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  • CHM580-NMR Assignment Ans

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    tirah
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    The document provides guidance on analyzing an NMR assignment, including functional group identification from FTIR, molecular weight from mass spectrum, proton assignments from 1H NMR including chemical shifts, splitting patterns, neighboring protons, and notations, and carbon assignments from 13C NMR including chemical shifts and notations. It suggests the compound has a carbonyl group, molecular weight of 132 g/mol, and proposes the structure.

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    The document provides guidance on analyzing an NMR assignment, including functional group identification from FTIR, molecular weight from mass spectrum, proton assignments from 1H NMR including chemical shifts, splitting patterns, neighboring protons, and notations, and carbon assignments from 13C NMR including chemical shifts and notations. It suggests the compound has a carbonyl group, molecular weight of 132 g/mol, and proposes the structure.

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    127 views2 pages

    CHM580-NMR Assignment Ans

    Uploaded by

    tirah
    The document provides guidance on analyzing an NMR assignment, including functional group identification from FTIR, molecular weight from mass spectrum, proton assignments from 1H NMR including chemical shifts, splitting patterns, neighboring protons, and notations, and carbon assignments from 13C NMR including chemical shifts and notations. It suggests the compound has a carbonyl group, molecular weight of 132 g/mol, and proposes the structure.

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    © All Rights Reserved
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    CHM580: NMR Assignment

    Guided Ans:

    FTIR Mass Spectrum

    Functional group presence: Molecular weight: 132 g/mol ….. (1)

    C=O ….. (1)

    1
    H NMR

    # Proton ɖ split Neighboring H Notation


    3 ~ 2.1 ppm s 0 a
    2 ~ 2.6 ppm d 1 b
    6 ~ 3.4 ppm s 0 c
    1 ~ 4.8 ppm t 2 d
    (4)
    13
    C NMR

    Type C ɖ Notation
    -CH3 ~ 30 ppm a
    H-C-H ~ 45 ppm b
    -CH3 ~ 52 ppm c
    C-H ~ 100 ppm d
    C ~ 208 ppm e
    (2)

    Structure:

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