COURSE OUTLINE

Department & Faculty: Chemical Engineering Dept, FKKKSA Subject & Code: Separation Process I (SKF 3323) Total Lecture Hours: 3 x 14 weeks Page 1 of 4 Semester: 1 Academic Session: 2007/2008

Lecturer Room No. Tel. No. E-mail Webpage: Prerequisite Synopsis

: : : : : : :

PROF. MADYA DR. MOHD AZIZI CHE YUNUS N12-205 07-5535647 azizi@cheme.utm.my www.cheme.utm.my/staff/azizi SKF 3323 This course introduces different types of unit operations involved in the chemical and other physical processing industries such as humidification absorption, distillation, liquid-liquid extraction and solid-liquid extraction (leaching). It also deals with design of separation operations using mass transfer principles.

LEARNING OUTCOMES
By the end of the course, students should be able to:

No .

Course Learning Outcome

Programme Learning Outcome(s) Addressed PO2

Assessment Methods

1.

Explain the differences of unit operation involved in the chemical industries Calculate the number of equilibrium stages for plate tower or height/diameter for packed tower in gasliquid separation Calculate the number of equilibrium stages for plate tower or height/diameter for packed tower in gasliquid separation Compare the number of equilibrium stages obtained by graphically and mathematically in absorption or distillation process Determine the number of equilibrium stages and the composition of solute leaving for liquid-liquid extraction and solid liquid extraction Cooperate in team working as part of a group of engineering students working to solve chemical engineering problems

HW, Q, T

2.

PO1, PO3

HW, Q, T, F

3.

PO2, PO5

HW, Q, T, F

4.

PO4, PO5

HW, Q, T, F

5.

PO3, PO4

HW, Q, T, F

6.

PO6,PO7, PO8

HW, PR

(T Test ; PR Project ; HW Homework ; Q Quiz, F Final Exam)

Prepared by: Name: DR. MOHD AZIZI CHE YUNUS Signature: Date:

Certified by: (Subject Panel Head) Name: Signature: Date:

Department & Faculty: Chemical Engineering Dept, FKK

Page 2 of 4 Semester: 1 Academic Session: 2012/2013

Subject & Code: Separation Process I (SKF 3323) Total Lecture Hours: 3 x 14 weeks Problem Solving (CR1 CR4) Lifelong Learning (LL1-LL3) Team working (TW1-TW5)

PROFESIONAL SKILL ADDRESSED

STUDENT LEARNING TIME

Teaching and Learning Activities 1. 2. Lecture Independent Study - self learning - information search - library search - reading - group discussion Assignment (5x) - self learning - group discussion Test (2) And Quizzes Exam (1x) Student Learning Time (hours) 42 55

3.

15

4. 5.

5 3

Total

120

TEACHING METHODOLOGY
Lecture and Discussion, Active Learning, Independent Study, Group Assignment.

Prepared by: Name: PM DR. MOHD AZIZI CHE YUNUS Signature: Date:

Certified by: (Subject Panel Head) Name: Signature: Date:

COURSE OUTLINE
Department & Faculty: Chemical Engineering Dept, FKK Subject & Code: Separation Process I (SKF 3323) Total Lecture Hours: 3 x 14 weeks Page 3 of 4 Semester: 1 Academic Session: 2012/2013

Week #
1-2

Topic
Gas-Liquid Separation Processes (Humidification) Types of separation processes and methods Equilibrium relations between phases Continuous humidification processes Gas-Liquid Separation Processes (Absorption) Absorption in plate and packed towers - dilute and concentrated mixtures Estimation of mass-transfer coefficients for packed towers Vapour-liquid separation processes Equilibrium relationship Simple distillation methods Binary fractional distillation using McCabe-Thiele method Multi-component distillation

Topic Outcomes
It is expected that students will be able to: identify and use equilibrium relationship design packed cooling towers using mass-transfer coefficient and HTU methods

3-5

It is expected that students will be able to: design plate and packed absorption towers using mass-transfer coefficient and HTU methods for dilute and concentrated mixtures determine mass-transfer coefficients

6 - 11

12-13

Liquid-liquid Extraction Types of equipment Phase equilibrium relationship Single-stage liquid-liquid extraction Continuous multistage countercurrent liquid-liquid extraction

It is expected that students will be able to: describe batch distillation and continuous fractional distillation design simple batch distillation design plate distillation column using McCabe-Thiele design multi-component column using FenskeUnderwood-Gilliland correlation . It is expected that students will be able to: identify the most common types of equipment used for liquid-liquid extraction plot extraction equilibrium data on right-triangular diagrams determine equilibrium-stage requirements for single and multistage counter-current liquid-liquid extraction

14

Liquid-solid Extraction (leaching) Equipments for liquid-solid leaching Single-stage leaching Counter-current multistage leaching :

It is expected that students will be able to: identify the most common types of equipment used for leaching determine equilibrium-stage requirements for single and multistage counter-current solid-liquid extraction

References

1) Transport Processes and Separation Process Principles 4 th Ed. by Geankoplis 2) Separation Process Principles by Seader and Henley. 3) Unit Operations of Chemical Engineering 5th Ed. by McCabe, Smith and Harriott.

Grading
No. 1 2 4 5 6 Assessment Assignments Quizzes TEST 1 TEST 2 Final Exam Overall Total Number 5 5 1 1 1 % each 1% 1% 20% 20% 50% % total 5 5 20 20 50 100 4th meeting 8th meeting As scheduled Dates