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Quench Tower Design PDF
Quench Tower Design PDF
1.4.2 The volumetric flowrate of the gas (QG) can be calculated by...............................9
1.4.3 The ratio of the liquid mass flow rate to the gas mass flow rate is given by..........9
1.4.8 The wall factor can be important for columns with an inadequate ratio of
1
1.4.12 The liquid mass velocity can be calculated as....................................................14
REFERENCES..................................................................................................................28
2
Tables
3
1.0 DESIGN OF A QUENCH TOWER
To Design a quench tower to cool hot gases flowing at a rate of 5730 kg/h using water
Quenching of reactor products is sometimes needed for sudden cooling, for removing
accomplished by introducing the hot gases into a liquid contacting device. When the liquid
evaporates or gets heated up, the energy necessary to heat up the liquid is obtained at the
expense of hot combustion gases, resulting in the reduction of gas temperature. The
temperature of the gases discharged from the quencher is at the adiabatic saturation
temperature of the gases if the operation is adiabatic and the gas leaves the quencher with
Spray towers
Venturi scrubbers
Packed towers
Spray towers or spray chambers consists of empty cylindrical vessels made of steel or
plastic and nozzles that spray liquid into the vessels. The inlet gas stream usually enters the
bottom of the tower and moves up, while the liquid is sprayed downward from one or more
levels. This flow of inlet gas and liquid in the opposite direction (counter current flow),
exposes the gas to the liquid, thereby enhancing the heat transfer.
1
Many nozzles are placed across the tower at different heights to spray all of the gas as it
moves up through the tower. The reason for using many nozzles is to maximize the heat
transfer. The liquid droplet must be large enough not to be carried out of the scrubber by the
many of the scale buildup and plugging problems associated with other scrubbers.
This is an inexpensive and control device primarily used for gas conditioning.
Very little space is required and only that amount of water that is needed to maintain
A venturi scrubber accelerates the gas stream to atomize the scrubbing liquid and to
improve gas-liquid contact. In a venturi scrubber, a throat section is built into the duct that
forces the gas stream to accelerate as the duct narrows and then expands. As the gas enters
the venturi throat, both gas velocity and turbulence increases. Depending on the scrubber
design, the scrubbing liquid is sprayed into the gas stream before the gas encounters the
venturi throat, or in the throat, or upwards against the gas flow in the throat.
2
1.2.3 Packed tower
Packed bed quenchers consist of a chamber containing layers of variously shaped packing
materials, such as Raschid rings, interlock saddles, pall ring, berl saddles, that provide large
surface area for liquid gas contact. The packing is held in place by wire mesh retainers and
supported by a place near the bottom of the scrubber. Cooling liquid is evenly introduced
Quench towers can either be cooled by a water or oil medium which gives the name
quench-water tower or quench-oil tower. Their function is to cool the superheated gas in
order to eliminate any further reaction that may occur and to also decrease the temperature
of the gas.
T FLOW,kg/hr FRACTION
H2 + CH4 542 9%
Propylene 168 3%
Butadiene 39.6 1%
Mixed
butenes 44.9 1%
C5+ 109 2%
N2 83.1 1%
CO2 194 3%
3
H2O 1780 31%
propane 70.9 1%
butane 9.11 0%
T FLOW,kg/hr FRACTION
Propylene 1.68E+02 4%
Butadiene 3.96E+01 1%
Mixed
butenes 4.49E+01 1%
C5+ 1.09E+02 3%
N2 8.31E+01 2%
CO2 1.94E+02 5%
propane 7.09E+01 2%
butane 9.11E+00 0%
4
NT FLOW PERCENTA
kg/hr GE
P×M
ρg = R ×T (Perry et al, 1997)
2.3 × 68.26
ρg = 0.08206× 613
ρg = 3.73 kg/m3
5
1.4.2 The volumetric flowrate of the gas (QG) can be calculated by
G
QG = ρg
Where,
1.5
QG = 3.73
= 0.402 m3/s
1.4.3 The ratio of the liquid mass flow rate to the gas mass flow rate is given by
L 5.11
G = 1.5 = 3.41
Flooding data for quench columns with countercurrent flow of gas and liquid can be
L ρG
X= ¿ 0.5
G ( ρL
3.73
¿ 0.5
X = 3.41 ( 1000 = 0.208
Flooding curve in quench tower can be accurately described by the polynomial regression
6
2
−[ 3.50221+1.028 lnx+ 0.11093( lnx) ]
Yflood = e
Yflood = 0.115
µL
¿
¿
Csflood = ( F p¿ )0.5 (Leva,1954)
Y flood
¿
0.115
0.5
Csflood = ( 27 × 0.0010.1 ) = 0.092 m/s
ρG
¿0.5
ρL −ρG
VGF ¿ (Leva, 1954)
Csflood
¿ ¿
3.73
1000−3.73
¿
VGF = ¿ = 1.5 m/s
¿
0.092
¿
7
1.4.5 Calculation of pressure drop at flooding
The pressure drop at flooding is strongly dependent on the packing factor for both random
For a given fluid flow rates and properties, and a given packing material, superficial gas
f = a fraction of flooding and is usually 0.7 for quench towers (Wiley and Jaime,1987)
4 × QG
D = ( f ×V gf × π )0.5 (Kister, 1992)
4 ×0.402
D = ( 0.7× 1.05 × π )0.5 = 0.83 m
D = 0.83 m
8
Hence the diameter of the column is 0.83 m
2
π ×D
A= 4
π ×(0.83)2
A= 4 = 0.541 m2
1.4.8 The wall factor can be important for columns with an inadequate ratio of effective
1 2 1 dp
=¿ 1+
KW 3 ( 1−ɛ ) D (Leibson et al, 1956)
Kw = wall factor
1−ɛ
dp = 6( a ) (Leibson et al, 1956)
1−0.951
dp = 6( 112.6 ) = 0.0026110
1 2 1 0.0026110
=¿ 1+ ( )
KW 3 1−0.951 0.83
9
1
KW = 1.043
KW = 0.959
v G ×d p × ρG × K W
ReG = (1−ɛ)(µG )
empirical expression:
64 1.8
Ψ = Cp ( R eG + ( ReG )0.08 ) (Leibson et al, 1956)
64 1.8
Ψ =0.763 ( 6671.24 + (6671.24)0.08 ) = 0.686
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1.4.11 Calculation of dry-gas-pressure drop
The dry-gas-pressure drop can be calculated from the dimensionally consistent correlating
V
∆ Po (¿¿ G)2
= Ѱ × a× ρ G × (Stichlmair et al, 1989)
Z ( ɛ)3 ×2 × K w
¿
2
∆ Po 0.686× 112.6 ×3.73 ×(1.05)
Z = (0.951)3 ×2 ×0.9900
∆ Po
Hence the dry-gas-pressure drop, Z = 177.39 Pa/m
L
2
Gx = π ×(D) (Seader and Henley, 1998)
4
5.11
2
Gx = π ×(0.83) = 9.444 kg/m2.s
4
11
Gx
ReL = a× µ L (Seader and Henley,1998)
Gx 9.444
ReL = a× µ L = 112.6 ×0.001 = 83.87
G x2 × a
FrL = (Seader and Henley,1998 )
g
2
G x × 112.6
FrL = 2
100 × 9.81
FrL = 0.1028
R eL
¿
¿
ah (Seader and Henley)
=0.85 Ch ׿
a
Where, Ch = is a (packing constant) characteristic of the particular type and size of packing
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ah = hydraulic, or effective, specific area of packing, m2/m3
R eL
¿
¿
ah
=0.85 Ch ׿
a
ah
Therefore, the ratio of specific areas is =¿ 1.606
a
The specific liquid holdup (i.e. volume of liquid holdup/volume of packed bed) in the
12(1.028)
2
hL 83.87
=( 1 ( 1.606 ¿ 3 = 0.724
3
¿¿
h L = 0.724
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1.4.15 Calculation of pressure drop when the bed is irrigated
When the packed bed is irrigated, the liquid holdup causes the pressure drop to increase.
The Correct pressure drop for liquid holdup is calculated with the equation
R eL
∆P ɛ
=¿ 200 (Billet and Schultes)
∆ PO ( ɛ−hL ) exp(
¿ ¿1.5
∆P 83.87
=¿ 0.951
( 200
∆ PO 0.951−0.724 ) exp ( = 5.5
¿¿ 1.5
∆P
∆ PO = 5.5
∆P
Z = 645.24 Pa/m
−0.19 0.21
HETP = A [ ] [ ]
σ
20
μ
0.2
Where,
A = Size of packing = 50 mm
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D = 0.83 m
−0.19 0.21
−3 69.8 0.0006
HETP = 50 ×10 20 ( ) ( 0.2 )
HETP ¿ 0.0116 m
NTU =
1
1−β [ x −y
ln ( 1−β ) 2 1 + β
x 1− y 1 ]
Where,
β = L/HG = 0.000381
15
NTU = 4.3
NTU = 5
( ( ))
−1
β
HETP
Hog = 1 (6)
ln
β
Hog = 2.01 m
Htotal = 2.01 x 5
Htotal = 10.05 m
Giving 0.457 allowance for disengagement of vapors at top and at bottom for liquid,
Htotal = 10.51 m
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Table 1.4 Summary of chemical engineering design of quench tower
Parameter value
The actual pressure drop when the bed is irrigated, Pa/m 645
110
Pi = 100 × 233.047 kPa = 256.352 kPa
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1.5.2 Design Temperature
Pi D i
,
2f i - Pi
e= (Sinnott, 2005b)
Where,
f is the design stress of stainless steel at 340oC = 100 N/mm2 (Sinnott, 2005c)
Pi is the internal design pressure of the shell = 256.352 kPa = 0.256 N/mm2
0.256 830
(2 100) 0.256
e= 2 mm
C v π ρ m g D m H v 0.8D m t
Wv (Sinnott, 2005e)
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Where,
CV = factor to account for the weight of nozzles, man ways, internal supports etc, which
Bending stresses result from the bending moments to which the vessel is subjected.
Bending moments will be caused by the wind loads on tall self-supported vessels, dead
weight and wind loads on piping and equipment which is attached to the vessel,
Pw
Dynamic wind pressure ( ) is 1280 N/m2 (Sinnott, 2005g).
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1.5.7 Analysis of Stress
Pi d i
σl
4t
(Sinnott, 2005h)
Hence,
0.256 x 830
σl 13.28 N/mm 2
4x4
Pi d i
σh 2 i
2t
σ h 2 13.28
σh 26.56
= N/mm2
WT
σw
π D i t t
(Sinnott, 2005i)
20
9988.98
σw 0.953 N / mm2
π 830 4 4
σ
Total axial or longitudinal stress ( z )
¿ 11.33 N /mm2
The maximum allowable stress for the material of construction is 100 N/mm 2. Since this
stress is higher than the maximum stress intensity at any point in the material, the design is
The support system designed for a separator and all tall vessels depends on the size, shape,
and weight of the vessel; the design temperature and pressure; the vessel location and
A skirt support is used for vertical columns. Its thickness is designed to withstand the dead-
weight loads and bending moments imposed on it by the separator. (Sinnott, 2005k)
Data
21
Specified skirt angle = 90 °C (straight cylinder skirt)
Maximum allowable stress, (σ max ) and Young’s modulus, (E) at ambient conditions are
The maximum dead-weight load on the skirt will occur when the vessel is full of water,
ρw = density of water
= 55785.05 N
= 65773.045 N
4 Ms W
σ bs= σ ws =
π ( Ds +t s ) t s , π ( D s +t s ) t s
Where,
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Ms = maximum bending stress at the base of skirt
ts = skirt thichness
σ s ( tensile ) =σ bs −σ ws
σ s ( compressive )=σ bs +σ ws
3
4 ×59241.96 Nm ×1 0
σ bs= = 5.35 N/mm2
π ( 830+20 ) 830× 20
55785.05 ×1 03
σ ws (test )= =1.044 N/mm2
π ( 830+ 20 ) × 20
9988 ×1 03
σ ws (operational)= = 0.19 N/mm2
π ( 830+ 20 ) × 20
^
Maximum σ s (compressive)=¿ 5.35 + 1.044 = 6.394 N/mm2
The skirt thickness should be such that under the worst combination of wind and dead-
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σs (tensile) < fsJsinϴs (Sinnott, 2005l)
ts
σ s ( compressive ) <0.125 E ( )
Ds
sin θ s ( Sinnott , 2005 m)
Where,
fs = maximum allowable design stress for the skirt material, normally taken at ambient
temperature, 20 0C
20
6.394< 0.125× 11350 × ( 830 ) sin ( 90)=246. 02
Since both criteria are satisfied, a thickness of 20 mm can be used for the skirt.
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Table 1.5
Parameter Value
Material Stainless steel 304
Summary of
Design pressure, kPa 256
Design temperature, oC 340 mechanical
Vessel thickness, mm 4
Longitudinal stress, N/mm2 13.28 engineering
Circumferential stress, N/mm2 26.56
Dead weight stress, N/mm2 0.953 calculations
Dead weight, N 9988
Total longitudinal stresses, N/mm2 14.233
Skirt support thickness, mm 20
Wind Loading, N/m 1072.64
Maximum stress intensity, N/mm2 11.33
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REFERENCES
Sinnott, R.K. (2005b) Chemical Engineering Design 4th ed., Laserwords private
Sinnott, R.K. (2005f) Chemical Engineering Design 4th ed., Laserwords private
Sinnott, R.K. (2005g) Chemical Engineering Design 4th ed., Laserwords private
Sinnott, R.K. (2005h) Chemical Engineering Design 4th ed., Laserwords private
Sinnott, R.K. (2005i) Chemical Engineering Design 4th ed., Laserwords private
Sinnott, R.K. (2005j) Chemical Engineering Design 4th ed., Laserwords private
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limited, Chennai, p:860
Sinnott, R.K. (2005k) Chemical Engineering Design 4th ed., Laserwords private
Sinnott, R.K. (2005l) Chemical Engineering Design 4th ed., Laserwords private
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