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Noncontacting Strain Measurements at High

Temperatures by the Digital Laser Speckle Technique


by M. Anwander, B. G. Zagar, B. Weiss and H. Weiss

ABSTRACT--This paper presents a newly developed laser- ferometer systems 9,10 In particular, for high-temperature ap-
based noncontacting strain sensor suitable for temperatures plications the following methods are most often described in
up to t200~ which was adapted to a comrnercial tensile the literature: the computer vision technique, electronic laser
testing machine equipped with an electrical furnace. The speckle interferometry (ESPI) and the digital laser speckle
principle of the strain sensor is based on tracking laser speck- correlation technique.
les through a digital correlation technique. Furthermore, the
Lr 11 used ESPI to measure in-plane deformation
description of the signal processing and the optical arrange-
ment is presented. Based on the experimental data, it can fields up to about 1500~ reporting problems with turbu-
be shown that this simple, laser-based strain sensor can be lence, changes in the microstructure of the specimen sur-
used successfully for the determination of mechanical and face, background radiation and mechanical stability. The
thermal strains up to temperatures of about 1200~ Using a thermal strain fields of metal ceramic compounds were de-
special data-processing procedure, it was feasible to minimize termined using digital speckle pattern interferometry up to
decorrelation effects caused by changes in the specimen sur- about 300~ In the framework of the joined European ac-
face due to, for example, slipband and microcrack formation, tion (COST Action 510), t2 both an ESPI system and a laser
surface oxidation and phase transformation and, thus, mea- speckle correlation-based system (to be described in this pa-
sure large mechanical strains. The strain resolution for the per) are being developed for applications in mechanical test-
selected setup was about 20 microstrains depending on the
ing at very high temperatures. Preliminary experimental re-
testing parameters.
sults are reported in Refs. 13 and 14.
KEY WORDS--Strain measurement, digital speckle correla- Speckle interferometric systems experience problems due
tion technique, thermal strain, large mechanical strain, high to the mechanical stability, in-plane and out-of-plane move-
test temperature ments, in practical realization of the determination of strain.
The computer vision technique introduced in Refs. 1, 15 and
24 to measure full-field in-plane surface deformation at tem-
In the field of mechanical testing of materials at elevated peratures up to 650~ based on the digital image correlation
temperatures, it is for various reasons desirable to determine technique seems to be an attractive method. However, as re-
mechanical and thermal strain values with noncontacting op- ported by the authors, this technique is limited until now to
tical methods. Both standard clip gages and strain gages are temperatures causing little self-radiation, since it uses white-
very limited in their operational temperature range, and even light images. In addition, precaution has to be taken to use
if applicable, they may cause local damage of the specimen a furnace window of high quality to prevent image distor-
surface or cause chemical surface reactions. tion, and the entire measuring system has to be placed on a
Most of the published optical systems aim for the deter- vibration-isolated optical table. The mechanical strain val-
mination of strain fields. A survey of the most commonly ues reported in Ref. 15 were determined in the elastic strain
used optical methods is given in Refs. 1-3 presenting their regime only. Coburn and Slevin 16 reported an automated
applicability, resolution and limitations. digital speckle system for the use of nondestructive testing
The best documented methods, which are used mostly for of ceramic specimens up to 600~ Their system is based
room temperature tests, are the holographic techniques,4 laser on the nonrecoverable loss of correlation, which they relate
speckle interferometry, digital speckle shearography,5 moir6 to irreversible changes of the ceramic surfaces. A recently
methods,6'7 speckle correlation techniquesl'8 and laser inter- introduced noncontacting Doppler laser extensometer 17 ap-
plying spatial and temporal heterodyning by the use of a com-
mercially available two-frequency laser is able to determine
M. Anwander (SEM Member) is a post doc. at the Inst. of Material Physics,
stress-strain curves of stainless steel specimens in the tem-
University of Vienna, A-f090 Austria. B. G. Zagar is Associate Profes- perature range of -40~ to 400~ The advantages reported
sor in the Department of Electrical Measurement and Measurement Signal are the determination of the mechanical response of materi-
Processing, Technical University Graz, A~OIO Graz, Austria. B. Weiss is als at high strain rates; however, difficulties may arise due
Professor at the Institute of Material Physics, University of Vienna, A-1090 to the low laser intensity, especially with higher specimen
Austria. H. Weiss is Full Professor in the Department of Electrical Mea-
surement and Measurement Signal Processing, Technical University Graz, temperatures and materials with impaired reflectivities.
A-8010 Graz, Austria. Only a very limited amount of the described noncontact-
Original manuscript submitted: September 10, 1998.
ing optical techniques to determine strain refer to a practical
Final manuscript received: September 13, 1999. realization of adapting such a system to a commercial ten-
sile testing machine. Due to this fact, it was the main goal

98 w Vot. 40, No. 1, March 2000


of this investigation to develop a laser-based noncontacting
strain sensor with the following properties: insensitive to
in-plane and out-of-plane movement of the mechanical test
system, with a high mechanical stability and easily adaptable
to testing machines. This sensor should essentially replace
the surface displacement conveying levers of clip gages by
laser optical means and should be operating up to 1200~
The principle of the system is based on tracking laser speckles
through a digital correlation technique, with special emphasis
being placed on overcoming the well-known decorrelation
effects.
The paper is structured as follows. First, properties of
laser speckles are detailed, followed by a short description
of the signal processing and the description of the optical ar- Fig. 2--Defining the formation of objective and subjective
rangement adapted to mechanical testing machines. Based on speckles
the experience obtained from measurements about the defor-
mation characteristics of various materials, the applicability
and limitations of such a laser-based strain sensor will be
presented, The power spectral density and the maximum spatial band-
width of the speckle intensity distribution in an imaging ge-
ometry is also important. It can be shown to consist of a
Basic Principles Dirac function (representing the mean intensity) plus the an-
Laser Speckles tocorrelation function of the intensity distribution over the
lens pupil. 18 This property allows one to influence the spa-
Laser speckles are a phenomenon that is experienced if an tial bandwidth simply by adjusting the pupil function using
optically rough surface is illuminated by a highly coherent appropriate aperture stops.
laser source. They are formed by the interference ofdephased Standard cross-correlation methods (see also Ref. 1) are
but coherent wavelets emanating from different microscopic used to determine translations of speckle fields over time, and
elements of the specimen surface and have a random-looking it becomes clear that higher spatial bandwidth gives narrower
pattern, an example of which is shown in Fig. 1. Usually, cross-correlation estimates, resulting in more accurate lag
objective and subjective speckles can be distinguished. Ob- parameters.
jective speckles form in a free-space geometry and can be
projected onto a screen, whereas subjective speckles form in Signal Processing
the image plane of an optical system. 18
In this section, the processing of speckle patterns neces-
Two important properties of laser speckles need to be men-
sary to obtain surface displacement vectors is described.
tioned, both of which are dependent on the statistics of the
As is known, besides pure mechanical stress, rigid body
surface, namely, its roughness and its reflectance properties.
motion in three-dimensional, as well as tilt and rotation of
However, they also very much depend on the features of the
the specimen being tested, will occur in most commercial
optics used to image speckle patterns.
mechanical testing systems. The image processing therefore
Referring to Fig. 2, the typical size Po of objective speck-
either needs to determine displacement components both in
les forming at a distance d from the scattering surface for
the straining direction and perpendicular to the straining di-
free-space geometry can be shown to depend on the size D
rection or has to be performed in a way that ensures that the
of the illuminated spot, the distance d to the screen and the
sensitivity to the unwanted components is close to zero.
wavelength k ~s as given in eq (1):
Yamaguchi8 has shown that by tracking speckle patterns
Xd emanating from surface elements illuminated by laser light,
Oo -~ - - . (1) the surface element displacement can be calculated. It can
D
also be shown that tilt and rotation of these surface elements
The typical size of subjective speckles Ps (in an imaging occurring during and in addition to surface translation will
geometry) can be calculated similarly if the limiting aperture negatively affect the accuracy of the tracking unless so-called
size Dlens is used instead of the spot size D in eq (1). focused speckles (subjective speckles) are used.
The principle setup for the determination of two-
dimensional surface element displacements (before and after
straining) by tracking speckles associated with them is shown
in Fig. 3.
The two-dimensional displacement vector 3surf is derived
from the location of the maximum of a digitally calculated
cross-correlation estimate as given in eq (2). 14 We define two
consecutive images I1(m, n) and I~(m, n) that represent the
digitized laser speckle images formed in the image plane of
the imaging optic (in Fig. 3) and recorded before and af-
Fig. 1--Typical speckle image as recorded by an area scan ter an incremental surface displacement, respectively, using
camera placed 135 mm apart from a rough aluminum speci- a geometrically stable charge-coupled device (CCD) imag-
men (the average speckle diameter is ~ 601~m) ing sensor with m and n being the coordinates of the light

ExperimentalMechanics 9 99
Fourier transform algorithm j9 is of O(N 2 In N) (provided
that M is set equal to N and both are powers of two). Fur-
thermore, the cross-covariance estimate as given in eq (2) is
calculated from only a single realization of the random pro-
cess generating speckles. To improve the accuracy of the
displacement vector ~surf, several estimates have to be calcu-
lated and averaged over time, thereby further decreasing the
performance.
In a practical realization, two 64 • 64 pixel subimages are
correlated to give one displacement vector requiring approx-
imately 1 s of computation time per pair of images. A novel
method of greatly improving system performance by employ-
ing optical computing techniques is currently under investi-
gation, and preliminary results were published recently,z~

Experimental Procedures
The optical arrangement to determine strain within a spec-
Fig. 3--Tracking surface element displacement by determin- imen is depicted in Fig. 4. As was described in the preceding
ing translations of laser speckles sections, the tracking of focused subjective speckles emanat-
ing from surface elements can be employed to optically re-
place levers of clip gages. To measure engineering strain ~ of
sensitive elements (pixels) of the camera, 0 < m < M and the specimen, two more or less distant surface elements are
0 < n < N. These images are recorded, stored and then repeatedly tracked. By determining the cumulated surface
cross correlated using the spatially limited cross-covariance element displacement Asurf from the incremental displace-
estimate X(i, k) as given by ments between consecutive images Asurf using eq (5),
N-k-1 M-i-1
X(i,k)= { ~ ~ [I'(m,n)-(I'(m,n))] Asurf E ~surf, (5)
overall repetitions
n=k m=i
taking their difference, Al, and dividing by a selectable but
D
[I"(m. -- i, n -- k) - (I"(m - i, n -- k))]} constant distance 10, any strain value (both mechanical and
thermal) can be determined as
1
(M- l i I)(N- I k I)' (2) Al [AsurflI -- AsurfI]
= -- = (6)
10 10
where
i, k = space-lag argument To determine this strain value, the following technical ar-
M, N = total number of picture elements of the camera rangement consisting of an illuminating system and two dis-
in the m- and n-directions, respectively placement recording systems are used (see Fig. 4). The illu-
I r (n, m) = recorded image before surface displacement minating light source consists of either a 5 mW He-Ne laser
I~1(n,m) = recorded image after surface displacement (k = 633 nm) attached to a beam expander illuminating a
( . . . ) = mean value. circular area of approximately 25 mm in diameter with a
sufficient intensity to properly expose the CCD cameras or
The location of the maximum of X (i, k) defines the vector two collimated laser diode beams, each having a diameter of
~image as given in eq (3) and depicted in Fig. 3: 3 ram, whose output power can be selected between 5 mW

~irnage = arg max


/ viJc
[X(i, k)] /E =
An '
(3)
and a maximum of 15 mW at k = 668 nm wavelength. The
latter illuminating system is especially well suited for high-
temperature testing of materials, since illuminating power
which is proportional to the incremental surface element dis- density at the specimen surface due to the laser light can
placement 5surf that can then be calculated by taking the op- outweigh the thermal radiation of the specimen. The proper
tical magnification V of the imaging system and geometrical exposure of the camera can then be controlled by a selectable
properties of the camera used into account: electronic shutter or by introducing filters into the optical
path.
The displacement recording system consists of two imag-
~surf = "~" L A n P n J' (4) ing systems with focal length f = 50 mm adjusted with
respect to the specimen and focused to yield an optical mag-
where
nification V ~ 3 and a standard 2/3 in. CCD camera feeding
V = optical magnification (= image size/object size)
their signals into a PC-based frame grabber where the sig-
P,n = pixel pitch in coordinate m; here typically ~ 8.6 Ixm
nal processing as described is performed. The base length
Pn = pixel pitch in coordinate n; here typically ~ 8.3 Ixm l0 as given by the separation of the optical axes was selected
3surf = incremental surface displacement estimate.
to be in good accordance with the base length of a standard
It is easily seen that the numerical complexity of eq (2) even clip gage of ,~ 22 mm. For this setup, the resolution of the
if it is calculated using the numerically very efficient fast displacement is physically limited by the wavelength used,

100 9 VoI. 40, No. 1, March 2000


F
A rf I CCD sensor I
ns I 9,'--71 ~ Zasurfl

-do ~1~ di ~ CCD sensor II


F
Fig. 4---A prototype laser speckle cross-correlation-based
strain sensor using an optical magnification V = do/di to
enhance resolution

Fig. 5--Overview of the experimental setup (optical


arrangement-furnace and testing machine)
k, the aperture of the imaging lenses, Dlens and the pixel
pitch of the CCD camera. According to eq (1) for an aper-
ture Dlens of 5 ram, the average speckle diameter is about
8.3 Ixm, which is in good agreement with the camera's pixel Results and Discussion
pitch of ~ 8.5 l~m. As already discussed, the displacement-
To test the applicability, the mechanical stability, the reso-
measuring procedure consists of a continuous comparison of
lution and the limitations of the optical strain sensor, a series
two speckle images at different times. One of the images is a
of tensile tests with various materials at room temperature
scaled, displaced and possibly distorted version of the other.
and at high temperatures were performed.
The distortion can be caused by any type of surface changes
(plastic deformation, oxidation effects, phase transformation Stress-strain Curves Determined at Room Temperature
and turbulence, etc.) and will negatively affect the quality
of the correlation function. To overcome such decorrelation Standard stress-strain curves were determined at room
effects, a repetitive reinitialization of the image acquisition temperature from technical aluminum alloys and pure metals
system is performed and speckle images are stored succes- (Mo) using the optical strain sensor and conventional strain
sively for later processing. Different time steps for image measurement systems. The loading rate used was about 100
acquisitions were selected based on experience with various N/s. The stress-strain curves at room temperature of two A1
materials, temperatures and deformation parameters. Details alloys are presented in Fig. 6. As indicated in the figure, the
of the applied method are described in the next chapter (see strain was determined simultaneously with the optical sys-
Figs. 6-10). The maximum measurement rate for this system tem and with strain gages (type HBM LY 11/120/3) and a
is one per second. commercial clip gage with a base length of 10 mm. As can
In the off-line signal processing, the correlation function be deduced from the data, good agreement between the vari-
for pairs of consecutive images is calculated and the displace- ous strain measurement techniques is evident. To overcome
ment vectors determined according to eq (6). Adding up in- decorrelation effects, the strain is determined in the follow-
dividual displacement differences (between the two record- ing way: the speckle images are recorded after each loading
ing units) resulted in the total displacement difference, which step (0, 1, 2 . . . . ) and the correlation procedure is performed
was converted to strain by dividing by l0 [eq (6)]. The optical between image 0 and 1, 1 and 2, and so on. The load steps
system was mounted to a base that was attached to a commer- are indicated in Fig. 6 and all following figures. The steps
cial, mechanically driven tensile testing machine (Shimadzu are small in the plastic regime and larger in the elastic region
AG) with a load capacity of 50 kN. A water-cooled chamber of the stress-strain curve. Data analysis indicated an uncer-
in combination with an electrical furnace that covers 2/3 of tainty of the strain of about 50 microstrain and a quantization
the circumference of the specimen was designed. This setup error of 20 microstrain.
allows one to reach specimen temperatures of about 1200~ It is well known that plastic deformation deteriorates the
in air. An overview of the optical system furnace and testing specimen surface, causing decorrelation, which limits the
machine is given in Fig. 5. applicability of optical devices. To study the effect of a
A quartz glass window with a diameter of ~ 50 mm was higher amount of plastic deformation, the experiments were
inserted into the water-cooled chamber, which faces the op- performed on recrystallized Mo with a slow strain rate of
tical strain gage. To obtain stress-strain curves, standard 4.5 • 10-4/S. 14'21 The results are presented in Fig. 7(a). The
dumbbell-shaped specimens with a gage length of about 30 elastic part of the stress-strain curve is presented in the inset
mm and cross sections of about 17 mm 2 were used. For of Fig. 7(a). The Young's modulus obtained was 300 • 20
the high-temperature measurements, these specimens were GPa. This value and the obtained stress-strain curve indi-
mounted into special grips consisting of a high temperature cate good agreement with literature. 25 The stress-strain curve
resistant Ni-base superalloy. TM To achieve proper alignment shows good agreement when obtained from crosshead move-
of the specimen axis parallel to the loading direction, a com- ment. Using the optical strain gage, it was also feasible
mercial positioning unit was used (of the type MTS 609.10S). to distinguish between the upper yield point and the lower

Experimental Mechanics 9 101


Fig. 6--Stress-strain curves of two AI alloys obtained with the laser speckle correlation system and conventional methods
at RT of AI 2024-'13 (composition: 4.5 wt. percent Cu, 1.5 percent Mg and 0.6 percent Mn, heat-treated) and of AIZn3Mg
(heat-treated)

yield point, which is typical for such body-centered cubic distance, the system is insensitive to mechanical instabili-
materialsY The high engineering strain of about 30 percent ties, air turbulence and so on. The method introduced in
was attributed partly to grainboundary cracking as deduced Ref. 15 in its present form is limited to temperatures causing
from the scanning electron micrograph [see Fig. 7(b)]. It may little self-radiation (< 650~ The ESPI techniques intro-
be deduced that the decorrelation effects due to even drastic duced by Aswendt 13 are sensitive to mechanical instabilities
surface changes can be overcome by the proposed recurring of the sample. The system introduced by Chiang 23 used laser
reinitialization of the signal-processing unit (using numerous speckles in combination with a pulsed laser to minimize the
small load steps). effect of thermal air turbulence. This testing device allowed
one to measure transient thermal strain fields; however, the
Deformation Behavior at Elevated Temperatures author reported data up to temperatures of 400~ only.
To study the stress-strain response of materials in the high-
To test the optical setup at high temperatures, we studied temperature range, we performed two types of tests. In Fig. 9,
the thermal expansion of test specimens that were supported the stress-strain response of an ODS PM 2000 alloy is mea-
within the furnace by gripping the specimen in the lower grip- sured at 1000~ with the optical system. Special gripping
ping system only. As may be deduced from Fig. 8, the thermal systems (Nimonic 90) were used. A comparison of the mea-
strain of an annealed Pt specimen measured with the optical sured data with data from the literature shows deviations in
method is plotted as function of temperature. The speci- the strain values on the order of several percentage points,
mens tested were small rods 3 mm in diameter and 40 mm which indicates good agreement if taking into account the
in length. The temperature of the specimen was measured accuracy of the different strain sensors (high-temperature clip
using small thermocouples attached to the specimen. The gage) and the difficulties encountered with high temperature
temperature deviations in the region where the strain mea- testing facilities.
surements were performed were about +2~ depending on To test the stress-strain response of ceramic specimens of
the required maximum temperature. The measurements were the type SiC/SiC 21 up to 1200~ the specimens were tested
performed several times up to 700~ and indicated an excel- in compression using a specially designed compression de-
lent reproducibility. Also included in this figure are strain vice. To align the testing rig, a spherical cap made of SiC was
data of Pt derived from literature. 2e Figure 8 also presents used in the hot section, as proposed by the relevant testing
thermal strain data of an Fe-based oxid dispersion strength- standards. The specimens tested were 35 mm in height, with
ened alloy (type ODS PM 2000) manufactured by powder a cross section of 10 x 10 mm. The results are presented
metallurgical techniques, 21 tested up to 1000~ The speci- in Fig. 10. Compression testing was started with a preload
mens were plates with a thickness of 2 mm and a width of of 500 N for prealignment. Then, the samples were grad-
10 mm. Although the specimens, due to heating, exhibited ually loaded to a maximum load of 5000 N and gradually
changes in the surface structure caused by the formation of unloaded. Two cycles were performed for each tempera-
an oxid film, the reproducibility is excellent. The calculated ture. For the temperature of 1100~ only elastic behavior
thermal expansion coefficient of about 12-16 x 10-6/~ in was observed, with a variation in strain of about 10 percent.
the temperature region im,estigated showed good agreement For the temperature of 1200~ we observed deviation from
with literature data. 21 linearity, indicating remaining plastic strain. To reduce the
Comparing the applicability of optical systems 15 to deter- influence of thermal radiation on the speckle image signal, a
mine thermal strain shows the advantages of the introduced polarizing filter and an interference filter were inserted into
laser sensor: due to the fact of using two spots in a selected the optical path of the sensor. A comparison of these results

102 9 VoL 40, No. 1, March2000


600

500
~r H
I
400

300
.=.

o~
200

100

0 10 20 30 40
strain in %

Fig. 7--a) Stress-strain curve of recrystallized Mo obtained at room temperature with the laser speckle correlation (LSC)
system, 14 (b) scanning electron micrograph of the deformed Mo specimen after 30 percent uniaxial deformation

with those presented in Refs. 13 and 21 determined with a tion of 20 microstrains. The laser-based strain sensor is being
high-temperature clip gage showed good agreement. designed with low laser intensities (< 15 mW), which may
be of importance if such systems are used in industrial envi-
Conclusions ronment; thus, special safety requirements are not necessary.
This paper describes a simple optical strain gage based At present, the strain measurements can be performed with a
on the digital laser speckle correlation technique. This sys- rate of about 1 Hz. An improvement in the measurement rate
tem using subjective speckle patterns is easily adaptable to to 100 Hz using a special optical design and line scan cam-
commercial tensile testing machines equipped with a suitable eras seems possible and will be published shortly. Based on
electrical furnace. The laser-based noncontacting strain sen- the obtained experimental data, it may be concluded that this
sor can replace commercial clip gages and is suitable for de- optical system is suitable to determine thermal and mechani-
termining stress-strain behavior of various metals, alloys and cal strains up to high temperatures (1200~ Compared with
ceramic materials up to high temperatures. Due to the special various other optical systems introduced in the literature, var-
data-processing procedure, the decorrelation effects caused ious specimen geometries can be used and no special surface
by any type of surface change are minimized. The special preparation is required. Due to its insensitivity to mechani-
design of the detection system using two laser diodes and two cal vibrations, turbulence and so on, the laser-based optical
lenses in a chosen distance of 20 mm results in a strain resolu- strain sensor seems suitable for technical applications.

Experimental Mechanics 9 103


0,016
error of measurem~
measurement
=o 0,012
ODS eM2o0o \
0~ measurement 2

0,008 d
0,004 7 . 0 ~ ~ literaturedata

0,000
0 400 800 1200
temperaturein ~
Fig. 8--Thermal strain data of a Pt standard specimen and thermal strain data of an oxid dispersion strengthened Fe-based
alloy (ODS PM 2000) as a function of temperature compared with literature data22 (specimen geometry: rod specimens with a
radius of 3 mm and a length of 40 mm)

200 0,00

T=1173 K ODS
T=ll00~ ^ ...~/1 o
E=138 +7 GPa \ o

t~
n
150
\. 9 IIIl
.=_,
-0,05 -

0 0
O

0
_ ~

c- r~
0
100 T=1273 K -0,10 8
E=126+6 GPa H error o f
I measurement
T=1200~
= error of -0,15
50 '. I---I measurement SiC/SiC

Am9

f -0,20 ! I
-6000 -4000 -2000 0
0,000 0,001 0,002 load in N
strain Fig. 10--Compression data under cyclic loading of a ceramic
Fig. 9--Stress-strain data of an oxid dispersion strengthened sample of the type SiC/SiC at test temperatures of 1100~
Fe-based alloy (ODS PM 2000) as function of temperature and 1200~ 21
(the measurements were started using a preload of 20 MPa)
References
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