TIU CHUN QUC GIA

TCVN 6934 : 2001

SN TNG - SN NH
TNG - YU CU K THUT
V PHNG PHP TH
 TIU CHUN QUC GIA
TCVN 6934 : 2001
SN TNG - SN NH TNG - YU CU K THUT V PHNG PHP TH
Wall paints - Emulsion paints - Specification and test methods
Li ni u
TCVN 6934 : 2001 do Tiu ban k thut tiu chun TCVN/TC35/SC2 Vt liu chng thm hon
thin trn c s d tho ca Vin Khoa hc Cng ngh vt liu xy dng, B Xy dng ngh,
Tng cc Tiu chun o lng Cht lng xt duyt, B Khoa hc, Cng ngh v Mi trng
(nay l B Khoa hc v Cng ngh) ban hnh.
Tiu chun ny c chuyn i nm 2008 t Tiu chun Vit Nam cng s hiu thnh Tiu
chun Quc gia theo quy nh ti Khon 1 iu 69 ca Lut Tiu chun v Quy chun k thut
v im a khon 1 iu 6 Ngh nh s 127/2007/N-CP ngy 1/8/2007 ca Chnh ph quy nh
chi tit thi hnh mt s iu ca Lut Tiu chun v Quy chun k thut.

SN TNG - SN NH TNG - YU CU K THUT V PHNG PHP TH

Wall paints - Emulsion paints - Specification and test methods
1. Phm vi p dng
Tiu chun ny p dng cho sn tng hp dng nh tng, ch yu gc arcrylic, dng sn
trang tr v bo v tng pha trong v ngoi cc cng trnh xy dng.
2. Tiu chun trch dn
TCVN 2090 - 1993 Sn. Phng php ly mu, bao gi, ghi nhn, vn chuyn v bo qun.
TCVN 2091 - 1993 Sn. Phng php xc nh mn.
TCVN 2094 - 1993 Sn. Phng php gia cng mng.
TCVN 2095 - 1993 Sn. Phng php xc nh ph.
TCVN 2096 - 1993 Sn. Phng php xc nh kh v thi gian kh.
TCVN 2097 - 1993 Sn. Phng php ct, xc nh bm dnh ca mng.
TCVN 2099 - 1993 Sn. Phng php xc nh bn un ca mng.
TCVN 2102 - 1993 Sn. Phng php xc nh mu sc.
TCVN 3121 - 1979 Va v hn hp va xy dng. Phng php th c l.
TCVN 4851 - 1989 (ISO 3696 : 1987) Nc dng phn tch trong phng th nghim. Yu cu
k thut v phng php th.
TCVN 5669 - 1992 Sn. Kim tra v chun b mu th.
TCVN 5670 - 1992 Sn. Tm chun th.
TCVN 6025 : 1995 B tng. Phn mc theo cng nn.
3. Yu cu k thut
Cc ch tiu k thut ca sn tng trong v sn tng ngoi c qui nh bng 1.
Bng 1 - Cc ch tiu k thut ca sn tng
Mc qui nh
Tn ch tiu
Sn tng trong Sn tng ngoi
1. Mu sc theo mu chun
2. mn, mm, khng ln hn 50
2
3. ph, g/m , ty thuc vo mu sc 125 200
4. bm dnh ca mng sn trn nn va xi
2
mng - ct, theo im, khng ln hn
5. Thi gian kh, gi
- kh b mt, khng ln hn 1
- kh hon ton (cp 1), khng ln hn 5
6. Hm lng cht khng bay hi tnh theo khi
50
lng, %, khng nh hn
7. nht, Pa.s (o iu kin RV4, SP4) 20 30 12 20
8. bn nc, gi, khng nh hn 250 1000
9. bn kim, gi, trong dung dch Ca(OH)2 bo
150 600
ha, pH = 14, khng nh hn
10. ra tri, chu k, khng nh hn 450 1200
11. Chu k nng lnh, chu k, khng nh hn - 50
4. Phng php th
4.1. Ly mu v chun b mu th
Ly mu th theo TCVN 2090 - 1993.
Chun b v kim tra mu th theo TCVN 5669 - 1992.
4.2. Chun b nn chun
Nn chun th l mt tm b tng c kch thc:
a) 150 mm x 100 mm x 10 mm v
b) 430 mm x 170 mm x 10 mm,
c gia cng bng va xi mng - ct vng ( mn di sng 5 mm), t mc 100 (tng ng
10 MPa theo TCVN 6025 : 1995) v c dng h theo TCVN 3121 - 1979.
Trc khi gia cng mng sn, b mt tm nn chun phi m bo phng, nhn.
4.3. Phng php xc nh mu sc: theo TCVN 2102 - 1993.
4.4. Phng php xc nh mn: theo TCVN 2091 - 1993.
4.5. Phng php xc nh ph: theo TCVN 2095 - 1993.
4.6. Phng php xc nh bm dnh:
Theo TCVN 2097 - 1993, trong ly mu theo iu 4.1 v tm nn chun theo iu 4.2.a ca
tiu chun ny.
4.7. Phng php xc nh kh v thi gian kh
Theo TCVN 2096 - 1993, trong ly mu theo iu 4.1 v tm nn chun theo iu 4.2.a ca
tiu chun ny.
4.8. Phng php xc nh hm lng cht khng bay hi
4.8.1. Nguyn tc: Sy mu cho dung mi bay hi hon ton, sau dng phng php khi
lng xc nh hm lng cht khng bay hi.
4.8.2. Ly mu: theo iu 4.1.
4.8.3. Dng c th nghim:
- cc cn;
- a thy tinh;
- tha s;
- bnh ht m;
- t sy;
- cn k thut chnh xc 0,01 g.
4.8.5. Tin hnh th
Sy cc cn nhit 110 C 5C n khi lng khng i. Trc mi ln cn u phi
ngui cc trong bnh ht m.
Cn 5 gam sn vo cc cn c sy trn, ri em sy cng nhit trn cho ti khi
lng khng i. Trc mi ln cn u phi ngui cc trong bnh ht m.
4.8.6. Tnh kt qu
Hm lng cht khng bay hi (X), c tnh bng phn trm, theo cng thc:

G3 - G1
X= 100
G2 - G1
trong
G1 l khi lng cc, tnh bng gam;
G2 l khi lng ca cc v mu sn trc khi sy, tnh bng gam;
G3 l khi lng ca cc v mu sn sau khi sy, tnh bng gam.
Kt qu l gi tr trung bnh cng ca kt qu th ba mu tin hnh song song, ly chnh xc n
mt n v.
4.9. Phng php o nht
4.9.1. Ly mu: theo iu 4.1.
4.9.2. Dng c th nghim
- cc thy tinh 500 ml;
- tha s;
- khn lau mm;
- cn k thut c chnh xc n 0,01 g;
- thit b o nht (nht k Brookfield).
4.9.3. Cch tin hnh
Vic o nht trn nht k Brocfield c tin hnh theo trnh t sau:
Kim tra v iu chnh nht k v v tr cn bng;
Chn, lp trc v t tc thch hp;
Nng trc bng cch vn vt iu chnh cao;
Cn khong 600 650 g mu sn cho vo cc thy tinh dung tch 500 ml. Cc mu c y
kn, nhit phng (27 C 2 C) n khi ht bt kh (khong 30 60 pht);
o
t cc mu vo nht k, iu chnh trc quay nm chnh tm cc mu;
H trc quay xung cc mu t su tng ng vi vch nh mc c nh du trn trc;
Bt cng tc trc nht k quay;
Ghi s c kim ng h sau khi nht k hot ng c khong 1 pht.
Tin hnh cn v o theo trnh t trn ln lt cho tng mu (3 mu).
4.9.4 Tnh kt qu
nht ca sn (h) tnh bng (Pa.s) theo cng thc:
h=K.a
trong
a l s c ca kim ng h;
K l h s tng ng ca tc v trc c chn (xem ph lc A).
Kt qu l gi tr trung bnh cng ca kt qu ba ln o.
4.10. Phng php xc nh bn nc ca mng sn
4.10.1. Nguyn tc: Ngm 2/3 din tch tm mu trong nc ct trong mt thi gian v iu kin
mi trng nht nh, sau quan st nh gi b mt mu.
4.10.2. Ly mu: theo iu 4.1.
4.10.3. Tm nn chun: theo iu 4.2.a.
4.10.4. Dng c th nghim:
- chu nha 5 lt;
- bp in;
- khn lau mm;
- nc ct theo TCVN 4851 - 1989 (ISO 3696 : 1987);
- parafin;
- chi qut sn (chiu rng 25 mm).
4.10.5. Cch tin hnh
Ly 3 tm nn chun, gia cng mng sn c hai mt theo TCVN 2094 - 1993. Sau khi mng sn
kh hon ton (theo TCVN 2096 -1993), ph kn mt vin xung quanh nn mu bng parafin.
Ngm 2/3 din tch tm mu ngp trong nc ct nhit 27 C 2 C trong thi gian khng t
hn:
- 250 gi cho sn tng trong;
- 1000 gi cho sn tng ngoi.
Sau khi ngm tm mu thi gian qui nh, vt tm mu ra khi nc v dng khn lau thm
kh b mt mu.
4.10.6. nh gi kt qu
Quan st ngay sau khi thm kh b mt tm mu v quan st tm mu tip sau 2 gi. Trong
3 tm mu nu c t nht 2 tm mng sn khng b ho mm, bong, trc, rp, phng hoc co
nt, khng c s khc bit ln v mu sc v bng gia phn tm mu c ngm trong
nc v phn tm mu khng ngm trong nc th kt lun mng sn t yu cu v bn
nc.
4.11. Phng php xc nh bn kim
4.11.1. Nguyn tc: Ngm 2/3 din tch tm mu trong dung dch Ca(OH)2 bo ha trong mt thi
gian v iu kin mi trng nht nh, sau quan st nh gi b mt mu.
4.11.2. Ly mu: theo iu 4.1.
4.11.3. Nn chun theo iu 4.2.a.
4.11.4. Dng c th nghim:
- chu thy tinh ng knh 250 300 mm;
- bnh nh mc 1000 ml;
- bp in;
- chi qut sn, rng 25 mm;
- khn lau mm;
- cn k thut chnh xc 0,01 g;
- parafin;
- nc ct theo TCVN 4851 - 1989 (ISO 3696 : 1987);
- bt canxi hydroxit Ca(OH)2;
- giy o pH (ch th t 1 14).
4.11.5. Cch tin hnh
a) iu ch dung dch Ca(OH)2 bo ha
Trong iu kin mi trng nhit 27 C 2 C, cn khong 1,2 g Ca(OH)2 cho vo bnh nh
mc 1000 ml nc ct, lc k, gn b phn khng tan, ly phn dung dch.
b) Trnh t th
Ly 3 tm nn chun, gia cng mng sn c hai mt nh TCVN 2094 - 1993. Sau khi mng sn
kh hon ton theo TCVN 2096 - 1993, ph kn mt vin xung quanh tm mu bng parafin.
Ngm 2/3 tm mu ngp trong dung dch Ca(OH)2 bo ha nhit 27C 2C trong thi gian
khng t hn:
- 150 gi i vi sn tng trong;
- 600 gi i vi sn tng ngoi.
Sau khi ngm tm mu thi gian qui nh, vt tm mu ra khi dung dch, dng nc my ra
sch v khn mm thm kh b mt tm mu.
4.11.6. nh gi kt qu
Quan st b mt tm mu ngay sau khi thm kh b mt, ri quan st tip sau 2 gi. Trong 3
tm mu nu c t nht 2 tm c mng sn khng b ha mm, bong trc, rp phng hoc co
nt, khng c s khc bit ln v mu sc v bng gia phn nn tm mu c ngm trong
dung dch v phn tm mu khng ngm trong dung dch, th kt lun mng sn t yu cu v
bn kim.
4.12. Phng php xc nh ra tri
4.12.1. Ly mu: theo iu 4.1.
4.12.2. Tm nn chun
a) Chn tm nn chun: theo iu 4.2.b.
b) Gia cng mng sn: sn 2 lp sn ph (khong 250 g/ tm mu chun, qui v hm lng
cht khng bay hi l 55 %).
4.12.3. Dng c ha cht th nghim:
- cn k thut c chnh xc 0,01 g;
- tha, bt s;
- a thy tinh;
- ng ong 1000 ml;
- chi qut sn, rng 25 mm;
- bnh phun dung dch ra;
- bn chi:
+ kch thc bn chi: 90 mm x 38 mm x 25 mm. Mt bn chi c c u 60 l c ng
knh l 3 mm. Trong cc l s cm thng gc lng bn chi;
+ lng bn chi: mm (tng t lng ui ln en) v di khong 19 20 mm;
- giy o pH;
- ng h bm giy;
- bt x phng.
4.12.4. Cch tin hnh
1) Th nghim nhit 27 C 2 C;
2) Pha dung dch ra: dng bt x phng pha thnh dung dch 5 % theo khi lng;
3) X l bn chi:
- trc khi dng, lng bn chi c ngm ngp 12 mm trong nc 30 pht, sau ngm tip
vo dung dch ra 15 pht. Khi lng bn chi c di nh hn 15 mm th phi thay bn chi
mi;
- pha trn ca bn chi c gn vi mt ming st c kch thc: 90 mm x 38 mm. Tng khi
lng ca bn chi v ming st khong 450 g.
4) Trnh t thao tc:
Tin hnh th ng thi trn ba tm mu.
t c nh tm mu, b mt ph sn pha trn.
t bn chi c x l ln trn b mt c ph sn ca tm mu. Ko bn chi di chuyn
qua, li (trung bnh l 45 chu k/pht) theo phng nm ngang trn b mt (khng n tay).
Mi chu k, bn chi s di chuyn khong 600 mm trong phm vi b rng 100 mm gia tm
mu (hnh 1). ng thi phun dung dch ra m bo b mt tm mu lun lun t (tc
phun khong 10 ml/pht).
Kch thc tnh bng milimt
 1. B mt tm mu;
2. Vng dch chuyn bn chi;
3. Vng quan st nh gi.
Hnh 1 - S vng c ra v vng quan st
Sau khi tin hnh:
- 450 chu k cho sn tng trong;
- 1200 chu k cho sn tng ngoi,
dng thao tc c v ra sch tm mu bng nc vi ri nghing 45 ni thong mt.
4.12.5. nh gi kt qu
Quan st mng sn trong phm vi 100 mm, tnh t tm ca tm mu bng mt thng di nh
sng ban ngy. Nu trong 3 tm mu th c t nht 2 mu khng b bo mn l b mt nn
chun, th kt lun mng sn t yu cu v ra tri.
4.13. Phng php th chu k nng lnh
4.13.1. Ly mu theo iu 4.1.
4.13.2. Tm nn chun theo iu 4.2.a.
4.13.3. Dng c v thit b:
- t sy;
- chu nha;
- khn lau mm;
- gi nn mu;
4.13.4. Tin hnh th
Ly 3 tm nn chun, gia cng mng sn mt mt theo TCVN 2094 - 1993, sau 7 ngy sau em
th.
2 tm mu vo t sy (tm cn li lm mu so snh), sy nhit 80C 5C. C sau 1
gi a cc tm mu ngm vo chu nc (khong thi gian a mu ra ngm khng qu 5
giy), lng nc c trong chu khng nh hn 5 lt, v lun lun c b xung, m bo
nhit ca nc trong chu bng nhit phng. Khi tm mu ngui n nhit phng
(khong 5 - 7 pht), ly tm mu ra, dng khn lau m thm kh b mt v xung quanh tm mu.
Php th c lp li nhiu ln nh trn cho ti khi t c s chu k qui nh th dng li,
(thi gian th khng qu 7 ngy, mi ngy th khng t hn 7 chu k).
4.13.5. nh gi kt qu
Ngay sau khi kt thc php th, b mt mng sn ca tm mu c thm kh v quan st k
di nh sng ban ngy. Nu khng c biu hin khc thng, khng c s bong trc hoc rn
chn chim v mc thay i mu sc khng ln so vi mu so snh th kt lun mu sn t
yu cu.

PH LC A
(Qui nh)
Bng tra h s (K) tnh kt qu nht Brookfield
Trc
RV1 RV2 RV3 RV4 RV5 RV6 RV7
Tc
2 50 200 500 1 000 2 000 5 000 20 000
4 25 100 250 500 1 000 2 500 10 000
10 10 40 100 200 400 1 000 4 000
20 5 20 50 100 200 500 2 000
[H n v SI: 1 Pa.s = 1000 cP].
V d:
Mt mu c o trc s 3 (RV3), tc 10 (SP 10) c s c (a) l 75.
Tra bng trn tm c h s (K) l 100.
Khi , nht (h) c tnh theo iu 4.9.4 nh sau:
h=a.K
= 75 x 100 = 7 500 cp
= 7,5 Pa.s
Kt qu c vit l: h (RV3, SP 10) = 7,500 Pa.s
 TIU CHUN QUC GIA
TCVN 6934 : 2001
SN TNG - SN NH TNG - YU CU K THUT V PHNG PHP TH

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