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Engineering Failure Analysis
Engineering Failure Analysis
www.elsevier.com/locate/engfailanal
Materials, Aeronautic and Automotive Engineering Department, Engineering School of Sao Carlos, University of Sao Paulo,
Sao Carlos-SP, 13.566-590, Brazil
b
Embraer S/A, Sao Jose dos Campos-SP, 12.227-901, Brazil
Received 10 September 2003; accepted 27 September 2003
Abstract
Quantitative fractography techniques have been implemented and frequently used in the Failure Analysis Laboratory
LANAF, at the Engineering School of Sao Carlos, for fatigue life estimations of structural components, whose
fracture surfaces are subjected to detailed inspection with the aid of scanning electron microscopes. This work describes
one of the recent activities in progress at the LANAF, in which fatigue crack initiation and propagation lives have been
estimated for an idealized aeronautical part tested in the laboratory, under variable amplitude loading condition
VAL, i.e., ight simulation testing. Fractographic reconstitution of sub-critical crack growth has been performed
through the identication of marking load patterns left in the wake of the propagating crack, which have been correlated to the signicant load levels applied during the fatigue test. A semi-automated procedure to estimate fatigue lives
under VAL has been developed and implemented by which a virtual marking load pattern is generated and compared
to the real pattern determined fractographically.
# 2004 Elsevier Ltd. All rights reserved.
Keywords: Aluminium alloys; Fatigue markings; Fractography; Marker loads; Quantitative fractography
1. Introduction
Fractographic techniques using scanning electron microscopes (SEM) are extensively used in failure
analysis of aeronautical components and structures [15]. The more advanced procedure employed on the
fatigue life estimation of in-service or in-test fractured components undergoing variable amplitude loading
VAL, is depicted in Fig. 1. The technique consists basically of generating a virtual pattern of fatigue
load marks provided by the applied loading spectrum, using preferably computational techniques, and
compares it with the pattern actually recorded on the fracture surface of the component, obtained through
microscopic survey. In summary, to be successful this procedure depends basically on the correct
* Corresponding author. Tel.: +55-16-273-9590; fax: +55-16-273-9574.
E-mail address: jrpan@sc.usp.br (J.R. Tarpani).
1350-6307/$ - see front matter # 2004 Elsevier Ltd. All rights reserved.
doi:10.1016/j.engfailanal.2003.09.004
548
Fig. 1. Schematic of the failure analysis procedure using quantitative fractography [4].
interpretation of the surface marking pattern printed by the higher cyclic loads (i.e. marker loads)
experienced by a ying aircraft or a tested structural component.
Fig. 2 shows typical load marking patterns impressed by the action of critical load sequences on the
fracture surface of an aeronautical component fatigue tested in the laboratory.
In order to estimate fatigue lives spent in both crack initiation and propagation stages, it is necessary to
obtain a plot similar to Fig. 3. From the numerical integration of the area under this curve, one can also
determine the number of ights as a function of the crack size, as well as the crack growth rate in the
structure or component analyzed.
The correct determination of fatigue crack initiation and propagation lives has obvious and important
implications for several steps of aircraft fabrication and maintenance, such as materials selection, component design, manufacturing processes, non-destructive inspection programs, and the ultimate failure
analysis as well.
In this work, an idealized aeronautical component was fatigue tested in a laboratory environment
in order to simulate its in-service performance under VAL. After testing, the fracture surfaces were
thoroughly analyzed in a SEM. The purpose was to determine the resulting crack surface marking
patterns, which were compared to those derived from a computer program, which had the simulated
ight load history as the input. The methodology described in Fig. 1 has been strictly followed, aimed at
determining both crack initiation and propagation lives of the fatigue-tested component.
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Fig. 2. Typical load marking patterns (arrowed) developed on the fracture surface of a fatigue-tested component: (a) near crack
origin; (b) intermediate location; (c) nal fracture position.
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Weight (%)
Si
Fe
Cu
Mn
Mg
Cr
Ni
Zn
Ti
Ca
P
Pb
Sb
Sn
Sr
V
Zr
B
Cd
Co
Al
Impurities
Fig. 6 shows two ight block sequences imposed on the component during the laboratory test. In total,
20 blocks of 6000 ights were sequentially applied to the component, therefore performing 120,000
simulated ights.
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Fig. 4. Tri-dimensional views of the microstructure of the aluminium alloy: (a) lower and (b) higher magnitude.
Fig. 5. (a) Partial view of the VAL-fatigue-tested component. The black arrow points out the approximate location of the fatigue
crack site. The full length of the failed ligament F2 ! F1 is 23 mm; (b) schematic of the cyclic loading arrangement imposed on the
tested component.
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Fig. 6. Two loading blocks applied sub-sequentially to the component tested, with the severest ight, numbered 1, occurring once at
each applied block of 6000 ights.
After testing, the components fracture surfaces were inspected in a SEM operating at a voltage of 20 kV
in both secondary and backscattered electrons imaging modes. The chief interest was to elucidate the entire
load marking nuances left on the wake of the propagating crack. This task was accomplished by using
image magnications ranging from 10 to 20,000.
A computer program was specically developed to generate virtual marker load patterns from the
available ight load history, which were compared to marking patterns determined fractographically.
During the programming, special attention was devoted to VAL-variables such as maximum tensile stress
peaks and eective number of tensile stress cycles within a block of simulated ights, since reliable
criteria had to be developed concerning the width of virtual marking bands and band spacing as well. Once
the software provided the virtual pattern of load marking bands expected in one block of ights, it was
straightforwardly compared to that real pattern, in an operation that resembled the reading of bar codes.
The procedure was repeated until a minimum matching between virtual and real patterns was achieved.
When a successful correlation was reached, the ight blocks counting along the fracture surface could be
accomplished manually.
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Fig. 7. Microstructural aspects of near fatigue crack site region, where the arrow points out two distinct second phases. The crack site
location, the borehole position and the fatigue crack surface are identied.
Fig. 8. EDX spectrum of (a) white and (b) black phases located in the neighbourhood of the fatigue crack nucleation site in the
borehole F2.
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Table 2
Chemical composition (wt%) of the intermetallic phases shown in Fig. 7
Element
O
Al
Mn
Mg
Cu
Zn
7.03
23.65
0.33
ND
67.76
1.24
0.43
89.47
ND
1.13
1.95
7.03
The copper and zinc contents are highlighted for the white and black phases, respectively. ND: non-detected.
Fig. 9. (a) Top view of the fatigue crack nucleation site pointed out by a white arrow; (b) contact marks due to the friction of the
threaded fastener with the internal surface of borehole F2, indicated by black arrows; (c, d) detail of the marks, where white arrows
indicate the marks and the black one the crack site position; (e) cross-sectional view of one surface mark generated during the
disassembly of the jig, where the white arrow indicates the direction of the movement for the fastener removal.
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Fig. 10. (a) Non-metallic inclusion located at the crack site of the fatigue-fractured ligament F2 ! F1; (b) energy absorption
spectrum resulting from EDX microanalysis.
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Fig. 11. SEM-microfractographs taken from the fracture surface of the fatigue-tested component at three dierent magnitudes of
image: (a) 70, (b) 230, and (c) 700. Arrows indicate the microscopic or local direction of crack growth along the fractured
ligament F2 ! F1.
assessed. Still in Fig. 12, the black arrow points out the fatigue crack nucleus position, which was rst seen
in Figs. 5(a), 7, 9(a), (b), (d) and 10(a).
Fig. 13 presents the resulting plot obtained from the fractographic analysis performed in this study,
according to the graphic format displayed earlier in Fig. 3. Two distinct methods have been used in order
to correlate the experimental data points, namely, general power-law and point-to-point linear tting.
Once the set of data points presented in Fig. 13 had been tted, the numerical integration of the area
under the tting curves was performed.
Fig. 14 plots results from both processes of numerical integration, by which one can estimate fatigue
crack initiation and propagation lives of the aeronautical part tested in fatigue. It can be observed that
power-law data tting predicts longer fatigue crack growth periods than a linear t, and, consequently,
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Fig. 12. Sequential positions occupied by the severest ight number 1 along the fatigue crack path on the ligament F2 ! F1.
Fig. 13. Fatigue crack growth data determined fractographically from the tested component.
Fig. 14. Fatigue crack growth estimations according to distinct tting methods: (a) number of ights vs. crack depth; (b) vice-versa.
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Fig. 15. Mean crack growth rate estimations according to the equivalent ight concept: (a) plotted against crack depth; (b) plotted
against number of simulated ights.
shorter crack nucleation periods, which is inferred to be 49,500 ights according to the former method
(recalling that total life of the component is 120,000 ights). On the other hand, according to the point-topoint linear data tting method, about 60,000 ights were necessary to start the crack growing in fatigue.
Therefore, from Fig. 14, two limiting situations can be postulated regarding periodic non-destructive
inspection and failure prevention of similar in-service components: rst, if fatigue crack initiation is the
main concern, i.e. fail-safe approach, the most conservative method is the power-law integration; second
and conversely, if cracking has already been established in the structural component, propagation becomes
of prime interest, i.e. damage-tolerant approach, and linear point-to-point integration is the most
conservative method.
Fig. 15 plots fatigue crack growth rate in function of crack depth and number of ights, respectively,
considering both integration methods shown in Fig. 13.
Almost imperceptible dierences are established in Fig. 15(a), regarding initial stages of crack growth.
Major dierences are noticed at higher levels of crack extension only. On the other hand, Fig. 15(b) allows
one to clearly dierentiate linear vs. power-law methods, as a result of the large dierences between fatigue
crack growth estimations exhibited in Fig. 14.
5. Concluding remarks
This article described one of the recent activities conducted in the Failure Analysis Laboratory
(LANAF) of the Engineering School of Sao Carlos in the eld of quantitative fractography.
In this study, crack initiation and propagation lives have been estimated for a fatigue tested aeronautical
part subjected to VAL, which has been imposed under laboratory controlled conditions, i.e. ight
simulation testing.
Fractographic reconstitution of sub-critical crack growth has been performed through the identication
of marking load patterns left in the wake of the propagating crack, which have been correlated to
signicant load levels applied during the fatigue test.
559
A semi-automated procedure to estimate fatigue life under VAL has been developed and implemented,
by which a virtual marking load pattern is generated and straightforwardly compared to the real one
determined fractographically.
Implications for the adoption of more or less conservative life estimations methods in the structural integrity
program of commercial eets have been discussed on the basis of both fail-safe and damage-tolerant
approaches.
Acknowledgements
The authors wish to express their gratitude to Embraer S/A for supplying the material tested and for
valuable discussions.
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