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C
7H A P T E R

Principles of
Film Radiography1-3

Timothy J. Kinsella, Carpenter Technology Corporation,


Reading, Pennsylvania (Part 7)

Parts 1 to 6 from Radiography in Modern Industry. © 1980, Eastman Kodak Company.


Reprinted with permission by the American Society for Nondestructive Testing.
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PART 1. Film Exposure

A dark spot, corresponding to the


Making Radiographs projected position and shape of the void,
will appear on the film when it is
Radiography is one of the oldest and most developed. Thus, a radiograph is a kind of
widely used of nondestructive testing shadow picture — the darker regions on
techniques. Despite its established the film representing the more penetrable
position, new developments are parts of the object and the lighter regions
constantly modifying the radiographic representing those more opaque to
techniques applied by industrial and gamma radiation or X-radiation.
scientific users, thereby producing Industrial radiography is tremendously MOVIE.
technical or economic advantages, or versatile. Radiographed objects range, in Conventional
both, over previous techniques. This size, from microscopic electronic parts to radiography
progressive trend continues with such mammoth missile components, in gives shadow
special equipment and techniques as product composition through virtually image.
microfocus X-ray generators, portable every known material and in
linear accelerators, radioscopy, neutron manufactured form over an enormously
radiography, imaging on paper, digital wide variety of castings, weldments and
image analysis and image enhancement. assemblies. Radiographic examination has
A radiograph is a photographic record been applied to organic and inorganic
produced by the passage of penetrating materials, to solids, liquids and even to
radiation through an object onto a film
(Fig. 1). When film is exposed to X-rays,
gamma rays or light, an invisible change
called a latent image is produced in the FIGURE 1. Diagram of setup for making industrial radiograph
film emulsion. The areas so exposed with X-rays.
become dark when the film is immersed
Anode
in a developing solution, the degree of
darkening depending on the amount of Focal spot
exposure. After development, the film is
rinsed, preferably in a special bath, to stop
development. The film is next put into a
fixing bath, which dissolves the
unexposed parts of the emulsion’s
sensitive salt. The film is washed to Diaphragm
remove the fixer and dried so that it may
be handled, interpreted and filed. The
developing, fixing and washing of the
exposed film may be done manually or in
automated processing equipment.
The diagram in Fig. 1 shows the
essential features in the exposure of a
radiograph. The focal spot is a small area
in the X-ray tube from which the
radiation emanates. In gamma Specimen
radiography, it is the capsule containing
the radioactive material that is the source
of radiation (for example, cobalt-60). In
either case the radiation proceeds in
straight lines to the object; some of the
rays pass through and others are absorbed Front screen
— the amount transmitted depending on
the nature of the material and its
Back screen
thickness. For example, if the object is a
steel casting having a void formed by a Film
gas bubble, the void produces a reduction Sheet of lead
of the total thickness of steel to be
{

penetrated. Hence, more radiation will High density Low density


pass through the section containing the in radiograph in radiograph
void than through the surrounding metal.

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gases. An industry’s production of transformer losses and voltage waveform


radiographs may vary from the occasional can change with tube current but a
examination of one or several pieces to compensation factor is usually applied to
the examination of hundreds of minimize the effects of these changes. In
specimens per hour. This wide range of normal industrial radiographic practice,
applications has resulted in the the variation from exact proportionality is
establishment of independent, not serious and may usually be ignored.
professional X-ray laboratories as well as Figure 2 shows spectral emission curves
radiographic departments within for an X-ray tube operated at two
manufacturing plants. Radiographic different currents, the higher being twice
testing performed by industry uses the milliamperage of the lower. Therefore,
customer specifications or industry each wavelength is twice as intense in one
standards provided by technical societies beam as in the other. Note that no
and regulatory bodies. wavelengths present in one beam are
To meet the growing and changing absent in the other. Hence, there is no
demands of industry, research and change in X-ray quality or penetrating
development in the field of radiography power.
are continually producing new sources of As would be expected, the total
radiation such as neutron generators and amount of radiation emitted by an X-ray
radioactive isotopes; lighter, more tube operating at a certain kilovoltage and
powerful, more portable X-ray equipment milliamperage is directly proportional to
as well as multimegavolt X-ray machines the time the tube is energized.
designed to produce highly penetrating Because the X-ray output is directly
radiation; new and improved radiographic proportional to both milliamperage and
films and automatic film processors; and time, it is directly proportional to their
improved or specialized radiographic product. (This product is often referred to
techniques. These factors, plus the as the exposure in units such as
activities of many dedicated people, milliampere minutes.) Algebraically, this
broadly expand radiography’s usefulness may be stated E = MT, where E is the
to industry. exposure, M the tube current and T the
exposure time. The amount of radiation
will remain constant if the exposure
remains constant, no matter how the
Factors Governing individual factors of tube current and
Exposure exposure time are varied. This permits
specifying X-ray exposures in terms such
Generally speaking, the optical density as milliampere minutes (mA·min) or
(called photographic density or simply milliampere seconds (mA·s), without
density) of any radiographic image stating the specific individual values of
depends on the amount of radiation tube current and time.
absorbed by the sensitive emulsion of the The kilovoltage applied to the X-ray
film. This amount of radiation in turn tube affects not only the quality but also
depends on several factors: the total the intensity of the beam. As the
amount and type of radiation emitted by kilovoltage is raised, X-rays of shorter
the X-ray tube or gamma ray source; the wavelength and hence of more
amount of radiation reaching the penetrating power, are produced as well as
specimen; the amount of radiation more X-rays of the same wavelength as at
specifically absorbed that is characteristic
of the test material; secondary and
scattered radiation; filtration; and the
intensifying action of screens, if used. FIGURE 2. Curves illustrating effect of change
Photographic density is discussed in milliamperage on intensity of X-ray beam.
elsewhere in this chapter.
High
Emission from X-Ray Source milliamperage
Intensity (relative unit)

The total amount of radiation emitted by


an X-ray tube depends on tube current
(milliamperage), voltage, target (source)
material and the time the tube is
energized.
When the other operating conditions
are held constant, a change in
milliamperage causes a change in the Low
intensity (quantity of radiation leaving the milliamperage
X-ray generator per unit time) of the
radiation emitted, the intensity being
approximately proportional to the Wavelength (µm)
milliamperage. The high voltage

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lower voltages. Shown in Fig. 3 are constant. This permits specifying gamma
spectral emission curves for an X-ray tube ray exposures in becquerel hours or curie
operated at two different kilovoltages but hours without stating specific values for
at the same milliamperage. Notice that source activity or time.
some shorter wavelengths present in the Because the gamma ray energy depends
higher kilovoltage beam are absent from on the isotope, there is no variable to
the lower kilovoltage beam. Further, all correspond to the kilovoltage factor
wavelengths present in the lower encountered in X-radiography. The only
kilovoltage beam are present in the more way to change the radiation penetrating
penetrating beam and in greater amount. power when using gamma rays is to
Thus, raising the kilovoltage increases change the source, for example, higher
both the penetration and the intensity of penetration cobalt-60 in place of lower
the radiation emitted from the tube. penetration iridium-192.

Emission from Gamma Ray Source


The total amount of radiation emitted Geometric Principles
from a gamma ray source during a Because X-rays and gamma rays obey the
radiographic exposure depends on the common laws of light, their shadow
activity of the source (in becquerels or formation may be simply explained in
curies) and the time of exposure. For a terms of light. It should be borne in mind
particular radioactive isotope, the that the analogy is not perfect because all
intensity of the radiation is approximately objects are, to a greater or lesser degree,
proportional to the activity (in becquerels transparent to X-rays and gamma rays and
or curies) of the source. If it were not for because scattering presents greater
absorption of gamma rays within the problems in radiography than in optics.
radioactive material itself, this However, the same geometric laws of
proportionality would be exact. In normal shadow formation hold for both light and
radiographic practice, the range of source penetrating radiation.
sizes used in a particular location is small Suppose that, as in Fig. 4a, there is
enough so that variations from exact light from a point L falling on a white
proportionality are not serious and may card C and that an opaque object O is
usually be ignored. interposed between the light source and
Thus, the gamma ray output is directly the card. A shadow of the object will be
proportional to both activity of the source formed on the surface of the card.
and time and hence is directly This shadow cast by the object will
proportional to their product. naturally show some enlargement because
Analogously to the X-ray exposure, the the source is smaller than the object and
gamma ray exposure E may be stated the object is not in contact with the card;
E = MT, where M is the source activity in the degree of enlargement will vary
becquerels or curies and T is the exposure according to the relative distances of the
time; the amount of gamma radiation object from the card and from the light
remains constant so long as the product source. For a point source, or one much
of source activity and time remains smaller than the object, the law governing
the size of the shadow may be stated: the
diameter of the object is to the diameter of
FIGURE 3. Curves illustrating effect of the shadow as the distance of the light from
change in kilovoltage on composition and the object is to the distance of the light from
intensity of X-ray beam. the card.
Mathematically, the degree of
Wavelengths Wavelengths
added by increased in
enlargement may be calculated with the
increasing intensity by following equations:
kilovoltage increasing
kilovoltage So Do
(1) =
Si Di
Intensity (relative unit)

High
which may also be expressed as Eq. 2:
kilovoltage
D 
(2) So = Si  o 
 Di 

Low
where Do = distance from radiation source
kilovoltage to object; Di = distance from radiation
source to image recording surface (or
radiographic film); So = size of object; and
Wavelength (µm) SI = size of shadow (or radiographic
image).

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The degree of sharpness of any shadow the source of light is not a point but a
depends on the size of the light source small area, the shadows cast are not
and on the position of the object between perfectly sharp (Figs. 4b to 4d) because
the light and the card — whether nearer each point in the source of light casts its
to or farther from one or the other. When own shadow of the object and each of
these overlapping shadows is slightly
displaced from the others, producing an
ill defined image.
FIGURE 4. Geometric principles of shadow formation: When the source is larger than the
(a) planes of object and film perpendicular to X-ray direction object, as when imaging a crack, the
from point source; (b) perpendicular, near nonpoint source; shadow will be smaller than the object.
(c) perpendicular, distant nonpoint source; (d) perpendicular, Depending on the distance from object to
midrange nonpoint source; (e) oblique, parallel object and film the image may be undetectable
film planes, point source; (f) oblique, object and film planes because only the black shadow is usually
not parallel, point source. detectable.
The form of the shadow may also differ
(a) (d) according to the angle that the object
L
makes with the incident light rays.
Deviations from the true shape of the
object as exhibited in its shadow image
are referred to as distortion or
L misalignment.
Figure 4a to 4f shows the effect of
changing the size of the source and of
changing the relative positions of source,
object and card. From an examination of
O these drawings, it will be seen that the
O following conditions must be fulfilled to
C C produce the sharpest, truest shadow of the
object.
1. The source of light should be small,
that is, as nearly a point as can be
(b) (e) L obtained (compare Fig. 4a and 4c).
2. The source of light should be as far
from the object as practical (compare
Fig. 4b and 4c).
L 3. The recording surface should be as
close to the object as possible
(compare Fig. 4b and 4d).
4. The light rays should be directed
O
perpendicularly to the recording
O surface (see Fig. 4a and 4e).
5. The plane of the object and the plane
C C of the recording surface should be
parallel (compare Fig. 4a and 4f).

(c) L (f) Radiographic Shadows


L The basic principles of shadow formation
must be given primary consideration to
ensure satisfactory sharpness and freedom
from distortion in the radiographic image.
A certain degree of distortion will exist in
every radiograph because some parts will
always be farther from the film than
others, the greatest magnification or
image shrinkage being evident in the
O images of those parts at the greatest
O
distance from the recording surface.
Note, also, that there is no distortion of
C C
shape in Fig. 4e — a circular object having
been rendered as a circular shadow.
However, under circumstances similar to
Legend those shown in Fig. 4e, it is possible that
C = film plane spatial relations can be distorted. In Fig. 5
L = radiation source the two circular objects can be rendered
O = test object either as two circles (Fig. 5a) or as a figure

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eight shaped shadow (Fig. 5b). It should 1. The focal spot should be as small as
be observed that both lobes of the figure other considerations will allow, for
eight have circular outlines. there is a definite relation between the
Distortion cannot be eliminated size of the focal spot of the X-ray tube
entirely but, with an appropriate and the definition in the radiograph. A
source-to-film distance, can be lessened to large focus tube, although capable of
a point where it will not be objectionable withstanding large loads, does not
in the radiographic image. permit the delineation of as much
detail as a small focus tube. Long
Application to Radiography source-to-film distances will aid in
showing detail when a large focus tube
The application to the geometric is used but it is advantageous to use
principles of shadow formation to the smallest focal spot permissible for
radiography leads to five general rules. the exposures required. Figures 6b and
Although these rules are stated in terms of 6h show the effect of focal spot size
radiography with X-rays, they also apply on image quality. As the focal spot size
to gamma radiography. increases from 1.5 mm (0.06 in.) in
Fig. 6b to 4.0 mm (0.16 in.) in Fig. 6h,
the definition of the radiograph starts
to degrade. This change is especially
FIGURE 5. Depending on direction of evident at the chamber edges that are
radiation, two circular objects can be no longer sharp.
rendered: (a) as two separate circles; (b) as 2. The distance between the anode and
two overlapping circles. the material examined should always
(a) be as great as practical. Comparatively
long source-to-film distances should
be used in the radiography of thick
materials to minimize the fact that
structures farthest from the film are
less sharply recorded than those nearer
to it. At long distances, radiographic
definition is improved and the image
is more nearly the actual size of the
object. Figures 6a to 6d show the
O1 effects of source-to-film distance on
image quality. As the source-to-film
O2
distance is decreased from 1730 mm
(68 in.) to 305 mm (12 in.) the image
becomes more distorted until at
C 305 mm (12 in.) it is no longer a true
representation of the casting. This is
particularly evident at the edges of the
(b) casting where the distortion is
greatest.
3. The film should be as close as possible
to the object being radiographed. In
practice, the film (in its cassette or
exposure holder) is placed in contact
with the object. In Fig. 6b and 6e, the
effects of object-to-film distance are
evident. As the object-to-film distance
is increased from zero to 102 mm
(4 in.), the image becomes larger and
O1
the definition begins to degrade.
O2 Again, this is especially evident at
chamber edges that are no longer
sharp.
C 4. The central ray should be as nearly
perpendicular to the film as possible
to preserve spatial relations.
5. As far as the shape of the specimen
Legend will allow the plane of maximum
C = film plane interest should be parallel to the plane
O1 = first test object
O2 = second test object
of the film.
In Fig. 6f and 6g, the effects of
object-film-source orientation are shown.
When compared to Fig. 6b, the image in
Fig. 6f is extremely distorted; although the

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FIGURE 6. Effects on image quality when geometric exposure factors are changed: (a) 1.75 m (68 in.) source-to-film distance,
0 mm (0 in.) object-to-film distance; (b) 1.5 mm (0.06 in.) focal spot, 0 mm (0 in.) object-to-film distance; (c) intermediate
focal spot size, intermediate source-to-film distance; (d) 0.30 m (12 in.) source-to-film distance; (e) 100 mm (4 in.)
object-to-film distance; (f) perpendicular film-to-source angle and 45 degree object-to-film angle; (g) perpendicular
film-to-source angle, parallel object-to-film angle; (h) 4.0 mm (0.10 in.) focal spot.

(a) (c) (e) (g)

(b) (d) (f) (h)

film is perpendicular to the central ray, Ug d


the casting is at a 45 degree angle to the (3) =
film and spatial relationships are lost. As F Do
the film is rotated to be parallel with the
casting (see Fig. 6g), the spatial or
relationships are maintained and the
distortion is lessened. d
(4) Ug = F
Do
Calculation of Geometric
Unsharpness where Do = source-to-object distance;
The width of the fuzzy boundary of the F = size of radiation source; d = the
shadows in Fig. 4c and 4d is known as the object-to-film distance; and
geometric unsharpness Ug. Because the Ug = geometric unsharpness.
geometric unsharpness is a calculable Because the maximum unsharpness
measure of the sharpness of the image involved in any radiographic procedure is
and can strongly affect the appearance of usually the significant quantity, the
the radiographic image, it is frequently object-to-film distance d is usually taken
necessary to determine its magnitude. as the distance from the source side of the
From the laws of similar triangles (see specimen to the film.
Fig. 7), it can be shown that: Do and d must be measured in the same
units — say, millimeters or inches. So long
as Do and d are in the same units, Eq. 3 or

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4 will always give the geometric film may be placed at a distance from the
unsharpness Ug in whatever units were specimen rather than in contact with it
used to measure the dimensions of the (Fig. 9). Such an arrangement results in an
source. The projected sizes of the focal enlarged radiograph without introducing
spots of X-ray tubes are usually stated in objectionable geometric unsharpness.
millimeters and Ug will also be in Enlargements of three to ten diameters by
millimeters. If the source size is stated in this technique are useful in the detection
inches, Ug will be inches. of fine structures otherwise invisible
For rapid reference, graphs of the type radiographically. As the enlargement
shown in Fig. 8 can be prepared with increases, the effective field of view
these equations. The graphs relate (inspection area) decreases. This can result
source-to-film distance, object-to-film in the requirement of multiple exposures
distance and geometric unsharpness. Note to cover an entire part. A benefit of
that the lines of Fig. 8 are all straight. geometric enlargement is a decrease in the
Therefore, for each source-to-object amount of object scattered radiation
distance, it is only necessary to calculate reaching the image plane. This effect can
the value of Ug for a single specimen improve contrast sensitivity.
thickness and then draw a straight line
through the point so determined and the Inverse Square Law
origin. It should be emphasized, however,
that a separate graph of the type shown in When the X-ray tube output is held
Fig. 8 must be prepared for each size of constant or when a particular radioactive
source. source is used, the radiation intensity
reaching the specimen (object) is
Geometric Enlargement
In most radiography, it is desirable to
have the specimen and the film as close FIGURE 8. Graph relating geometric unsharpness Ug to
together as possible to minimize specimen thickness and source-to-object distance, for 5 mm
geometric unsharpness. An exception to (0.2 in.) source size.
this rule occurs when the source of 1.0 (40)
radiation is extremely minute, that is, a
in.)

in.)

fraction of a millimeter, as in a microfocus


m (10

(20

source or betatron. In such a case, the


0.9 (36)
mm
250 m

500

)
in.

FIGURE 7. Geometric construction for determining geometric 0.8 (32)


tance

(30

unsharpness Ug where source is smaller than object. See


m
0m
ject dis

Eq. 4.
75

.)

F 0.7 (28)
in
-to-ob

0
(4
Geometric unsharpness, mm (10–3 in.)

Source
m
00
Source

0.6 (24)
1.

.)
in
0
(5
m
25

.)
1.

0.5 (20) in
Do 0
(6
m )
50 in.
1. (7
0
0.4 (16) m
75 n.)
1. 0i
(8
0m
Object
0.3 (12) 2.0

d
0.2 (8)

Film plane

0.1 (4)

Ug

0
Legend 0 25 50 75 100 125 150
Do = source-to-object distance (1) (2) (3) (4) (5) (6)
d = object-to-film distance
F = radiation source Specimen thickness, mm (in.)
Ug = geometric unsharpness

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governed by the distance between the that at the level C1. The exposure that
tube (source) and the specimen, varying would be adequate at C1 must be
inversely with the square of this distance. increased four times to produce at C2 a
The explanation that follows is in terms radiograph of equal density. In practice,
of X-rays and light but applies to gamma this can be done by increasing the time or
rays as well. by increasing the milliamperage.
Because X-rays conform to the laws of The inverse square law can be
light they diverge when they are emitted expressed algebraically as follows:
from the anode and cover an increasingly
larger area with lessened intensity as they I1 D22
travel from their source. This principle is (5) =
illustrated in Fig. 10. In this example, it is
I2 D12
assumed that the intensity of the X-rays
emitted at the anode A remains constant where I1 and I2 are the intensities at
and that the X-rays passing through the distances D1 and D2, respectively.
aperture B cover an area of 25.8 cm2
(4 in.2) on reaching the recording surface
C1, which is 305 mm (12 in.) from the
anode (distance D). Relations of Source
When the recording surface is moved Strength (Milliamperage),
305 mm (12 in.) farther from the anode,
to C2, so that the distance (2D) from the
Distance and Time
anode is 610 mm (24 in.) or twice its With a given kilovoltage of X-radiation or
earlier value, the X-rays will cover with the gamma radiation from a
103.4 cm2 (16 in.2) — an area four times particular isotope, the three factors
as great as that at C1. It follows, therefore, governing the exposure are the
that the radiation per square centimeter milliamperage (for X-rays) or source
on the surface at C2 is only one fourth of strength (for gamma rays), time and

FIGURE 9. With very small focal spot, FIGURE 10. Schematic diagram illustrating
enlarged image can be obtained. Degree of inverse square law.
enlargement depends upon ratio of A
source-to-film and source-to-specimen
distances.
Anode
Focal spot B

Diaphragm

Void C1
Specimen
2D

C2

Film and
cassette
Legend
A = radiation source
B = focal point
C1 = first film plane
C2 = second film plane
D = source-to-film distance

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source-to-film distance. The numerical calculations based on the inverse square


relations among these three quantities are law would indicate because of absorption
demonstrated below, using X-rays as an of the X-rays by the air. Most industrial
example. The same relations apply for radiography, however, is done with
gamma rays, provided the number of radiation so penetrating that the air
becquerels (curies) in the source is absorption need not be considered. These
substituted wherever milliamperage comments also apply to the
appears in an equation. time-to-distance relations discussed below.
The necessary calculations for any
changes in focus-to-film distance D, Relationship of Time and Distance
milliamperage M or time T are matters of
simple arithmetic and are illustrated in Rule: If tube current (mA) is held constant,
the following example. As noted earlier, the exposure time T required for a given
kilovoltage changes cannot be calculated exposure is directly proportional to the square
directly but must be obtained from the of the focus-to-film distance D:
exposure chart of the equipment or the
operator’s log book. (8) T1 : T2 = D12 : D22

Relationship of Source Strength or


and Distance
Rule: If exposure time is held constant, the T1 D12
=
milliamperage (M) required for a given T2 D22
exposure is directly proportional to the square
of the source-to-film distance (D). The
equation is expressed as follows: Relation of Milliamperage to Time
Rule: If distance is held constant but
(6) M1 : M 2 = D12 : D22 exposure must be changed, the milliamperage
M required for a given exposure is inversely
proportional to the time T:
or

M1 D12 (9) M1 : M 2 = T2 : T1
=
M2 D22
or
For example, suppose that with a given M1 T2
exposure time and kilovoltage, a properly =
exposed radiograph is obtained with 5 mA M2 T1
(M1) at a distance of D1 of 120 mm
(30 in.) and that it is desired to increase Another way of expressing this is to say
the sharpness of detail in the image by that for a given set of conditions (voltage,
increasing the focus-to-film distance D2 to distance and others), the product of
240 mm (60 in.). The correct milliamperage and time is constant for
milliamperage M2 to obtain the desired the same photographic effect. Thus:
radiographic density at the increased
distance D2 may be computed from the (10) M1 T1 = M 2 T2 = M 3 T3
proportion: = C (a constant)

(7) 5 : M2 = 30 2 : 60 2 This commonly referred to as the


reciprocity law. (Important exceptions are
discussed below.)
or

5 302
Tabular Solution of Source
= Strength, Time and Distance
M2 602
Problems
Problems of the types discussed above
or
may also be with a table similar to
Table 1. The factor between the new and
602 3600 the old exposure time, milliamperage, or
M2 = 5 × = 5 ×
302 900 milliampere minute (mA·min) value
appears in the box at the intersection of
= 5 × 4 = 20 mA
the column for the new source-to-film
distance and the row for the old
When very low kilovoltages, say 20 kV source-to-film distance.
or less, are used, the X-ray intensity Note that some approximation is
decreases with distance more rapidly than involved in such a table because the

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values in the boxes are rounded off to two Departures may be apparent, however, if
significant digits. However, the errors the intensity is changed by a factor of 4 or
involved are always less than 5 percent more. Because intensity may be changed
and, in general, are insignificant in actual by changing the source-to-film distance,
practice. Also, a table of this type cannot failure of the reciprocity law may appear
include all source-to-film distances. to be a violation of the inverse square law.
However, in any one radiographic Applications of the reciprocity law over a
department, only a few source-to-film wide intensity range sometimes arise and
distances are used in the great bulk of the the relation between results and
work and a table of reasonable size can be calculations may be misleading unless the
made using only these few distances. possibility of reciprocity law failure is kept
in mind. Failure of the reciprocity law
means that the efficiency of a light
sensitive emulsion in responding to the
Reciprocity Law light energy depends on the light
In the preceding text, it has been assumed intensity.
that exact compensation for a decrease in
the time of exposure can be made by Exposure Factor
increasing the milliamperage according to
the relation M1T1 = M2T2. This may be The exposure factor is a quantity that
written MT = C and is an example of a combines milliamperage (X-rays) or source
general photochemical law: the same strength (gamma rays), time and distance.
effect is produced for IT = constant, where Numerically the exposure factor equals
I is intensity of the radiation and T is the
time of exposure. This is called the X - ray
Milliamperes × Time
reciprocity law and is true for direct X-ray (11) = exposure
and lead screen exposures. For exposure to Distance2 factor
light, it is not quite accurate and, because
some radiographic exposures are made and
with the light from fluorescent
intensifying screens, the law cannot be Activity × Time Gamma ray
strictly applied. (12) = exposure
Formally defined, the Bunsen-Roscoe Distance2 factor
reciprocity law states that the result of a
photochemical reaction is dependent only Activity is measured in becquerels (Bq) or
on the product of radiation intensity I and curies (Ci), where 3.7 × 1010 Bq = 37 GBq
the duration of the exposure T and is = 1.0 Ci.
independent of absolute values of either Radiographic techniques are sometimes
quantity. given in terms of kilovoltage and
Errors that result for assuming the exposure factor, or radioactive isotope and
validity of the reciprocity law are usually exposure factor. In such a case, it is
so small that they are not noticeable in necessary merely to multiply the exposure
examples of the types given here. factor by the square of the distance to

TABLE 1. Value of source strength–time (mA·min) is multiplied by factor shown in this table when
source-to-film distance is changed. (The same factors apply regardless of unit of distance — for
example, multiply by same factor if both old and new distance are measured in inches instead of
millimeters.)
Old New Source-to-Film Distance (mm)
Source-to-Film ________________________________________________________________________________________
Distance (mm) 250 300 350 400 450 500 550 600 650 700 750 800
250 1.0 1.4 2.0 2.6 3.2 4.0 4.8 5.6 6.8 7.8 9.0 10.0
300 0.70 1.0 1.4 1.8 2.3 2.8 3.4 4.0 4.8 5.4 6.3 7.1
350 0.51 0.74 1.0 1.3 1.6 2.0 2.5 3.0 3.4 4.0 4.6 5.2
400 0.39 0.56 0.77 1.0 1.3 1.6 1.9 2.2 2.6 3.1 3.5 4.0
450 0.31 0.45 0.60 0.79 1.0 1.2 1.5 1.8 2.1 2.4 2.8 3.2
500 0.25 0.36 0.49 0.64 0.81 1.0 1.2 1.4 1.7 2.0 2.2 2.6
550 0.21 0.30 0.40 0.53 0.67 0.83 1.0 1.2 1.4 1.6 1.9 2.1
600 0.17 0.25 0.34 0.44 0.56 0.69 0.84 1.0 1.2 1.4 1.6 1.8
650 0.15 0.21 0.29 0.38 0.48 0.59 0.72 0.85 1.0 1.2 1.3 1.5
700 0.13 0.18 0.25 0.33 0.41 0.51 0.62 0.74 0.86 1.0 1.1 1.3
750 0.11 0.16 0.22 0.28 0.36 0.45 0.54 0.64 0.75 0.87 1.0 1.1
800 0.10 0.14 0.19 0.25 0.32 0.39 0.47 0.56 0.66 0.77 0.88 1.0

Principles of Film Radiography 149


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find, for example, the milliampere Suppose, for example, it is desired to


minutes or the curie hours required. change from radiographing 38 mm
(1.5 in.) thick steel to radiographing
50 mm (2 in.) thick steel. For a given
X-ray machine, the 50 mm (2 in.) thick
Determination of Exposure steel will require more than 10 times the
Factors exposure in milliampere minutes at
170 kV than the 38 mm (1.5 in.) thick
steel requires. However, increasing the
X-Rays kilovoltage to a little more than 200 will
The focus-to-film distance is easy to yield a comparable radiograph with the
establish by actual measurement, the same milliampere minutes.
milliamperage can conveniently be Therefore, kilovoltage is an important
determined by the milliammeter supplied variable because economic considerations
with the X-ray machine and the exposure often require that exposure times be kept
time can be accurately controlled by a within fairly narrow limits. It is desirable,
good time switch. The tube voltage, as a rule, to use as low a kilovoltage as other
however, is difficult and inconvenient to factors will permit. In the case of certain
measure accurately. Furthermore, designs high voltage X-ray machines, the
of individual machines differ widely and technique of choosing exposure
may give X-ray outputs of a different conditions may be somewhat modified.
quality and intensity even when operated For instance, the kilovoltage may be fixed
at the nominal values of peak kilovoltage rather than adjustable at the will of the
and milliamperage. operator, leaving only milliamperage,
Consequently, although specified exposure time, film type and focus-to-film
exposure techniques can be duplicated distance as variables.
satisfactorily in the factors of
source-to-film distance, milliamperage Gamma Rays
and exposure time, one apparatus may With radioactive materials, the variable
differ materially from another in the factors are more limited than with X-rays.
kilovoltage setting necessary to produce Not only is the quality (energy or
the same radiographic density. Because of wavelength) of the radiation fixed by the
this, the kilovoltage setting for a given nature of the radiation emitter, but also
technique should be determined by trial the intensity is fixed by the amount of
on each X-ray generator. In the radioactive material in the particular
preliminary tests, published exposure source. The only variables under the
charts may be followed as an approximate control of operators and the only
guide. It is customary for equipment quantities they need to determine are the
manufacturers to calibrate X-ray machines source-to-film distance, film type and the
at the factory and to furnish suitable exposure time. As in the case of
exposure charts. For the unusual problems X-radiography, it is desirable to develop
that arise, it is desirable to record in a trial exposures using the gamma ray
logbook all the data on exposure and sources under standardized conditions
techniques. In this way, operators will and to record all data on exposures and
soon build up a source of information techniques.
that will make them more competent to
deal with difficult situations.
For developing trial exposures, a
standardized technique should always be Radiographic Contrast
used so that any variation in the quality
of the trial radiographs may then be In a radiograph, the various intensities
attributed to the exposure alone. This transmitted by the specimen are rendered
technique obviates many of the variable as different densities in the image. The
factors common to radiographic work. density differences from one area to
Because an increase of kilovoltage another constitute radiographic contrast.
produces a marked increase in X-ray Details in the image are visible by reason
output and penetration (see Fig. 3), it is of the contrast between them and their
necessary to maintain a close control of background. Within appropriate limits,
this factor to secure radiographs of the greater the contrast or density
uniform density. In many types of differences in the radiograph, the more
industrial radiography where it is definitely various details will stand out.
desirable to maintain constant exposure However, if overall contrast is increased
conditions for source-to-film distance, too much, there may be an actual loss in
milliamperage and exposure time, it is detail visibility in both the thick and the
common practice to vary the kilovoltage thin regions of the specimen as the image
in accordance with the thickness of the is too light or too dark to display useful
material to be examined to secure proper contrast (see discussion of film contrast,
density in the radiographic image. below).

150 Radiographic Testing


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Radiographic contrast is the result of density to which the radiograph is


both subject contrast and film contrast. exposed and film processing.
Subject contrast is governed by the range The classification of film types and
of radiation intensities transmitted by the their speeds are discussed in the chapter
specimen. A flat sheet of homogeneous on film processing.
material of nearly uniform thickness
would have very low subject contrast.
Conversely, a specimen with large
variations in thickness, which transmits a Radiographic Sensitivity
wide range of intensities, would have high Radiographic sensitivity refers to the size
subject contrast. Overall subject contrast of the smallest detail that can be seen in a
could be defined as the ratio of the radiograph or to the ease with which the
highest to the lowest radiation intensities images of small details can be detected.
falling on the film. The subject contrast is Sensitivity depends on the sharpness
affected by the X-ray kilovoltage. As and the contrast of the radiograph. Thus,
shown in Fig. 11, a lower kilovoltage will the grain size of the film, as well as its
increase subject contrast and so increase contrast and other factors such as the
sensitivity to small variations in the exposure geometry and radiation energy,
object. Contrast is also affected by affect sensitivity.
scattered radiation, removal of which In radiography of materials of
increases subject contrast, and by the approximately uniform thickness, where
energy of the primary radiation. the range of transmitted X-ray intensities
is small, a technique producing high
Choice of Film contrast may satisfactorily render all
portions of the area of interest and the
Different films have different contrast radiographic sensitivity will usually be
characteristics. Thus, a film of high greater than with a technique producing
contrast may give a radiograph of low contrast. If, however, the part
relatively low overall contrast if the radiographed transmits a wide range of
subject contrast is very low; conversely, a X-ray intensities, then a technique
film of low contrast may give a producing lower contrast may be
radiograph of relatively high overall necessary to achieve radiographic
contrast if the subject contrast is very sensitivity in all regions of the part.
high. With any given specimen, the
contrast of the radiograph will depend on
the kilovoltage or quality of the X-rays or
gamma rays, the contrast characteristics of
the film, the type of screen, scatter, the

FIGURE 11. As kilovoltage increases, subject contrast


decreases. More wavelengths penetrate subject in both thick
and thin sections, thus reducing overall difference in
exposure between them: (a) low kilovoltage selected for four
half value layers in thick section; (b) kilovoltage increased to
get two half value layers in thick section.
(a) (b)

Low kV High kV

Half value layer

Half value layer

I0 I0 I0 I0
I = I = I = I =
16 4 4 2

Principles of Film Radiography 151


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PART 2. Absorption and Scattering

from the specimen are usually


Radiation Absorption in unimportant radiographically; those from
materials in contact with the film, such as
Specimen screens of lead or other materials, are very
When X-rays or gamma rays strike an important.
absorber (Fig. 12), some radiation is
absorbed or deflected and some passes Radiographic Equivalency of
through undeviated. It is the intensity
variation of the undeviated radiation from
Materials
area to area in the specimen that forms Because various wavelengths exist in
the useful image in a radiograph. The X-rays and gamma rays and because
radiation that is scattered is not image considerable scattered radiation reaches
forming. Scattered radiation will expose the film, the laws of radiation absorption
the film and thus tend to obscure the must be given in a general way.
useful radiographic image. Therefore, The absorption of a specimen depends
scatter must be carefully controlled. on its thickness, on its density and on the
(Scattered radiation and the means for atomic composition of the material.
reducing its effects are discussed in detail Comparing two specimens of the same
below.) Another portion of the original composition, the thicker or the more
beam’s energy is spent in liberating dense will absorb more radiation and so
electrons from the absorber. The electrons require more kilovoltage or exposure, or
both, to produce the same photographic
result.
However, the atomic elements in a
FIGURE 12. Schematic diagram of some ways X-ray or specimen often exert a far greater effect
gamma ray energy is dissipated on passing through matter. upon X-ray absorption than either the
Electrons from specimens are usually unimportant thickness or the density. For example, lead
radiographically; those from lead foil screens are very is about 1.5 times as dense as ordinary
important. steel but at 220 kV, 2.5 mm (0.1 in.) of
lead absorbs as much as 30.5 mm (1.2 in.)
of steel. Brass is only about 1.1 times as
dense as steel, yet, at 150 kV, the same
exposure is required for 6.4 mm (0.25 in.)
of brass as for 8.9 mm (0.35 in.) of steel.
Table 2 gives approximate radiographic
equivalence factors. It should be
emphasized that this table is approximate
Primary radiation and is intended merely as a guide because
it is based on a compilation of data from
many sources. In a particular instance, the
exact value of the radiographic
equivalence factor will depend on the
quality of the X-radiation and the
Absorber thickness of the specimen. It will be noted
from this table that the relative
absorptions of the different materials are
not constant but change with kilovoltage
and that as the kilovoltage increases the
differences between all materials tend to
become less. In other words, as
kilovoltage is increased, the radiographic
Secondary X–rays or absorption of a material becomes less
gamma rays Electrons dependent on the atomic numbers of its
Unabsorbed constituents.
primary radiation For X-rays generated at voltages more
(image forming) than 1 MeV and for materials not
differing too greatly in atomic number
(steel and copper, for example), the

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TABLE 2. Approximate radiographic equivalence factors.a


X-Rays (kV)
___________________________________________________ Gamma Rays
______________________________________________
Material 50 100 150 220 400 1000 2000 4 to 25b Iridium-192 Cesium-137 Cobalt-60 Radium
Magnesium 0.6 0.6 0.5 0.08
Aluminum 1.0 1.0 0.12 0.18 0.35 0.35 0.35 0.40
2024 aluminum alloy 2.2 1.6 0.16 0.22 0.35 0.35 0.35
Titanium 0.45 0.35
Steel 12.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0
Steel alloyc 12.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0 1.0
Copper 18.0 1.6 1.4 1.4 1.3 1.1 1.1 1.1 1.1
Zinc 1.4 1.3 1.3 1.0 1.1 1.0 1.0 1.0
Brassd 1.4 1.3 1.3 1.2 1.2 1.0 1.1 1.1 1.1 1.1
Nickel alloye 16.0 1.4 1.3 1.3 1.3 1.3 1.0 1.3 1.3 1.3 1.3
Zirconium 2.3 2.0 1.0
Lead 14.0 12.0 5.0 2.5 3.0 4.0 3.2 2.3 2.0
Uranium 25.0 3.9 12.6 5.6 3.4

a. Aluminum is the standard metal at 50 kV and 100 kV; steel is the standard metal with high voltages and gamma rays. The thickness of another metal is
multiplied by the corresponding factor to obtain the approximate equivalent thickness of the standard metal. The exposure applying to this thickness of the
standard metal is used. Example: to radiograph 12.7 mm (0.5 in.) of copper at 220 kV, multiply 12.7 mm (0.5 in.) by the factor 1.4, obtaining an equivalent
thickness of 17.8 mm (0.7 in.) of steel.
b. 4 to 25 MeV.
c. Alloy consisting of 18 percent chromium, 8 percent nickel.
d. Tin or lead alloyed in brass will increase these factors.
e. Alloy consisting of 73 percent nickel, 15 percent chromium.

radiographic absorption for a given Scattering of radiation occurs and is a


thickness of material is roughly problem in radiography with both X-rays
proportional to the density of the and gamma rays. In the text which
material. However, even at high voltages follows, the discussion is in terms of
or with penetrating gamma rays, the X-rays but the same general principles
effect of composition on absorption apply to gamma radiography.
cannot be ignored when dealing with In the radiography of materials that are
materials that differ widely in atomic thick relative to the radiation energy,
number. For instance, the absorption of scattered radiation forms most of the total
lead for 1 MeV X-rays is about five times radiation. For example, in the radiography
that of an equal thickness of steel, of a 19 mm (0.75 in.) thickness of steel,
although its density is only 1.5 times as the scattered radiation from the specimen
great. is almost twice as intense as the primary
radiation; in the radiography of a 50 mm
(2 in.) thickness of aluminum, the
scattered radiation is 2.5 times as great as
Scattered Radiation the primary radiation. Preventing scatter
When a beam of X-rays or gamma rays from reaching the film markedly improves
strikes any object, some of the radiation is the quality of the radiographic image.
absorbed, some is scattered and some As a rule, the greater portion of the
passes straight through. The electrons of scattered radiation affecting the film is
the atoms constituting the object scatter from the specimen under examination (A
radiation in all directions, much as light is in Fig. 13). However, any portion of the
dispersed by fog. The wavelengths of film holder or cassette that extends
much of the radiation are increased by beyond the boundaries of the specimen
the scattering process and hence the and thereby receives direct radiation from
scatter is of longer wavelength and is the X-ray tube also becomes a source of
somewhat softer, or less penetrating, than scattered radiation that can affect the
the unscattered primary radiation. Any film. The influence of this scatter is most
material — whether specimen, cassette, noticeable just inside the borders of the
tabletop, walls or floor — that receives the image (B in Fig. 13) and is often referred
direct radiation is a source of scattered to as undercut. In a similar manner,
radiation. Unless suitable measures are primary radiation striking the film holder
taken to reduce the effects of scatter, it or cassette through a thin portion of the
will reduce the contrast over the whole specimen will cause scattering into the
image or parts of it. Scatter forms fog of shadows of the adjacent thicker portions.
nonuniform density.

Principles of Film Radiography 153


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Another source of scatter that may and gamma ray sources. For example, a
undercut a specimen is shown as C in mask (see Fig. 15) for use with 200 kV
Fig. 13. If a filter is used near the tube, X-rays could easily be light enough for
this too will scatter X-rays. However, convenient handling. A mask for use with
because of the distance from the film, cobalt-60 radiation, on the other hand,
scattering from this source is negligible. would be thick, heavy and probably
Any other material, such as wall or floor, cumbersome. In any event, with either
on the film side of the specimen may also X-rays or gamma rays, the means for
scatter an appreciable quantity of X-rays reducing the effects of scattered radiation
back to the film, especially if the material must be chosen on the basis of cost,
receives the direct radiation from the convenience and effectiveness.
X-ray tube or gamma ray source (Fig. 14).
This is referred to as backscattered Lead Foil Screens
radiation.
Lead screens, mounted in contact with
the film, diminish the effect on the film
of scattered radiation from all sources.
Reduction of Scatter They are beyond doubt the least
Although scattered radiation can never be expensive, most convenient and most
completely eliminated, a number of universally applicable means of
means are available to reduce its effect. combating the effects of scattered
The various techniques are discussed in radiation. Lead screens lessen the scatter
terms of X-rays. Although most of the reaching the films regardless of whether
same principles apply to gamma and the screens permit a decrease or
megavolt X-ray radiography, differences in necessitate an increase in the radiographic
application arise because of the highly exposure. The nature of the action of lead
penetrating radiation emitted by megavolt

FIGURE 14. Intense backscattered radiation


FIGURE 13. Sources of scattered radiation. may originate in the floor or wall.
Collimating, masking or diaphragming
Anode
should be used. Backing the cassette with
Focal spot lead may give adequate protection.
Anode
Focal spot

Diaphragm

Filter

Diaphragm

Specimen

Film

A A C A
A
Specimen
B B B

Film and cassette

Legend
A = transmitted scatter
B = scatter from cassette Floor or wall
C = diffraction scatter

154 Radiographic Testing


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screens is discussed more below. Definite Masks and Diaphragms


means must be provided to ensure good
Scattered radiation originating in matter
contact with the film to ensure image
outside the specimen is most serious for
sharpness.
specimens that have high absorption for
Many X-ray holders or cassettes
X-rays because the scattering from
incorporate a sheet of lead foil in the back
external sources may be large compared to
for the specific purpose of protecting the
the primary image forming radiation that
film from backscatter from the table or
reaches the film through the specimen. If
other objects. This lead will not serve as
many specimens of the same article are to
an intensifying screen — first because it
be radiographed, it may be worthwhile to
usually has a paper facing and second
cut an opening of the same shape, but
because it often is not lead of radiographic
slightly smaller, in a sheet of lead and
quality.
place this on the object. The lead serves to
When radiographic film cassettes fitted
reduce the exposure in surrounding areas
with a sheet of lead foil in the back for
and thus to reduce scattered radiation
protection against backscatter are used
from this source. Because scatter also
with gamma rays or with X-rays above
arises from the specimen itself, it is good
200 kV, the film should always be
practice, wherever possible, to limit the
enclosed between double lead screens;
cross section of an X-ray beam to cover
otherwise, the secondary radiation from
only the area of the specimen that is of
the lead backing is sufficient to penetrate
interest in the examination.
the intervening felt or paper and cast a
For occasional pieces of work with low
shadow of this material on the film giving
energy radiation, where a cutout
a granular or mottled appearance.
diaphragm would not be economical,
barium clay packed around the specimen
may serve the same purpose. The clay
FIGURE 15. Combined use of metallic shot and lead mask for should be thick enough so that the film
lessening scattered radiation is conducive to good density under the clay is somewhat less
radiographic quality. If several round bars are to be than that under the specimen. Otherwise,
radiographed, they may be separated along their lengths the clay itself contributes appreciable
with lead strips held on edge by wooden frame and voids scattered radiation.
filled with fine shot. One of the most satisfactory
arrangements, combining effectiveness
Anode and convenience, is to surround the
Focal spot object with copper or steel shot having a
diameter of about 0.25 mm (0.01 in.) or
less (Fig. 15). Steel is best for objects of
low atomic number; copper, for steel and
objects of higher atomic number than
iron. The materials flow and are effective
for filling cavities or irregular edges of
Diaphragm
objects, such as castings, where a normal
exposure for thick parts would result in an
overexposure for thinner parts. Of course,
it is preferable to make separate exposures
for thick and thin parts but this is not
always practical.
In some cases, a lead diaphragm or lead
cone on the tube head may be a
convenient way to limit the area covered
by the X-ray beam. Such lead diaphragms
are particularly useful where the desired
cross section of the beam is a simple
Fine metallic shot Specimen
geometric figure, such as a circle, square
or rectangle.

Filters
In general, filters are limited to
radiography with X-rays below 1 MeV. A
simple metallic filter mounted in the
X-ray beam near the X-ray tube (Fig. 16)
Lead mask may adequately serve the purpose of
eliminating overexposure in the thin
regions of the specimen and in the area
Film and cassette surrounding the part (Table 3). Such a
filter is particularly useful for reducing
scatter undercut in cases where a mask

Principles of Film Radiography 155


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around the specimen is impractical. Of In regions of strong undercut, the


course, an increase in exposure of contrast is increased by a filter because the
kilovoltage will be required to compensate only effect of the undercutting radiation
for the additional absorption. is to obscure the desired image. In regions
The underlying principle of the where the undercut is negligible, a filter
technique is that the filter absorbs more has the effect of decreasing the contrast in
of the softer radiation of the primary the finished radiograph.
beam than it does the harder radiation. A filter reduces excessive subject
This causes a greater change in the contrast (and hence radiographic contrast)
amount of radiation passing through the by hardening the radiation. The longer
thin parts than through the thicker parts. wavelengths do not penetrate the filter to
as great an extent as do the shorter
wavelengths. Therefore, the beam
emerging from the filter contains a higher
FIGURE 16. Filter placed near X-ray tube proportion of the more penetrating
reduces subject contrast and eliminates wavelengths (see Fig. 17).
much of secondary radiation, which tends to The choice of a filter material should
obscure detail in periphery of specimen. be made on the basis of availability and
ease of handling. For the same filtering
Anode
effect, the thickness of filter required is
Focal spot
less for those materials having higher
absorption. In many cases, copper or brass
is the most useful, because filters of these
materials will be thin enough to handle
easily yet not so thin as to be delicate (see
Diaphragm Fig. 18).
Rules for filter thicknesses are difficult
to formulate exactly because the amount
Filter of filtration required depends not only on
the material and thickness range of the
specimen but also on the distribution of
material in the specimen and on the
amount of scatter to be eliminated. In the
radiography of aluminum, a filter of
copper about 4 percent of the greatest
thickness of the specimen should provide
the thickness necessary. With steel, a
copper filter should ordinarily be about
20 percent, or a lead filter about 3
percent, of the greatest specimen
thickness for the greatest useful filtration.
The foregoing values are maximum
Specimen
values; depending on circumstances,
useful radiographs can often be made
with far less filtration.

FIGURE 17. Curves illustrating effect of filter


on composition and intensity of X-ray beam.
Film and cassette Wavelengths
reduced in
intensity by
addition of filter
Intensity (relative unit)

Unfiltered
TABLE 3. Effect of metallic filter on X-ray intensity. beam
Original
X-Ray Intensity
Specimen Remaining after
Thickness
_______________ Addition of Filter
__________________
Region mm (in.) (percent)

Outside specimen 0 (0) < 10 Filtered


beam
Thin section 6.4 (0.25) ~ 30
Medium section 12.7 (0.50) ~ 40
Wavelength (relative unit)
Thick section 25.4 (1.0) ~ 55

156 Radiographic Testing


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In radiography with X-rays up to at black arrows in Fig. 19. Thus, the shadows
least 250 kV, a 0.125 mm (0.005 in.) front of the lead strips are blurred to the point
lead screen is an effective filter for the that they do not appear in the final
scatter from the bulk of the specimen. radiograph.
Additional filtration between specimen The potter-bucky diaphragm
and film only tends to contribute complicates industrial radiographic testing
additional scatter from the filter itself and and necessarily limits the flexibility of the
harden the beam unnecessarily. arrangement of the X-ray tube, the
specimen and the film. Grids can,
Grid Diaphragms however, be of great value in the
radiography of beryllium more than
One of the most effective ways to reduce 75 mm (3 in.) thick and in the
scattered radiation from an object being examination of other low absorption
radiographed at energies up to 400 kV is materials of moderate and great
with a potter-bucky diaphragm. This thicknesses.
apparatus (Fig. 19) consists of a moving Special forms also have been designed
grid, composed of lead strips held in for the radiography of steel with voltages
position by intervening strips of a as high as 200 to 400 kV. These
material transparent to X-rays. The lead diaphragms are not used at higher
strips are tilted, so that the plane of each voltages or with gamma rays because
is in line with the focal spot of the tube. relatively thick lead strips would be
The slots between the lead strips are needed to absorb the radiation scattered
several times as deep as they are wide. The at these energies. This in turn would
lead strips have the function of absorbing require a potter-bucky diaphragm, with
the very divergent scattered rays from the
object being radiographed, so that most of
the exposure is made by the primary rays
emanating from the focal spot of the tube FIGURE 19. Schematic diagram showing how primary X-rays
and passing between the lead strips. pass between lead strips of potter-bucky diaphragm. Most of
During the course of the exposure, the scattered X-rays are absorbed because they strike sides of
grid is moved, or oscillated (out of strips.
synchronization with the X-ray pulse) in a Anode
plane parallel to the film as shown by the
Focal spot

FIGURE 18. Maximum filter thickness for aluminum and steel.

2.5

2.25 Diaphragm
Steel (lead filter)

2.0
Material thickness (relative unit)

1.75
Aluminum (copper filter)

1.5

Specimen
1.25

1.0

0.75
Steel (copper filter)

0.5

Film and cassette


0.25 Potter-bucky diaphragm
0 1.0 2.0 3.0

Filter thickness (relative unit)

Principles of Film Radiography 157


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the associated mechanism, of an and thus as a basis for the acceptance or


uneconomical size and complexity. the rejection of parts.

Mottling Caused by X-Ray Scattering in High Voltage


Diffraction Megavolt Radiography
A special form of scattering caused by Lead screens should always be used in the
X-ray diffraction is encountered 1 or 2 MeV range. The common
occasionally. It is most often observed in thicknesses, 0.125 mm (0.005 in.) front
the radiography of fairly thin metallic and 0.25 mm (0.010 in.) back, are both
specimens whose grain size is large satisfactory and convenient. Some users,
enough to be an appreciable fraction of however, find a 0.25 mm (0.010 in.) front
the part thickness. The radiographic screen of value because of its greater
appearance of this type of scattering is selective absorption of the scattered
mottled and may be confused with the radiation from the specimen.
mottled appearance sometimes produced At these voltages filtration at the tube
by porosity or segregation. It can be offers no improvement in radiographic
distinguished from these conditions by quality. Filters at the film improve the
making two successive radiographs, with radiograph in the examination of uniform
the specimen rotated slightly (1 to sections but give poor quality at the edges
5 degrees) between exposures, about an of an image because of undercut of
axis perpendicular to the central beam. A scattered radiation from the filter itself.
pattern caused by porosity or segregation Hence, filtration should not be used in
will change only slightly; however, one the radiography of specimens containing
caused by diffraction will show a marked narrow bars, for example, no matter what
change. The radiographs of some the thickness of the bars in the direction
specimens will show a mottling from both of the primary radiation. Also, filtration
effects and careful observation is needed should be used only where the film can
to differentiate between them. be adequately protected against
Relatively large crystal or grain in a backscattered radiation.
relatively thin specimen may in some Lead filters are most convenient for
cases diffract an appreciable portion of the this voltage range. When used between
X-ray energy falling on the specimen, specimen and film, filters are subject to
much as if it were a small mirror. This will mechanical damage. Care should be taken
result in a light spot on the developed to reduce this to a minimum, lest filter
radiograph corresponding to the position anomalies be confused with structures in
of the particular crystal and may also or on the specimen. In radiography with
produce a dark spot in another location if megavolt X-rays, specimens of uniform
the diffracted, or reflected, beam strikes sections may be conveniently divided into
the film. Should this beam strike the film three classes. Below 38 mm (1.5 in.) of
beneath a thick part of the specimen, the steel, filtration affords little improvement
dark spot may be mistaken for a void in in radiographic quality. Between 38 and
the thick section. This effect is not 100 mm (1.5 and 4.0 in.) of steel, the
observed in most industrial radiography, thickest filter, up to 3 mm (0.125 in.)
for most specimens are composed of a lead, that allows a reasonable exposure
multitude of very minute crystals or time, may be used. Above 100 mm
grains variously oriented; hence scatter by (4.0 in.) of steel, filter thicknesses may be
diffraction is essentially uniform over the increased to 6.3 mm (0.25 in.) of lead,
film area. In addition, the directly economic considerations permitting. It
transmitted beam usually reduces the should be noted that in the radiography
contrast in the diffraction pattern to a of extremely thick specimens with
point where it is no longer visible on the megavolt X-rays, fluorescent screens may
radiograph. increase the photographic speed to a
The mottling caused by diffraction can point where filters can be used without
be reduced and in some cases eliminated requiring excessive exposure time.
by raising the kilovoltage and by using A very important point is to block off
lead foil screens. The former is often of all radiation except the useful beam with
positive value even though the heavy (12.7 to 25.4 mm [0.5 in. to 1 in.])
radiographic contrast is reduced. Because lead at the tubehead. This step is called
definite rules are difficult to formulate, collimation. Unless this is done, radiation
both approaches should be tried in a new striking the walls of the X-ray room will
situation and perhaps both used together. scatter back enough to seriously affect the
It should be noted, however, that in quality of the radiograph. This will be
some instances, the presence or absence especially noticeable if the specimen is
of mottling caused by diffraction has been thick or has parts projecting relatively far
used as a rough indication of grain size from the film.

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PART 3. Radiographic Screens

the photographic action on the film,


Functions of Screens largely by reason of the electrons emitted
and partly by the secondary X-rays
Radiographic screens help radiographers emitted by the lead; (2) it absorbs the
to use more fully the X-ray or gamma ray longer wavelength scattered radiation
energy reaching the film. The physical more than the primary; and (3) it
principles underlying the action of both intensifies the primary radiation more
lead foil and fluorescent screens are than the scattered radiation. The
discussed elsewhere and only the practical differential absorption of the secondary
applications are discussed here. radiation and the differential
When an X-ray or gamma ray beam intensification of the primary radiation
strikes a film, usually less than one result in diminishing the effect of
percent of the energy is absorbed. Because scattered radiation, producing greater
the formation of the radiographic image is contrast and clarity in the radiographic
governed by the absorbed radiation, more image. This reduction in the effect of the
than 99 percent of the available energy in scattered radiation decreases the total
the primary radiation reaching the film intensity of the radiation reaching the
performs no useful photographic work. film and lessens the net intensification
Obviously, any means of more fully using factor of the screens. The absorption of
this wasted energy, without complicating primary radiation by the front lead screen
the technical procedure, is highly also diminishes the net intensifying effect;
desirable. Three types of radiographic and, if the incident radiation does not
screens are commonly used for this have sufficient penetrating power, the
purpose — lead, fluorescent and actual exposure required may be even
fluorometallic (metal phosphor). Metals greater than without screens. At best, the
other than lead are sometimes used in exposure time is one half to one third of
megavolt radiography. Lead screens may that without screens but the advantage of
be in the form of thin foil, usually screens in reducing scattered radiation
mounted on a thin cardboard or plastic still holds.
sheet, or in the form of a lead compound, The quality of the radiation necessary
usually lead oxide, evenly coated on a to obtain an appreciable intensification
thin support. The lead compound screens from lead foil screens depends on the type
are usually used only for radiography of film, the kilovoltage and the thickness
below 150 kV. and nature of the material through which
the rays must pass (Fig. 20). In the
radiography of aluminum, for example,
using a 0.125 mm (0.005 in.) front screen
Lead Foil Screens and a 0.25 mm (0.010 in.) back screen,
For radiography with X-ray or gamma ray the thickness of aluminum must be about
energies between 150 kV and 2 MeV, lead 150 mm (6 in.) and the kilovoltage as
foil screens in intimate contact with both high as 160 kV to secure any advantage in
sides of the film, within the film holder, exposure time with lead screens. In the
will reduce exposure times and improve radiography of steel, lead screens begin to
radiographic quality by reducing scatter. give appreciable intensification with
Foils as thin as 0.10 to 0.15 mm (0.004 to thicknesses in the neighborhood of
0.006 in.) are commonly used. To reduce 6.3 mm (0.25 in.), at voltages of 130 to
backscatter from the table or floor of the 150 kV. In the radiography of 32 mm
room an additional lead sheet 3 to 6 mm (1.25 in.) steel at about 200 kV, lead
(0.12 to 0.25 in.) thick is usually placed screens permit an exposure of about
behind the film holder. one third of that without screens
The choice of screens and filters for (intensification factor of 3). With
radiography above 1 to 2 MeV is more cobalt-60 gamma rays, the intensification
complicated, as discussed in the section factor of lead screens is about 2. Lead foil
on high energy radiography. screens, however, do not detrimentally
affect the definition or graininess of the
Effects of Lead Screens radiographic image to any material degree
so long as the lead and the film are in
Lead foil in direct contact with the film intimate contact.
has three principal effects: (1) it increases

Principles of Film Radiography 159


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Lead foil screens also diminish the


effect of scattered radiation. Scattered FIGURE 21. Upper area shows decreased
radiation from the specimen itself is cut density caused by paper between lead
almost in half by lead screens, screen and film. Electron shadow picture of
contributing to maximum clarity of detail paper structure has also been introduced.
in the radiograph; this advantage is
obtained even under conditions where the
lead screen makes an increase in exposure
necessary.
In radiography with gamma rays or
high voltage X-rays, films loaded in metal
cassettes without screens are likely to
record the effect of secondary electrons
generated in the lead covered back of the
cassette. These electrons, passing through
the felt pad on the cassette cover, produce
a mottled appearance because of the
structure of the felt. Films loaded in the
customary lead backed cardboard
exposure holder may also show the
structure of the paper that lies between
the lead and the film (Fig. 21). To avoid
these effects, film should be enclosed
between double lead screens, care being
taken to ensure good contact between
film and screens. Thus, lead foil screens
are essential in practically all radiography
with gamma rays or megavolt X-rays. If, FIGURE 22. Between film and lead foil
for any reason, screens cannot be used screens: (a) good contact gives sharp image;
with these radiations, a lightproof plastic (b) poor contact gives fuzzy image.
holder with no metal backing should be
used. (a)
Contact between the film and the lead
foil screens is essential to good
radiographic quality. Areas lacking contact
produce fuzzy images, as shown in
Fig. 22b.

FIGURE 20. Effects of kilovoltage on intensification properties


of lead screens.

Intensification
1.0
A
Density difference (relative unit)

0.8 B

0.6 (b)

0.4

C
0.2

–0.2

–0.4
Absorption 50 75 100 125 150 175 200 225

Kilovoltage

Legend
A. 0.05 mm (0.002 in.) lead oxide, 0.01 mm (0.0004 in.) lead equivalent.
B. 0.12 mm (0.005 in.).
C. 0.25 mm (0.01 in.) lead.

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Selection and Care of Lead steel wool. If this is done carefully, the
Screens shallow scratches left by the steel wool
will not produce dark lines in the
Lead foil for screens must be selected with radiograph.
extreme care. Commercially pure lead is Films could be fogged if left between
satisfactory. An alloy of 6 percent lead foil screens longer than is reasonably
antimony and 94 percent lead, being necessary, particularly under conditions of
harder and stiffer, has better resistance to high temperature and humidity. When
wear and abrasion. Tin coated lead foil screens have been freshly cleaned with an
should be avoided, because irregularities abrasive, this effect will be increased;
in the tin cause a variation in the prolonged contact between film and
intensifying factor of the screens, screens should be delayed for 24 h after
resulting in mottled radiographs. Minor cleaning.
blemishes do not affect the usefulness of
the screen but large blisters or cavities
should be avoided.
Most of the intensifying action of a Fluorescent Screens
lead foil screen is caused by the electrons
Certain chemicals fluoresce; that is, they
emitted under X-ray or gamma ray
have the ability to absorb X-rays and
excitation. Because electrons are readily
gamma rays and immediately emit light;
absorbed even in thin or light materials,
the intensity of the emitted light depends
small flakes of foreign material — for
on the intensity of the incident radiation.
example, dandruff or tobacco — will
These fluorescent materials can be used in
likewise produce light spots on the
radiography by first being finely
completed radiograph. For this same
powdered, mixed with a suitable binder,
reason, protective coatings on lead foil
then coated in a thin, smooth layer on a
screens should be removed before use.
special cardboard or plastic support.
The coating should not produce static
For the exposure, film is clamped
electricity when rubbed against or placed
firmly between a pair of these fluorescent
in contact with film (see Fig. 23).
screens. The photographic effect on the
Deep scratches on lead foil screens, on
film, then, is the sum of the effects of the
the other hand, will produce dark lines on
X-rays and of the light emitted by the
the radiograph (Fig. 24).
screens. For example, in the radiography
Surface contaminants may be removed
of 12.7 mm (0.5 in.) steel at 150 kV, a
from lead foil screens with a mild
factor as high as 125 has been observed.
household detergent or cleanser and a
soft, lint-free cloth. If more thorough
cleaning is necessary, screens may be very
gently rubbed with the finest grade of FIGURE 24. Number of electrons emitted (per surface unit of
lead) is essentially uniform. More electrons can reach film in
vicinity of scratch, resulting in dark line on radiograph. (For
FIGURE 23. Static marks result from poor illustrative clarity, electron paths have been shown as straight
film handling. Static marks may also be and parallel; actually, electrons are emitted diffusely.)
treelike or branching.

X-rays

Film

Electrons from lead foil

Scratch
Back lead screen

Principles of Film Radiography 161


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In radiography of 19.1 mm (0.75 in.) steel


at 180 kV, factors of several hundred have FIGURE 25. Light and ultraviolet radiation
been obtained experimentally. from typical fluorescent screen spreads
Under these latter conditions, the beyond X-ray beam that excites
intensification factor has about reached fluorescence.
its maximum and diminishes both for X-rays
lower voltage and thinner steel and for
higher voltage and thicker steel. Using
cobalt-60 gamma rays for very thick steel,
the factor may be 10 or less.

Limitations
Despite their great effect in reducing Fluorescent
layer
exposure time, fluorescent screens are not
widely used in industrial radiography.
This is mainly because they may give poor
definition, compared to a radiograph
made directly or with lead screens. The
poorer definition results from the
spreading of the light emitted from the Visible light
screens, as shown in Fig. 25. The light
from any particular portion of the screen
spreads out beyond the confines of the
X-ray beam that excited the fluorescence.
The other reason fluorescent screens
are seldom used in industrial radiography
is because they may produce screen mottle
on the finished radiograph. This mottle is
characteristic in appearance, very much
larger in scale and much softer in outline
than the graininess associated with the
film itself. Screen mottle is associated with
purely statistical variations in the
numbers of absorbed X-ray photons, from
one tiny area of the screen to the next.
Thus, screen mottle tends to become
greater as the kilovoltage of the radiation
increases. The higher the kilovoltage, the
more energetic, on the average, are the
X-ray photons. Therefore, on absorption
in the screen, a larger burst of light is
produced. The larger the bursts, the fewer
that are needed to produce a given
density and the greater is the purely
statistical variation in the number of
photons from one small area to the next.

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PART 4. Industrial X-Ray Films

Modern radiographic films for general this silver, suspended in the gelatin on
radiography consist of an emulsion both sides of the base, that constitutes the
(gelatin containing a radiation sensitive image (see Fig. 28).
silver halide compound) and a flexible,
transparent base that sometimes contains
a tint. Usually, the emulsion is coated on
both sides of the base in layers about FIGURE 27. Cross section of unprocessed
0.0125 mm (5 × 10–4 in.) thick (see Fig. 26 emulsion on one side of radiographic film
and 27). Putting emulsion on both sides (2000 diameters). Note greater quantity of
of the base doubles the amount of grains as compared to developed grains of
radiation sensitive silver compound and Fig. 28.
thus increases the speed. At the same
time, the emulsion layers are thin enough
so that developing, fixing and drying can
be accomplished in a reasonable time.
However, some films for radiography in
which the highest detail visibility is
required have emulsion on only one side
of the base.
When X-rays, gamma rays or light
strike the grains of the sensitive silver
compound in the emulsion, a change
takes place in the physical structure of the
grains. This change cannot be detected by
ordinary physical techniques. However,
when the exposed film is treated with a
chemical solution (called a developer), a
reaction takes place, causing the
formation of black, metallic silver. It is

FIGURE 26. Silver bromide grains of


radiographic film emulsion
(2500 diameters). Grains have been
dispersed to show shape and relative sizes FIGURE 28. Cross section showing
more clearly; in actual coating, crystals are distribution of developed grains in
much more closely packed. radiographic film emulsion exposed to give
moderate density.

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Although an image may be formed by steel up to 6.3 mm (0.25 in.) thick at 120
light and other forms of radiation, as well to 150 kV, film Y might be substituted for
as by gamma rays or X-rays, the properties film X. If short exposure times are
of the latter two are of distinct character essential, a faster film (or faster
and, for this reason, the sensitive combination of film and screen) can be
emulsion must be different from those used. For example, 38 mm (1.5 in.) steel
used in other types of photography. might be radiographed at 200 kV using
fluorescent screens with a film particularly
sensitive to blue light, rather than a direct
exposure film with lead screens.
Selection of Films for Figure 29 indicates the direction that
Industrial Radiography these substitutions take. The direct
exposure films may be used with or
As pointed out above, industrial without lead screens, depending on the
radiography now has many widely diverse kilovoltage and the thickness and shape
applications. There are many of the specimen.
considerations to be made in obtaining Fluorescent intensifying screens must
the best radiographic results, for example: be used in radiography requiring the
(1) the composition, shape and size of the highest possible photographic speed. The
part being examined — and, in some light emitted by the screens has a much
cases, its weight and location as well; greater photographic action than the
(2) the type of radiation used — whether X-rays either alone or combined with the
X-rays from an X-ray machine or gamma emission from lead screens. To secure
rays from a radioactive material; (3) the adequate exposure within a reasonable
kilovoltages available with the X-ray time, screen type radiographic films
equipment; (4) the intensity of the sandwiched between fluorescent
gamma radiation; (5) the kind of intensifying screens are often used in
information sought — whether it is radiography of steel in thicknesses greater
simply an overall inspection or the critical than about 50 mm (2 in.) at 250 kV and
examination of some especially important greater than 75 mm (3 in.) at 400 kV.
portion, characteristic or feature; and
(6) the resulting relative emphasis on
definition, contrast, density and time
required for proper exposure. All of these Photographic Density
factors are important in the determination
of the most effective combination of Photographic density refers to the
radiographic method and radiographic quantitative measure of film blackening
film. and is also called optical density and
The selection of a film for the sensitometric density. When no danger of
radiography of any particular part confusion exists, photographic density is
depends on the thickness and material of usually spoken of merely as density.
the specimen and on the voltage range of Density is defined by the equation:
the available X-ray machine. In addition,
the choice is affected by the relative I0
(13) D = log
importance of high radiographic quality It
or short exposure time. Thus, an attempt
must be made to balance these two where D = density; Io = light intensity
opposing factors. As a consequence, it is incident on film; and It = light intensity
not possible to present definite rules on transmitted.
the selection of a film. If high quality is Table 4 illustrates some relations
the deciding factor, a slower (less between transmittance, percent
sensitive) and finer grained film should be
substituted for a faster (more sensitive)
one — for instance, for the radiography of
TABLE 4. Transmittance, percent transmittance, opacity
and density relationships.
FIGURE 29. Choice of film depends on relative emphasis on Percent
high speed or high radiographic quality. Transmittance Transmittance Opacity Density
I t · I o–1 I t · I o–1 × 100 I o· I t–1 log I o· I t–1
Improving quality
1.00 100 1 0
0.50 50 2 0.3
Screen type film Fast Slow 0.25 25 4 0.6
with fluorescent direct exposure direct exposure
screens type film type film 0.10 10 10 1.0
0.01 1 100 2.0
0.001 0.1 1000 3.0
Increasing speed 0.0001 0.01 10 000 4.0

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transmittance, opacity and density. It of the chart. Wherever this density occurs
shows that an increase in density of 0.3 on the stepped wedge radiographs, there
reduces the light transmitted to half of its are corresponding values of thickness,
former value. In general, because density milliampere minutes and kilovoltage. It is
is a logarithm, a certain increase in density unlikely that many of the radiographs will
always corresponds to the same percentage contain a value of exactly 1.5 in density
decrease in transmittance. but the correct thickness for this density
can be found by interpolation between
steps. Thickness and milliampere minute
values are plotted for the different
Densitometers kilovoltages in the manner shown in
A densitometer is an optical instrument Fig. 30.
for measuring photographic densities. Another technique, requiring fewer
Film density to a required range is usually stepped wedge exposures but more
specified in radiographic procedures. The arithmetical manipulation, is to make one
densitometer must be available to see that step tablet exposure at each kilovoltage
specifications are met. The densitometer is and to measure the densities in the
essential for creating characteristic curves, processed stepped wedge radiographs. The
discussed elsewhere. exposure that would have given the
Different types of densitometers, both chosen density (in this case 1.5) under
visual and photoelectric, are available any particular thickness of the stepped
commercially. For purposes of practical wedge can then be determined from the
industrial radiography there is no great characteristic curve of the film used. The
premium on high accuracy in a values for thickness, kilovoltage and
densitometer. A much more important exposure are then plotted.
property is reliability, that the Note that thickness is on a linear scale
densitometer should reproduce readings and that milliampere minutes are on a
from day to day. nonlinear scale. The logarithmic scale is
not necessary but is very convenient
because it compresses an otherwise long
scale. A further advantage of the
X-Ray Exposure Charts logarithmic exposure scale is that it
An exposure chart is a graph showing the usually allows the location of the points
relation between material thickness,
kilovoltage and exposure (Figs. 30 to 32).
In its most common form, an exposure FIGURE 30. Typical X-ray exposure chart for steel may be
chart resembles Fig. 30. These graphs are applied to film X (see Fig. 33), with lead foil screens, at
adequate for determining exposures in the 1.5 film density and 1.0 m (40 in.) source-to-film distance.
radiography of uniform plates but they
serve only as rough guides for objects, 100
such as complicated castings, having wide 80
variations of thickness.
100 kV

1.8
V

kV

60
120 k

Exposure charts are usually available


kV

160
140

from manufacturers of X-ray equipment.


V

40
0k

Because, in general, such charts cannot be


18

used for different X-ray machines unless 1.5 30


kV

suitable correction factors are applied,


0
20

individual laboratories sometimes prepare 20


Exposure (mA·min)

their own. 1.2


Log exposure

kV

Preparing an Exposure Chart 10


0
22

A simple technique for preparing an 0.9 8


exposure chart is to make a series of 6
radiographs of a pile of metal plates (of
equal thickness but different lengths) 0.6 4
consisting of a number of steps. This step
tablet, or stepped wedge, is radiographed 3
at several different exposure times at each
of a number of kilovoltages. The exposed 0.3 2
films are all processed under conditions
identical to those that will later be used
for routine work. Each radiograph consists 0 1
of a series of photographic densities 0 6.4 12.7 19 25.4 31.8 38.1
corresponding to the X-ray intensities (0.25) (0.50) (0.75) (1.00) (1.25) (1.50)
transmitted by the different thicknesses of
metal. A certain density, for example 1.5, Equivalent thickness, mm (in.) of steel
is selected as the basis for the preparation

Principles of Film Radiography 165


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for any one kilovoltage to be well 2. A change in source-to-film distance


approximated by a straight line. may be compensated for by the
An exposure chart usually applies only inverse square law. Some exposure
to a single set of conditions, determined charts give exposures in terms of
by (1) the X-ray machine used; (2) a exposure factor rather than in terms of
certain source-to-film distance; (3) a milliampere minutes or milliampere
particular film type; (4) processing seconds. Charts of this type are readily
conditions used; (5) the film density on applied to any value of source-to-film
which the chart is based; (6) the type of distance.
screens (if any) that are used; and (7) the 3. A different type of film can be
material tested. corrected by comparing the difference
Only if the conditions used in making in the amount of exposure necessary
the radiograph agree in all particulars to give the same density on both films
with those used in preparation of the (from relative exposure charts such as
exposure chart can values of exposure be those described below). For example,
read directly from the chart. Any change to obtain a density of 1.5 using film Y,
requires the application of a correction 0.6 more log exposure is required than
factor. The correction factor applying to for film X (Fig. 33).
each of the above conditions is discussed This log exposure difference
separately. corresponds to an exposure factor of
1. It is sometimes difficult to find a 3.99. To obtain the same density on
correction factor to make an exposure film Y as on film X, multiply the
chart prepared for one X-ray machine original exposure by 3.99 to get the
applicable to another. Different X-ray new exposure. Conversely, if going
machines operating at the same from film Y to film X, divide the
nominal kilovoltage and original exposure by 3.99 to obtain the
milliamperage settings may give not new exposure.
only different intensities but also
different qualities (energies) of
radiation. FIGURE 32. Typical gamma ray exposure chart for
iridium-192, based upon the use of film X (see Fig. 33).

FIGURE 31. Typical X-ray exposure chart for 500 (10.0)


use when exposure and distance are held 400 (8.0)
constant and kilovoltage is varied to 300 (6.0)
conform to specimen thickness. Film X (see
D = 2.5
Fig. 33), exposed with lead foil screens to
200 (4.0)
Exposure factor, GBq·min·cm–2 (Ci·min·in.–2)

density of 1.5, source-to-film distance is D = 2.0


1.0 m (40 in.) and exposure is 50 mA·min. 150 (3.0) D = 1.5

220
100 (2.0)

200

50 (1.0)
180
40 (0.8)
Kilovoltage (kV)

160 30 (0.6)

140 20 (0.4)

15 (0.3)
120
10 (0.2)
100

80 5 (0.1)
0 25 50 75 100
60 (1) (2) (3) (4)
0 7 13 19 25 31 38
(0.25) (0.50) (0.75) (1.00) (1.25) (1.50) Steel thickness, mm (in.)

Steel thickness, mm (in.)

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These procedures can be used to These contain scales on which the various
change densities on a single film as factors of specimen thickness source
well. Simply find the log E difference strength and source-to-film distance can
needed to obtain the new density on be set and from which exposure time can
the film curve; read the corresponding be read directly.
exposure factor from the chart; then
multiply to increase density or divide
to decrease density.
4. A change in processing conditions Characteristic Curve
causes a change in effective film speed. The characteristic curve, sometimes
If the processing of the radiographs referred to as the sensitometric curve or the
differs from that used for the H and D curve (after Hurter and Driffield,
exposures from which the chart was who first used it in 1890), expresses the
made, the correction factor must be relation between the exposure applied to
found by experiment. a photographic material and the resulting
5. The chart gives exposures to produce a photographic density. The characteristic
certain density. If a different density is curves of three typical films, exposed
required, the correction factor may be between lead foil screens to X-rays, are
calculated from the film’s given in Fig. 33. Such curves are obtained
characteristic curve. by giving a film a series of known
6. If the type of screen is changed — for exposures, determining the densities
example, from lead foil to fluorescent produced by these exposures and then
— it is easier and more accurate to plotting density against the logarithm of
make a new exposure chart than to relative exposure.
determine correction factors Relative exposure is used because there
7. Material can be changed by using the are no convenient units, suitable to all
material equivalence table (Table 2). kilovoltages and scattering conditions, in
In some radiographic operations, the which to express radiographic exposures.
exposure time and the source-to-film The exposures given a film are expressed
distance are set by economic in terms of some particular exposure,
considerations or on the basis of previous giving a relative scale. In practical
experience and test radiographs. The tube radiography, this lack of units for X-ray
current is, of course, limited by the design intensity or quantity is no hindrance, as
of the tube. The specimen and the will be seen below. The logarithm of the
kilovoltage are variables. When these
conditions exist, the exposure chart may
take a simplified form as shown in Fig. 31,
which allows the kilovoltage for any FIGURE 33. Characteristic curves of three typical X-ray films,
particular specimen thickness to be exposed between lead foil screens.
chosen. Such a chart will be particularly
useful when uniform sections must be 4.0
radiographed in large numbers by
relatively untrained persons. This type of
exposure chart may be derived from a 3.5
chart similar to Fig. 30 by following the
horizontal line corresponding to the
chosen milliampere minute value and 3.0
noting the thickness corresponding to this
exposure for each kilovoltage. These
2.5
thicknesses are then plotted against
kilovoltage.
Density D

2.0

Gamma Ray Exposure


1.5
Charts
A typical gamma ray exposure chart is
shown in Fig. 32. It is somewhat similar 1.0
to Fig. 30; however, with gamma rays, Film Z Film X
Film Y
there is no variable factor corresponding
to the kilovoltage. Therefore, a gamma ray 0.5
exposure chart contains one line, or
several parallel lines, each of which
corresponds to a particular film type, film 0
0 0.5 1.0 1.5 2.0 2.5 3.0
density or source-to-film distance. Gamma
ray exposure guides are also available in Log relative exposure
the form of linear or circular slide rules.

Principles of Film Radiography 167


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relative exposure, rather than the relative under actual radiographic conditions
exposure itself, has a number of should be used in solving practical
advantages. It compresses an otherwise problems. However, it is not always
long scale. Furthermore, in radiography, possible to produce characteristic curves
ratios of exposures or intensities are in a radiography department and curves
usually more significant than the prepared elsewhere must be used. Such
exposures of the intensities themselves. curves prove adequate for many purposes
Pairs of exposures having the same ratio although it must be remembered that the
will be separated by the same interval on shape of the characteristic curve and the
the log relative exposure scale, no matter speed of a film relative to that of another
what their absolute value may be. depend strongly on developing
Consider the pairs of exposures in Table 5. conditions. The accuracy attained when
As can be seen in Fig. 33, the slope (or using ready made characteristic curves is
steepness) of the characteristic curves is governed largely by the similarity between
continuously changing throughout the the developing conditions used in
length of the curves. For example, two producing the characteristic curves and
slightly different thicknesses in the object those for the films whose densities are to
radiographed transmit slightly different be evaluated.
exposures to the film. These two Quantitative use of characteristic
exposures have a certain small log E curves are worked out in Figs. 34 and 35.
interval between them; that is, they have Note that D is used for density and log E
a certain ratio. The difference in the for logarithm of relative exposure.
densities corresponding to the two In the first example (Fig. 34), suppose a
exposures depends on just where on the radiograph made of film Z with an
characteristic curve they fall; the steeper exposure of 12 mA·min has a density of
the slope of the curve, the greater is this 0.8 in the region of maximum interest. It
density difference. For example, the curve is desired to increase the density to 2.0 for
of film Z (Fig. 33) is steepest in its middle the sake of the increased contrast there
portion. This means that a certain log E available.
interval in the middle of the curve
corresponds to a greater density difference
than the same log E interval at either end
of the curve. In other words, the film FIGURE 34. Characteristic curve of film Z (see Fig. 33).
contrast is greatest where the slope of the 4.0
characteristic curve is greatest. For film Z,
as has been pointed out, the region of
greatest slope is in the central part of the 3.5
curve. For films X and Y, however, the
slope — and hence the film contrast —
continuously increases throughout the 3.0
useful density range. The curves of most Film z
industrial radiographic films are similar to
those of films X and Y. 2.5
Density D

Use of Characteristic Curve


2.0
The characteristic curve can be used in
solving quantitative problems arising in
radiography, in the preparation of 1.5 3
technique charts and in radiographic
research. Characteristic curves made
1.0 2

TABLE 5. Equivalent exposure ratios. 0.5 1

Log Interval in
Relative Relative Log Relative
Exposure Exposure Exposure 0
0 0.5 1.0 1.5 2.0 2.5 3.0
1 0.0
5 0.70 } 0.70 Log relative exposure

2 0.30
10 1.00 } 0.70 Legend
1. Log E = 1.62 at D = 2.0.
2. Log E = 1.00 at D = 0.8.
30 1.48
150 2.18 } 0.70 3. Difference in log E is 0.62.

168 Radiographic Testing


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1. Log E at D = 2.0 is 1.62.


2. Log E at D = 0.8 is 1.00.
3. The difference in log E is 0.62. The
antilogarithm of this difference is 4.2.
Therefore, the original exposure is
multiplied by 4.2 giving 50 mA·min to
produce a density of 2.0.
In the second example (see Fig. 35),
film X has higher contrast than film Z at
D = 2.0 and also a finer grain. Suppose
that, for these reasons, it is desired to
make the radiograph on film X with a
density of 2.0 in the same region of
maximum interest.
1. Log E at D = 2.0 for film X is 1.91.
2. Log E at D = 2.0 for film Z is 1.62.
3. The difference in log E is 0.29. The
antilogarithm of this difference
is 1.95.
Therefore, the exposure for D = 2.0 on
film Z is multiplied by 1.95, giving
97.5 mA·min for a density of 2.0 on
film X.

FIGURE 35. Characteristic curves of two X-ray films exposed


with lead foil screens.
4.0

3.5

3.0

2.5
Film Z Film X
Density D

2.0

1.5
2

1.0
1

0.5

0
0 0.5 1.0 1.5 2.0 2.5 3.0

Log relative exposure

Legend
1. Log E = 1.91 at D = 2.0.
2. Log E = 1.62 at D = 2.0.
3. Difference in Log E is 0.29.

Principles of Film Radiography 169


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PART 5. Radiographic Image Quality and Detail


Visibility

Film contrast refers to the slope


Controlling Factors (steepness) of the characteristic curve of
the film. It depends on the type of film,
Because the purpose of most radiographic on the processing it receives and density.
testing is to examine specimens for It also depends on whether the film’s
heterogeneity, a knowledge of the factors exposure is direct, with lead screens or
affecting the visibility of detail in the with fluorescent screens. Film contrast is
finished radiograph is essential. Table 6 independent, for most practical purposes,
shows the relationships of the various of the wavelengths and distribution of the
factors influencing image quality and radiation reaching the film and hence is
radiographic sensitivity; following are a independent of subject contrast.
few important definitions. The steepness of the characteristic
Radiographic sensitivity is a general or curve is sometimes referred to as gamma
qualitative term referring to the size of the (Γ). Higher gamma films have more
smallest detail that can be seen in a contrast.
radiograph or to the ease with which the Definition refers to the sharpness of
images of small details can be detected. outline in the image. It depends on the
Phrased differently, it is a reference to the types of screens and film used, the
amount of information in the radiograph. radiation energy (wavelengths) and the
Note that radiographic sensitivity depends geometry of the radiographic setup.
on the combined effects of two
independent sets of factors: radiographic
contrast (the density difference between a
small detail and its surroundings) and Subject Contrast
definition (the abruptness and the
Subject contrast decreases as the
smoothness of the density transition). See
kilovoltage is increased. The decreasing
Fig. 36.
slope (steepness) of the lines of the
Radiographic contrast is the difference in
exposure chart (Fig. 30) as kilovoltage
density between two areas of a
increases illustrates the reduction of
radiograph. It depends on both subject
subject contrast as the radiation becomes
contrast and film contrast.
more penetrating. For example, consider a
Subject contrast is the ratio of X-ray or
steel part containing two thicknesses, 19
gamma ray intensities transmitted by two
and 25 mm (0.75 and 1 in.), which is
selected portions of a specimen. Subject
radiographed first at 160 kV and then at
contrast depends on the nature of the
200 kV.
specimen, on the energy (spectral
In Table 7, column 3 shows the
composition, hardness or wavelengths) of
exposure in milliampere minutes required
the radiation used and on the intensity
to reach a density of 1.5 through each
and distribution of the scattered radiation
thickness at each kilovoltage. These data
but is independent of time, milliamperage
are from the exposure chart in Fig. 30. It
or source strength, distance and the
is apparent that the milliampere minutes
characteristics or treatment of the film
required to produce a given density at any
(Fig. 11).

TABLE 6. Factors controlling radiographic sensitivity.


Radiographic Contrast
_______________________________________________________________________ Radiographic Definition
___________________________________________________
Subject Contrast Film Contrast Geometrical Factors Graininess Factors
Affected by Affected by Affected by Affected by

Specimen thickness variations Type of film Focal spot size Type of film
Radiation quality Development time, temperature and agitation Distance from focal point to film Type of screen
Scattered radiation Density Distance from specimen to film Radiation quality
Activity of the developer Abrupt specimen thickness variations Development
Contact of screen to film

170 Radiographic Testing


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kilovoltage are inversely proportional to


FIGURE 36. Radiographic definition: the corresponding X-ray intensities
(a) advantage of higher contrast is offset by passing through the different sections of
poor definition; (b) despite lower the specimen. Column 4 gives these
contrast better rendition of detail is obtained relative intensities for each kilovoltage.
by improved definition. Column 5 gives the ratio of these
intensities for each kilovoltage.
(a) Column 5 shows that, at 160 kV, the
intensity of the X-rays passing through
the 19 mm (0.75 in.) section is 3.8 times
greater than that passing through the
25 mm (1 in.) section. At 200 kV, the
radiation through the thinner portion is
only 2.5 times that through the thicker.
Thus, as the kilovoltage increases, the
ratio of X-ray transmission of the two
thicknesses decreases, indicating a lower
subject contrast.

Film Contrast
The dependence of film contrast on
density must be kept in mind when
considering problems of radiographic
sensitivity. In general, the contrast of
radiographic films, except those designed
for use with fluorescent screens, increases
continuously with density in the usable
(b) density range. Therefore, for films that
exhibit this continuous increase in
contrast, the best density to use is the
highest that can be conveniently viewed
with the illuminators available. Adjustable
high intensity illuminators are
commercially available and greatly
increase the maximum density that can
be viewed.
High densities have the further
advantage of increasing the range of
radiation intensities that can be usefully
recorded on a single film. In
X-radiography, this in turn permits use of
the lower kilovoltage, resulting in
increased subject contrast and
radiographic sensitivity.
The slope of screen film contrast
becomes steep at densities greater than
2.0. Therefore, other things being equal,
the greatest radiographic sensitivity will
be obtained when the exposure is
adjusted to give this density.

TABLE 7. Exposure of steel part containing two Film Graininess and Screen
thicknesses. Mottle
Exposure to The image on an radiographic film is
Voltage Thickness Give D = 1.5 Relative Ratio of formed by countless minute silver grains,
(kV) mm (in.) (mA·min) Intensity Intensities the individual particles being so small
that they are visible only under a

}
160 20 (0.75) 18.5 3.8 microscope. However, these small particles
3.8 are grouped together in relatively large
25 (1.0) 70.0 1.0
masses visible to the naked eye or with a

}
200 20 (0.75) 4.9 14.3 magnification of only a few diameters.
2.5 These masses result in a visual impression
25 (1.0) 11.0 5.8
called graininess.

Principles of Film Radiography 171


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All films exhibit graininess to a greater quality indicator, its dimensions and how
or lesser degree. In general, the slower it is to be employed. Even if image quality
films have lower graininess. Thus, film Y indicators are not specified, their use is
(Fig. 33) would have a lower graininess advisable because they provide an
than film X. effective check on the quality of the
The graininess of all films increases as radiographic inspection and evidence that
the radiation energy increases, although radiographic sensitivity is achieved.
the rate of increase may be different for
different films. The graininess of the Hole Image Quality Indicators
images produced at high kilovoltages
makes the slow, inherently fine grain A common image quality indicator in the
films especially useful in the megavolt United States consists of a small
and multimegavolt range. When sufficient rectangular piece of metal, containing
exposure can be given, fine grain films are several (usually three) holes, the diameter
also useful with gamma rays. of which are related to the thickness of
Lead screens have no significant effect the image quality indicator (Fig. 37).
on film graininess. However, graininess is The ASTM International plaque type
affected by processing conditions, being image quality indicator4 contains three
directly related to the degree of holes of diameters T, 2T, and 4T, where T
development. For instance, if is the thickness of the image quality
development time is increased for the indicator. Because of the practical
purpose of increasing film speed, the difficulties in drilling tiny holes in thin
graininess of the resulting image is materials, the minimum diameters of
likewise increased and vice versa. these three holes are 0.25, 0.50 and
However, adjustments in development 1.00 mm (0.01, 0.02, and 0.04 in.),
technique made to compensate for respectively. Thick image quality
changes in temperature or activity of a indicators of the hole type would be very
developer will have little effect on large because of the diameter of the 4T
graininess, because they are made to hole. Therefore, image quality indicators
achieve the same degree of development more than 0.46 mm (0.180 in.) thick are
as would be obtained in the fresh in the form of disks, the diameters of
developer at a standard processing which are four times the thickness (4T)
temperature. and which contain only two holes, of
Another source of irregular density in diameters T and 2T. Each image quality
uniformly exposed areas is the screen indicator is identified by a lead number
mottle encountered in radiography with showing the thickness in thousandths of
fluorescent screens. The screen mottle an inch.
increases markedly as hardness of the The ASTM International image quality
radiation increases. This mottle limits the indicator permits the specification of a
use of fluorescent screens at high voltage number of levels of radiographic
and with gamma rays. Yet another source sensitivity, depending on the
of mottle occurs when some films are requirements of the job. For example, the
exposed to megavolt radiation. This is specifications may call for a radiographic
most noticeable in radiography of quality level of 2-2T. The first symbol, 2,
materials of uniform thickness. indicates that the image quality indicator
shall be 2 percent of the thickness of the
specimen; the second symbol (2T)
indicates that the hole having a diameter
Image Quality Indicators twice the image quality indicator
A standard test piece is usually included thickness shall be visible on the finished
in every radiograph as a check on the radiograph. The quality level 2-2T is
adequacy of the radiographic method. probably the one most commonly
The test piece is commonly referred to as specified for routine radiography.
a penetrameter or an image quality indicator However, critical components may require
(IQI). The image quality indicator is a more rigid standards and require a level of
simple geometric form made of the same 1-2T or 1-1T. On the other hand, the
material as, or a material similar to, the radiography of less critical specimens may
specimen being radiographed. It contains be satisfactory if a quality level of 2-4T or
some small structures (holes, wires and 4-4T is achieved. The more critical the
others), the dimensions of which bear radiographic examination — that is, the
some numerical relation to the thickness higher the level of radiographic sensitivity
of the part being tested. The image of the required — the lower the numerical
image quality indicator on the radiograph designation for the quality level.
is permanent evidence that the Another ASTM International image
radiographic examination was conducted quality indicator design required by some
under proper conditions. specifications is the wire type that consists
Codes or agreements between customer of sets of wires arranged in order of
and vendor may specify the type of image increasing diameter (Fig. 38).

172 Radiographic Testing


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FIGURE 37. Image quality indicator of ASTM International, according to ASTM Standard
E 1025: (a) design for image quality indicator type numbers 5 to 20, with tolerances of
±0.0005; (b) design for image quality indicator type numbers 21 to 59 with tolerances of
±0.0025 in. and for image quality indicator type numbers 60 to 179, with tolerance of
±0.005 in.; (c) design for image quality indicator type numbers over 180, with tolerances of
±0.010 in. (Except for relative thickness T, all measurements in these diagrams are in inches;
1.00 in. = 25.4 mm.)

(a)
4 T diameter

T diameter
2 T diameter

Identification
number
0.5 in.

0.25 in. 0.25 in. T


0.438 in.
0.75 in.
1.5 in.

(b) 4 T diameter
Identification
number T diameter

2 T diameter

1.0 in.

0.375 in. 0.375 in. T


0.75 in.
1.375 in.
2.25 in.

(c)

1.33 T

2T

4T

0.83 T

Principles of Film Radiography 173


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All sections of the ASME Boiler and side image quality indicator normally
Pressure Vessel Code require an image required.
quality indicator identical to the ASTM When such a specification is not made,
plaque or wire type image quality the required film side image quality
indicator.5 indicator may be found experimentally. In
the example above, a short section of tube
Equivalent Image Quality of the same dimensions and materials as
the item under test would be used in the
Indicator Sensitivity experiment. The required image quality
Ideally, the image quality indicator should indicator would be placed on the source
be made of the same material as the side and a range of image quality
specimen. However, this is sometimes indicators on the film side. If the source
impossible because of practical or side image quality indicator indicated that
economic difficulties. In such cases, the the required radiographic sensitivity was
image quality indicator may be made of a being achieved, the image of the smallest
radiographically similar material — that
is, a material having the same
radiographic absorption as the specimen
but which is better suited to the making FIGURE 38. Examples of wire type image quality indicators:
of image quality indicators. Tables of (a) ASTM Standard E 747 (set B, Alternate 2); (b) Deutsche
radiographically equivalent materials have Industrie Norm 54109, German standard image quality
been published, grouping materials with indicator.
similar radiographic absorptions. In
(a)
addition, an image quality indicator made
of a particular material may be used in the 6.35 mm (0.25 in.)
radiography of materials having greater minimum lead letters
radiographic absorption. In such a case, and numbers
Largest
there is a certain penalty on radiographic wire number
technicians because they are setting more
rigid radiographic quality standards for
Encapsulated
themselves than those which are actually between clear vinyl
required. This penalty is often outweighed plastic of 1.52 mm
by avoiding the problems of obtaining (0.06 in.)
Material maximum
image quality indicators for an unusual grade thickness
material. number
In some cases the materials involved
do not appear in published tabulations. Set
Under these circumstances the identification Length minimum
comparative radiographic absorption of number 25.4 mm (1.0 in.)
two materials may be determined for sets A and B
experimentally. A block of the material
under test and a block of the material
proposed for image quality indicators,
equal in thickness to the part being
examined, can be radiographed side by 6 wires
side on the same film with the technique equally 5.08 mm (0.200 in.) (minimum
to be used in practice. If the film density spaced distance between axis of wires is
under the proposed image quality not less than 3 times wire
diameter and not more than
indicator material is equal to or greater 5.08 mm [0.200 in.])
than the film density under the specimen
material, that proposed material is (b)
suitable for fabrication of image quality
indicators.
In practically all cases, the image
quality indicator is placed on the source
side of the specimen, in the least
advantageous geometric position. In some
instances, however, this location for the
image quality indicator is not feasible. An
example would be the radiography of a
circumferential weld in a long tubular
structure, using a source position within
the tube and film on the outer surface. In
such a case film side image quality
indicator must be used. Some codes
specify the film side image quality
indicator that is equivalent to the source

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visible hole or wire size in the film side the wire image quality indicator is only
image quality indicators would be used to made from materials that can be formed
determine the image quality indicator and into wires. A quality level of 2-2T may be
the hole or wire size to be used on the specified for the radiography of, for
production radiographs. example, commercially pure aluminum
Although the smallest visible hole and 2024 aluminum alloy, even though
criterion is the best one in most cases for these have appreciably different
plaque image quality indicators, in some compositions and radiation absorptions.
cases the best criterion is the smallest The hole image quality indicator would,
visible hole in the thinnest image quality in each case, be made of the appropriate
indicator. In rare cases neither of these material. To achieve the same quality of
rules of thumb is correct. Therefore, for radiographic inspection for equal
critical applications, the best criterion for thicknesses of these two materials, it
equivalent sensitivity should be would be necessary to specify different
determined by calculations based on the wire diameters — that for 2024 alloy
visible features of the film side image would probably have to be determined by
quality indicators and using the equations experiment.
given in the appendix to ASTM E 1025.4
Sometimes the shape of the part being Special Image Quality Indicators
examined precludes placing the image
quality indicator on the part. When this Special image quality indicators have been
occurs, the image quality indicator may designed for certain classes of
be placed on a block of radiographically radiographic testing. An example is the
similar material of the same thickness as radiography of electronic components in
the specimen. The block and the image which some of the significant factors are
quality indicator should be placed as close the continuity of fine wires or the
as possible to the specimen. presence of tiny balls of solder. Special
image quality indicators have been
designed consisting of fine wires and
Wire Image Quality Indicators small metallic spheres within a plastic
A number of wire image quality indicator block.9
designs are in use. The ASTM E 747 image The block is covered on top and
quality indicator6 and the European wire bottom with steel about as thick as the
image quality indicator7,8 (Fig. 38) are case of the electronic component.
widely used. These consist of a number of
wires of various diameters sealed in a Image Quality Indicators and
plastic envelope that carries the necessary
identification symbols. The image quality Visibility of Discontinuities
is indicated by the thinnest wire visible It should be remembered that even if a
on the radiograph. The system is such certain hole in an image quality indicator
that only three image quality indicators, is visible on the radiograph, a cavity of
each containing seven wires, can cover a the same diameter and thickness may not
very wide range of specimen thicknesses. be visible. The image quality indicator
Sets of Deutsche Industrie Norm image holes, having sharp boundaries, result in
quality indicators are available in abrupt, though small, changes in metal
aluminum, copper and steel whereas thickness whereas a natural cavity having
ASTM image quality indicators are more or less rounded sides causes a
available in three light metal and five gradual change. Therefore, the image of
heavy metal groups. the image quality indicator hole is sharper
and more easily seen in the radiograph
Comparison of Image Quality than is the image of the cavity.
Similarly, a fine crack may be of
Indicator Designs considerable extent but if the X-rays or
The hole type image quality indicator is, in gamma rays pass from source to film in a
a sense, a go/no-go gage; that is, it indicates direction other than parallel to the plane
whether or not a specified quality level has of the crack, its image on the film may
been attained but, in most cases, does not not be visible because of the very gradual
indicate whether requirements have been or small transition in photographic
exceeded or by how much. The wire image density. Thus, an image quality indicator
quality indicator on the other hand is a is used to indicate the quality of the
series of image quality indicators in a radiographic method and not to measure
single unit. As such, they have the the size of flaw which can be shown.
advantage that the radiographic quality In the case of a wire image quality
level achieved can often be read directly indicator, the visibility of a wire of a
from the processed radiograph. certain diameter does not ensure that a
The hole image quality indicator can discontinuity of the same cross section
be made of any material that can be will be visible. The human eye perceives
formed into thin sheets and drilled but much more readily a long boundary than

Principles of Film Radiography 175


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it does a short one, even if the density


difference and the sharpness of the image
are the same. However, the equivalency
between the hole and wire ASTM
International image quality indicators was
developed on the basis of empirical data
as well as theoretical numbers.

Viewing and Interpreting


Radiographs
The viewing of the finished radiograph is
discussed elsewhere in this volume.

176 Radiographic Testing


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PART 6. Film Handling and Storage

in the darkroom with black pressure


Film Handling sensitive tape. The tape should extend
beyond the edges of the strip 7 to 13 mm
Radiographic film should always be (0.25 to 0.5 in.) to provide a positive light
handled carefully to avoid physical tight seal.
strains, such as pressure, creasing,
buckling, friction and others. The normal
pressure applied in a cassette to provide
good contacts is not enough to damage Identifying Radiographs
the film. However, when films are loaded
Because of their high absorption, lead
in semiflexible holders and external
numbers or letters affixed to the film
clamping devices are used, care should be
holder or test object furnish a simple
taken to ensure that this pressure is
means of identifying radiographs. They
uniform. If a film holder bears against a
may also be used as reference marks to
few high spots, such as those that occur
determine the location of discontinuities
on an unground weld, the pressure may
within the specimen. Such markers can be
be great enough to produce desensitized
conveniently fastened to the film holder
areas in the radiograph. Precaution is
or object with adhesive tape. A code can
particularly important when using
be devised to minimize the amount of
envelope packed films.
lettering needed. Lead letters are
Crimp marks or marks resulting from
commercially available in a variety of sizes
contact with fingers that are moist or
and styles. The thickness of the chosen
contaminated with processing chemicals
letters should be great enough so that
can be avoided if large films are grasped
their image is clearly visible on exposures
by the edges and allowed to hang free. A
with the most penetrating radiation
convenient supply of clean towels is an
routinely used. Under some circumstances
incentive to dry the hands often and well.
it may be necessary to put the lead letters
Envelope packed films avoid these
on a radiation absorbing block so that
problems until the envelope is opened for
their image will not be burned out. The
processing. Thereafter, of course, the usual
block should be considerably larger than
care must be taken.
the legend itself.
Another important precaution is to
Flash box identification should be
avoid withdrawing film rapidly from
included where a corner of a radiograph is
cartons, exposure holders or cassettes.
blocked with lead to minimize exposure.
Such care will materially help to eliminate
The unexposed corner is flashed with
objectionable circular or treelike black
light transmitted through typed or hand
markings in the radiograph, the results of
written information exposed onto the
static electric discharges.
film.
The interleaving paper must be
removed before the film is loaded
between either lead or fluorescent screens.
When using exposure holders without Shipping of Unprocessed
screens, the paper should be left on the
film for the added protection that it Films
provides. At high voltage, direct exposure If unprocessed film is to be shipped, the
techniques are subject to the problems package should be carefully and
mentioned earlier: electrons emitted by conspicuously labeled, indicating the
the lead backing of the cassette or contents, so that the package may be
exposure holder may reach the film segregated from any radioactive materials,
through the intervening paper or felt and high heat or pressure. It should further be
record an image of this material on the noted that customs inspection of
film. This effect is magnified by lead or shipments crossing international
fluorescent screens. In the radiography of boundaries sometimes includes
light metals, direct exposure techniques fluoroscopic inspection. To avoid damage
are the rule and the paper folder should from this cause, packages, personnel
be left on the interleaved film when baggage and the like containing
loading it in the exposure holder. unprocessed film should be plainly
Ends of a length of roll film factory marked and the attention of inspectors
packed in a paper sleeve should be sealed drawn to their sensitive contents.

Principles of Film Radiography 177


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fixer) permissible for storage of


Storage of Unprocessed radiographs.
Although many factors affect the
Film storage life of radiographs, one of the
most important is the residual thiosulfate
left in the radiograph after processing and
X-Ray Film Storage drying. Determined by the methylene
With X-rays generated up to 200 kV, it is blue test, the maximum level is 2 mg·cm–2
feasible to use storage compartments lined on each side of coarse grain radiographic
with a sufficient thickness of lead to films. For short term storage
protect the film. At higher kilovoltages, requirements, the residual thiosulfate
protection becomes increasingly difficult; content can be at a higher level but this
film should be protected not only by the level is not specified by the American
radiation barrier for protection of National Standards Institute.
personnel but also by increased distance Washing of the film after development
from the source. and fixing, therefore, is very important.
At 100 kV, a 3 mm (0.125 in.) thickness The methylene blue test and silver
of lead should normally be adequate to densitometric test are laboratory
protect film stored in a room adjacent to procedures performed on clear areas of
the X-ray room if the film is not in the the processed film.
line of the direct beam. At 200 kV, the Temperature and humidity should be
lead thickness should be increased to carefully controlled. Radiographic film
6.4 mm (0.25 in.). should be stored with precautions
With megavolt X-rays, films should be specified in ASTM E 1254.10
stored beyond the concrete or other
protective wall at a distance at least five
times farther from the X-ray tube than the
Storage Suggestions
area occupied by personnel. The storage Regardless of the length of time a
period should not exceed the times radiograph is to be kept, these suggestions
recommended by the manufacturer. should be followed to provide for
These rules of thumb may be ignored if maximum stability of the radiographic
suitable radiation surveys indicate image.
radiation levels low enough to avoid 1. Avoid storage in the presence of
fogging during the maximum time period chemical fumes.
that the film will be stored. 2. Avoid short term cycling of
temperature and humidity.
Storage near Gamma Rays 3. Place each radiograph in its own
folder to prevent possible chemical
When radioactive material is not in use,
contamination by the glue used in
the shielding container in which it is
making the storage envelope (negative
stored helps provide protection for film.
preserver). Several radiographs may be
In many cases, however, the container for
stored in a single storage envelope if
a gamma ray source will not provide
each is in its own interleaving folder.
satisfactory protection to stored
4. Never store unprotected radiographs
radiographic film. In such cases, the
in bright light or sunlight.
emitter and stored film should be
5. Avoid pressure damage caused by
separated by a sufficient distance to
stacking a large number of radiographs
prevent fogging.
horizontally in a single pile or by
forcing more radiographs than can
Heat, Humidity and Fumes comfortably fit into a single file
The effects of heat, humidity and fumes drawer or shelf.
on stored film are discussed elsewhere.2 Radiographic film offers a means of
precise discontinuity detection and
documentation. Despite the introduction
of digital means of image capture, display
Storage of Exposed and and storage, film radiography will
Processed Film continue to be an important part of
nondestructive testing well into the
Archival storage is a term commonly used
twenty first century.
to describe the keeping quality of
radiographic film. It has been defined by
the American National Standards Institute
(ANSI) as those storage conditions suitable Microfilm
for the preservation of photographic film
having permanent value. The American Radiographic film images can be copied to
National Standards Institute does not microfilm and microfiche for storage. A
define archival storage in years but in microfiche the size of a postcard can store
terms of the thiosulfate content (residual more than a hundred radiographic

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images. Like film negatives, microfilm and


microfiche require climate control to
prevent degradation of the medium when
stored for years.
In the twenty-first century,
microfilming services offer image
digitization and will provide the images
on compact disks or digital video disks.
Film digitization is discussed below.

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PART 7. Film Digitization

Film digitization is the conversion of onto the much smaller charge coupled
existing radiographic film images to a element. A narrow line of diffuse light is
digital format for electronic image passed through the film and the
analysis, management, transmission and transmitted light is focused onto the
storage. Film digitization also permits charge coupled device array, one line at a
disposal of film that would degrade over time. Once one line of data is collected, a
time. second line is then scanned.
In film digitization, film densities are The total density range of charge
converted into digital values by measuring coupled devices can be affected if, when
light transmitted through the film and there is a rapid and drastic change in light
assigning each measurement a digital level, the charge coupled device
value and a particular location. Three momentarily becomes saturated. The
primary parameters affect the resulting image may be corrected by changing the
image quality of film digitization: density sampling time (integration period). At
range, density resolution and spatial high light levels, the integration period is
resolution (pixel size). reduced to avoid saturation of the charge
Optical density (OD) is a logarithmic coupled device whereas at low light levels,
function. This means that at optical the integration period is increased to
density 0, 100 percent of the incident achieve an adequate ratio of signal to
photons are transmitted through the film; noise. To obtain optical density dynamic
at 1.0 optical density, only 10 percent ranges up to five, multiple scans may be
make it through; at 2.0 optical density, performed at varying charge coupled
only 1 percent; and at 3.0 optical density, device integration periods and scan
only 0.1 percent. It is difficult to measure speeds.
higher densities with the same accuracy The density resolution of charge
and precision as lower densities. coupled device digitizers is determined by
There are two basic methods of the conversion of the logarithmic density
digitizing film. The first method makes scale to a linear voltage scale. For
the measurement using a diffuse light example, at an optical density of zero,
source and a charge coupled device (CCD) maximum light passes through the film,
whereas the second uses a combination of so the charge coupled device element
a laser and a photomultiplier tube produces the maximum voltage. Because
(PMT).11,12 optical density is a logarithmic function,
only 10 percent of the light transmitted at
an optical density of 0 will be detected at
an optical density of 1. If the charge
Charge Coupled Device coupled device’s maximum voltage is
Film Digitization Systems calibrated to be 10 V, then the voltage
output at an optical density of 1 is 1.0 V,
A charge coupled device film digitizer at 2 it is 0.1 V, at 3 it is 0.01 V and at 4 it
illuminates the full width of the film with is 0.001 V. Therefore, if the charge
a diffuse light source and then uses a lens coupled device output of 10 V is digitized
system to focus the light down to the size at 12 bits or 4096 density levels, then an
of the charge coupled device elements. optical density from 0 to 1 will produce
The charge coupled device is a silicon an output of 9 V, which equates to
semiconductor device consisting of a large 3686 density levels (90 percent of 4096).
number of gridlike elements sensitive to The output of densities from 1 to 2 will
light. When light energy impinges on the equate to 369 levels; densities from 2 to 3,
charge coupled device elements, the to 37 levels; and densities from 3 to 4,
photons generate a charge within each 4 levels. While this results in a nonlinear
element. Periodically, the element is density resolution, it is similar to the
discharged and the amplitude of the original image and as a result is adequate
charge is measured. In this way, light for many purposes. It is important that
amplitude can be converted to a the application and image analysis
proportionate electrical signal related to requirements are thoroughly understood
the density at any given point. before a particular digitizer is used.
In film digitization systems, a linear Another aspect of charge coupled
array of charge coupled device elements is devices is spatial resolution. The elements
used with optics to focus the film image

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can be arrayed along one or two depend on overall laser beam quality,
dimensions. The array’s resolution is detector noise and electronic noise.
sometimes given as the element size It is important that the application and
because all charge coupled device chips image analysis requirements of a
have a large number of elements (for particular digitizer are thoroughly
example, 4000 or 6000) that in theory can understood before it is used. There are
be digitized into a like number of pixels. several ways to determine experimentally
For example, the 1 cm2 chip in a video the performance of a film digitizer. One
camera is said to have a resolution of method is to scan a modulation transfer
about 20 µm. Once the various focusing function (MTF) pattern to validate
lens aberrations are coupled together, the performance. Another, simpler method, is
true resolving capability of the charge to place a strip of cellophane tape over
coupled device chip is low. A home video the image of a step wedge. This
camera is surely not able to discern translucent tape will produce a density
objects 20 µm apart. difference of about 0.03 optical density.
Therefore, it is important to The idea here is to demonstrate (1) the
differentiate between the chip dynamic range of the system (when the
specifications versus those of the imaging steps begin to be difficult to differentiate)
system. The resolution of the imaging and (2) the density resolution (at what
system depends in part on the quality of density the tape can no longer be seen).
the focusing optics and in part on the
cross talk between charge coupled
elements (as when one photon activates
more than one element). Other Considerations
Beyond the technical issues of the
scanning scheme, other issues are related
to image size relative to the display and
Laser Film Digitization storage medium. All the information may
Systems be captured in memory, but both the
Laser scanners use a nonimaging processor size and monitor size limit what
photomultiplier tube to detect light can be worked with or displayed.
transmitted through the film. The laser For example, let us assume that each
beam is a focused beam of coherent light pixel contains 12 bits of grayscale
of known value and is transmitted information plus 4 bits of header
through the film at one discreet point. information. This equates to 16 bits or
The transmitted light is then detected by 2 bytes. The image size then, is the total
the photomultiplier tube and digitized number of pixels times two bytes. If the
into a value directly proportional to the scan resolution is 100 µm (0.004 in.),
density of the film at that point. then a 14 × 17 in. image would contain
The photomultiplier tube has a wide 3500 pixels (14 in. ÷ 0.004 in.) ×
dynamic range, a good ratio of signal to 4300 pixels (17 in. ÷ 0.004 in.) or a total
noise and uses a log amplification process of about 1.5 × 107 pixels. Having 2 bytes
such that a uniform density resolution is of information per pixel results in an
maintained over the entire range. The log image size of 30 megabytes. If the scan
amplifier normalizes the extremely high resolution were increased to 50 µm
number of photons detected at low (0.002 in.), then the image size would
optical densities versus the relatively low increase by 4× to 120 megabytes.
number of photons detected at high Some monitors may not be able to
optical densities. For example, if a laser display the entire image. For example,
film digitizer converts each optical density cathode ray tubes may have display
measurement into a pixel value 1000× the resolutions of 1200 × 1600 or 2000 ×
optical density at that point, then there 2500. Therefore, it is important to
are 1000 levels from 0 to 1 optical density, remember that, depending on the
from 1 to 2 optical density, from 2 to 3 magnification of the image on the
optical density, and so on. This would monitor, there may actually be more raw
provide a density resolution of 0.001 data available than are displayed. To
optical density at all levels. display an image that has either more or
The spatial resolution of a laser scanner fewer data displayed than are in the raw
is determined by the point of laser light image, pixel mapping techniques are
that impinges on the film. Because there used. Pixel replication or pixel
is only a single beam, there is no cross interpolation are used when magnifying
talk between pixels and a true limiting beyond the image resolution. When
resolution equal to the laser spot size can reducing the image size, pixel averaging is
be achieved. Typical laser spot sizes are used.
100 µm (0.004 in.) and 50 µm (0.002 in.). Digital images may contain 12-bit (or
However, the actual resolution will more) digital data that must be displayed
on a monitor that only displays 8 bits
(about what the human eye can discern).

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A method must then be employed to map


the original 4096 gray scale levels of data
onto the available 256 display levels. This
is commonly done either (1) by selecting
which 256 levels of the original 4096 are
displayed or (2) by equally dividing the
4096 levels over the available 256.

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References

1.Quinn, R.A. and C.C. Sigl, eds. 12.Soltani, P.K., C.R. Chittick, T. Chuang,
Radiography in Modern Industry, fourth M.J. Dowling, G.R. Kahley and
edition. Rochester, NY: Eastman T.E. Kinsella. “Advances in 2D
Kodak Company (1980). Radiography for Industrial
2.Nondestructive Testing Handbook, Inspection.” Presented at the
second edition: Vol. 3, Radiography and International Conference on Quality
Radiation Testing. Columbus, OH: Control by Artificial Vision. Le Creusot,
American Society for Nondestructive France: Institut Universitaire de
Testing (1985). Technologie (May 1997).
3.Nondestructive Testing Handbook,
second edition: Vol. 10, Nondestructive
Testing Overview. Columbus, OH:
American Society for Nondestructive
Testing (1996).
4.ASTM E 1025, Standard Practice for
Design, Manufacture, and Material
Grouping Classification of Hole-Type
Image Quality Indicators (IQI) Used for
Radiology. Philadelphia, PA: American
Society for Testing and Materials.
5.ASME Boiler and Pressure Vessel Code.
New York, NY: American Society of
Mechanical Engineers.
6.ASTM E 747, Standard Practice for
Design, Manufacture and Material
Grouping Classification of Wire Image
Quality Indicators (IQI) Used for
Radiology. West Conshohocken, PA:
ASTM International.
7.DIN 54109. Non-Destructive Testing;
Image Quality of Radiographs;
Recommended Practice for Determining
Image Quality Values and Image Quality
Classes. Berlin, Germany: Deutsche
Institut für Normung [German
Institute for Standardization] (1989).
Superseded by EN 462 (DIN).
8.EN 462 P1 (DIN), Non-Destructive
Testing — Image Quality of Radiographs
— Image Quality Indicators (Wire Type)
and Determination of Image Quality
Value. Brussels, Belgium: European
Committee for Standardization
(1994).
9.ASTM E 801, Standard Practice for
Controlling Quality of Radiological
Examination of Electronic Devices. West
Conshohocken, PA: ASTM
International (2001).
10.ASTM E 1254, Standard Guide for
Storage of Radiographs and Unexposed
Radiographic Film. West
Conshohocken, PA: ASTM
International (1998).
11.“CCD Versus Laser Film Digitization
Systems.” Liberty Technologies,
Incorporated, Imaging Systems
Division.

Principles of Film Radiography 183

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