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  • 3.lampiran Perhitungan

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    Elsa Rahmadayani
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    This document contains calculations of acidity-alkalinity from experimental data. It determines: 1) The normality of NaOH and HCl standard solutions used in the experiment. 2) The acidity and alkalinity values of a tapioca waste water sample based on titration with NaOH and HCl, finding acidity of 30.624 mg/L CO2 and 0.528 mg/L H+. 3) The acidity and alkalinity of the sample according to Indonesian standard SNI 06-2422-1991, determining values for methyl orange acidity, total acidity, phenolphthalein alkalinity, and total alkalinity.

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    This document contains calculations of acidity-alkalinity from experimental data. It determines: 1) The normality of NaOH and HCl standard solutions used in the experiment. 2) The acidity and alkalinity values of a tapioca waste water sample based on titration with NaOH and HCl, finding acidity of 30.624 mg/L CO2 and 0.528 mg/L H+. 3) The acidity and alkalinity of the sample according to Indonesian standard SNI 06-2422-1991, determining values for methyl orange acidity, total acidity, phenolphthalein alkalinity, and total alkalinity.

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    © All Rights Reserved
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    47 views5 pages

    3.lampiran Perhitungan

    Uploaded by

    Elsa Rahmadayani
    This document contains calculations of acidity-alkalinity from experimental data. It determines: 1) The normality of NaOH and HCl standard solutions used in the experiment. 2) The acidity and alkalinity values of a tapioca waste water sample based on titration with NaOH and HCl, finding acidity of 30.624 mg/L CO2 and 0.528 mg/L H+. 3) The acidity and alkalinity of the sample according to Indonesian standard SNI 06-2422-1991, determining values for methyl orange acidity, total acidity, phenolphthalein alkalinity, and total alkalinity.

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    of 5

    LAMPIRAN

    Hasil Perhitungan Asidi-Alkalinitas


    Dari data yang telah diperoleh, maka dapat dilakukan perhitungan sebagai berikut :
    a. Standarisasi Larutan NaOH 0,1 N
    Diketahui
    : Volume NaOH = 9,8 mL
    Ditanya
    : N NaOH ?
    Jawab
    :
    Normalitas NaOH
    =

    =
    =

    b. Standarisasi Larutan HCl 0,1 N


    Diketahui
    : Volume HCl = 5,7 mL
    Ditanya
    : NHCl?
    Jawab
    :
    Normalitas HCl
    =

    =
    =
    N
    c. Perhitungan Asiditas Alkalinitas
    Asiditas
    Diketahui

    : Volume sampel limbah tahu = q = 5 mL


    Normalitas NaOH

    = 0,051 N

    Normalitas HCl

    = 0,087 N

    p (larutan NaOH 0,1 N) = 2,4 mL


    q (larutan HCl 0,1 N)

    = 0,8 mL

    Ditanya

    : nilai asiditas ?

    Jawab

    : p > q, maka asiditas disebabkan oleh CO2 dan H+

    LP.II-1

    LP.II-2

    CO2(mg/L)

    =
    = (1000/100) x 0,8 x 0,087 x 44
    = 10 x 0,8 x 0,087 x 44
    = 30,624 mg/L

    H+ (mg/L)

    =
    = 10 x [(2,4 x 0,051) (0,8 x 0,087)] x 1
    = 10 x 0,0528
    = 0,528 mg/L

    Alkalinitas
    Diketahui : Volume sampel = 5 mL
    Normalitas HCl = 0,087 N
    p (larutan NaOH 0,1 N) = 2 mL
    q (larutan HCl 0,1 N) = 0,1 mL
    : nilai alkalinitas ?

    Ditanya
    Jawab
    :
    p > q, maka alkalinitas air tersebut disebabkan oleh

    dan

    (mg/L)
    = 10 x (2 0,1) x 0,087 x 17

    = 10 x 1,9 x 1,479
    = 28,101 mg/L

    = (1000/100) x 0,1 x 0,087 x 60


    = 10 x 0,1 x 0,087 x 60
    = 4,35 mg/L

    d. Pengukuran Asiditas-Alkalinitas Berdasarkan SNI 06-2422-1991


    Asiditas Metil Orange (pH air < 4,3)

    LP.II-3

    Diketahui

    Ditanya

    : Volume titrasi NaOH = 1,8 mL


    Volume sampel

    = 10 mL

    Normalitas NaOH

    = 0,051 N

    : asiditas metil orange ?

    Jawab :
    Asiditas metil orange
    =

    =
    = 45,9 mg/L CaCO3
    Asiditas Total (pH < 8,3)
    Diketahui

    Ditanya

    : Volume titrasi NaOH = 2 mL


    Volume sampel

    = 10 mL

    Normalitas NaOH

    = 0,051 N

    : asiditas total ?

    Jawab :
    Asiditas Total

    = (1000/10) x 2 x 0,051 x (10/2)


    = 100 x 2 x 0,051 x 5
    = 510 mg/L CaCO3
    Alkalinitas Fenolphtalein
    Diketahui

    Ditanya

    : Volume titrasi HCl = 0,2 mL


    Volume sampel

    = 10 mL

    Normalitas HCl

    = 0,087 N

    : alkalinitas fenophtalein ?

    LP.II-4

    Jawab :
    Alkalinitas fenophtalein
    =

    =
    = 8,7 mg/L CaCO3
    Alkalinitas Total
    Diketahui

    Ditanya

    : Volume titrasi HCl = 2 mL


    Volume sampel

    = 10 mL

    Normalitas HCl

    = 0,087 N

    : alkalinitas total ?

    Jawab :
    Alkalinitas Total

    = (1000/10) x 2 x 0,087 x (10/2)


    = 100 x 2 x 0,087 x 5
    = 87 mg/L CaCO3

    LP.II-5

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