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A journal to advance the fundamental understanding of food texture and sensory perception
KEYWORDS ABSTRACT
Crispy, crunchy, instant controlled pressure
drop, puncture test, strawberry, texture The aim of this study was to evaluate the effect of hot air drying, freeze drying and
analysis swell drying (which is a coupling of hot air drying to instant controlled pressure
drop DIC) on strawberry to compare and contrast its quality in terms of texture,
3
Corresponding author.
such as crunchy and crispy features, correlated with the expansion ratios and the
TEL: +33 5 46 45 87 66;
FAX: +33 5 46 45 86 16;
microstructure’s modification. The obtained results showed that swell-dried
EMAIL: kallaf@univ-lr.fr strawberry had a high crispness behavior. Also, its relative expansion ratio was
thrice more than air-dried samples. Moreover, it was observed that saturated
Received for Publication April 26, 2013 steam pressure of DIC texturing operation compared with the thermal holding
Accepted for Publication April 25, 2014 time had a significant effect on the maximum penetration distance and the
Published online Article Accepted on average of microruptures force on crunchiness and crispness, respectively. Hence,
April 30, 2014
these structural changes provide a versatile swell-dried strawberry as highly func-
doi:10.1111/jtxs.12070
tional snack that was able to be evaluated instrumentally by puncture test.
PRACTICAL APPLICATIONS
Puncture test is an instrumental measurement that helps to describe the crispness
of snacks, biscuits, extruded products, etc. Swell-drying process is defined
as instant controlled pressure drop (DIC)-assisted hot air drying. The
thermomechanical effects of DIC are mainly induced by the abrupt pressure drop
toward a vacuum (about 5 kPa) after shortly subjecting the material to saturated
steam pressure (from 0.1 up to 0.6 MPa). The abrupt pressure drop rate (ΔP/
Δt > 0.5 MPa/s) causes an autovaporization of product’s water, promoting instant
cooling of the product, which immediately decrease the product’s temperature
under its Tg allowing to cross the glass transition Tg, which immediately stops the
thermal effects avoiding any resulting degradation. The impact of DIC on straw-
berry can be observed in expansion ratio and much better through texture content
as crispy and/or crunchy snacking. Hence, it is necessary to instrumentally
describe the mechanical behavior of such a brittle-dried strawberry. The texture
measurements allow using it as one of multicriteria optimization of DIC texturing
processing parameters.
246 Journal of Texture Studies 45 (2014) 246–259 © 2014 Wiley Periodicals, Inc.
M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES
disintegrate when incorporated in fresh form into food 2012). Moreover, this structural change provides a highly
products such as yoghurts, ice creams as well as other pro- functional snack; thanks to a preservation of vitamins,
cessed products. Food industry commonly uses strawberry bioactive compounds, color and flavor.
in dried form to extend its shelf life and to handle it easily as However, texture is a very important feature of all kinds
ingredient. Up to now, solar drying, HAD, FD and vacuum of foods that directly impacts in the consumer acceptability.
drying are the conventional methods used to process fruits More specifically, texture has a specific importance in such a
and vegetables. However, they present some disadvantages snacking. Texture is primarily the response of tactile senses
for the product quality, such as significant deterioration of to physical stimuli that results from contact between some
bioactive compounds and structural textural damages. part of the body and the food (Bourne 2002a). Food mate-
Indeed, the shrinkage of product is usually produced by rial structure at both macro (porosity and relative density)
very long time exposure of HAD. In addition, the difficulties and micro (cell wall thickness, cell diameter and distribu-
in processing, as the low ability of grinding and rehydration, tion) scales as well as having closed or open pores affects the
are barriers to adopt hot air process for a large range of mechanical properties (Sozer et al. 2011; Van Vliet and
fruits and vegetables (Mounir et al. 2012). Furthermore, FD Primo-Martín 2011).
is a costly process in terms of manufacturing, mainly due to The new concept of snacks from dried fruits and veg-
high energy consumption coupled with loss of flavor and etables is defined with crunchiness and crispiness as the tex-
color, which greatly reduces its acceptability and end uses tural features that better describe their quality and even
(Ratti 2001). freshness (Luyten et al. 2004). They are related to foodstuff
A new drying operation has been proposed as an alterna- as brittle materials, which mean absence of plastic behavior;
tive to the following: (1) improve the texture and quality only elastic behavior until rupture exists. They relatively
attributes of dried foods and (2) reduce the energy con- easily break, producing a sharp sound (Al Chakra et al.
sumption, resulting in low manufacturing cost. It also has 1996; Luyten et al. 2004; Saeleaw and Schleining 2011). The
the ability to handle ranges of food products, regardless distinction between crispy and crunchy features is not so
of their heat sensitivity (e.g., strawberry, cranberry, clear. Indeed, different works suggest that crispness and
blackberry, guava, mango, onion, carrot, pepper, potato, crunchiness are usually differently identified (Table 1),
apple, etc.) (Albitar et al. 2011; Mounir et al. 2011, 2012; although they belong to the most frequently used texture
Alonzo-Macías et al. 2012; Téllez-Pérez et al. 2012). This descriptors in United States, Japan, France and Austria
operation of SD couples the conventional HAD to the tech- (Bourne 2002a; Roudaut et al. 2002; Nishinari et al. 2008;
nology of instant controlled pressure drop, called in French, Saeleaw and Schleining 2011; Van Vliet and Primo-Martín
Détente Instantanée Contrôlée (DIC). 2011).
DIC was defined in 1988 by Allaf and Vidal as a high- The question is still open (Roudaut et al. 2002). The defi-
temperature short-time treatment followed by an abrupt nitions given vary between different studies and likely
pressure drop toward a vacuum (pressure drop rate higher between countries and products (Roudaut et al. 2002;
than 0.5 MPa/s). DIC-assisted HAD is a texturing stage Luyten et al. 2004; Nishinari et al. 2008). Sometimes, the
between pre and final HAD operation. This coupling is panelists as well as consumers found it very difficult to dis-
better known as SD (Kamal et al. 2008; Albitar et al. 2011; tinguish between crispy and crunchy terms and needed con-
Mounir et al. 2011; Alonzo-Macías et al. 2012). Therefore, stant probing. However, all insisted that they could perceive
the SD products have a controlled texture expansion with a difference between the two concepts, although struggling
higher sensorial quality and functional properties. This to describe this difference, indicating that it was only slight
texture change results in higher porosity, increasing the spe- (Saeleaw and Schleining 2011).
cific surface area and reducing the diffusion resistance of By this research, crunchiness and crispness were defined
moisture during the final dehydration step (Mounir et al. according to French language and culture. Crunchiness,
Journal of Texture Studies 45 (2014) 246–259 © 2014 Wiley Periodicals, Inc. 247
TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF
“croquant,” is defined as a linear elastic behavior until the providing more information about different snack food
complete fracture (brittle; e.g., hot air-dried products, texture attributes.
almonds). On the other hand, crispness, “croustillant,” is The aim of this study was to evaluate the effect of SD,
understood as the same but small continuous linear elastic which is DIC-assisted HAD, compared with other drying
behavior until the successive fractures during chewing (e.g., processes such as conventional HAD and FD on the two
SD and FD products, biscuits). At the same time, to carry types of texture (i.e., crunchy and crispy behavior) in the
out measurements of the physical aspects of texture percep- specific case of strawberry (Fragaria var. Camarosa).
tion in foods, different methods have been proposed. They
involve two main categories: sensory and instrumental
MATERIALS AND METHODS
analysis. These last measurements include mechanical mea-
surements (e.g., compression, penetration) and acoustical
Sample Preparation
procedures (Roudaut et al. 2002; Van Vliet and
Primo-Martín 2011), and sometimes, a combination of The strawberries (Fragaria var. Camarosa) were purchased
acoustic analysis with mechanical testing for analyzing the from a local market (La Rochelle, France). They were cut in
crispness is used. Nonetheless, instrumental measurements 4- to 5-mm transverse slices. Afterward, the total quantity
are generally preferred to objectively evaluate the attributes was divided in three batches to carry out different tech-
related to the mechanical properties (Altamirano-Fortoul niques of HAD, FD and SD.
et al. 2012).
To describe the texture (i.e., crunchiness and crispness
Treatment Drying Methods
features) in the swollen food products, a puncture test has
been widely applied (Van Hecke et al. 1998) (Roudaut et al. HAD. The slices of strawberries were dried in a hot air drier
2002). This test measures the force required to push a punch (Universal Oven UNB Model 800, Memmert Company,
or probe into a food. It is characterized by the following: (1) Germany.) at 50C. The initial relative humidity of air was 2.2%
a force measuring instrument; (2) penetration of the probe and an air flux rate of 1.2 m/s. Slices were dried until attaining
into the food causing irreversible crushing (i.e., to fracture 3.0% of moisture content db for around 24 h. Afterward, the
separately the different cell walls constituting the product) samples were analyzed and recorded as HAD.
or flowing of the food; and (3) the depth of penetration
usually held constant (Bourne 2002b). Hence, the deforma- FD. An FD equipment (model RP2V, Serail Company, Le
tion behavior of crunchy/crispy food products is often Coudray Saint Germer, France) was used for drying the batch
studied as a function of time/displacement at lower rates of of strawberry slices. The conditions were divided in three
deformation in order to be able to study the possible differ- steps: external freezing (at −20C/2 h), sublimation (−20C,
ent fracture events separately (Van Hecke et al. 1998; 0.66 Pa/12 h) and desorption (25C, 0.66 Pa/12 h). Subse-
Saeleaw and Schleining 2011). It means that for crispy prod- quently, the samples were analyzed and recorded as FD.
ucts, the force-deformation pattern is characterized by a
series of sharp force peaks corresponding to the rupture of SD. As SD is a DIC-assisted HAD, the batch of strawberry
individual cell walls (Van Hecke et al. 1998; Roudaut et al. slices was partially hot air dried at the same conditions
2002). described in HAD method (50C with an initial relative
Regarding the different instruments and settings to punc- humidity of 2.2% and an air flux rate of 1.2 m/s) until 18%
ture test, there is no information or any criteria to select db. This first step needed about 8 h. Subsequently, the slices
them. The model including the diameter and velocity of the were placed in airtight bags and stored in a cold chamber at
probe (i.e., cylindrical or needle) depends on the food 5C by 24 h to homogenize their moisture content (18% db).
product (Altamirano-Fortoul et al. 2012). Afterward, the partially hot air-dried strawberries were
Therefore, instrumental methods, as puncture test, treated by DIC equipment (ABCAR-DIC Process, La
and microstructure analysis could be an alternative for Rochelle, France) according to the DoE (Table 2). Finally,
DIC, instant controlled pressure drop; DoE, design of experiments; P, saturated steam pressure; t,
thermal holding time.
248 Journal of Texture Studies 45 (2014) 246–259 © 2014 Wiley Periodicals, Inc.
M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES
mi − md
Wdb % = . Eq. (1)
md
Assessment Methods
Water Moisture Content. Moisture content was deter-
mined using a slightly modified Karathanos method (1999).
Briefly, the strawberry samples were quantified gravimetri- FIG. 2. SCHEMATIC TIME–PRESSURE PROFILES OF A DIC PROCESS
cally by triplicate. Samples of mi = 2.5 ± 0.1 g were dried at (A) Vacuum establishment; (B) steam injection; (C) high steam pressure
65C for 48 h in an adequate oven UFE 400 (Memmert), for thermal treatment time; (D) instant controlled pressure drop
thus reaching the final mass md: toward vacuum; and (E) atmospheric pressure establishment.
Journal of Texture Studies 45 (2014) 246–259 © 2014 Wiley Periodicals, Inc. 249
TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF
FIG. 3. (A) SCHEMATIC DIAGRAM OF PUNCTURE TEST. (B) THEORETICAL FORCE-DEFORMATION CURVES OBTAINED BY PUNCTURE TEST:
CRUNCHY BEHAVIOR: MAXIMUM PENETRATION FORCE, Fmax (N); MAXIMUM PENETRATION DISTANCE, Xmax (MM) AND TOTAL WORK, Wmax, (J).
(C) THEORETICAL FORCE-DEFORMATION CURVES OBTAINED BY PUNCTURE TEST: CRISPY BEHAVIOR: THE PENETRATION DISTANCE FOR EACH
MICRORUPTURE PEAK, ΔX (MM); THE INDIVIDUAL FORCE DROPS FOR EACH MICRORUPTURE PEAK (ΔF, N) AND THE AVERAGE WORK FOR
MICRORUPTURES, wrupture (J). (D) REAL FORCE-DEFORMATION CURVE RECORDED BY PUNCTURE TEST: CRUNCHY AND CRISPY BEHAVIOR
fication parameters (Fig. 3C). Calculating the ratio of n Where ΔX is the penetration distance for each
divided by the maximum penetration distance (Xmax) is to microrupture peak (mm) and ΔF is the individual force
have the spatial microrupture frequency. The workload of drop for each microrupture peak (N). All of these param-
each puncturing until the microrupture wrupture worth to be eters (i.e., Xmax, Wmax, <F>, N, f, wrupture, ΔX and ΔF) were
identified as well as the mean of each micropuncturing
rupture force f = <ΔF> (Table 4).
TABLE 4. CRISPY DESCRIPTION PARAMETERS
250 Journal of Texture Studies 45 (2014) 246–259 © 2014 Wiley Periodicals, Inc.
M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES
calculated until Fmax was reached (Fig. 3D). Measurements 8 and 11) was observed; thanks to a scanning electronic
were carried out with five repetitions, and the final values microscope (SEM) JEOL 5410LVFEI Quanta 200F (Philips,
were the arithmetic mean. Croissy-sur-Seine, France). Each sample was placed on a
covered support using carbon adhesive, and the scanning
Expansion Ratios was carried out under partial vacuum (7 Pa) with an accel-
For porous materials, two expansion ratios are normally erating voltage of 20 kV.
defined: the absolute expansion ratio (εabsolute) and the rela-
tive expansion ratio (εrelative). εabsolute is the ratio of the appar-
DoE and Statistical Studies
ent volume of the product and the volume of the solid itself,
while εrelative reflects the final volume after processing (FD To study the effect of saturated steam pressure and thermal
and SD) compared with the HAD. The εabsolute and the holding time of DIC treatment on the crunchiness and
εrelative are strictly linked to the product’s density (ρ, crispness features, and the expansion ratios of dried straw-
g/cm3), and they were calculated to each sample as follows: berries, a two-parameter, five-level central composite rotat-
able design was used (Table 2). The DoE yielded 4 = 22
ρintrinsic factorial points, 4 = 2 × 2 axial points and three center
Absolute expansion ratio: ε absolute = Eq. (8)
ρspecific points for replications (Table 5). This central composite
design of 11 experiments was run in random in order
ρspecific of HAD product
Relative expansion ratio: ε relative = to minimize the effects of unexpected variability on the
ρspecific of SD or FD product studied responses due to external factors (Table 2).
Eq. (9) The different crunchiness parameters retained as
responses (dependent variables) were the maximum pen-
where ρintrinsic is the intrinsic (or true) density of solid itself. etration force (Fmax, N), the maximum penetration distance
To measure the intrinsic density (ρintrinsic, g/cm3) of each (Xmax, mm), the total work at Xmax (Wtotal, J) and the <F>
sample (HAD, FD and SD), a gas Pycnometer Micromeritics (<F>, N). Crispness was evaluated through the total
AccuPyc 1330 (Quantachrome Instruments, Florida, USA) number of peaks (n), the spatial frequency of structural
with helium was used. microruptures (N, m), the average of microrupture force (f,
ρspecific is the apparent density of dried samples. In the N) and the average work for microruptures (wrupture, J).
present work, it was not possible to adopt the Archimedes These parameters as well as the expansion ratios considered
method for measuring ρspecific because of the possible inter- at both aspects of absolute (εabsolute) and relative (εrelative) were
actions between product and water. Thus, to determine such added to the initial dependent variables.
specific density (ρspecific, g/cm3), a tapped method was carried In terms of texture parameters, this response surface
out. Briefly, 71/200-μm diameter sand (ρsand = 909.2 g/cm3) methodology was used to optimize the treatment condi-
was poured into the cylinder (100 mL and 37.018 ± 0.001 g tions to meet the consumer requirements. The statistical
of weight). The sand-filled cylinder was then tapped for analyses were performed with Statgraphics (Centurion XV,
1,000 times on an Autotap Quantachrome DA-3 (Boynton Statpoint Technologies, Inc., Warrenton, Virginia, USA),
Beach, Florida, USA). During the tapping, the sand volume thus inserting for each dependent variable Y, Pareto Charts
was decreased, and a quantity of sand was added during the to show the relevance of each independent variables
operation in order to refill the cylinder. Then, the weight (P < 0.05), response surface to identify their impact and a
was registered, and the mass of sand (ms,1, g) was calculated. mathematical empirical model:
Subsequently, this method is repeated adding a known mass
dried sample (msample about 2 ± 0.001 g) into the cylinder
TABLE 5. CODED AND REAL LEVELS FOR INDEPENDENT VARIABLES
with the sand included. The weight was recorded, and the
USED IN TWO-VARIABLE, FIVE-LEVEL ROTATABLE EXPERIMENTAL
new mass of sand (ms,2, g) was calculated. Thus, the specific DESIGN
density of each sample (HAD, FD and SD) was calculated as
P: processin t: processing
follows:
Coded level g pressure (MPa) time (s)
Journal of Texture Studies 45 (2014) 246–259 © 2014 Wiley Periodicals, Inc. 251
TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF
n n n −1 n
Y = β0 + ∑ βi χi + ∑ βii χi2 + ∑ ∑ βij χi χ j + ε Eq. (11)
i =1 i =1 i =1 j = 2
where βi, βii, βij are the regression coefficients, Xi and Xj are
the independent variables, ε is random error, i and j are the
indices of the factors. R2 value was also evaluated to accurate
fitting models to real data.
Depending on various responses, a multicriteria optimi-
zation can be done.
Expansion Ratios
Strawberry’s expansion ratios are parameters that allowed
analyzing globally the effect of drying technique (HAD, FD
and SD) on the product’s structure. The results gathered in
Table 6 shown that FD strawberry had the highest value of
expansion ratios, εabsolute and εrelative, completely opposite to
HAD parameters. Therefore, SD samples had intermediate
expansion ratios between HAD and FD samples. More-
over, under certain conditions of DIC process (DIC 5:
P = 0.53 MPa and t = 13 s), SD relative expansion ratio was
thrice more than HAD samples (εrelative = 3.62 compared
with 1).
In this sense, expansion greatly depends on the DIC
saturated steam pressure, while the thermal treatment time
has negligible effect (Figure 4). The empirical model we
obtained through Statgraphic statistical evaluation was with
R2 = 83.62%:
SD sample 1 2 3 4 5 6 7 8 9 10 11 HAD FD
εabsolute 4.09 3.77 3.54 3.64 4.52 3.21 2.44 1.91 1.19 2.90 3.05 1.15 18.26
εrelative 3.48 3.10 2.92 2.97 3.62 2.70 2.07 1.59 1.03 2.49 2.60 1.00 14.13
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M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES
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254 Journal of Texture Studies 45 (2014) 246–259 © 2014 Wiley Periodicals, Inc.
M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES
Journal of Texture Studies 45 (2014) 246–259 © 2014 Wiley Periodicals, Inc. 255
TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF
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M. ALONZO-MACÍAS, G. MONTEJANO-GAITÁN AND K. ALLAF TEXTURE MEASUREMENT OF DRIED STRAWBERRY SLICES
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