Green University of Bangladesh

Topic- Standardization of Sodium Hydroxide solution

with standard Oxalic Acid solution
CHE106

CREATED BY, ASSIGNED BY,

MD. RAHUL ISLAM JOY – 212902070 MR. SUBRATA PAL
ABDULLAH HASBIN SANET - 212902008 LECTURER
JUNDUB AHMED – 212902023 DEPARTMENT OF TEXTILE
FARZANA ISLAM JENIA - 212902010 GREEN UNIVERSITY OF BANGLADESH
Standardization of Sodium Hydroxide solution with
standard Oxalic Acid solution
Content

 Introduction
 Theory
 Phenolphthalein
 Precautions
 Preparation
 Titration
 Observations
 Calculation & Results
 Discussion
Introduction

 Standard solution.
 Objectives
Theory

 Acid base Titration

 Reaction
 Formula: (COOH)2 + 2NaOH → (COONa)2 + 2H2O
Why Phenolphthalein is used as indicator

Phenolphthalein
Precautions

 Weighing of oxalic acid crystals need weights of 2g + 1g + 100mg + 50mg.

 While weighing do not spill the substance on balance pan.
 Rotate the knob of balance gently.
 Keep the weights in weights box at proper places after weighing
 Wash the watch glass carefully so that even a single crystal is not left on the watch glass.
 Bring the watch glass close to funnel while transferring weighed substance and transfer it gently. Wash it
repeatedly with distilled water.
 Wash the burette with water after titration is over.
 The last few drops should be added using pipette to avoid extra addition of distilled water above the
mark on the neck of the measuring cylinder.
Preparation of Standard Oxalic Acid Solution  (C2H2O4.2H2O)
Titration of Sodium Hydroxide and Oxalic Acid Solution
Observations
 Calculation & Result

50 42.6 7.8

42.4 34.4 8

34.4 26.4 8

Determinate strength of NaOH solution is 0.08

Discussion
Thank you! sir
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