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Article history: The Weibull modulus, a material parameter describing the size effect of brittle material, of high-
Received 2 February 2019 performance fiber-reinforced concretes (HPFRCs) was investigated under compression and flexure. The
Received in revised form 30 May 2019 compressive specimens were as follows: 70.7 70.7 70.7 mm (cube), 100 100 100 mm (cube),
Accepted 19 July 2019
150 150 150 mm (cube), Ø100 200 mm (cylinder), Ø150 300 mm (cylinder). The bending speci-
mens were as follows: 40 40 120 mm, 100 100 300 mm and 150 150 450 mm. For each size
or shape, two HPFRCs having different fiber content were examined as follows: HPFRC1 having no fiber
Keywords:
and HPFRC2 containing 1.0% macro hooked fibers blended with 0.5% micro smooth fibers by volume.
High-performance
Size effect
There was a clear size effect on the compressive and bending parameters for both the investigated
Weibull HPFRCs. The derived Weibull modulus of the investigated HPFRCs for the mechanical parameters varied
Brittleness from 1.33 to 8.74. Furthermore, the correlation between the bending and compressive strengths of the
Hybrid fiber two HPFRCs and their conversion factors for various sizes and shapes of the compressive specimens were
explored.
Ó 2019 Elsevier Ltd. All rights reserved.
https://doi.org/10.1016/j.conbuildmat.2019.07.234
0950-0618/Ó 2019 Elsevier Ltd. All rights reserved.
744 D.-L. Nguyen et al. / Construction and Building Materials 226 (2019) 743–758
Table 1
Composition of mortar matrices.
HPFRC
Cement (Type 3) Silica fume Silica sand Fly ash Superplas-ticizer Water Water curing
0.80 0.07 1.00 0.20 0.04 0.26 25 °C/28 days
UHPFRC
Cement (Type 1) Silica fume Silica sand Silica powder Superplas-ticizer Water Water curing
1.00 0.25 1.10 0.30 0.067 0.20 90 °C/3 days
the lower capillary attraction of water [11]. The rest of the water representative ductile materials exhibiting constant failure
around the particle after hydrating will vaporize and originate strengths regardless of the specimen size. The size effect of brittle
the porosity inside the concrete. These reasons help decrease the materials on strength has been mainly responsible for the
air voids embedded in the concrete and produce the very densified following trend: the bigger-sized specimen produces lower
microstructures of HPFRCs and UHPFRCs. Even though HPFRCs has
demonstrated lower compressive strength than UHPFRCs, HPFRCs
has still been encouraged to apply in civil infrastructure owing to
its superior tensile properties and simpler curing, i.e, HPFRCs can
be cured in normal condition with temperature ranging from 20
to 30 degrees Celsius, whereas UHPFRCs often requires special
treatments in production such as high temperature curing, high
pressure, extensive vibration [3]. In addition, HPFRCs using fly
ash, one of waste products from a coal-fired power plant, will help
increase fly ash utilization and environmentally friendly impacts.
Strength dependences on size of concretes or structural mem-
bers made from concrete have been reported in many studies
[11–21]. Also, high-strength concrete was reported to produce a
clear size and shape effect on compressive strength [22]. This
natural property is entirely dissimilar to metals, which are
Fig. 1. Characteristic compressive and flexural behavior of HPFRC with their main
parameters. Fig. 3. Photos of two steel fibers used in their hybrid system.
D.-L. Nguyen et al. / Construction and Building Materials 226 (2019) 743–758 745
strength. Consequently, the phenomenon of size effect highly advanced material may demonstrate its size effect on the mechan-
affects the reliability and safety factor of construction, thus it ical properties. Few studies [23–27] reported the size effect on
should be considered noticeably in design work, which has been fiber-reinforced concrete. According to [23], HPFRCs produced a
primarily based on the reported data from small specimens tested significant size effect on the bending response but an insignificant
in laboratories. size effect on the tensile response of HPFRCs. The engineered
Although the ductility of HPFRCs or UHPFRCs could be cement composites were evaluated to produce an unimportant size
improved by embedded fibers bridging the tiny cracks and devel- effect on bending in comparison with reinforced concrete speci-
oping a work hardening behavior, it is still in question whether this mens [24]. The significant size effect on bending resistance of
Table 2
Properties of fibers.
Fiber type Diameter (mm) Length (mm) Aspect ratio (L/d) Density (g/cc) Tensile strength (MPa) Shape
Macro fiber 0.5 35 70 7.9 >1200 circular, hooked
Micro fiber 0.2 13 65 7.9 >2500 circular, smooth
a) Compression b) Bending
Fig. 5. Test setup for compression and bending test.
746 D.-L. Nguyen et al. / Construction and Building Materials 226 (2019) 743–758
Table 3
Compressive resistances of the investigated HPFRCs.
b) What model can be used to explain the size effect on com- a load-drop response with brittle failure revealed by the large
pression and flexure? Under direct tension, a weakest-link in a explosion. In this research, the peak ultimate stress and its corre-
chain was modeled for the size effect on tensile resistance [35]. sponding strain were notated as rcu and ecu ; respectively, while
The chain breaks when the weakest element fails, and the more the area under the compressive stress versus strain response curve
elements in the chain, the higher probability containing the defect prior to the peak was derived as the compressive toughness,
element, which is the weakest element, will result an easy break notated T cu . The rcu can be obtained by dividing the maximum
failure. However, failure mechanism in compression or flexure is measured force (P max ) by the cross-sectional area. Under direct ten-
dissimilar to that in tension, and building new models is needed sion and bending, the work hardening behaviors of HPFRC, com-
to explain the size effect on them. monly called strain hardening in tension or deflection hardening
c) For normal concrete, direct or indirect tensile strength is in bending, can be generated with a suitable type and an appropri-
strongly dependent upon compressive strength. Practically, the ate volume content of added fibers [38,39]. The work hardening
relationship between the indirect tensile strength and cylin- behavior refers to the increase of stress (or force) after the first
der compressive strength has been recommended as square root s- crack and is accompanied by multiple tiny-cracks produced by
cale according to ACI 318 [36]. For HPFRC, the relationship embedded fibers bridging the cracks. The work hardening response
between the bending strength and the compressive strength is is one of the most superior structural properties of HPFRC because
identical to that of conventional concrete? this mechanism can result its high ductility, high toughness, and it
Motivated by those questions, the authors carried out the can warn the critical state of structural members before collapsing.
experimental research which focused on the brittleness of HPFRCs A typical deflection hardening response curves of HPFRC is illus-
by mean of the Weibull modulus in both compression and bending. trated in Fig. 1b. In this figure, the limit of proportionality, notated
The data in this paper was partially based on the master thesis [37] LOP, is at the end of the linear elastic portion, while the modulus of
of the last author, and the first author was the thesis advisor. The rupture, notated MOR, is at the peak bending stress after the first
main target of this research was to explore the brittleness of crack. The condition for deflection hardening behavior is that the
HPFRCs causing size effect on the compressive and bending resis- bending strength at MOR, fMOR, is greater than or equal to the bend-
tance of HPFRCs. There are four objectives in this research as fol- ing stress at LOP, fLOP. The area under the bending stress-
lows: (1) to investigate the compressive and bending response of normalized deflection relationship curve prior to the peak is
HPFRCs, (2) to explore the relationship between bending strength derived as the flexural toughness, notated as TMOR. The normalized
and compressive strength, (3) to discover the Weibull modulus in deflection (d=S) is obtained by dividing the midspan deflection by
compressive and bending failure of HPFRCs, and 4) to propose the length of span, while the bending stress, notated as f, under
models for explaining the size effect in compression and bending. the three-point bending test (3PBT), can be computed by Eq. [1].
The relationship between the moment, loading force, and bending
strength at MOR is given by Eq. [2]:
2. Characteristic parameters in mechanical responses of HPFRC
PS
f ¼ 1:5 2
ð1Þ
Like other concretes, HPFRC produces significantly bh
stronger resistance in compression than in tension. The compres- 2
sive behavior of HPFRCs often demonstrates a quasi-linear PMOR S bh
MMOR ¼ ¼ f MOR ð2Þ
response prior to the peak of curve, as shown in Fig. 1a, and then 4 6
Table 4
Compressive parameters of the investigated HPFRCs.
Specimen type (Specimen name) Compressive strength, rcu Strain capacity, ecu (%) Compressive toughness,
(MPa) T cu (MPa)
HPFRC1 HPFRC2 HPFRC1 HPFRC2 HPFRC1 HPFRC2
70.7 70.7 70.7 (CU070) 84.49 98.07 0.34 0.33 0.153 0.163
80.41 114.36 0.33 0.37 0.147 0.221
97.44 117.32 0.39 0.44 0.197 0.312
Average value 87.45 109.92 0.35 0.38 0.166 0.232
Standard deviation 8.89 10.37 0.03 0.06 0.028 0.075
100 100 100 (CU100) 79.94 99.06 0.31 0.33 0.133 0.176
79.40 101.01 0.27 0.3 0.112 0.146
90.80 91.63 0.3 0.31 0.141 0.138
Average value 83.38 97.23 0.29 0.31 0.129 0.153
Standard deviation 6.43 4.95 0.02 0.02 0.015 0.020
150 150 150 (CU150) 78.09 97.15 0.25 0.32 0.098 0.167
71.63 83.56 0.28 0.24 0.116 0.103
68.26 91.23 0.24 0.3 0.084 0.149
Average value 72.66 90.65 0.26 0.29 0.100 0.140
Standard deviation 5.00 6.81 0.02 0.04 0.016 0.033
Ø100 200 (CY100) 71.05 81.97 0.24 0.35 0.141 0.165
73.85 81.56 0.28 0.29 0.105 0.117
70.17 73.78 0.22 0.3 0.078 0.119
Average value 71.69 79.10 0.25 0.31 0.108 0.13
Standard deviation 1.92 4.61 0.03 0.03 0.031 0.027
Ø150 300 (CY150) 61.71 70.12 0.19 0.29 0.041 0.118
68.75 75.71 0.24 0.3 0.015 0.116
71.34 83.44 0.26 0.2 0.080 0.057
Average value 67.27 76.42 0.23 0.26 0.046 0.10
Standard deviation 4.98 6.69 0.04 0.06 0.033 0.034
A testing plan was designed to investigate the size effect on the compressive
and bending response of the HPFRCs, as described in the flowchart of Fig. 2. As
described in Fig. 2, there are five series of the compressive specimens with different
sizes and shapes as follows: cube 70.7 70.7 70.7 mm (named CU070), cube
100 100 100 mm (named CU100), cube 150 150 150 mm (named CU150),
cylinder Ø100 200 mm (named CY100), cylinder Ø150 300 mm (named
CY150). Under bending, there are three series of bending specimens with identical
shapes but different sizes as follows : 40 40 120 mm (named BE040),
100 100 300 mm (named BE100) and 150 150 450 mm (named BE150).
Two types of HPFRCs were investigated for each series, and they had the same mor-
tar matrix but different fibers added: HPFRC1 containing no fiber whereas HPFRC2
containing 1% macro steel hooked fibers blended with 0.5% micro smooth fibers by
volume.
The photos of steel hooked fibers and smooth fibers mixed in HPFRC2 are shown
in Fig. 3, while the photos of componential materials manufacturing HPFRCs are
shown in Fig. 4. Table 1 provides the composition and Table 2 provides the proper-
(a) Size and geometry effect on ties of the fibers used. The hooked and smooth fibers had their aspect ratios of
compressive strength 35 mm/0.5 mm and 13 mm/0.2 mm, respectively. All componential materials were
mixed by laboratory mixer having 150-L volume capacity. The dry componential
materials including cement, silica sand, fly ash, silica fume were firstly mixed for
10 min. Then water was added. Next, super plasticizer was regularly added and
mixed for 15–20 min. When the mortar showed appropriate flowabiliy and viscos-
ity, the micro fibers then the macro fibers were step by step distributed by hand and
mixed for about 5–10 min (for HPFRC2 with hybrid steel fibers). Next, the mixture
was cast in specimen molds, then vibrated slightly for minimizing the air foams
embedded inside the poured specimen. After that, the poured specimens were cov-
ered using plastic sheets and placed in a laboratory room prior to demolding for one
day at room temperature. The specimens were cured in water for 28 days at a tem-
perature of 22–29 °C after demolding. Later, the specimens were moved out of the
curing water then dried under laboratory temperature. The specimens were exper-
imentally examined at the age of 30–34 days.
and the cylinders, the size effect was not clear, e.g., the compres- cylinder specimen. Fig. 9 shows the compressive stresses versus
sive strength of the CU150 was higher than that of the CY100 strain response curves of the HPFRCs. As displayed in Fig. 9, regard-
despite having a bigger size than the CY100, as described in less of the specimen types, the ascending portions up to the peak
Fig. 7(a). There was a central zone with no lateral stress in the stresses were almost linear and rather consistent with each other.
cylinder specimen, whereas the cube specimen had lateral stress Beyond the peak stresses, the descending portions did not produce
throughout its height, as illustrated in Fig. 8 [40]. This was consid- a sudden drop load like those of the UHPFRCs [41]. The lower den-
ered as the main cause of the low compressive strength in the sity of the HPFRC may cause a difference of failure behavior after
a
a
Centeral zone unaffected
by lateral stress
H=2d
30o
a
0.268d
30o
Cube specimen affected by lateral
stresses throughout its height
d
Fig. 8. Ratio of height to diameter effecting on concrete strength of cylinder and cube specimen.
Table 5
Bending resistances of the investigated HPFRCs.
Table 6
Bending parameters of the investigated HPFRCs.
Specimen type (Specimen name) Bending strength, f MOR (MPa) Normalized deflectiondMOR =S Bending toughness, T MOR
(%) (MPa)
HPFRC1 HPFRC2 HPFRC1 HPFRC2 HPFRC1 HPFRC2
40 40 120 (BE040) 9.40 34.17 0.68 0.78 0.032 0.124
10.35 37.09 0.72 0.78 0.037 0.129
11.48 39.23 0.79 0.76 0.047 0.134
Average value 10.41 36.83 0.73 0.77 0.039 0.129
Standard deviation 1.04 2.54 0.06 0.01 0.008 0.005
100 100 300 (BE100) 7.42 21.18 0.49 0.88 0.019 0.101
7.42 18.97 0.55 0.96 0.019 0.110
7.36 21.18 0.57 0.83 0.025 0.107
Average value 7.40 20.44 0.54 0.89 0.021 0.106
Standard deviation 0.04 1.28 0.05 0.06 0.003 0.005
150 150 450 (BE150) 2.71 14.30 0.41 0.43 0.005 0.035
4.12 15.33 0.48 0.45 0.008 0.038
3.63 15.90 0.57 0.40 0.012 0.035
Average value 3.49 15.17 0.48 0.43 0.009 0.036
Standard deviation 0.71 0.81 0.08 0.02 0.004 0.002
HPFRCs were observed, although the size effect on normalized significantly enhanced owing to the addition of discrete fibers in
deflection of HPFRC2 was not particularly clear. the plain mortar matrix, which can generate a favorable achieve-
ment from the fiber-matrix bond and the fiber pullout
4.3. Sensitivity of size to the compression and bending parameters of [6,26,27,38]. The square root scale between the bending strength
the investigated HPFRCs and the compressive strength of HPFRCs has often been reported
[44,45] although some other researchers suggested a power rela-
In order to discover the most sensitive mechanical parameter of tionship between them [46,47]. In this research, the authors used
investigated HPFRCs, a linear relationship between normalized the square root relationship and explored the coefficient of MOR,
mechanical parameter and normalized size was built for each ser- a, as given in Eq. [4] for the HPFRCs.
ies, as illustrated in Fig. 13. In this figure, the relationship with stif- qffiffiffiffi
0
fer slope demonstrates a higher sensitivity. In this study, the f r ¼ 0:63 f c ð3Þ
normalized size and the normalized mechanical parameter of each
shape were defined as the ratio of the value of the smallest speci- qffiffiffiffi
0
men to that of the largest specimen (size of 150 mm: CU150 for f MOR ¼ a f c ð4Þ
cube, CY150 for cylinder and BE150 for bending prism). The
0
mechanical parameters included rcu ; ecu and T cu under compres- where f c is the compressive strength using a cylinder specimen of
sion, f MOR ; dMOR =S and T MOR under bending. Table 7 and Fig. 14 pro- 150x300 mm, f r and f MOR are the bending strength of normal con-
vide the values of all the mechanical parameters and the derived cretes and HPFRCs, respectively.
slopes indicating their sensitivity. For both HPFRC1 and HPFRC2, Table 8 provides the derived values of a for both HPFRC1 and
the toughness was the most sensitive mechanical parameter in HPFRC2 according to various types of tested bending specimens.
both compression and bending, and their ranking was The a of HPFRC2 were derived as 1.74 (BE150), 2.34 (BE100) and
T cu > ecu > rcu in compression, and T MOR > f MOR > dMOR =S in bending. 4.21 (BE040), and these values were much higher than that of nor-
In the same HPFRC, the bending specimen was more sensitive than mal concrete with a = 0.63. Compared with the HPFRC2, the
the cube, and the cylinder specimen was observed to produce a HPFRC1 produced a lower a: 0.43 (BE150), 0.90 (BE100) and 1.27
lowest sensitivity. Generally, the HPFRC1 was more sensitive than (BE040), and these values were also different from that of normal
the HPFRC2. The toughness was the most sensitive mechanical concrete, although the a range of HPFRC1, from 0.43 to 1.27, con-
parameter because it was affected by the size effect on strength tained a value of 0.63. The enhancements of the bending strength
in addition to the size effect on strain (or normalized deflection). and the square root of compressive strength of the HPFRCs were
Besides, the bending specimen contained a compressive zone and scattered and very dependent upon the investigated HPFRC, i.e.,
a tensile zone, which was size-dependent [23]. The combination dependent upon the embedded fibers.
of their size effects could result the more sensitivity than the com-
pressive specimen. Finally, the fact that HPFRC2 was mixed by 4.5. Conversion factors with different sizes and shapes for the
hybrid steel fibers helped this material become more ductile to compressive specimens of the HPFRCs
failure, i.e., the crack bridging of the embedded fibers could effi-
ciently prevent quick crack propagation. This is the possible reason Up until now, there have been two main shapes for the com-
that leads to less brittleness of HPFRC2. pressive specimens, including the cube and cylinder, according to
the testing standards applied. The cylinder specimen of
4.4. Relationship between the bending strength and compressive 150 300 mm has been used mainly in Australia, Canada, United
strength of the HPFRCs States, while the cube specimens with sizes of 150 mm and
100 mm have been used commonly in Europe [48]. Therefore, the
For normal concrete, there is a strong correlation between the demand for a conversion of compressive strength with various
modulus of rupture and the compressive strength, which is com- sizes and shapes of specimens is very high, even for HPFRCs. In this
monly described under the square root proportionality in some study, the conversion factors, b, of the tested compressive speci-
codes, e.g., ACI 318 [36] provides Eq. [3] for this type of relation- mens were based on the cube specimens of 150 mm (CU150).
ship. For HPFRCs, the direct tensile strength or indirect tensile is Eq. [5] was used to convert the compressive strengths of all the
752 D.-L. Nguyen et al. / Construction and Building Materials 226 (2019) 743–758
tested series, and the conversion factors are summarized in Table 9. rCU150
b¼ cu
ð5Þ
As shown in Table 9, the conversion factors for HPFRC2 were the rSpe:
cu
type
where m and V E are the Weibull modulus and the effective volume
of the specimen, respectively. The effective volume of the specimen
was derived based on the loading condition, while the Weibull
modulus was considered a material parameter notifying a size
effect degree.
As described in Eq. [6], if two specimens have effective vol-
umes: V E1 > V E2 , they will produce their strengths: S1 > S2 . A mate-
rial with a greater value of m implies less brittle; and a metal or
ductile material has an infinite value of m. The probability of failure
Pf ðSÞ, in Weibull’s theory, is given in Eq. [7] by Weibull [33]. This
equation could be written into [8] using a logarithmic function.
m
S
Pf ðSÞ ¼ 1 exp V E ð7Þ
S0
( " #)
1
In ln
¼ m lnðSÞ þ lnðV E Þ m lnðS0 Þ ð8Þ
(b) Size effect on normalized deflection at MOR 1 Pf ðSÞ
yi ¼ mxi þ b ð9Þ
where S0 and S are the scale parameter and the maximum failure
strength, respectively. P f ðSÞ is i=ðn þ 1Þ, n is the number of analysed
specimens while i is the order of failure strength:
S1 S2 ::: Si ::: Sn .
Using the least square method on the linearized regression
model given by Eq. [9], the value of the Weibull modulus, m, can
n h io
be estimated using Eq. [10] with the data: yi ¼ ln ln ð1i=ðnþ1Þ 1
Þ
P
and the corresponding xi ¼ lnðSi Þ, the average value yav ¼ 1n i yi
P
and xav ¼ 1n i xi .
P
i ½ðyi
yav Þðxi xav Þ
m¼ P 2
½10
i ðxi xav Þ
Table 7
Derived slope to discover the sensitivity of normalized size to the normalized mechanical parameters (referred to Figs. 13, 14).
The derived slope are in brackets while the normalized mechanical parameters are outside.
754 D.-L. Nguyen et al. / Construction and Building Materials 226 (2019) 743–758
Table 9
Conversion factors with different sizes and shapes for the compressive specimen.
specimen
CU070 CU100 CU150 CY100 CY150
HPFRC1 CU150 0.83 0.87 1.00 1.01 1.08
HPFRC2 CU150 0.82 0.93 1.00 1.15 1.19
Normal concrete CU150 0.85 0.91 1.00 1.17 1.20
5.3. Proposed models for size effect on compression and bending of the
HPFRCs
6. Conclusions
Fig. 15. Using the least-squares method to obtain the Weibull modulus of the Fig. 16. Weibull distribution of the compressive parameters.
compressive parameters.
756 D.-L. Nguyen et al. / Construction and Building Materials 226 (2019) 743–758
Table 10
Weibull modulus of the investigated HPFRCs.
Acknowledgments
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