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212 Journal of the American Ceramic Society-Rose Vol. 69, No.

References York, I9Sh


‘“J.R. Rice, “A Path Independent Integral and the Approximate Analysis of Strain
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IL. R. F, Rose and M. V. Swain, “Two K Curves for Partially Stabilized Zirconia”; “B. Budiansky and J. R. Rice, “Conservation Laws and Energy-Release Rates,” J .
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*M. V. Swain, “R-Curve Behaviour of Magnesia Partially Stabilized Zirconia and W.E. Eshelby, “Elastic Inclusions and Inhomogeneities”; pp. 87-140 in Progress
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conia”: this issue, pp. 173-80. bridge University Press, Cambridge, 1975.
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formation Toughened Ceramics”; to he published in J. Am. Ceram. SOC. Plane Extension and Plate Bending Problem,” J . Appl. Mech., 329, 306-12 (1962).
5N.I. Muskhelishvili, Some Basic Problems of the Mathematical Theory of Elas- I5R. M. McMeeking and A. G . Evans, “Mechanics of Transformation Toughening
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J. Am. Cerurn. SOC., 69 [3] 212-14 (1986)

Effective Fracture Toughness of Microcracked Materials


L.R.F. ROSE
Aeronautical Research Laboratories, Melbourne 3001, Australia

Explicit analytical formulas are derived for the stress intensity


factors at the tips of a main crack and of a microcrack for the
two-dimensional case of a collinear microcrack. This config-
uration is used to derive an estimate of the toughness de- where K N denotes the nominal (mode I) stress intensity factor. The
gradation due to microcracks linking up with an advancing angular dependence for each stress component is given in Ref. 4.
main crack. The implications of this estimate for theoretical The problem is to determine the resulting stress field when a
predictions of the toughening due to stress-induced micro- collinear microcrack is introduced ahead of the main crack. * This
cracking are discussed. microcrack is represented mathematically by a cut between x = a
and x = b, as in Fig. 1. The relevant boundary conditions are
I. Introduction u
, = Uq = 0 (2)

T HE occurrence of stress-induced microcracking around a


main-crack tip has been recognized as an important tough-
ening mechanism in zirconia-toughened ceramics. The aim of
for y + O? along
a,&, 0) + d&,0)
--M < x < 0, and a < x < b;
(3)
this note is to present an exact stress analysis for a two-dimensional
configuration involving a single microcrack ahead of a main crack, for r * b.
The problem just stated belongs to a restricted class for which
and to discuss its relevance to theoretical estimates of microcrack
toughening. the solution can be expressed in terms of a single (Westergaard)
complex potential,6 instead of the usual two Muskhelishvili poten-
tials.’ The same Westergaard potential Z(z)can be used for all three
11. Stress Analysis cracking modes, with appropriate changes to the stress components
The configuration being considered is shown in Fig. I . It is specified in Eq. (2),but only mode I will be considered here. The
assumed that (i) the main crack can be regarded as a semi-infinite problem can be solved by using a conformal transplantation,8
crack in an infinite body; (ii) the nominal stress field which would specified by z += 5 = 6 .The transplanted boundary conditions
prevail in the absence of the microcrack is given by the singular in the 5-plane correspond to those for two collinear cracks of equal
term in the near-tip asymptotic expansion for an elastic crack-tip length perturbing a uniform stress field. Using the known solution
stress field; i.e., relative to polar coordinates (Y, 0) with the main- for the latter problem,’ and reverting to the z-plane, we obtain
crack tip as origin, the components of the nominal stress tensor are Z(Z) = K N ( z - ~ C ) / [ ~ ~-T aZ) ((Z Z- b)]”’ (4)
C =E(k’)/K(k’) (5)
Received July 1, 1985; revised copy received November 13, 1985: approved k 2 = a/b k’ = (1 - k‘)I’* (6)
November 13, 1985.
*After submission of the present work, it was found that a solution of this prbblem where, following standard notation,” we use E , K to denote the
has recently been presented by R ~ b i n s t e i n ,using
~ a different approach from that
adopted here. but obtaining, of course, the same final result. The use which is made complete elliptic integrals of the second kind and the first kind,
of the result in Ref. 5 is also different from that discussed here in Sections 111 and IV respectively, and k , k’ to denote their modulus and complementary
March 1986 Effective Fracture Toughness of Microcracked Materials 213
1 I I
Y I 1 I I I
l

Fig. 1. Two-dimensional configuration of collinear


microcrack ahead of main crack, showing coordinate
axes used in text.

modulus. (Note that K is used to denote an elliptic integral only in


Eq. (5); elsewhere K is used to denote the stress intensity factor,
again following standard notation.)
The complete elastic field can be determined from the potential
in Eq. (4), but the main interest is in the stress intensity factors at
the three crack tips, which are given by
a/ b
K(x = O ) / K N = C/k (7)
K(x = a ) / K N = (C - k2)/kk' Fig. 2. Stress intensity factors for crack tips at ( i ) x = 0,
(8) (ii) x = n , and (iii) x = b in Fig. 1, normalized relative to nomi-
K(x = b ) / K N = (1 - C ) / k ' nal stress intensity factor, KN.
(9)
These expressions can be readily evaluated using tabulated values
for the elliptic integrals,'" and the results are shown in Fig. 2. For
the crack tip at x = b , K / K N 4 1 , as a / b + 0, whereas for the If we now regard the linking up of the main crack with this
crack tips at x = 0 and x = a, K diverges as a / b = k 2 -+ 0, the collinear microcrack as an idealized repeat unit in the crack growth
asymptotic behavior at both of these crack tips being given by process, the effect of all the other microcracks being accounted for
K / K N = I/[k log (4/k)] (k + 0) (10) by a uniform reduction in the effective modulus, we can derive an
estimate for KO from the results given in Eqs. (7) to (9).
An important feature of these results is that

111. Toughness Degradation Due to Microcrack Linkup


K(x = 0) > K(x = a) > K ( x = b) (14)
The preceding analysis can be used to derive an estimate for the
i.e., of the three crack tips, the main-crack tip has the largest K .
effective fracture toughness of a microcracked material, as fol- Consequently, if we assume that crack extension could occur at
lows. Consider an isotropic elastic material which is permeated either of these crack tips when the relevant K reaches a definite
by a homogeneous, isotropic, distribution of microcracks. Let N critical value K c , then, under increasing K N ,crack extension would
denote the average number of microcracks per unit volume, so that in fact begin from the main-crack tip, and if K N is kept constant,
= N-113 the linkup of the main crack with the microcrack would proceed
(11)
unstably, rather than quasi-statically. Denoting by KO the value
gives a measure of the average distance between neighboring mi- of K N at which this linking up is initiated, we derive from Eq. ( 7 )
crocracks. Suppose that a planar "main crack," of characteristic the relation
linear dimension much larger than I , is introduced into this micro-
cracked material and is made to grow quasi-statically. Let A denote Ko/K, = k/C
the area fraction of the fracture plane corresponding to pre- which is shown graphically by curve (i) of Fig. 3. This KOcan be
existing microcracks, which are assumed not to grow themselves used as an estimate of the effective fracture toughness of a micro-
during the process of main-crack growth, but to link up with the cracked body, with K , denoting the intrinsic fracture toughness of
main crack if they lie on, or close to, the fracture plane. Then the material without microcracks.
A = N2'3(c2) (12) It is of interest to compare this estimate with simpler estimates
based on a rule of mixtures for the work of fracture,"." which
where (c2) denotes the average of the projected area of the micro- leads to
cracks onto the fracture plane, if it is assumed, as a reasonable
approximation, that the main crack links up with all the micro- Ko/K, = (1 - A)'" = (a/b)'/' = k ( 16)
cracks lying within a layer adjacent to the fracture plane, of thick- or based on a rule of mixtures for K,I3.I4which gives
ness I (measured normal to the fracture plane). To estimate the
effective fracture toughness KO, we proceed to a two-dimensional Ko/K, = 1 - A = a / b = k2 (17)
configuration in which the main crack is regarded as a semi-infinite
crack, and the closest microcracks which are about to link up with These estimates are shown as curves ( i i ) and (iii), respectively, in
the main crack are represented by a single (two-dimensional) col- Fig. 3. It is clear that there is a substantial difference between
linear microcrack, as in Fig. 1. With this representation, we these three estimates, except at the limits a / b -+ 0 and a / b -+ 1 .
may set In particular, for a / b = 0.5, Eq. (15) predicts a reduction in
toughness of only 3%, instead of 29% according to Eq. (16), or
a/b = 1-A (13) 50% according to Eq. (17).
214 Journal of the American Ceramic Society-Rose Vol. 69, No. 3
where h denotes the height of the transformed zone or the micro-
cracked zone. The precise expression for C will depend on the
dynamical conditions which are specified for stress-induced trans-
formation or microcracking to occur, but the toughness increment
EV% should scale with KO. This KO can be interpreted as an
effective toughness which depends on the intrinsic fracture tough-
ness K , for the material, but with an allowance made for the
crack-plane interactions which occur as a side effect of either
transformation toughening or microcracking .
An important difference arises at this stage between these two
toughening mechanisms. With the former, the crack-plane inter-
actions generally increase KO relative to Kc.14s17 For example, in
PSZ, K, = 2 MPa.m”2 whereas KO 4 MPa-m”*. With micro-
cracking, on the other hand, the principal crack-plane interaction
is the linking up of the main crack with microcracks, which would
be expected to reduce KO.This reduction can be estimated by
regarding KO as the fracture toughness for a hypothetical material
permeated by a homogeneous distribution of pre-existing (as op-
posed to stress-induced) microcracks. An estimate was derived
for this KO in Section 111. This estimate, given by Eq. (15), was
shown to be substantially higher than previous estimates”-13 based
alb on a rule of mixtures, given by Eqs. (16) and (17).
Since the potential increase in toughness due to stress-induced
Fig. 3. Estimates for effective fracture toughness of mi-
crGcracked material basedon (i) Eq. (15), (ii)-Eq. (16), and microcracking ( Z f i in Eq. (19)) should be approximately propor-
(iii) Eq. (17). tional to KO,these differences deserve closer scrutiny. In this con-
nection, it should be recognized that, in practice, stress-induced
microcracking is usually associated with internal stresses, due, for
example, to thermal expansion anisotropy within the grains of a
Two aspects of these results may appear puzzling. First, one polycrystal. ‘*.I9 The estimate for KOgiven by Eq. (15) ignores such
might have expected, intuitively, that the rule of mixtures should localized stresses, but an extension of the present calculations is
underestimate the interaction between main crack and microcrack, currently being attempted with the aim of accounting for internal
and consequently should overestimate the effective toughness. stresses. It should be noted that current estimates of KO based on
On closer inspection, however, it becomes evident that Eq. (16) a rule of mixtures also fail to take into account explicitly the effect
would give the correct value for KO if the linking up occurred of internal stresses.
quasi-statically, which would require that K N be continually de-
creased to maintain K at the main-crack tip just equal to K,. If
instead K N is kept constant, the linking up proceeds unstably and
more energy is dissipated than would be required in a quasi-static
process. This accounts for the higher estimate of KO given by References
Eq. (15) relative to Eq. (16). (Note that the length scale of the ID. J. Green, P. S. Nicholson, and J. D. Emhury, “FractureToughnessof a Partially
Stabilized Zro, in the System CaO-ZrO,,” J. Am. Ceram. Soc., 56 [12] 619-23
linking up process should be small compared with the crack length (1973).
or specimen dimensions, so that macroscopic crack growth can be *N. Claussen, “Fracture Toughness of A1,03 with an Unstahilized Zro, Dispersed
Phase,” J. Am. Ceram. Soc., 59 (1-21 49-51 (1976).
considered to be occurring quasi-statically even though the linking ’N. Claussen, J. Steeb, and R. F. Pabst, “Effect of Induced Microcracking on the
up process is unstable.) Fracture Toughness of Ceramics,” Bull. Am. Ceram. Soc., 56 [6] 559-62 (1977).
Secondly, the estimates of KO discussed above do not depend on 4B. R. Lawn and T. R. Wilshaw, Fracture of Brittle Solids; pp. 53-54. Cambridge
University Press, Cambridge, 1975.
the elastic modulus, so that the microcracks which do not link up 5A. A. Rubinstein, “Macrocrack Interaction with a Semi-infinite Microcrack
with the main crack do not seem to affect KO.However, it can be Array,” Int. J. Fracr., 27, 113-19 (1985).
6P. C. Paris and G. C. Sih, “Stress Analysis of Cracks,” App. I; pp. 63-66 in
argued that if the intrinsic work of fracture is regarded as a material ASTM STP 381. American Society for Testing and Materials, Cleveland, OH, 1965.
constant, a reduction in effective modulus due to a homogeneous ’N.I. Muskhelishvili, Some Basic Problems of the Mathematical Theory of Elas-
ticity. Noordhoff. Groningen, 1953.
distribution of microcracks should be compensated for by a reduc- ‘P. Henrici, Applied And Computational Complex Analysis, Vol. 1, Section 5.6.
tion in the effective Kc. Thus, K, in Eqs. (15) to (17) should in fact Wiley, New York, 1974.
be taken to be Kc given by ’T. J. Willmore, “The Distribution of Stress in the Neighbourhood of a Crack,”
Q.J. Mech. Appl. Math., 2, 53-63 (1949).
lop. F. Byrd and M. D. Friedman, Handbook of Elliptic Integrals for Engineers
Fc = @ / E ) “ Z K c (18) and Scientists, 2nd ed., revised. Springer-Verlag. Berlin, 1971,
“W. Kreher and W. Pompe, “Increased Fracture Toughness of Ceramics by
for plane stress, where E denotes the intrinsic Young’s modulus for Energy-Dissipative Mechanisms,” J. Mater. Sci., 16, 694-706 (1981).
the material without microcracks, and E the effective modulus for ‘,A. G. Evans and K. T. Faber, “Toughening of Ceramics by Circumferential
Microcracking,”J. Am. Ceram. Soc., 64 [7] 394-98 (1981).
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the relative values of KO given by these estimates. Materials,” J. Am. Ceram. Soc., 67 141 255-60 (1984).
I4A.G. Evans and R. M. Cannon. “Touehenine of Brittle Solids bv Martensitic
Transformations”;to be published in Acta fietall.-
15B. Budiansky and R. I. O’Connell, “Elastic Moduli of a Cracked Solid,” Int. J.
IV. Application to the Theory of Microcrack Toughening Solids Struct., 12, 81-97 (1976).
I6R.G. Hoagland and 1. D. Emhury, “A Treatment of the Inelastic Deformation
The theoretical analysis of the toughening due to stress-induced Around a Crack Tip due to Microcracking,” J. Am. Ceram. Soc., 63 [7-81 404-10
(19x0~
m i c r ~ c r a c k i n g ” - ’follows
~ ~ ~ ~ a pattern similar to that used for \.___

I’M: V. Swain and L. R. F. Rose, “Toughening of Ceramics”; pp. 47>94 in Ad-


transformation toughening. I4,l7 In both cases the nominal stress vances in Fracture Research, Val. 1. Edited by s.R. Valluri et al. Pergamon Press,
intensity factor during quasi-static steady-state cracking can be Oxford, 1984.
‘‘1. I. Cleveland and R. C. Bradt, “Grain Size/Microcracking Relations for Pseu-
written in the form dobrookite Oxides,” J. Am. Ceram. Soc., 61 [11-12] 478-81 (1978).
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K:$ = KO f C-\/si (19) ing in Ceramics,” J. Am. Ceram. Soc., 62 [ll-121 560-63 (1979). n

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