TECHNIQUE S PREPARED BY: MARK JESSON L. SOPOSO SEPARATION TECHNIQUES
Although very useful in separating, analysing, and
identifying the components of a mixture, chromatography does not allow you to separate the components of a mixture into usable form. In cases when you need usable forms of the component of a mixture, you use other methods of separation. SEPARATION TECHNIQUES
The choice for the separation technique will depend on the
properties of the substances within your mixture. Different methods will be used in separating a solid from another solid and in separating a liquid from a solution.
Here are a few separation techniques and how and when to
use them. Mechanical or Manual Separation
Thismethod is used to manually
separate (with the use of hands, forceps, sieves, magnets, or tongs) a solid from another solid. For example, Filtration
This method is used to separate
small, insoluble solid particles dispersed or suspended in a liquid medium (e.g., SAND in WATER). In this process, the liquid medium and the suspended particles are passed through a filter or sieve. The solid particles retained in the filter or sieved are called residues, and the liquid that passes through the filter is called the filtrate. Decantation
This method is used to separate a dense
and insoluble solid (i.e., too large to be filtered using standard filtration setup) from liquid. Example, In washing rice, you slowly tilt the container so that the water will spill over slowly, leaving the rice grains in the container Evaporation
Insoluble solids can be obtained
form a liquid suspension either through filtration or decantation. However, some solids like salt and sugar dissolve after being placed in water. Toseparate dissolved solids from liquid solution, you can simply heat the solution until all the water or liquid evaporates, leaving the solid behind. This process is called evaporation to dryness. This method is used by salt farmers in Pangasinan to obtain salt from seawater. Using a Separating Funnel
Liquids such as oil and
water do not readily mix. Liquids that do not mix or dissolve in each other are called immiscible liquids. Immiscible liquids can be separated from one another using a separating funnel In using this technique, first put the two liquids inside the separating funnel, making sure that the tap is closed. Place a beaker under the funnel and then open the tap. This will allow the lower layer to drain to the beaker. Close the tap after draining the lower layer. Dissolution
This method is used to separate an insoluble solid from a
soluble solid using a liquid solvent. Suppose you spill a cup of sugar in your rice container. Separating the sugar from the rice manually can be difficult. However, you can separate the rice from the sugar simply by washing the rice. The sugar dissolves in water. Distillation In the process of evaporation, only the dissolved solid can be obtained. The liquid solvent evaporates into the atmosphere. How can you collect a liquid from a solution? The liquid solvent can be separated from a solution through a process called distillation. This method involves heating the solution until it boils and then condensing vapour back to liquid form in a separate container. Pure water can be distilled from a salt solution using distillation. The extracted liquid from a distillation process is called distillate.