University of Southern Queensland; Tongji University; Qingdao University
of Technology; Guangzhou University; Anhui Jianzhu University
RP Wang, H (corresponding author), Univ Southern Queensland, Ctr Future Mat,
Toowoomba, Qld 4350, Australia.; Zhang, ZH (corresponding author), Tongji Univ, Sch
Mat Sci & Engn, Key Lab Adv Civil Engn Mat, Minist Educ, Shanghai 201804, Peoples R
China.
EM drzhangzuhua@126.com; Hao.Wang@usq.edu.au
RI Wang, yanru/JAX-5241-2023; Zhang, Zuhua/AAK-5391-2020; wang,
yixuan/JGM-3893-2023
OI Zhang, Zuhua/0000-0002-7153-5120;
FU National Natural Science Foundation of China (NSFC) [U2001225, 51878263,
52278236]
FX The leadership and participation of Zuhua Zhang are supported by the
National Natural Science Foundation of China (NSFC) grants (U2001225,
51878263) . The participation of Aiguo Wang was supported by NSFC grant
(52278236) .
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10.1016/j.conbuildmat.2017.07.027
NR 66
TC 13
Z9 13
U1 25
U2 45
PI OXFORD
SN 0008-8846
EI 1873-3948
JI Cem. Concr. Res.
PD MAR
PY 2023
VL 165
AR 107068
DI 10.1016/j.cemconres.2022.107068
EA DEC 2022
PG 14
GA 7R2GB
UT WOS:000909894000001
DA 2023-12-05
ER
PT J
AU Chokkalingam, P
El -Hassan, H
El-Dieb, A
El -Mir, A
AF Chokkalingam, Ponalagappan
El -Hassan, Hilal
El-Dieb, Amr
El -Mir, Abdulkader
TI Development and characterization of ceramic waste powder-slag blended
geopolymer concrete designed using Taguchi method
LA English
DT Article
DE Ceramic waste powder (CWP); Slag; Geopolymer concrete; Performance
evaluation; Taguchi method
ID BLAST-FURNACE SLAG; HIGH-PERFORMANCE CONCRETE; ALKALI-ACTIVATED MORTARS;
PARTIAL REPLACEMENT; CEMENT MORTAR; HIGH-VOLUME; STRENGTH; DURABILITY;
WORKABILITY; TEMPERATURE
AB The ability to utilize industrial by-products in the production of cement-free
geopolymer concrete is a promising technology. However, the development,
characterization, and optimization of geopolymer concrete made with ceramic waste
powder (CWP) and ground granulated blast furnace slag (or simply slag) have not
been examined yet. This paper investigates the mechanical and durability properties
of geopolymer concrete incorporating CWP and slag. Taguchi method was employed to
design sixteen CWP-slag blended geopolymer concrete mixes. Five factors with four
levels were considered in the design, including binder content, CWP replacement
percentage by slag, alkali-activator solution to binder ratio (AAS/Binder), sodium
silicate (SS) to sodium hydroxide (SH) ratio (SS/SH), and SH solution molarity.
Results showed that geopolymer concrete properties remarkably degraded when CWP
served as the sole binding material. However, combining 40 % CWP and 60 % slag
yielded superior performance than the control mix made with 100 % slag.
Correlations between mechanical and durability properties were developed in the
form of regression models. The optimal compressive strength response (58.9 MPa) of
CWP geopolymer concrete was attained using 450 kg/m(3) of binder content, 60 % of
CWP replacement by slag, 0.5 of AAS/Binder, 1.5 of SS/SH, and 10 M of SH solution
molarity. Scanning electron microscope and energy-dispersive X-ray spectroscopy
highlighted the formation of calcium aluminum silicate hydrate and calcium silicate
hydrate gels. Experimental findings provide evidence of the ability to utilize CWP
in the production of structural grade geopolymer concrete.
C1 [Chokkalingam, Ponalagappan; El -Hassan, Hilal; El-Dieb, Amr; El -Mir,
Abdulkader] United Arab Emirates Univ, Dept Civil & Environm Engn, POB 15551, Al
Ain, U Arab Emirates.
C3 United Arab Emirates University
RP El -Hassan, H (corresponding author), United Arab Emirates Univ, Dept Civil &
EM helhassan@uaeu.ac.ae
RI El-Mir, Abdulkader/G-3306-2016
OI El-Mir, Abdulkader/0000-0003-4905-7561
FU United Arab Emirates University (UAEU) [31N453]
FX The United Arab Emirates University (UAEU) provided funding for this
work through Grant [31N453] . The UAEU lab staff and engineers?
contributions are much appreciated.
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U2 15
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD SEP 26
PY 2022
VL 349
AR 128744
DI 10.1016/j.conbuildmat.2022.128744
EA AUG 2022
PG 16
GA 4F1VC
UT WOS:000848302900003
DA 2023-12-05
ER
PT J
AU Occhicone, A
Vukcevic, M
Boskovic, I
Mingione, S
Ferone, C
AF Occhicone, Alessio
Vukcevic, Mira
Boskovic, Ivana
Mingione, Serena
Ferone, Claudio
TI Alkali-Activated Red Mud and Construction and Demolition Waste-Based
Components: Characterization and Environmental Assessment
SO MATERIALS
LA English
DT Article
DE red mud; blast-furnace slag; construction and demolition wastes;
geopolymer-based materials; pavement blocks; LCA
ID FLY-ASH; GEOPOLYMER; CEMENT; BLOCKS; IMPACT
AB The aluminum Bayer production process is the most diffused process in the world,
but it creates a high amount of basic waste material known as red mud (RM). The use
of RM as a precursor of alkali-activated materials is one of the best opportunities
for both the ecosystem and the economy. In the present work, mortar samples were
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C1 [Occhicone, Alessio; Ferone, Claudio] Univ Naples Parthenope, Ctr Direz, Dept
[Vukcevic, Mira; Boskovic, Ivana] Univ Montenegro, Fac Met & Technol, Dzordza
Vasingtona Bb, Podgorica 81000, Montenegro.
[Mingione, Serena] Empa Swiss Fed Labs Mat Sci & Technol, Lab Concrete & Asphalt
Chem, CH-8600 Dubendorf, Switzerland.
C3 Parthenope University Naples; University of Montenegro; Swiss Federal
Institutes of Technology Domain; Swiss Federal Laboratories for
Materials Science & Technology (EMPA)
RP Occhicone, A (corresponding author), Univ Naples Parthenope, Ctr Direz, Dept
EM alessio.occhicone001@studenti.uniparthenope.it; mirav@ucg.ac.me;
ivabo@ac.me; serena.mingione@empa.ch; claudio.ferone@uniparthenope.it
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OI Occhicone, Alessio/0000-0002-3652-4987; Ferone,
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NR 34
TC 13
Z9 13
U1 6
U2 23
PU MDPI
PI BASEL
EI 1996-1944
J9 MATERIALS
JI Materials
PD FEB
PY 2022
VL 15
IS 4
AR 1617
DI 10.3390/ma15041617
PG 14
Physics
GA ZT4HF
UT WOS:000769118400001
PM 35208157
DA 2023-12-05
ER
PT J
AU Pang, L
Liu, ZG
Wang, DQ
An, MZ
AF Pang, Lang
Liu, Zhenguo
Wang, Dengquan
An, Mingzhe
TI Review on the Application of Supplementary Cementitious Materials in
Self-Compacting Concrete
SO CRYSTALS
LA English
DT Article
DE self-compacting concrete; supplementary cementitious materials;
hydration mechanisms; microstructure; fresh properties
ID BLAST-FURNACE SLAG; CONFORMING FLY-ASH; SILICA FUME; LIMESTONE POWDER;
COMPRESSIVE STRENGTH; MIX DESIGN; ELECTRICAL-RESISTIVITY; PERFORMANCE
EVALUATION; DURABILITY PROPERTIES; MECHANICAL-PROPERTIES
AB For the sustainable development of construction materials, supplementary
cementitious materials (SCMs) are commonly added to self-compacting concrete (SCC).
This paper reviewed the application techniques and hydration mechanisms of SCMs in
SCC. The impacts of SCMs on the microstructure and performance of SCC were also
discussed. SCMs are used as a powder material to produce SCC by replacing 10% to
50% of cement. Hydration mechanisms include the pozzolanic reaction, alkaline
activation, and adsorption effect. Moreover, the filling effect and dilution effect
of some SCMs can refine the pore structure and decrease the temperature rise of
concrete, respectively. Specifically, the spherical particles of fly ash can
improve the fluidity of SCC, and the aluminum-containing mineral phase can enhance
the resistance to chloride ion penetration. Silica fume will increase the water
demand of the paste and promote its strength development (a replacement of 10%
results in a 20% increase at 28 days). Ground-granulated blast furnace slag may
reduce the early strength of SCC. The adsorption of Ca2+ by CaCO3 in limestone
powder can accelerate the hydration of cement and promote its strength development.
C1 [Pang, Lang; An, Mingzhe] Beijing Jiaotong Univ, Sch Civil Engn, Beijing 100044,
Peoples R China.
[Liu, Zhenguo] Beijing Urban Construct Grp, Beijing 100023, Peoples R China.
[Wang, Dengquan] Tsinghua Univ, Dept Civil Engn, Beijing 100084, Peoples R
China.
C3 Beijing Jiaotong University; Tsinghua University
RP Wang, DQ (corresponding author), Tsinghua Univ, Dept Civil Engn, Beijing 100084,
Peoples R China.
EM 20121088@bjtu.edu.cn; liuzhenguothu@163.com;
wangdq16@mails.tsinghua.edu.cn; mzhan@bjtu.edu.cn
RI Liu, Zhen/IAQ-0136-2023; ZHAO, S/IWV-4219-2023
FX FundingThis work was funded by Natural Science Foundation of China [No.
51478248].
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NR 92
TC 13
Z9 13
U1 5
U2 22
PU MDPI
PI BASEL
EI 2073-4352
J9 CRYSTALS
JI Crystals
PD FEB
PY 2022
VL 12
IS 2
AR 180
DI 10.3390/cryst12020180
PG 14
WC Crystallography; Materials Science, Multidisciplinary
SC Crystallography; Materials Science
GA ZK0MF
UT WOS:000762690900001
OA gold
DA 2023-12-05
ER
PT J
AU Matos, AM
Sousa-Coutinho, J
AF Matos, Ana Mafalda
Sousa-Coutinho, Joana
TI Municipal solid waste incineration bottom ash recycling in concrete:
Preliminary approach with Oporto wastes
LA English
DT Article
DE Municipal solid waste incineration bottom ash; (MIBA); Cement materials;
Supplementary cementitious materials (SCM); Waste recycling; Circular
construction
ID GLASS POWDER; CORK WASTE; FLY-ASH; CEMENT; MORTAR; DURABILITY; STRENGTH;
CARBONATION; SLAG
AB The present research explored the feasibility of using dry finely ground bottom
ash (GBA) from municipal solid waste incineration as SCM for concrete mixtures in
cooperation with a local waste management company, LIPOR. A first study was
performed using GBA as a sole partial replacement for Portland cement in paste and
mortar specimens. GBA showed both beneficial and detrimental effects on
paste/mortar mixtures. In terms of fresh properties, water demand on paste and
workability on mortar containing GBA as cement replacement kept the same as
reference specimens paste/mortars. Setting time was not affected by GBA
incorporation, and ASR expansion was mitigated. The disadvantageous effect, namely,
mechanical strength loss on GBA mortar, was mainly due to metallic aluminium, found
on the main oxide composition and SEM of GBA, which is associated with hydrogen gas
evolution. Thus, the amount of aluminium content remaining in MIBA should be
analysed even after the ageing process.
C1 [Matos, Ana Mafalda] Univ Porto, Fac Engn, CONSTRUCT, Porto, Portugal.
[Sousa-Coutinho, Joana] FEUP DEC, Rua Dr Roberto Frias, P-4200465 Porto,
Portugal.
C3 Universidade do Porto; Universidade do Porto
RP Matos, AM (corresponding author), Univ Porto, Fac Engn, CONSTRUCT, Porto,
Portugal.
EM ana.matos@fe.up.pt
RI Matos, Ana Mafalda/AAX-5720-2020
OI Matos, Ana Mafalda/0000-0002-1646-4665
FU CONSTRUCT-Instituto de I&D em Estruturas e Construcoes - FCT/MCTES
(PIDDAC) [UIDB/04708/2020, UIDP/04708/2020]
FX This work was financially supported by: Base Funding-UIDB/04708/2020 and
Programmatic Funding-UIDP/04708/2020 of the CONSTRUCT-Instituto de I&D
em Estruturas e Construcoes-funded by national funds through the
FCT/MCTES (PIDDAC) . Collaboration and materials supply by LIPOR and
Secil is gratefully acknowledged. The authors would also like to thank
Engineer Ana Cunha for collaboration on experiments, as well as the
support of LEMC.
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NR 51
TC 13
Z9 13
U1 5
U2 31
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD MAR 14
PY 2022
VL 323
AR 126548
DI 10.1016/j.conbuildmat.2022.126548
EA JAN 2022
PG 15
GA YT0EV
UT WOS:000751043700003
DA 2023-12-05
ER
PT J
AU Kiatpachai, P
Kaewkamrop, T
Mesgarpour, M
Ahn, HS
Dalkiliç, AS
Mahian, O
Wongwises, S
AF Kiatpachai, Parinya
Kaewkamrop, Thawatchai
Mesgarpour, Mehrdad
Ahn, Ho Seon
Dalkilic, Ahmet Selim
Mahian, Omid
Wongwises, Somchai
TI Air-side performance of embedded and welded spiral fin and tube heat
exchangers
SO CASE STUDIES IN THERMAL ENGINEERING
LA English
DT Article
DE Heat transfer; Energy; Finned tube; Heat exchanger; Spiral fin-and-tube
heat exchangers
ID PITCHES
AB This paper presents the air-side performance (ASP) of embedded and welded spiral
fin and tube heat exchangers (SFTHXs). Six heat exchangers were tested to
investigate the effects of fin-base connections and fin pitch. Test sections were
fabricated from steel tubes, with two rows of tubing and a Z-shaped water flow
arrangement, and an aluminum fin with various fin pitches. The experiment was done
at a high Reynolds number of air flow (4000-18000). The results show that fin pitch
had no effect on the ASP of embedded SFTHXs. In contrast, fin pitch influenced the
ASP of the welded SFTHX. Moreover, the pressure drop decreased with increasing fin
pitch, whereas the friction factor was lower for a smaller fin pitch. Due to better
fin base connections, an embedded spiral fin generally provided a higher heat
transfer rate than a welded spiral fin did. The pressure drop of the welded spiral
fin was greater than that of the embedded spiral fin, possibly because the welded
spiral fin had melted slag at the fin base.
C1 [Kiatpachai, Parinya] Chulachomklao Royal Mil Acad, Acad Div, Dept Mech Engn,
Nakhon 26001, Nayok, Thailand.
[Kiatpachai, Parinya; Kaewkamrop, Thawatchai; Mesgarpour, Mehrdad; Wongwises,
Somchai] King Mongkuts Univ Technol Thonburi KMUTT, Dept Mech Engn, Fluid Mech
Thermal Engn & Multiphase Flow Res Lab, Bangkok 10140, Thailand.
[Ahn, Ho Seon] Incheon Natl Univ, Dept Mech Engn, Incheon, South Korea.
[Dalkilic, Ahmet Selim] Yildiz Tech Univ, Dept Mech Engn, Istanbul, Turkey.
[Mahian, Omid] Xi An Jiao Tong Univ, Sch Chem Engn & Technol, Xian, Peoples R
China.
[Mahian, Omid] Ferdowsi Univ Mashhad, Ctr Nanotechnol Renewable Energies, Dept
Mech Engn, Mashhad, Razavi Khorasan, Iran.
[Wongwises, Somchai] Natl Sci & Technol Dev Agcy NSTDA, Pathum Thani 12120,
Thailand.
C3 King Mongkuts University of Technology Thonburi; Incheon National
University; Yildiz Technical University; Xi'an Jiaotong University;
Ferdowsi University Mashhad; National Science & Technology Development
Agency - Thailand
RP Wongwises, S (corresponding author), King Mongkuts Univ Technol Thonburi KMUTT,
Dept Mech Engn, Fluid Mech Thermal Engn & Multiphase Flow Res Lab, Bangkok 10140,
Thailand.
EM somchai.won@kmutt.ac.th
RI Dalkilic, Ahmet Selim/AHD-6377-2022; Dalkılıç, Ahmet Selim/G-2274-2011
OI Dalkilic, Ahmet Selim/0000-0002-5743-3937; Dalkılıç, Ahmet
Selim/0000-0002-5743-3937; Ahn, Ho Seon/0000-0002-1036-3038
FU "Research Chair Grant" National Science and Technology Development
Agency (NSTDA), Thailand; Thailand Science Research and Innovation
(TSRI), Thailand under Fundamental Fund 2022 (Project: Advanced
Materials and Manufacturing for Applications in New S-curve Industries)
FX The work was supported by the "Research Chair Grant" National Science
and Technology Development Agency (NSTDA), Thailand and the Thailand
Science Research and Innovation (TSRI), Thailand under Fundamental Fund
2022 (Project: Advanced Materials and Manufacturing for Applications in
New S-curve Industries).
CR ANSI, 2000, 332000 ANSI ASHRAE
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PI AMSTERDAM
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J9 CASE STUD THERM ENG
JI Case Stud. Therm. Eng.
PD FEB
PY 2022
VL 30
AR 101721
DI 10.1016/j.csite.2021.101721
EA JAN 2022
PG 11
WC Thermodynamics
SC Thermodynamics
GA 0X8BD
UT WOS:000789924100005
OA gold
DA 2023-12-05
ER
PT J
AU Coetsee, T
De Bruin, F
AF Coetsee, Theresa
De Bruin, Frederik
TI Reactions at the molten flux-weld pool interface in submerged arc
welding
SO HIGH TEMPERATURE MATERIALS AND PROCESSES
LA English
DT Article
DE oxygen; chromium; aluminium; powder; flux
ID SLAG-METAL REACTIONS; EQUILIBRIUM; CHEMISTRY; TI
AB In submerged arc welding (SAW) of chromium (Cr) containing steels, Cr is usually
added to the weld metal from the weld wire, and not from the welding flux.
Manufacturing of weld wires of specific compositions is expensive and time
consuming and cannot closely match all the desired alloy compositions. Therefore,
the weld wire chemistry is usually over matched to the base plate composition.
Better matching between the weld metal and base plate is possible if the weld metal
incorporates Cr from Cr containing metal powder, instead of sourcing Cr from weld
wire of limited Cr content. Because Cr is easily oxidised, the oxygen partial
pressure in SAW must be controlled. This work illustrates the control of the oxygen
potential at the molten flux-weld pool interface by using aluminium (Al) powder
addition. The controlled oxygen potential at the molten flux-weld pool interface
ensures increased Cr powder transfer into the weld pool, without interfering with
oxygen transfer from the plasma arc to the weld pool. The objective of this work is
to use targeted powder additions to better control Cr reactions in SAW to improve
Cr metal transfer to the weld metal and maintain an acceptable level of oxygen in
the weld metal.
C1 [Coetsee, Theresa; De Bruin, Frederik] Univ Pretoria, Dept Mat Sci & Met Engn,
ZA-0002 Pretoria, South Africa.
RP Coetsee, T (corresponding author), Univ Pretoria, Dept Mat Sci & Met Engn, ZA-
0002 Pretoria, South Africa.
EM theresa.coetsee@up.ac.za
RI De Bruin, Frederik Johannes/IZE-6573-2023
OI De Bruin, Frederik Johannes/0000-0001-7102-7508; Coetsee,
Theresa/0000-0003-2028-5755
FU National Research Foundation of South Africa [BRICS171211293679]
FX This work is funded in part by the National Research Foundation of South
Africa (BRICS171211293679).
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U1 1
U2 7
PU WALTER DE GRUYTER GMBH
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PA GENTHINER STRASSE 13, D-10785 BERLIN, GERMANY
SN 0334-6455
EI 2191-0324
J9 HIGH TEMP MAT PR-ISR
JI High Temp. Mater. Process.
PD DEC 31
PY 2021
VL 40
IS 1
BP 421
EP 427
DI 10.1515/htmp-2021-0051
PG 7
GA YC3JN
UT WOS:000739591400001
OA gold
DA 2023-12-05
ER
PT J
AU Königsberger, M
Zelaya-Lainez, L
Lahayne, O
Pichler, BLA
Hellmich, C
AF Konigsberger, Markus
Zelaya-Lainez, Luis
Lahayne, Olaf
Pichler, Bernhard L. A.
Hellmich, Christian
TI Nanoindentation-probed Oliver-Pharr half-spaces in alkali-activated
slag-fly ash pastes: Multimethod identification of microelasticity and
hardness
SO MECHANICS OF ADVANCED MATERIALS AND STRUCTURES
LA English
DT Article
DE Alkali-activated materials; microscopy; image analysis; ultrasonic
testing; micromechanics; nanoindentation
ID CHEMO-MECHANICAL PROPERTIES; MICROMECHANICAL PROPERTIES; CEMENT PASTE;
SURFACE-ROUGHNESS; CREEP-PROPERTIES; ELASTIC CONTACT; MODULUS; PHASES;
BONE; LOAD
AB The mechanical interactions of C-(N-)A-S-H (Calcium-sodium-aluminum-silicate-
hydrate) gel with slag and fly ash inclusions in alkali-activated materials (AAM)
are quantified through image-supported grid nanoindentation. Nonuniform
distributions of indent-specific indentation properties reveal that the elasticity-
related domain is up to 130 times the contact indentation depth, while the
hardness-related domain, in turn, is by a factor of two to three smaller. These
rather large domains are consistent with the slag/fly-ash inclusions being much
stiffer and harder than the surrounding C-(N-)A-S-H gel. Corresponding Hashin-
Shtirkman bounds for the overall AAM stiffness consistently frame ultrasonic data
characterizing this homogenized material scale. This confirms our new testing
protocol.
C1 [Konigsberger, Markus; Zelaya-Lainez, Luis; Lahayne, Olaf; Pichler, Bernhard L.
A.; Hellmich, Christian] TU Wien, Inst Mech Mat & Struct, A-1040 Vienna, Austria.
[Konigsberger, Markus] Univ Libre Bruxelles, Brussels, Belgium.
C3 Technische Universitat Wien; Universite Libre de Bruxelles
RP Hellmich, C (corresponding author), TU Wien, Inst Mech Mat & Struct, A-1040
Vienna, Austria.
EM christian.hellmich@tuwien.ac.at
OI Lahayne, Olaf/0000-0002-5252-1356; Zelaya-Lainez,
Luis/0000-0003-3298-9792
FU Belgian National Funds for Scientific Research (FNRS)
FX The first author gratefully acknowledges financial support from the
Belgian National Funds for Scientific Research (FNRS).
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NR 47
TC 13
Z9 13
U1 1
U2 5
PI PHILADELPHIA
SN 1537-6494
EI 1537-6532
J9 MECH ADV MATER STRUC
JI Mech. Adv. Mater. Struct.
PD OCT 26
PY 2022
VL 29
IS 26
BP 4878
EP 4889
DI 10.1080/15376494.2021.1941450
EA JUN 2021
PG 12
WC Materials Science, Multidisciplinary; Mechanics; Materials Science,
Characterization & Testing; Materials Science, Composites
SC Materials Science; Mechanics
GA 6T2SQ
UT WOS:000675723100001
DA 2023-12-05
ER
PT J
AU Ma, ZH
Liao, HQ
Wang, L
Cheng, FQ
AF Ma, Zhuohui
Liao, Hongqiang
Wang, Li
Cheng, Fangqin
TI Effects of iron/silicon/magnesium/aluminum on CaO carbonation of
CO2 in steel slag-based building materials during carbonation
curing
LA English
DT Article
DE Carbonation curing; CO2 sequestration; CaO; Metal oxide; Non-metal
oxide; Steel slag
ID CALCIUM-CARBONATE; ACCELERATED CARBONATION; MINERAL CARBONATION;
STEELMAKING SLAG; CARBIDE SLAG; FLY-ASH; DIOXIDE SEQUESTRATION; AQUEOUS
CARBONATION; S-H; CAPTURE
AB Carbonation curing can enhance the mechanical properties of steel slag-based
building materials and consume large amounts of CO2, making it a widely process.
Due to the complexity of steel slag, in addition to CaO, other concomitant
metallic/nonmetallic elements, such as Fe, Si, Mg and Al also have a certain
influence on carbonation reaction. In this study, Fe2O3, Fe3O4, SiO2, MgO and Al2O3
was added to CaO to form a binary system according to the chemical composition of
real steel slag. The influences of these oxides on the carbonation rate and CaO
carbonation efficiency were investigated, respectively. The results showed that
compared with pure CaO, the rates of carbonation reaction of CaO + Fe2O3, CaO +
Fe3O4, CaO + SiO2, CaO + MgO and CaO + Al(2)O3 were increased by 5.5%, 13.2%,
13.2%, 6.9% and 8.5%, respectively. The carbonation efficiency of CaO in CaO +
Fe2O3, CaO + Fe3O4, CaO + MgO, CaO + Al2O3 increased by 3.6%, 4.3%, 10.1%, and
1.2%, respectively. Synergistic effect was recognized between CaO and Fe2O3, Fe-3
O-4, MgO and Al2O3, respectively. The carbonation efficiency of CaO in CaO + SiO2
decreased by 2.4%. One reason should be the carbonation products, which exhibited
ectopic dispersion and covered the surfaces of Fe2O3, Fe3O4, MgO and Al2O3, which
effectively helped to avoid in-situ aggregation and thus covered the surfaces of
the CaO particles. This improved the carbonation reaction rate and efficiency.
Another reason could be the alkaline oxides, such as Fe2O3, Fe3O4 and MgO, and
amphoteric oxides, such as Al2O3, stimulated the carbonation reaction of CaO and
CO2, while acid oxides, such as SiO2, inhibited the carbonation reaction. (C) 2021
C1 [Ma, Zhuohui; Liao, Hongqiang; Wang, Li; Cheng, Fangqin] Shanxi Univ, State
Environm Protect Key Lab Efficient Utilizat, Engn Res Ctr CO2 Emiss Reduct &
Resource Utilizat, Minist Educ China,Inst Resources & Environm Engn, Taiyuan
C3 Ministry of Education, China; Shanxi University
RP Liao, HQ (corresponding author), Shanxi Univ, State Environm Protect Key Lab
Efficient Utilizat, Engn Res Ctr CO2 Emiss Reduct & Resource Utilizat, Minist Educ
China,Inst Resources & Environm Engn, Taiyuan 030006, Peoples R China.
EM liaohq@sxu.edu.cn
OI Wang, Li/0000-0002-0412-2617
FU Major Scientific and Technological Innovation Project of Shandong
Province [2019JZZY020306]
FX This work was financially supported by the Major Scientific and
Technological Innovation Project of Shandong Province (No.
2019JZZY020306).
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Z9 13
U1 11
U2 59
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD SEP 6
PY 2021
VL 298
AR 123889
DI 10.1016/j.conbuildmat.2021.123889
EA JUN 2021
PG 12
GA UB7IC
UT WOS:000686014300009
DA 2023-12-05
ER
PT J
AU Bao, SX
Qin, L
Zhang, YM
Luo, YP
Huang, XL
AF Bao, Shenxu
Qin, Lei
Zhang, Yimin
Luo, Yongpeng
Huang, Xiulin
TI A combined calcination method for activating mixed shale residue and red
mud for preparation of geopolymer
LA English
DT Article
DE Shale residue; Red mud; Separated calcination; Combined calcination;
Geopolymer; Compressive strength
ID F FLY-ASH; COMPRESSIVE STRENGTH; MICROSTRUCTURE; TEMPERATURE;
METAKAOLIN; VANADIUM; TECHNOLOGY; MORTAR; SLAG
AB High alkaline-containing red mud (RM) and shale residue (SR) were mixed and
calcined (i.e. combined calcination, CC) to boost SR reactivity. The CC samples
were used to prepare SR/RM-based geopolymers under various alkaline solutions and
curing temperatures, and the obtained geopolymers were compared with those prepared
by SR and RM calcined separately (i.e. separated calcination, SC). The results
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under 20 degrees C and 60 degrees C curing. The greater destruction degree of
quartz that mainly supplied by SR and the decomposition of more cancrinite in RM
occurred in the CC samples, which can be proved by the alkaline leaching tests that
more silicon and aluminum substances were dissolved for CC sample compared to that
of SC sample. Consequently, the polymerization of calcium with active silicon and
aluminum was enhanced in the samples prepared by CC, leading to the denser
microstructure and higher compressive strength. These results indicate that the
high alkali containing RM can effectively improve the reactivity of SR for the
preparation of geopolymers. (c) 2021 Elsevier Ltd. All rights reserved.
C1 [Bao, Shenxu; Qin, Lei; Zhang, Yimin; Luo, Yongpeng] Wuhan Univ Technol, Sch
Resources & Environm Engn, Wuhan 430070, Peoples R China.
[Bao, Shenxu; Zhang, Yimin] Hubei Key Lab Mineral Resources Proc & Environm,
[Zhang, Yimin] Wuhan Univ Sci & Technol, State Environm Protect Key Lab Mineral
Met Resour, Wuhan 430081, Peoples R China.
[Huang, Xiulin] Hubei Univ, Sch Mat Sci & Engn, Wuhan 430062, Peoples R China.
C3 Wuhan University of Technology; Wuhan University of Science &
Technology; Hubei University
RP Bao, SX (corresponding author), Wuhan Univ Technol, Sch Resources & Environm
Engn, Wuhan 430070, Peoples R China.
EM sxbao@whut.edu.cn
OI Bao, Shenxu/0000-0003-1295-3389
FU Major Technical Innovation Project of Hubei Province [2018ACA157]
FX The Major Technical Innovation Project of Hubei Province (2018ACA157)
funded this work.
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Yang ZT, 2019, CONSTR BUILD MATER, V221, P308, DOI
10.1016/j.conbuildmat.2019.06.034
Zhang M, 2018, CEMENT CONCRETE COMP, V93, P175, DOI
10.1016/j.cemconcomp.2018.07.008
NR 41
TC 13
Z9 14
U1 4
U2 30
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD AUG 23
PY 2021
VL 297
AR 123789
DI 10.1016/j.conbuildmat.2021.123789
EA JUN 2021
PG 8
GA WG1UT
UT WOS:000706784100031
DA 2023-12-05
ER
PT J
AU Zheng, XY
Wu, J
AF Zheng, Xiyao
Wu, Jun
TI Early Strength Development of Soft Clay Stabilized by One-Part Ground
Granulated Blast Furnace Slag and Fly Ash-Based Geopolymer
LA English
DT Article
DE one-part geopolymer; ground granulated blast furnace slag; fly ash;
microstructure; hydration
ID EXPERIMENTAL FEASIBILITY; ENGINEERING BEHAVIOR; CEMENT; RESISTANCE;
AGGREGATE; CONCRETE; HEAT
AB One-part or "just add water" geopolymer is a cementitious material, which is
friendly to environment and users in applications. However, the mechanical behavior
of the soft soil stabilized by one-part geopolymer is not well acknowledged. In
this study, soft clay was stabilized with ground granulated blast furnace slag
(GGBFS) and fly ash (FA)-based geopolymer, which is a mixture of solid
aluminosilicate precursor (Al-Si raw materials: GGBFS and FA), solid alkali
activator, and water. The objective was to adopt one-part geopolymer as an
alternative soil binder to completely replace ordinary Portland cement (OPC) for
stabilizing the soft clay and evaluate the effect of the factors (i.e., GBFS/FA
ratio in Al-Si precursor, activator/Al-Si precursor ratio, and water/binder ratio)
that influenced the early strength. Results showed that the increase of the FA
content in the Al-Si precursor increased the unconfined compressive strength (UCS)
values significantly through the geopolymerization process. The highest UCS values
were achieved with 90% GGBFS to 10% FA in the precursor when the
activator/precursor and water/binder ratio is 0.15 and 0.7, respectively. The UCS
values of geopolymer-stabilized clay could reach 1.5 MPa at 14 days at ambient
temperature, which is much higher than that of OPC-stabilized clay. The
microstructure and mineralogy analyses indicated that the prolific hydration
products, such as calcium silicate hydrate (C-S-H), calcium aluminum hydrate (C-A-
H), and calcium aluminum silicate hydrate (C-A-S-H), contributed greatly to
strengthen the soft clay by forming the soil skeleton and infilling among clay
particles, while sodium aluminosilicate (N-A-S-H) gel is only served to fill the
part of porosities in the soil and cannot effectively enhance the UCS of the one-
part geopolymer-stabilized soft clay. This paper results suggested that one-part
GGBFS-FA-based geopolymers have the potential to replace OPC in the manufacture of
stabilized soft clay.
C1 [Zheng, Xiyao; Wu, Jun] Shanghai Univ Engn Sci, Sch Urban Railway Transportat,
Shanghai, Peoples R China.
C3 Shanghai University of Engineering Science
RP Wu, J (corresponding author), Shanghai Univ Engn Sci, Sch Urban Railway
Transportat, Shanghai, Peoples R China.
EM cvewujun@163.com
RI Wu, Jun/CAG-4971-2022
FU National Natural Science Foundation [52078288]
FX Grateful acknowledgment is made to the National Natural Science
Foundation (no. 52078288) to support this project. The assistance of Mr.
Xiao Xin from the Yancheng Institute of Technology for conducting the
SEM and EDS analysis is appreciated.
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NR 36
TC 13
Z9 13
U1 11
U2 50
PI LAUSANNE
SN 2296-8016
J9 FRONT MATER
JI Front. Mater.
PD APR 16
PY 2021
VL 8
AR 616430
DI 10.3389/fmats.2021.616430
PG 15
GA RV8AV
UT WOS:000646050500001
OA gold
DA 2023-12-05
ER
PT J
AU Scott, ISPC
Penn, CJ
AF Scott, Isis S. P. C.
Penn, Chad J.
TI Estimating the variability of steel slag properties and their influence
in phosphorus removal ability
SO CHEMOSPHERE
LA English
DT Article
DE Phosphorus; Phosphorus sorption materials; Steel slag; Phosphorus
removal capacity
ID EUTROPHICATION; PRECIPITATION; PERFORMANCE; WATERS; OXIDES; MODEL
AB Steel slag has been proven to be an effective phosphorus (P) removal media, and
a potential aid to mitigate point and nonpoint P pollution in freshwater systems.
However, the behavior of steel slag as a P sorption material (PSM) is often
oversimplified through the generalization of its chemical and physical properties,
preventing proper design of P removal structures. In this work, we tested eighteen
steel slag samples from different batches, production processes, and steel-making
plants, for the purpose of relating slag origin and chemical and physical
properties to P removal ability, under two different flow regimes. Slag samples
were also coated with aluminum (Al) and tested for P removal. Characterization
included elemental composition, particle density, buffer capacity, and P removal
ability. There was great variability in the evaluated properties across slag
sources and origin, compelling the individual characterization of steel slag
samples, since their intrinsic characteristics were key variables in determining
their potential P removal capacity. Specifically, electrical conductivity (EC),
bulk density, particle density and magnesium (Mg) content could explain around 70%
of the variability of P removal by uncoated steel slags. Increasing residence time
(RT) always increased P removal for uncoated slags. Steel slags showed a high
variability in their P removal ability, but such variability was considerably
decreased by coating the slags with Al. Additionally, the Al-coating process
significantly improved P removal performance under more rapid flows (lower RT). (C)
C1 [Scott, Isis S. P. C.] Univ Maryland, Dept Environm Sci & Technol, College Pk,
MD 20742 USA.
[Penn, Chad J.] Natl Soil Eros Res Lab ARS USDA, 275 S Russell St, W Lafayette,
IN 47907 USA.
C3 University System of Maryland; University of Maryland College Park
RP Scott, ISPC (corresponding author), Univ Maryland, Dept Environm Sci & Technol,
College Pk, MD 20742 USA.
EM ispscott@umd.edu; chad.penn@usda.gov
OI Penn, Chad/0000-0003-2644-6097
FU United States Department of Agriculture (USDA-ARS)
FX This work was supported by the United States Department of Agriculture
(USDA-ARS).
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TC 13
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U2 41
PI OXFORD
SN 0045-6535
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J9 CHEMOSPHERE
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PD AUG
PY 2021
VL 276
AR 130205
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EA MAR 2021
PG 14
GA RZ1DU
UT WOS:000648339700105
PM 34088092
DA 2023-12-05
ER
PT J
AU Li, CB
Ma, BG
Tan, HB
Zhang, T
Liu, XH
Chen, P
AF Li, Chunbao
Ma, Baoguo
Tan, Hongbo
Zhang, Ting
Liu, Xiaohai
Chen, Pian
TI Effect of triisopropanolamine on chloride binding of cement paste with
ground-granulated blast furnace slag
LA English
DT Article
DE Triisopropanolamine; Chloride immobilization; Binding; AFm; Aluminum
phase
ID SURFACE FRACTAL DIMENSION; PORE STRUCTURE; FLY-ASH; COMPRESSIVE
STRENGTH; BLENDED CEMENTS; HYDRATION; CONCRETE; SULFATE; MICROSTRUCTURE;
PRODUCTS
AB Chloride was one of important factors resulting in steel bar corrosion in
reinforced concrete when using sea resources. In this paper, an attempt to promote
the chloride binding capacity of the cement-ground-granulated blast furnace slag
(GGBS) system was made by adding triisopropanolamine (TIPA). The paste was prepared
by 70 wt% cement and 30 wt% GGBS, sodium chloride, TIPA (0.03%, 0.06% and 0.10%, by
weight of binder) and water. The paste was cured for 7 d and 60 d, and the chloride
binding ratio (CBR) were measured. The hydration heat and compressive strength were
examined, then the hydrates and pore structure of the hardened paste were also
analyzed; and the effect of TIPA on aluminum and ferric dissolution of GGBS was
also studied. The results showed that TIPA could promote CBR at both 7 d and 60 d.
The reason was ascribed to three aspects: (1) TIPA facilitate the formation of FS,
which contribute to chemical binding; (2) TIPA promoted the formation of C-S(A)-H
gel, which would increase the physical binding; (3) TIPA refined the pore structure
and increased fractal dimension, which could enhance the migration resistance.
Furthermore, TIPA promoted cement hydration and pozzolanic reaction of GGBS by
facilitated the dissolution of aluminum and ferric in GGBS. Additionally, the
formation of Friedel's salt was promoted due to the transformation of ettringite to
AFm-like phase promoted by TIPA. Such results suggested a new way to improve
chloride binding capacity of cementitious materials by adding alkanolamine. (C)
C1 [Li, Chunbao; Ma, Baoguo; Tan, Hongbo; Zhang, Ting; Liu, Xiaohai; Chen, Pian]
Wuhan Univ Technol, State Key Lab Silicate Mat Architectures, Wuhan 430070, Peoples
R China.
[Zhang, Ting] Tongji Univ, Sch Mat Sci & Engn, Shanghai 201804, Peoples R China.
C3 Wuhan University of Technology; Tongji University
RP Tan, HB (corresponding author), Wuhan Univ Technol, State Key Lab Silicate Mat
EM thbwhut@whut.edu.cn
OI Liu, Xiaohai/0000-0002-8357-109X
FU National Key RAMP;D Program of China [2016YFC0701003-5]
FX The financial assistance of the ongoing project by National Key R&D
Program of China (2016YFC0701003-5) is acknowledgement by authors.
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NR 70
TC 13
Z9 13
U1 5
U2 51
PU ELSEVIER SCI LTD
PI OXFORD
SN 0950-0618
EI 1879-0526
PD SEP 30
PY 2020
VL 256
AR UNSP 119494
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PG 12
GA LY9IM
UT WOS:000540841400079
DA 2023-12-05
ER
PT J
AU Kim, J
Azimi, G
AF Kim, Jihye
Azimi, Gisele
TI Recovery of scandium and neodymium from blast furnace slag using acid
baking-water leaching
SO RSC ADVANCES
LA English
DT Article
ID RARE-EARTH-ELEMENTS; RESIDUE RED MUD; BAUXITE RESIDUE; EXTRACTION;
TEMPERATURE; CONCENTRATE; PHOSPHATE; ALUNOGEN; COAL
AB The current study puts the emphasis on developing a pyro-hydrometallurgical
process, called acid baking-water leaching, to recover scandium and neodymium from
blast furnace slag produced by the ironmaking industry. In this process, the feed
is mixed with concentrated sulfuric acid, digested at 200-400 degrees C, and
leached in water at ambient conditions. This process offers several advantages
including less acidic waste generation and rapid kinetics. With fundamental
investigations into the digestion mechanism, acid to slag mass ratio and baking
temperature are determined to have the most significant positive and negative
impacts, respectively. At low acid to slag ratio, the silicate bearing phases in
the feed do not digest, resulting in low extraction. At 200 degrees C baking
temperature, a hydrated aluminum sulfate ((Al(H2O)(6))(2)(SO4)(3)(H2O)(4.4)) phase
with weak hydrogen bonds is formed that leaches in water rapidly (<10 min); while
at 400 degrees C, Al-2(SO4)(3)with strong ionic bonds is formed that leaches at
slower kinetics (>4 h). Fundamental investigations into the water leaching process
indicate that the diffusion of water through the firm solid product (ash layer) is
the rate determining step. We expect the results of this study would help enable
valorization of industrial byproducts, in particular ironmaking slag.
C1 [Kim, Jihye; Azimi, Gisele] Univ Toronto, Dept Chem Engn & Appl Chem, Lab
Strateg Mat, 200 Coll St, Toronto, ON M5S 3E5, Canada.
[Azimi, Gisele] Univ Toronto, Dept Mat Sci & Egn, 184 Coll St, Toronto, ON M5S
3E4, Canada.
C3 University of Toronto; University of Toronto
RP Azimi, G (corresponding author), Univ Toronto, Dept Chem Engn & Appl Chem, Lab
Strateg Mat, 200 Coll St, Toronto, ON M5S 3E5, Canada.; Azimi, G (corresponding
author), Univ Toronto, Dept Mat Sci & Egn, 184 Coll St, Toronto, ON M5S 3E4,
Canada.
EM g.azimi@utoronto.ca
OI Kim, Jihye/0000-0002-7903-7855
FU Natural Sciences and Engineering Research Council of Canada (NSERC)
[503603]; Ontario Centres of Excellence (OCE) [503616]; Tenova
Goodfellow [503604]
FX This work was supported by Natural Sciences and Engineering Research
Council of Canada (NSERC) [grant number 503603]; Ontario Centres of
Excellence (OCE) [grant number 503616]; and Tenova Goodfellow [grant
number 503604]. We thank Mr Vittorio Scipolo from Tenova Goodfellow for
the collaboration throughout the project. We thank Mr Kok Long Ng for
help with SEM-EDS and Dr Raiden Acosta for help with XRF, XRD, TG-DSC,
and PSA.
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SC Chemistry
GA NI2SV
UT WOS:000565206400030
PM 35518186
DA 2023-12-05
ER
PT J
AU Jeong, TS
Park, JH
AF Jeong, Tae Su
Park, Joo Hyun
TI Effect of Fluorspar and Industrial Wastes (Red Mud and Ferromanganese
Slag) on Desulfurization Efficiency of Molten Steel
LA English
DT Article
ID CALCIUM SILICATE MELTS; HOT METAL; SULFIDE CAPACITY; THERMOCHEMICAL
ANALYSIS; REDUCTION BEHAVIOR; EAF SLAG; CAF2; KINETICS; ALUMINUM; FEO
AB Fluorspar (CaF2) has been widely used to control the physicochemical properties
of slag in steelmaking processes. However, it is very important to reduce the
CaF(2)consumption because it causes various environmental problems. In the current
study, therefore, the effect of industrial waste materials such as red mud (RM) and
ferromanganese slag (FMS) on the desulfurization behavior of molten steel was
investigated to find potential substitutes for fluorspar. Compared to conventional
10 pct CaF2-containing ladle slag, when excess industrial wastes were added (i.e.,
more than 10 mass pct), the composition of the slag was dramatically changed
(SiO(2)increases, while FetO and MnO decrease). Therefore, the sulfide capacity of
the slag decreased, and the viscosity of the slag increased. Thus, the
desulfurization efficiency was also reduced. However, when the RM or FMS were added
not more than 10 mass pct to lean-CaF2(3 pct) slag, the sulfide capacity of the
slag was equivalent to 10 pct CaF2-containing ladle slag; thus, the desulfurization
efficiency was also equivalent with lower melting point and higher fraction of
liquid phase. Consequently, it was confirmed that a small amount (less than 10 mass
pct) of industrial wastes can be added as a desulfurization fluxing agent as a
partial substitute for fluorspar.
C1 [Jeong, Tae Su; Park, Joo Hyun] Hanyang Univ, Dept Mat Engn, Ansan 15588, South
Korea.
[Park, Joo Hyun] KTH Royal Inst Technol, Dept Mat Sci & Engn, S-10044 Stockholm,
Sweden.
C3 Hanyang University; Royal Institute of Technology
RP Park, JH (corresponding author), Hanyang Univ, Dept Mat Engn, Ansan 15588, South
Korea.
FU Industrial Strategic Technology Development program - Ministry of Trade,
Industry & Energy (MOTIE), Korea [10063056]; Competency Development
Program for Industry Specialists of the MOTIE, Korea [P0002019]; Korea
Evaluation Institute of Industrial Technology (KEIT) [10063056] Funding
Source: Korea Institute of Science & Technology Information (KISTI),
National Science & Technology Information Service (NTIS)
FX This work was partly supported by the Industrial Strategic Technology
Development program (Grant Number 10063056) funded by the Ministry of
Trade, Industry & Energy (MOTIE), Korea. In addition, this research was
partly funded by the Competency Development Program for Industry
Specialists (Grant Number P0002019) of the MOTIE, Korea.
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U2 11
PU SPRINGER
PI NEW YORK
SN 1073-5615
EI 1543-1916
PD OCT
PY 2020
VL 51
IS 5
BP 2309
EP 2320
DI 10.1007/s11663-020-01889-7
EA JUN 2020
PG 12
Engineering
GA NP5NW
UT WOS:000542512900001
DA 2023-12-05
ER
PT J
AU Kashefi, K
Pardakhti, A
Shafiepour, M
Hemmati, A
AF Kashefi, Kazem
Pardakhti, Alireza
Shafiepour, Majid
Hemmati, Azadeh
TI Process optimization for integrated mineralization of carbon dioxide and
metal recovery of red mud
LA English
DT Article
DE Indirect CO2 mineralization; Red mud; pH swing; Mineral carbonation;
Calcium carbonate; Carbon capture; Storage
ID MUSSEL INSPIRED CHEMISTRY; BLAST-FURNACE SLAG; PH-SWING PROCESS; CO2
SEQUESTRATION; FACILE PREPARATION; STEELMAKING SLAG; REMOVAL; CAPTURE;
PRODUCTS; CALCIUM
AB Indirect carbonation of red mud (RM), the alkaline waste of Jajarm alumina
production plant, was carried out via a novel ex-situ multistep route. The process
includes three consecutive stages of acid leaching of RM for extraction of minerals
including aluminum (Al), magnesium (Mg), iron (Fe), calcium (Ca), and etc, pH swing
process for achieving a high purity calcium source, and finally carbonation
process. The influence of time, temperature, acid types, and acid concentration on
the extraction performance were studied to assess the optimum process conditions.
The optimized parameters in aspects of acid molarity, type, temperature and
extraction time was achieved by by 2 M hydrochloric acid (HCl) at 40 degrees C
within 30 min, respectively. About 85 % of calcium was extracted from RM at 80
degrees C within 2 h by HCl with the concentration of 1 M. The pH swing process was
employed to ensure high purity Ca-containing solution by increasing the pH from 2.3
(leached solution) to 9.5. The carbonation of Ca-enriched leachate with sodium
carbonate (Na2CO3), produced from the scrubbing of CO2 by sodium hydroxide (NaOH),
was carried out and calcium carbonate (CaCO3) with considerable purity of 98 % was
obtained. The carbonation efficiency was estimated at 32.71 %. Furthermore, the
benefit of ex-situ mineral carbon sequestration on the site that both RM and CO2
are simultaneously attainable can improve the cost-efficiency of the process.
C1 [Kashefi, Kazem; Pardakhti, Alireza; Shafiepour, Majid] Univ Tehran, Fac
Environm, Dept Environm Engn, POB 11155-4563, Tehran, Iran.
[Hemmati, Azadeh] Islamic Azad Univ, Sci & Res Branch, Dept Petr & Chem Engn,
POB 14515-775, Tehran, Iran.
C3 University of Tehran; Islamic Azad University
RP Pardakhti, A (corresponding author), Univ Tehran, Fac Environm, Dept Environm
Engn, POB 11155-4563, Tehran, Iran.
EM arparda@yahoo.com
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Z9 13
U1 6
U2 63
PU ELSEVIER SCI LTD
PI OXFORD
SN 2213-2929
EI 2213-3437
PD APR
PY 2020
VL 8
IS 2
AR 103638
DI 10.1016/j.jece.2019.103638
PG 12
SC Engineering
GA LB6KW
UT WOS:000524743700088
DA 2023-12-05
ER
PT J
AU Wang, Y
Zhang, R
Zhao, X
Min, Y
Liu, CJ
AF Wang, Yu
Zhang, Rui
Zhao, Xuan
Min, Yi
Liu, Chengjun
TI Structural Transformation of Molten
CaO-SiO2-Al2O3-FexO
Slags during Secondary Refining of Steels
LA English
DT Article
DE secondary steelmaking; refining slag; melt structure; Raman spectroscopy
ID SILICATE-BASED SLAGS; CALCIUM-ALUMINATE; PHYSICAL-PROPERTIES; VISCOSITY
PROPERTY; ANIONIC STRUCTURE; MELTS; GLASSES; TEMPERATURE; AL2O3;
SPECTROSCOPY
AB According to the variation of compositions during steel secondary refining
process, the ice-quenched samples of CaO-SiO2-FexO-Al2O3 system were prepared, the
structure were detected via the method of Raman spectroscopy, and the evolution of
structural units were further analyzed. The results showed that, for the Fe3+
cation, two types of units of tetrahedral fourfold coordination ([FeO4]) and
octahedral sixfold coordination ([FeO6]) coexisted in the molten slag, and the
ratio of [FeO6]/[FeO4] increases with the decreasing ratio of CaO/(SiO2+Al2O3). For
the Al3+ cations, four types of aluminum units of Q(Al)(2), Q(Al)(3), Q(Al)(4)
coexisted in the molten slag and the lower polymerized units Q(Al)(2) transform
into the higher polymerized Q(Al)(3) and Q(Al)(4) along with the ratio of
Al/(Al+Si) increasing from 0.41 to 0.85. For the Si4+ cations, Q(Si)(0), Q(Si)(1)
and Q(Si)(2) are the main types of [SiO4]-tetrahedral units, the Ca2+ cations of
oxygen coordination in [SiO4]-tetrahedral units are gradually replaced by Al3+,
which just act as network modifier, with the increase of Al/(Si+Al) ratio.
Accordingly, the degree of polymerization of molten slag presented in NBO/T
increases with the process of secondary steelmaking.
C1 [Wang, Yu; Zhang, Rui; Zhao, Xuan; Min, Yi; Liu, Chengjun] Minist Educ, Key Lab
Ecol Met Multimetall Ores, Shenyang 110819, Peoples R China.
[Wang, Yu; Zhang, Rui; Zhao, Xuan; Min, Yi; Liu, Chengjun] Northeastern Univ,
Sch Met, Shenyang 110819, Peoples R China.
RP Min, Y (corresponding author), Minist Educ, Key Lab Ecol Met Multimetall Ores,
Shenyang 110819, Peoples R China.; Min, Y (corresponding author), Northeastern
Univ, Sch Met, Shenyang 110819, Peoples R China.
EM miny@mail.neu.edu.cn
RI liu, xinyu/IWD-6630-2023
FU National key R&D Program of China [2017YFC0805100]; National Natural
Science Foundation of China [51674069, 51974075]; Fundamental Research
Funds for the Central Universities of China [182506001]
FX This work was supported by the National key R&D Program of China (Grant
No. 2017YFC0805100), the National Natural Science Foundation of China
(Grant No. 51674069, 51974075) and the Fundamental Research Funds for
the Central Universities of China (Grant No. 182506001).
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BP 220
EP 225
PG 6
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PT J
AU Purwanti, IF
Kurniawan, SB
Imron, MF
AF Purwanti, Ipung Fitri
Kurniawan, Setyo Budi
Imron, Muhammad Fauzul
TI Potential of Pseudomonas aeruginosa isolated from
aluminium-contaminated site in aluminium removal and recovery from
wastewater
SO ENVIRONMENTAL TECHNOLOGY & INNOVATION
LA English
DT Article
DE Aluminium recovery; Aluminium removal; Bacteria; Biological treatment;
pH
ID NONVIABLE BIOMASS; HEAVY-METALS; BIOSORPTION; BIODEGRADATION;
HYDROCARBONS; DEGRADATION; DIESEL; BATCH; SLAG; PH
AB This paper discusses the potential of Pseudomonas aeruginosa in treating
aluminium containing wastewater and aluminium recovery potential from the produced
biomass. The species of P. aeruginosa was isolated from aluminium contaminated
site. This isolate had characteristics of acid resistant up to pH 5 and aluminium
resistant up to 250 mg/L. Aluminium removal test showed that the isolated P.
aeruginosa removed up to 46.08 +/- 1.95% of 50mg/L aluminium initial concentration
from wastewater. The potential of aluminium recovered from cells biomass reached
34.2 +/- 4.25% with centrifugation and 16.8 +/- 3.02% without centrifugation.
Further application in real condition should accommodate the settling velocity of
bacteria and aluminium precipitation during treatment, in order to achieve high
removal and recovery efficiency. (C) 2019 Elsevier B.V. All rights reserved.
C1 [Purwanti, Ipung Fitri] Inst Teknol Sepuluh Nopember, Fac Civil Environm & Geo
Engn, Dept Environm Engn, Kampus ITS Sukolilo,Jalan Raya ITS, Surabaya 60111,
Indonesia.
[Kurniawan, Setyo Budi] Politekn Perkapalan Negeri Surabaya, Study Program Waste
Treatment Engn, Dept Marine Engn, Jalan Tekn Kimia,Kampus ITS Sukolilo, Surabaya
60111, Indonesia.
[Imron, Muhammad Fauzul] Univ Airlangga, Dept Biol, Fac Sci & Technol, Study
Program Environm Engn, Kampus C UNAIR,Jalan Mulyorejo, Surabaya 60115, Indonesia.
C3 Institut Teknologi Sepuluh Nopember; Airlangga University
RP Imron, MF (corresponding author), Univ Airlangga, Dept Biol, Fac Sci & Technol,
Study Program Environm Engn, Kampus C UNAIR,Jalan Mulyorejo, Surabaya 60115,
Indonesia.
EM purwanti@enviro.its.ac.id; setyobudi.kurniawan@gmail.com;
fauzul.01@gmail.com
RI Imron, Muhammad Fauzul/Q-7775-2019; Kurniawan, Setyo Budi/Q-6349-2019;
Imron, Muhammad Fauzul/ISV-1451-2023
OI Imron, Muhammad Fauzul/0000-0003-2649-2421; Kurniawan, Setyo
Budi/0000-0002-0791-1638;
FU Ministry of Research, Technology and Higher Education Indonesia by the
scheme of Penelitian Unggulan Perguruan Tinggi 2017; Indonesia Endowment
Fund for Education; Universitas Airlangga
FX This research was supported by the Ministry of Research, Technology and
Higher Education Indonesia by the scheme of Penelitian Unggulan
Perguruan Tinggi 2017 and the Indonesia Endowment Fund for Education by
the research grant for the LPDP awardee 2017. The author would also
deliver our gratitude to Universitas Airlangga for sponsoring this
publication.
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NR 45
TC 13
Z9 13
U1 0
U2 11
PU ELSEVIER
PI AMSTERDAM
SN 2352-1864
J9 ENVIRON TECHNOL INNO
JI Environ. Technol. Innov.
PD AUG
PY 2019
VL 15
AR 100422
DI 10.1016/j.eti.2019.100422
PG 8
WC Biotechnology & Applied Microbiology; Engineering, Environmental;
SC Biotechnology & Applied Microbiology; Engineering; Environmental
Sciences & Ecology
GA IP9ZW
UT WOS:000480410500026
DA 2023-12-05
ER
PT J
AU Huang, GD
Ji, YS
Zhang, LL
Hou, ZH
Zhang, L
Wu, SR
AF Huang, Guodong
Ji, Yongsheng
Zhang, Linglei
Hou, Zhihui
Zhang, Li
Wu, Shourong
TI Influence of calcium content on structure and strength of MSWI bottom
ash-based geopolymer
LA English
DT Article
DE chemical properties; composite materials; compressive strength
ID FLY-ASH; BLENDED CEMENT; CONCRETE; IMPACT; STABILIZATION; PERFORMANCE;
ADDITIONS; ALUMINUM; RECOVERY; MORTARS
AB This study explored the strength limitations of municipal solid waste
incineration (MSWI) bottom ash-based geopolymer, which can limit its use in
building materials. The calcium content in MSWI bottom ash was increased by the
addition of varying amounts of granulated blast furnace slag (GBFS) and calcium-
containing chemicals. The results showed that the low calcium content of MSWI
bottom ash in geopolymer was the main cause of insufficient polymerisation. Both
GBFS and calcium-containing chemicals improved geopolymer microstructure and
enhanced the degree of polymerisation, which clearly improved the compressive
strength. However, further increases in geopolymer compressive strength were not
significant when the GBFS content was greater than 40%, and the compressive
strength decreased sharply when hydrated Ca(OH)(2) content was greater than 5%.
C1 [Huang, Guodong] China Univ Min & Technol, Xuzhou, Jiangsu, Peoples R China.
[Huang, Guodong] Anhui Univ Sci & Technol, Huainan, Anhui, Peoples R China.
[Ji, Yongsheng] State Key Lab Geomech & Deep Underground Engn, Xuzhou, Jiangsu,
Peoples R China.
[Zhang, Linglei; Hou, Zhihui; Zhang, Li; Wu, Shourong] China Univ Min & Technol,
Sch Mech & Civil Engn, Xuzhou, Jiangsu, Peoples R China.
C3 China University of Mining & Technology; Anhui University of Science &
Technology; China University of Mining & Technology
RP Ji, YS (corresponding author), State Key Lab Geomech & Deep Underground Engn,
Xuzhou, Jiangsu, Peoples R China.
EM jysbh@126.com
OI Ji, Yongsheng/0000-0002-7414-9719
FU Fundamental Research Funds of the Central Universities [2018XKQYMS02];
FRFCU
FX The authors are grateful for the financial support from the Fundamental
Research Funds of the Central Universities (2018XKQYMS02). The research
work belongs to one part of the projects which are financially supported
by FRFCU.
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NR 34
TC 13
Z9 14
U1 9
U2 60
PU ICE PUBLISHING
PI WESTMINISTER
SN 0024-9831
EI 1751-763X
J9 MAG CONCRETE RES
JI Mag. Concr. Res.
PD APR
PY 2019
VL 71
IS 7
BP 362
EP 372
DI 10.1680/jmacr.17.00542
PG 11
GA HO8AM
UT WOS:000461171800005
DA 2023-12-05
ER
PT J
AU Yu, DW
Paktunc, D
AF Yu, Dawei
Paktunc, Dogan
TI Carbothermic reduction of chromite fluxed with aluminum spent potlining
LA English
DT Article
DE chromite; carbothermic reduction; ferrochrome; aluminum spent potlining
ID KINETICS; SPL
AB Aluminum spent potlining (SPL) was employed as both the fluxing agent and a
source of carbonaceous reductant for the carbothermic reduction of chromite, aiming
to allow effective separation of alloy from the slag component. The experimental
results show that the carbonaceous component of the SPL is more reactive towards
chromite reduction compared to graphite. The formation of refractory spinel
(MgAl2O4) on chromite particles hinders further reduction and alloy growth. The
slag-making components of the SPL (e.g. nepheline and NaF) form molten slags at low
temperatures (similar to 1300 degrees C) and partly dissolve the refractory spinel
as well as the chromite. Destruction of the spinel layer with enhanced mass
transfer greatly improves the alloy growth, which can be further promoted by
reduction at a higher temperature (e.g. 1500 degrees C). Ferrochrome alloy
particles grow large enough at 1500 degrees C in the presence of SPL, allowing
effective separation from the slag component using elutriation separation.
C1 [Yu, Dawei; Paktunc, Dogan] Nat Resources Canada, CanmetMIN, 555 Booth St,
Ottawa, ON K1A 0G1, Canada.
[Yu, Dawei] Cent S Univ, Sch Met & Environm, Changsha 410083, Hunan, Peoples R
China.
C3 Natural Resources Canada; Lands & Minerals Sector - Natural Resources
Canada; CanmetMINING; Central South University
RP Yu, DW (corresponding author), Nat Resources Canada, CanmetMIN, 555 Booth St,
Ottawa, ON K1A 0G1, Canada.; Yu, DW (corresponding author), Cent S Univ, Sch Met &
Environm, Changsha 410083, Hunan, Peoples R China.
EM dawei.yu@csu.edu.cn
RI Paktunc, Dogan/AAT-2246-2021; Yu, Dawei/AAE-7736-2021
OI Paktunc, Dogan/0000-0003-4965-3531
FU NRCan under the Rare Earth Elements and Chromite RD Program
FX The following contributions are acknowledged: Shudip Faiyaz for
performing the SEM analyses and the elutriation separation, Derek Smith
for XRD analyses, Ruiping Wang for chemical analysis of the products,
and KWG Resources Inc. for providing the chromite ore samples. The study
was funded by NRCan under the Rare Earth Elements and Chromite R&D
Program.
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NR 42
TC 13
Z9 15
U1 2
U2 32
PI AMSTERDAM
SN 1003-6326
EI 2210-3384
PD JAN
PY 2019
VL 29
IS 1
BP 200
EP 212
DI 10.1016/S1003-6326(18)64929-5
PG 13
GA HK0YS
UT WOS:000457631400021
DA 2023-12-05
ER
PT J
AU Madhav, TV
Reddy, IVR
Ghorpade, VG
Jyothirmai, S
AF Madhav, T. Venu
Reddy, I. V. Ramana
Ghorpade, Vaishali G.
Jyothirmai, S.
TI Compressivestrength study of geopolymer mortar using quarry rock dust
LA English
DT Article
DE Geopolymer; Alkaline solution; Cement concrete; Fly ash; Slag;
Sustainable technology
AB India is one of the Developing countries that needs to face the environmental
pollution. We have many ways to reduce environmental pollution that causes by
production of Portland cement and by the increasing of waste material. Geopolymer
is the term used to represent the binders produced by polymeric reaction of
alkaline liquid with silicon and aluminium as source materials. Common river sand
is expensive due to excessive cost of transportation from natural sources. Also
large-scale depletion of these sources creates environmental problems. River sand
is most commonly used fine aggregate in the production of concrete poses the
problem of acute shortage in many areas. In such a situation the Quarry rock dust
can be an economic alternative to the river sand.
Quarry Rock Dust can be defined as residue, tailing or other non-voluble waste
material after the extraction and processing of rocks to form fine particles less
than 4.75 mm. This paper presents the feasibility of the usage of Quarry Rock Dust
as a substitute for Natural Sand in geopolymer mortar. The by-product materials
considered in this study are combination of GGBFS and Fly ash. The experimental
program involves casting of geopolymer mortar cubes by using GGBFS, Flyash and
Quarry rock dust and testing them at 1 day, 3 days and 7 days for compressive
strength. Different parameter considered in this study is alkaline fluid to binder
ratio Keeping 12-Molarity of the alkaline liquid and the ratio of sodium hydroxide
to sodium meta silicate as constant (1:2). (C) 2018 Elsevier B.V. All rights
reserved.
C1 [Madhav, T. Venu; Jyothirmai, S.] Audisankara Coll Engn & Technol, Dept Civil
Engn, Gudur 524101, Andhra Prades, India.
[Reddy, I. V. Ramana] SVU Coll Engn, Dept Civil Engn, Tirupati 517502, Andhra
Prades, India.
[Ghorpade, Vaishali G.] JNTUA Coll Engn, Civil Engn Dept, Anantapuram 515002,
Andhra Prades, India.
C3 Sri Venkateswara University; JNTUA College of Engineering Anantapur;
Jawaharlal Nehru Technological University - Anantapur
RP Madhav, TV (corresponding author), Audisankara Coll Engn & Technol, Dept Civil
Engn, Gudur 524101, Andhra Prades, India.
EM vtmadhav@gmail.com
RI Ghorpade, Vaishali/HHN-3836-2022
CR Davidovits J., 1999, GEOP 99 INT C SAINT
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NR 8
TC 13
Z9 13
U1 1
U2 52
PI AMSTERDAM
SN 0167-577X
EI 1873-4979
J9 MATER LETT
JI Mater. Lett.
PD NOV 15
PY 2018
VL 231
BP 105
EP 108
DI 10.1016/j.matlet.2018.07.133
PG 4
GA GR1XT
UT WOS:000442349900028
DA 2023-12-05
ER
PT J
AU Czech, B
Hojamberdiev, M
Bogusz, A
AF Czech, Bozena
Hojamberdiev, Mirabbos
Bogusz, Aleksandra
TI Impact of thermal treatment of calcium silicate-rich slag on the removal
of cadmium from aqueous solution
LA English
DT Article
DE Slag; Cd(II); Adsorption kinetics; Adsorption isotherms
ID WASTE-WATER; METAL-IONS; FURNACE-SLAG; STEEL SLAG; SORPTION; CD(II);
ADSORPTION; CD; COPPER; NANOCOMPOSITES
AB The problem of wastewater treatment and inorganics removal and the waste
management including slags is of great importance nowadays. Three types of treated
calcium silicate-rich slags were tested. The impact of thermal treatment of slag in
air (SA), under NH3 atmosphere (SN), and in the presence of flux (SF) at different
temperatures (500-1000 degrees C) on removal of cadmium from aqueous solution was
investigated. The treatment had the impact on slag characteristics. In the slag
samples thermally treated in air, SiO2, clinopyrexene, larnite, CaSiO3, Ca3SiO5,
Ca8Si5O18, and olivine crystalline phases were formed. A very similar trend was
observed for the slag samples heat treated under NH3 atmosphere except the
formation of wollastonite at 1000 degrees C. Depending on the flux employed in the
thermal treatment of slag, various crystalline phases were formed. Each alkaline
earth metal chloride (CaCl2, SrCl2, and BaCl2) flux affected differently.
Potassium, iron, magnesium, aluminum, silicon, calcium, and lead are the main
elemental components of the slag. The slag sample thermally treated with CaCl2 flux
showed the highest potential for Cd(II) adsorption followed by the SN sample
series. The results strictly indicate the complex mechanism of Cd(II) adsorption
onto the slag materials considering both chemical adsorption (a pseudo-second
order) and intraparticle diffusion. Cd(II) adsorption proceeded according to the
Langmuir, Temkin or Freundlich models. The best results can be obtained using a
low-cost slag adsorbent thermally treated under NH3 atmosphere. (C) 2018 Elsevier
C1 [Czech, Bozena] Marie Curie Sklodowska Univ, Fac Chem, Dept Environm Chem, Pl M
Cure Sklodowskiej 3, PL-20031 Lublin, Poland.
[Hojamberdiev, Mirabbos] Nagoya Univ, Dept Mat Phys, Chikusa Ku, Furo Cho,
Nagoya, Aichi 4648603, Japan.
[Bogusz, Aleksandra] Natl Res Inst, Inst Environm Protect, Dept Ecotoxicol, Ul
Krucza 5-11, PL-00548 Warsaw, Poland.
C3 Maria Curie-Sklodowska University; Nagoya University; Institute of
Environmental Protection - National Research Institute
RP Czech, B (corresponding author), Marie Curie Sklodowska Univ, Fac Chem, Dept
Environm Chem, Pl M Cure Sklodowskiej 3, PL-20031 Lublin, Poland.; Hojamberdiev, M
(corresponding author), Nagoya Univ, Dept Mat Phys, Chikusa Ku, Furo Cho, Nagoya,
Aichi 4648603, Japan.
EM bczech@hektor.umcs.lublin.pl; hmirabbos@gmail.com
RI Czech, Bożena/C-6914-2013; Hojamberdiev, Mirabbos/C-8182-2014
OI Czech, Bożena/0000-0002-4895-5186; Hojamberdiev,
Mirabbos/0000-0002-5233-2563; Bogusz, Aleksandra/0000-0002-5218-381X
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