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    3 views31 pages

    Truyên khối _Qmeo

    Uploaded by

    Hoàng Phước Khải

    Copyright:

    © All Rights Reserved
    Download as PDF or read online from Scribd
    Flag for inappropriate content
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    mi ee — "ety Sag e a caLs, “eae te mRING Ge Ics ad BL usr Gos RCC) & ENG fi mae a pe tl ni a oe oil Card Chuong 1 Kién thirc co’ ban vé qua trinh truyén khéi 4. Binh nghia: Qué tri ci chuyén vat chat ti pha nay sang pha khdc ki hal pha tiép xc nhau try tgp go la 8 trinh tray kh Viauvd mtn: duvet tong mae pe ind eryt vo sh ng) ‘Thanh phan pha Cac cu tir tao nén mot pha nhdt dinh (ran, long, khi) dug dac trung béi lung hién hiru cia nd trong pha dé tweng quan tung déi véi cc cu ts khc hod vi toan hn hop. Bai lwong phé bién biéu dién thanh phan pha Pha léng, pha khi: ndng dé theo thanh phan khéi long, thanh phan mal ha khi: thé tich ring phan, ép suat riéng phan Pha rén: thanh phan khéi lugng, than phn mol SSG adie & | Phin mot ” te (rae L Frm | | bg 00 not | Neg 468 wong Quan hé gitta cdc nng 46 thanh phan pha yal ay ey 1, Si tng Hiéng hn hap ede edu ti tao h8 mot pha ling Pa Pa Pa h6! lugng phan tr eda hn hep: My=DxM, M,+(1-x,)M, ‘can bang pha ‘Tai mBi dibu kign xd dinh s6 tn tai mgt méi quan h cdn bing dita néng d9 cia cdu ti trong hai pha va duge bibu dién bang dung can bang. ++ Kh cn bang thi sy KhuBch tén téng cng cia hal pha bing 0, qué trinh khudeh tan cia hai pha vao nhau bang nhau, ++ Knichua cd bing, 58 xay ra qué tinh khuéch tan cia cu {ir git hal pha dé diva he vé trang thal can bang, Sie han cin au nh tan Kt a 9 at vong ncn bang. Dong ive Khuéch tn cia cut 1 sy ohdnh eh nding a CChibu ea dng truydn kh (khubch tin) ltr not ©6 nbng a 620 dn no’ c6 néng 46 thép hon, CChiéu khuéeh tn cia cu tir s8 tuan theo quy lugt: | Néunhuy yag— -6Ol Pa + Fan vot la pha ting, . va pha kh = ¥,¥, avn tc Timea) x,y" ndng 60 cha = ammoniac trong Z pha lng va pha khi cia pha kh v0 Weng, va cia long vio ki Ban du, x= 0/y20 So s4nh dinh lugt Raoult va Hens paHx stan awe P= Paix ; nf eit ‘ig at Hae pana ing cro mmemasie |) - in()-H amar ‘8m ut Rac pd dng eh cu eng a ng eh ng tol 2)- ra AL. Khuéch tan phan tir - Xay ra trong lop mang & ché d@ chuyén dng dong = Dong lie la chénh Iéch ndng dé gitta hai bé mat tiép xc. Khuéch tan tir noi nong d6 cao dén noi nong dé thap trong lép mang - Xay ra rat chim. - Phu thudc vio bé mat, thoi gian, néng dh... H, 43 CO, 340 HO 189 0, 256 «80, 422 S 829 N, 312 NO 238 GL 48.4 Ar 299M, 384,832 co 307 NH, 258 718 2. Khuéch tén 461 uy " Xay ra trong nhn pha & ché d@ chuyén dong xoay = Xay ra la nhi sy xéo tron clia cdc phan tir trong dong "Déng lye cua qué trinh khuéch tan 46i lu la sy chénh léch ning d6 trong nhn va néng 46 be mist tip xu Khuéch tan phan tir quyét dinh téc 46 cho cd qué trinh khudch téo begets Khuéch tan trong dung dich A- reine “Tena ng hin gra eb tA, 8 au tin Phen ong ng Mera N,=tePe eu ,C, (nekmis 64 Cs nbn snl caves seCsruns rbd chuyin tango uy = Mea tHe Ce we CoC Luge eu A ua Pia org cl chdn dog tho vn te ting io 0 peg cht aan pt. sy Nerney Nyt Np) Ss By Ae ete atu tn thas mo ahuorg ong ch pruong nn org ne orn drow ed etna Tera remap pa ab dont ae mi enc an es mikoora Thane Mpebet ts com gator x Leet b. Khuéch tan dang mol, nghich chiéu ot pa es phe ios ‘oa Pe iogrd) Been) 082 Lame 82 108 eae = 8208 orate Bal ip dy: cael rue nude tn ema gion id cus mt veh ee obs BY co “e,Ning 80 con oar oa Benen Bw Sea wee (thts eb natch to esl rng ude a. tO" ci ne 5 ena cnt mingle KLR sara = 790 gn H0 8 100 kg tine .@ 20: Pity 80 “3 a. A khuéch tan én dinh, 8 khéng khuéch tan eI, =0,M= const Say Veit tng 08 yg ty ai rie ‘pearing go cot ing ung oI R= 0.082 LaenynotKy 82.08? senyoLK) = 8208 femal) Dong Luc Khuéch Tan [Néu tin theo pha ®, syeyt=¥ sy hay ayey-y" ‘Néu tin theo pha ©, axext—x, hay Axeeoxt ‘ih rie: gg vat etl chayd, gua mgt don v it ip xe ha wong ml an v no gin as bo ng GO Wd on vi He ery by hute vot nid tend vt) oa pha ob ob ‘uli tn, 6 nh, Toga dng) it 8, Ap sub, keg, Rh gett ‘ct eh 98 dng dang pi ign rong yen Hb ‘Chun sb Royle (Re): de tug ooo chuybn dg cia dna hy 2. Chui s5schmiat (So): gc tung tinh cn vty cla ms tubng (mela a5 nova 8 neon i) {3 Chub s Gras (G7 abe rung ene gus nn abs uty nin 4. Ghul 6 Pecot Po: tung cho uy thd rong ml rg Bag (Rese) 5. Chun sb Sherwood (Sh: 9c tamg qa iin yn ab mat ‘chu nae Stns hau gion of eying nan Chuong2 ‘Thép dm va Thép mam truyén khdi: phan tén edu ti tty pha khi vao pha lng va ngue li 4 | Phuong phap: Tang bé mt tiép nic | Cac togi hg 56 truyén kh on heb Truydn kod eh | Trvdnndt | nnn [tena ‘allonnalne allem na Wahi | Na= Kets | Molen Kad, [maven raiay | tra ering sue to torg vie tlt tn sng ony rg mile ‘eo ce me cae ue dr tu vn rv anne gh oy ‘anagram dt wong engin gre chun aon Hin: ‘cc kiéu mamidia trong thap truyén khdi (ndp thy, hap thu, chung cét) ‘9 x Me vn hh en) Mey abe nD hp Théng sé chinh can tim khi thiét ké Thap Mam hay Thap Chém ? ~ $6 mam hoge Chibu cao c6t chém > quyét dinh higu qua truyen kndi + Bygng kinh > quyét inh bai nang sudt + Luu ugmg dng khilléng > anh hudmg bai avéng kinh va nang sudt, quyét dah trang thai lam vige eda thap, rain ce nh in op at mon | seman sais ain dom hi crs at Sip Sou ny ‘Thiét ké thap mam (tt) ch mip hte owe eng aon qu myc ing ‘a anda co dy se veo evong nna. 9 C3 con Treo eninge, Chg ne: yh do ie ng vt as og ng ng ‘ning elt css orm a gunhinycranea. cy an in hn ctr i sha yan Lop atm Sunecne Lapa aoe ei ey han vt bm nu hi poo at 8. Lt abn (pacing suppor) 4p va ng§p lyt trong thap 46 Chuong 3 Qua trinh Chung va Chung cat 1. Hin hep hai efu tir colttingneatanhatn on oie) “tng nea nr abso hae "ating sng an 60m {4.Chit ng ha tan hon toe: ote at cian ne vn ah pant ‘ha bute ae hahah a in, | Hin gp kang ding pi ay dang eh tye dng con tng bun en sang: can ningitng avaan eo rm Raa bung es ie thong bee dil eat HB hep ing pi at eg i vot mann pnd ng pi nn ye, Tigao oben pis Kng ls gust rg eth ap act ann. “Pha ng pig rong peo? 2. ina ndng ni tan vie aba mse) Vly pani aude matin tea uve Ap sultg pnt cb ee bu gaan 0 ‘pant nna nen ang Spa herb ane hitman en, Ao ult nage in top Ary a8. sue - “heen ev o85 ne, Nh 2g ne apn to za ws nie “palate cosebus mayen ca 1.2 ehit ting ns tant hin ‘28 bay ol a Nb hp cain hal eng bg neh Pr. rong gh ts, hn pong anne aun eh na masa thon ne nny nda hyo ora Wh iy ng Glin a ding mst Pay (Rat don) » Te const lr. Ling fe Ling Hot Hot ‘Glan db ing se Ey Su cn auan ns mth sha lng v pho rang cn Bg no vam 5 8 tong oa hh igen po rn =) Prinvungoin coo cane | Dyonaramats err aN olga EP ‘molpiaF DE Glin 6b mann pds mabey ‘3. Tinh ton thiét ké thép chung eft bina pip McCabe Thiele ‘50 6b cong nab corbin vi he ung ede mét bn tip chung et ‘Cie bal oan ab tye hig tht i hod chin Wg thdng tha chug oft 1. Tahtotn eta wg rao oh avo, i ah rng u rng) 2, Oyattn cin rg ning gpa tah oan ab ob | rod nie {hn tig vce tira ob is 6 (vo, oh ab a pen ‘Sonstrgvayenrmgt nage bari toh wy ig eh Bp ‘Sich 3. Tinh oan cae ye such em eh ng pO ep. 4 Tian ng echo map ch ot Be fl ng oa ba me oo ng ely) 5. Tnhtosn 20 aba on vt itu ch hig rg cic ba ton ab tye ig tide kd ht i chinh trong M6 thdng tp chung eft 1. Tenn tn ing cl bein cc thing af a borg v ng chute abr 2, Bem eis ide sh Nite a ho NS hop. Burg 6udra init eda pb chan, pn eS dung mi 4 Tab msm yg ul i 6m hsb rita ne (isp mam) aeons eatop sb pe) 8. nnana cao 1, Tie eh cov adn nn np nb inte apts eet ag (sEvebe mn chon as rghit ab ay TTB 2 2. Tyco bangabcia mimtng no mn ata gy rte Seon pp 46 thi McCabe-Thiele » Sep: age Sepe telae clasp. oy Soh teammate Sep xicamthteev oop co Soitat Seb etal Spr veann ng — Chi sé hi lwu tdi thiéu cho dung dich dang phi ete - | " as Chveng 5 QUATRINH || HAP THU ix BO HOA TAN CAN BANG. Nong 6 cit ha tantrong “TL ‘pha ling cho dn khi bao ha 9i 8.46 hoa tan cia cht Kh tpinhigt 66 va dp sust dé. f Ap suat CB cao ma dé hoa tan hé thi chit khi dé hda tan kém | va nguge I. : TRINH HAP THU NGHICH DONG e ou-9=7 £80 hoa tan gidm khi nh a « ‘ing va zero khi dung méi si. rnhiBu Su tir thi d6 hoa tan ing doc ap nhau va biéu suat riéng phn. 4 trinh hap thu cing chié P a ‘Mot cdg cd ut ian 200 kl hig 25°C vp sus 1 ee maha bar Thanh phn gm: Sant mae maton = gutta clung hydrocarbon va thép mam a6 hép thu 98% benzene, pits thu, iu néu sud lvong dung mila 30.25 kml h ili hé $8 géc cia déme cin bing x. g 25°C and 5 ba, Bit hydrogen gn nbur kong Np samaanee Kae aenzene [0.182 Chuong 6 igm Dinh nghia COREE Ran LR en ee CHUONG 6: HAP PHU Sates es ea lt = SRE ee Reg lease ee Rea Teer Ne Chuone 6 Poort Pee eC aure nTl te iaeenl Pe ee ae ed i ee ee et nt Pewee Oot eng pene ee er pene tn ed © Cie giai dogn hap phy - Cee oer Sete Peace Ce eC Ceti erd Cee EC Ca TET Sa ae Ona aod ML. Chit Hap Phy ConeNa Chuong 7 Qua trinh va Thiét bi TRICH LY Liy nase 8 rio" dia tn Daun khng ton trong ric cn ding th tan rét tit trong nie C6 mot hin hup ding trong dia tn. Lm sao dé téch ding ra khsi dau &n ? Burung tan mot phin trong di &n, & “richly 1 phen phip elt hi bin at téch had tedn {ote mit pin) mit hote nh cl tt pha rin hate Wing sang pha ling dang mdi bing cSch cho hel phe Nep = Niu tdch eft ha ton trong hit ing 9h? go 8 ech y Hing ~ ling = Niu teh chit ha ton trong eit rin th go rch ly organic solvent water colbe Soltbtecorpounds Sereoinde & ‘Seporatory Funnel Extraction Procedure & - aaa Dong mas [ Thy 1 ha Rapist Pave Bas SA) t t —, ‘oan agen 4 rie { ‘Roem ] ome moe warm ReBIA) 0 Ena(B) s 1. Trich ly mot bie CP) (a) ®OoO® a S tan eh nig i doe + Ted lin dag dich du F aim dng msi dB va elu atch ‘gil lu tpn bd) v6 dang m6 th $ vo nha eho a hi dt duge cin bing + Tih 2 pha ling pha: pha aim dung mois S wich Agi 1 pha wick), pha ca It gn dung mdi du B a el A (go th piu rophiad, Tuy nhin aéuB va Sha tan mit pin vio nhau {bind pha gm 3 elu ns (A, BVA), + Hin agyén dang itch A va B aK. 2. Trich ly nhitu bie - . Trich ly nhitu bic chéo dang (cross-flow) ra 3. Trich ly nhitu bac ee . Teich fy mhidu bc ngune city (couer=flow) Bos i ea eae adndn so" ~OLEELGE &. o cs Ss EERO Ae : ec 1. Trich ly mot bic EE 2. Trich ly nhitu bic - D. Boe gidn 43 6 hin hop phan thanh hai pha Kei phan tdch hn hop M than pha P v8 Q tae ahng qu ie sau 6c diém M, @, P cing rim trn mit ding ting trong ‘hy tam gi. Diem M chia pha P va. @ theo ty f sou phaP_ MQ pha MP B. Gian do 3 cau tir Ba cfu ti tr lin wi nhau th go thn mae pha, hai pha HAY ba pia King hoa tn vi nhau khdng kee theo mt pia ng ha hoe hay hop cht in thé ign ten th hin am ge. Thin ph 06 th ‘mal hay KL. B Cho bit hin ph trong ting inbep Cho bgt pha fu hint es Cho biét thin phn edu tong tg ph (Cho bgt hugng ed tim pha Cho bit tt ehoyen pha ‘ ; es NeuyéN TAc TRICH LY Baby Gh Ar cite F loivetndatedocta imme Pt ES point Na viet pinscher ap hak hp ting ng 1s ey bapa Gy Pp (ede akde dg me vps 7 "lk pa ia dang pba Nia kh ng ra phn ‘ehie ve dag lo hop Een lu bw hap dh tg SQ, cleAB iE) Tien cana moe spe aie ea apy cs oh lo 3 bgp ela ube Sct cp am salem), 'Néu then dang mai vo R, ma thinh phn ca he be eu ta has ‘days pha P, vi Qa, vi tchréng. Dung dich hai pth duge hi hop Eva R, vi Ry 8 ca nk ch B hom tong Ry cir nh iy tah dage ee i B nguyen chit Cin clu Ath 4 tinh Knit i da can ch dat due did Fy, te li pao diém ci dung tgp ayn, vo dng cin bing chia ha Thip phan 1ahdprimg:2-9 phn phan Phin chias-bng dn: Spha ning Logi thip c6 tim ngiin “Thap phun: phe én tye chiém tn bp the ch thi va te fbn sling Phe phn tn pun ths hat ih vé yen qu, phn Yn vo ph Tn tue Bin mor a co nr eh nda dc hat ese pha ph én ip ‘upg i ch ra ht phe in ye. Nog sult cam ng hig sult hp 8 ty. na ee ain pha cia, aco pi ty dng Gétvong Kn bétmet gar (ray) ma sag co ga Soma Ung 08 9 te thay mre “Tu cae adm Raa bbs, ta dng ce dvong 7 song song vr canh ac “Tu cde dm Ea bibt, ta dung fe drémg @, song song vei canh ac Cc ang 7 va two cng ct rina tl eae adm Pyeng Ung. ‘Buéng cong qua ote dd F991 18 aang to ha. * Tu dibm Ry a v8 dubng thing song song v6" BC cl dung Lo han tal Py To Py ta v8 dong song song v6i AC et dues chit aE, wong Gn Tht b rich ly nhidu be ‘é cinh Khudy L-thanh tid j-th mgd -trye Khudy:4-pha nhesS-pheu phum6-pha 2 mhe ‘ing suit vi hu sut phy thude vio ef hin Kha, cng me quan he its ai ha (is didn ci Jogi ny li ning sult le va higu suit txomg db cao. Ngo + clin 6 log thip ding cn Khu tuabin, thank tide bis 2piings 3a i; ongin tren; SB Loa hpi 1 hp King cng chy chuyén, Nid phuona php ‘hin ding, ting 8 cing bom piston “Tin nln ng: 250 chu h/Phat ‘er bien Behn ing om C8 the dig ln dpm rch hot kg 5 kh legng riéng Khe rheu 0.05 gen mang trong tra hap my ng ‘i thi. Tie trict Ay ty tm, ‘ThiGs bi ih yy ten 1 mt hing hin ty quay nan én mse ‘rye nia gang. . 8 yong quay: 1500-5000 ving/pht,bén rong o6 tm agin hin soi de 66 1 eo thin sinh 6 tone thing, pha nn va pha nhe di ‘vo thing qua ede rinh& try. Hai pha chuyén dng nguge chida nha va eng dir theo ef rh 6 true ig su ied ly rt ao, dui te dng ei ye Ly te vn tbe ta pi phan tn eng nfur evimg d9 khudy tn dupe ing, en nig ‘Lop hit i ec yy ti ing dng tt dicho higu s6 khSi Ieoog riéng ia bai pha nhs, PUREE R GI «1 CWE C RRO lac- (0? > C6 3 phuong phap: ¥ Phuong phap nhiét v Phuong phap héa ly. v Phuong phap nhiét két hop co” hoc. Phuong phap nhiét J cosoaoan hii #8), levossaned Lt “ene ‘en Phuong phap héa ly ows et TOT pe | PP nhiét két hop co’ hoc I Tinh Luc Hoc Qua Trinh Say khong khi-+ hoi nude = Hn hyp khong kit “Cac kha niém aac trung cho hh khéng khi Am: + Bd 2m tuyét déi (ham &m) : ¥ (kg hoi nu6e / ka “ Cach sir dung gian dH - ¥ Xe dinh trang thai hén hop khong khi kh} khéng khi 4m + 89 2m twong 46i (46 bao hda hoi nus) * Xe dinh nhigt d6 diém suong - Pardp suit rigng phin eta ho * (ts) > dé trénh hién ton; * Hol nuée tang > Pa = Py: 8088 > Par = 1 gung ty hoi nude trén bé mit vat liga * quan ne giua 7 va 9: * Xe dinh nhi¢t 46 bau ust (ty) GIAN DO H-Y CUA HON HOP KHONG KHi AM oma i —— Sungenmeby ang apo, eg ah (on Sigehngen ‘ovens ener Ureawe 2 meng oss cy ‘dy ly thuyét kB = dt ng done ei Bc = siy ty thuyét 3 rvbng hop sSy the = Nhigtb6 sung lan nom hig tn that, nd H, > Hy Nhe bé sung khéng di bi tn tht nd HH nist b sung bang nig tn tit, Hy = (si thuyét) bn cno rap re 96m Pei hm enor imi Spina ° mb . ie Cain bing vat chat va nang mg tromg thi bj sdy boing khang Kh Nye tf roaratomg Chit wi hit ta Khong khi > sy bing khong kh Sadi: + Phcomg tite bys + Sly 6 bd sung nhigt ‘wong phone Largng nhigt cin thie tiga. chide, ‘ng edp &b6 phn dt ne mk com Sage Syne hey wong png sy fy ohana, ABC: khong bB sung nhigt ; ABC typeby phim VUES OG Sing nist gy inne + Amin tic

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