ŠKOLA: Prirodoslovno – grafička škola SMJER: Kemijski tehničar

Predmet: Opća kemija s vježbama

Datum izvođenja vježbe: ________________
Ime i prezime:___________________________

Naziv vježbe: PREKRISTALIZACIJA Red.br.vježbe

Pribor:
Dvije Erlenmayerove tikvice (250mL), stakleni lijevak, menzura, Büchnerov lijevak, boca za odsisavanje, stakleni štapić,
filtrirni papir, vodena sisaljka, plamenik, mrežica
Kemijske tvari:
benzojeva kiselina, aktivni ugljen, voda
Opis rada:
1. Napravi naborani filter papir.
2. Na vagi izvaži 2g nečiste benzojeve kiseline.
3. U tikvici pomiješaj2g benzojeve kiseline s 50 mL destilirane vode.
4. Lagano zagrijavaj i dodaj na vrhu noža aktivni ugljen.
5. Nastavi zagrijavati do vrenja.
6. U grlo tikvice koja je zagrijana postavi lijevak s naboranim filtrirnim papirom tako da se lijevak ugrije.
7. Vruć lijevak presi na drugu tikvicu i odmah filtriraj vrelu smjesu kroz filtrirni papir.
8. Tikvicu se filtratom ohladi vodovodnom vodom.
9. Kristale iz hladne otopine odvoji pomoću Bühnerova lijevka i isperi s malo hladne vode.
Dobivene kristale suši na izvaganom filtrirnom papiru u eksikatoru.

Skica:

Zapažanja:
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
Zaključak:
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________
_________________________________________________________________________________________________________

Pregledao: ___________________________ __________________________

Nakon prve filtracije u Erlenmeyerovioj tikvici se nalazi homogena smjesa.

Profiltrirana Vrsta smjese

Zapažanja:

- Otapanje nečiste benzojeve kiseline u destiliranoj vodi – heterogena smjesa

- Zašto se stvaraju plinovi

Što moraju znati za shvaćanje ove lekcije

- Vrste smjesa
- Promjene topljivosti plinova i krutina s temperaturom.