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SPECIAL ISSUE ARTICLE

Conventional and bobbin friction stir welding


of 12% chromium alloy steel using composite
refractory tool materials
W. M. Thomas*, C. S. Wiesner, D. J. Marks and D. G. Staines
The use of matching tapers to provide a hot friction drive coupling for composite refractory tools
for conventional and bobbin friction stir welding of 12% chromium alloy steel is described. The
feasibility of using self-reacting (Bobbin) friction stir welding for steel has been demonstrated and
the resulting microstructures have been evaluated.
Keywords: Friction stir welding, Bobbin, Self-reacting stir welding, 12% chromium steel

Introduction Objectives
To determine the feasibility of conventional and bobbin
Friction stir technology is a continuous hot shear
FSW of 8 mm and 12 mm thick 12%Cr steel and to
process involving a non-consumable rotating tool of
establish the weld properties and microstructures
harder material than the workpiece itself. The probe
produced.
portion of the tool is entered into the workpiece creating
To determine the practicability and the effect of
a plasticised region around the immersed probe and the
composite tools, comprising different shoulder and
contacting part of the shoulder. There is a volumetric
probe refractory materials, on welding performance.
contribution to heat generation from adiabatic heating
due to deformation within a third body region that
surrounds the probe and part of the shoulder. The Experimental
shoulder region of the tool provides an additional
Composite tool designs for conventional and
friction treatment to the workpiece top surface and
prevents plasticised joint material from being expelled.
bobbin FSW
Essentially, the shoulder and probe thermomechanically Composite tools comprising of two different refractory
soften and then separate the material being processed by metal alloys were used. The material for the shoulder
the passage of the probe through the material. The was selected to produce a smooth surface finish and the
material flows around the probe and is then forge material for the probe was selected to have high strength
welded together at the trailing edge of the probe. This and to achieve good coupling to the steel at the welding
separation and welding together occur continuously by temperature. The tool was made using a ‘Morse taper’
backfilling from the probe and compaction/containment principle, which is an ideal arrangement for securing the
from the shoulder. This transient separation/rewelding two materials under extremely hot welding conditions
operation happens during and before the trailing edge of (Fig. 2).
the shoulder moves away from the processed/weld track. The matching tapered coupling allows for the secure
The transient plasticised region immediately coalesces and efficient combination of different refractory materi-
and forms a solid phase bond as the tool moves away. als and provides a unique hot friction drive. The conical
probe part compresses the tapered bore of the shoulder
The friction stir welding (FSW) process was patented
to produce hoop stresses within the shoulder. These
by TWI in December 1991, and this patent also included
hoop stresses can be accommodated easily by increasing
the first example of a self-reacting (bobbin) stir weld in
the thickness and/or diameter of the shoulder.
aluminium.
Frictional contact across the entire conical surface
Previous work on FSW of steel area of the interface between inner and outer matching
tapers is sufficient to provide a large amount of torque
A growing number of papers cover the FSW of steel, but
transmission. Therefore, splines, bolts or keys and
only limited work has been reported on bobbin stir
keyways and similar stress raisers are not required.
welding of steel. The following investigation describes
Bobbin FSW has been shown to be effective for
recent work at TWI on welding steel using both
joining hollow extrusions and lap joints. Essentially,
conventional and bobbin stir welding techniques. The
there are two types of bobbin, or self-reacting techni-
basic principle of bobbin stir welding is shown in Fig. 1. ques: technique of a fixed gap, between the shoulders1–3
and one that allows the gap between the shoulders to
adapt during the welding operation.4–9 Published
TWI Ltd, Granta Park, Great Abington, Cambridge CB21 6AL, UK investigations have confirmed the practicability of the
*Corresponding author, email wayne.thomas@twi.co.uk self-reacting technique.1–9 The self-reacting principle of

ß 2009 Institute of Materials, Minerals and Mining


Published by Maney on behalf of the Institute
Received 1 December 2008; accepted 27 January 2009
DOI 10.1179/136217109X415893 Science and Technology of Welding and Joining 2009 VOL 14 NO 3 247
Thomas et al. Conventional and bobbin FSW of 12%Cr alloy steel

a bobbin tool showing two shoulders separated by pre-


set fixed length; b bobbin tool showing self-contained
reactive forces
1 Salient features of self-reacting (bobbin) stir welding:
15workpiece; 25top shoulder; 35probe; 45bottom
shoulder; 55reactive forces

all bobbin techniques means that the normal down force


required by conventional FSW is essentially eliminated.
The reactive forces within the weld are contained a conventional FSW tool with single tapered coupling
between the bobbin shoulders (Fig. 1b). design; b bobbin stir welding tool showing friction
tapered coupling designed for refractory material
Material shoulders, refractory material probe and hot work tool
All welding trials were carried out on 12% chromium steel body
alloy steel supplied to DIN 1?4003. For conventional 2 Composite refractory tools: securing different refrac-
FSW, 12 mm thick and 1000 mm long plates were tory materials by tapered friction coupling design
supplied and used in the hot rolled condition, which
exhibited a microstructure that consists of tempered composition (316L stainless steel) were placed under the
martensite, without any significant fraction of delta weld region to protect the anvil and the root region of
ferrite. For bobbin trials, 8 mm thick and 500 mm long the weld from metal pick-up. Equal thickness plates
test specimens were machined from 12 mm thick plate. were placed underneath the remaining workpiece to
Welding procedure maintain flatness.
The steel workpiece plates were secured with work Weld and metallurgical assessment
holding fixtures onto the machine traverse table. For
All welds were visually examined for surface roughness,
conventional FSW, a pilot hole of smaller diameter than
the presence of surface breaking defects and side flash. A
the probe was drilled between the abutting plates at the
start of the weld seam. For bobbin stir welding, an number of welds were tensile and bend tested, together
interference slot with a width similar to the probe with metallurgical examination. All sections were pre-
diameter was machined between abutting plates at the pared in the direction looking towards the start of the
start of each butt weld, to allow most of the contact face weld, and for clarity, all macrographs are marked
from both shoulders to engage before the probe made ‘advancing side’ and ‘retreating side’. Sections from
full contact. Touchdown conditions were set to minimise the 12% chromium alloy were polished to a 1 mm finish
the stress on the tool. Traversing was initiated after and etched in an ethanol solution containing 2?5% picric
sufficient time to plasticise the workpiece material in acid and 2?5% hydrochloric acid.
contact with the shoulder and probe. The FSW opera-
tion was carried out at ambient temperature, and no Results
auxiliary preheat or interpass heating of the workpiece
was used. Friction stir welds were produced with Welding trials
the welding direction parallel to the rolling direction For conventional FSW, 1 m long test specimens were
of the plate. To prevent the friction stir welded work- produced using composite tools (with a tapered probe
piece material adhering, an oxidised carbon steel anvil and three flats) at rotational speed 584 rev min21,
support plate was used. However, this was not success- traverse rate 2?5 mm s21 and axial force of 32 kN.
ful in preventing carbon steel pick-up. Therefore, sacri- Bobbin stir welds were made using, initially parallel, and
ficial, nominally 1 mm thick strips of similar material then tapered probes with three flats at rotational speed

Science and Technology of Welding and Joining 2009 VOL 14 NO 3 248


Thomas et al. Conventional and bobbin FSW of 12%Cr alloy steel

584 rev min21 and traverse rate 1?25 mm s21. No axial


force was required.
Trials with composite tools
Figure 3 shows both conventional FSW and bobbin
tools that comprise two refractory materials, the probe
manufactured from a refractory alloy with high tungsten
content and the shoulders manufactured from refractory
alloy with a low tungsten content. The shoulders and
probe of the bobbin tool are attached to a hot work tool
steel body.
Surface appearance
The surface of the steel welds exhibited a uniform
surface ripple (caused by the final sweep of the trailing
edge of the rotating tool). The FSW weld was essentially
smooth and flush with the surface (Fig. 4). No pro-
tective gas was used to shield the workpiece from
atmospheric contamination during welding. However, a
cooling blast of air was applied to the top and bottom
shoulders of the bobbin tool.
Start and stop regions
Unless run-on and run-off plates are used, then start and
stop regions may need to be discarded. Figure 5,
however, shows that for conventional FSW, reasonable
backfilling of a predrilled pilot hole can be achieved
providing that the pilot hole was drilled slightly smaller
than the probe. The use of a larger diameter pilot hole
than the probe diameter leads to incomplete backfilling
(Fig. 5b).
For conventional FSW, a stop and restart can if
a conventional FSW tool showing taper probe with three necessary be accommodated anywhere along the seam.
flats; b bobbin tool showing parallel probe with three However, a disadvantage of the fixed gap bobbin
flats (later improved versions were made with tapered technique is that to exit the tool needs either:
probe and smaller bottom shoulder) (i) to complete an open ended joint
3 Typical composite refractory tools (ii) to break out of the work piece

a conventional FSW; b top surface bobbin tool; c bottom surface bobbin tool; d detail of surface appearance
4 Typical surface appearance of friction stir welded 12%Cr alloy steel plate using composite tools

Science and Technology of Welding and Joining 2009 VOL 14 NO 3 249


Thomas et al. Conventional and bobbin FSW of 12%Cr alloy steel

a complete backfilling of pilot hole with hole smaller a root region; b detail of root region
than probe diameter; b partial backfilling of pilot hole 6 Carbon steel pick-up from anvil support shims
made with hole slightly larger than probe diameter
5 Macrosections of backfilled pilot holes
friction stir welds, although these may be further
subdivided for certain materials. These regions are:
(iii) to reverse back the same way that it entered (a (i) unaffected parent material
double welding operation). (ii) material that has been affected by heat, but not
mechanically deformed. This is defined as the
Mechanical properties
heat affected zone (HAZ)
All tensile tests samples showed failure outside the weld (iii) material that has been affected by heat and
region, at parent material strength levels (average UTS: mechanically deformed. This is defined as the
511?5 N mm22). Face, root and side bends achieved thermomechanically affected zone (TMAZ).
180u. With respect to aluminium friction stir welds, the
thermomechanically and dynamically recrystallised
Sacrificial anvil support plates and carbon
regions can normally be differentiated within the weld.
pick-up The 12%Cr steel used in this work exhibits a crystal-
Unlike bobbin stir welding, conventional FSW needs an lographic transformation on cooling, which obscures
anvil support plate of a higher melting point material any evidence of thermomechanical recrystallisation.
than the workpiece material being welded. For conve- Therefore, in the context of this report, the TMAZ
nience, oxidised sacrificial shims are used to prevent will also encompass the central weld region, which
adhesion with the anvil. However, if these sacrificial
shim plates are made from dissimilar steel such as
carbon steel, then significant material pick-up can occur.
Figure 6 shows carbon steel friction stirred into the
12%Cr steel. Such carbon steel contamination within the
12% chromium steel weld can have serious implications
for localised corrosion resistance.
Carbon steel contamination from the support plates
can be avoided using a ceramic anvil material, compa-
tible sacrificial shims plates or bobbin stir welding. A
typical macrosection of a sound weld using a stainless
steel (grade 316L) sacrificial shim plate is shown in
Fig. 7.

Microstructural assessment of 12% chromium


alloy steel friction stir welds
Studies of a number of materials indicate that there are 7 Conventional FSW butt weld in 12 mm thick 12%Cr
three primary microstructural regions to consider in alloy steel with shim plate

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Thomas et al. Conventional and bobbin FSW of 12%Cr alloy steel

(Fig. 8) defined the TMAZ/HAZ boundary, separating


the comparatively large grains observed in the centre of
the weld from the finer grained structure associated with
the HAZ.
Immediately beside the TMAZ/HAZ boundary, a
‘transformed’ HAZ was observed, where untempered
martensite had formed following transformation from
austenite during cooling (visual assessment indicated
ferrite levels up to y40%). Further, away from the
TMAZ, beside the parent metal, a visibly different
‘untransformed’ HAZ was observed, characterised by
the formation of carbides around the original tempered
martensite. It was clear that this ‘untransformed’ HAZ
had not been sufficiently hot to exceed the austenite
transformation temperature, resulting in a similar,
8 Plasticity induced grain flow at boundary between although visibly different microstructure to that of the
TMAZ and HAZ on advancing side parent steel, presumably resulting from some growth of
carbides. The HAZ/parent steel boundary was defined as
cannot be differentiated as a result of crystallographic the point at which carbide precipitation and grain
transformation. coarsening stops.
Therefore, the microstructures of the steels studied in The large delta ferrite grains and reduced martensite
this work has been categorised in this way. fraction present within the TMAZ would be expected to
reduce the toughness exhibited by the welded joint
Conventional friction stir weld (compared with the parent steel). Improvement in
Microexamination of the TMAZ revealed a fairly toughness could be achieved by the use of steel with a
equiaxed microstructure, indicating that recrystallisation lower ferrite factor and possibly by modification of the
had occurred. Recrystallisation within the TMAZ has welding parameters.
also led to an increased ferrite grain size (of the order of
100–150 mm compared with the parent material). The Microstructural assessment of 12% chromium
untempered martensite content, which varied over the alloy steel bobbin friction stir welds
depth of the weld, was visually assessed to lie between 15 Figure 9a highlights the macroscopic appearance of an
and 40% within the TMAZ. etched section taken through the bobbin weld. The main
An abrupt change in structure was observed at the features observed were the TMAZ and HAZ present on
edge of the TMAZ where a plastically deformed zone either side of the weld. The presence of a distinct banded

a etched cross-section through friction stir bobbin weld in 12%Cr steel; b higher magnification view of fine grained ferrite
banding; c higher magnification view of fully ferritic band; d representative microstructure on TMAZ/HAZ boundary on
retreating side of weld
9 Bobbin stir weld

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Thomas et al. Conventional and bobbin FSW of 12%Cr alloy steel

zone can be observed at the right hand side of the image Refractory metal FSW tools
(the advancing side of the weld), where a much finer Initial trials on the FSW of steel were carried out at TWI
grained ferritic–martensitic structure could be observed Ltd in 1997. These were conducted with pure tungsten
(Fig. 9b). The presence of a band of fully ferritic FSW tool. Because this material is brittle at room
material was also observed towards the centre of the temperature, the tool was preheated by an oxyacetylene
weld (Fig. 9c). flame to about 400–500uC, and the 12%Cr steel was
Microexamination of the sample revealed an apparent heated, mainly from close proximity when heating the
similarity in ferrite grain size (estimated to be about tool. This preheat was designed to start the welding at a
100–200 mm diameter) and untempered martensite con- temperature above the ductile–brittle transition tem-
tent (y20%) for both the top and bottom of the weld. perature of the tungsten. However, the ductile–brittle
This suggested that the level of heat input was similar for transition temperature of tungsten can be decreased
both sides of the weld. This would be expected for a below room temperature by the addition of other
bobbin weld, as the locations where the shoulders of the elements such as rhenium or lanthanum oxide. All welds
tool contact both top and bottom surfaces of the plate made during the trial were carried out without any
will generate heat, resulting in higher temperatures at the preheat. The investigation has demonstrated that dif-
surfaces and coarsening of the delta ferrite grains. ferent types of refractory materials are easily secured by
The TMAZ/HAZ region of the weld is illustrated in a matching taper under extremely hot welding condi-
Fig. 9d, where a transition from the comparatively large tions while subject to high torsional loads. Used in
grained ferrite and untempered martensite structure of combination, refractory materials can achieve smoother
the TMAZ to the fine grained of the parent material can weld surfaces while still providing good coupling with
be observed. Beside the TMAZ/HAZ boundary, the extremely hot plasticised weld metal.
transition is characterised by a reduction in ferrite grain
size to that of the parent material. The HAZ itself Self-reacting bobbin FSW
consisted of fine grained ferrite, of a similar grain size to Bobbin tools are similar to conventional FSW tools that
the parent material; however, it appeared that the struc- are driven from one side in that the tool behaves as a
ture of the untempered martensite was better defined rotating cantilever; nevertheless, they differ in certain
within the HAZ, illustrating that some transformation aspects as follows.
had occurred, although no grain growth was observed. There are a number of features that make bobbin stir
This is a similar result to that observed previously for welding of steel attractive. Two shoulders provide
the ‘conventional’ friction stir weld of 12%Cr steel. sufficient heat generation from both sides of the work-
The origin of the fine grained microstructural banding piece without any heat loss through the anvil support
on the advancing side of the weld is not clear. There plate. Containment of reactive forces within the tool
appear to be alternating bands of martensite and ferrite itself means that compressive deformation (squashing)
within this part of the sample; the untempered marten- of the probe does not occur. The probe of a conven-
site volume fraction is much higher, around 50%, on this tional FSW tool is subjected to multiaxial forces
side of the joint, which is attributable to either dif- comprising torsion, bending and compression. The
ferences in composition, deformation (and hence degree probe of a single sided bobbin tool is also subjected to
of recrystallisation) or temperature. Significant variation multiaxial forces comprising of comparatively higher
in composition seems unlikely. Given that it is present levels of torsion and bending, but only tensile forces
on the advancing side of the weld, it would seem likely rather than compressive forces are applied through the
that differences in deformation of the material during probe.
welding have resulted in differing degrees of recrystalli- The use of a tapered probe for both conventional and
sation, or that a temperature gradient existed across the bobbin stir welding provides for a more uniformly
weld. The differing phase balance on the two sides stressed tool, which displaces substantially less material
suggests that different peak temperatures were attained during welding than a cylindrical pin type probe.
and hence supports the concept of a temperature Furthermore, the use of a tapered probe for the bobbin
gradient across the weld. tool enables a proportional reduction in the diameter of
The previous work conducted on a conventional the lower shoulder of the bobbin tool.
friction stir weld highlighted a small fully ferritic band Reduction in the lower shoulder diameter results in
within the TMAZ. Therefore, it is possible that the lower frictional contact and resistance, therefore less
geometry of the bobbin is altering both the material flow torque and bending moment on the tool. The additional
(a possible bifurcated flow), and heat input, in a manner frictional contact provided by the lower shoulder and
that is conducive to the formation of this banded the absence of a backing anvil, which acts as a heat sink,
structure. means that the operating temperature will be higher
than that of similar conventional welds. Tool design and
Discussion process conditions will need to be adjusted to allow the
welding travel speed to be increased benefiting from this
Friction stir weldability trials additional heat generation. Both adaptive and fixed gap
The work reported is encouraging as it demonstrates self-reacting techniques will need to be developed to
that FSW can be applied successfully to steel plate. FSW meet the challenges of ferrous base materials.
has produced sound single sided welds in 12 mm thick Bobbin welds essentially eliminate partial penetration,
12%Cr steel plate at a welding travel speed of lack of penetration or root defects. Preliminary trials
2?5 mm s21. Preliminary bobbin stir trials also show have also shown that lap welds produced by the bobbin
promise with 8 mm thick 12% chromium alloy steel technique have fewer problems with the adverse
plate welded at 1?25 mm s21. orientation of the notch at the edge of the weld.

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Thomas et al. Conventional and bobbin FSW of 12%Cr alloy steel

Conclusions References
Based on the results and discussions given above, the 1. W. M. Thomas, E. D. Nicholas, J. C. Needham, M. G. Murch,
following conclusions can be made: P. Temple-Smith and C. J. Dawes: ‘Improvements relating to
friction welding’, European Patent Specification 0615480B1.
1. Successful friction stir welds have been produced
2. K. J. Colligan and J. R. Pickens: in ‘Friction stir welding and
in 12 mm and 8 mm thick 12% chromium alloy steel. processing III’, (ed. K. V. Jata et al.), 161–170; 2005, Warrendale,
2. The feasibility of using self-reacting (bobbin) FSW PA, TMS.
for 12% chromium alloy steel has been demonstrated 3. M. Skinner and S. R. L. Edwards: Mater. Sci. Forum, 2003, 426–
and the resulting microstructures have been evaluated. 432, 2849–2854.
4. F. Marie, D. Allehaux and B. Esmiller: Proc. 5th Int. Symp. on
3. The use of a matching taper drive coupling to ‘Friction stir welding’, Metz, France, September 2004, TWI,
provide secure combinations of different refractory Session 01, process developments, paper 1.
materials for composite tools has been demonstrated 5. G. Sylva and R. Edwards: Proc. 5th Int. Symp. on ‘Friction stir
for conventional and self-reacting FSW tools. welding’, Metz, France, September 2004, TWI, Session 01, process
developments, paper 2.
6. D. Otsuka and Y. Sakai: Proc. 7th Int. Symp. on ‘Friction stir
Acknowledgement welding’, Awaji Island, Japan, May 2008, TWI, Session 8A, process
control/3, paper 1.
The authors are grateful for the support and contribu- 7. F. Marie, B. Guerin, D. Deloison and D. Aliaga: Proc. 7th Int.
tions provided by Dr P. Woollin, Dr I. M. Norris and Symp. on ‘Friction stir welding’, Awaji Island, Japan, May 2008,
Mr C. E. D. Rowe (Cedar Metals Ltd). TWI, Session 8A, process control/3, paper 2.

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