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Processing of
titanium & aluminium alloys
Cecilia Poletti
u www.tugraz.at
2
Overview
β stabilizing α stabilizing
Recrystallization summer school 2014
11.09.2014
9
Titanium alloys: classification
Ti-5Al-5Mo-5V-3Cr-1Zr
(Ti55531)
𝑻𝜷 ~𝟖𝟎𝟎°𝑪
Ti-6Al-4V
(Ti64)
𝑻𝜷 ~𝟏𝟎𝟎𝟎°𝑪
E/ρ
Titanium
Steels
Magnesium
Aluminium
Ingot Billet
Bar
Sponge
Slab Plate
Sheet
Cold strip
Recrystallization summer school 2014
11.09.2014
17
Processing from an ingot
𝛼+𝛽
I II III IV
Homogenization Deformation Recrystallization Ageing
Recrystallization summer school 2014
11.09.2014
19
Primary processing: open die forging
II
Forging
Recrystallization summer school 2014
11.09.2014
25
Flow curves Ti64
970°C α+β
1150°C β
1070°C strain 0
Compression tests +
water quenching
Warchomicka, F.; Poletti, M. C.; Stockinger, M.; Degischer, H. P.:Materials
science forum 706-709 (2012) 252 - 257
subgrains
Deformation
bands
11.09.2014
31
How are beta grains refined?
low strain-240min-
1070°C rate 0s 15s
60s
0.1/s
1 Strain
50µm
Recrystallization summer school 2014
11.09.2014
33
Deformation in alpha+beta:Ti64
930°C 0.1/s
60
Point to point
Point to origin
50
30
20
10
0
0.0 0.2 0.4 0.6 0.8 1.0
relative distance [-]
36
Deformation in alpha + beta (Ti55531)
Low Taylor factor (dark) lower stored energy
better orientation for the deformation
20 µm 10 µm
b transus temp.
20 µm
Def. bands
5 µm
Def. bands
b DRV
20 µm
gDRX
b DRV + gDRX gDRX
10 µm
50 µm
11.09.2014
40
Grain
refinement by
TiB addition
(cast)
11.09.2014
42
Heat treatments after deformation
Temperature [°C]
III IV
Recrystallization Annealing
11.09.2014
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Heat treatment in beta
0 min 2 min
10 min
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Heat treatment in beta
-Q
D - D K t exp
n n
0
Krumphals, A., Poletti, C., Warchomicka, F., Stockinger, M., Sommitsch, C.
RT
(2014) International Journal for Multiscale Computational Engineering
11.09.2014
45
Cooling from beta
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Cooling from alpha + beta
50μm
100μm 100μm
Rolling direction
C
B
A
20 µm
Pinching off
a) 50µm b) 50µm
Al-Fe-Mn-Si
particles
Mg2Si
Al-Fe-Mn-Si
particles
Mg2Si
2 µm 2 µm
300°C 500°C
σ n𝑝1
𝐴𝑝1 = ε exp Q RT = Z𝑝
G
σ n1
𝐴1 sinh α1 = ε exp Q RT = Z
G
σ − σth n
𝐴2 sinh α( ) = ε exp Q RT =Z
G
th = 21.5MPa
20 th = 20MPa
d [MPa]
th = 16MPa
15 th = 15.5MPa
10
400°C = 300°C = 0.69
5 550°C = 0.18 Poletti, C., Wójcik,
T., Sommitsch, C
500°C = 0.2 Metallurgical and
Materials
Transactions A
0 (2013) Volume 44,
Issue 3, pp 1577-
0.0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1.0 1586
Recrystallization summer school 2014
11.09.2014
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Cold
deformation
and particles
Outlook
0.00
Hot workpiece, hot die
0.39
0.26
0.13
0.00
Recrystallization summer school 2014
11.09.2014
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Hot die and isothermal forging