G 05512005

14 12 1
(JISF) (JSA)

JIS G 0551 : 1998 JIS G 0552 : 1998

ISO 643 : 2003SteelsMicrographic

determination of the apparent grain size

JIS G 0551
A

B
C

5 JIS
B 2 (ASTM)

G 05512005

1
1.

2.

3.

4.

5.

6.

6.1

6.2

6.3

7.

7.1

7.2

10

8.

13

8.1

13

8.2

13

9.

14

15
B

16

32

36

38

40

41

JIS 44

3
G 05512005

JIS
G 05512005

SteelsMicrographic determination of the apparent grain size

2003 2 ISO 643SteelsMicrographic determination of the

apparent grain size

5
1.

ISO/IEC Guide 21 IDT
MOD

NEQ
ISO 643 : 2003, SteelsMicrographic determination of the apparent grain size (MOD)

2.

JIS G 0561
ISO 3785

3.

SteelDesignation of test piece axes

3.1

3.1.1

3.1.2

0.25 %

3.2

1 mm2 m G

4
G 05512005

m = 8 2G
m 16 G 1
3.3

(intercept) N

1
1/2 N
N
LT mm N L

3.4

(intersection) P

P
P LT mm
P L

3.5

5 5

6.3.2

925 (McQuaid

Ehn)
3.6

1 3

20 % 3

5
G 05512005

(N) 16
(21/21)N7

(P) 7 P7

(N) (P)

6
G 05512005

4.

1
1

1
a=
m

mm

AF

mm2

mm

d=

79.8 mm
( = 5 000mm2)
100

g 100

K=

1
m

g
100

1 mm l = 1 / N L = 1 / PL

l
L

mm

LT

mm

1 mm2

g 100

n1

n2

n 100

D 100

ng

D g

NL

Nx

1 mm

Ny

1 mm

Nz

1 mm

P
PL

m = 2n100 100
m = 2K2ng g

n100 = n1 +

NL =

N
LT

PL =

P
LT

n2
2

N xN y N z ISO 3785

ISO 3785 : 1976

a)

b)

c)

Y X Z

7
G 05512005

5.

a) b)
7.1.1

a)
1)

7.1.2

2)

planimetric method
7.1.3

1
7.2

b)

1 C 1

6.

6.1

6.2

25 %

6.3
6.3.1

(Glyceregia)
(Kalling) (No. 2) (Marbles)

60 % 1.4 V 60120
10 % 6 V 60
60 %
6.3.2 6.3.3

6.3.2

925 (McQuaidEhn)

6.3.2.1

925

8
G 05512005

6.3.2.2

2 925 6
600 30150 /h 1 mm

6080 % 4020 %
30

6.3.2.3

a)

6 V 60

b)

25 %
a) b)

le ChatelierIgewski 2 g
25 g 100 ml

6.3.3

a)

BechetBeaujard 6.3.3.1

b)

(Kohn) 6.3.3.2

c)

6.3.3.3

d)

6.3.3.4

e)

6.3.3.5

f)

g)

6.3.3.1
6.3.3.1.1

1)

2)

BechetBeaujard

(P) 0.005 %
6.3.3.1.2

BechetBeaujard

9
G 05512005

a)

0.35 %85010 1.5

b)

0.35 %88010 1.5

6.3.3.1.3

0.5 %

1 60

6.3.3.2
6.3.3.2.1

(Kohn)

6.3.3.2.2

1 Pa

10 15

6.3.3.2.3

6.3.3.2.2

(Vilella) 1 g 5 ml 100 ml

(Differential Interference Contrast)

6.3.3.3

6.3.3.3.1

0.250.6 %

1 % 1 % 1.5 %

6.3.3.3.2

10
G 05512005

650720

1.

15
20
12 mm6 mm3 mm

2.

6.3.3.3.3

6.3.3.4
6.3.3.4.1

0.7 %

6.3.3.4.2

Ac3

30

a)

1225 mm

b)

6.3.3.5

482704

6.3.3.6

7.
7.1

7.1.1

3.2 (1)

m = 8 2 G (1)
(1) (2a) (2b)

G=

log m
3 (2a)
log 2

G=

log m
3 (2b)
0.301

11
G 05512005

7.1.2

100 B 1

(00) 10 G

B
0.5
3 510
g 100 G
M

G = M + 6.64 log

g
(3)
100

2
2

25

50

100

200

10

400

10

11

12

500

5.6

6.6

7.6

800

8.6

9.6

10

11

10.6

11.6

12.6

12

13

14

7.1.3

(Planimetric method)

C C.1
7.1.4

1
510 3

G=

(a b )
b

G
a
b
3

12

6.5
7

6
2

39
14

10

65

ab

G
65
6.5
10

12
G 05512005

7.2

(N) (P)

2
2 500 mm
mm

mm

79.58

250.0

53.05

166.7

26.53

83.3
500.0 mm

150 mm 100 mm

7.2.3 3

50
250

13
G 05512005
mm

2
7.2.1

P
N P

7.2.1.1

a)

N1

b)

N0.5

c)

N0.5

7.2.1.2

a)

P1

b)

P1

c)

P1.5
C C.2 (Snyder-Graff)
N
2 2

14
G 05512005

7.2.2

2
2 500 mm
4050
250 mm
25

1.5 2
7.2.3

N P

N P

LT
N L = N / LT PL = P / LT

N P
2

1 mm N L 1 mm PL

N L = ( N LX N LY N LZ )1 / 3 PL = ( PLX PLY PLZ )1 / 3

XY Z

1.

1 mm N L 1 mm PL
1 (l) C 1

2.

1.

2.

3.

15
G 05512005

3
8.

8.1 8.2 3

8.1
8.1.1

FG
8.1.2

FG3.5(10)
8.2
8.2.1

10 3.5

Gc925 (McQuaidEhn) (6.3.2)

Gb BechetBeaujard (6.3.3.1)
Gk (Kohn) (6.3.3.2)
Gp (6.3.3.3)
Gg (6.3.3.4)
Gm (6.3.3.5)
Gf 1
Gd2 1
Gh 1
Gj 1
Go 1
Gs 1
Gq 1

16
G 05512005

8.2.2

a)

Gc8.5(10) 6.3.2. 925 (McQuaidEhn)

10 8.5

Gf6.5(10) 920 l.5 h 1 920 1.5 10

6.5
b)

Gc3.6(10) 6.3.2. 925 (McQuaidEhn)

10 3.6

9.

a)

b)

c)

d)

ASTM E112-96e2

Standard Test Methods for Determining Average Grain Size

925
(McQuaidEhn) 6.3.2

Bechet
Beaujard 6.3.3.1

0.005 %

(Kohn) 6.3.3.2

6.3.3.3

0.250.6 %
MnMo1 %Cr1 %CrMo1.5 %CrNi

6.3.3.4

0.70.8 %

6.3.3.5

0.025 %

Mn 550600

6.3.3.6

6.2

Accm

2 1

ASTM E112 Plate

925 (McQuaidEhn)
Plate

ASTM E112 Plate

B 1

100

 ASTM E112 Plate

B 1

100

 B 1

100

 ASTM E112 Plate

B 1

100

 ASTM E112 Plate

B 1

100

 ASTM E112 Plate

B 1

100

 ASTM E112 Plate

B 1

100

 ASTM E112 Plate

B 1

100

 ASTM E112 Plate

B 1

100

 ASTM E112 Plate

B 1

100

 ASTM E112 Plate

B 1

100

ASTM E112 Plate

B 2

 ASTM E112 Plate

B 2

 ASTM E112 Plate

B 2

 ASTM E112 Plate

B 2

18

C.1 (Planimetric method)

79.8 mm
50
C 1

D=79,8 mm
AF=5 000 mm2
C 1

2 (n1, n2) n1 n2

n100 = n1 +

n2
(C.1)
2

1 mm2 m
m = 2n100 (C.2)
g m

g2
ng (C.3)
m =
5 000
5 000 (mm2)

19

(1/2) (1/2)

50 2 %

1/4 3/4

n1

n2 C 2
C.1
n100 = (n1 + 0.5n2 + 1) (C.4)

C 2

1 mm2 m

g2
m = n g (C.5)
AF
AF (mm2)
1 mm2

a=

1
(C.6)
m

20

d = a 1/2(C.7)
m G C 1 (C.2) (C.3) (C.5)
m G
C 1

1 mm m

1
d
a

mm
mm2

l
mm
7

0.062 5

0.046

0.092

0.125

0.092

0.185

0.25

0.185

0.50

0.37

1 mm

16

3.577

0.279

2.828

2.529

0.395

0.37

1.788

0.559

0.75

1.414

1.265

0.790

0.75

1.5

0.894

1.118

1.5

0.707

0.5

0.632

1.582

1(00)

0.500

0.25

0.447

2.237

12

0.354

0.125

0.320

3.125

16

12

24

0.250

0.062 5

0.226

4.42

32

24

48

0.177

0.031 2

0.160

6.25

64

48

96

0.125

0.015 6

0.113

8.84

128

96

192

0.088 4

0.007 81

0.080

12.5

256

192

384

0.062 5

0.003 90

0.056 6

17.7

512

384

768

0.044 2

0.001 95

0.040 0

25.0

1 024

768

1 536

0.031 2

0.000 98

0.028 3

35.4

2 048

1 536

3 072

0.022 1

0.000 49

0.020 0

50.0

4 096

3 072

6 144

0.015 6

0.000 244

0.014 1

70.7

10

8 192

6 144

12 288

0.011 0

0.000 122

0.010 0

100

11

16 384

12 288

24 576

0.007 8

0.000 061

0.007 07

141

12

32 768

24 576

49 152

0.005 5

0.000 030

0.005 00

200

13

65 536

49 152

98 304

0.003 9

0.000 015

0.003 54

283

14

131 072

98 304

196 608

0.002 8

0.000 007 5

0.002 50

400

15

262 144

196 608

393 216

0.002 0

0.000 003 7

0.001 70

588

16

524 288

393 216

786 432

0.001 4

0.000 001 9

0.001 20

833

17

1 048 576

786 432

1 572 864

0.001 0

0.000 000 95

0.000 87

1 149

C.2 (SnyderGraff)
C.2.1

C.2.2

10 %

21

C.2.3

1 000 125 mm

5
C.2.4

1
C.3
C.3.1

ASTM G (ASTM)

C.3.2 1

G (ASTM) = 0

100 32.0 mm 1

0
a)

1
G (ASTM) = 3.287 7 6.643 9 log10 l (C.8)

b)

G (ASTM ) = 3.287 7 6.643 9 log10 N L (C.9)

C.3.3

G (ASTM) = 1 (1 mm2) 15.5

(1 mm2)
G (ASTM ) = 2.954 2 + 3.321 9 log10 m (C.10)
C.3.4

ASTM

1 1/20
1/2
7.1.1 2a2b
G = 3 + 3.321 9 log10 m (C.11)
(C.10)
G (ASTM ) G = 0.045 8

JIS G 0551

1.

2.

30 1.5

a)

A3

b)

1015 mm 3050 mm

1015 mm Al 2050
2030
0.4 mm

c)

1015 mm 1015 mm

1
1 g 1.181.5 ml
100 ml
d)

15 mm 40 mm

10 mm 5 mm

JIS G 0561
e)

1015 15 %

210

f)

10 % 10 % 65 %

g)

JIS G 0552

1.

2.

1
1 10 50

1
2

m I1 I 2
n = 500

100 L1 L2
G=

log n
+ 1 1
0.301

G
n
m
L1 L2

100 25 mm

1
mm
I1 I2 L1 L2

2 1 2 (1) n G
3.

a)

2 (1) 2 1

b)

(1)
100 25 mm
25 mm 2 (1) 2 1

(1)

2 1

1.

2.

3.

7.1.4

3.1

FG[3 (70 %)6 (30 %)](10) 10 3 70 %

6 30 %
3.2

1.

Gf6.3(13){6.8 (67 %)2.5 (33 %)}(7) 920 1.5 h 1 920

1.5 20
13
6.3 7
6.8 67 % 2.5
33 %
2.

Gf6.3(3)2.5(7) 920 l.5 h 1 920

1.5 10
3
6.3 7
2.5
3.

Gf{6.8 (67 %)2.5 (33 %)}(20)920 1.5 h 1 920

1.5 20

6.8 67 % 2.5 33 %

JIS G 0552

1.

2.

B
4 1

4 1

100

4 1

100

44

5
JIS G 05512005

ISO 643 : 2003

SteelsMicrographic determination of the apparent grain size

() JIS

JIS

() ()

() JIS

() JIS

1.

ISO 643

1.

IDT

2.

3
ISO 3785
JIS G 0552
JIS G 0561

2.

3
ISO 3785
ISO 14250
ASTM E 112

MOD/

ISO 14250
JIS G 0561

ISO 14250 Steel Metallographic

characterization of duplex grain size
and distributions.

ASTM E112
JIS G 0561 JIS

3.

3.

MOD/

JIS
ISO

4.

4.

IDT

JIS
5 %

JIS G 0552 : 1998

5 %
5 %

5.

IDT

6.1

IDT

6.2

25 %

6.2

23 %

MOD/

43

G 05510000

5.
6.1

10

JIS G 05512005
() JIS

6.3.1

6.3.2
925

(McQuaid
Ehn)
6.3.3

7.1.1

7.1.2

7.1.3

7.1.4

ISO 643 : 2003

SteelsMicrographic determination of the apparent grain size

925

() ()

6.3.1

6.3.4

() JIS

IDT

MOD/

(McQuaid Ehn)

7 a)g)

6.3

MOD/

7.1.1

IDT

ASTM
E112

7.1.2

ASTM E112
a b

MOD/

7.1.3

IDT

510

7.1.4

MOD/

() JIS

JIS

ISO

925

JIS

JIS

1 ISO

JIS ASTM E112

ASTM E112

JIS ISO

JIS

ISO
JIS

11

JIS G 05512005
() JIS

7.2

ISO 643 : 2003

SteelsMicrographic determination of the apparent grain size

() ()

7.2

() JIS

MOD/

JIS G 0552 : 1998

3 ISO 14250
ISO 14250 3

ISO
14250

() JIS

8.

8.

ISO

MOD/

JIS

9.

9.

MOD/

8.
JIS

MOD/

1
JIS

ISO

ASTM E112

ASTM E112

MOD/

ISO

C.3.2
1

C
(C.8)

G (ASTM) L

MOD/

(C.8) L l

1
l ISO

JIS

12

JIS G 05512005

ISO 643 : 2003

SteelsMicrographic determination of the apparent grain size

() JIS

() ()

() JIS

() JIS

MOD/

ISO

ISO

MOD/

ISO

ISO

MOD/

ISO

ISO

MOD/

ISO

JIS
ISO

JIS MOD
1.

2.

IDT
MOD/
MOD/
MOD/
JIS
MOD

13

JIS
G 05512005

g
100

g
100

17 11 1