クボタ　HIP　CH701 CH702 CH713 ENG

1
Corporate Data
( as of March 31, 2010)
Established February 1890
Employees Consolidated 24,778
( Non-Consolidated 9,379)
Capital ¥84,070 million
(US$ 989million / EURO 764million)
Consolidated Net Sales ¥930,600 million
(US$10,948million / EURO 8,460million)
Net Sales ¥450,400 million
(US$5,299million / EURO 4,095million)
* Currency Exchange Rate

¥85/US$ & ¥110/EURO
2
Air Condition Equip. Div.
3
Social Infrastructure
Consolidated Div.
Vending machinery Div.

Electronic Equipped Machinery Div.
Material R&D Dept.
Steel Pipe Div. Ceramics Mfg. Dept.
Material Div. Steel Castings & Roll Mfg. Dept.
KUBOTA Corporation
Johkasou Business Unit

Water&Environment Systems
Consolidated Div.
Water Engineering & Solution Div. Membrane Systems Business Unit

Water & Sewage Engineering
Pumps Div. Business Unit
Pipe Systems Div. Industrial Materials Business Unit
Valves Business Unit
Ductile Iron Pipe Business Unit
Farm & Industrial Machinery
Others
Recycling Equipment Business Unit
Consolidated Div.
Construction Machinery Div.

Engine Div.
Farm Machinery Div.
Tractor Div.
4
Consolidated Div.

Material R&D Dept.
KUBOTA Corporation

Consolidated Div.

Others
Consolidated Div.

Engine Div.
Farm Machinery Div.
Tractor Div.
Consolidated Div.
TRACTOR
Mini-Excavator Engine
Combine Harvester
5
6
Consolidated Div.

Material R&D Dept.
KUBOTA Corporation

Consolidated Div.

Others
Consolidated Div.

Engine Div.
Farm Machinery Div.
Tractor Div.
Water & Environment Systems
Consolidated Div.
Pump
Ductile Iron Pipes
Valve
7
Water & Environment Systems
Consolidated Div.
Sewage Treatment Plant Sewage Sludge Incinerator
Ceramic Membrane filtration System 8

9
Consolidated Div.

Material R&D Dept.
KUBOTA Corporation

Consolidated Div.

Others
Consolidated Div.

Engine Div.
Farm Machinery Div.
Tractor Div.
Consolidated Div.
Cracking Coils
for petrochemical Industry
Column
Steel Pipe
Pile Vending Machines Air Conditioning Equip. 10

Ceramic
11
HIP &
Consolidated Div.

s

Material R&D Dept.
KUBOTA Corporation

Consolidated Div.

Others
Consolidated Div.

Engine Div.
Farm Machinery Div.
Tractor Div.
-Product 5- Ceramics and HIP Cylinder
Ceramics thermocouple Ceramics Parts for Pump and Valve

protection tube
HIP Cylinder & Screw for

Injection & Extrusion machine
12
Steel Castings Business
Manufacturing Plant of Steel Castings Business
Hirakata Plant Kubota Metal Corp. Jingsu Baoxin Kubota

(Japan) (Canada) Kubota Industrial Saudi Arabia
(China) (Saudi Arabia)
Territory : Territory :
Asia North America Territory : Territory :
Russia South America China Middle East
Europe Africa
13
Organization Material Div.
Ceramics Mfg. Dept. Amagasaki Sales Dept.
Plant Osaka, Tokyo
Hirakata Plant
Material R&D Dept.
Steel Castings Mfg. Dept Planning & Control Dept.

Management Plan
Affiliates Control
Accounting
Manufacturing Production Maintenance Quality Engineering

Sec. Planning Sec. Sec. Assurance Sec. Gr.
Manufacturing Purchasing Maintenance Quality Design

Assurance
Production Production Safety Control
Control Planning Quality Field Service
Control
Quotation
14
Steel Casting
Manufacturing Plant.
( as of April , 2010)
【Business】
Manufacturing with Centrifugal Castings
and Static Castings (Ceramics and HIP Cylinder)
Desining, Reserch & Development and Field Services
【 Workforces】
Plant Manager Mr. Kenji Kobiki
Employee 300
Plant Area 85,000 ㎡ Building 33,000 ㎡
15
Plant History
1937 （S12) Started Producing Steel Castings by Static Casting Process
1952 （S27） Successfully Developed First Centrifugal Castings in Japan
Started Industrial Production of Centrifugal Castings
1962 （S37） Moved to Hirakata City for Plant Expansion
1969 （S44） Development and Production of G-Column was Officially Awarded
1978 （S53） Developed G-Piles and Started its Marketing
1979 （S54） Completed Closed system lines for Frun Static Casting Process
1992 （H 4） Invested New Casting and Machining Line for G-Columns & Piles
2002 （H14） Completed New Production System and Layout
2007 （H19） 70 Years Anniversary for Steel Casting Division
16
To contents
Kubota HIP Materials Sub-contents
About HIP
About each Kubota’s material
Comparison with general materials

(contain of high Cr casting iron)
Comparison with other company’s materials

W&P Cyl W&P Skr
About Kubota’s materials for each resin
17
About HIP
Kubota Corporation
Material Consolidated Div.
New Consolidated material Dep.
18
About HIP
HIP:the abbreviation of Hot Isostatic Pressing

HIP is
a technology of isotropic compression and compacting of objective
material by use of high-temperature and high-pressure gas.
Properties of HIP
■ Flexibility of Alloy Design
■ Homogeneous and Fine Microstructure
■ Composite Structure by Solid State Bonding
■ High-density Materials
■ Near-net-shape
19
HIP Equipment
Vessel Size Max. Temperature 1300℃
Φ600*1600H Max. Pressure 200Mpa
Pressure Gas Pressure
Medium (Ar) Vessel
Heater
Work Piece
Schematic Diagram of HIP Equipment HIP Equipment of KUBOTA

20
Comparison of properties
HIP Centrifugal Casting Spray Overlay
Micro Size Fine Coarse Fine Coarse

-
Struct Homogen- Good Bad (segregation) Bad (segregation) Bad ( segregation )
ure eity
Pore Perfect (no pore) Imperfect Porous Imperfect
Dispersed Homogeneous (Out-) segregate Segregate Segregate

Phase
(Hard
particles)
No limitations Small size Small size
Shape limitations Complicated shape is OK Simple shape only
impossible impossible
Solid state Solid phase-liquid Liquid state

phase bonding Physical joint
Bonding bonding bonding
Higher bonding Dilution from Weakly bonding Dilution from

strength the outer layer strength the outer layer
Alloy design Free Limited Limited Limited
21
Kubota HIP Materials for
Cylinder
Alloy Composition HRc W.R C.R Application
CH101 Ni-Base 56-60 2 3
CH201 Ni-Base 58-63 3 3 With glass fiber
CH202 Ni-Base+Ceramics 60-65 4 3 Kneading zone
CH401 Co-Base 56-61 3 4 PPS+GF
CH402 Co-Base+Ceramics 59-64 4 4 PPS+GF
CH501 Ni-Base 40-45 1 5++ Fluoric resins
CH601 Fe-Base 63-67 5+ 1 Plastic magnet
CH701 Co-Base 54-59 2 5 Large Size,PVC
CH702 Co-Base+Ceramics 58-62 4 4 PVC,PPS
Kubota
W.R.:Wear Resistance C.R.:Corrosion Resistance 22
Cylinder
CH101 Ni-Base 56-60 2 3
Kubota
To contents
To material
contents
next
back
Kubota HIP Materials for Cylinder

good To table
CH601 CH713
Wear resistance
CH702
CH202 CH402
CH201 CH401
CH101 CH701
CH502
N.S.:
N.S. CH501 Nitriding steel
good
Corrosion resistance 24
Characteristic of CH700
CH702, CH713 HIP’ed
Material for Barrel
Kubota Corporation
New Materials & Development Sales Group
Material Sales Dept.
Sep.2011
25
Introduction
CH700 series are superior corrosion resistant materials
for plastic machines. These materials can be used at all
conditions –needed for high toughness ,needed for high
wear resistant.
Corrosion resistance
High toughness Wear resistance
CH701 CH702 CH713
High toughness use: large cylinder,

section suffered high torque or large load
Wear resistance use: adding a lot of GF, kneading zone

26
Cylinder
CH101 Ni-Base 56-60 2 3
Kubota
High Toughness Material:CH701
Any problems - inner clack etc, were happened
in large inner diameter cylinder. Because of large load
It is necessary wear & corrosion resistant material with high toughness.
CH701
28
Test Condition
Ring
Crack Resistance Test
(Screw)
Ring: AISI D2/JIS SKD11

Plate:Test Materials
Test Velocity:0.5m/s
Load:100,200,260kgf
Ｐ Plate Estimation: No Crack(PT)
(Cylinder)
Wear Test ,Bending Test
29
Results of Test (1)
Good Bad
○ ×
30
Results of Test (2)
25
20 Test piece
Results of Crack Resistance Test

15
Load Ring
Alloy 10
100kgf 200kgf 260kgf
CH701 ○ ○ ○ 5
CH201 × × × 0
CH701 CH201 ST12
ST12 ○ ○ ○
Results of Wear Test
Ring Material :ASTM52100(HRC60) JIS-SUJ-2
Test Velocity :1.90m/s
Test Length :400m
Load :60N
31
Specimens
Alloy Composition/note HRc Process Application/note

CH701 Co-Base 54-59 HIP Large Size,PVC
CH702 Co-Base+Ceramics 58-62 HIP PVC,PPS
CH713 Co-Base+Ceramics 61-66 HIP PVC,PPS
CH201 Ni-Base 58-63 HIP With glass fiber
N.S. Nitraiding Steel 54-59 Casting
SKD AISI D2/JIS SKD11 58-62 Casting
H.C.C High Cr Cast Iron 61-66 Casting
ST12 Stellite#12 50-55 Welding
32
Comparison of Property(2)
Result of Bending Test
3000
2500
Bending Strength (MPa)
2000
1500
1000
500
0
CH701 CH702 CH713 CH201 NitraidingSKD11 High Cr St12
Steel D2 Cast Iron
33
Result of Wear Test
40
Ring Material :ASTM52100(HRC60)
Specific Wear rate (X10-9 mm2/N)
35 JIS-SUJ-2
30 Test Length :400m
15 Load :60N
Test piece
10
Ring
5
0
Steel D2 Cast Iron
34
Test Condition
・Wear Test
・Bending Test
・Corrosion Test
Solution Concentration Temperature Time
HCl(Hydrochloric Acid) 20wt% 50℃(323K) 48hr
HBr(Hydrobromic Acid) 10wt% 50℃(323K) 48hr
HF(Hydrofluoric Acid) 10wt% 50℃(323K) 48hr
Acrylic Acid 30wt% 40℃(313K) 168hr
35
Result of HCl Corrosion Test
800
400
Corrosion rate (g/m2/hr)
Solution:20wt%HCl
Temp.:323K
40
20
0
Steel D2 Cast Iron
36
Result of HBr Corrosion Test
100
Solution:10wt%HBr
10 Temp.:323K
0.1
0.01

Steel D2 Cast Iron
37
Result of HF Corrosion Test
800
Solution:10wt%HF
400 Temp.:323K
40
30
20
10
0.7 0.8
0
Steel D2 Cast Iron
38
Result of Acrylic Acid Corrosion Test
4
Solution:30wt%CH2CHCOOH
2 Temp.:313K
0.4
0.3
0.2
0.1
0.01 0.02 0.04 0.01
0.0
Steel D2 Cast Iron
39
Conclusion of CH700
Wear Corrosion Resistance Feature of CH700

Alloy High Toughness
Resistance HCl HBr HF Acrylic Acid
High Corrosion
CH701 2+ 5 4 4 5
Resistance
CH702 5 5 4 3 5 (HCl,HBr,-COOH)
CH713 5++ 5 4 3 5 High Wear Resistance
CH201 3 3 3 4 3
Application Of CH700
N.S. 1 1 1 1 1
Large Size
SKD 3 1 1 1 1 PVC
H.C.C 3 1 1 1 1 PPS+GF
ST12 2 3 3 2 5
40
Characteristic comparison of WC
content various materials
Item Material Method
A CH713 HIP
Ni-Base alloy + WC(Large

B Casting
particle)
Ni-Base alloy + WC(Small Sinteri
C
particle) ng
41
WC Particle(Hv2000)
Matrix(HRC50)
Soft Matrix than CH713 matrix
B Melt method with WC Wear out preferentially
Matrix : Powder metallurgy Fine small

WC particles.
Good wear and

abrasion resistance
WC Particle(Hv2000)
A Hip'ed CH713
42
Hardness and Bending Test
Hardness Bending Strength
62 1800
60 1600
B e n din g Stre n gth (MPa)

1400
58
Hardness(HRC)
1200
56
1000
54 800
600
52
400
50
200
48 0
CH713 CH702 A B CH713 CH702 A B
43
Result of Wear Test
Specific Wear rate Ring Material :ASTM52100
(HRC60)
1.6 JIS-SUJ-2
Specific Wear rate (X10-9 mm2/N)
1.4 Test Length :400m

Load :60N
1.2 Test piece
1
Ring
0.8
0.6
0.4
0.2
0
CH713 CH702 A B
44
Result of HCl and HBr Corrosion Test
Solution:20wt%HCl Solution:10wt%HBr
Temp.:323K Temp.:323K
0.9 1.8
0.8 1.6
T h e r e l at i ve c o m par i so n o f C H2 0 1
0.7 1.4
The rel a ti v e com pa ri s on of CH 201
0.6 1.2
0.5 1
0.4 0.8
0.3 0.6
0.2 0.4
0.1 0.2
0 0
CH713 CH702 A B CH713 CH702 A B
45
メインフィード
TEX65α（４号機）
ノーマルベントノーマルノーマルＳＦ／Ｖベントノーマルノーマルノーマル
KUBOTA CH702
C10 C9 C8 C7 C6 C5 C4 C3 C2 C1
予備品の準備が必要なバレル取替え検討が必要なバレル
Closed Barrel (Ni Base Casting material)
Top end Barrel (Ni Base Casting material) Side feed Barrel (Ni Base Casting material)
46

クボタ HIP CH701 CH702 CH713 ENG

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1

* Currency Exchange Rate

Vending machinery Div.

Johkasou Business Unit

Water Engineering & Solution Div. Membrane Systems Business Unit

Construction Machinery Div.

Vending machinery Div.

Johkasou Business Unit

Water Engineering & Solution Div. Membrane Systems Business Unit

Construction Machinery Div.

Vending machinery Div.

Johkasou Business Unit

Water Engineering & Solution Div. Membrane Systems Business Unit

Construction Machinery Div.

Ductile Iron Pipes

Sewage Treatment Plant Sewage Sludge Incinerator

Ceramic Membrane filtration System 8

Vending machinery Div.

Johkasou Business Unit

Water Engineering & Solution Div. Membrane Systems Business Unit

Construction Machinery Div.

Pile Vending Machines Air Conditioning Equip. 10

Vending machinery Div.

Electronic Equipped Machinery Div.

Johkasou Business Unit

Water Engineering & Solution Div. Membrane Systems Business Unit

Construction Machinery Div.

Ceramics thermocouple Ceramics Parts for Pump and Valve

HIP Cylinder & Screw for

Hirakata Plant Kubota Metal Corp. Jingsu Baoxin Kubota

Steel Castings Mfg. Dept Planning & Control Dept.

Manufacturing Production Maintenance Quality Engineering

Manufacturing Purchasing Maintenance Quality Design

Kubota HIP Materials Sub-contents

About each Kubota’s material

Comparison with general materials

Comparison with other company’s materials

About Kubota’s materials for each resin

HIP:the abbreviation of Hot Isostatic Pressing

Schematic Diagram of HIP Equipment HIP Equipment of KUBOTA

HIP Centrifugal Casting Spray Overlay

Micro Size Fine Coarse Fine Coarse

Dispersed Homogeneous (Out-) segregate Segregate Segregate

Solid state Solid phase-liquid Liquid state

Higher bonding Dilution from Weakly bonding Dilution from

Alloy design Free Limited Limited Limited

Kubota HIP Materials for Cylinder

High toughness Wear resistance

CH701 CH702 CH713

High toughness use: large cylinder,

Wear resistance use: adding a lot of GF, kneading zone

It is necessary wear & corrosion resistant material with high toughness.

Ring: AISI D2/JIS SKD11

Wear Test ,Bending Test

Results of Crack Resistance Test

Alloy Composition/note HRc Process Application/note

CH701 CH702 CH713 CH201 NitraidingSKD11 High Cr St12

Wear Corrosion Resistance Feature of CH700

Item Material Method

Ni-Base alloy + WC(Large

B Melt method with WC Wear out preferentially

Matrix : Powder metallurgy Fine small

Good wear and

クボタ　HIP　CH701 CH702 CH713 ENG

クボタ　HIP　CH701 CH702 CH713 ENG