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PhamVan Eight erlenmeyer flasks were dried and cleaned.

Four 100 ml erlenmeyer flasks were


numbered 1 to 4 to carry out the adsorption process. Four 100 ml regular conical flasks were numbered
from 1’ to 4’ to carry out the post-adsorption process. Four activated carbon filter paper glass funnels
were prepared. A 25ml buret were filled with butylic alcohol of different concentrations. Butylic alcohol
solution were knowned concentration 0.1; 0.2 ; 0.3 ; 0.4M. Four triangle flasks were filled with activated
carbon and 25ml of solution with the above concentration was added to each flask. Working principle of
surface tension measuring device (Figure 4). During the measurement process, the temperature must be
stable. Before measuring, check the button and the locking pipes to ensure tightness The temperature
were stabilized open the lock slowly so that the water in the pressure reducing tank flows into the cup.
Then the pressure in the system is smaller than the outside pressure. The pressure difference were
reflected by the height h of manomet. It takes about 10 to 20 seconds for an air bubble to escape. When
an air bubble escapes from the capillary, h has the largest value. Record that value. The height h were
determined in nanometers based on the following relationships :

Draw a graph of the relationship "h-C" . On the other hand, to determine the adsorption rate, you only
need to know the concentration before and after adsorption and then apply the formulas :

Four triangle flasks (1 to 4) were filled with activated carbon and 25ml of solution with the above
concentration was added to each flask. Shake with a shaker to speed up the adsorption and let it adsorb for
about 60 minutes. Measure the value of distilled water and four values h of four concentration solutions
per volume of distilled water and each solution needs to be the same so that the measurement status of the
samples is nearly the same. Measure the h value corresponding to the solution in flasks 1' to 4'. The
measurement sequence of dilution before concentration and then .h was obtained and used to determine
inference from the standard curve graph “h-C”

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