Spectro Test

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SPECTROTEST
Mobile Spectrometer for

Metal Analysis
Original operating instructions

Table of Contents
1 Description of instrument .................................................................................... 5
1.1 Description .......................................................................................................................... 5
1.2 Function .............................................................................................................................. 5
1.3 Overview ............................................................................................................................. 6
1.3.1 Connections (rear) ................................................................................................. 6
1.3.2 Instrument .............................................................................................................. 7
2 Safety.................................................................................................................. 8
2.1 Symbols used ..................................................................................................................... 8
2.2 User information.................................................................................................................. 9
2.3 Intended use ..................................................................................................................... 10
2.4 Prohibited operating conditions ........................................................................................ 10
2.5 Residual risks.................................................................................................................... 10
3 Technical data................................................................................................... 13
4 Transportation/Setting-up ................................................................................. 14
4.1 Set-up ............................................................................................................................... 14
4.2 Dimensions and weight ..................................................................................................... 15
4.3 Gas supply (sparks operating mode) ................................................................................ 16
4.3.1 Argon bottle fastening.......................................................................................... 17
5 Operation .......................................................................................................... 18
5.1 General arrangement of display and buttons ................................................................... 18
5.1.1 Instrument ............................................................................................................ 18
5.1.2 Brightness adjustment ......................................................................................... 18
5.1.3 Sample probe ...................................................................................................... 19
6 Initial start-up .................................................................................................... 21

6.1 Preparing the instrument for use ...................................................................................... 21
6.2 Switching on the instrument .............................................................................................. 21
6.3 Standby mode ................................................................................................................... 22
6.4 Switching off the instrument .............................................................................................. 22
6.5 Measuring procedure ........................................................................................................ 23
6.5.1 Preparing the measuring procedure .................................................................... 24
6.5.2 Proceed with the measurement ........................................................................... 25
• Sample measurement, analysis .......................................................................... 25
• Example measurement, Sorting .......................................................................... 26
• ICALization of the measuring instrument (ICAL) ................................................. 27
6.6 Replacing parts of sample probe ...................................................................................... 28
6.6.1 General arrangement of test probe parts ............................................................ 28
6.6.2 Changing the sample probe ................................................................................ 29
6.6.3 Changing the adapter .......................................................................................... 29
6.6.4 Changing the electrode ....................................................................................... 30
SPECTROTEST — 05.12.2017 —3
7 Maintenance ..................................................................................................... 31
7.1 Maintenance schedule ...................................................................................................... 31
7.2 Cleaning the adapter ......................................................................................................... 32
7.3 Cleaning the light inlet windows of the sample probe and of the adapter ........................ 32
7.4 Replacing the air filter ....................................................................................................... 34
7.5 Replacing the sample probe air filter ................................................................................ 35
7.6 Replacing the CO2 and fine dust filter unit ........................................................................ 36
7.7 Cleaning/sharpening the electrodes ................................................................................. 37
8 Troubleshooting................................................................................................ 38
9 Spare parts and consumables .......................................................................... 41
10 De-commissioning ............................................................................................ 41
11 Manufacturer address ...................................................................................... 41
—4 SPECTROTEST — 05.12.2017
Description of instrument
1 Description of instrument
1.1 Description
Designation: SPECTROTEST
Model: TXC03 / TXC35
Type: 76004718 / 76004720
1.2 Function
The sample probe evaporates sample material by means of arc discharge or spark
discharge. In this process, the released atoms and ions are stimulated to emit
radiation. A fiber-optics directs this radiation to the optical system. Here the
radiation is evaluated.
Data are already stored in the unit's memory. The measured values are compared
with these data. The results are then displayed on the screen.
1.3 Overview
1.3.1 Connections (rear)
Fig. 1
No. Component No. Component
1 VGA 4 USB
2 HDMI 5 Argon connection
3 LAN
1.3.2 Instrument
Fig. 2
1 Housing (spectrometer) 9 Test probe
2 Screen 10 Locking device for transport

trolley/instrument
3 Storage compartment 11 Roller brake
4 Test probe support 12 Argon bottle retaining strap

 Can also be installed on the
side.
5 Transport carriage (can be 13 Type plate

disassembled)
6 Adapter 14 Air filter
7 Sample probe connection 15 CO2 and fine dust filter (behind

the cover)
8 Drawer for optional rechargeable 16  Power supply connection

battery  Fuse
Safety
2 Safety
Every user of the instrument must have understood these operating instructions.
This applies in particular to the safety regulations.
2.1 Symbols used

The following symbols are used in these abbreviated operating instructions and/or
on the instrument.
If required, additional important information is available in connection with these
symbols.
Warning! Risk of injury!
Warning! Risk of electric shock!
Warning! Risk of burns!
Warning! Danger of poisoning!
Warning! UV radiation!
Notice!
Warns of activities or conditions that may adversely affect the safety or function of
the instrument.
Information
Displays information that is important for the correct and safe use of the
instrument.
Safety
2.2 User information

 Compliance with all safety instructions is mandatory. It's for your own safety.
 Non-compliance with the operating and safety instructions may lead to injuries
and can cause a health hazard.
 The instrument - in its transport packaging - may only be transported by
expert organizations or by specifically trained personnel.
 In order to move the instrument around, use either the recesses grip or place
the instrument onto the transport trolley. Other types of transportation are not
permitted.
 Only proceed with the maintenance task as described in Chapter
“Maintenance” of the operating instructions. Any other services (e.g., technical
maintenance) or repairs must only be performed by service personnel
authorized by the instrument manufacturer.
 During the operation and while performing maintenance tasks compliance
with safety instructions and accident prevention regulations is mandatory.
This regulation is, for example, DIN EN 61010 or any other comparable
national standard.
 The safety measures must be checked following every technical maintenance
or repair activity. This check must be performed according to
VBG4/DIN EN 61010 or a comparable national standard.
 Compliance with the maintenance schedule specified by the manufacturer
and recording all maintenance activities is mandatory. This will maintain the
operational safety of the instrument.
 Never tamper with the safety devices! If it is suspected that a safety device
does not work properly, shut down the instrument immediately!
 Please observe the information labels provided on the instrument.
 Only genuine spare parts must be used when repairing the instrument. The
use of non-genuine spare parts will make the CE Declaration of Conformity
null and void.
 The instrument must only be connected to the mains power supply with a
protective grounding conductor.
 If an instrument is positioned on a sloped surface and equipped with wheels,
it may roll away during the operation. Secure the instrument while in
operation. This applies also when the instrument is being transported.
 Compliance with the relevant safety regulations when using tools and
operating equipment is mandatory.
 Prior to opening the instrument, disconnect the power plug. The instrument is
only completely disconnected from power if the power plug is removed.
Safety
2.3 Intended use

This instrument analyzes and identifies metals. Only such metals may be analyzed
for which the instrument has been calibrated by the manufacturer or by qualified
technical personnel.
2.4 Prohibited operating conditions

Do not operate the instrument if one of the following conditions exists:
 If the instrument is faulty or damaged.
 If the instrument is not maintained at regular intervals.
 If the ambient conditions do not comply with the specification.
 If the area where the instrument is used is not a commercial/industrial
premise.
2.5 Residual risks

This instrument has been manufactured in accordance the latest state-of-the-art
technology. Nevertheless, residual risks cannot be completely excluded.
Warning! Risk of injury and health hazard!

 The instrument is operated with argon. Argon is heavier than air. It can
accumulate in a closed room, especially on the floor or lower-lying areas.
 Ensure to provide adequate ventilation. If necessary, install oxygen
sensors.
 The CO2 filter unit (optional) contains chemicals.
 The applicable safety data sheet is available at
http://www.spectro.com/msds.
 Protective gloves and goggles must be worn when replacing the filter
unit.
 When disposing of the filter unit, compliance with legal regulations is
mandatory.
— 10 SPECTROTEST — 05.12.2017
Safety
Warning! Danger of poisoning!

 Metal vapors may be generated from the sample material. Depending on the
sample material, these vapors may be toxic, e.g. in case of heavy metals.
 Ensure that protective equipment is worn in such cases, e.g. a
breathing apparatus and extraction equipment is installed. The
protective methods must ensure that the applicable threshold limit
values (TLV) and/or comparable national standards are not exceeded.
Warning! Risk of electrical shock!

When the instrument is switched on, there is a risk of an electric shock when the
electrode is touched or when the sample is removed during a measurement.
For a healthy person, this electric shock is of no concern. These are low currents
and voltages which are below the limit values of EN61010. However, a shock
may cause a subsequent accident, e.g. a fall from a ladder.
 Never touch the sample while a measurement is in progress.
 Avoid any contact with the electrode if the excitation is activated (plasma
generator).
 Always shut down the excitation (plasma generator) when working on the
spark stand (stationary spectrometers) or on the test probe (mobile
spectrometers).
 On mobile spectrometers, as an alternative, the probe can also be
disconnected from the instrument.
 For voltage ranges, see page 12.

 Contacting the electrode increases the risk of burn injuries. During normal
operation, the electrode will heat up to several hundred degrees.
 Never touch the electrode with your bare hands, even after shutting
down the spectrometer. Always use pliers.
 If an adapter is used for several measurements in a row, it can get hot.
 Touch the adapter only after it has sufficiently cooled.
 A sample can get hot if it is measured several times.
 Touch the sample only after it has sufficiently cooled.
SPECTROTEST — 05.12.2017 — 11
Safety
The arc on the spark stand generates UV radiation. UV radiation may cause
damage to the eyes or skin.
 Use the appropriate sample adapter for samples that are not completely
covered by the spark stand opening.
 Take appropriate protective measures (e.g. wear safety goggles) when the
spark stand or the adapter openings are not fully covered.
Information
A high-voltage pulse ignites the plasma.
After the ignition, an alternating voltage (spark mode) or a direct voltage (arc
mode) is applied to the electrode.
The following table shows the respective voltage ranges:
High-voltage High-voltage Burning voltage Burning voltage

ignition pulse, ignition pulse, arc mode spark mode
arc mode spark mode
Spectro test 6 - 12 KV, 1 - 12 KV, 30 - 60 V, 20 - 200 V,

TXC03 / typically 8 KV typically 5 KV typically 40 V typically 30 V
TXC35
 When the instrument is switched on, there is an inherent risk of an electrical

emission during a spark test, especially if the sample is removed during the
measuring process.
 For a healthy person, this electrical transmission is of no concern. These
are electromagnetic fields of low intensity. Due to this transmission, the
electromagnetic characteristics of the device may be outside the limits of
EN61326-1 in some areas. As a result, disturbances of radio
transmissions can occur in the immediate (near) range of the
spectrometer. This means, for example, interference during the reception
of radio transmissions is possible (crackling, image disturbances).
 Users of life-sustaining or supporting medical devices (e.g., insulin
pumps, pacemakers, defibrillators, EEG, ECG devices, etc.) should not
be affected by CE-compliant devices. For this group of operators,
however, it is strongly recommended to contact the manufacturer of the
instrument before using the spectrometer!
— 12 SPECTROTEST — 05.12.2017
Technical data
3 Technical data
Description Value
Power supply 100 - 240 V, ±10%, 50/60 Hz (compliant with DIN EN

61010-1)
Power during test 320 W
Power during stand-by 60 W
Power supply fuses 16 A (slow-blow)
Storage conditions -20 – 50°C; -5 – 120°F,

freezing and condensation must be avoided.
Permissible ambient 5 – 40 °C; 40 – 105 °F

temperature (according to DIN EN 61010-1)
Atmospheric humidity max. 80% compliant with (as per DIN EN 61010-1)
Argon gas connection
 Inlet pressure 5 bar ±10%; 72 psi
 Quality ≥ 4.8 (99.998 %)
 Consumption of standard Constant flow: 15 L/h

probe Analytic flow: 120 L/h
Flushing: 120 L/h
 UV probe consumption Constant flow: 15 L/h plus 10 L/h UV optics

Analytic flow: 120 L/h
Flushing: 185 L/h
Protection class IP 23 (DIN 40050)
SPECTROTEST — 05.12.2017 — 13
Transportation/Setting-up
4 Transportation/Setting-up
4.1 Set-up
Warning! Risk of injury!

Improper use of the transport trolley can result in accidents.
 Use the optional transport trolley only to transport the instrument and the
associated argon bottle.
 Never use the transport trolley to transport people.
 Compliance with the safety requirements for the transport of gas bottles is
mandatory.
 Only place the gas bottle onto the transport trolley when the instrument is
already placed on it.
 In order to move the instrument around, use either the recesses grip or place
the instrument onto the transport trolley. Other types of transportation are not
permitted.
Notice! Damage to instrument!

 The instrument can tip over or roll away.
 Always ensure that the instrument is standing safely and firmly. Always
use the roller brakes to secure the transport trolley.
 When moving the instrument,
 lock the drawer
 always hang the probe into the transport bracket.
 if the floor is uneven, tip the transport trolley onto both large wheels.
 fasten the instrument when using a separate transport trolley.
 When transporting the instrument on a truck
 use an appropriate cover to protect the display.
 remove the argon bottle from the transport trolley.
— 14 SPECTROTEST — 05.12.2017

Corrosive vapors may damage the instrument.
 Place the instrument in an environment free from corrosive vapors.
Information! Measurement errors!

 If the instrument is subject to vibrations and shocks, measurement errors
may occur during the measuring process.
 The instrument must be installed at a vibration- and shock-free location.
 Avoid mechanical impacts.
 Measurement errors may result from temperature differences inside the
instrument.
 Install the instrument so that it cannot heat up or cool down on one side
only.
4.2 Dimensions and weight
Name Value
Unit height 670 mm (26.3’’)
Unit width 425 mm (16.7’’)
Unit depth 330 mm (13.0’’)
Unit weight 33 kg (72.7 lbs)
SPECTROTEST — 05.12.2017 — 15
4.3 Gas supply (sparks operating mode)

Information! Measurement errors!
Impurities in the argon supply cause measuring errors.
 Ensure oil and grease-free laying of the argon supply line.
The spectrometer requires an argon supply line.

A suitable pressure reducer is required for the argon supply (bottles or liquid gas
tank).
 Adjustable output pressure 0 - 10 bar
 Argon inlet pressure at the instrument is 5 bar ±10%, 72 psi
A PTFE hose with quick release provided by SPECTRO supplies the argon
(instrument side):
 Diameter OD 6 / ID 4, length 0.8 m
 When using longer lines and/or smaller tube diameters, a possible pressure
drop must be taken into account.
— 16 SPECTROTEST — 05.12.2017
4.3.1 Argon bottle fastening
Information
The argon bottles may only be moved on the transport trolley if the bottle is
properly secured with the retaining straps and the instrument is also located on the
transport trolley.
The transport carriage is equipped with a retaining strap for argon bottles with
different diameters.
Fig. 3
1 Installation of the retaining strap 2 Installation of the retaining strap

for argon bottles with a small for argon bottles with a large
diameter. diameter.
SPECTROTEST — 05.12.2017 — 17
Operation
5 Operation
5.1 General arrangement of display and buttons
5.1.1 Instrument
1 2 3 4 5
6
Fig. 4
No. Control element Function
1 Switch Switches the instrument on.
2 Switch Sets the sample probe to stand-by mode
3 Track ball Same as mouse function on a PC
4+5 Mouse button function Same as mouse buttons on a PC
6 Standard keyboard Same as PC keyboard
5.1.2 Brightness adjustment

In order to adjust the brightness of the display, open the Tray Tool
"Powermanagement Pro Mobile" via the Windows taskbar.
 The brightness adjustment screen opens.
 Adjust the desired brightness.
— 18 SPECTROTEST — 05.12.2017
Operation
5.1.3 Sample probe

Information
In order to prevent inadvertent triggering of a measurement, the "Start
measurement" key is disabled after one minute (adjustable), if the key is not
activated in the meantime. To unlock, briefly press the button.
SPECTROTEST — 05.12.2017 — 19
Operation
Fig. 5: Test probe
No. Display/button Function
1 Status display of the  green light

test probe  ready
 red light
 not ready
 Malfunction
 Blinking red
 A measurement is in process
2 “Start measurement” button

Use this button to proceed with the measurement.
This button must kept depressed during the entire
measurement.
3 “Reset” button
This button is used to reset any error messages displayed ob
the PC.
— 20 SPECTROTEST — 05.12.2017
Initial start-up
6 Initial start-up
6.1 Preparing the instrument for use

Information
Use only the power cable supplied with the instrument.
Before switching on the instrument, proceed as follows:

1. Arrest the instrument using the roller brakes.
2. Connect the argon supply hose to the connector jack on the back side of the
instrument (no argon is required for arc discharge).
 Ensure to latch the quick-release fastener properly.
3. Set the argon pressure to 5 bar ±10%.
 The instrument is ready for use.
6.2 Switching on the instrument

To switch on the unit, proceed as follows:
1. Press the "Power" button and keep it pressed for approx. 2 seconds.
 The unit is switched on.
 The computer is turned on.
 The most recently used application program is started.
 Depending on the sample probe that is used, the system is flushed with
argon for 5 or 15 minutes. If the arc program with carbon analysis is
loaded, the system is flushed with purified air for 15 seconds.
2. Wait for the argon flushing process to be completed.
 The flushing progress is displayed on the screen.
3. To switch on the plasma generator, press the switch:
 The sample probe status display lights up green.

 The unit is now ready to measure.
SPECTROTEST — 05.12.2017 — 21
Initial start-up
6.3 Standby mode

The stand-by mode is only possible with mains power supply. In the case of
battery power supply, the unit will be switched off completely.
1. Connect the unit to the mains power supply.
2. To switch off the plasma generator, press the switch:
3. Select the dialog item "Shut down" and confirm the dialog box.
 The program is terminated.
 The computer is turned off.
 The unit is switched off.
4. Close the argon bottle.
 The unit is in the stand-by mode.
6.4 Switching off the instrument

To switch off the unit, proceed as follows:
1. Select the dialog item "Shut down" and confirm the dialog box.
 The program is terminated.
 The computer is turned off.
 The unit is switched off.
2. Close the argon bottle.
3. Unplug the mains power plug. The unit is only completely disconnected from
power if the power plug is unplugged.
 The unit is now switched off.
— 22 SPECTROTEST — 05.12.2017
Initial start-up
6.5 Measuring procedure

The arc on the spark stand generates UV radiation. UV radiation may cause
damage to the eyes or skin.
 Use the appropriate sample adapter for samples that are not completely
covered by the spark stand opening.
 Take appropriate protective measures (e.g. wear safety goggles) when the
spark stand or the adapter openings are not fully covered.
Warning! Risk of electrical shock!

If the instrument is switched on, there is an inherent risk of electric shock from the
electrode and the sample. This can happen if contact with the test probe adapter
is lost during the measuring procedure.
For a healthy person, this electric shock is of no concern. These are low currents
and voltages which are below the limit values of EN 61010. However, a shock
may cause a subsequent accident, e.g. a fall from a ladder.
 Therefore, make sure that the sample never loses contact with the test probe
adapter during the analysis.
SPECTROTEST — 05.12.2017 — 23
Initial start-up
6.5.1 Preparing the measuring procedure

Before starting the measurement, proceed as follows:
1. Check the adapter and the sample for moisture.
 It is important that no moisture is visible on the outside.
 If necessary, dry the sample.
2. Check if the adapter is clean.
3. If necessary, prepare the sample surface by grinding, milling, etc.
4. Ensure that the correct sample probe, electrode, and adapter are installed.
 The measurement will be blocked if a wrong sample probe/testing
program combination is used.
 Change the sample probe.
5. Check the safety measures if you work with toxic samples.
 The measurement is now prepared.
— 24 SPECTROTEST — 05.12.2017
Initial start-up
6.5.2 Proceed with the measurement
Sample measurement, analysis

To perform a measurement, proceed as follows:
1. Start an analysis program via "Application profiles" or via the corresponding
function key.
2. Hold the test probe (adapter) onto the sample. If you use an application profile
for a spark method, ensure that the sample covers the opening of the adapter
completely.
3. Press and hold the "Start Measurement" key for the entire duration of the
measurement.
 The measurement is fully automated. The progress is displayed in the
measurement window.
 The measurement is finished automatically.
 During the measurement, the red status indicator of the test probe
flashes.
 When the measurement is finished, the status indicator of the test probe
turns green.
 If necessary, the measuring device prompts you to perform an
ICAL-standardization, see page 27.
 The measurement results are displayed on the screen.
 The measurement is complete.
SPECTROTEST — 05.12.2017 — 25
Initial start-up
Example measurement, Sorting

To perform a measurement, proceed as follows:
1. Start a sorting program via "Application profiles" or via the corresponding
function key and follow the software instructions.
2. Measure the reference sample first.
 Hold the test probe (adapter) onto the sample.
 Follow the instructions displayed by the software.
 Press and hold the "Start Measurement" key for the entire duration of the
measurement.
 The measurement is fully automated. The progress is displayed in
the measurement window.
 The measurement is finished automatically.
 During the measurement, the red status indicator of the test probe
flashes.
 When the first measurement is finished, the status indicator of the
test probe turns green.
 If a measurement result is poor, the status indicator of the test probe
lights up red and the measurement must be repeated.
 When the minimum number of good measurements is reached, the
counter for good samples is incremented by one point (this depends on
the program settings).
3. Now, measure the sample to be checked.
 If the measurement result is good, the counter for good samples is
increased by one point on the screen. Now, the next sample can be
measured.
 If the measurement result is poor, the counter for poor samples is
increased by one point on the screen
 Depending on the program settings, two repeat measurements must
be carried out. If these measurement results are also poor, the
counter for poor samples is increased by one point on the screen.
 Now, the next sample can be measured.
 The measurement is complete.
— 26 SPECTROTEST — 05.12.2017
Initial start-up
ICALization of the measuring instrument (ICAL)

For the ICALization, the ICAL sample must be measured 5 times. The average
values of these measurement results are calculated and stored in the instrument.
In order to standardize the instrument, proceed as follows:
1. Place a clean rod electrode in the sample probe, see page 30 (in arc mode:
silver electrode).
2. Call up the ICAL function with the "ICAL" button or with the corresponding
function key.
3. Follow the instructions on the screen and perform the necessary 5
measurements with the reference sample.
4. Poor measurements are highlighted in the ICAL measurement window and
can be deleted. Please repeat the respective measurements.
 The instrument is ICALized.
SPECTROTEST — 05.12.2017 — 27
Initial start-up
6.6 Replacing parts of sample probe
Caution! Risk of burns!

6.6.1 General arrangement of test probe parts
Fig. 6
No. Display
1 Adapter
 In the illustration on the left-hand side is the adapter for the arc excitation
 In the illustration on the right-hand side is the adapter for the arc excitation
2 Knurled screw for the adapter
3 Test probe
 In the illustration on the left-hand side is the standard test probe for the
arc/spark excitation
 In the illustration on the right-hand side is the test probe for the arc/spark
excitation incl. UV optics
4 Electrode
5 Holder for light-sensitive surface, air optics
6 Locking wheel for the electrode
7 Air filter
— 28 SPECTROTEST — 05.12.2017
Initial start-up
6.6.2 Changing the sample probe

To change the sample probe, proceed as follows:
2. Open the sample probe connector clamp.

3. Disconnect the connector from the sample probe.
4. Plug in the new sample probe and close the clamp again.
 When plugging in the new sample probe, ensure that the brass plugs for
the fiber-optics and the argon supply are located on the right-hand side.
6. Standardize the unit, see page 27.

 The sample probe has been changed and the unit has been set to the new
conditions.
6.6.3 Changing the adapter

Changing the adapter is necessary when another type of discharge (arc or spark)
is required. This also requires changing the electrode.
To change the adapter, proceed as follows:
2. Loosen the knurled screw of the adapter.

3. Pull out the adapter.
4. Change the electrode, see page 21.
5. Plug in the new adapter.
 The spark discharge adapter is sealed with an O-ring.
 Press the adapter beyond the resistance.
 The adapter must make contact over its entire surface.
 On the arc discharge adapter, the opening must point towards the fiber-
optics.
6. Fix the adapter in place using the knurled screw.
 The adapter has now been changed.
SPECTROTEST — 05.12.2017 — 29
Initial start-up
6.6.4 Changing the electrode

The arc excitation uses silver or copper electrodes, while the spark excitation uses
only tungsten electrodes.
To replace the electrode, proceed as follows:
1. To switch the plasma generator off, press the following switch:
2. Use the knurled screw to loosen the adapter.

3. Pull out the adapter.
4. Loosen the electrode on the locking wheel.
 Notice! A spring is located underneath the electrode. The electrode can
drop out when loosening the locking wheel. Hold the electrode with a pair
of pliers as you loosen and remove the electrode.
5. Pull out the electrode.
6. Insert the new electrode.
7. Install the adapter. Use the knurled screw to fasten the adapter.
8. Use the spacer to set the gap of

the electrode.
 Press the spacer (1) onto
the adapter (2). The
electrode is pushed to its
correct position.
Fig. 7
9. Use the locking wheel to fasten the electrode in place.
10. To switch the plasma generator on, press the following switch:
 The electrode has been replaced.
— 30 SPECTROTEST — 05.12.2017
Maintenance
7 Maintenance
Information
In order to ensure the availability and operational safety of the equipment, we
recommend having the system checked for correct operation and performance at
least once per year by specialized technicians. To find contact addresses of
service organizations authorized by SPECTRO go to www.spectro.com
7.1 Maintenance schedule

The maintenance intervals specified in the following table are guidelines which
should be observed as a minimum requirement. The maintenance intervals may
vary, depending on the use of the instrument.
To ensure the flawless function of the instrument, proceed with the following
maintenance tasks:
After every measurement Necessary tasks
Cleaning the electrode Clean the electrode with a small wire brush.
Start of work Necessary tasks
Checking the argon supply Min. pressure in bottle: 10 bar.
Cleaning the adapter See page 32.
Checking the focal spot Visual inspection
ICALization See page 27.
As required
Cleaning the windows of the sample probe See page 32.

and of the adapter
Cleaning the air filter (housing) Every month or more often if necessary See
page 34.
Replacing the air filter (sample probe) Every month or more often if necessary See
page 35.
Fine dust filter unit Replace every six months or more

frequently if necessary (the system will
display a message) See page 36.
CO2 filter unit Replace every six months or more

frequently if necessary (the system will
display a message) See page 36
SPECTROTEST — 05.12.2017 — 31
Maintenance
Further maintenance tasks
Replacing the ICALization sample
Checking the wheels and brakes of the

transport carriage
7.2 Cleaning the adapter

During the measurements, the adapter gets soiled.
After completing work, clean the adapter on the inside and outside, using a cloth
free of lint, oil and grease. Commercially available cotton swabs are also useful for
cleaning.
7.3 Cleaning the light inlet windows of the sample probe and of
the adapter
Touch the sample only after it has sufficiently cooled.
To clean the light-sensitive surface, proceed as follows:

2. Use the knurled screw (2) to

loosen the adapter (1) and pull
out the adapter.
 Use a cotton swab to clean
the light-sensitive surface in
the test probe (3).
Fig. 8
— 32 SPECTROTEST — 05.12.2017
Maintenance
3. Hold the adapter and carefully

slide the window retainer (1) out
of the guide.
Fig. 9
4. Remove the light-sensitive

surface (1) and the exposed O-
ring.
 Direct contact with the
optical surfaces must be
avoided.
 The UV probe (right-hand
side) uses two light-
sensitive surfaces, both
must be cleaned.
5. Clean the light-sensitive surface
using optical paper or a lint-free
soft cloth.
Fig. 10
6. Reinstall the light-sensitive surface (two light-sensitive surfaces for the UV
probe).
 Make sure that the O-rings are correctly positioned under the light-
sensitive surface.
7. Reinstall the adapter to the test probe.
8. To switch the plasma generator on, press the following switch:
 The cleaning of the light-sensitive surfaces on the probe and adapter is

completed.
SPECTROTEST — 05.12.2017 — 33
Maintenance
7.4 Replacing the air filter

Change the air filters monthly (more frequently if necessary).
To replace the air filter, proceed as follows:
1. Disconnect the instrument from the power supply (see page 22).
2. Release the "unit/transport

carriage" locking mechanism
and take the instrument off the
transport carriage.
Fig. 11
3. Loosen the knurled screws.
Fig. 12
4. Lower the base plate (2).
5. Remove the clogged filter (1).
Fig. 13
6. Insert the new filter.
— 34 SPECTROTEST — 05.12.2017
Maintenance
 Ensure that the filter is aligned correctly and that it is properly seated.
The recess in the filter mat must be above the connector in the base
plate.
7. Raise the base plate and use the knurled screws to secure it.
8. Place the instrument back on the transport carriage and use the locking
mechanism to secure it.
 The air filter has been changed.
7.5 Replacing the sample probe air filter

To replace the filter, proceed as follows:
2. Separate the sample probe from the instrument.

 Open the sample probe connector clamp.
 Disconnect the connector from the sample probe.
3. Loosen the screws (1).

4. Remove the cover (2).
5. Replace the filter.
6. Reinstall the cover (2).
7. Tighten the screws.
Fig. 14
 The air filter has been changed.
SPECTROTEST — 05.12.2017 — 35
Maintenance
7.6 Replacing the CO2 and fine dust filter unit

Warning! Risk of injury and health hazard!
The CO2 filter unit (optional) contains chemicals.
 The applicable safety data sheet is available at
http://www.spectro.com/msds.
 Protective gloves and goggles must be worn when replacing the filter unit.
 When disposing of the filter unit, compliance with legal regulations is
mandatory.
To replace the filter, proceed as follows:

1. Switch the instrument off (see page 22)
2. Release the "unit/transport

carriage" locking mechanism
and take the instrument off the
transport carriage.
Fig. 15
3. Loosen the knurled screws.
Fig. 16
— 36 SPECTROTEST — 05.12.2017
Maintenance
4. Lower the base plate (1).
Fig. 17
5. Unscrew the CO2 filter unit (1)
and the fine dust filter unit (2)
and replace them.
Fig. 18
6. Raise the base plate and use the knurled screws to secure it.
7. Place the instrument back on the transport carriage and use the locking
mechanism to secure it.
 The CO2 filter unit and the fine dust filter unit have been changed.
7.7 Cleaning/sharpening the electrodes

Clean the electrodes after the completion of the tasks.

The "soft" rod electrodes (silver and copper) must be resharpened when their tips
are worn.
SPECTROTEST — 05.12.2017 — 37
Troubleshooting
8 Troubleshooting
Improperly performed repairs may damage the instrument.
 Do not repair the instrument yourself. Always notify your immediate
supervisor or contact your Service Center.
Fault Possible cause Remedy
The unit cannot be The mains power supply Check if the mains power supply
switched on plug is not properly plug was properly plugged in.
(The computer does not plugged in.
boot) The battery does not have Check whether the drawer with
proper contact with the the storage battery is properly
contact plate of the unit. seated.
The battery is not charged. Charge the battery as described

in the separate instruction
manual.
A computer component or Please contact your service

another subassembly center.
connected with it is
defective.
The unit can be switched Defective cable or display. Please contact your service
on, but no data are center.
shown on the display.
The software reacts A virus scanner has been Add the directory "C:\Spectro
slowly (e.g. long installed. Smart Studio\Spark Analyzer Pro
measuring times) Mobile" or the processes
"TXC03MeasurementGUI.exe"
and "TXC03MethDevGUI.exe" to
the exceptions that should not be
scanned.
The keyboard does not Defective cable or Please contact your service
react. keyboard. center.
The trackball does not The trackball surface is Clean the trackball surface.
move freely and/or it soiled.
does not trigger any
movements on the Defective cable or Please contact your service
screen. trackball. center.
— 38 SPECTROTEST — 05.12.2017
Troubleshooting
No correct focal spot in The pressure controller on See the error message in the
the spark mode. the gas cylinder is not software status line.
open wide enough. Adjust the required pressure.
The pressure monitor and Please contact your service

the flow controller inside center.
the unit are not properly
adjusted any more.
The argon supply line Let the quick-release coupling

quick-release coupling is lock properly.
not properly locked on the
unit.
The adapter is not locked Check whether the adapter is

in properly up to the stop. properly seated and correct it if
necessary.
The electrode gap is not Adjust the electrode gap using

correct. the spacer.
The sample surface has Prepare the surface to be tested

not been properly in a suitable way with the aid of
prepared (not polished, abrasive paper (disk sander or
observe roughness). hand sander).
The sample surface is not Prepare the surface to be tested

flat enough or it has air in a suitable way with the aid of
inclusions. abrasive paper (disk sander or
hand sander).
The argon outlet (exhaust) Flush it with the aid of the "Flush"
of the sample probe is function.
plugged with condensate. While flushing, close the sample
opening of the adapter and close
the exhaust for approx. 1 second,
then open it.
Insufficient maintenance Clean the adapter thoroughly.

(cleaning) of the adapter,
especially of the Teflon
insert, has caused
clogging of the flushing
bores.
SPECTROTEST — 05.12.2017 — 39
Troubleshooting
The unit does not The measuring window of Press "Esc" or click the
generate sparks in the the software has a "not measuring window with the left
arc or spark mode. active" status in Windows. "mouse button" of the trackball.
The electrode gap is too Clean the electrode and re-adjust

small. the gap using the spacer.
The sample probe start Please contact your service

button is defective. center.
The plasma generator  Have the former settings

parameters of the program restored by qualified
that is used were modified personnel.
or deleted.  Please contact your service
center.
The plasma generator is Please contact your service

defective. center.
The actual values are The adapter is reversed in Turn the adapter so that one
below the stored limit the arc mode. opening faces the fiber-optics
values for the reference window.
elements (error
message). The spark (arc) adapter is Check whether the adapter is
not locked in properly up properly seated and correct it if
to the stop. necessary.
The electrode gap is not Adjust the electrode gap using

correct. the spacer.
The samples have not See the information given under

been properly prepared. “No correct focal spot in the spark
mode”.
The material was not Go to the suitable global program

measured with a program if available (e.g. to Co-01)
associated with the base
(e.g. Co sample with a Fe
base program).
— 40 SPECTROTEST — 05.12.2017
Spare parts and consumables
9 Spare parts and consumables

You can find the spare parts and consumables for this instrument under "Support -
Parts Catalogue" (Service – Parts Catalogue) on our website at www.spectro.com.
Use only genuine spare parts for repairing the instrument. The use of non-genuine
spare parts will make the CE Declaration of Conformity null and void. Excepted
are spare parts from manufacturers approved by SPECTRO.
Only the use of genuine spare parts and consumables ensures the safe operation
and achievement of the specified output.
10 De-commissioning
Only organizations or persons authorized by the instrument manufacturer shall be
permitted to de-commission the instrument. Please contact your Service Center.
11 Manufacturer address
SPECTRO Analytical Instruments GmbH
Boschstr. 10
D-47533 Kleve
Germany
Tel.: +49.2821.8 92-0
Fax: +49.2821.8 92-22 00
http://www.spectro.com
SPECTROTEST — 05.12.2017 — 41

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Mobile Spectrometer for

Original operating instructions

6 Initial start-up .................................................................................................... 21

9 Spare parts and consumables .......................................................................... 41

11 Manufacturer address ...................................................................................... 41

1.3.1 Connections (rear)

No. Component No. Component

2 HDMI 5 Argon connection

No. Component No. Component

1 Housing (spectrometer) 9 Test probe

2 Screen 10 Locking device for transport

3 Storage compartment 11 Roller brake

4 Test probe support 12 Argon bottle retaining strap

5 Transport carriage (can be 13 Type plate

6 Adapter 14 Air filter

7 Sample probe connection 15 CO2 and fine dust filter (behind

8 Drawer for optional rechargeable 16  Power supply connection

2.1 Symbols used

Warning! Risk of injury!

Warning! Risk of electric shock!

Warning! Risk of burns!

Warning! Danger of poisoning!

2.2 User information

2.3 Intended use

2.4 Prohibited operating conditions

2.5 Residual risks

Warning! Risk of injury and health hazard!

Warning! Danger of poisoning!

Warning! Risk of electrical shock!

Warning! Risk of burns!

High-voltage High-voltage Burning voltage Burning voltage

Spectro test 6 - 12 KV, 1 - 12 KV, 30 - 60 V, 20 - 200 V,

 When the instrument is switched on, there is an inherent risk of an electrical

Power supply 100 - 240 V, ±10%, 50/60 Hz (compliant with DIN EN

Power during test 320 W

Power during stand-by 60 W

Power supply fuses 16 A (slow-blow)

Storage conditions -20 – 50°C; -5 – 120°F,

Permissible ambient 5 – 40 °C; 40 – 105 °F

Argon gas connection

 Inlet pressure 5 bar ±10%; 72 psi

 Quality ≥ 4.8 (99.998 %)

 Consumption of standard Constant flow: 15 L/h

 UV probe consumption Constant flow: 15 L/h plus 10 L/h UV optics

Protection class IP 23 (DIN 40050)

Warning! Risk of injury!

Notice! Damage to instrument!

Notice! Damage to instrument!

Information! Measurement errors!

4.2 Dimensions and weight

Unit height 670 mm (26.3’’)

Unit width 425 mm (16.7’’)

Unit depth 330 mm (13.0’’)

Unit weight 33 kg (72.7 lbs)

4.3 Gas supply (sparks operating mode)

The spectrometer requires an argon supply line.

4.3.1 Argon bottle fastening

No. Component No. Component

1 Installation of the retaining strap 2 Installation of the retaining strap

5.1 General arrangement of display and buttons

No. Control element Function

1 Switch Switches the instrument on.