Magnetic Hysteresis Measurement Techniques
Magnetic Hysteresis Measurement Techniques
X, MONTH 2024 1
Abstract—Different magnetic needle probe setups are pre- The needle probe method can be used for the non-
sented, and their strengths and weaknesses are explored. A destructive evaluation of the magnetic properties of a fer-
new setup, combining the advantages of the other setups, is romagnetic sample. The wrapping coil is replaced by two
presented. Finite element simulations are implemented to show
the effect of the excitation yokes and residual stresses on the conductive probes touching the surface of the sample. Such
magnetic flux symmetry. The error sources affecting the precision setup is equivalent to a wrapping coil of one turn [7], [8].
of the experimental measurements are analysed and quantified. It only requires electrical contact between the measurement
Solutions to minimize them are also proposed. By minimizing probes and the sample surface. As a result, it can be used
error sources, the obtained experimental measurements closely on large samples instead of drilling holes. However, the
follow the reference hysteresis loop obtained from a wrapping
coil in the unidirectional case. The proposed measurement device main disadvantage is that the signal-to-noise ratio can not be
notably provides enhanced accuracy for surface measurements improved as easily as for the wrapping coil method. Hence,
when wrapping coils are not implementable. the needle probe method requires low-noise amplifiers and
Index Terms—Magnetic needle probe measurements, non- a precisely defined experimental setup in order to obtain a
destructive testing, magnetic hysteresis. reliable measurement.
This paper presents different needle probe setups and their
main assumptions. An important assumption concerns the
I. I NTRODUCTION
magnetic flux symmetry inside the sample. The error sources
I ZZ ⃗
∂B
E ⃗ =−
⃗ · dl · ⃗ndS (1)
∂S S ∂t
Hence, by connecting two conductive probes to the sample
surface, the induced voltage between the two will allow to
measure the variation of the magnetic flux in the sample.
Since the probes only need to touch the sample, the needle
probe method allows for flexible setups and non-invasive
multidimensional measurements.
This method has been patented in the 1950s by three differ-
ent authors [7]–[9]. The very weak amplitude of the measured
voltages requires strong amplifications to precisely measure
the magnetic flux variation in the material. Theoretical studies
have been carried out [10]–[15] to better evaluate uncertainty
sources and alternative setups [12], [16] have been devised
to minimize their effect on the experimental measurements.
The magnetic needles method has since been employed with
good results in a great variety of materials [17], [18] for the
measurement of rotational losses [19] and defect detection Fig. 1: The four different methods for needle probe mea-
[20]. surements described in this paper: a. Original Setup (OS); b.
Four different setups have been identified in the literature, Single-Side Original Setup (SSOS); c. Air Flux Compensation
and each of them is described in this paper. These setups are Setup (AFCS); d. Transverse Needle Probe Setup (TNPS).
shown in Fig. 1. They are denoted as follows:
• the Original Setup (OS), described by Czeija and of the setup and for the scanning of the entire sample surface,
Zawischa [7] and Werner [8] in their patents, in but at the price of a greater air surface.
which a pair of needle probes is placed on each side
of the sample, hence giving two voltages Vtop and Vbottom .
A. Preamble: magnetic fields definition
• the Single-Side Original Setup (SSOS), patented by For this section, the general definition for the magnetic
⃗ in the material is considered:
induction vector B
Czeija and Zawischa [7] and Stauffer [9], [10], which
has then been employed in the subsequent decades [21].
Bx (t)
This setup is a simplified OS, in which the measurement ⃗
B(t) = By (t) (2)
on the bottom face has been removed. As a result,
Bz (t)
the change in magnetization within the sample can be
measured using a single voltage V , under the assumption To enhance the readability of the equations, the integral
that the magnetic flux in the sample is symmetrical. form of the magnetic flux is substituted with Φ as follows:
ZZ
∂B⃗
• the Air Flux Compensation Setup (AFCS) [16], Φ(S) = · ⃗ndS (3)
derived from the OS by adding a pair of needles that S ∂t
are short-circuited, but isolated from the sample. Two Given a surface S of boundary ∂S, the induced voltage
voltage measurements are required to describe the Vind on ∂S can be calculated through Maxwell-Faraday’s law
magnetic flux variation in one direction: the voltage in as follows:
the sample Vair and the air voltage Vsample . I
Vind = E ⃗ = −Φ(S)
⃗ · dl (4)
• the Transverse Needle Probe Setup (TNPS) [12], in ∂S
which two pairs of needle probes are placed in the The surface S can be separated into two parts Sair and
same fashion as in the OS. This setup is equivalent to Ssample depending on whether there is air or ferromagnetic
a differential measurement. material in a precise point of S. Such decomposition is
Fig. 1 shows that each needle probe setup will be affected by illustrated in Fig. 2 to 6 and the resulting equation is given
magnetic flux variation in the air between the needle probes. below:
Such effect must be minimized to avoid unwanted drift in the
reconstructed hysteresis cycle. One way to achieve this is to
Φ(S) = Φ(Sair ) + Φ(Ssample ) (5)
print the needle probes directly on the sample surface [18].
Such probes would be fixed on the sample, which could be a An assumption that can reasonably be made is that the
limit since only one position is allowed. Needle probe setups measurement device has an infinite impedance, hence no
can be realized with spring contact probes to ensure the contact current flows on the cables connecting the needle probes to
between probes and sample, allowing for an easy positioning the measurement device.
IEEE TRANSACTIONS ON MEASUREMENTS AND INSTRUMENTATION , VOL. XX, NO. X, MONTH 2024 3
B. Original Setup
Considering a magnetic field B ⃗ normal to the cross-section
Ssample , Fig. 2 shows the OS and the associated Maxwell-
Faraday’s surfaces Ssample , Sair t and Sair b .
Vcoil ≈ Vt + Vb (15)
If the setup is not symmetrical (as detailed in the next
paragraphs), then Vt will not be identical to Vb , hence an
asymmetry factor ϵASYM can be defined:
v
uR T
u [Vt (t) − Vb (t)]2 dt
ϵASYM (%) ≈ 100t 0 R T (16)
2 (t)dt
Vcoil
0
Fig. 7: Simulated structure on COMSOL. Dimensions are in
Simulations are carried out for a duration T = 4f1exc , fexc
mm.
being the excitation frequency. This implies that only the
first magnetization curve of the material is simulated to keep
uses tetrahedral elements. The coils are modeled using a reasonable simulation times.
homogenized multi-turn conductor model.
The material properties are given in Tab. II. Note that other B. Geometrical asymmetry
configurations with different geometries (coils on the yoke One way to introduce asymmetry in the through-thickness
legs, thinner sample, shorter yokes) and material properties magnetic flux is to break the symmetry of the excitation system
were studied. However, the conclusions drawn from such (coils and yoke). Several examples have been tested with
studies are identical to the ones presented here. The sample fexc = 1 Hz:
material is an Iron-Cobalt alloy, whose magnetization function • Case 0: two excitation yokes (perfectly symmetrical),
M (H) and parameters are taken from [22]. chosen as reference;
• Case 1: one excitation yoke;
TABLE II: Electromagnetic properties used in the FE model.
• Case 2: two excitation yokes, with one yoke generating
Properties Yoke Coil Sample 10% more magnetic flux compared to the other;
Electric conductivity (MS/m) 1 6 3 • Case 3: two excitation yokes, one yoke being moved
Relative permittivity 1 1 1 5 mm in the X direction;
Relative magnetic permeability 104 1 Non-linear [22] • Case 4: two excitation yokes, one yoke being moved
5 mm in the Y direction (normal to the sample surface);
Simulated needle probe measurements are obtained by inte- • Case 5: two excitation yokes, one yoke being moved
grating the simulated electric field following the paths in Fig. 5 mm in the Z direction;
8 counter-clock-wise. • Case 6: two excitation yokes, one yoke being rotated of
10° compared to the other one.
Results are shown in Table III.
TABLE III: Asymmetry factor in different simulation cases.
Case 0 1 2 3 4 5 6
ϵASYM (%) 0.16 8.41 0.61 0.27 2.92 0.25 0.23
C. Material asymmetry
An asymmetry in the material properties of the sample
(e.g. due to residual stresses) can cause an asymmetry in the
through-thickness magnetic flux, even if the excitation setup is
perfectly symmetric. Various through-thickness uniaxial stress
profiles were studied. These are similar to those introduced by
a rolling process [23]. The analytical magneto-elastic model
[22] was used to compute anhysteretic B(H) curves as a
function of uniaxial stress (see Fig. 9). The simulated stress
profile is given in Fig. 10. Fig. 11: Simulated wrapping coil (Vt + Vb ) and top (2Vt )
and bottom (2Vb ) Single-Side Original Setup (SSOS) mea-
surements on a sample with residual stress.
v
u PN
u (x[i] − y[i])2
RED(%) = 100t i=1
PN (26)
2
i=1 x[i]
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IEEE TRANSACTIONS ON MEASUREMENTS AND INSTRUMENTATION , VOL. XX, NO. X, MONTH 2024 11
A PPENDIX I In the case of the SSOS, only one of either V1′ 2′ or V3′ 4′
D ETAILED CALCULATIONS FOR EACH NEEDLE PROBE is available, while the same Maxwell-Faraday surfaces are
SETUP defined (Eq. (27a) and (27c)). To be able to solve such system,
A. Original Setup (OS) and Single-Side Original Setup (SSOS) one must assume that the electric field is symmetric:
Fig. 18 shows the OS and the Maxwell-Faraday’s surfaces
V12 = V34 , V23 = V41 (34)
Ssample , Sair t and Sair b .
Hence, Eq. (27a) and (27c) become:
Fig. 18: Air and sample surfaces in the Original Setup (OS). B. Air Flux Compensation Setup (AFCS)
The Maxwell-Faraday surfaces for the AFCS are shown in
The magnetic flux variation in each surface Sair t , Sair b and Fig. 19. This setup being an extension of the SSOS, Eq. (28)
Ssample can be linked to the measured voltages as follows: and (34) are supposed true for this setup.
V2′ 1′ + V1′ 1 + V12 + V22′ = −Φ(Sair t )
(27a)
V4′ 3′ + V3′ 3 + V34 + V44′ = −Φ(Sair b ) (27b)
V21 + V14 + V43 + V32 = −Φ(Ssample ) (27c)
Vii′ = 0 (28)
Hence, by combining Eq. (27a), (27c) and (28):
Fig. 19: Air and sample surfaces in the Air Flux Compensation
Setup (AFCS).
V2′ 1′ + V12 + V4′ 3′ + V34 = −Φ(Sair t ) − Φ(Sair b ) (29)
The measured voltages V1′ 2′ and V3′ 4′ define two Maxwell-
Faraday surfaces S + Sair + and Sair - :
V2′ 1′ + V4′ 3′ = − Φ(Sair t ) − Φ(Sair b )
− Φ(Ssample ) − (V14 + V32 ) (30) V2′ 1′ + V14 + V43 + V32 = −Φ(S) − Φ(Sair + ) (39)
To obtain the magnetic flux variation inside the sample, two V6′ 5′ = −Φ(Sair - ) (40)
extra assumptions are made to remove parasitic effects: ⇒ V2′ 1′ − V6′ 5′ =
• the residual vertical electric field is negligible: 1
− (V32 + V14 ) − Φ(Sair + ) + Φ(Sair - ) − Φ(Ssample ) (41)
2
V14 + V32 ≈ 0 (31)
To simplify Eq. (41), the ”no air flux term” assumption is
• the air flux term is negligible: modified in ”negligible air flux outside the air loop”:
Φ(Sair t ) + Φ(Sair b ) ≈ 0 (32)
Φ(Sair + ) − Φ(Sair - ) ≈ 0 (42)
In this case, the magnetic flux variation inside the material
for the OS setup is given by: In this case:
⃗
( RR
∂B
ZZ ⃗
∂B · ⃗ndS ≈ 2(V1′ 2′ − V5′ 6′ )
· ⃗ndS ≈ V1′ 2′ + V3′ 4′ (33) RRSsample∂ B⃗∂t (43)
Ssample ∂t Sair - ∂t
· ⃗ndS = V5′ 6′
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V2′ 1′ + V14 + V4′ 3′ + V32 = ΣΦ (48a)
ΣΦ = −Φ(S
air t + ) − Φ(Ssample ) − Φ(Sair b + )
V6′ 5′ = −Φ(Sair t - ) (48b)
V8′ 7′ = −Φ(Sair b - )
(48c)
Combining these equations gives a first link between the
four measured voltages and the magnetic flux variation in the
sample:
Fig. 20: Air and sample surfaces in the Transverse Needle
Probe Setup (TNPS). V2′ 1′ + V14 + V4′ 3′ + V14 − V6′ 5′ − V8′ 7′ =
= −[Φ(Sair t + ) − Φ(Sair t - )] − Φ(Ssample )
C. Transverse Needle Probe Setup (TNPS) − [Φ(Sair b + ) − Φ(Sair b - )] (49)
Fig. 20 shows the Maxwell-Faraday surfaces for the TNPS. With the assumptions (6) and that the air surfaces are
The two measured voltages V1′ 4′ and V2′ 3′ can be exploited identical (Sair t + = Sair t - , Sair b + = Sair b - ):
for a differential measurement:
ZZ ⃗
∂B
V4′ 1′ = −V14 − Φ(Sair + ) − Φ(Ssample + ) (44) · ⃗nds ≈ [V1′ 2′ − V5′ 6′ ] + [V3′ 4′ − V7′ 8′ ] (50)
V3′ 2′ = −V23 − Φ(Sair - ) − Φ(Ssample - ) (45) Ssample ∂t
⇒ V4′ 1′ − V3′ 2′ =
− (V14 − V23 ) − [Φ(Sair + ) + Φ(Sair - )] − [Φ(Ssample + ) − Φ(Ssample - )] A PPENDIX II
(46) D ETAILED CALCULATIONS FOR THE CNPS
If Eq. (6) and (32) are verified: This section details the calculations for the CNPS to obtain
the equation linking the magnetic flux variation in the sample
ZZ ⃗
∂B Φ(Ssample ) and the measured voltages ei . Fig. 22 and 23 de-
· ⃗nds ≈ V1′ 4′ − V2′ 3′ (47)
S ∂t scribe the setup and the associated Maxwell-Faraday surfaces.
Fig. 21: Air and sample surfaces in the Complete Needle Probe e1 − e3 = −Φ(Ssample ) − Φ(Sair tot top ) − Φ(Sair tot bottom ) (51a)
Setup (CNPS). e2 = −Φ(Sair int top ) (51b)
−e4 = −Φ(Sair int bottom ) (51c)
By applying Maxwell-Faraday’s law to the surfaces
Sair t + + Ssample + Sair b + , Sair t - and Sair b - : Eq. (51b) can be simplified thanks to assumptions 3 and 5:
IEEE TRANSACTIONS ON MEASUREMENTS AND INSTRUMENTATION , VOL. XX, NO. X, MONTH 2024 13
∂Bn
Φ(S) = S (63)
∂t
4
∂Bn X
(t) ≈ αk Vkk′ (t) (64)
∂t
k=1
1
α1 = − SG1
α = Lneedles 1
2 Lair SG2
1
(65)
α3 = SG
3
α4 = − LLneedles 1
air SG4
Lneedles
Φ(Sair tot top ) ≈ e2 (58)
Lair
Applying the same reasoning to the bottom surface and
applying Assumption 1 gives:
Lneedles
Φ(Sair tot bottom ) ≈ e4 (59)
Lair
Fig. 24: Lengths and angle definition for the angle shift error.
Finally, injecting Eq. (58) on Eq. (51a) gives:
The position of each probe is:
Lneedles
e1 − e3 ≈ −Φ(S) + (e2 − e4 ) (60)
Lair
∆x + Lneedles cos(β) ∆x − Lneedles cos(β)
Lneedles Lneedles , T1′ =
Φ(S) ≈ − e1 − e2 + e3 − e4 (61) T1 = h h
Lair Lair ∆z − Lneedles sin(β) ∆z + Lneedles sin(β)
V1 Lneedles V2 V3 Lneedles V4 (66)
Φ(S) ≈ − − + −
G1 Lair G2 G3 Lair G4
−∆x + Lneedles cos(β)
−∆x − Lneedles cos(β)
(62) −h , B3′ = −h
B3 =
In the classical case in which the magnetic flux is supposed −∆z + Lneedles sin(β) −∆z − Lneedles sin(β)
uniform inside the sample: (67)
IEEE TRANSACTIONS ON MEASUREMENTS AND INSTRUMENTATION , VOL. XX, NO. X, MONTH 2024 14
The normal to the air surface (defined by T2 and T2′ ) on the In the general case, one can return to the case αX = 0 by
XZ plane is given as [sin(γ); cos(γ)], hence: rotating the X axis, hence this case will be considered in this
section.
Φeffective (Sair t - ) = Φideal (Sair t - ) cos(γ) (76) In RUV , and taking into account ∆G and ∆α, B ⃗ becomes:
Like the liftoff, the air-sample angle mismatch will merely
add a constant coefficient to the measured air flux, which will
(
BU (t) = BX (t)
result in an increased drift on the experimental B(H) loops:
BV (t) = (1 + ∆G) [−BX (t) sin(∆α) + BY (t) cos(∆α)]
dΦmeas (80)
Vind = (77)
dt (
Φmeas = Φ(S) + [1 − cos(γ)]Φ(Sair t ) (78) BU (t) = B(t) cos(α)
BV (t)
However, in the large majority of cases, the error generated 1+∆G = −B(t) sin(∆α) cos(α) + B(t) cos(∆α) sin(α)
by the air-sample angle mismatch can be ignored, since (81)
cos(γ) > 0.99 for |γ| < 8°. Only evident alignment issues (
can have a noticeable effect on the measured flux. BU (t) = B(t) cos(α)
(82)
BV (t) = (1 + ∆G) [B(t) sin(α − ∆α)]
D. Gain mismatch and non-orthogonality angle
Two main sources of error in the 2D reconstruction have ⃗ and angle α of B
The norm ||B|| ⃗ in the two frames will
been identified: be:
• the gain mismatch ∆G between two inputs, linked to the
(
fact that two sets of each electronic component (whose ⃗ XY = |B(t)|
||B||
gain can be regulated thanks to resistors) will more often (83)
αXY = α
than not have different performances (or values, in the
case of resistors);
• the non-orthogonality angle ∆α between the two mea-
q
⃗ U V = |B(t)| cos2 (α) + (1 + ∆G)2 sin2 (α − ∆α)
||B||
surement axis. This angle can have a noticeable value, h i
since the needle distance is usually small. For example, αU V = atan (1 + ∆G) sin(α−∆α)
cos(α)
for a needle distance of 10 mm and a positioning uncer- (84)
tainty of 0.5 mm, then ∆α = atan(0.5/10) = 2.8°. Hence, if ∆G and ∆α are not zero, both ||B|| ⃗ and αU V
The measured 2D magnetic field can be described in two will change in function of the excitation angle α. Even if, in
frames of reference: the 1D case, the difference αU V will be constant since α is
• the external orthogonal frame of reference, of axis X and ⃗
fixed, in the case of rotating magnetic fields the measured B
Y: RXY ; will be distorted, which requires to measure experimentally
• the needle probes frame of reference, defined by the ∆G and ∆α to obtain an accurate induction measurement.
normal of the two pairs of probes U and V: RUV . The magnitude and angle distortions are noted ϵM and ϵA and
RUV is not orthogonal a priori, the angle between U and V are given below:
being π2 − ∆α. Moreover, several other angles can be defined:
the angle between the U and X axis αX and between the V and
⃗
ϵM (α)
= |||B(t)|
B||U V
−1
Y axis αY and the angle between the magnetic field and the p
= cos (α) + (1 +h ∆G)2 sin2 (α − ∆α)i− 1
2 (85)
X axis (or the U axis) θ (or α). This also implies that θ = α
= αU V − α = atan (1 + ∆G) sin(α−∆α)
ϵA (α) −α
and αY = ∆α. The different angles are shown in Fig. 26. cos(α)
(1 + x)2 ≈ 1 + 2x
sin(α − x) ≈ sin(α) − x cos(α)
Fig. 26: Angle definitions. sin2 (α − x) ≈ sin2 (α) − x sin(2α)
√ x
⃗ is assumed 1D, and can be described
The magnetic field B 1+x≈1+
2
in RXY as follows: x
( atan(α + x) ≈ atan(α) + 2
BX (t) = B(t) cos(α) α +1
(79)
BY (t) = B(t) sin(α) Hence:
IEEE TRANSACTIONS ON MEASUREMENTS AND INSTRUMENTATION , VOL. XX, NO. X, MONTH 2024 16
∆α 1 p
min ϵA (θ) + =− |∆α| + ∆α2 + ∆G2 (89)
2 2
∆α 1 p
max ϵA (θ) + = |∆α| + ∆α2 + ∆G2 (90)
2 2
In most cases, ∆α should be negligible compared to ∆G:
for example, a gain mismatch of 10% will be matched by
∆α ≈ 6°, which can be easily avoided by carefully manufac-
turing the needle probes support.