Professional Documents
Culture Documents
Investigation of Moisture Removal
Investigation of Moisture Removal
points. Further investigation demonstrated that water, were used (wherever possible) as in the original
once in the rudder, can migrate easily along the structure.
leading edge via the highly porous foam adhesive that A major challenge was to duplicate the paths
was used to bond the titanium channel and the by which water migrate from cell to cell of the
honeycomb core [12]. If such paths are taken honeycomb core. Such paths may include skin-to-core
advantage of during drying operation, it was disbonds, honeycomb core node disbonds, crushed
hypothesized that it would be feasible to remove water core and other types of core damage [10]. Since
from the rudder non-invasively and efficiently. adhesive failure disbonds or weakened bonds were the
primary source of part failure, it is conceivable that
skin-to-core disbonds are also the most important type
of degradation mechanism and a major form of water
path. In this study, only skin-to-core disbonds were
simulated within the honeycomb core area due to the
uncertainty about the contributions of other types of
defects to water ingress, and the difficulty of
duplicating these defects. Although this simplification
would impact water removal rates, the comparative
study of the various drying parameters would still
yield useful information to identify an accelerated
method to remove water from the CF-18 rudders.
The water ingress occurrence cumulative map
indicates that the water ingress area with 60%
occurrence is approximately 25mm deep and 50mm
wide, and located near the upper hinge area. Several
methods to generate disbonded areas in the sandwich
Leading Trailing coupons were attempted, including embedding
edge edge Teflon® film, spraying the bonding surfaces with the
mold release agent FreKote®, and removing the skin-
Fig. 2 Water ingress cumulative occurrence map to-honeycomb adhesive. Non-destructive inspection
developed based on 202 CF-18 rudders inspected (NDI) using thermography and ultrasound indicated
between 1999-2004 using thermography. that thermographic inspection was able to detect all
the areas with embedded defects whereas ultrasonic
3. Experimental only detected areas without the adhesive (see Fig. 4).
This suggests that although applications of release
3.1 Coupon Design and Fabrication agents such as Teflon or FreKote causes chemical
Composite honeycomb sandwich coupons disbonds, physical barriers to water egress may
were fabricated including critical features and remain. Therefore, all the panels for the comparative
representative water ingress paths for moisture study of drying parameters were fabricated with
removal experiments [13]. As shown in Fig. 3, this adhesive removed from a window area of 25mm by
design took into account features that are important for 50mm. Several panels with embedded Teflon were
rudder moisture ingress such as a hole in the front also used to study the influence of the disbond
Titanium spar and the porous foam adhesive along the generation methods on moisture removal.
leading edge. The same materials for the skins, core
and adhesives, and the same manufacturing process
CHUN LI, R. Ueno, V. Lefebvre
Specimen Rudder
Ti Spar
Film
Adhesive
Foam
Adhesive
Facesheet
Disbond
Potting compound
Fig. 3: Cross-section of leading edge of CF-18 rudder (left: design schematic, right: actual specimen)
a) disbonds b)
Fig. 4: NDI inspection of the fabricated sandwich panels (460mm X 280mm) with removed adhesive in six
simulated disbonded areas of 25mm X 50 mm using a) Thermography b) Ultrasonic Inspection
In the test panels, the silicone rubber adhesive and lack of information, great care was taken to ensure
sealant RTV162 was applied to seal the three edges of the same starting condition for each of these coupons.
the coupons, and a hole of 4.8mm was drilled on the
3.2 Moisture Removal approaches
centre of the front spar to simulate the jig hole or holes
for the ground studs and hinges [13]. Syringes were Water removal has been studied for centuries
then used to inject water in the honeycomb cells in the as a means of preservation of food, wood and crop
disbonded area, and then into the foam adhesive. To dehydration, fabrication of paper, textiles,
inject water into the honeycomb cells, an X-ray image pharmaceutical and construction products,
was taken of each coupon to indicate the centre of dehumidification in the air conditioning industry and
each honeycomb cell and 101 holes of 0.8mm in sewage treatment. Various techniques have been
diameter were drilled in the centre of each honeycomb developed to achieve efficient moisture removal,
cell in the window area. 0.1 g of water (or 20% cell including the application of heat, vacuum [14],
volume) was injected into each drilled hole, which ultrasound [15][16], centrifugal forces [17][18] and
was then sealed using epoxy paste adhesive Hysol EA electrical pulses [19].
9396. Water was then injected into the foam adhesive In this study, various moisture removal
though the drilled hole on the spar. The total water approaches were studied with consideration of the
amount injected into each coupon was approximately drying parameters that are potentially effective, low-
20 g, with 10 g in the cells and 10 g in the foam cost and easy-to-apply. Such parameters include
adhesive. Due to the complex nature of water paths heating, vacuum, vibration and generation of
INVESTIGATION OF AN ACCELERATED MOISTURE REMOVAL APPROACH
OF A COMPOSITE AIRCRAFT CONTROL SURFACE
additional moisture channels. Each of these factors baseline case were selected and applied to real
was investigated as follows: rudders.
Heating: Heating is the most commonly used
3.3 Test Scenarios of Moisture Removal
method for moisture removal. Heating can be
conducted by various means such as convection, Eight Test Scenarios (TSs) were investigated as listed
conduction, radiation and microwave [20]. According in Table 1. The sandwich coupons were subjected to
to a previous study, prolonged exposure to a humid the given condition and the weight of the coupons
environment above 85 °C may cause permanent were monitored periodically depending on the drying
adhesive degradation [21]. In this study, the drying rate. In all tests, coupons were placed flat, with the
temperature was set to be around 70 °C. disbonded interface on the bottom side. The drying
Vacuum: Vapour can travel through any effectiveness was evaluated by the weight loss of the
existing moisture paths easily. Based on water phase composite sandwich coupons, using Eqn (1).
diagrams, water can evaporate at a temperature well
Weight reduction
below 100 °C at less than atmospheric pressure. % Moisture removed = × 100% (1)
Maximum vacuum was used in the experimental Total water amount
study, with an achievable level of about a pressure of where the total water amount was calculated based on
11 kPa at the lab or in the field. This pressure is well the measured coupon weight before and after water
below 20 kPa, the required minimum for water injection. The typical coupon weight after water
evaporation at 70 °C. injection was around 400 g and the resolution of
Vibration: Energy from vibration allows water weight measurement was 0.01 g. Each test scenario
to be separated from surfaces and move easily with was repeated two to four times. Since consistent
minimal energy input. This technology is especially results were obtained, only one set of results for each
attractive as a means of drying heat-sensitive test scenario is shown in this paper.
materials, because it has been found to be very
effective for room temperature drying with no more Table 1: Test scenarios for moisture removal
than 1 °C temperature increase [22]. In this study, an experiments on simulated CF-18 rudder composite
ultrasonic vibration source on the order of 10 MHz sandwich coupons
was generated by Tektronix PG508 50MHz pulse No Methods Equipment Required
generator. The vibration signal was enhanced to 20
dB by an EIN RF power amplifier (model 411 LA, 10 TS1 Low heating only Heating at 40°C in a convection
oven
watts linear, Rochester, NY) and was transmitted to
the bottom surface of the coupon via a cylindrical TS2 Intermediate heating Heating at 70°C in a convection
transducer with a surface of 60mm in diameter. only (Baseline) oven
Water Ingress/Egress Channel: Years of TS3 Vacuum only Room temperature and maximum
service led to material aging and possibly damage in vacuum in a vacuum oven
the rudders. Some types of damage such as node TS4 Combined vibration Drying in a vacuum oven using
disbonds and core crushing cannot easily be simulated and vacuum ultrasonic vibration
in the coupons, but they could be important water
TS5 Combined heating Drying in a temperature controlled
ingress paths. To demonstrate the influence of other and vacuum vacuum oven, or in a vacuum bag
possible core damage, a hole of 0.25mm in diameter in a temperature controlled oven
was created in the centre of the first rows of (two types of coupon design)
honeycomb cells near the spar. TS6 Combined heating, Heating at 70 °C and maximum
The above drying factors as well as their vacuum and vacuum, with additional water
combinations were studied using fabricated sandwich additional drying channel in a vacuum oven
coupons. The drying time, defined to be the time to channels
reach 90% water removal, was compared with a * Unless specified, vacuum refers to maximum vacuum
baseline case where only intermediate heating at 70 °C (typically 11 kPa).
was applied. Methods that are more effective than the
CHUN LI, R. Ueno, V. Lefebvre
3.4. Test Results and Discussions was related to the low permeability of the thin layer of
adhesive between the disbonded area and the foam
3.4.1 Effect of Heat and Vacuum
adhesive at the leading edge, as shown in Fig. 3. This
It is not surprising that the drying rate thin layer of adhesive formed due to resin flow during
increases with temperature. An increase of the drying processing and slowed down the water removal rate
temperature from 40 ºC (low) to 70 ºC (intermediate) during the process. In these trials, the honeycomb
enhanced the water removal amount from 24% to 53% sandwich coupons were placed with the disbonded
after 10 continuous days of drying (see Fig. 5). side facing up. While water evaporates at a constant
Elapsed time in all the graphs is the accumulative time rate under set conditions, the limited gap between the
during which the coupons were kept at the set core and the facehsheet, and the longer travel distance
conditions. At the end of 10 days of drying, the water from the entry point limited the water migration rate.
removal rate at the low temperature dropped to nearly Furthermore, the vapour concentration in the cells
zero. Although drying at the intermediate temperature reduces with time, leading to a reduced vapour
in the baseline scenario continued to remove water migration rate. The tests suggested that if skin-to-core
after 10 days, it was too slow to be practical for repair disbonds are the primary water ingress paths, it is
operations. important to avoid direct pressure on the skin to close
100% these gaps. Therefore, should vacuum bagging be
used for such water removal, care has to be taken to
90% Heat & vacuum
avoid direct contact of the bagging materials.
80% A similar overall drying efficiency was
observed for vacuum-only and heat-only approaches.
Heat only (70°C)
70% However, the effectiveness varies with the stage of the
% Moisture Removed
water via the skin. It was found that for the energy beginning; it took only about 6 hours to remove up to
and spectrum of the vibration used for this study, 85% water from the coupons. The rate was then
vibration- assisted vacuum drying did not increase the reduced to a similar value as the coupons without
water drying rate. One possible explanation is that the additional water channel, showing that, despite of the
total power of the transducer used for this study did direct path from the disbonded to the foam adhesive
not meet the required power for effective dewatering area, the moisture removal rate for water that is further
as studied previously. In contrast, the rate was away from the entry point was dominated by the
reduced because sealing of the vacuum oven was permeability of water migration from cell to cell. The
affected by the vibration transducer cables, increasing introduced channel was investigated to demonstrate
the pressure from 11 kPa to 20 kPa. Further the effect of the channels that may have existed in the
investigation is needed to understand the effect of rudders. In particular, no additional channels would
vibration on water removal within sandwich be introduced to the real practice of CF-18 rudder
structures. moisture removal.
100% 100%
Heat &
90% 90% vacuum
80% 80%
Heat & vacuum
70% 70%
% Moisture Removed
% Moisture Removed
60%
60%
Vacuum only
50%
Vacuum & vibration 50%
40%
40%
30%
30%
20%
20%
10%
10%
0%
0 10 20 30 40 50 0%
Elapsed Time (days) 0 2 4 6 8 10
Elapsed Time (days)
Fig. 6 Effect of vibration
Fig. 7 Effect of water ingress/egress channel
3.4.3 Effect of Water Ingress/Egress Channel
In this study, other types of water paths such 3.4.4 Effect of Coupon Design
as node disbonds were not taken into account in the Fig. 8 shows the different moisture removal
coupon design. To account for the effect of other rates of coupons with different disbond design. All
types of water migration paths that may exist in the the coupons were subjected to vacuum drying at an
CF-18 rudders, a small hole of a diameter of 5mm was elevated temperature of 70 ºC. As suggested by
drilled into the first and second row of the honeycomb ultrasonic test results, the coupon with the application
walls and the coupons were subjected to the combined of Teflon or FreKote to create skin-to-core disbonds
heating and vacuum condition, as shown in Test showed no indication of physical disbonds while
Scenario 6 in Table 1. The test results (Fig. 7) shows adhesive removal did show evidence of these
that the inclusion of a water channel through the disbonds. A maximum of 50% of the water was
honeycomb core led to a significant reduction in removed from the coupons that had no indication of
drying time from 11 days to 0.5 days. Again, the physical disbonds, with all of these occurring in the
water removal rate was extremely fast at the first 3 hours.
CHUN LI, R. Ueno, V. Lefebvre
Water in Core
80% drying was compared for all the test methods. It has
Coupon with evidence of
70%
physical disbonds been found that combined vacuum and heating method
% Moisture Removed
Water in Foam
Coupon without evidence of
30% 3.6 Field Tests of Rudder Moisture Removal
physical disbonds
20% Prior to this study, moisture removal was
10% attempted on a rudder with significant water ingress
Test Scenario: 70°C, vacuum detected by infrared thermography (see Fig. 9). In this
0%
trial, sealant on the front spar was removed and the
0 20 40 60
rudder was subjected to an elevated temperature in the
Elapsed Time (days)
range 70 to 90 ºC. After nearly two months of the
Fig. 8 Effect of design of skin-to-core disbonds experiment, little success was achieved as indicated in
Fig. 10.
Little further drying was observed in the next The same rudder was then used for drying
60 days equivalent of continuous drying time, as trials using the approach developed in this work. In
shown in Fig. 8. Further NDI on the coupons indicated this experiment, the sealant jig hole above the upper
complete water retention in the honeycomb cells, grounding stud was removed, while hinges and
suggesting that only water in the foam adhesive had grounding studs remained in place for the first
been removed. On the other hand, when physical attempt. The upper and middle hinge areas, including
disbonds are present, it was possible to completely the exposed jig hole, were sealed in a vacuum bag and
remove water both in the foam adhesive and in the then placed in a temperature-controlled oven. The
core. It took around 12 days to reach 90% moisture drying temperature was set to 70 ºC while maximum
removal and about 30 days to completely remove the vacuum was applied. After a one-day trial, inspection
water. The observed moisture removal results using thermography was conducted on the rudder,
confirmed the speculation that while chemical showing significant water removal as shown in
disbonds may be created by all the mentioned Fig. 11. Area with water ingress has shrunk by 60%,
methods, they do not guarantee the generation of indicating the effectiveness of the combined heating
water ingress/egress paths. and vacuum drying method.
Table 2: Comparison of estimated time to remove 90% of moisture for the studied test scenarios
Temperature Vibration
Room temperature Low Intermediate
Vibration
(22 ºC) (40 ºC) (70 ºC)
(TS1) more than 500
No vacuum N/A (Baseline TS2) 90 days* N/A
days*
(TS3) (TS5)
Maximum vacuum N/A (TS4) 500 days*
300 days* 11 days
(TS6)
vacuum and channel N/A N/A N/A
0.5 day
* The drying time was calculated by extrapolating the experimental curve to reach 90% water removal.
INVESTIGATION OF AN ACCELERATED MOISTURE REMOVAL APPROACH
OF A COMPOSITE AIRCRAFT CONTROL SURFACE
Water
Water
Fig. 9 Thermography image showing Fig. 10 Moisture ingress area Fig. 11 Moisture ingress area after
moisture ingress area in a CF18 rudder after two months of moisture 8 hours of vacuum-assisted drying
panel removal at around 80 ºC at 70 ºC