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8.

0
7.5
7.0
6.5
6.0
5.5
5.0
4.5
4.0
f1 (ppm)
3.5
3.0
2.5
2.0
1.5

3.1446

3.3346
1.0883

2.0782
1.0035
3.1424

2.0543
2.0055
1.0000

OH
CH3
CH3

1.0
0.5
0.0
-0.5

1.84
1.83
1.82
1.82
1.81
1.80
1.80
1.78
1.71
1.57
1.31
1.30
1.29
1.28
1.28
1.27
1.26
1.26
1.25
1.24
1.16
1.15
1.14
1.13
1.12
1.12
1.11
1.10
1.08
0.87
0.86
0.84

7.46
7.45
7.43
7.43
7.37
7.35
7.33
7.26
7.25
7.23

200
190
180
170
160
150
140
130
120
110
100
90
f1 (ppm)
80
70
60
50
40
30
20
10
0

13.99

30.07
26.14
23.02

43.96

77.38
77.06
76.75
74.65

128.05
126.41
124.79

148.13

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