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ME 241
MATERIALS LABORATORY
Cold Working and Rockwell Hardness
Names of all group members, alphabetically
Group number:
Name of experiment:
Date performed:
1.
1|Page
Abstract:
.
2|Page
Table of Contents
1. Abstract:........................................................................................................................................ 1
1 Introduction: ................................................................................................................................. 4
6 Conclusion: ................................................................................................................................... 9
7 References: ................................................................................................................................. 11
3|Page
1 Introduction:
Cold working is a widely used process in metallurgy to enhance the mechanical properties of metals
and alloys. By subjecting materials to plastic deformation at temperatures below their recrystallization
point, cold working induces changes in the microstructure, resulting in improvements in strength,
hardness, and other mechanical characteristics. Understanding the effects of cold working on material
properties is essential for optimizing manufacturing processes and designing components with
desired performance attributes.
In this report, we investigate the relationship between cold working and Rockwell hardness for two
commonly used metal alloys: 260-Brass and 110-Cu alloy. Through a series of experiments, we
explore how variations in cold work percentage affect the average hardness of these materials. The
experimental setup includes a cold rolling machine for deformation and a Rockwell hardness tester
for measuring material hardness.
The objectives of this study are twofold: first, to quantify the changes in material hardness resulting
from different levels of cold working, and second, to analyze the underlying mechanisms responsible
for these changes. By examining the effects of cold working on brass and Cu samples, we aim to
study into the relationship between deformation-induced microstructural changes and macroscopic
mechanical properties like hardness.
This report outlines the experimental procedures, results obtained, and scientific approach to the
mechanisms involved in changing mechanical properties. By comparing the relationship between
4|Page
cold work percentage and Rockwell hardness, we can design the cold workability conditions to
achieve the desired level of properties for given applications.
2 Experimental Setup:
Following are the equipment used in the experiment.
• Safety Glasses
• Callipers
5|Page
indenter. The major load was set to 100 kgf, and the machine automatically applied the load after
contacting the sample surface. The hardness reading was then recorded from the tester's display.
This process was repeated for additional percentages of cold working, such as 10%.
6|Page
The results from the experiment are presented in Table 1, detailing the thickness, percentage of cold
work, and Rockwell hardness (HRC) for both 110 Copper Alloy and 260 Brass specimens at various
stages of cold working.
properties. The cold working processes also provide a way to directionally influence the
microstructural changes [6-8]. Several researchers have been investigated the effect of plastic
deformation to microstructure of material. Li et.al investigated the combination effect of plastic
deformation and phase transformation on the evolution of microstructure and property of NiTi alloy
[9]. Ren et.al studied grain refinement and mechanical response of U-5.5 wt.%Nb alloy produced by
cold rolling and heat treatment [10]. Kawalko et.al investigated microstructure evolution of CP
titanium during deformation process followed by cold rolling [11].This study aims find out the effect
of cold rolling process on changes in microstructure and hardness of 260-brass and 110-Cu alloy.
Hardness, one of mechanical property that important to consider, is measure of a material’s resistance
to localized plastic deformation. Hardness is an indicator of wear resistance [12]. Brass is widely used
as an industrial material, clinical and scientific application because of its excellent characteristics
such as high corrosion resistance, nonmagnetic, good plasticity deformability, and machinability
[13,14]
To assess the validity of our experimental findings, we compare Table 1 with published results for
copper and brass alloys. Published data can serve as a benchmark for evaluating the accuracy and
consistency of our experimental measurements. Any discrepancies observed between our results and
published data may indicate potential errors or variations in experimental conditions.
80 5 % Cold Work
10% Cold Work
70
60
Hardness (HRC)
50
40
30
20
10
0
110 Cu alloy 260 Brass
Samples
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To visualize the relationship between cold work percentage and material hardness, we plot the data
from Table 1 on a graph. The x-axis represents the percentage of cold work, while the y-axis
represents Rockwell hardness (HRC). By plotting both brass and copper data on the same graph, we
can directly compare the effects of cold working on the two materials and identify any differences
or similarities in their behaviour.
Hardness measurements were not taken right next to the edge or immediately adjacent to the first
indentation to minimize the influence of edge effects and indentation overlap on the accuracy of
measurements. Placing indentations too close together or near edges can lead to erroneous readings
due to interactions between neighbouring indentations and surface irregularities.
The differences in hardness between copper and brass at any given percentage of cold work can be
attributed to variations in their material properties, including composition, crystal structure, and
alloying elements. Brass typically contains zinc as an alloying element, which can influence its
mechanical properties differently from pure copper. Additionally, differences in grain size, grain
boundaries, and dislocation densities may contribute to variations in hardness between the two
materials.
6 Experimental Error
Potential sources of error in the experiment include variations in sample preparation, measurement
technique, and equipment calibration. To decrease experimental error, it is essential to standardize
procedures, calibrate equipment regularly, and minimize environmental fluctuations during testing.
Additionally, increasing sample size and conducting multiple trials can help improve the reliability
and accuracy of experimental results. By critically analysing the results from Table 1 and addressing
the points outlined above, we can gain valuable insights into the effects of cold working on material
hardness, compare experimental data with published results, and identify opportunities for
improving experimental techniques and minimizing errors.
7 Conclusion:
the experiment conducted to investigate the effects of cold working on the hardness of 110 Copper
Alloy and 260 Brass specimens has provided valuable insights into the relationship between plastic
deformation and material properties. Through a series of measurements and analyses, several key
findings have emerged, shedding light on the mechanical behaviour of these metal alloys under
different levels of cold work.
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8 References:
[1] A.S. Darmawan, W.A. Siswanto, T. Sujitno, Advanced Materials Research, 789, 347 (2013).
[2] Y. Lian, J. Huang, J. Zhang, C. Zhao, W. Gao, Z. Zhang, M. Ma, Materials Science &
Engineering A, 712, 663 (2018).
[3] A.S. Darmawan, A.D. Anggono, A. Hamid, MATEC Web of Conferences, 154, 01105 (2018).
[4] Y. Bai, T. He, Y. Liu, Materials Characterization, 137, 142 (2018).
[5] A. Hamid, I. Baba, W. Sani, International Journal on Advanced Science, Engineering and
Information Technology, 7 (2), 446 (2017).
[6] C. Lan, Y. Wu, L. Guo, F. Chen, Materials Science and Engineering: A, 690, 170 (2017).
[7] S. Wang, L. Niu, C. Chen, Y.L. Jia, M.P. Wang, Z. Li, Z.H. Zhong, P. Lu, P. Li, Y.C. Wu,
Fusion Engineering and Design, 125, 510 (2017).
[8] M. Eskandari, M.A. Mohtadi-Bonab, J.A. Szpunar, Materials and Design, 90, 618 (2016).
[9] Y. Li, J.Y. Li, M. Liu, Y.Y. Ren, F. Chen, G.C. Yao, Q.S. Mei, Journal of Alloys and
Compounds, 653, 156 (2015).
[10] Z. Ren, R. Ma, G. Hu, J. Wu, Z. Wang, C. Luo, Journal of Nuclear Materials, 494, 72
(2017).
[11] J. Kawałko, P. Bobrowski, P. Koprowski, A. Jarze˛bska, M. Bieda, M. Łagoda, K.
Sztwiertnia, Journal of Alloys and Compounds, 707, 298 (2017).
[12] A. S. Darmawan, W. A. Siswanto, T. Sujitno, Applied Mechanics and Materials, 315,
700 (2013).
[13] J. Li, Y. Ren, M. Ibrahim, Songbai, K. Yang, Materials Letters, 202, 162 (2017).
[14] H. Imai, Y. Kosaka, A. Kojima, S. Li, K. Kondoh, J. Umeda, H. Atsumi, Powder
Technology, 198, 417 (2010).
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