BATCH RECORD FRAKSINASI MINYAK JAHE MERAH batch 1

FORM ISIAN PROSES

BATCH : 1
KODE BAHAN : MJM
TEKANAN : 10 mmhg
TANGGAL : 22-Okt-21
UMPAN : 600 gram
OPERATOR : RISNA

PERTAM
CUTTING
TEKANAN SUHU (°C) PENAM BAHAN
FRAKSI JAM FRAKSI NOTES
(mmhg) PUNG BERAT
TEORITIS BAHAN UAP 1
22/10/2021 (ml)
10 10.14 20 - 1 0
10 10.38 80 42 1 0
F1
10 10.50 85 49 1 40
10 11.03 90 50 2 30 70 mL
10 11.18 120 45 2 10 mati lampu
15 11.38 142 30 2 0
F2
15 12.13 159 100 2 40
15 12.40 170 120 2 40 80 mL
15 13.00 185 150 2
15 13.20 190 150 2

25/10/2021 10 10.00 20 -
10 10.30 80 42
10 11.15 90 49
10 12.00 100 50
10 12.30 120 45
10 12.45 135 30
10 13.30 163 100
10 14.30 180 120
10 15.15 190 150
10 16.30 198 150

TOTAL 150 ml
RESIDU 350 ml
 FORM ISIAN PROSES

BATCH : 2
KODE BAHAN : MJM
TEKANAN : 10 mmhg
UMPAN : 650 gram
OPERATOR : RISNA

PERTAM
TEKANAN SUHU (°C) PENAM BAHAN
JAM FRAKSI NOTES
(mmhg) PUNG BERAT
BAHAN UAP 1
01/11/2021 (ml)
10 09.40 20 -
10 10.44 25 21 1
10 11.12 80 50 1 15
10 11.24 92 80 1 70 F1
10 11.30 95 80 1 20 115 gr
10 11.52 120 72 2
10 12.04 130 80 2 20
10 12.35 140 73 2 20
10 13.00 145 65 2 15 F2 45 gr
10 13.06 145 65 2
10 13.30 145 81 3 5
10 14.00 145 86 3 10
10 14.30 148 83 3 10
10 15.00 148 68 3 10 F3 35 gr

BATCH RECORD FRAKSINASI 02/11/2021

10
10
10
09.20
10.00
10.30
25
94
100
21
25
30
1
1
1
-
-
-

MINYAK JAHE MERAH batch 2

10 11.00 120 40 1
10 11.30 139 43 1
10 12.00 148 100 1 20
10 12.30 152 120 1 10
10 13.00 152 120 1 30
10 13.30 152 120 1 20
10 14.00 152 120 1 10
10 14.30 152 120 2 25
10 15.00 152 120 2 10
10 .15.30 152 120 2 10 F4 125 gr

10 09.25 25 27
03/11/2021
10 10.15 80 27
10 11.00 100 27
10 11.30 110 27
10 12.00 125 27
10 12.30 136 32
10 13.00 140 50
10 13.30 145 80
10 14.00 150 90
10 14.30 150 100
10 15.00 152 100
10 .15.30 152 100
10 16.00 158 100
10 16.30 158 110 3 5
10 17.00 158 110 3 40
10 17.30 158 110 3 30
10 18.00 158 115 3 30
10 18.30 158 115 4 20
10 19.00 158 115 4 25 F5 135 gr
10 19.30 160 120 -
10 20.00 160 122 -
TOTAL 480 ml 455 gram
RESIDU 265 ml 195
 Data Tabulasi Hasil Analisa GCMS Fraksi Minyak Jahe Merah

M.Jahe Merah F1. Jahe Merah F2 . Jahe Merah R. Jahe Merah

NO SENYAWA
R.TIME KADAR (%) R.TIME KADAR (%) R.TIME KADAR (%) R.TIME KADAR (%)
1 β Ocimen 10.832 4,230
2 α Pinene 10.907 15,01
3 Camphene 11.321 32,504 11.320 12,382
4 6-Methyl-5-Hepten-2one 12.125 16,572 12.129 21,257
5 β Myrcene 12.719 4,405 12.788 10,481 12.794 7,954
6 β Phellandrene 13.904 7,561
7 trans Sabinene Hydrat 13.978 13,328 13.985 19,414
8 Cyclobutane 14.040 4,126 14.407 6,275
9 2-nonanone 15.783 3,248
10 Nerol 20.961 5,573
11 Citral 21.178 3,390
12 Benzene (α curcumene) 27.475 5,618 27.543 16,48
13 Zingiberene 27.920 28,57 27.968 30,323
14 β Cubebene 28.144 7,515
15 Farnesene 28.171 8,422 28.231 6,509
16 β Bisabolene 28.284 8,987 28.348 11,694
17 β Sesquiphelandrene 28.633 18,359 28.690 11,646
18 Sabinene 28.827 3,282
19 Trimethyl 28.918 3,69
PENGUJIAN AKTIVITAS ANTIOKSIDAN MINYAK JAHE MERAH

IC 50 Minyak Jahe Merah

60%
f(x) = 0.01 x + 0.01
Peredaman 50%
R² = 0.87
KONSENTRASI ABSORBANSI IC50
(%Inhibisi)
0 0,876 0% 40%
16 0,862 2%

%Inhibisi
32 0,607 31% 30%
72,0
48 0,48 45%
20%
64 0,476 46%
80 0,442 50%
10%

Nilai IC50 (50-100), termasuk ken dalam kategori 0%

0 10 20 30 40 50 60 70 80 90
antioksidan sedang KONSENTRASI (ppm)
Linear ()
 PENGUJIAN AKTIVITAS ANTIOKSIDAN ASAM ASKORBAT

Peredaman
KONSENTRASI ABSORBANSI IC50
(%Inhibisi)
0 0,876 0%
3 0,869 1%
6 0,852 2%
16,8
9 0,795 9%
12 0,607 31%
15 0,490 44%

Nilai IC50 (0-50), termasuk ke dalam kategori

antioksidan KUAT