2/5/2020 CN101874949A - Back-washing regeneration method of ceramic membrane method brine refining process filter - Google Patents

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Back-washing regeneration method of ceramic membrane method brine re ning process lter

Abstract
CN101874949A
The invention relates to the technical eld of chlor-alkali chemical industry production, in particular
China
to a back-washing regeneration method of a ceramic membrane method brine re ning process lter;
the ceramic membrane method primary brine ltering re ning process is a novel re ned brine
ltering production process in chlor-alkali industry brine re ning process at home and abroad; at Download PDF Find Prior Art Similar
present, the process has the disadvantages of high back-washing frequency and unclean silt
removal, and a primary ltering side membrane pipe is easy to block by bridging brine sludge in Other languages: Chinese
crude brine and ber matters, so as to cause the primary ltering pressure to be raised to above
Inventor: 孙占瑞, 宋渊, 康志恩, 王启蒙, 王强
0.5MPa, stopping is needed to carry out regeneration cleaning, and the normal production is
affected. In the invention, crude brine is adopted and ows backwards from two grades to one
grade, and back-washing is carried out for a plurality of times forcibly at the re ned brine side, one- Worldwide applications
grade ltering pressure of the lter can be reduced below 0.3MPa, normal production is restored,
2009 CN
and the production running time can be increased.

Application CN 200910263893 events

2009-12-22 Application led by 河北盛华化工有限公司

2009-12-22 Priority to CN 200910263893

2010-11-03 Publication of CN101874949A

Info: Cited by (2), Legal events, Similar documents, Priority and

Related Applications

External links: Espacenet, Global Dossier, Discuss

Claims (1) Hide Dependent

translated from Chinese

1. Brine puri cation process of a ceramic lter membrane backwash reproducing method, wherein the speci c steps are as follows: a, when one side of the lter to increase
the ltration pressure of 0.45 MPa, salt water outlet valve to close, isolating failed brine into the salt water system, a lter circulation pump stops operation, a reduced
pressure to the inlet end surface membrane tube 0.15-0.2MPa; b, an open bottom side of the lter blowdown valve and brine recirculation valve failed to open a feed
pump the ow of crude brine by the two pressure 0.2-0.28MPa opposite direction to a ow rate of 0.7m / s, forming saline back ush pressure 0.12-0.15MPa, the
membrane and the end face of the inner wall of mud caking salt separating off the impurities is discharged through the outfall lter; C, when the reverse ow of the crude
brine for 10 minutes, the automatic control system to select the manual operation, the recoil forced embodiment salt water side membrane ow velocity 1.4m / s, 1- 3
times, 10 seconds each; D, when the reverse ow of the crude brine run for 20 minutes, and ltering raw brine circulation pump start, the valve opening the bypass circuit,
a closed bottom side discharge valve, stopping the operation of a feed pump, an observation side of the lter Pressure lter, as 0.35MPa or less, 5 minutes after the
sample analysis cycle, to close the valve after passing the bypass loop, salt water outlet valve is opened, then the system returns to normal operation.

Description translated from Chinese

Regeneration method backwash brine puri cation process of the ceramic lter membrane

FIELD

[0001] The present invention relates to the eld of alkali chemical brine puri cation technology, speci cally to the backwash reproducing method of brine puri cation
process of a ceramic lter membrane.

Background technique

[0002] The ceramic membrane is a brine puri cation process at home and abroad in the chlor-alkali industry brine puri cation process a new salt water lter production
process. The process for its process is short, less equipment, small footprint, low investment, low operating costs, assisted with less chemical nishing agents and other
advantages and features of domestic chlor-alkali industry in terms of promotion of primary brine puri cation. Salt as raw materials currently used ve chlor have different
degrees during a production run of high frequency recoil, in addition to mud net, one side of the membrane ltration tube is easily crude salt water and salt slurry brous
bridge plug, resulting in a ltration pressure of up to 0. 5MPa above, due to the pressure difference, the failure recoil (recoil pressure 0. 45-0 5MPa;.. a normal working
pressure 0. 35-0 4MPa) ux attenuation lter, not do not stop cleaning regeneration phenomenon. Regeneration shorter washing cycle is generally 7-10 days, low
production e ciency, high throughput Ceramic membrane capacity to play, seriously affected the normal production.

SUMMARY

[0003] The object of the present invention is to provide a ceramic membrane process brine puri cation method of regeneration of the lter backwash, can not stop, fast
recovery lter ux, extended production runs ceramic membrane ltration time with brine.

[0004] The speci c steps of this aspect of the invention is as follows:

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2/5/2020 CN101874949A - Back-washing regeneration method of ceramic membrane method brine refining process filter - Google Patents
[0005] a, a side of the lter when the ltration pressure was increased to 0. 45MPa, salt water outlet valve to close, isolating the salt water into the brine system failure,
stop ltering circulation pump is operated, a reduced pressure in the inlet end face of the lm tube is 0.15-0. 2MPa.

[0006] b, an open bottom side of the lter blowdown valve and brine recirculation valve failed to open a feed pump, the crude brine 0. 2-0. 28MPa by the two counter- ow
direction to a pressure, the ow rate was 0. 7m / s, forming saline back ush pressure 0. 12-0. 15MPa, the detached impurities caking salt slurry and the end face of the
inner wall of the membrane lter is discharged through the outfall.

[0007] c, when the reverse ow of the crude brine for 10 minutes, the automatic control system to select the manual operation, the recoil forced embodiment salt water
side membrane ow velocity 1. 4m / s, 1-3 times for 10 seconds .

[0008] d, when the reverse ow of the crude brine to run for 20 minutes, ltered raw brine circulation pump start, the valve opening the bypass circuit, a closed bottom
side discharge valve, stopping the operation of a feed pump, a lter was observed pressure side of the lter, as 0. 35MPa or less, the cycle after 5 min the sample analysis
results, closing the bypass valve after passing cycle, salt water outlet valve is opened, then the system returns to normal operation.

[0009] aspect of the present invention is directed to a high-pressure working principle of cross- ow ltration apparatus ceramic membrane brine puri cation salt as raw
materials currently used, due to the circulating pump provided on a side of the lter's pressure side appears a brine lter the crude crude salt brine inlet end surface is
easily formed salts in water and mud clogging impurities brous ceramic membrane tube and passage due to the pressure difference recoil effect poor circumstances. A
take measures to reduce the inlet pressure 0. 15-0. 2MPa during the recoil cycle to a ow of saline from the two opposite directions, washed with brine and back ush
pressure blocking lm itself, the force of gravity the inner wall and the end face of salt slurry and separation of impurities down agglomerates, and the lter is discharged
through the outfall. Regular cleaning will reduce the chance of the membrane potential bypass passageway crude salt is a salt water mud and brous impurities clogging
the lter can be too long to maintain a high ux operation state, the regeneration extended cleaning cycle, continuous large-scale industrial production.

[0010] The advantage of the present invention is an effective solution to a ceramic membrane lter in the brine puri cation salt as a raw material in the production
apparatus due to the large amount of impurities contained in the salt results in one side of the membrane ltration ux decline tube blockage, can not be continuously
played high throughput advantages of the ceramic membrane. The entire device does not stop, does not consume chemical agents, does not increase the power
consumption, a backwash a ltration pressure of 10-30 minutes per week for a long time can be maintained at 0. 35MPa or less, to maintain a high ux ltration, washing
regeneration cycle consists of 10 extended to 30 days or more days, monthly production additional 36 hours running time, extended production runs around the lter time
400 hours per year, the savings of about 15 cubic purity hydrochloric acid cleaning agent.

BRIEF DESCRIPTION

Schematic [0011] FIG. 1 embodiment of the present invention. DETAILED DESCRIPTION

[0012] When the salt slurry and the formation of impurities clogging the initial brous ceramic membrane tube bridge, the regeneration should backwashing embodiment,
the following steps:

[0013] a, when one side of the lter to increase the ltration pressure of 0.45 MPa, salt water outlet valve to close, isolating the salt water into the brine system failure,
stop ltering circulation pump is operated, a reduced pressure to the inlet end surface of the lm tube 0.15-0. 2MPa.

[0014] b, an open bottom side of the lter blowdown valve and brine recirculation valve failed to open a feed pump, the crude brine 0. 2-0. 28MPa by the two counter- ow
direction to a pressure, the ow rate was 0. 7m / s, forming saline back ush pressure 0. 12-0. 15MPa, the detached impurities caking salt slurry and the end face of the
inner wall of the membrane lter is discharged through the outfall.

[0015] C, when the reverse ow of the crude brine for 10 minutes, the automatic control system to select the manual operation, the recoil forced embodiment salt water
side membrane ow velocity 1. 4m / s, 1-3 times for 10 seconds ; recoil times can be determined according to the crude brine fouling the membrane tubes where inner
channel wall.

[0016] d, when the reverse ow of the crude brine to run for 20 minutes, ltered raw brine circulation pump start, the valve opening the bypass circuit, a closed bottom
side discharge valve, stopping the operation of a feed pump, a lter was observed pressure side of the lter, as 0. 35MPa or less, the cycle after 5 min the sample analysis
results, closing the bypass valve after passing cycle, salt water outlet valve is opened, then the system returns to normal operation.

Cited By (2)

Publication number Priority date Publication date Assignee Title

CN104984586A * 2015-07-10 2015-10-21 四川航天电液控制有限公司 High-low pressure automatic backwash lter station

CN108101075A * 2017-12-23 2018-06-01 安徽名创新材料科技有限公司 A kind of ceramic membrane brine recti cation process

Family To Family Citations

* Cited by examiner, † Cited by third party, ‡ Family to family citation

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Priority And Related Applications

Priority Applications (1)

Application Priority date Filing date Title

CN 200910263893 2009-12-22 2009-12-22 Back-washing regeneration method of ceramic membrane method brine re ning process lter

Applications Claiming Priority (1)

Application Filing date Title

CN 200910263893 2009-12-22 Back-washing regeneration method of ceramic membrane method brine re ning process lter

Legal Events

Date Code Title Description

2010-11-03 C06 Publication

2010-12-15 C10 Request of examination as to substance

2013-01-30 C12 Rejection of an application for a patent

Concepts

machine-extracted Download Filter table

Name Image Sections Count Query match

methods abstract,title 6 0

re ning abstract,title 4 0

washing abstract,title 4 0

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2/5/2020 CN101874949A - Back-washing regeneration method of ceramic membrane method brine refining process filter - Google Patents

ceramic abstract,title 3 0

regeneration abstract,title 3 0

ltration abstract 5 0

production abstract 5 0

alkali abstract 2 0

crude oil abstract 2 0

chemical industry abstract 1 0

cleaning abstract 1 0

ber abstract 1 0

increased abstract 1 0

industry abstract 1 0

reduced abstract 1 0

sludge abstract 1 0

Show all concepts from the description section

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