TRƯỜNG ĐẠI HỌC SƯ PHẠM KĨ THUẬT TP.

HCM
KHOA CÔNG NGHỆ HÓA HỌC & THỰC PHẨM
-------

BÁO CÁO THÍ NGHIỆM

HÓA PHÂN TÍCH

Họ và tên:
GVHD: Nguyễn Quốc Thắng
NHÓM:
LỚP: 19116CL2A ( Thứ 6 t1-t5 )
THÀNH VIÊN:

TP. HỒ CHÍ MINH – 10/2020

THỜI GIAN: BUỔI: THỨ:

BÁO CÁO THÍ NGHIỆM BÀI 3

PHƯƠNG PHÁP CHUẨN ĐỘ ACID - BASE
PHA DUNG DỊCH CHUẨN ACID OXALIC
XÁC ĐỊNH NỒNG ĐỘ DUNG DỊCH NaOH VÀ DUNG DỊCH H3PO4

I. NGUYÊN TẮC VÀ CÁCH TIẾN HÀNH

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II. KẾT QUẢ THÍ NGHIỆM
TN1.Pha dung dịch chuẩn H2C2O4 0,1N từ tinh thể H2C2O4.2H2O

- Số gam H2C2O4.2H2O (chất gốc) cần lấy để pha 100,0 mL dung dịch H2C2O4 0,1000N.
mtheo. =---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
- Cân chính xác khối lượng H2C2O4.2H2O, mrel. = ---------------------------------------------------
- Nồng độ thực của H2C2O4 (khoảng tin cậy ±ɛ0,95%) : -----------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN2. Pha dung dịch NaOH gần đúng 0,1N. Xác định lại nồng độ
TN2.1 Pha dung dịch NaOH
Số gam NaOH cần lấy để pha 250 mL dung dịch NaOH  0,1N là: ------------------------------
----------------------------------------------------------------------------------------------------------
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-----------------------------------------------------------------------------------------------------------
TN2.2. Xác định nồng độ dung dịch NaOH

NaOH H2C2O4
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình

Biểu diễn CN của NaOH kèm theo ε0.95

CN = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
Biểu diễn nồng độ NaOH dưới dạng: CM, TNaOH, TH2C2O4/NaOH
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TN3. Xác định nồng độ dung dịch H3PO4
TN3.1. Chuẩn độ với chỉ thị metyl da cam
CN của NaOH là:
NaOH H3PO4
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình

Biểu diễn CM của H3PO4 kèm theo ε0.95

CM = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN3.2. Chuẩn độ với chỉ thị phenolphtalein

NaOH H3PO4
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
Biểu diễn CM của H3PO4 kèm theo ε0.95
CM =-----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
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III. ĐÁNH GIÁ KẾT QUẢ
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IV. CÂU HỎI VÀ BÀI TẬP
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Chữ ký GVHD

THỜI GIAN: BUỔI: THỨ:

BÁO CÁO THÍ NGHIỆM BÀI 4

PHA DUNG DỊCH CHUẨN Na2CO3, XÁC ĐỊNH ĐỘ CHUẨN DUNG DỊCH
HCl, XÁC ĐỊNH NaOH VÀ Na2CO3 TRONG HỖN HỢP

I.NGUYÊN TẮC VÀ CÁCH TIẾN HÀNH

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II. KẾT QUẢ THÍ NGHIỆM

TN1. Pha dung dịch chuẩn Na2CO3 0,1000 N từ muối rắn Na2CO3 (M=105,99 g/mol)

- Số gam Na2CO3 (chất gốc) cần lấy để pha 50,00 mL dung dịch Na2CO3 0,1000N.
mtheo. =---------------------------------------------------------------------------------------------------
- Cân chính xác khối lượng Na2CO3, mrel. =---------------------------------------------------------
- Nồng độ thực của Na2CO3 (khoảng tin cậy ± ɛ0,95%) : ----------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN2. Pha dung dịch HCl gần đúng 0,1N và xác định lại nồng độ
TN2.1 Pha dung dịch HCl gần đúng 0,1N
- Thể tích HCl đậm đặc cần lấy để pha 250,0 mL dung dịch HCl  0,1N là: ---------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN2.2. Xác định nồng độ dung dịch HCl

HCl Na2B4O7
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

Biểu diễn CN của HCl kèm theo ε0.95

CN = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN3. Xác định nồng độ dung dịch hỗn hợp NaOH + Na2CO3

HCl (phenolphtalein) HCl (metyl da cam) NaOH + Na2CO3

Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

Biểu diễn CM của NaOH kèm theo ε0.95

CM = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
Biểu diễn CM của Na2CO3 kèm theo ε0.95
CM = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
III. ĐÁNH GIÁ KẾT QUẢ
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IV. CÂU HỎI VÀ BÀI TẬP
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Chữ ký GVHD
THỜI GIAN: BUỔI: THỨ:

BÁO CÁO THÍ NGHIỆM BÀI 5

PHƯƠNG PHÁP CHUẨN ĐỘ PEMANGANATE, XÁC ĐỊNH ĐỘ CHUẨN

CỦA DUNG DỊCH KMnO4 BẰNG H2C2O4
XÁC ĐỊNH HÀM LƯỢNG Fe2+ BẰNG DUNG DỊCH KMNO4

I. NGUYÊN TẮC VÀ CÁCH TIẾN HÀNH

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II. KẾT QUẢ THÍ NGHIỆM
TN1. Pha dung dịch KMnO4 và xác định nồng độ KMnO4
TN1.1. Pha dung dịch KMnO4

- Số gam KMnO4 cần lấy để pha 100,00 mL dung dịch KMnO4 0,1N.
mtheo. =---------------------------------------------------------------------------------------------------
- Cân chính xác khối lượng KMnO4, mrel. = --------------------------------------------------------
- Nồng độ KMnO4-------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN1.2. Xác định nồng độ KMnO4 bằng dung dịch chuẩn H2C2O4

KMnO4 H2C2O4
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

a) Biểu diễn CN của KMnO4 kèm theo ε0.95

CN = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
b) Tính nồng độ KMnO4: CM, TKMnO4 , TH2C2O4/KMnO4
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TN2. Xác định hàm lượng Fe2+ trong muối Mohr bằng dung dịch KMnO4
 KMnO4 Fe2+
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

Biểu diễn hàm lượng của Fe2+ kèm theo ε0.95 (biết MFe = 55.85)
Tính hàm lượng Fe2+ ra g/l và tính nồng độ chuẩn của KMnO 4 theo sắt (tức là tìm xem
1mL dung dịch KMnO4 có thể oxy hóa bao nhiêu gam Fe2+)
Hàm lượng Fe = --------------------------------------------------------------------------------------
ε0.95 =----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
μ = -----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TKMnO4/Fe2+-----------------------------------------------------------------------------------------------
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III. ĐÁNH GIÁ KẾT QUẢ
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IV. CÂU HỎI VÀ BÀI TẬP
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Chữ ký GVHD

THỜI GIAN: BUỔI: THỨ:

BÁO CÁO THÍ NGHIỆM BÀI 6

PHƯƠNG PHÁP CHUẨN ĐỘ IOD

PHA DUNG DỊCH CHUẨN Na2S2O3
XÁC ĐỊNH ĐỘ CHUẨN DUNG DỊCH Na2S2O3, ĐỊNH LƯỢNG H2O2

I. NGUYÊN TẮC VÀ CÁCH TIẾN HÀNH

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II. KẾT QUẢ THÍ NGHIỆM
TN1. Pha dung dịch Na2S2O3 và xác định nồng độ Na2S2O3

TN1.1. Pha dung dịch Na2S2O3

- Số gam Na2S2O3.5H2O cần lấy để pha 100,00 mL dung dịch Na2S2O3 0,1 N
mtheo. =---------------------------------------------------------------------------------------------------
- Cân chính xác khối lượng Na2S2O3.5H2O, mrel. = -------------------------------------------------
- Nồng độ Na2S2O3 ------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN1.2. Xác định nồng độ dung dịch Na2S2O3 bằng DD chuẩn K2Cr2O7 0,1000 N

Na2S2O3 K2Cr2O7
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV
Biểu diễn CN của Na2S2O3 kèm theo ε0.95
CN = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
2. Xác định nồng độ dung dịch H2O2
CN của Na2S2O3 là:------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

Na2S2O3 H2O2
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

Biểu diễn nồng độ H2O2 kèm theo ε0.95

CN =-----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = --------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
III. ĐÁNH GIÁ KẾT QUẢ
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IV. CÂU HỎI VÀ BÀI TẬP
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 Chữ ký GVHD

THỜI GIAN: BUỔI: THỨ:

BÁO CÁO THÍ NGHIỆM BÀI 7

PHƯƠNG PHÁP ĐO BẠC

ĐỊNH LƯỢNG AgNO3 THEO PHƯƠNG PHÁP MOHR VÀ PP FAJANS
I. NGUYÊN TẮC VÀ CÁCH TIẾN HÀNH
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II. KẾT QUẢ THÍ NGHIỆM
TN1. Pha dung dịch chuẩn NaCl 0,0500 N

- Số gam NaCl cần lấy để pha 100,00 mL dung dịch NaCl 0,0500 N
mtheo. =---------------------------------------------------------------------------------------------------
- Cân chính xác khối lượng NaCl, mrel. = ------------------------------------------------------------
- Nồng độ NaCl (0.95) -------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN 2: Xác định nồng độ AgNO3 theo phương pháp MOhr

NaCl AgNO3
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

Biểu diễn nồng độ của AgNO3

CN =-----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

TN 3: Xác định nồng độ AgNO3 theo phương pháp Fajans (chỉ thị hấp phụ)

NaCl AgNO3
Dụng cụ
σ
Lần 1
 Lần 2
Lần 3
Trung bình
SV

Biểu diễn nồng độ của AgNO3

CN = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 =----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
μ = ------------------------------------------------------------------------------------------------------
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III. ĐÁNH GIÁ KẾT QUẢ
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IV. CÂU HỎI VÀ BÀI TẬP
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Chữ ký GVHD

THỜI GIAN: BUỔI: THỨ:

BÁO CÁO THÍ NGHIỆM BÀI 8

PHƯƠNG PHÁP CHUẨN ĐỘ COMPLEXON
XÁC ĐỊNH NỒNG ĐỘ TRILON B
XÁC ĐỊNH ĐỘ CỨNG CỦA NƯỚC VÀ NỒNG ĐỘ Al3+

I. NGUYÊN TẮC VÀ CÁCH TIẾN HÀNH

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II. KẾT QUẢ THÍ NGHIỆM
TN1. Pha dung dịch Trilon B –Xác định lại nồng độ dung dịch Trilon B
TN1.1. Pha dung dịch Trilon B

- Số gam Trilon B cần lấy để pha 100,00 mL dung dịch Trilon B 0,0100 M
mtheo. =---------------------------------------------------------------------------------------------------
- Cân chính xác khối lượng Trilon B , mrel. =--------------------------------------------------------
- Nồng độ Trilon B -----------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN 1.2 Xác định lại nồng độ dung dịch Trilon B
ZnSO4 TRilon B
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

Nồng độ Trilon B là
CN = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

TN2. Xác định độ cứng nước máy

Nước máy Tiilon B
Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

Biểu diễn đô ̣ cứng chung của nước kèm theo ε0.95 (số mili đlg/L)
Độ cứng = ---------------------------------------------------------------------------------------------
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ε0.95 = ---------------------------------------------------------------------------------------------------
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μ = ------------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
TN3. Xác định hàm lượng Al3+

Zn2+ Al3+ Trilon B

Dụng cụ
σ
Lần 1
Lần 2
Lần 3
Trung bình
SV

Biểu diễn nồng độ của Al3+ (biết MAl = 26.98)

CN = ----------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------
ε0.95 = ---------------------------------------------------------------------------------------------------
-----------------------------------------------------------------------------------------------------------

μ = ------------------------------------------------------------------------------------------------------
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III. ĐÁNH GIÁ KẾT QUẢ
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IV. CÂU HỎI VÀ BÀI TẬP
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