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Definition of resilient

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FEDERAL AGENCY

FOR TECHNICAL REGULATION AND METROLOGY

NATIONAL
STANDARD
GOST R and s about
RUSSIAN 105-E03—
FEDERATIONS 2011

MATERIALS TEXTILE
Determination of color fastness
Part EOZ

Method for determination of color fastness


to the action of chlorinated water
(swimming pool water)
ISO 105-E03: 2010
Textiles - Tests for color fastness - Part E03: Color fastness to chlorinated
water (swimming-pool water)
(IDT)

Official edition

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Moscow
Standardinform
2012

copies of certificates

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GOST R ISO 105-E03-2011

Foreword

The goals and principles of standardization in the Russian Federation are established by the Federal Law of
December 27, 2002 No. 184-FZ "On technical regulation", and the rules for the application of national
standards of the Russian Federation - GOST R 1.0-2004 “Standardization in the Russian Federation.
Basic provisions "

Information about the standard

1 PREPARED by the Technical Committee TC 412 "Textile". Open joint stock


Society "All-Russian Scientific Research Institute of Certification" (JSC "VNIIS") on
based on our own authentic translation into Russian of the international standard specified in
paragraph 4

2 INTRODUCED by the Office of Technical Regulation and Standardization of the Federal Agency
on technical regulation and metrology

3 APPROVED AND PUT INTO EFFECT by the Order of the Federal Agency for Technical
regulation and metrology of December 6, 2011 No. 708-st

4 This standard is identical to the international standard ISO 105-E03: 2010 "Materials
textile. Determination of color fastness. Part of the EOZ. Method for determination of color fastness
to the action of chlorinated water (swimming pool water) "(ISO 105-E03: 2010" Textiles - Tests
for color fastness - Part E03: Color fastness to chlorinated water (swimming-pool water) ").
In the application of this International Standard, it is recommended to use instead of the reference international
native standards corresponding to them reference national standards of the Russian Federation,
details of which are given in the appendix YES

5 REPLACE GOST R ISO 105-E03-99

Information about changes to this standard is published in the annually published


information index "National Standards", and the text of changes and amendments - in the month
published information signs "National Standards". In case of revision
(replacement) or cancellation of this standard, a corresponding notice will be published
in the monthly published information index "National Standards". Compliant
information, notice and texts are also posted in the information system of the general
use - on the official website of the Federal Agency for Technical Regulation and
metrology on the Internet

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© Standartinform. 2012

This standard may not be reproduced, in whole or in part,, replicated or raced.


extended as an official publication without the permission of the Federal Agency for Technical
regulation and metrology

and

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GOST R ISO 105-E03-2011

Content

1 area of use............................................... .................................................. .........................................one

2 Regulatory references .......................................... .................................................. ............................................one

3 The essence of the method ............................................... .................................................. ...............................................one

4 Apparatus ................................................ .................................................. .................................................. ...... 2


5 Reagents ................................................ ............................ 2

6 Test piece .............................................. ........ 3

7 Test procedure ............................................... .................................................. ...................................... 3

8 Test report ............................................... .................................................. ......................................... 3

Appendix YES (informative) Compliance information with referenced International Standards


reference national standards of the Russian Federation ..................................... 4

Bibliography................................................. .................................................. .................................................. .five

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in

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4

GOST R ISO 105-E03-2011

NACIONALNYSTANDARTROSIJSKOJFEDERACI

MATERIALS TEXTILE

Determination of color fastness

Part EOZ

Method for determination of color fastness to chlorinated water


(swimming pool water)

Textiles. Tests for color fastness.


Part E03. Color fastness to chlorinated water (swimming-pool water)

Date of introduction - 2013—01—01

1 area of use

This International Standard specifies requirements for a method for determining color fastness.
stylish materials of all kinds to the action of active chlorine in the concentrations used for de
water infection in swimming pools (chlorination to a minimum residual
chlorine).
Three alternative test conditions apply. Concentration is active
chlorine 50 mg / l and 100 mg / l are used when testing materials for swimwear; concentration
active chlorine 20 mg / l - for testing the materials of swimwear, such as bathrobes
and towels.

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2 Normative references
This standard uses normative references to the following international
standards:
ISO 105-A01: 2010 Textiles. Tests for color fastness. Part A01. General principles
tests (ISO 105-A01: 2010. Textiles - Tests for color fastness - Part A01: General
principles of testing)
ISO 105-A02: 1993 Textiles. Tests for color fastness. Part A02. Gray scale for
color change assessments (ISO 105-A02: 1993, Textiles - Tests for color fastness - Part A02: Gray scale
for assessing change in color)
ISO 105-A05: 1996 Textiles. Tests for color fastness. Part A05. Instrumental
assessment of discoloration to determine grayscale points (ISO 105-A05; 1996. Textiles - Tests
for color fastness - Part A05: Instrumental assessment of change in color for determination of gray scale
rating)
ISO 3696: 1987 Water for laboratory analysis. Technical requirements and test methods
(ISO 3696: 1987, Water for analytical laboratory use - Specification and test methods)

3 The essence of the method

The test sample of the material is treated with a weak solution of chlorine of a given concentration,
and then dried. The color change of the sample is assessed using a gray scale or an instrument
tally. Three different test conditions are used.

Official edition

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GOST R ISO 105-E03-2011

4 Apparatus

4.1 Mechanical installation, consisting of a water bath in which horizontally placed


on the shaft are radially mounted containers made of glass or stainless steel with a diameter
(75 ± 5) mm. height (125 110) mm and capacity (550 ± 50) ml. Distance from the bottom of containers to
shaft - (45 1 10) mm. The shaft with containers rotates at a frequency of (40 ± 2) rpm. Water temperature
baths are controlled by a thermostat in such a way as to maintain the working temperature in the vessels
solution ± 2 ° C.
It is allowed to use other test installations providing similar results.
tats.
4.2 Instrument for measuring pH value with an accuracy of 0.02 units.
4.3 Gray scale for assessing discoloration in accordance with ISO 105-A02.
4.4 Spectrophotometer or colorimeter for assessing color changes as required
ISO 105-A05.
4.5 Analytical balance, to the nearest ± 0.01 g (see ISO 105-A01).

5 Reagents

5.1 An aqueous solution of sodium hypochlorite (NaOCI) of the following composition.


- active chlorine: from 140 g / l to 160 g / l;
- sodium chloride (NaCI): from 120 g / l to 170 g / l;
- sodium hydroxide (NaOH): max. 20 g / l;
- sodium carbonate (Na2C 0 3): maximum 20 g / l;
- iron (Fe): maximum 0.01 g / l.
All sodium hypochlorite solutions must be prepared immediately prior to testing.
niyami.
5.2 An aqueous solution of sodium hypochlorite, containing 100 mg / l of active chlorine, at

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pH = (7.50 ± 0.05).
Solutions are prepared with water of the 3rd class of purification (5.7) as follows:
- solution 1: add water to a volume of 1 l to 20.0 ml of sodium hypochlorite solution (5.1);
- solution 2: 14.35 g KH, P04 (5.5) per 1 liter;
- solution 3: 20.05 g Na2HP04-2H20 (5.6) per 1 l or 40.35 g # 2HPO4-12H2O (5.6) per 1 liter.
Next, to 25.0 ml of solution 1 add a solution of potassium iodide (KI) and hydrochloric acid (HCI), and release
The poured iodine is titrated with a sodium thiosulfate solution with (Na2S20 3) = 0.1 mol / L. As an indicator
use starch.
Let the volume of sodium thiosulfate required be equal to Y ml.
To prepare a working solution pH = (7.50 ± 0.05) take:
705X)
—— ml of solution 1,

100.0 ml of solution 2,
500.0 ml of solution 3,
add water to a volume of 1 liter.
Before use, you must check the pH value of the solution using a calibrated
pH measuring instrument (4.2).
If necessary, adjust the pH by adding either sodium hydroxide solution
s (NaOH) = 0.1 mol / L. or an acetic acid solution with (CH3COOH) = 0.1 mol / l.
5.3 Aqueous solution of sodium hypochlorite (NaOCI). containing 50 mg of active chlorine per 1 liter. at
pH = (7.50 1 0.05).
Follow a procedure similar to that described in 5.2, but for the preparation of each liter of working
th solution at pH = (7.50 i 0.05) take ml of solution 1.
2V
5.4 Aqueous solution of sodium hypochlorite (NaOCI). containing 20 mg of active chlorine per 1 liter, at
pH = (7.50 ± 0.05).
Follow a procedure similar to that described in 5.2, but for the preparation of each liter of working
th solution at pH = (7.50 ± 0.05) take ml of solution 1.

5.5 Potassium dihydrogen phosphate (KH2P 0 4).

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GOST R ISO 105-E03-2011

5.6 Dinatohydrogen phosphate dihydrate (Na2HP04 2H20) or dinatohydrogenphosphate-dodocagid-


rat (Na2HP04 ■ 12H..O).
5.7 Water of the 3rd class of purification according to ISO 3696.

6 Test piece

6.1 If the test sample is tissue, use a sample size


(40 ± 2) x (100 ± 2) mm.
6.2 If the test sample is a yarn, then a knitted fabric is knitted from it and
a sample measuring (40 ± 2) x (100 ♦ 2) mm is twisted or made from parallel strands of yarn with a length
(100 i 2) mm swab with a diameter of approximately (5 ± 2) mm. tying it up at both ends.
6.3 If the sample to be tested is loose fiber, then a sufficient quantity
comb and press in the form of a piece measuring (40 ± 2) x (100 ♦ 2) mm. Determine the mass of the fiber
and sew it onto a piece of polyester or polypropylene fabric that serves as a backing. When
When calculating the bath modulus (7.1), only the mass of the fibers is allowed

7 Test procedure

7.1 Each specimen is tested in a separate container of the machine (4.1). Immersed
Place the sample in a sodium hypochlorite solution (5.2.5.3 or 5.4) at a bath modulus of 100: 1. providing full
wetting the sample. Close the container and stir at 27 ° C ± 2 ° C in the dark for
for 1 hour.

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7.2 Remove the sample from the container, squeeze or centrifuge, and hang dry.
condition at room temperature in a darkened room.
7.3 Evaluate the change in color of each sample compared to the original sample by using
gray scale soup (4.3) and / or instrumental (4.4).

8 Test report

The test report must contain the following information:


a) a reference to this International Standard:
b) information needed to identify the test sample:
c) grayscale and / or instrumental assessment of the color change of each
sample;
d) active chlorine concentration (5.2,5.3.5.4);
e) any agreed or otherwise deviated from the established procedure.

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GOST R ISO 105-E03-2011

Appendix YES

(reference)

Conformity information with referenced International Standards


reference national standards of the Russian Federation

Table YES.1

Reference designation Power


Designation and title of the relevant national standard
international standard conformity

ISO 105-A01.2010 hut GOST R ISO 105-A01—99 “Textile materials. Define


improvement of color fastness. Part A01. General requirements for conducting
tests "

ISO 105-A02: 1993 hut GOST R ISO 105-A02—99 “Textile materials. Define
improvement of color fastness. Part A02. Gray scale for measuring change

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coloring "

ISO 105-A05: 1996 hut GOST R ISO 106-A05-99 “Textile materials. Define
improvement of color fastness. Part A05. Instrumental assessment method
color changes to determine gray scale points "

ISO 3696: 198 / hut •

* There is no corresponding national standard. Before it is approved, it is recommended to use


Russian translation of this International Standard. Translation of this international camp
dart is in the Federal Information Fund of Technical Regulations and Standards.

NOTE - In this table, the following symbol is used for the degree of correspondence
Consequences of standards:
- UT - identical standards.

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GOST R ISO 105-E03-2011

Bibliography

[1] ISO 105-J01 Textile. Tests for color fastness. Part J01. General measurement principles
surface painting

[2] ISO 105-J03 Textile. Tests for color fastness. Part J03. Method for calculating color differences
chiy

[3] ААТСС ТМ 162 Color fastness to water: chlorinated pools

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GOST R ISO 105-E03-2011

UDC 677.04.001.4:006.354 OKS 59.080.01 M09

Key words: method, samples, color fastness, aqueous solution, test report, chlorine
drawn water

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Editor U.V. Grigorieva

Technical editor V. N. Prusakova

Proofreader M.I. Pershina

Computer layout by I. Napeykina

Put in a set 26.09.2012 Signed to print on 25 10.2012. Format 60 * 8 4 ^ Lriap headset.

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