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  • Lab Work Progress: Name: Nurul Shuhada Binti Abdul Razak ID: SA16096

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    Nurul Shuhada conducted an experiment to determine the acid value of biodiesel samples produced using different catalyst bead loads and reaction temperatures. The methodology involved preparing reagents and running a titration. Results showed that acid value decreased with increasing temperature and more catalyst beads. Various characterization techniques were then used to analyze the catalyst, including FTIR, FESEM, BET, TGA-DTG, and BET.

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    Remove TAN in diesel fuel

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    Lab Work Shu

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    Nurul Shuhada conducted an experiment to determine the acid value of biodiesel samples produced using different catalyst bead loads and reaction temperatures. The methodology involved preparing reagents and running a titration. Results showed that acid value decreased with increasing temperature and more catalyst beads. Various characterization techniques were then used to analyze the catalyst, including FTIR, FESEM, BET, TGA-DTG, and BET.

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    1 views4 pages

    Lab Work Progress: Name: Nurul Shuhada Binti Abdul Razak ID: SA16096

    Uploaded by

    Matt Detectorist
    Nurul Shuhada conducted an experiment to determine the acid value of biodiesel samples produced using different catalyst bead loads and reaction temperatures. The methodology involved preparing reagents and running a titration. Results showed that acid value decreased with increasing temperature and more catalyst beads. Various characterization techniques were then used to analyze the catalyst, including FTIR, FESEM, BET, TGA-DTG, and BET.

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    © All Rights Reserved
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    of 4

    LAB WORK PROGRESS

    NAME: NURUL SHUHADA BINTI ABDUL RAZAK


    ID: SA16096
    METHODOLOGY

    A. Preparation of NH3-EG (ammonia-ethylene glycol)


    B. Preparation of ET-KOH solution
    C. Preparation for reaction (blank)
    D. Titration

    `
    `
    RESULTS FOR ACID VALUE

    By using this equation,


    Acid value= volume Et-KOH consumed X Molarity of Et-KOH X 56.11
    sample size (g)
    400°C 700°C 900°C
    1 bead 3 beads 1 bead 3 beads 1 bead 3 beads

    10:90 0.84 0.79 0.79 0.67 0.45 0.45

    30:70 0.61 0.67 0.79 0.67 0.28 0.40

    50:50 0.67 0.56 0.67 0.79 0.45 0.37


    CHARACTERIZATION OF CATALYST

    • FTIR
    • FESEM
    • BET
    • TGA-DTG
    • BET

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