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  • Praktikum Biodiesel

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    putri wahyuni
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    The document contains data from experiments on biodiesel production through transesterification. It includes tables of raw materials used, measurements taken over time (15, 30, 45, 60 minutes), stoichiometric calculations, and graphs plotting conversion percentage, yield percentage, and other variables against reaction time. The results show that longer reaction times of 45-60 minutes led to higher conversion percentages and yield percentages of around 42-46% compared to shorter reaction times of 15-30 minutes with 35-38% yields.

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    PRAKTIKUM BIODIESEL

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    The document contains data from experiments on biodiesel production through transesterification. It includes tables of raw materials used, measurements taken over time (15, 30, 45, 60 minutes), stoichiometric calculations, and graphs plotting conversion percentage, yield percentage, and other variables against reaction time. The results show that longer reaction times of 45-60 minutes led to higher conversion percentages and yield percentages of around 42-46% compared to shorter reaction times of 15-30 minutes with 35-38% yields.

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    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
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    18 views8 pages

    Praktikum Biodiesel

    Uploaded by

    putri wahyuni
    The document contains data from experiments on biodiesel production through transesterification. It includes tables of raw materials used, measurements taken over time (15, 30, 45, 60 minutes), stoichiometric calculations, and graphs plotting conversion percentage, yield percentage, and other variables against reaction time. The results show that longer reaction times of 45-60 minutes led to higher conversion percentages and yield percentages of around 42-46% compared to shorter reaction times of 15-30 minutes with 35-38% yields.

    Copyright:

    © All Rights Reserved
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    of 8

    Data Pendukung Data Literatur

    BM
    Komponen (gr/ml)
    t (menit) Massa Pikno isi t air t mix (gr/mol)
    15 20.804 0.49 2.28 Minyak Nabati 284.39 0.915
    30 20.7602 0.49 2.22 Metanol 32.04 0.792

    45 20.72 0.49 2.01


    FAME (Biodiesel) 285.2 0.85
    60 20.686 0.49 1.89 Gliserol 92 1.26

    Data Pengamatan
    Volume Massa Kadar Massa biodiesel murni
    t(menit) biodiesel (gr/ml) biodisel (mm2/s) biodisel
    (ml) (gr/) (x1)
    15 120 0.901 108.0708 3.771 0.77 83.215
    30 128 0.896 114.7149 3.654 0.78 89.478
    45 135 0.892 120.4457 3.294 0.832 100.211
    60 140 0.889 124.4306 3.085 0.863 107.384

    Stokiometri Pembuatan Biodiesel


    T= 15 menit

    m 0.824 2.47 - -
    r 0.097 0.292 0.097 0.292
    s 0.727 2.18 0.097 0.292

    %Konversi =
    x 100% = 35.41

    %Yield =
    x 100% 35.512

    T= 30 menit

    m 0.824 2.47 - -
    r 0.105 0.314 0.105 0.314
    s 0.719 2.16 0.105 0.314
    %Konversi =
    x 100% = 38.08

    %Yield =
    x 100% 38.185

    T = 45 Menit

    m 0.824 2.47 - -
    r 0.117 0.351 0.117 0.351
    s 0.707 2.12 0.117 0.351

    %Konversi =
    x 100% =
    42.644

    %Yield =
    x 100%
    42.765

    T = 60 menit

    m 0.824 2.47 - -
    r 0.126 0.377 0.126 0.377
    s 0.698 2.10 0.126 0.377

    %Konversi =
    x 100% =
    45.696

    %Yield =
    x 100%
    45.826

    Grafik Hubungan antara Waktu(me


    50.00
    45.00
    Waktu Konversi 40.00
    15 35.41 35.00
    Konversi(%)

    30 38.08 30.00
    45 42.644 25.00
    60 45.696 20.00
    15.00
    10.00
    5.00
    0.00
    10 20 30 4
    Waktu(M
    20.00

    Ko
    15.00
    10.00
    5.00
    0.00
    10 20 30 4
    Waktu(M

    Waktu Yield Grafik Hubungan Waktu(men


    15 35.51 50.00
    30 38.18 45.00
    45 42.765 40.00
    60 45.826 35.00
    30.00

    Yield(%)
    25.00
    20.00
    15.00
    10.00
    5.00
    0.00
    10 20 30
    Waktu(M

    Waktu Nilai -LN(1-XA) (1-xa) Grafik Hubungan Waktu(men


    15 -0.437 0.65 0.000
    30 -0.479 0.62 10 20 30 4
    -0.100
    45 -0.556 0.57
    60 -0.611 0.54 -0.200
    –Ln(1-Xa)
    -0.300

    -0.400

    -0.500

    -0.600

    -0.700
    Waktu (M

    Waktu 1/n Grafik Hubungan Waktu(m


    15 0.73
    0.73
    30 0.72
    0.73
    45 0.707 0.72
    60 0.698 0.72
    1/n(mol-1)

    0.71
    0.71
    0.70
    0.70
    0.69
    0.69
    0.68
    10 20 30 4
    Waktu (M
    0.71

    1/n(m
    0.70
    0.70
    0.69
    0.69
    0.68
    10 20 30 4
    Waktu (M
    (mm2/s)

    19.98
    0.55
    2.3
    0.96

    Berat Pikno Kosong 11.7981


    Massa biodiesel murni
    Berat pikno isi aquadest 21.7981
    Volume Pikno 10
    aquadest 0.9

    Perb. Minyak methanol = 2:1 Volum total=300ml

    Mol Metanol : 2.47

    Massa metanol = Rho x V = 79.2

    M FAME sisa 83.21452

    Mol FAME = 0.292

    Massa Trigliserida = Mol x BM = 234.329

    Mol Metanol : 2.47

    Massa metanol = Rho x V = 79.2


    M FAME sisa 89.478

    Mol FAME = 0.314

    Massa Trigliserida = Mol x BM = 234.329

    Mol Metanol : 2.47

    Massa metanol = Rho x V = 79.2

    M FAME sisa 100.2108

    Mol FAME = 0.351

    Massa Trigliserida = Mol x BM = 234.329

    Mol Metanol : 2.47

    Massa metanol = Rho x V = 79.2

    M FAME sisa 107.384

    Mol FAME = 0.377

    Massa Trigliserida = Mol x BM = 234.329

    n antara Waktu(menit) terhadap Konversi(%)

    20 30 40 50 60 70
    Waktu(Menit)
    20 30 40 50 60 70
    Waktu(Menit)

    bungan Waktu(menit) terhadap Yield(%)

    20 30 40 50 60 70
    Waktu(Menit)

    ungan Waktu(menit) dengan –Ln(1-Xa)


    20 30 40 50 60 70

    Waktu (Menit)

    Hubungan Waktu(menit) dengan 1/n

    20 30 40 50 60 70
    Waktu (Menit)
    20 30 40 50 60 70
    Waktu (Menit)

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